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NC0006254_Groundwater Monitoring Report July 2021_20210719
PO Box 604 ▪ Fletcher, NC 28732 ▪ Cell: 828-508-4510 July 19, 2021 Mr. Brett Laverty NCDEQ Division of Water Resources Asheville Regional Office 2090 US Highway 70 Swannanoa, NC 28778 RE: Groundwater Analytical Results – July 7, 2021 Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina Mr. Laverty: On July 7, 2021, Singleton Environmental, Inc. (SEI) visited the Blue Ridge Tissue site located at 1427 Yadkin River Road in Patterson, North Carolina, to collect groundwater samples from monitoring wells MW-1, MW-2, MW-3, MW-4, MW-6, MW-7 and MW-8. The depth to groundwater in the monitoring wells ranged from 5.85 feet in MW-4 to 51.05 feet in MW-2. Refer to Table 1 for all monitoring well groundwater depths and Figure 1 for all monitoring well locations. All groundwater samples, with the exception of MW-2, were collected using a peristaltic pump connected to a Horiba U52-2 water quality meter with a flow through cell to collect groundwater parameters (temperature, pH, specific conductivity, dissolved oxygen, ORP, and turbidity). Groundwater sample MW-2 was collected using a bailer once three well volumes were removed. Groundwater from the same bail as the sample was also poured into the flow cell to collect the approximate parameters. The groundwater samples were submitted on ice to Pace Analytical for the analysis of 8-RCRA Metals, pH, ammonia, TKN, sulfate, nitrogen, nitrite and nitrate. MW-2 was also analyzed for total dissolved solids (TDS) using EPA Method SM 2540C, and volatile organic compounds (VOCs) using EPA Method 6200B. The groundwater parameters for all samples are outlined in Table 2. The laboratory analysis of groundwater samples MW-1 detected levels of iron and manganese above the NCAC 2L groundwater standards. The laboratory analysis of MW-2 detected levels of barium, iron, manganese, and ammonia above the NCAC 2L groundwater standards. The laboratory analysis of groundwater samples MW-3 detected levels of iron, manganese and ammonia above the NCAC 2L groundwater standards. The laboratory analysis of groundwater samples MW-4 detected levels of iron and manganese above the NCAC 2L groundwater standards. Laboratory analysis of groundwater samples MW-6, MW-7, and MW-8 did not detect any compounds exceeding the NCAC 2L groundwater standards. The analytical results are shown on attached Table 2 and the attached laboratory data sheets. During the April 2017 groundwater sampling event, AECOM reported a possible sheen on the groundwater in monitoring well MW-4. During the July 2021 event a sheen was not observed; Singleton Environmental, Inc. Singleton Environmental, Inc. however, a VOC sample was collected from each monitoring well and analyzed using EPA Method 6200B. None of the concentrations were detected above the minimum laboratory detection levels. The compound levels detected in the groundwater analysis for the July 2021 sampling event were comparable to the March 2021 and November 2020 sampling events, with the exception of arsenic and chromium being absent in MW-2, and iron being absent in MW-7 as compared to the March 2021 sampling event. Singleton Environmental, Inc. recommends sampling the monitoring wells again in November 2021. If you have any questions you can reach me at (828) 508-4510. Sincerely, Chris Singleton, P.G. Singleton Environmental, Inc. cc: Dave Hallock, Blue Ridge Tissue Corporation Attachments @A @A @A @A @A @A @A @A MW-2 MW-3 MW-4 MW-1 @A MW-5 MW-7 MW-6 MW-8 1 2 8 0 12601 3 2 0 1340 1360 1380 124014201240 1420 Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/AirbusDS, USDA, USGS, AEX, Getmapping, Aerogrid, IGN, IGP, swisstopo, and theGIS User Community Figure 60540673 1 May 2017 § 0 200 400Feet 1 inch = 200 feet Y a d k i n R i v e r R d Whisnant RdYad k i n R i v e r Yadkin R iver Roby Martin Rd#0 Site Layout MapBlue Ridge Tissue CorporationPatterson, North Carolina Legend Property Boundary Yadkin River Flow Direction #Land Surface Elevation Contour (ft above mean sea level) Monitoring Well Location Abandoned Water Well#0@A Well ID Date Installed Total Depth (feet bls) Screened Interval (feet bls) Top of Casing Elevation (feet msl) Date Water Level Measured Depth to Water (feet BTOC) Groundwater Elevation (feet msl) MW-1 02/08/11 11 6-11 1253.71 07/07/21 12.32 1,241.39 MW-2 08/12/09 50 40-50 1323.03 07/07/21 51.05 1,271.98 MW-3 08/13/09 20 10-20 1299.02 07/07/21 17.37 1,281.65 MW-4 08/13/09 15 5-15 1247.23 07/07/21 5.85 1,241.38 MW-5 08/16/11 21 11-21 1285.46 N/A N/A N/A MW-6 08/06/14 29 19-29 1341.55 07/07/21 26.76 1,314.79 MW-7 08/06/14 24 14-24 1274.41 07/07/21 18.95 1,255.46 MW-8 08/06/14 20 10-20 1253.14 07/07/21 14.83 1,238.31 Notes: bls - feet below land surface BTOC - below top of casing msl - above mean sea level NG - not gauged AECOM Table 1 Monitoring Well Construction and Groundwater Elevations Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina Sample ID MW-1 MW-2*MW-3 MW-4 MW-6 MW-7 MW-8 Sample Date 07/07/21 07/07/21 07/07/21 07/07/21 07/07/21 07/07/21 07/07/21 Temperature (°C)NS 17.8 N/A 21.04 18.44 23.86 20.75 16.30 pH (standard units)NS 6.02 N/A 6.31 6.26 5.82 6.15 5.87 Specific Conductivity (mS/cm)NS 0.211 N/A 0.498 0.194 0.015 0.084 0.096 Dissolved Oxygen (mg/L)NS 2.30 N/A 1.40 0.76 5.38 3.91 6.35 ORP (mV)NS -41.0 N/A 32.0 -25.0 140.0 102.0 74.0 Turbidity (NTU)NS 7.5 N/A 8.6 7.7 5.9 3.1 2.3 Gallons Pumped NS 2 1.00 3 1.5 2.5 1.5 2 Cloudy/Odor No/No No/No Cloudy/Odor Cloudy/Odor No/No No/No No/No No/No Total Barium (ug/L)700 108 1790 278 73.8 77.4 53.2 12 Total Iron (ug/L)300 17100 60600 34800 11200 ND 62.3 ND Total Manganese (ug/L)50 2410 648 4060 1230 13.8 ND ND Aresenic (ug/L)10 ND ND ND ND ND ND ND Chromium (ug/L)10 ND ND ND ND ND ND ND Lead (ug/L)15 ND ND ND ND ND ND ND Sulfate N/A ND 1.4 18.9 2.4 ND 2.2 19 Amonia (mg/L)1.5 0.41 7.3 6.5 0.92 ND ND ND TKN (mg/L)N/A 0.54 16.2 13.9 1.2 ND ND ND Nitrogen NO2 plus NO3 (mg/L)N/A 0.061 0.1 0.2 0.072 0.11 1.2 2.8 Nitrate (mg/L)10 0.061 0.1 0.14 0.072 0.11 1.2 2.8 Nitrite (mg/L)1 ND 0.16 0.055 ND ND ND ND pH (standard units)N/A 6.3 6.5 6.4 6.5 5.6 6.4 6 Total Disolved Solids (mg/L)N/A N/A 339 N/A N/A N/A N/A N/A EPA Method 6200B for VOCs N/A ND ND ND ND ND ND ND Notes: Samples analyzed for total and dissolved iron, barium and manganese by EPA Method 200.7 2L Standard - North Carolina groundwater quality standards established in Title 15A of the North Carolina Administrative Code, Subchapter 2L, Section 0.20 °C - degrees Celsius µS/cm - microsiemens per centimeter EPA - United States Environmental Protection Agency mg/L - milligrams per liter mV - millivolt NA - Not analyzed NS - No standard NTU - Nephelometric Turbidity Unit RCRA - Resource Conservation Recovery Act Bold samples indicate concentrations above the 2L Standard *MW-2 purged with disposable bailer, water quality parameters collected from same bail as sample. 2L Standard Field Parameters Analytical Parameters Table 2 Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina #=CL# July 15, 2021 LIMS USE: FR - CHRIS SINGLETON LIMS OBJECT ID: 92548091 92548091 Project: Pace Project No.: RE: Chris Singleton Singleton Environmental P.O. Box 2012 Enka, NC 28728 Blue Ridge Tissue Corp. MWs Dear Chris Singleton: Enclosed are the analytical results for sample(s) received by the laboratory on July 07, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton lorri.patton@pacelabs.com Project Manager 1(828)254-7176 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 1 of 44 #=CP# CERTIFICATIONS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 2 of 44 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92548091001 MW-1 EPA 200.7 Rev 4.4 1994 6 PASI-ADS SM 6200B 63 PASI-CPM1 SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92548091002 MW-2 EPA 200.7 Rev 4.4 1994 6 PASI-ADS SM 6200B 63 PASI-CPM1 SM 2540C-2011 1 PASI-AZMC SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92548091003 MW-3 EPA 200.7 Rev 4.4 1994 6 PASI-ADS SM 6200B 63 PASI-CPM1 SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92548091004 MW-4 EPA 200.7 Rev 4.4 1994 6 PASI-ADS SM 6200B 63 PASI-CPM1 SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92548091005 MW-6 EPA 200.7 Rev 4.4 1994 6 PASI-ADS SM 6200B 63 PASI-CPM1 SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92548091006 MW-7 EPA 200.7 Rev 4.4 1994 6 PASI-ASH1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 3 of 44 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts SM 6200B 63 PASI-CPM1 SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92548091007 MW-8 EPA 200.7 Rev 4.4 1994 6 PASI-ADS SM 6200B 63 PASI-CPM1 SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 4 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-1 Lab ID:92548091001 Collected:07/07/21 10:40 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 07/13/21 15:53 7440-38-207/12/21 12:2010.0 1 Barium 108 ug/L 07/13/21 15:53 7440-39-307/12/21 12:205.0 1 Chromium ND ug/L 07/13/21 15:53 7440-47-307/12/21 12:205.0 1 Iron 17100 ug/L 07/13/21 15:53 7439-89-6 P807/12/21 12:2050.0 1 Lead ND ug/L 07/13/21 15:53 7439-92-107/12/21 12:205.0 1 Manganese 2410 ug/L 07/13/21 15:53 7439-96-507/12/21 12:205.