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HomeMy WebLinkAboutNC0006254_Groundwater Monitoring Report November 2021_20211118PO Box 604 ▪ Fletcher, NC 28732 ▪ Cell: 828-508-4510 November 18, 2021 Mr. Brett Laverty NCDEQ Division of Water Resources Asheville Regional Office 2090 US Highway 70 Swannanoa, NC 28778 RE: Groundwater Analytical Results – November 3, 2021 Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina Mr. Laverty: On November 3, 2021, Singleton Environmental, Inc. (SEI) visited the Blue Ridge Tissue site located at 1427 Yadkin River Road in Patterson, North Carolina, to collect groundwater samples from monitoring wells MW-1, MW-2, MW-3, MW-4, MW-6, MW-7 and MW-8. The depth to groundwater in the monitoring wells ranged from 6.26 feet in MW-4 to 51.55 feet in MW-2. Refer to Table 1 for all monitoring well groundwater depths and Figure 1 for all monitoring well locations. All groundwater samples, with the exception of MW-2, were collected using a peristaltic pump connected to a Horiba U52-2 water quality meter with a flow through cell to collect groundwater parameters (temperature, pH, specific conductivity, dissolved oxygen, ORP, and turbidity). Groundwater sample MW-2 was collected using a bailer once three well volumes were removed. Groundwater from the same bail as the sample was also poured into the flow cell to collect the approximate parameters. The groundwater samples were submitted on ice to Pace Analytical for the analysis of 8-RCRA Metals, pH, ammonia, TKN, sulfate, nitrogen, nitrite and nitrate. MW-2 was also analyzed for total dissolved solids (TDS) using EPA Method SM 2540C, and volatile organic compounds (VOCs) using EPA Method 6200B. The groundwater parameters for all samples are outlined in Table 2. The laboratory analysis of groundwater samples MW-1 detected levels of iron and manganese above the NCAC 2L groundwater standards. The laboratory analysis of MW-2 detected levels of arsenic, chromium, lead, barium, iron, manganese, and ammonia above the NCAC 2L groundwater standards. The laboratory analysis of groundwater samples MW-3 detected levels of iron, manganese and ammonia above the NCAC 2L groundwater standards. The laboratory analysis of groundwater samples MW-4 detected levels of iron and manganese above the NCAC 2L groundwater standards. Laboratory analysis of groundwater samples MW-6, MW-7, and MW- 8 did not detect any compounds exceeding the NCAC 2L groundwater standards. The analytical results are shown on attached Table 2 and the attached laboratory data sheets. During the April 2017 groundwater sampling event, AECOM reported a possible sheen on the groundwater in monitoring well MW-4. During the November 2021 event a sheen was not Singleton Environmental, Inc. Singleton Environmental, Inc. observed; however, a VOC sample was collected from each monitoring well and analyzed using EPA Method 6200B. None of the concentrations were detected above the minimum laboratory detection levels. The compound levels detected in the groundwater analysis for the November 2021 sampling event were higher than the July 2021 and March 2021 sampling events. Also note arsenic, lead, and chromium concentrations in MW-2 were detected at levels higher than in March 2021. Singleton Environmental, Inc. recommends sampling the monitoring wells again in March 2022. If you have any questions you can reach me at (828) 508-4510. Sincerely, Chris Singleton, P.G. Singleton Environmental, Inc. cc: Dave Hallock, Blue Ridge Tissue Corporation Attachments @A @A @A @A @A @A @A @A MW-2 MW-3 MW-4 MW-1 @A MW-5 MW-7 MW-6 MW-8 1 2 8 0 12601 3 2 0 1340 1360 1380 124014201240 1420 Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/AirbusDS, USDA, USGS, AEX, Getmapping, Aerogrid, IGN, IGP, swisstopo, and theGIS User Community Figure 60540673 1 May 2017 § 0 200 400Feet 1 inch = 200 feet Y a d k i n R i v e r R d Whisnant RdYad k i n R i v e r Yadkin R iver Roby Martin Rd#0 Site Layout MapBlue Ridge Tissue CorporationPatterson, North Carolina Legend Property Boundary Yadkin River Flow Direction #Land Surface Elevation Contour (ft above mean sea level) Monitoring Well Location Abandoned Water Well#0@A Well ID Date Installed Total Depth (feet