NC0006254_Groundwater Monitoring Report November 2020_20201123

PO Box 604 ▪ Fletcher, NC 28732 ▪ PH: 828-667-5001 ▪ Cell: 828-508-4510

November 23, 2020
Mr. Brett Laverty
NCDEQ Division of Water Resources
Asheville Regional Office
2090 US Highway 70
Swannanoa, NC 28778

RE: Groundwater Analytical Results – November 2020
Blue Ridge Tissue Corporation
1427 Yadkin River Road
Patterson, North Carolina

Mr. Laverty:

On November 9, 2020, Singleton Environmental, Inc. (SEI) visited the Blue Ridge Tissue site
located at 1427 Yadkin River Road in Patterson, North Carolina, to collect groundwater samples
from monitoring wells MW-1, MW-2, MW-3, MW-4, MW-6, MW-7 and MW-8. The depth to
groundwater in the monitoring wells ranged from 4.83 feet in MW-4 to 49.24 feet in MW-2.
Refer to Table 1 for all monitoring well groundwater depths and Figure 1 for all monitoring well
locations.

All groundwater samples, with the exception of MW-2, were collected using a peristaltic pump
connected to a Horiba U52-2 water quality meter with a flow through cell to collect groundwater
parameters (temperature, pH, specific conductivity, dissolved oxygen, ORP, and turbidity).
Groundwater sample MW-2 was collected using a bailer once three well volumes were removed.
Groundwater from the same bail as the sample was also poured into the flow cell to collect the
approximate parameters. The groundwater samples were submitted on ice to Pace Analytical for
the analysis of 8-RCRA Metals, pH, ammonia, TKN, sulfate, nitrogen, nitrite and nitrate. MW-2
was also analyzed for total dissolved solids (TDS) using EPA Method SM 2540C, and MW-4 was
also analyzed for volatile organic compounds (VOCs) using EPA Method 6200B. The
groundwater parameters for all samples are outlined in Table 2.

The laboratory analysis of groundwater samples MW-1 detected levels of iron and manganese
above the NCAC 2L groundwater standards. The laboratory analysis of MW-2 detected levels of
arsenic, barium, iron, manganese and ammonia above the NCAC 2L groundwater standards. The
laboratory analysis of groundwater samples MW-3 detected levels of iron, manganese and
ammonia above the NCAC 2L groundwater standards. The laboratory analysis of groundwater
samples MW-4 detected levels of iron and manganese above the NCAC 2L groundwater
standards. Laboratory analysis of groundwater samples MW-6, MW-7, and MW-8 did not detect
any compounds exceeding the NCAC 2L groundwater standards. The analytical results are shown
on attached Table 2 and the attached laboratory data sheets.

During the April 2017 groundwater sampling event, AECOM reported a possible sheen on the
groundwater in monitoring well MW-4. During the November 2020 event a sheen was not
Singleton Environmental, Inc.
Singleton Environmental, Inc.
observed; however, a VOC sample was collected and analyzed using EPA Method 6200B. None
of the concentrations were detected above the minimum laboratory detection levels.

The compound levels detected in the groundwater analysis for the November 2020 sampling event
were comparable to the March 2020 and July 2020 sampling events. Singleton Environmental,
Inc. recommends sampling the monitoring wells again in March 2021.

If you have any questions you can reach me at [phone].

Sincerely,

Chris Singleton, P.G.
Singleton Environmental, Inc.

cc: Dave Hallock, Blue Ridge Tissue Corporation

Attachments
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MW-2
MW-3
MW-4
MW-1
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MW-5
MW-7
MW-6
MW-8
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2
8
0
12601
3
2
0
1340
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1380
124014201240
1420
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/AirbusDS, USDA, USGS, AEX, Getmapping, Aerogrid, IGN, IGP, swisstopo, and theGIS User Community
Figure
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1
May 2017
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0 200 400Feet
1 inch = 200 feet
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Whisnant RdYad
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Yadkin
R
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Roby Martin Rd#0
Site Layout MapBlue Ridge Tissue CorporationPatterson, North Carolina
Legend
Property Boundary
Yadkin River Flow Direction
#Land Surface Elevation Contour (ft above mean sea level)
Monitoring Well Location
Abandoned Water Well#0@A
Well ID Date Installed Total Depth (feet
bls)
Screened Interval
(feet bls)
Top of Casing
Elevation (feet msl)
Date Water Level
Measured
Depth to Water (feet
BTOC)
Groundwater Elevation
(feet msl)
MW-1 02/08/11 11 6-11 1253.71 11/09/20 11.80 1,241.91
MW-2 08/12/09 50 40-50 1323.03 11/09/20 49.24 1,273.79
MW-3 08/13/09 20 10-20 1299.02 11/09/20 16.15 1,282.87
MW-4 08/13/09 15 5-15 1247.23 11/09/20 4.83 1,242.40
MW-5 08/16/11 21 11-21 1285.46 N/A N/A N/A
MW-6 08/06/14 29 19-29 1341.55 11/09/20 27.00 1,314.55
MW-7 08/06/14 24 14-24 1274.41 11/09/20 6.80 1,267.61
MW-8 08/06/14 20 10-20 1253.14 11/09/20 13.50 1,239.64
Notes:
bls - feet below land surface BTOC - below top of casing msl - above mean sea level NG - not gauged
AECOM
Table 1
Monitoring Well Construction and Groundwater Elevations
Blue Ridge Tissue Corporation
1427 Yadkin River Road
Patterson, North Carolina
Sample ID MW-1 MW-2*MW-3 MW-4 MW-6 MW-7 MW-8
Sample Date 11/09/20 11/09/20 11/09/20 11/09/20 11/09/20 11/09/20 11/09/20
Temperature (°C)NS 19.8 N/A 22.90 23.80 19.24 23.70 25.30
pH (standard units)NS 6.37 N/A 6.32 6.30 5.04 5.98 6.85
Specific Conductivity (mS/cm)NS 0.515 N/A 0.533 0.228 0.02 0.083 0.108
Dissolved Oxygen (mg/L)NS 2.27 N/A 1.32 1.38 7.39 6.92 5.66
ORP (mV)NS -23.0 N/A -38.0 3.0 218.0 204.0 19.0