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 07/09/21 14:03 71-43-20.50 1 Bromobenzene ND ug/L 07/09/21 14:03 108-86-10.50 1 Bromochloromethane ND ug/L 07/09/21 14:03 74-97-50.50 1 Bromodichloromethane ND ug/L 07/09/21 14:03 75-27-40.50 1 Bromoform ND ug/L 07/09/21 14:03 75-25-20.50 1 Bromomethane ND ug/L 07/09/21 14:03 74-83-95.0 1 n-Butylbenzene ND ug/L 07/09/21 14:03 104-51-80.50 1 sec-Butylbenzene ND ug/L 07/09/21 14:03 135-98-80.50 1 tert-Butylbenzene ND ug/L 07/09/21 14:03 98-06-60.50 1 Carbon tetrachloride ND ug/L 07/09/21 14:03 56-23-50.50 1 Chlorobenzene ND ug/L 07/09/21 14:03 108-90-70.50 1 Chloroethane ND ug/L 07/09/21 14:03 75-00-31.0 1 Chloroform ND ug/L 07/09/21 14:03 67-66-30.50 1 Chloromethane ND ug/L 07/09/21 14:03 74-87-31.0 1 2-Chlorotoluene ND ug/L 07/09/21 14:03 95-49-80.50 1 4-Chlorotoluene ND ug/L 07/09/21 14:03 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 07/09/21 14:03 96-12-81.0 1 Dibromochloromethane ND ug/L 07/09/21 14:03 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 07/09/21 14:03 106-93-40.50 1 Dibromomethane ND ug/L 07/09/21 14:03 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 07/09/21 14:03 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 07/09/21 14:03 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 07/09/21 14:03 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 07/09/21 14:03 75-71-80.50 1 1,1-Dichloroethane ND ug/L 07/09/21 14:03 75-34-30.50 1 1,2-Dichloroethane ND ug/L 07/09/21 14:03 107-06-20.50 1 1,1-Dichloroethene ND ug/L 07/09/21 14:03 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 07/09/21 14:03 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 07/09/21 14:03 156-60-50.50 1 1,2-Dichloropropane ND ug/L 07/09/21 14:03 78-87-50.50 1 1,3-Dichloropropane ND ug/L 07/09/21 14:03 142-28-90.50 1 2,2-Dichloropropane ND ug/L 07/09/21 14:03 594-20-70.50 1 1,1-Dichloropropene ND ug/L 07/09/21 14:03 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 07/09/21 14:03 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 07/09/21 14:03 10061-02-60.50 1 Diisopropyl ether ND ug/L 07/09/21 14:03 108-20-30.50 1 Ethylbenzene ND ug/L 07/09/21 14:03 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 5 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-1 Lab ID:92548091001 Collected:07/07/21 10:40 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 07/09/21 14:03 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 07/09/21 14:03 98-82-80.50 1 Methylene Chloride ND ug/L 07/09/21 14:03 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 07/09/21 14:03 1634-04-40.50 1 Naphthalene ND ug/L 07/09/21 14:03 91-20-32.0 1 n-Propylbenzene ND ug/L 07/09/21 14:03 103-65-10.50 1 Styrene ND ug/L 07/09/21 14:03 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 07/09/21 14:03 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 07/09/21 14:03 79-34-50.50 1 Tetrachloroethene ND ug/L 07/09/21 14:03 127-18-40.50 1 Toluene ND ug/L 07/09/21 14:03 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 07/09/21 14:03 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 07/09/21 14:03 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 07/09/21 14:03 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 07/09/21 14:03 79-00-50.50 1 Trichloroethene ND ug/L 07/09/21 14:03 79-01-60.50 1 Trichlorofluoromethane ND ug/L 07/09/21 14:03 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 07/09/21 14:03 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 07/09/21 14:03 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 07/09/21 14:03 108-67-80.50 1 Vinyl chloride ND ug/L 07/09/21 14:03 75-01-41.0 1 m&p-Xylene ND ug/L 07/09/21 14:03 179601-23-11.0 1 o-Xylene ND ug/L 07/09/21 14:03 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)109 %07/09/21 14:03 17060-07-070-130 1 4-Bromofluorobenzene (S)102 %07/09/21 14:03 460-00-470-130 1 Toluene-d8 (S)99 %07/09/21 14:03 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.3 Std. Units 07/11/21 13:06 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate ND mg/L 07/09/21 12:02 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 0.41 mg/L 07/09/21 14:58 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 0.54 mg/L 07/10/21 05:15 7727-37-907/09/21 18:480.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 6 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-1 Lab ID:92548091001 Collected:07/07/21 10:40 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 0.061 mg/L 07/08/21 00:270.040 1 Nitrogen, Nitrate 0.061 mg/L 07/08/21 00:27 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 07/08/21 00:27 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 7 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-2 Lab ID:92548091002 Collected:07/07/21 11:00 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 07/13/21 16:09 7440-38-207/12/21 12:2010.0 1 Barium 1790 ug/L 07/13/21 16:09 7440-39-307/12/21 12:205.0 1 Chromium ND ug/L 07/13/21 16:09 7440-47-307/12/21 12:205.0 1 Iron 60600 ug/L 07/13/21 16:09 7439-89-6 P807/12/21 12:2050.0 1 Lead ND ug/L 07/13/21 16:09 7439-92-107/12/21 12:205.0 1 Manganese 648 ug/L 07/13/21 16:09 7439-96-507/12/21 12:205.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 07/09/21 14:21 71-43-20.50 1 Bromobenzene ND ug/L 07/09/21 14:21 108-86-10.50 1 Bromochloromethane ND ug/L 07/09/21 14:21 74-97-50.50 1 Bromodichloromethane ND ug/L 07/09/21 14:21 75-27-40.50 1 Bromoform ND ug/L 07/09/21 14:21 75-25-20.50 1 Bromomethane ND ug/L 07/09/21 14:21 74-83-95.0 1 n-Butylbenzene ND ug/L 07/09/21 14:21 104-51-80.50 1 sec-Butylbenzene ND ug/L 07/09/21 14:21 135-98-80.50 1 tert-Butylbenzene ND ug/L 07/09/21 14:21 98-06-60.50 1 Carbon tetrachloride ND ug/L 07/09/21 14:21 56-23-50.50 1 Chlorobenzene ND ug/L 07/09/21 14:21 108-90-70.50 1 Chloroethane ND ug/L 07/09/21 14:21 75-00-31.0 1 Chloroform ND ug/L 07/09/21 14:21 67-66-30.50 1 Chloromethane ND ug/L 07/09/21 14:21 74-87-31.0 1 2-Chlorotoluene ND ug/L 07/09/21 14:21 95-49-80.50 1 4-Chlorotoluene ND ug/L 07/09/21 14:21 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 07/09/21 14:21 96-12-81.0 1 Dibromochloromethane ND ug/L 07/09/21 14:21 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 07/09/21 14:21 106-93-40.50 1 Dibromomethane ND ug/L 07/09/21 14:21 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 07/09/21 14:21 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 07/09/21 14:21 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 07/09/21 14:21 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 07/09/21 14:21 75-71-80.50 1 1,1-Dichloroethane ND ug/L 07/09/21 14:21 75-34-30.50 1 1,2-Dichloroethane ND ug/L 07/09/21 14:21 107-06-20.50 1 1,1-Dichloroethene ND ug/L 07/09/21 14:21 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 07/09/21 14:21 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 07/09/21 14:21 156-60-50.50 1 1,2-Dichloropropane ND ug/L 07/09/21 14:21 78-87-50.50 1 1,3-Dichloropropane ND ug/L 07/09/21 14:21 142-28-90.50 1 2,2-Dichloropropane ND ug/L 07/09/21 14:21 594-20-70.50 1 1,1-Dichloropropene ND ug/L 07/09/21 14:21 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 07/09/21 14:21 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 07/09/21 14:21 10061-02-60.50 1 Diisopropyl ether ND ug/L 07/09/21 14:21 108-20-30.50 1 Ethylbenzene ND ug/L 07/09/21 14:21 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 8 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-2 Lab ID:92548091002 Collected:07/07/21 11:00 