bls) Screened Interval (feet bls) Top of Casing Elevation (feet msl) Date Water Level Measured Depth to Water (feet BTOC) Groundwater Elevation (feet msl) MW-1 02/08/11 11 6-11 1253.71 11/03/21 12.38 1,241.33 MW-2 08/12/09 50 40-50 1323.03 11/03/21 51.55 1,271.48 MW-3 08/13/09 20 10-20 1299.02 11/03/21 18.77 1,280.25 MW-4 08/13/09 15 5-15 1247.23 11/03/21 6.26 1,240.97 MW-5 08/16/11 21 11-21 1285.46 N/A N/A N/A MW-6 08/06/14 29 19-29 1341.55 11/03/21 29.05 1,312.50 MW-7 08/06/14 24 14-24 1274.41 11/03/21 20.15 1,254.26 MW-8 08/06/14 20 10-20 1253.14 11/03/21 15.22 1,237.92 Notes: bls - feet below land surface BTOC - below top of casing msl - above mean sea level NG - not gauged AECOM Table 1 Monitoring Well Construction and Groundwater Elevations Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina Sample ID MW-1 MW-2*MW-3 MW-4 MW-6 MW-7 MW-8 Sample Date 11/03/21 11/03/21 11/03/21 11/03/21 11/03/21 11/03/21 11/03/21 Temperature (°C)NS 15.5 N/A 15.09 12.78 14.40 11.65 15.62 pH (standard units)NS 7.06 N/A 6.79 6.25 5.35 5.64 5.89 Specific Conductivity (mS/cm)NS 0.52 N/A 0.746 0.383 0.029 0.113 0.11 Dissolved Oxygen (mg/L)NS 1.53 N/A 1.92 2.99 6.92 5.00 5.77 ORP (mV)NS -41.0 N/A -25.0 -6.0 252.0 164.0 197.0 Turbidity (NTU)NS 7.3 N/A 3.4 7.6 9.3 1.5 0.9 Gallons Pumped NS 2 1.00 3.5 2 3 1.75 2 Cloudy/Odor No/No No/No Cloudy/Odor Cloudy/Odor No/No No/No No/No No/No Total Barium (ug/L)700 258 3120 279 98.8 73.2 52.4 13.9 Total Iron (ug/L)300 26400 175000 37100 16000 ND ND ND Total Manganese (ug/L)50 4800 1160 4730 1570 14.8 ND ND Aresenic (ug/L)10 ND 50.8 ND ND ND ND ND Chromium (ug/L)10 ND 307 ND ND ND ND ND Lead (ug/L)15 ND 37.8 ND ND ND ND ND Sulfate N/A ND 1.6 18.3 12.1 ND 1.6 17.6 Amonia (mg/L)1.5 0.58 14.3 14.5 1.3 ND ND ND TKN (mg/L)N/A 0.93 17.8 17.1 1.8 ND ND ND Nitrogen NO2 plus NO3 (mg/L)N/A ND ND ND ND 0.045 1.1 2.4 Nitrate (mg/L)10 ND ND ND ND 0.045 1.1 2.4 Nitrite (mg/L)1 ND 0.092 0.06 ND ND ND ND pH (standard units)N/A 6.2 6.3 6.2 6.1 5 5.9 5.5 Total Disolved Solids (mg/L)N/A N/A 386 N/A N/A N/A N/A N/A EPA Method 6200B for VOCs N/A ND ND ND ND ND ND ND Notes: Samples analyzed for total and dissolved iron, barium and manganese by EPA Method 200.7 2L Standard - North Carolina groundwater quality standards established in Title 15A of the North Carolina Administrative Code, Subchapter 2L, Section 0.20 °C - degrees Celsius µS/cm - microsiemens per centimeter EPA - United States Environmental Protection Agency mg/L - milligrams per liter mV - millivolt NA - Not analyzed NS - No standard NTU - Nephelometric Turbidity Unit RCRA - Resource Conservation Recovery Act Bold samples indicate concentrations above the 2L Standard *MW-2 purged with disposable bailer, water quality parameters collected from same bail as sample. 2L Standard Field Parameters Analytical Parameters Table 2 Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina #=CL# November 11, 2021 LIMS USE: FR - CHRIS SINGLETON LIMS OBJECT ID: 92570488 92570488 Project: Pace Project No.: RE: Chris Singleton Singleton Environmental 105 Charlotte Highway Asheville, NC 28803 Blue Ridge Tissue Corp 11/3 Dear Chris Singleton: Enclosed are the analytical results for sample(s) received by the laboratory on November 03, 2021. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton lorri.patton@pacelabs.com Project Manager 1(828)254-7176 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 1 of 44 #=CP# CERTIFICATIONS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 2 of 44 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92570488001 MW-1 EPA 200.7 Rev 4.4 1994 6 PASI-ACBV SM 6200B 63 PASI-CNSCQ SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92570488002 MW-2 EPA 200.7 Rev 4.4 1994 6 PASI-ADS SM 6200B 63 PASI-CNSCQ SM 2540C-2015 1 PASI-AZMC SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92570488003 MW-3 EPA 200.7 Rev 4.4 1994 6 PASI-ACBV SM 6200B 63 PASI-CNSCQ SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92570488004 MW-4 EPA 200.7 Rev 4.4 1994 6 PASI-ACBV SM 6200B 63 PASI-CNSCQ SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92570488005 MW-6 EPA 200.7 Rev 4.4 1994 6 PASI-ACBV SM 6200B 63 PASI-CNSCQ SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92570488006 MW-7 