Turbidity (NTU)NS 6 N/A 7.5 2.5 2 1.5 4.5
Gallons Pumped NS 2.5 2.00 3 2 2 1.75 2.5
Total Barium (ug/L)700 374 1,800 260 83 84.2 57.4 16.4
Total Iron (ug/L)300 28,600 70,500 29,800 11,700 ND 229 ND
Total Manganese (ug/L)50 5,750 669 3,100 1,340 20.5 5.6 ND
Aresenic (ug/L)10 ND 14.9 ND ND ND ND ND
Chromium (ug/L)10 ND 7.1 ND ND ND ND ND
Lead (ug/L)15 ND ND ND ND ND ND ND
Sulfate N/A ND 1.4 19.5 2.3 ND 1.9 22.3
Amonia (mg/L)1.5 0.54 13.7 15.7 0.79 ND ND ND
TKN (mg/L)N/A 0.77 13.3 14.4 0.97 ND ND ND
Nitrogen NO2 plus NO3 (mg/L)N/A 0.14 0.047 0.22 ND ND 1.2 3.3
Nitrate (mg/L)10.0 0.14 ND 0.18 ND ND 1.2 3.3
Nitrite (mg/L)1.0 ND 0.068 0.044 ND ND ND ND
pH (standard units)N/A 6.6 6.6 6.5 6.5 5.3 6.3 6.1
Total Disolved Solids (mg/L)N/A N/A 340 N/A N/A N/A N/A N/A
EPA Method 6200B for VOCs N/A N/A N/A N/A ND N/A N/A N/A
Notes:
Samples analyzed for total and dissolved iron, barium and manganese by EPA Method 200.7
2L Standard - North Carolina groundwater quality standards established in Title 15A of the North Carolina Administrative Code, Subchapter 2L, Section 0.20
°C - degrees Celsius
µS/cm - microsiemens per centimeter
EPA - United States Environmental Protection Agency mg/L - milligrams per liter
mV - millivolt
NA - Not analyzed NS - No standard
NTU - Nephelometric Turbidity Unit
RCRA - Resource Conservation Recovery Act
Bold samples indicate concentrations above the 2L Standard
*MW-2 purged with disposable bailer, water quality parameters collected from same bail as sample.
2L
Standard
Field Parameters
Analytical Parameters
Table 2
Blue Ridge Tissue Corporation
1427 Yadkin River Road
Patterson, North Carolina
#=CL#
November 17, 2020
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92504779
92504779
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
P.O. Box 2012
Enka, NC 28728
Blue Ridge Tissue Corp 11/9/20
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on November 09, 2020. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen for
[e-mail]
Project Manager
Lorri Patton
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 33
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 33
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92504779001 MW-1 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
SM 4500-H+B-2011 1 PASI-ASMK
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ACJL
92504779002 MW-2 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
SM 2540C-2011 1 PASI-AALP
SM 4500-H+B-2011 1 PASI-ASMK
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ACJL
92504779003 MW-3 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
SM 4500-H+B-2011 1 PASI-ASMK
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ACJL
92504779004 MW-4 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
SM 6200B 63 PASI-CSAS
SM 4500-H+B-2011 1 PASI-ASMK
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ACJL
92504779005 MW-6 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
SM 4500-H+B-2011 1 PASI-ASMK
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ACJL
92504779006 MW-7 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
SM 4500-H+B-2011 1 PASI-ASMK
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 33
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 353.2 Rev 2.0 1993 3 PASI-ACJL
92504779007 MW-8 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1
SM 4500-H+B-2011 1 PASI-ASMK
EPA 300.0 Rev 2.1 1993 1 PASI-ACDC
EPA 350.1 Rev 2.0 1993 1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ACJL
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Sample:MW-1 Lab ID:92504779001 Collected:11/09/20 10:40 Received:11/09/20 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 11/10/20 10:12 7440-38-2 BC11/10/20 02:0010.0 1
Barium 374 ug/L 11/10/20 10:12 7440-39-311/10/20 02:005.0 1
Chromium ND ug/L 11/10/20 10:12 7440-47-311/10/20 02:005.0 1
Iron 28600 ug/L 11/10/20 10:12 7439-89-611/10/20 02:0050.0 1
Lead ND ug/L 11/10/20 10:12 7439-92-111/10/20 02:005.0 1
Manganese 5750 ug/L 11/10/20 10:12 7439-96-511/10/20 02:005.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 6.6 Std. Units 11/15/20 12:32 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate ND mg/L 11/10/20 18:20 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 0.54 mg/L 11/12/20 12:59 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 0.77 mg/L 11/12/20 05:50 7727-37-911/11/20 04:100.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 0.14 mg/L 11/11/20 00:15 M10.040 1
Nitrogen, Nitrate 0.14 mg/L 11/11/20 00:15 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 11/11/20 00:15 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Sample:MW-2 Lab ID:92504779002 Collected:11/09/20 11:00 Received:11/09/20 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic 14.9 ug/L 11/10/20 10:16 7440-38-2 BC11/10/20 02:0010.0 1
Barium 1800 ug/L 11/10/20 10:16 7440-39-311/10/20 02:005.0 1
Chromium 7.1 ug/L 11/10/20 10:16 7440-47-311/10/20 02:005.0 1
Iron 70500 ug/L 11/10/20 10:16 7439-89-611/10/20 02:0050.0 1
Lead ND ug/L 11/10/20 10:16 7439-92-111/10/20 02:005.0 1
Manganese 669 ug/L 11/10/20 10:16 7439-96-511/10/20 02:005.0 1
Analytical Method: SM 2540C-2011
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 340 mg/L 11/13/20 12:1225.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 6.6 Std. Units 11/15/20 12:38 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 1.4 mg/L 11/10/20 18:35 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 13.7 mg/L 11/12/20 13:03 7664-41-70.30 3
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 13.3 mg/L 11/12/20 05:51 7727-37-911/11/20 04:100.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 0.047 mg/L 11/11/20 00:18 M10.040 1