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 07/09/21 14:21 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 07/09/21 14:21 98-82-80.50 1 Methylene Chloride ND ug/L 07/09/21 14:21 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 07/09/21 14:21 1634-04-40.50 1 Naphthalene ND ug/L 07/09/21 14:21 91-20-32.0 1 n-Propylbenzene ND ug/L 07/09/21 14:21 103-65-10.50 1 Styrene ND ug/L 07/09/21 14:21 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 07/09/21 14:21 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 07/09/21 14:21 79-34-50.50 1 Tetrachloroethene ND ug/L 07/09/21 14:21 127-18-40.50 1 Toluene ND ug/L 07/09/21 14:21 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 07/09/21 14:21 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 07/09/21 14:21 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 07/09/21 14:21 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 07/09/21 14:21 79-00-50.50 1 Trichloroethene ND ug/L 07/09/21 14:21 79-01-60.50 1 Trichlorofluoromethane ND ug/L 07/09/21 14:21 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 07/09/21 14:21 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 07/09/21 14:21 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 07/09/21 14:21 108-67-80.50 1 Vinyl chloride ND ug/L 07/09/21 14:21 75-01-41.0 1 m&p-Xylene ND ug/L 07/09/21 14:21 179601-23-11.0 1 o-Xylene ND ug/L 07/09/21 14:21 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)112 %07/09/21 14:21 17060-07-070-130 1 4-Bromofluorobenzene (S)103 %07/09/21 14:21 460-00-470-130 1 Toluene-d8 (S)100 %07/09/21 14:21 2037-26-570-130 1 Analytical Method: SM 2540C-2011 Pace Analytical Services - Asheville 2540C Total Dissolved Solids Total Dissolved Solids 339 mg/L 07/12/21 16:3525.0 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.5 Std. Units 07/11/21 13:18 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 1.4 mg/L 07/09/21 12:15 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 7.3 mg/L 07/09/21 14:59 7664-41-70.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 9 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-2 Lab ID:92548091002 Collected:07/07/21 11:00 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 16.2 mg/L 07/10/21 05:16 7727-37-907/09/21 18:480.50 1 Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 0.10 mg/L 07/08/21 00:280.040 1 Nitrogen, Nitrate 0.10 mg/L 07/08/21 00:28 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 07/08/21 00:28 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 10 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-3 Lab ID:92548091003 Collected:07/07/21 11:15 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 07/13/21 16:12 7440-38-207/12/21 12:2010.0 1 Barium 278 ug/L 07/13/21 16:12 7440-39-307/12/21 12:205.0 1 Chromium ND ug/L 07/13/21 16:12 7440-47-307/12/21 12:205.0 1 Iron 34800 ug/L 07/13/21 16:12 7439-89-6 P807/12/21 12:2050.0 1 Lead ND ug/L 07/13/21 16:12 7439-92-107/12/21 12:205.0 1 Manganese 4060 ug/L 07/13/21 16:12 7439-96-507/12/21 12:205.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 07/09/21 14:39 71-43-20.50 1 Bromobenzene ND ug/L 07/09/21 14:39 108-86-10.50 1 Bromochloromethane ND ug/L 07/09/21 14:39 74-97-50.50 1 Bromodichloromethane ND ug/L 07/09/21 14:39 75-27-40.50 1 Bromoform ND ug/L 07/09/21 14:39 75-25-20.50 1 Bromomethane ND ug/L 07/09/21 14:39 74-83-95.0 1 n-Butylbenzene ND ug/L 07/09/21 14:39 104-51-80.50 1 sec-Butylbenzene ND ug/L 07/09/21 14:39 135-98-80.50 1 tert-Butylbenzene ND ug/L 07/09/21 14:39 98-06-60.50 1 Carbon tetrachloride ND ug/L 07/09/21 14:39 56-23-50.50 1 Chlorobenzene ND ug/L 07/09/21 14:39 108-90-70.50 1 Chloroethane ND ug/L 07/09/21 14:39 75-00-31.0 1 Chloroform ND ug/L 07/09/21 14:39 67-66-30.50 1 Chloromethane ND ug/L 07/09/21 14:39 74-87-31.0 1 2-Chlorotoluene ND ug/L 07/09/21 14:39 95-49-80.50 1 4-Chlorotoluene ND ug/L 07/09/21 14:39 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 07/09/21 14:39 96-12-81.0 1 Dibromochloromethane ND ug/L 07/09/21 14:39 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 07/09/21 14:39 106-93-40.50 1 Dibromomethane ND ug/L 07/09/21 14:39 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 07/09/21 14:39 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 07/09/21 14:39 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 07/09/21 14:39 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 07/09/21 14:39 75-71-80.50 1 1,1-Dichloroethane ND ug/L 07/09/21 14:39 75-34-30.50 1 1,2-Dichloroethane ND ug/L 07/09/21 14:39 107-06-20.50 1 1,1-Dichloroethene ND ug/L 07/09/21 14:39 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 07/09/21 14:39 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 07/09/21 14:39 156-60-50.50 1 1,2-Dichloropropane ND ug/L 07/09/21 14:39 78-87-50.50 1 1,3-Dichloropropane ND ug/L 07/09/21 14:39 142-28-90.50 1 2,2-Dichloropropane ND ug/L 07/09/21 14:39 594-20-70.50 1 1,1-Dichloropropene ND ug/L 07/09/21 14:39 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 07/09/21 14:39 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 07/09/21 14:39 10061-02-60.50 1 Diisopropyl ether ND ug/L 07/09/21 14:39 108-20-30.50 1 Ethylbenzene ND ug/L 07/09/21 14:39 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 11 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-3 Lab ID:92548091003 Collected:07/07/21 11:15 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 07/09/21 14:39 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 07/09/21 14:39 98-82-80.50 1 Methylene Chloride ND ug/L 07/09/21 14:39 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 07/09/21 14:39 1634-04-40.50 1 Naphthalene ND ug/L 07/09/21 14:39 91-20-32.0 1 n-Propylbenzene ND ug/L 07/09/21 14:39 103-65-10.50 1 Styrene ND ug/L 07/09/21 14:39 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 07/09/21 14:39 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 07/09/21 14:39 79-34-50.50 1 Tetrachloroethene ND ug/L 07/09/21 14:39 127-18-40.50 1 Toluene ND ug/L 07/09/21 14:39 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 07/09/21 14:39 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 07/09/21 14:39 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 07/09/21 14:39 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 07/09/21 14:39 79-00-50.50 1 Trichloroethene ND ug/L 07/09/21 14:39 79-01-60.50 1 Trichlorofluoromethane ND ug/L 07/09/21 14:39 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 07/09/21 14:39 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 07/09/21 14:39 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 07/09/21 14:39 108-67-80.50 1 Vinyl chloride ND ug/L 07/09/21 14:39 75-01-41.0 1 m&p-Xylene ND ug/L 07/09/21 14:39 179601-23-11.0 1 o-Xylene ND ug/L 07/09/21 14:39 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)114 %07/09/21 14:39 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %07/09/21 14:39 460-00-470-130 1 Toluene-d8 (S)99 %07/09/21 14:39 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.4 Std. Units 07/11/21 13:24 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 18.9 mg/L 07/09/21 12:29 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 6.5 mg/L 07/09/21 15:01 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 13.9 mg/L 07/10/21 05:17 7727-37-907/09/21 18:480.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 12 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-3 Lab ID:92548091003 Collected:07/07/21 11:15 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 0.20 mg/L 07/08/21 00:300.040 1 Nitrogen, Nitrate 0.14 mg/L 07/08/21 00:30 14797-55-80.040 1 Nitrogen, Nitrite 0.055 mg/L 07/08/21 00:30 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 13 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-4 Lab ID:92548091004 Collected:07/07/21 13:15 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 07/13/21 16:16 7440-38-207/12/21 12:2010.0 1 Barium 73.8 ug/L 07/13/21 16:16 7440-39-307/12/21 12:205.0 1 Chromium ND ug/L 07/13/21 16:16 7440-47-307/12/21 12:205.0 1 Iron 11200 ug/L 07/13/21 16:16 7439-89-6 P807/12/21 12:2050.0 1 Lead ND ug/L 07/13/21 16:16 7439-92-107/12/21 12:205.0 1 Manganese 1230 ug/L 07/13/21 16:16 7439-96-507/12/21 12:205.