EPA 200.7 Rev 4.4 1994 6 PASI-ACBV REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 3 of 44 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts SM 6200B 63 PASI-CNSCQ SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92570488007 MW-8 EPA 200.7 Rev 4.4 1994 6 PASI-ACBV SM 6200B 63 PASI-CNSCQ SM 4500-H+B-2011 1 PASI-ASMK EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-ANGP EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 4 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-1 Lab ID:92570488001 Collected:11/03/21 09:45 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 11/09/21 04:37 7440-38-211/05/21 10:0310.0 1 Barium 258 ug/L 11/09/21 04:37 7440-39-311/05/21 10:035.0 1 Chromium ND ug/L 11/09/21 04:37 7440-47-311/05/21 10:035.0 1 Iron 26400 ug/L 11/09/21 04:37 7439-89-611/05/21 10:0350.0 1 Lead ND ug/L 11/09/21 04:37 7439-92-111/05/21 10:035.0 1 Manganese 4800 ug/L 11/09/21 04:37 7439-96-511/05/21 10:035.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/05/21 05:08 71-43-20.50 1 Bromobenzene ND ug/L 11/05/21 05:08 108-86-10.50 1 Bromochloromethane ND ug/L 11/05/21 05:08 74-97-50.50 1 Bromodichloromethane ND ug/L 11/05/21 05:08 75-27-40.50 1 Bromoform ND ug/L 11/05/21 05:08 75-25-20.50 1 Bromomethane ND ug/L 11/05/21 05:08 74-83-95.0 1 n-Butylbenzene ND ug/L 11/05/21 05:08 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/05/21 05:08 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/05/21 05:08 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/05/21 05:08 56-23-50.50 1 Chlorobenzene ND ug/L 11/05/21 05:08 108-90-70.50 1 Chloroethane ND ug/L 11/05/21 05:08 75-00-31.0 1 Chloroform ND ug/L 11/05/21 05:08 67-66-30.50 1 Chloromethane ND ug/L 11/05/21 05:08 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/05/21 05:08 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/05/21 05:08 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/05/21 05:08 96-12-81.0 1 Dibromochloromethane ND ug/L 11/05/21 05:08 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/05/21 05:08 106-93-40.50 1 Dibromomethane ND ug/L 11/05/21 05:08 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/05/21 05:08 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/05/21 05:08 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/05/21 05:08 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/05/21 05:08 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/05/21 05:08 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/05/21 05:08 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/05/21 05:08 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/05/21 05:08 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/05/21 05:08 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/05/21 05:08 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/05/21 05:08 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/05/21 05:08 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/05/21 05:08 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/05/21 05:08 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/05/21 05:08 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/05/21 05:08 108-20-30.50 1 Ethylbenzene ND ug/L 11/05/21 05:08 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 5 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-1 Lab ID:92570488001 Collected:11/03/21 09:45 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/05/21 05:08 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/05/21 05:08 98-82-80.50 1 Methylene Chloride ND ug/L 11/05/21 05:08 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/05/21 05:08 1634-04-40.50 1 Naphthalene ND ug/L 11/05/21 05:08 91-20-32.0 1 n-Propylbenzene ND ug/L 11/05/21 05:08 103-65-10.50 1 Styrene ND ug/L 11/05/21 05:08 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/05/21 05:08 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/05/21 05:08 79-34-50.50 1 Tetrachloroethene ND ug/L 11/05/21 05:08 127-18-40.50 1 Toluene ND ug/L 11/05/21 05:08 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/05/21 05:08 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/05/21 05:08 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/05/21 05:08 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/05/21 