Nitrogen, Nitrate ND mg/L 11/11/20 00:18 14797-55-80.040 1
Nitrogen, Nitrite 0.068 mg/L 11/11/20 00:18 14797-65-0 M10.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Sample:MW-3 Lab ID:92504779003 Collected:11/09/20 11:20 Received:11/09/20 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 11/10/20 10:19 7440-38-2 BC11/10/20 02:0010.0 1
Barium 260 ug/L 11/10/20 10:19 7440-39-311/10/20 02:005.0 1
Chromium ND ug/L 11/10/20 10:19 7440-47-311/10/20 02:005.0 1
Iron 29800 ug/L 11/10/20 10:19 7439-89-611/10/20 02:0050.0 1
Lead ND ug/L 11/10/20 10:19 7439-92-111/10/20 02:005.0 1
Manganese 3100 ug/L 11/10/20 10:19 7439-96-511/10/20 02:005.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 6.5 Std. Units 11/15/20 12:44 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 19.5 mg/L 11/10/20 18:49 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 15.7 mg/L 11/12/20 13:04 7664-41-70.30 3
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 14.4 mg/L 11/12/20 06:02 7727-37-911/11/20 22:260.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 0.22 mg/L 11/11/20 00:210.040 1
Nitrogen, Nitrate 0.18 mg/L 11/11/20 00:21 14797-55-80.040 1
Nitrogen, Nitrite 0.044 mg/L 11/11/20 00:21 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Sample:MW-4 Lab ID:92504779004 Collected:11/09/20 13:15 Received:11/09/20 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 11/10/20 10:23 7440-38-2 BC11/10/20 02:0010.0 1
Barium 82.5 ug/L 11/10/20 10:23 7440-39-311/10/20 02:005.0 1
Chromium ND ug/L 11/10/20 10:23 7440-47-311/10/20 02:005.0 1
Iron 11700 ug/L 11/10/20 10:23 7439-89-611/10/20 02:0050.0 1
Lead ND ug/L 11/10/20 10:23 7439-92-111/10/20 02:005.0 1
Manganese 1340 ug/L 11/10/20 10:23 7439-96-511/10/20 02:005.0 1
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/11/20 19:25 71-43-20.50 1
Bromobenzene ND ug/L 11/11/20 19:25 108-86-10.50 1
Bromochloromethane ND ug/L 11/11/20 19:25 74-97-50.50 1
Bromodichloromethane ND ug/L 11/11/20 19:25 75-27-40.50 1
Bromoform ND ug/L 11/11/20 19:25 75-25-20.50 1
Bromomethane ND ug/L 11/11/20 19:25 74-83-95.0 1
n-Butylbenzene ND ug/L 11/11/20 19:25 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/11/20 19:25 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/11/20 19:25 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/11/20 19:25 56-23-50.50 1
Chlorobenzene ND ug/L 11/11/20 19:25 108-90-70.50 1
Chloroethane ND ug/L 11/11/20 19:25 75-00-31.0 1
Chloroform ND ug/L 11/11/20 19:25 67-66-30.50 1
Chloromethane ND ug/L 11/11/20 19:25 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/11/20 19:25 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/11/20 19:25 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/11/20 19:25 96-12-81.0 1
Dibromochloromethane ND ug/L 11/11/20 19:25 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/11/20 19:25 106-93-40.50 1
Dibromomethane ND ug/L 11/11/20 19:25 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/11/20 19:25 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/11/20 19:25 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/11/20 19:25 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/11/20 19:25 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/11/20 19:25 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/11/20 19:25 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/11/20 19:25 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/11/20 19:25 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/11/20 19:25 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/11/20 19:25 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/11/20 19:25 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/11/20 19:25 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/11/20 19:25 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/11/20 19:25 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/11/20 19:25 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/11/20 19:25 108-20-30.50 1
Ethylbenzene ND ug/L 11/11/20 19:25 100-41-40.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
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Page 8 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Sample:MW-4 Lab ID:92504779004 Collected:11/09/20 13:15 Received:11/09/20 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Hexachloro-1,3-butadiene ND ug/L 11/11/20 19:25 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/11/20 19:25 98-82-80.50 1
Methylene Chloride ND ug/L 11/11/20 19:25 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/11/20 19:25 1634-04-40.50 1
Naphthalene ND ug/L 11/11/20 19:25 91-20-32.0 1
n-Propylbenzene ND ug/L 11/11/20 19:25 103-65-10.50 1
Styrene ND ug/L 11/11/20 19:25 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/11/20 19:25 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/11/20 19:25 79-34-50.50 1
Tetrachloroethene ND ug/L 11/11/20 19:25 127-18-40.50 1
Toluene ND ug/L 11/11/20 19:25 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/11/20 19:25 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/11/20 19:25 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/11/20 19:25 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/11/20 19:25 79-00-50.50 1
Trichloroethene ND ug/L 11/11/20 19:25 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/11/20 19:25 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/11/20 19:25 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/11/20 19:25 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/11/20 19:25 108-67-80.50 1
Vinyl chloride ND ug/L 11/11/20 19:25 75-01-41.0 1
m&p-Xylene ND ug/L 11/11/20 19:25 179601-23-11.0 1
o-Xylene ND ug/L 11/11/20 19:25 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %11/11/20 19:25 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %11/11/20 19:25 460-00-470-130 1