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 07/09/21 14:57 71-43-20.50 1 Bromobenzene ND ug/L 07/09/21 14:57 108-86-10.50 1 Bromochloromethane ND ug/L 07/09/21 14:57 74-97-50.50 1 Bromodichloromethane ND ug/L 07/09/21 14:57 75-27-40.50 1 Bromoform ND ug/L 07/09/21 14:57 75-25-20.50 1 Bromomethane ND ug/L 07/09/21 14:57 74-83-95.0 1 n-Butylbenzene ND ug/L 07/09/21 14:57 104-51-80.50 1 sec-Butylbenzene ND ug/L 07/09/21 14:57 135-98-80.50 1 tert-Butylbenzene ND ug/L 07/09/21 14:57 98-06-60.50 1 Carbon tetrachloride ND ug/L 07/09/21 14:57 56-23-50.50 1 Chlorobenzene ND ug/L 07/09/21 14:57 108-90-70.50 1 Chloroethane ND ug/L 07/09/21 14:57 75-00-31.0 1 Chloroform ND ug/L 07/09/21 14:57 67-66-30.50 1 Chloromethane ND ug/L 07/09/21 14:57 74-87-31.0 1 2-Chlorotoluene ND ug/L 07/09/21 14:57 95-49-80.50 1 4-Chlorotoluene ND ug/L 07/09/21 14:57 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 07/09/21 14:57 96-12-81.0 1 Dibromochloromethane ND ug/L 07/09/21 14:57 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 07/09/21 14:57 106-93-40.50 1 Dibromomethane ND ug/L 07/09/21 14:57 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 07/09/21 14:57 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 07/09/21 14:57 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 07/09/21 14:57 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 07/09/21 14:57 75-71-80.50 1 1,1-Dichloroethane ND ug/L 07/09/21 14:57 75-34-30.50 1 1,2-Dichloroethane ND ug/L 07/09/21 14:57 107-06-20.50 1 1,1-Dichloroethene ND ug/L 07/09/21 14:57 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 07/09/21 14:57 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 07/09/21 14:57 156-60-50.50 1 1,2-Dichloropropane ND ug/L 07/09/21 14:57 78-87-50.50 1 1,3-Dichloropropane ND ug/L 07/09/21 14:57 142-28-90.50 1 2,2-Dichloropropane ND ug/L 07/09/21 14:57 594-20-70.50 1 1,1-Dichloropropene ND ug/L 07/09/21 14:57 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 07/09/21 14:57 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 07/09/21 14:57 10061-02-60.50 1 Diisopropyl ether ND ug/L 07/09/21 14:57 108-20-30.50 1 Ethylbenzene ND ug/L 07/09/21 14:57 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 14 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-4 Lab ID:92548091004 Collected:07/07/21 13:15 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 07/09/21 14:57 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 07/09/21 14:57 98-82-80.50 1 Methylene Chloride ND ug/L 07/09/21 14:57 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 07/09/21 14:57 1634-04-40.50 1 Naphthalene ND ug/L 07/09/21 14:57 91-20-32.0 1 n-Propylbenzene ND ug/L 07/09/21 14:57 103-65-10.50 1 Styrene ND ug/L 07/09/21 14:57 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 07/09/21 14:57 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 07/09/21 14:57 79-34-50.50 1 Tetrachloroethene ND ug/L 07/09/21 14:57 127-18-40.50 1 Toluene ND ug/L 07/09/21 14:57 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 07/09/21 14:57 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 07/09/21 14:57 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 07/09/21 14:57 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 07/09/21 14:57 79-00-50.50 1 Trichloroethene ND ug/L 07/09/21 14:57 79-01-60.50 1 Trichlorofluoromethane ND ug/L 07/09/21 14:57 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 07/09/21 14:57 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 07/09/21 14:57 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 07/09/21 14:57 108-67-80.50 1 Vinyl chloride ND ug/L 07/09/21 14:57 75-01-41.0 1 m&p-Xylene ND ug/L 07/09/21 14:57 179601-23-11.0 1 o-Xylene ND ug/L 07/09/21 14:57 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)112 %07/09/21 14:57 17060-07-070-130 1 4-Bromofluorobenzene (S)102 %07/09/21 14:57 460-00-470-130 1 Toluene-d8 (S)99 %07/09/21 14:57 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.5 Std. Units 07/11/21 13:46 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 2.4 mg/L 07/09/21 13:09 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 0.92 mg/L 07/09/21 15:02 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 1.2 mg/L 07/10/21 05:18 7727-37-907/09/21 18:480.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 15 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-4 Lab ID:92548091004 Collected:07/07/21 13:15 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 0.072 mg/L 07/08/21 00:370.040 1 Nitrogen, Nitrate 0.072 mg/L 07/08/21 00:37 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 07/08/21 00:37 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 16 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-6 Lab ID:92548091005 Collected:07/07/21 12:30 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 07/13/21 16:19 7440-38-207/12/21 12:2010.0 1 Barium 77.4 ug/L 07/13/21 16:19 7440-39-307/12/21 12:205.0 1 Chromium ND ug/L 07/13/21 16:19 7440-47-307/12/21 12:205.0 1 Iron ND ug/L 07/13/21 16:19 7439-89-6 P807/12/21 12:2050.0 1 Lead ND ug/L 07/13/21 16:19 7439-92-107/12/21 12:205.0 1 Manganese 13.8 ug/L 07/13/21 16:19 7439-96-507/12/21 12:205.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 07/09/21 15:15 71-43-20.50 1 Bromobenzene ND ug/L 07/09/21 15:15 108-86-10.50 1 Bromochloromethane ND ug/L 07/09/21 15:15 74-97-50.50 1 Bromodichloromethane ND ug/L 07/09/21 15:15 75-27-40.50 1 Bromoform ND ug/L 07/09/21 15:15 75-25-20.50 1 Bromomethane ND ug/L 07/09/21 15:15 74-83-95.0 1 n-Butylbenzene ND ug/L 07/09/21 15:15 104-51-80.50 1 sec-Butylbenzene ND ug/L 07/09/21 15:15 135-98-80.50 1 tert-Butylbenzene ND ug/L 07/09/21 15:15 98-06-60.50 1 Carbon tetrachloride ND ug/L 07/09/21 15:15 56-23-50.50 1 Chlorobenzene ND ug/L 07/09/21 15:15 108-90-70.50 1 Chloroethane ND ug/L 07/09/21 15:15 75-00-31.0 1 Chloroform ND ug/L 07/09/21 15:15 67-66-30.50 1 Chloromethane ND ug/L 07/09/21 15:15 74-87-31.0 1 2-Chlorotoluene ND ug/L 07/09/21 15:15 95-49-80.50 1 4-Chlorotoluene ND ug/L 07/09/21 15:15 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 07/09/21 15:15 96-12-81.0 1 Dibromochloromethane ND ug/L 07/09/21 15:15 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 07/09/21 15:15 106-93-40.50 1 Dibromomethane ND ug/L 07/09/21 15:15 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 07/09/21 15:15 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 07/09/21 15:15 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 07/09/21 15:15 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 07/09/21 15:15 75-71-80.50 1 1,1-Dichloroethane ND ug/L 07/09/21 15:15 75-34-30.50 1 1,2-Dichloroethane ND ug/L 07/09/21 15:15 107-06-20.50 1 1,1-Dichloroethene ND ug/L 07/09/21 15:15 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 07/09/21 15:15 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 07/09/21 15:15 156-60-50.50 1 1,2-Dichloropropane ND ug/L 07/09/21 15:15 78-87-50.50 1 1,3-Dichloropropane ND ug/L 07/09/21 15:15 142-28-90.50 1 2,2-Dichloropropane ND ug/L 07/09/21 15:15 594-20-70.50 1 1,1-Dichloropropene ND ug/L 07/09/21 15:15 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 07/09/21 15:15 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 07/09/21 15:15 10061-02-60.50 1 Diisopropyl ether ND ug/L 07/09/21 15:15 108-20-30.50 1 Ethylbenzene ND ug/L 07/09/21 15:15 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 17 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-6 Lab ID:92548091005 Collected:07/07/21 12:30 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 07/09/21 15:15 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 07/09/21 15:15 98-82-80.50 1 Methylene Chloride ND ug/L 07/09/21 15:15 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 07/09/21 15:15 1634-04-40.50 1 Naphthalene ND ug/L 07/09/21 15:15 91-20-32.0 1 n-Propylbenzene ND ug/L 07/09/21 15:15 103-65-10.50 1 Styrene ND ug/L 07/09/21 15:15 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 07/09/21 15:15 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 07/09/21 15:15 79-34-50.50 1 Tetrachloroethene ND ug/L 07/09/21 15:15 127-18-40.50 1 Toluene ND ug/L 07/09/21 15:15 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 07/09/21 15:15 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 07/09/21 15:15 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 07/09/21 15:15 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 07/09/21 15:15 79-00-50.50 1 Trichloroethene ND ug/L 07/09/21 15:15 79-01-60.50 1 Trichlorofluoromethane ND ug/L 07/09/21 15:15 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 07/09/21 15:15 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 07/09/21 15:15 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 07/09/21 15:15 108-67-80.50 1 Vinyl chloride ND ug/L 07/09/21 15:15 75-01-41.0 1 m&p-Xylene ND ug/L 07/09/21 15:15 179601-23-11.0 1 o-Xylene ND ug/L 07/09/21 15:15 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)111 %07/09/21 15:15 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %07/09/21 15:15 460-00-470-130 1 Toluene-d8 (S)97 %07/09/21 15:15 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 5.6 Std. Units 07/11/21 13:35 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate ND mg/L 07/09/21 13:22 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia ND mg/L 07/09/21 15:03 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 07/10/21 05:19 7727-37-907/09/21 18:480.