05:08 79-00-50.50 1 Trichloroethene ND ug/L 11/05/21 05:08 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/05/21 05:08 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/05/21 05:08 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/05/21 05:08 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/05/21 05:08 108-67-80.50 1 Vinyl chloride ND ug/L 11/05/21 05:08 75-01-41.0 1 m&p-Xylene ND ug/L 11/05/21 05:08 179601-23-11.0 1 o-Xylene ND ug/L 11/05/21 05:08 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)98 %11/05/21 05:08 17060-07-070-130 1 4-Bromofluorobenzene (S)99 %11/05/21 05:08 460-00-470-130 1 Toluene-d8 (S)105 %11/05/21 05:08 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.2 Std. Units 11/07/21 13:07 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate ND mg/L 11/04/21 21:49 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 0.58 mg/L 11/05/21 10:25 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 0.93 mg/L 11/10/21 04:55 7727-37-911/09/21 19:390.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 6 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-1 Lab ID:92570488001 Collected:11/03/21 09:45 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 ND mg/L 11/04/21 00:210.40 10 Nitrogen, Nitrate ND mg/L 11/04/21 00:21 14797-55-80.40 10 Nitrogen, Nitrite ND mg/L 11/03/21 23:52 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 7 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-2 Lab ID:92570488002 Collected:11/03/21 11:15 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic 50.8 ug/L 11/10/21 12:47 7440-38-2 D311/05/21 10:0350.0 5 Barium 3120 ug/L 11/10/21 12:47 7440-39-3 D311/05/21 10:0325.0 5 Chromium 307 ug/L 11/10/21 12:47 7440-47-3 D311/05/21 10:0325.0 5 Iron 175000 ug/L 11/10/21 12:47 7439-89-611/05/21 10:032505 Lead 37.8 ug/L 11/10/21 12:47 7439-92-1 D311/05/21 10:0325.0 5 Manganese 1160 ug/L 11/10/21 12:47 7439-96-5 D311/05/21 10:0325.0 5 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/05/21 05:25 71-43-20.50 1 Bromobenzene ND ug/L 11/05/21 05:25 108-86-10.50 1 Bromochloromethane ND ug/L 11/05/21 05:25 74-97-50.50 1 Bromodichloromethane ND ug/L 11/05/21 05:25 75-27-40.50 1 Bromoform ND ug/L 11/05/21 05:25 75-25-20.50 1 Bromomethane ND ug/L 11/05/21 05:25 74-83-95.0 1 n-Butylbenzene ND ug/L 11/05/21 05:25 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/05/21 05:25 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/05/21 05:25 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/05/21 05:25 56-23-50.50 1 Chlorobenzene ND ug/L 11/05/21 05:25 108-90-70.50 1 Chloroethane ND ug/L 11/05/21 05:25 75-00-31.0 1 Chloroform ND ug/L 11/05/21 05:25 67-66-30.50 1 Chloromethane ND ug/L 11/05/21 05:25 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/05/21 05:25 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/05/21 05:25 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/05/21 05:25 96-12-81.0 1 Dibromochloromethane ND ug/L 11/05/21 05:25 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/05/21 05:25 106-93-40.50 1 Dibromomethane ND ug/L 11/05/21 05:25 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/05/21 05:25 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/05/21 05:25 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/05/21 05:25 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/05/21 05:25 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/05/21 05:25 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/05/21 05:25 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/05/21 05:25 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/05/21 05:25 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/05/21 05:25 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/05/21 05:25 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/05/21 05:25 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/05/21 05:25 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/05/21 05:25 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/05/21 05:25 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/05/21 05:25 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/05/21 05:25 108-20-30.50 1 Ethylbenzene ND ug/L 11/05/21 05:25 