Toluene-d8 (S)101 %11/11/20 19:25 2037-26-570-130 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 6.5 Std. Units 11/15/20 13:07 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 2.3 mg/L 11/10/20 19:03 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 0.79 mg/L 11/12/20 13:06 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 0.97 mg/L 11/12/20 06:03 7727-37-911/11/20 22:260.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
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Page 9 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Sample:MW-4 Lab ID:92504779004 Collected:11/09/20 13:15 Received:11/09/20 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 ND mg/L 11/11/20 00:230.040 1
Nitrogen, Nitrate ND mg/L 11/11/20 00:23 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 11/11/20 00:23 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
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Asheville, NC 28804
[phone]
Page 10 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Sample:MW-6 Lab ID:92504779005 Collected:11/09/20 12:20 Received:11/09/20 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 11/10/20 10:27 7440-38-2 BC11/10/20 02:0010.0 1
Barium 84.2 ug/L 11/10/20 10:27 7440-39-311/10/20 02:005.0 1
Chromium ND ug/L 11/10/20 10:27 7440-47-311/10/20 02:005.0 1
Iron ND ug/L 11/10/20 10:27 7439-89-611/10/20 02:0050.0 1
Lead ND ug/L 11/10/20 10:27 7439-92-111/10/20 02:005.0 1
Manganese 20.5 ug/L 11/10/20 10:27 7439-96-511/10/20 02:005.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 5.3 Std. Units 11/15/20 12:55 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate ND mg/L 11/10/20 19:18 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 11/12/20 13:07 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 11/12/20 06:04 7727-37-911/11/20 22:260.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 ND mg/L 11/11/20 00:260.040 1
Nitrogen, Nitrate ND mg/L 11/11/20 00:26 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 11/11/20 00:26 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
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Page 11 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Sample:MW-7 Lab ID:92504779006 Collected:11/09/20 12:45 Received:11/09/20 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 11/10/20 10:30 7440-38-2 BC11/10/20 02:0010.0 1
Barium 57.4 ug/L 11/10/20 10:30 7440-39-311/10/20 02:005.0 1
Chromium ND ug/L 11/10/20 10:30 7440-47-311/10/20 02:005.0 1
Iron 229 ug/L 11/10/20 10:30 7439-89-611/10/20 02:0050.0 1
Lead ND ug/L 11/10/20 10:30 7439-92-111/10/20 02:005.0 1
Manganese 5.6 ug/L 11/10/20 10:30 7439-96-511/10/20 02:005.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 6.3 Std. Units 11/15/20 13:01 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 1.9 mg/L 11/10/20 19:32 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 11/12/20 13:09 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 11/12/20 06:06 7727-37-911/11/20 22:260.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 1.2 mg/L 11/11/20 00:270.040 1
Nitrogen, Nitrate 1.2 mg/L 11/11/20 00:27 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 11/11/20 00:27 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Sample:MW-8 Lab ID:92504779007 Collected:11/09/20 11:50 Received:11/09/20 14:40 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 11/10/20 10:34 7440-38-2 BC11/10/20 02:0010.0 1
Barium 16.4 ug/L 11/10/20 10:34 7440-39-311/10/20 02:005.0 1
Chromium ND ug/L 11/10/20 10:34 7440-47-311/10/20 02:005.0 1
Iron ND ug/L 11/10/20 10:34 7439-89-611/10/20 02:0050.0 1
Lead ND ug/L 11/10/20 10:34 7439-92-111/10/20 02:005.0 1
Manganese ND ug/L 11/10/20 10:34 7439-96-511/10/20 02:005.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 6.1 Std. Units 11/15/20 12:50 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 22.3 mg/L 11/11/20 12:55 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 11/12/20 13:10 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 11/12/20 06:07 7727-37-911/11/20 22:260.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 3.3 mg/L 11/11/20 00:280.040 1
Nitrogen, Nitrate 3.3 mg/L 11/11/20 00:28 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 11/11/20 00:28 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
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Asheville, NC 28804
[phone]
Page 13 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
579083
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
200.7 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92504779001, 92504779002, 92504779003, 92504779004, 92504779005, 92504779006, 92504779007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3063673
Associated Lab Samples:92504779001, 92504779002, 92504779003, 92504779004, 92504779005, 92504779006, 92504779007
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 BC11/10/20 08:57
Barium ug/L ND 5.0 11/10/20 08:57
Chromium ug/L ND 5.0 11/10/20 08:57
Iron ug/L ND 50.0 11/10/20 08:57
Lead ug/L ND 5.0 11/10/20 08:57
Manganese ug/L ND 5.0 11/10/20 08:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3063674LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 540500 108 85-115
Barium ug/L 493500 99 85-115
Chromium ug/L 481500 96 85-115
Iron ug/L 52005000 104 85-115
Lead ug/L 528500 106 85-115
Manganese ug/L 494500 99 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3063675MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92503683001
3063676
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 110 70-130106 3500ND548531
Barium ug/L 500 101 70-130100 150035.8 541 537