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 18 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-6 Lab ID:92548091005 Collected:07/07/21 12:30 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 0.11 mg/L 07/08/21 00:320.040 1 Nitrogen, Nitrate 0.11 mg/L 07/08/21 00:32 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 07/08/21 00:32 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 19 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-7 Lab ID:92548091006 Collected:07/07/21 12:50 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 07/14/21 22:15 7440-38-207/14/21 13:2510.0 1 Barium 53.2 ug/L 07/14/21 22:15 7440-39-307/14/21 13:255.0 1 Chromium ND ug/L 07/14/21 22:15 7440-47-307/14/21 13:255.0 1 Iron 62.3 ug/L 07/14/21 22:15 7439-89-607/14/21 13:2550.0 1 Lead ND ug/L 07/14/21 22:15 7439-92-107/14/21 13:255.0 1 Manganese ND ug/L 07/14/21 22:15 7439-96-507/14/21 13:255.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 07/09/21 15:33 71-43-20.50 1 Bromobenzene ND ug/L 07/09/21 15:33 108-86-10.50 1 Bromochloromethane ND ug/L 07/09/21 15:33 74-97-50.50 1 Bromodichloromethane ND ug/L 07/09/21 15:33 75-27-40.50 1 Bromoform ND ug/L 07/09/21 15:33 75-25-20.50 1 Bromomethane ND ug/L 07/09/21 15:33 74-83-95.0 1 n-Butylbenzene ND ug/L 07/09/21 15:33 104-51-80.50 1 sec-Butylbenzene ND ug/L 07/09/21 15:33 135-98-80.50 1 tert-Butylbenzene ND ug/L 07/09/21 15:33 98-06-60.50 1 Carbon tetrachloride ND ug/L 07/09/21 15:33 56-23-50.50 1 Chlorobenzene ND ug/L 07/09/21 15:33 108-90-70.50 1 Chloroethane ND ug/L 07/09/21 15:33 75-00-31.0 1 Chloroform ND ug/L 07/09/21 15:33 67-66-30.50 1 Chloromethane ND ug/L 07/09/21 15:33 74-87-31.0 1 2-Chlorotoluene ND ug/L 07/09/21 15:33 95-49-80.50 1 4-Chlorotoluene ND ug/L 07/09/21 15:33 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 07/09/21 15:33 96-12-81.0 1 Dibromochloromethane ND ug/L 07/09/21 15:33 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 07/09/21 15:33 106-93-40.50 1 Dibromomethane ND ug/L 07/09/21 15:33 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 07/09/21 15:33 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 07/09/21 15:33 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 07/09/21 15:33 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 07/09/21 15:33 75-71-80.50 1 1,1-Dichloroethane ND ug/L 07/09/21 15:33 75-34-30.50 1 1,2-Dichloroethane ND ug/L 07/09/21 15:33 107-06-20.50 1 1,1-Dichloroethene ND ug/L 07/09/21 15:33 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 07/09/21 15:33 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 07/09/21 15:33 156-60-50.50 1 1,2-Dichloropropane ND ug/L 07/09/21 15:33 78-87-50.50 1 1,3-Dichloropropane ND ug/L 07/09/21 15:33 142-28-90.50 1 2,2-Dichloropropane ND ug/L 07/09/21 15:33 594-20-70.50 1 1,1-Dichloropropene ND ug/L 07/09/21 15:33 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 07/09/21 15:33 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 07/09/21 15:33 10061-02-60.50 1 Diisopropyl ether ND ug/L 07/09/21 15:33 108-20-30.50 1 Ethylbenzene ND ug/L 07/09/21 15:33 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 20 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-7 Lab ID:92548091006 Collected:07/07/21 12:50 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 07/09/21 15:33 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 07/09/21 15:33 98-82-80.50 1 Methylene Chloride ND ug/L 07/09/21 15:33 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 07/09/21 15:33 1634-04-40.50 1 Naphthalene ND ug/L 07/09/21 15:33 91-20-32.0 1 n-Propylbenzene ND ug/L 07/09/21 15:33 103-65-10.50 1 Styrene ND ug/L 07/09/21 15:33 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 07/09/21 15:33 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 07/09/21 15:33 79-34-50.50 1 Tetrachloroethene ND ug/L 07/09/21 15:33 127-18-40.50 1 Toluene ND ug/L 07/09/21 15:33 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 07/09/21 15:33 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 07/09/21 15:33 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 07/09/21 15:33 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 07/09/21 15:33 79-00-50.50 1 Trichloroethene ND ug/L 07/09/21 15:33 79-01-60.50 1 Trichlorofluoromethane ND ug/L 07/09/21 15:33 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 07/09/21 15:33 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 07/09/21 15:33 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 07/09/21 15:33 108-67-80.50 1 Vinyl chloride ND ug/L 07/09/21 15:33 75-01-41.0 1 m&p-Xylene ND ug/L 07/09/21 15:33 179601-23-11.0 1 o-Xylene ND ug/L 07/09/21 15:33 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)114 %07/09/21 15:33 17060-07-070-130 1 4-Bromofluorobenzene (S)102 %07/09/21 15:33 460-00-470-130 1 Toluene-d8 (S)99 %07/09/21 15:33 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.4 Std. Units 07/11/21 13:41 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 2.2 mg/L 07/09/21 13:36 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia ND mg/L 07/09/21 15:08 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 07/10/21 05:23 7727-37-907/09/21 18:480.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 21 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-7 Lab ID:92548091006 Collected:07/07/21 12:50 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 1.2 mg/L 07/08/21 00:340.040 1 Nitrogen, Nitrate 1.2 mg/L 07/08/21 00:34 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 07/08/21 00:34 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 22 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-8 Lab ID:92548091007 Collected:07/07/21 12:00 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 07/13/21 16:25 7440-38-207/12/21 12:2010.0 1 Barium 12.0 ug/L 07/13/21 16:25 7440-39-307/12/21 12:205.0 1 Chromium ND ug/L 07/13/21 16:25 7440-47-307/12/21 12:205.0 1 Iron ND ug/L 07/13/21 16:25 7439-89-6 P807/12/21 12:2050.0 1 Lead ND ug/L 07/13/21 16:25 7439-92-107/12/21 12:205.0 1 Manganese ND ug/L 07/13/21 16:25 7439-96-507/12/21 12:205.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 07/09/21 15:51 71-43-20.50 1 Bromobenzene ND ug/L 07/09/21 15:51 108-86-10.50 1 Bromochloromethane ND ug/L 07/09/21 15:51 74-97-50.50 1 Bromodichloromethane ND ug/L 07/09/21 15:51 75-27-40.50 1 Bromoform ND ug/L 07/09/21 15:51 75-25-20.50 1 Bromomethane ND ug/L 07/09/21 15:51 74-83-95.0 1 n-Butylbenzene ND ug/L 07/09/21 15:51 104-51-80.50 1 sec-Butylbenzene ND ug/L 07/09/21 15:51 135-98-80.50 1 tert-Butylbenzene ND ug/L 07/09/21 15:51 98-06-60.50 1 Carbon tetrachloride ND ug/L 07/09/21 15:51 56-23-50.50 1 Chlorobenzene ND ug/L 07/09/21 15:51 108-90-70.50 1 Chloroethane ND ug/L 07/09/21 15:51 75-00-31.0 1 Chloroform ND ug/L 07/09/21 15:51 67-66-30.50 1 Chloromethane ND ug/L 07/09/21 15:51 74-87-31.0 1 2-Chlorotoluene ND ug/L 07/09/21 15:51 95-49-80.50 1 4-Chlorotoluene ND ug/L 07/09/21 15:51 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 07/09/21 15:51 96-12-81.0 1 Dibromochloromethane ND ug/L 07/09/21 15:51 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 07/09/21 15:51 106-93-40.50 1 Dibromomethane ND ug/L 07/09/21 15:51 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 07/09/21 15:51 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 07/09/21 15:51 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 07/09/21 15:51 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 07/09/21 15:51 75-71-80.50 1 1,1-Dichloroethane ND ug/L 07/09/21 15:51 75-34-30.50 1 1,2-Dichloroethane ND ug/L 07/09/21 15:51 