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 8 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-2 Lab ID:92570488002 Collected:11/03/21 11:15 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/05/21 05:25 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/05/21 05:25 98-82-80.50 1 Methylene Chloride ND ug/L 11/05/21 05:25 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/05/21 05:25 1634-04-40.50 1 Naphthalene ND ug/L 11/05/21 05:25 91-20-32.0 1 n-Propylbenzene ND ug/L 11/05/21 05:25 103-65-10.50 1 Styrene ND ug/L 11/05/21 05:25 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/05/21 05:25 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/05/21 05:25 79-34-50.50 1 Tetrachloroethene ND ug/L 11/05/21 05:25 127-18-40.50 1 Toluene ND ug/L 11/05/21 05:25 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/05/21 05:25 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/05/21 05:25 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/05/21 05:25 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/05/21 05:25 79-00-50.50 1 Trichloroethene ND ug/L 11/05/21 05:25 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/05/21 05:25 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/05/21 05:25 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/05/21 05:25 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/05/21 05:25 108-67-80.50 1 Vinyl chloride ND ug/L 11/05/21 05:25 75-01-41.0 1 m&p-Xylene ND ug/L 11/05/21 05:25 179601-23-11.0 1 o-Xylene ND ug/L 11/05/21 05:25 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)98 %11/05/21 05:25 17060-07-070-130 1 4-Bromofluorobenzene (S)99 %11/05/21 05:25 460-00-470-130 1 Toluene-d8 (S)106 %11/05/21 05:25 2037-26-570-130 1 Analytical Method: SM 2540C-2015 Pace Analytical Services - Asheville 2540C Total Dissolved Solids Total Dissolved Solids 386 mg/L 11/05/21 17:0025.0 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.3 Std. Units 11/07/21 13:19 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 1.6 mg/L 11/04/21 22:34 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 14.3 mg/L 11/05/21 10:50 7664-41-70.30 3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 9 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-2 Lab ID:92570488002 Collected:11/03/21 11:15 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 17.8 mg/L 11/10/21 04:56 7727-37-911/09/21 19:390.50 1 Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 ND mg/L 11/04/21 00:292.0 50 Nitrogen, Nitrate ND mg/L 11/04/21 00:29 14797-55-82.0 50 Nitrogen, Nitrite 0.092 mg/L 11/04/21 00:16 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 10 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-3 Lab ID:92570488003 Collected:11/03/21 10:40 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 11/09/21 04:43 7440-38-211/05/21 10:0310.0 1 Barium 279 ug/L 11/09/21 04:43 7440-39-311/05/21 10:035.0 1 Chromium ND ug/L 11/09/21 04:43 7440-47-311/05/21 10:035.0 1 Iron 37100 ug/L 11/09/21 04:43 7439-89-611/05/21 10:0350.0 1 Lead ND ug/L 11/09/21 04:43 7439-92-111/05/21 10:035.0 1 Manganese 4730 ug/L 11/09/21 04:43 7439-96-511/05/21 10:035.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/05/21 05:43 71-43-20.50 1 Bromobenzene ND ug/L 11/05/21 05:43 108-86-10.50 1 Bromochloromethane ND ug/L 11/05/21 05:43 74-97-50.50 1 Bromodichloromethane ND ug/L 11/05/21 05:43 75-27-40.50 1 Bromoform ND ug/L 11/05/21 05:43 75-25-20.50 1 Bromomethane ND ug/L 11/05/21 05:43 74-83-95.0 1 n-Butylbenzene ND ug/L 11/05/21 05:43 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/05/21 05:43 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/05/21 05:43 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/05/21 05:43 56-23-50.50 1 Chlorobenzene ND ug/L 11/05/21 05:43 108-90-70.50 1 Chloroethane ND ug/L 11/05/21 05:43 75-00-31.0 1 Chloroform ND ug/L 11/05/21 05:43 67-66-30.50 1 Chloromethane ND ug/L 11/05/21 05:43 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/05/21 05:43 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/05/21 05:43 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/05/21 05:43 96-12-81.0 1 Dibromochloromethane ND ug/L 11/05/21 05:43 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/05/21 05:43 106-93-40.50 