Chromium ug/L 500 102 70-130102 0500ND513512
Iron ug/L 5000 106 70-130105 15000125065506510
Lead ug/L 500 105 70-130104 1500ND527522
Manganese ug/L 500 102 70-130101 050062.5 570 568
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3063677MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92503546017
3063678
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 111 70-130113 1500ND558565
Barium ug/L 500 103 70-130105 250020.9 535 547
Chromium ug/L 500 99 70-130103 350014.0 511 528
Iron ug/L 5000 100 70-130103 3500054355205690
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
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Asheville, NC 28804
[phone]
Page 14 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3063677MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92503546017
3063678
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead ug/L 500 103 70-130105 2500ND514523
Manganese ug/L 500 98 70-130101 3500ND495510
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
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Asheville, NC 28804
[phone]
Page 15 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
579554
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92504779004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3065946
Associated Lab Samples:92504779004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/11/20 11:22
1,1,1-Trichloroethane ug/L ND 0.50 11/11/20 11:22
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/11/20 11:22
1,1,2-Trichloroethane ug/L ND 0.50 11/11/20 11:22
1,1-Dichloroethane ug/L ND 0.50 11/11/20 11:22
1,1-Dichloroethene ug/L ND 0.50 11/11/20 11:22
1,1-Dichloropropene ug/L ND 0.50 11/11/20 11:22
1,2,3-Trichlorobenzene ug/L ND 2.0 11/11/20 11:22
1,2,3-Trichloropropane ug/L ND 0.50 11/11/20 11:22
1,2,4-Trichlorobenzene ug/L ND 2.0 11/11/20 11:22
1,2,4-Trimethylbenzene ug/L ND 0.50 11/11/20 11:22
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/11/20 11:22
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/11/20 11:22
1,2-Dichlorobenzene ug/L ND 0.50 11/11/20 11:22
1,2-Dichloroethane ug/L ND 0.50 11/11/20 11:22
1,2-Dichloropropane ug/L ND 0.50 11/11/20 11:22
1,3,5-Trimethylbenzene ug/L ND 0.50 11/11/20 11:22
1,3-Dichlorobenzene ug/L ND 0.50 11/11/20 11:22
1,3-Dichloropropane ug/L ND 0.50 11/11/20 11:22
1,4-Dichlorobenzene ug/L ND 0.50 11/11/20 11:22
2,2-Dichloropropane ug/L ND 0.50 11/11/20 11:22
2-Chlorotoluene ug/L ND 0.50 11/11/20 11:22
4-Chlorotoluene ug/L ND 0.50 11/11/20 11:22
Benzene ug/L ND 0.50 11/11/20 11:22
Bromobenzene ug/L ND 0.50 11/11/20 11:22
Bromochloromethane ug/L ND 0.50 11/11/20 11:22
Bromodichloromethane ug/L ND 0.50 11/11/20 11:22
Bromoform ug/L ND 0.50 11/11/20 11:22
Bromomethane ug/L ND 5.0 11/11/20 11:22
Carbon tetrachloride ug/L ND 0.50 11/11/20 11:22
Chlorobenzene ug/L ND 0.50 11/11/20 11:22
Chloroethane ug/L ND 1.0 11/11/20 11:22
Chloroform ug/L ND 0.50 11/11/20 11:22
Chloromethane ug/L ND 1.0 11/11/20 11:22
cis-1,2-Dichloroethene ug/L ND 0.50 11/11/20 11:22
cis-1,3-Dichloropropene ug/L ND 0.50 11/11/20 11:22
Dibromochloromethane ug/L ND 0.50 11/11/20 11:22
Dibromomethane ug/L ND 0.50 11/11/20 11:22
Dichlorodifluoromethane ug/L ND 0.50 11/11/20 11:22
Diisopropyl ether ug/L ND 0.50 11/11/20 11:22
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
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Page 16 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3065946
Associated Lab Samples:92504779004
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 11/11/20 11:22
Hexachloro-1,3-butadiene ug/L ND 2.0 11/11/20 11:22
Isopropylbenzene (Cumene)ug/L ND 0.50 11/11/20 11:22
m&p-Xylene ug/L ND 1.0 11/11/20 11:22
Methyl-tert-butyl ether ug/L ND 0.50 11/11/20 11:22
Methylene Chloride ug/L ND 2.0 11/11/20 11:22
n-Butylbenzene ug/L ND 0.50 11/11/20 11:22
n-Propylbenzene ug/L ND 0.50 11/11/20 11:22
Naphthalene ug/L ND 2.0 11/11/20 11:22
o-Xylene ug/L ND 0.50 11/11/20 11:22
sec-Butylbenzene ug/L ND 0.50 11/11/20 11:22
Styrene ug/L ND 0.50 11/11/20 11:22
tert-Butylbenzene ug/L ND 0.50 11/11/20 11:22
Tetrachloroethene ug/L ND 0.50 11/11/20 11:22
Toluene ug/L ND 0.50 11/11/20 11:22
trans-1,2-Dichloroethene ug/L ND 0.50 11/11/20 11:22
trans-1,3-Dichloropropene ug/L ND 0.50 11/11/20 11:22
Trichloroethene ug/L ND 0.50 11/11/20 11:22
Trichlorofluoromethane ug/L ND 1.0 11/11/20 11:22
Vinyl chloride ug/L ND 1.0 11/11/20 11:22
1,2-Dichloroethane-d4 (S)%96 70-130 11/11/20 11:22
4-Bromofluorobenzene (S)%96 70-130 11/11/20 11:22
Toluene-d8 (S)%101 70-130 11/11/20 11:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3065947LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.250 104 60-140
1,1,1-Trichloroethane ug/L 49.850 100 60-140
1,1,2,2-Tetrachloroethane ug/L 47.550 95 60-140
1,1,2-Trichloroethane ug/L 49.550 99 60-140
1,1-Dichloroethane ug/L 48.850 98 60-140
1,1-Dichloroethene ug/L 53.150 106 60-140
1,1-Dichloropropene ug/L 50.550 101 60-140
1,2,3-Trichlorobenzene ug/L 50.550 101 60-140
1,2,3-Trichloropropane ug/L 47.950 96 60-140
1,2,4-Trichlorobenzene ug/L 54.850 110 60-140
1,2,4-Trimethylbenzene ug/L 51.050 102 60-140
1,2-Dibromo-3-chloropropane ug/L 50.150 100 60-140
1,2-Dibromoethane (EDB)ug/L 50.950 102 60-140
1,2-Dichlorobenzene ug/L 51.750 103 60-140
1,2-Dichloroethane ug/L 43.450 87 60-140
1,2-Dichloropropane ug/L 51.350 103 60-140
1,3,5-Trimethylbenzene ug/L 52.050 104 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3065947LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 53.250 106 60-140
1,3-Dichloropropane ug/L 51.150 102 60-140
1,4-Dichlorobenzene ug/L 52.250 104 60-140
2,2-Dichloropropane ug/L 51.250 102 60-140
2-Chlorotoluene ug/L 52.450 105 60-140
4-Chlorotoluene ug/L 51.050 102 60-140