107-06-20.50 1 1,1-Dichloroethene ND ug/L 07/09/21 15:51 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 07/09/21 15:51 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 07/09/21 15:51 156-60-50.50 1 1,2-Dichloropropane ND ug/L 07/09/21 15:51 78-87-50.50 1 1,3-Dichloropropane ND ug/L 07/09/21 15:51 142-28-90.50 1 2,2-Dichloropropane ND ug/L 07/09/21 15:51 594-20-70.50 1 1,1-Dichloropropene ND ug/L 07/09/21 15:51 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 07/09/21 15:51 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 07/09/21 15:51 10061-02-60.50 1 Diisopropyl ether ND ug/L 07/09/21 15:51 108-20-30.50 1 Ethylbenzene ND ug/L 07/09/21 15:51 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 23 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-8 Lab ID:92548091007 Collected:07/07/21 12:00 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 07/09/21 15:51 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 07/09/21 15:51 98-82-80.50 1 Methylene Chloride ND ug/L 07/09/21 15:51 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 07/09/21 15:51 1634-04-40.50 1 Naphthalene ND ug/L 07/09/21 15:51 91-20-32.0 1 n-Propylbenzene ND ug/L 07/09/21 15:51 103-65-10.50 1 Styrene ND ug/L 07/09/21 15:51 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 07/09/21 15:51 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 07/09/21 15:51 79-34-50.50 1 Tetrachloroethene ND ug/L 07/09/21 15:51 127-18-40.50 1 Toluene ND ug/L 07/09/21 15:51 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 07/09/21 15:51 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 07/09/21 15:51 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 07/09/21 15:51 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 07/09/21 15:51 79-00-50.50 1 Trichloroethene ND ug/L 07/09/21 15:51 79-01-60.50 1 Trichlorofluoromethane ND ug/L 07/09/21 15:51 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 07/09/21 15:51 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 07/09/21 15:51 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 07/09/21 15:51 108-67-80.50 1 Vinyl chloride ND ug/L 07/09/21 15:51 75-01-41.0 1 m&p-Xylene ND ug/L 07/09/21 15:51 179601-23-11.0 1 o-Xylene ND ug/L 07/09/21 15:51 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)113 %07/09/21 15:51 17060-07-070-130 1 4-Bromofluorobenzene (S)102 %07/09/21 15:51 460-00-470-130 1 Toluene-d8 (S)101 %07/09/21 15:51 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.0 Std. Units 07/11/21 13:29 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 19.0 mg/L 07/09/21 13:49 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia ND mg/L 07/09/21 15:09 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 07/10/21 05:24 7727-37-907/09/21 18:480.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 24 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Sample:MW-8 Lab ID:92548091007 Collected:07/07/21 12:00 Received:07/07/21 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 2.8 mg/L 07/08/21 00:310.040 1 Nitrogen, Nitrate 2.8 mg/L 07/08/21 00:31 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 07/08/21 00:31 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 25 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 632691 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 200.7 MET Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3323426 Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091007 Matrix:Water Analyzed Arsenic ug/L ND 10.0 07/13/21 15:47 Barium ug/L ND 5.0 07/13/21 15:47 Chromium ug/L ND 5.0 07/13/21 15:47 Iron ug/L 68.9 50.0 P807/13/21 21:01 Lead ug/L ND 5.0 07/13/21 15:47 Manganese ug/L ND 5.0 07/13/21 15:47 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3323427LABORATORY CONTROL SAMPLE: LCSSpike Arsenic ug/L 485500 97 85-115 Barium ug/L 497500 99 85-115 Chromium ug/L 493500 99 85-115 Iron ug/L 50105000 100 85-115 Lead ug/L 490500 98 85-115 Manganese ug/L 487500 97 85-115 Parameter Units MS Result % Rec Limits Qual% RecConc. 3323428MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92548091001 3323429 MSD Result MSD % Rec RPD MSDMS Spike Conc. Arsenic ug/L 500 99 70-13099 0500ND494495 Barium ug/L 500 99 70-130100 0500108606607 Chromium ug/L 500 99 70-130100 1500ND495500 Iron ug/L 5000 96 70-130100 15000171002190022100 Lead ug/L 500 97 70-13099 1500ND489495 Manganese ug/L 500 95 70-130102 1500241028802920 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 26 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 633318 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 200.7 MET Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92548091006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3326476 Associated Lab Samples:92548091006 Matrix:Water Analyzed Arsenic ug/L ND 10.0 07/14/21 21:59 Barium ug/L ND 5.0 07/14/21 21:59 Chromium ug/L ND 5.0 07/14/21 21:59 Iron ug/L ND 50.0 07/14/21 21:59 Lead ug/L ND 5.0 07/14/21 21:59 Manganese ug/L ND 5.0 07/14/21 21:59 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3326477LABORATORY CONTROL SAMPLE: LCSSpike Arsenic ug/L 458500 92 85-115 Barium ug/L 495500 99 85-115 Chromium ug/L 513500 103 85-115 Iron ug/L 49205000 98 85-115 Lead ug/L 483500 97 85-115 Manganese ug/L 483500 97 85-115 Parameter Units MS Result % Rec Limits Qual% RecConc. 3326478MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92548091006 3326479 MSD Result MSD % Rec RPD MSDMS Spike Conc. Arsenic ug/L 500 88 70-13089 1500ND442446 Barium ug/L 500 95 70-13096 050053.2 530 531 Chromium ug/L 500 99 70-13099 0500ND495494 Iron ug/L 5000 98 70-13098 0500062.3 4970 4960 Lead ug/L 500 93 70-13092 1500ND464461 Manganese ug/L 500 93 70-13093 0500ND465467 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 27 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 632168 SM 6200B SM 6200B 6200B MSV Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3320736 Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 0.50 07/09/21 12:32 1,1,1-Trichloroethane ug/L ND 0.50 07/09/21 12:32 1,1,2,2-Tetrachloroethane ug/L ND 0.50 07/09/21 12:32 1,1,2-Trichloroethane ug/L ND 0.50 07/09/21 12:32 1,1-Dichloroethane ug/L ND 0.50 07/09/21 12:32 1,1-Dichloroethene ug/L ND 0.50 07/09/21 12:32 1,1-Dichloropropene ug/L ND 0.50 07/09/21 12:32 1,2,3-Trichlorobenzene ug/L ND 2.0 07/09/21 12:32 1,2,3-Trichloropropane ug/L ND 0.50 07/09/21 12:32 1,2,4-Trichlorobenzene ug/L ND 2.0 07/09/21 12:32 1,2,4-Trimethylbenzene ug/L ND 0.50 07/09/21 12:32 1,2-Dibromo-3-chloropropane ug/L ND 1.0 07/09/21 12:32 1,2-Dibromoethane (EDB)ug/L ND 0.50 07/09/21 12:32 1,2-Dichlorobenzene ug/L ND 0.50 07/09/21 12:32 1,2-Dichloroethane ug/L ND 0.50 07/09/21 12:32 1,2-Dichloropropane ug/L ND 0.50 07/09/21 12:32 1,3,5-Trimethylbenzene ug/L ND 0.50 07/09/21 12:32 1,3-Dichlorobenzene ug/L ND 0.50 07/09/21 12:32 1,3-Dichloropropane ug/L ND 0.50 07/09/21 12:32 1,4-Dichlorobenzene ug/L ND 0.50 07/09/21 12:32 2,2-Dichloropropane ug/L ND 0.50 07/09/21 12:32 2-Chlorotoluene ug/L ND 0.50 07/09/21 12:32 4-Chlorotoluene ug/L ND 0.50 07/09/21 12:32 Benzene ug/L ND 0.50 07/09/21 12:32 Bromobenzene ug/L ND 0.50 07/09/21 12:32 Bromochloromethane ug/L ND 0.50 07/09/21 12:32 Bromodichloromethane ug/L ND 0.50 07/09/21 12:32 Bromoform ug/L ND 0.50 07/09/21 12:32 Bromomethane ug/L ND 5.0 07/09/21 12:32 Carbon tetrachloride ug/L ND 0.50 07/09/21 12:32 Chlorobenzene ug/L ND 0.50 07/09/21 12:32 Chloroethane ug/L ND 1.0 07/09/21 12:32 Chloroform ug/L ND 0.50 07/09/21 12:32 Chloromethane ug/L ND 1.0 07/09/21 12:32 cis-1,2-Dichloroethene ug/L ND 0.50 07/09/21 12:32 cis-1,3-Dichloropropene ug/L ND 0.50 07/09/21 12:32 Dibromochloromethane ug/L ND 0.50 07/09/21 12:32 Dibromomethane ug/L ND 0.50 07/09/21 12:32 Dichlorodifluoromethane ug/L ND 0.50 07/09/21 12:32 Diisopropyl ether ug/L ND 0.50 07/09/21 12:32 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 28 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3320736 Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Matrix:Water Analyzed Ethylbenzene ug/L ND 0.50 07/09/21 12:32 Hexachloro-1,3-butadiene ug/L ND 2.0 07/09/21 12:32 Isopropylbenzene (Cumene)ug/L ND 0.50 07/09/21 12:32 m&p-Xylene ug/L ND 1.0 07/09/21 12:32 Methyl-tert-butyl ether ug/L ND 0.50 07/09/21 12:32 Methylene Chloride ug/L ND 2.0 07/09/21 12:32 n-Butylbenzene ug/L ND 0.50 07/09/21 12:32 n-Propylbenzene ug/L ND 0.50 07/09/21 12:32 Naphthalene ug/L ND 2.0 07/09/21 12:32 