1 Dibromomethane ND ug/L 11/05/21 05:43 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/05/21 05:43 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/05/21 05:43 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/05/21 05:43 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/05/21 05:43 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/05/21 05:43 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/05/21 05:43 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/05/21 05:43 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/05/21 05:43 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/05/21 05:43 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/05/21 05:43 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/05/21 05:43 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/05/21 05:43 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/05/21 05:43 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/05/21 05:43 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/05/21 05:43 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/05/21 05:43 108-20-30.50 1 Ethylbenzene ND ug/L 11/05/21 05:43 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 11 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-3 Lab ID:92570488003 Collected:11/03/21 10:40 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/05/21 05:43 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/05/21 05:43 98-82-80.50 1 Methylene Chloride ND ug/L 11/05/21 05:43 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/05/21 05:43 1634-04-40.50 1 Naphthalene ND ug/L 11/05/21 05:43 91-20-32.0 1 n-Propylbenzene ND ug/L 11/05/21 05:43 103-65-10.50 1 Styrene ND ug/L 11/05/21 05:43 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/05/21 05:43 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/05/21 05:43 79-34-50.50 1 Tetrachloroethene ND ug/L 11/05/21 05:43 127-18-40.50 1 Toluene ND ug/L 11/05/21 05:43 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/05/21 05:43 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/05/21 05:43 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/05/21 05:43 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/05/21 05:43 79-00-50.50 1 Trichloroethene ND ug/L 11/05/21 05:43 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/05/21 05:43 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/05/21 05:43 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/05/21 05:43 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/05/21 05:43 108-67-80.50 1 Vinyl chloride ND ug/L 11/05/21 05:43 75-01-41.0 1 m&p-Xylene ND ug/L 11/05/21 05:43 179601-23-11.0 1 o-Xylene ND ug/L 11/05/21 05:43 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)96 %11/05/21 05:43 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %11/05/21 05:43 460-00-470-130 1 Toluene-d8 (S)103 %11/05/21 05:43 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.2 Std. Units 11/07/21 13:13 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 18.3 mg/L 11/04/21 22:49 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 14.5 mg/L 11/05/21 10:51 7664-41-70.30 3 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 17.1 mg/L 11/10/21 04:57 7727-37-911/09/21 19:390.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 12 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-3 Lab ID:92570488003 Collected:11/03/21 10:40 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 ND mg/L 11/04/21 00:282.0 50 Nitrogen, Nitrate ND mg/L 11/04/21 00:28 14797-55-82.0 50 Nitrogen, Nitrite 0.060 mg/L 11/03/21 23:53 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 13 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-4 Lab ID:92570488004 Collected:11/03/21 13:10 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 11/09/21 04:46 7440-38-211/05/21 10:0310.0 1 Barium 98.8 ug/L 11/09/21 04:46 7440-39-311/05/21 10:035.0 1 Chromium ND ug/L 11/09/21 04:46 7440-47-311/05/21 10:035.0 1 Iron 16000 ug/L 11/09/21 04:46 7439-89-611/05/21 10:0350.0 1 Lead ND ug/L 11/09/21 04:46 7439-92-111/05/21 10:035.0 1 Manganese 1570 ug/L 11/09/21 04:46 7439-96-511/05/21 10:035.