Benzene ug/L 50.250 100 60-140
Bromobenzene ug/L 49.850 100 60-140
Bromochloromethane ug/L 47.850 96 60-140
Bromodichloromethane ug/L 49.450 99 60-140
Bromoform ug/L 48.750 97 60-140
Bromomethane ug/L 58.050 116 60-140
Carbon tetrachloride ug/L 50.050 100 60-140
Chlorobenzene ug/L 50.850 102 60-140
Chloroethane ug/L 40.950 82 60-140
Chloroform ug/L 48.950 98 60-140
Chloromethane ug/L 43.750 87 60-140
cis-1,2-Dichloroethene ug/L 47.650 95 60-140
cis-1,3-Dichloropropene ug/L 52.150 104 60-140
Dibromochloromethane ug/L 53.450 107 60-140
Dibromomethane ug/L 52.150 104 60-140
Dichlorodifluoromethane ug/L 44.750 89 60-140
Diisopropyl ether ug/L 46.550 93 60-140
Ethylbenzene ug/L 50.350 101 60-140
Hexachloro-1,3-butadiene ug/L 51.350 103 60-140
Isopropylbenzene (Cumene)ug/L 53.550 107 60-140
m&p-Xylene ug/L 102100 102 60-140
Methyl-tert-butyl ether ug/L 47.250 94 60-140
Methylene Chloride ug/L 45.550 91 60-140
n-Butylbenzene ug/L 53.850 108 60-140
n-Propylbenzene ug/L 52.150 104 60-140
Naphthalene ug/L 52.250 104 60-140
o-Xylene ug/L 51.950 104 60-140
sec-Butylbenzene ug/L 52.550 105 60-140
Styrene ug/L 52.750 105 60-140
tert-Butylbenzene ug/L 44.850 90 60-140
Tetrachloroethene ug/L 51.350 103 60-140
Toluene ug/L 50.450 101 60-140
trans-1,2-Dichloroethene ug/L 50.050 100 60-140
trans-1,3-Dichloropropene ug/L 50.950 102 60-140
Trichloroethene ug/L 51.650 103 60-140
Trichlorofluoromethane ug/L 43.150 86 60-140
Vinyl chloride ug/L 44.250 88 60-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3065948MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92504666003
3065949
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 104 60-140107 320ND20.7 21.3
1,1,1-Trichloroethane ug/L 20 91 60-14097 620ND18.3 19.3
1,1,2,2-Tetrachloroethane ug/L 20 98 60-140102 420ND19.6 20.4
1,1,2-Trichloroethane ug/L 20 95 60-140100 520ND19.1 20.0
1,1-Dichloroethane ug/L 20 88 60-14090 220ND17.7 18.0
1,1-Dichloroethene ug/L 20 94 60-14097 420ND18.8 19.5
1,1-Dichloropropene ug/L 20 89 60-14093 420ND17.9 18.6
1,2,3-Trichlorobenzene ug/L 20 114 60-140110 420ND22.9 22.0
1,2,3-Trichloropropane ug/L 20 99 60-140102 320ND19.8 20.4
1,2,4-Trichlorobenzene ug/L 20 116 60-140112 420ND23.1 22.3
1,2,4-Trimethylbenzene ug/L 20 104 60-140105 1200.96 21.8 22.0
1,2-Dibromo-3-chloropropane ug/L 20 102 60-140108 520ND20.5 21.6
1,2-Dibromoethane (EDB)ug/L 20 100 60-140105 420ND20.1 20.9
1,2-Dichlorobenzene ug/L 20 106 60-140106 020ND21.2 21.2
1,2-Dichloroethane ug/L 20 81 60-14086 620ND16.2 17.2
1,2-Dichloropropane ug/L 20 96 60-140102 720ND19.1 20.5
1,3,5-Trimethylbenzene ug/L 20 109 60-140110 120ND22.2 22.3
1,3-Dichlorobenzene ug/L 20 107 60-140108 120ND21.5 21.6
1,3-Dichloropropane ug/L 20 99 60-140106 720ND19.9 21.3
1,4-Dichlorobenzene ug/L 20 106 60-140108 220ND21.2 21.5
2,2-Dichloropropane ug/L 20 93 60-14097 420ND18.5 19.4
2-Chlorotoluene ug/L 20 107 60-140109 220ND21.4 21.8
4-Chlorotoluene ug/L 20 105 60-140105 020ND21.0 21.1
Benzene ug/L 20 91 60-14097 620ND18.3 19.3
Bromobenzene ug/L 20 105 60-140107 220ND21.0 21.3
Bromochloromethane ug/L 20 87 60-14092 520ND17.4 18.4
Bromodichloromethane ug/L 20 95 60-14099 520ND18.9 19.9
Bromoform ug/L 20 94 60-14098 420ND18.8 19.6
Bromomethane ug/L 20 97 60-14097 120ND19.4 19.3
Carbon tetrachloride ug/L 20 93 60-140100 720ND18.7 20.1
Chlorobenzene ug/L 20 104 60-140106 220ND20.8 21.2
Chloroethane ug/L 20 78 60-14080 220ND15.7 16.0
Chloroform ug/L 20 93 60-14098 5200.59 19.2 20.2
Chloromethane ug/L 20 71 60-14074 320ND14.3 14.7
cis-1,2-Dichloroethene ug/L 20 86 60-14091 520ND17.3 18.2
cis-1,3-Dichloropropene ug/L 20 98 60-140104 520ND19.7 20.8
Dibromochloromethane ug/L 20 103 60-140107 420ND20.6 21.5
Dibromomethane ug/L 20 101 60-140105 420ND20.2 21.1
Dichlorodifluoromethane ug/L 20 75 60-14080 620ND15.0 16.0
Diisopropyl ether ug/L 20 84 60-14088 520ND16.8 17.6
Ethylbenzene ug/L 20 102 60-140105 320ND20.4 21.1
Hexachloro-1,3-butadiene ug/L 20 118 60-140110 720ND23.5 22.0
Isopropylbenzene (Cumene)ug/L 20 110 60-140116 520ND22.1 23.1
m&p-Xylene ug/L 40 103 60-140107 440ND41.3 42.8
Methyl-tert-butyl ether ug/L 20 83 60-14087 620ND16.5 17.5
Methylene Chloride ug/L 20 79 60-14083 520ND15.9 16.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3065948MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92504666003
3065949
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 115 60-140113 120ND22.9 22.6
n-Propylbenzene ug/L 20 111 60-140112 120ND22.1 22.3
Naphthalene ug/L 20 105 60-140102 3202.2 23.2 22.5
o-Xylene ug/L 20 104 60-140108 420ND20.8 21.7
sec-Butylbenzene ug/L 20 113 60-140113 020ND22.6 22.7
Styrene ug/L 20 103 60-140106 320ND20.6 21.3
tert-Butylbenzene ug/L 20 97 60-14097 020ND19.4 19.4
Tetrachloroethene ug/L 20 105 60-140107 320ND21.0 21.5
Toluene ug/L 20 96 60-140102 620ND19.2 20.4
trans-1,2-Dichloroethene ug/L 20 87 60-14093 720ND17.4 18.7
trans-1,3-Dichloropropene ug/L 20 97 60-140102 520ND19.4 20.4
Trichloroethene ug/L 20 99 60-140103 420ND19.8 20.7
Trichlorofluoromethane ug/L 20 80 60-14085 620ND16.0 17.0
Vinyl chloride ug/L 20 73 60-14077 520ND14.5 15.3
1,2-Dichloroethane-d4 (S)%96 70-13099
4-Bromofluorobenzene (S)%98 70-13099
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
580169
SM 2540C-2011
SM 2540C-2011
2540C Total Dissolved Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92504779002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3068935
Associated Lab Samples:92504779002
Matrix:Water
Analyzed
Total Dissolved Solids mg/L ND 25.0 11/13/20 12:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3068936LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids mg/L 254250 102 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92504779002