o-Xylene ug/L ND 0.50 07/09/21 12:32 sec-Butylbenzene ug/L ND 0.50 07/09/21 12:32 Styrene ug/L ND 0.50 07/09/21 12:32 tert-Butylbenzene ug/L ND 0.50 07/09/21 12:32 Tetrachloroethene ug/L ND 0.50 07/09/21 12:32 Toluene ug/L ND 0.50 07/09/21 12:32 trans-1,2-Dichloroethene ug/L ND 0.50 07/09/21 12:32 trans-1,3-Dichloropropene ug/L ND 0.50 07/09/21 12:32 Trichloroethene ug/L ND 0.50 07/09/21 12:32 Trichlorofluoromethane ug/L ND 1.0 07/09/21 12:32 Vinyl chloride ug/L ND 1.0 07/09/21 12:32 1,2-Dichloroethane-d4 (S)%111 70-130 07/09/21 12:32 4-Bromofluorobenzene (S)%99 70-130 07/09/21 12:32 Toluene-d8 (S)%100 70-130 07/09/21 12:32 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3320737LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 56.650 113 60-140 1,1,1-Trichloroethane ug/L 51.650 103 60-140 1,1,2,2-Tetrachloroethane ug/L 50.050 100 60-140 1,1,2-Trichloroethane ug/L 51.450 103 60-140 1,1-Dichloroethane ug/L 49.050 98 60-140 1,1-Dichloroethene ug/L 49.550 99 60-140 1,1-Dichloropropene ug/L 50.550 101 60-140 1,2,3-Trichlorobenzene ug/L 52.550 105 60-140 1,2,3-Trichloropropane ug/L 53.650 107 60-140 1,2,4-Trichlorobenzene ug/L 52.750 105 60-140 1,2,4-Trimethylbenzene ug/L 52.250 104 60-140 1,2-Dibromo-3-chloropropane ug/L 54.350 109 60-140 1,2-Dibromoethane (EDB)ug/L 54.550 109 60-140 1,2-Dichlorobenzene ug/L 49.650 99 60-140 1,2-Dichloroethane ug/L 48.650 97 60-140 1,2-Dichloropropane ug/L 48.850 98 60-140 1,3,5-Trimethylbenzene ug/L 52.150 104 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 29 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3320737LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichlorobenzene ug/L 49.450 99 60-140 1,3-Dichloropropane ug/L 52.150 104 60-140 1,4-Dichlorobenzene ug/L 50.550 101 60-140 2,2-Dichloropropane ug/L 52.950 106 60-140 2-Chlorotoluene ug/L 50.350 101 60-140 4-Chlorotoluene ug/L 50.250 100 60-140 Benzene ug/L 47.950 96 60-140 Bromobenzene ug/L 49.450 99 60-140 Bromochloromethane ug/L 49.950 100 60-140 Bromodichloromethane ug/L 53.950 108 60-140 Bromoform ug/L 64.850 130 60-140 Bromomethane ug/L 69.550 139 60-140 Carbon tetrachloride ug/L 57.750 115 60-140 Chlorobenzene ug/L 52.150 104 60-140 Chloroethane ug/L 51.250 102 60-140 Chloroform ug/L 51.450 103 60-140 Chloromethane ug/L 58.050 116 60-140 cis-1,2-Dichloroethene ug/L 48.450 97 60-140 cis-1,3-Dichloropropene ug/L 53.650 107 60-140 Dibromochloromethane ug/L 59.750 119 60-140 Dibromomethane ug/L 48.250 96 60-140 Dichlorodifluoromethane ug/L 52.150 104 60-140 Diisopropyl ether ug/L 50.950 102 60-140 Ethylbenzene ug/L 51.550 103 60-140 Hexachloro-1,3-butadiene ug/L 54.850 110 60-140 Isopropylbenzene (Cumene)ug/L 52.950 106 60-140 m&p-Xylene ug/L 104100 104 60-140 Methyl-tert-butyl ether ug/L 51.250 102 60-140 Methylene Chloride ug/L 51.650 103 60-140 n-Butylbenzene ug/L 52.850 106 60-140 n-Propylbenzene ug/L 50.650 101 60-140 Naphthalene ug/L 51.550 103 60-140 o-Xylene ug/L 51.950 104 60-140 sec-Butylbenzene ug/L 50.150 100 60-140 Styrene ug/L 51.750 103 60-140 tert-Butylbenzene ug/L 44.050 88 60-140 Tetrachloroethene ug/L 52.650 105 60-140 Toluene ug/L 47.550 95 60-140 trans-1,2-Dichloroethene ug/L 50.650 101 60-140 trans-1,3-Dichloropropene ug/L 57.350 115 60-140 Trichloroethene ug/L 48.350 97 60-140 Trichlorofluoromethane ug/L 50.850 102 60-140 Vinyl chloride ug/L 50.650 101 60-140 1,2-Dichloroethane-d4 (S)%108 70-130 4-Bromofluorobenzene (S)%103 70-130 Toluene-d8 (S)%98 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 30 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3320738MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92547837012 3320739 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 5000 117 60-140120 35000ND58406000 1,1,1-Trichloroethane ug/L 5000 115 60-140118 25000ND57505890 1,1,2,2-Tetrachloroethane ug/L 5000 103 60-140107 55000ND51305370 1,1,2-Trichloroethane ug/L 5000 106 60-140111 55000ND52905560 1,1-Dichloroethane ug/L 5000 106 60-140109 35000ND53005430 1,1-Dichloroethene ug/L 5000 109 60-140110 05000ND54505480 1,1-Dichloropropene ug/L 5000 104 60-140107 35000ND52205360 1,2,3-Trichlorobenzene ug/L 5000 99 60-140105 65000ND49505270 1,2,3-Trichloropropane ug/L 5000 108 60-140109 15000ND53905440 1,2,4-Trichlorobenzene ug/L 5000 96 60-140101 55000ND48205070 1,2,4-Trimethylbenzene ug/L 5000 110 60-140112 25000177072607380 1,2-Dibromo-3-chloropropane ug/L 5000 111 60-140113 15000ND55505630 1,2-Dibromoethane (EDB)ug/L 5000 108 60-140110 25000ND53905500 1,2-Dichlorobenzene ug/L 5000 105 60-140108 35000ND52605410 1,2-Dichloroethane ug/L 5000 103 60-140109 55000ND51505430 1,2-Dichloropropane ug/L 5000 106 60-140109 35000ND53005470 1,3,5-Trimethylbenzene ug/L 5000 120 60-140121 15000ND60106050 1,3-Dichlorobenzene ug/L 5000 102 60-140106 45000ND50805310 1,3-Dichloropropane ug/L 5000 108 60-140111 25000ND54005530 1,4-Dichlorobenzene ug/L 5000 105 60-140105 15000ND52405270 2,2-Dichloropropane ug/L 5000 73 60-14072 15000ND36303600 2-Chlorotoluene ug/L 5000 109 60-140113 35000ND54605640 4-Chlorotoluene ug/L 5000 106 60-140108 35000ND52805420 Benzene ug/L 5000 105 60-140109 2500069001210012300 Bromobenzene ug/L 5000 109 60-140108 15000ND54605390 Bromochloromethane ug/L 5000 107 60-140112 55000ND53305590 Bromodichloromethane ug/L 5000 114 60-140117 25000ND57005840 Bromoform ug/L 5000 122 60-140125 35000ND60906260 Bromomethane ug/L M1500022960-140201 135000ND1150010000 Carbon tetrachloride ug/L 5000 126 60-140126 05000ND63006320 Chlorobenzene ug/L 5000 109 60-140112 35000ND54405620 Chloroethane ug/L 5000 119 60-140118 15000ND59505890 Chloroform ug/L 5000 112 60-140114 25000ND56005700 Chloromethane ug/L 5000 117 60-140120 35000ND58306010 cis-1,2-Dichloroethene ug/L 5000 105 60-140108 35000ND52505390 cis-1,3-Dichloropropene ug/L 5000 103 60-140105 35000ND51305260 Dibromochloromethane ug/L 5000 121 60-140119 15000ND60405970 Dibromomethane ug/L 5000 104 60-140106 25000ND51905310 Dichlorodifluoromethane ug/L 5000 95 60-14095 05000ND47604740 Diisopropyl ether ug/L 5000 109 60-140111 15000288083208420 Ethylbenzene ug/L 5000 110 60-140114 25000229078107980 Hexachloro-1,3-butadiene ug/L 5000 95 60-140106 115000ND47505290 Isopropylbenzene (Cumene)ug/L 5000 114 60-140115 05000ND57005730 m&p-Xylene ug/L 10000 107 60-140112 21000082901900019500 Methyl-tert-butyl ether ug/L 5000 106 60-140112 5500042257406030 Methylene Chloride ug/L 5000 121 60-140125 35000ND60706250 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 31 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3320738MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92547837012 3320739 MSD Result MSD % Rec RPD MSDMS Spike Conc. n-Butylbenzene ug/L 5000 99 60-140105 65000ND49705270 n-Propylbenzene ug/L 5000 105 60-140108 2500019454705580 Naphthalene ug/L 5000 101 60-140108 6500060556305990 o-Xylene ug/L 5000 109 60-140114 35000423096809930 sec-Butylbenzene ug/L 5000 105 60-140108 35000ND52405420 Styrene ug/L 5000 111 60-140113 25000ND55405670 tert-Butylbenzene ug/L 5000 96 60-140100 45000ND48105010 Tetrachloroethene ug/L 5000 102 60-140105 35000ND50905250 Toluene ug/L 5000 89 60-140100 25000291003360034100 trans-1,2-Dichloroethene ug/L 5000 107 60-140107 05000ND53605370 trans-1,3-Dichloropropene ug/L 5000 109 60-140108 05000ND54505420 Trichloroethene ug/L 5000 105 60-140105 05000ND52305230 Trichlorofluoromethane ug/L 5000 115 60-140113 25000ND57405640 Vinyl chloride ug/L 5000 111 60-140110 15000ND55605490 1,2-Dichloroethane-d4 (S)%104 70-130106 4-Bromofluorobenzene (S)%101 70-130102 Toluene-d8 (S)%98 70-130101 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 32 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 632787 SM 2540C-2011 SM 2540C-2011 2540C Total Dissolved Solids Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92548091002 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3324115 Associated Lab Samples:92548091002 Matrix:Water Analyzed Total Dissolved Solids mg/L ND 25.0 07/12/21 16:33 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3324116LABORATORY CONTROL SAMPLE: LCSSpike Total Dissolved Solids mg/L 242250 97 90-110 Parameter Units Dup Result QualifiersRPDResult 92548368002 3324117SAMPLE DUPLICATE: Total Dissolved Solids mg/L 538 7503 Parameter Units Dup Result QualifiersRPDResult 92548021001 3324118SAMPLE DUPLICATE: Total Dissolved Solids mg/L 377 1373 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 33 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 632625 SM 4500-H+B-2011 SM 4500-H+B-2011 4500H+B pH Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Parameter Units Dup Result QualifiersRPDResult 92547561001 3323242SAMPLE DUPLICATE: pH at 25 Degrees C Std. Units 6.1 D6,H356.4 Parameter Units Dup Result QualifiersRPDResult 92548091001 3323243SAMPLE DUPLICATE: pH at 25 Degrees C Std. Units 6.4 H316.