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/05/21 06:00 71-43-20.50 1 Bromobenzene ND ug/L 11/05/21 06:00 108-86-10.50 1 Bromochloromethane ND ug/L 11/05/21 06:00 74-97-50.50 1 Bromodichloromethane ND ug/L 11/05/21 06:00 75-27-40.50 1 Bromoform ND ug/L 11/05/21 06:00 75-25-20.50 1 Bromomethane ND ug/L 11/05/21 06:00 74-83-95.0 1 n-Butylbenzene ND ug/L 11/05/21 06:00 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/05/21 06:00 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/05/21 06:00 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/05/21 06:00 56-23-50.50 1 Chlorobenzene ND ug/L 11/05/21 06:00 108-90-70.50 1 Chloroethane ND ug/L 11/05/21 06:00 75-00-31.0 1 Chloroform ND ug/L 11/05/21 06:00 67-66-30.50 1 Chloromethane ND ug/L 11/05/21 06:00 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/05/21 06:00 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/05/21 06:00 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/05/21 06:00 96-12-81.0 1 Dibromochloromethane ND ug/L 11/05/21 06:00 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/05/21 06:00 106-93-40.50 1 Dibromomethane ND ug/L 11/05/21 06:00 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/05/21 06:00 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/05/21 06:00 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/05/21 06:00 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/05/21 06:00 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/05/21 06:00 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/05/21 06:00 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/05/21 06:00 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/05/21 06:00 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/05/21 06:00 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/05/21 06:00 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/05/21 06:00 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/05/21 06:00 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/05/21 06:00 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/05/21 06:00 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/05/21 06:00 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/05/21 06:00 108-20-30.50 1 Ethylbenzene ND ug/L 11/05/21 06:00 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 14 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-4 Lab ID:92570488004 Collected:11/03/21 13:10 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/05/21 06:00 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/05/21 06:00 98-82-80.50 1 Methylene Chloride ND ug/L 11/05/21 06:00 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/05/21 06:00 1634-04-40.50 1 Naphthalene ND ug/L 11/05/21 06:00 91-20-32.0 1 n-Propylbenzene ND ug/L 11/05/21 06:00 103-65-10.50 1 Styrene ND ug/L 11/05/21 06:00 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/05/21 06:00 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/05/21 06:00 79-34-50.50 1 Tetrachloroethene ND ug/L 11/05/21 06:00 127-18-40.50 1 Toluene ND ug/L 11/05/21 06:00 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/05/21 06:00 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/05/21 06:00 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/05/21 06:00 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/05/21 06:00 79-00-50.50 1 Trichloroethene ND ug/L 11/05/21 06:00 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/05/21 06:00 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/05/21 06:00 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/05/21 06:00 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/05/21 06:00 108-67-80.50 1 Vinyl chloride ND ug/L 11/05/21 06:00 75-01-41.0 1 m&p-Xylene ND ug/L 11/05/21 06:00 179601-23-11.0 1 o-Xylene ND ug/L 11/05/21 06:00 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)98 %11/05/21 06:00 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %11/05/21 06:00 460-00-470-130 1 Toluene-d8 (S)105 %11/05/21 06:00 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.1 Std. Units 11/07/21 13:42 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 12.1 mg/L 11/04/21 23:04 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 1.3 mg/L 11/05/21 10:30 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 1.8 mg/L 11/10/21 04:58 7727-37-911/09/21 19:390.