3068937SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 353 4340
Parameter Units
Dup
Result QualifiersRPDResult
92504856011
3068938SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 834 1842
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
580427
SM 4500-H+B-2011
SM 4500-H+B-2011
4500H+B pH
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92504779001, 92504779002, 92504779003, 92504779004, 92504779005, 92504779006, 92504779007
Parameter Units
Dup
Result QualifiersRPDResult
92503755023
3070418SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 7.6 H317.7
Parameter Units
Dup
Result QualifiersRPDResult
92505707001
3070419SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 5.8 D6,H386.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 22 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
579131
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92504779001, 92504779002, 92504779003, 92504779004, 92504779005, 92504779006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3063770
Associated Lab Samples:92504779001, 92504779002, 92504779003, 92504779004, 92504779005, 92504779006
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 11/10/20 12:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3063771LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 49.550 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3063772MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92504677001
3063773
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L M15011190-110112 0509.9 65.6 65.8
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3063774MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92504705003
3063775
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 110 90-110110 0502.6 57.6 57.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 23 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
579438
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92504779007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3065396
Associated Lab Samples:92504779007
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 11/11/20 12:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3065397LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 48.650 97 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3065398MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92504779007
3065399
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 102 90-110104 15022.3 73.3 74.2
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3065400MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92504668005
3065401
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L 50 102 90-110105 2509.0 59.9 61.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 24 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
579814
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
350.1 Ammonia
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92504779001, 92504779002, 92504779003, 92504779004, 92504779005, 92504779006, 92504779007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3067171
Associated Lab Samples:92504779001, 92504779002, 92504779003, 92504779004, 92504779005, 92504779006, 92504779007
Matrix:Water
Analyzed
Nitrogen, Ammonia mg/L ND 0.10 11/12/20 12:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3067172LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/L 5.05 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3067173MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92504340001
3067174
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L M6514290-110158 1587.0 94.1 94.8
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3067175MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92503316005
3067176
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 93 90-11093 05ND4.7 4.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 25 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
579435
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92504779001, 92504779002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3065381
Associated Lab Samples:92504779001, 92504779002
Matrix:Water
Analyzed
Nitrogen, Kjeldahl, Total mg/L ND 0.50 11/12/20 05:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3065382LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/L 9.810 98 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3065383MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92503354005
3065384
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L M1108290-11088 6102.0 10.2 10.8
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3065385MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92503879001
3065386
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L M11011090-110114 21011.0 22.1 22.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 26 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
579439
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92504779003, 92504779004, 92504779005, 92504779006, 92504779007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3065402
Associated Lab Samples:92504779003, 92504779004, 92504779005, 92504779006, 92504779007
Matrix:Water
Analyzed
Nitrogen, Kjeldahl, Total mg/L ND 0.50 11/12/20 05:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3065403LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/L 9.410 94 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3065404MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92503429001
3065405
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L 10 99 90-11096 310ND10.3 10.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 27 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
579361
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite, Unpres.