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 34 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 632325 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 300.0 IC Anions Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3321618 Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Matrix:Water Analyzed Sulfate mg/L ND 1.0 07/09/21 10:28 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3321619LABORATORY CONTROL SAMPLE: LCSSpike Sulfate mg/L 48.150 96 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3321620MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92548021001 3321621 MSD Result MSD % Rec RPD MSDMS Spike Conc. Sulfate mg/L 50 93 90-11091 15082.1 129 128 Parameter Units MS Result % Rec Limits Qual% RecConc. 3321622MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92548228001 3321623 MSD Result MSD % Rec RPD MSDMS Spike Conc. Sulfate mg/L 50 99 90-11099 0501.2 50.7 50.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 35 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 632324 EPA 350.1 Rev 2.0 1993 EPA 350.1 Rev 2.0 1993 350.1 Ammonia Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3321612 Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Matrix:Water Analyzed Nitrogen, Ammonia mg/L ND 0.10 07/09/21 14:31 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3321613LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Ammonia mg/L 5.05 99 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3321614MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92547911003 3321615 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Ammonia mg/L 5 100 90-110100 05ND5.0 5.0 Parameter Units MS Result % Rec Limits Qual% RecConc. 3321616MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92547912001 3321617 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Ammonia mg/L 5 100 90-110101 152.4 7.4 7.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 36 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 632467 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 351.2 TKN Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3322359 Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Matrix:Water Analyzed Nitrogen, Kjeldahl, Total mg/L ND 0.50 07/10/21 05:00 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3322360LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Kjeldahl, Total mg/L 9.210 92 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3322361MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92548039009 3322362 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Kjeldahl, Total mg/L M11015390-110152 01048.3 63.5 63.5 Parameter Units MS Result % Rec Limits Qual% RecConc. 3322367MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92548086001 3322368 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Kjeldahl, Total mg/L M1,R1107690-11098 2510ND7.8 10.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 37 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 632012 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 353.2 Nitrate + Nitrite, Unpres. Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3320069 Associated Lab Samples:92548091001, 92548091002, 92548091003, 92548091004, 92548091005, 92548091006, 92548091007 Matrix:Water Analyzed Nitrogen, Nitrate mg/L ND 0.040 07/08/21 00:04 Nitrogen, Nitrite mg/L ND 0.040 07/08/21 00:04 Nitrogen, NO2 plus NO3 mg/L ND 0.040 07/08/21 00:04 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3320070LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Nitrate mg/L 1.61.5 107 90-110 Nitrogen, Nitrite mg/L 1.01 100 90-110 Nitrogen, NO2 plus NO3 mg/L 2.62.5 104 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3320071MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92548039003 3320072 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Nitrate mg/L 1.5 111 90-110111 11.5ND 1.7 1.7 Nitrogen, Nitrite mg/L 1 102 90-110101 010.072 1.1 1.1 Nitrogen, NO2 plus NO3 mg/L 2.5 108 90-110107 12.50.066 2.8 2.7 Parameter Units MS Result % Rec Limits Qual% RecConc. 3320073MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92548101001 3320074 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Nitrate mg/L 1.5 219 90-110166 51.511.6 14.9 14.1 Nitrogen, Nitrite mg/L M11090-11001NDNDND Nitrogen, NO2 plus NO3 mg/L M12.5 131 90-110100 52.511.6 14.9 14.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 38 of 44 #=QL# QUALIFIERS Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS The precision between the sample and sample duplicate exceeded laboratory control limits.D6 Sample was received or analysis requested beyond the recognized method holding time.H3 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than the blank or were below the reporting limit.P8 RPD value was outside control limits.R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 39 of 44 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92548091001 632691 632813MW-1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92548091002 632691 632813MW-2 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92548091003 632691 632813MW-3 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92548091004 632691 632813MW-4 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92548091005 632691 632813MW-6 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92548091006 633318 633427MW-7 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92548091007 632691 632813MW-8 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92548091001 632168MW-1 SM 6200B 92548091002 632168MW-2 SM 6200B 92548091003 632168MW-3 SM 6200B 92548091004 632168MW-4 SM 6200B 92548091005 632168MW-6 SM 6200B 92548091006 632168MW-7 SM 6200B 92548091007 632168MW-8 SM 6200B 92548091002 632787MW-2 SM 2540C-2011 92548091001 632625MW-1 SM 4500-H+B-2011 92548091002 632625MW-2 SM 4500-H+B-2011 92548091003 632625MW-3 SM 4500-H+B-2011 92548091004 632625MW-4 SM 4500-H+B-2011 92548091005 632625MW-6 SM 4500-H+B-2011 92548091006 632625MW-7 SM 4500-H+B-2011 92548091007 632625MW-8 SM 4500-H+B-2011 92548091001 632325MW-1 EPA 300.0 Rev 2.1 1993 92548091002 632325MW-2 EPA 300.0 Rev 2.1 1993 92548091003 632325MW-3 EPA 300.0 Rev 2.1 1993 92548091004 632325MW-4 EPA 300.0 Rev 2.1 1993 92548091005 632325MW-6 EPA 300.0 Rev 2.1 1993 92548091006 632325MW-7 EPA 300.0 Rev 2.1 1993 92548091007 632325MW-8 EPA 300.0 Rev 2.1 1993 92548091001 632324MW-1 EPA 350.1 Rev 2.0 1993 92548091002 632324MW-2 EPA 350.1 Rev 2.0 1993 92548091003 632324MW-3 EPA 350.1 Rev 2.0 1993 92548091004 632324MW-4 EPA 350.1 Rev 2.0 1993 92548091005 632324MW-6 EPA 350.1 Rev 2.0 1993 92548091006 632324MW-7 EPA 350.1 Rev 2.0 1993 92548091007 632324MW-8 EPA 350.1 Rev 2.0 1993 92548091001 632467 632583MW-1 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92548091002 632467 632583MW-2 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92548091003 632467 632583MW-3 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92548091004 632467 632583MW-4 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92548091005 632467 632583MW-6 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92548091006 632467 632583MW-7 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92548091007 632467 632583MW-8 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92548091001 632012MW-1 EPA 353.2 Rev 2.0 1993 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 40 of 44 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92548091 Blue Ridge Tissue Corp. MWs Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92548091002 632012MW-2 EPA 353.2 Rev 2.0 1993 92548091003 632012MW-3 EPA 353.2 Rev 2.0 1993 92548091004 632012MW-4 EPA 353.2 Rev 2.0 1993 92548091005 632012MW-6 EPA 353.2 Rev 2.0 1993 92548091006 632012MW-7 EPA 353.2 Rev 2.0 1993 92548091007 632012MW-8 EPA 353.2 Rev 2.0 1993 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 07/15/2021 10:55 AM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 41 of 44 Page 42 of 44 Page 43 of 44 Page 44 of 44