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92504779001, 92504779002, 92504779003, 92504779004, 92504779005, 92504779006, 92504779007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3065213
Associated Lab Samples:92504779001, 92504779002, 92504779003, 92504779004, 92504779005, 92504779006, 92504779007
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.040 11/11/20 00:12
Nitrogen, Nitrite mg/L ND 0.040 11/11/20 00:12
Nitrogen, NO2 plus NO3 mg/L ND 0.040 11/11/20 00:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3065214LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 1.51.5 103 90-110
Nitrogen, Nitrite mg/L 1.01 101 90-110
Nitrogen, NO2 plus NO3 mg/L 2.62.5 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3065215MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92504779001
3065216
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 70 90-11069 11.50.14 1.2 1.2
Nitrogen, Nitrite mg/L 1 91 90-11091 11ND0.95 0.95
Nitrogen, NO2 plus NO3 mg/L M12.5 80 90-11080 02.50.14 2.1 2.1
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3065217MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92504779002
3065218
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 63 90-11063 01.5ND 0.95 0.94
Nitrogen, Nitrite mg/L M118590-11085 010.068 0.92 0.92
Nitrogen, NO2 plus NO3 mg/L M12.5 73 90-11073 02.50.047 1.9 1.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 28 of 33
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.BC
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 29 of 33
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92504779
Blue Ridge Tissue Corp 11/9/20
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92504779001 579083 579109MW-1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92504779002 579083 579109MW-2 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92504779003 579083 579109MW-3 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92504779004 579083 579109MW-4 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92504779005 579083 579109MW-6 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92504779006 579083 579109MW-7 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92504779007 579083 579109MW-8 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92504779004 579554MW-4 SM 6200B
92504779002 580169MW-2 SM 2540C-2011
92504779001 580427MW-1 SM 4500-H+B-2011
92504779002 580427MW-2 SM 4500-H+B-2011
92504779003 580427MW-3 SM 4500-H+B-2011
92504779004 580427MW-4 SM 4500-H+B-2011
92504779005 580427MW-6 SM 4500-H+B-2011
92504779006 580427MW-7 SM 4500-H+B-2011
92504779007 580427MW-8 SM 4500-H+B-2011
92504779001 579131MW-1 EPA 300.0 Rev 2.1 1993
92504779002 579131MW-2 EPA 300.0 Rev 2.1 1993
92504779003 579131MW-3 EPA 300.0 Rev 2.1 1993
92504779004 579131MW-4 EPA 300.0 Rev 2.1 1993
92504779005 579131MW-6 EPA 300.0 Rev 2.1 1993
92504779006 579131MW-7 EPA 300.0 Rev 2.1 1993
92504779007 579438MW-8 EPA 300.0 Rev 2.1 1993
92504779001 579814MW-1 EPA 350.1 Rev 2.0 1993
92504779002 579814MW-2 EPA 350.1 Rev 2.0 1993
92504779003 579814MW-3 EPA 350.1 Rev 2.0 1993
92504779004 579814MW-4 EPA 350.1 Rev 2.0 1993
92504779005 579814MW-6 EPA 350.1 Rev 2.0 1993
92504779006 579814MW-7 EPA 350.1 Rev 2.0 1993
92504779007 579814MW-8 EPA 350.1 Rev 2.0 1993
92504779001 579435 579789MW-1 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92504779002 579435 579789MW-2 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92504779003 579439 579790MW-3 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92504779004 579439 579790MW-4 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92504779005 579439 579790MW-6 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92504779006 579439 579790MW-7 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92504779007 579439 579790MW-8 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92504779001 579361MW-1 EPA 353.2 Rev 2.0 1993
92504779002 579361MW-2 EPA 353.2 Rev 2.0 1993
92504779003 579361MW-3 EPA 353.2 Rev 2.0 1993
92504779004 579361MW-4 EPA 353.2 Rev 2.0 1993
92504779005 579361MW-6 EPA 353.2 Rev 2.0 1993
92504779006 579361MW-7 EPA 353.2 Rev 2.0 1993
92504779007 579361MW-8 EPA 353.2 Rev 2.0 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/17/2020 04:44 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 30 of 33
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