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 15 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-4 Lab ID:92570488004 Collected:11/03/21 13:10 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 ND mg/L 11/04/21 00:180.20 5 Nitrogen, Nitrate ND mg/L 11/04/21 00:18 14797-55-80.20 5 Nitrogen, Nitrite ND mg/L 11/04/21 00:03 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 16 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-6 Lab ID:92570488005 Collected:11/03/21 12:10 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 11/09/21 04:49 7440-38-211/05/21 10:0310.0 1 Barium 73.2 ug/L 11/09/21 04:49 7440-39-311/05/21 10:035.0 1 Chromium ND ug/L 11/09/21 04:49 7440-47-311/05/21 10:035.0 1 Iron ND ug/L 11/09/21 04:49 7439-89-611/05/21 10:0350.0 1 Lead ND ug/L 11/09/21 04:49 7439-92-111/05/21 10:035.0 1 Manganese 14.8 ug/L 11/09/21 04:49 7439-96-511/05/21 10:035.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/05/21 06:18 71-43-20.50 1 Bromobenzene ND ug/L 11/05/21 06:18 108-86-10.50 1 Bromochloromethane ND ug/L 11/05/21 06:18 74-97-50.50 1 Bromodichloromethane ND ug/L 11/05/21 06:18 75-27-40.50 1 Bromoform ND ug/L 11/05/21 06:18 75-25-20.50 1 Bromomethane ND ug/L 11/05/21 06:18 74-83-95.0 1 n-Butylbenzene ND ug/L 11/05/21 06:18 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/05/21 06:18 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/05/21 06:18 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/05/21 06:18 56-23-50.50 1 Chlorobenzene ND ug/L 11/05/21 06:18 108-90-70.50 1 Chloroethane ND ug/L 11/05/21 06:18 75-00-31.0 1 Chloroform ND ug/L 11/05/21 06:18 67-66-30.50 1 Chloromethane ND ug/L 11/05/21 06:18 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/05/21 06:18 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/05/21 06:18 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/05/21 06:18 96-12-81.0 1 Dibromochloromethane ND ug/L 11/05/21 06:18 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/05/21 06:18 106-93-40.50 1 Dibromomethane ND ug/L 11/05/21 06:18 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/05/21 06:18 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/05/21 06:18 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/05/21 06:18 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/05/21 06:18 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/05/21 06:18 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/05/21 06:18 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/05/21 06:18 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/05/21 06:18 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/05/21 06:18 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/05/21 06:18 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/05/21 06:18 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/05/21 06:18 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/05/21 06:18 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/05/21 06:18 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/05/21 06:18 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/05/21 06:18 108-20-30.50 1 Ethylbenzene ND ug/L 11/05/21 06:18 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 17 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-6 Lab ID:92570488005 Collected:11/03/21 12:10 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/05/21 06:18 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/05/21 06:18 98-82-80.50 1 Methylene Chloride ND ug/L 11/05/21 06:18 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/05/21 06:18 1634-04-40.50 1 Naphthalene ND ug/L 11/05/21 06:18 91-20-32.0 1 n-Propylbenzene ND ug/L 11/05/21 06:18 103-65-10.50 1 Styrene ND ug/L 11/05/21 06:18 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/05/21 06:18 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/05/21 06:18 79-34-50.50 1 Tetrachloroethene ND ug/L 11/05/21 06:18 127-18-40.50 1 Toluene ND ug/L 11/05/21 06:18 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/05/21 06:18 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/05/21 06:18 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/05/21 06:18 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/05/21 06:18 79-00-50.50 1 Trichloroethene ND ug/L 11/05/21 06:18 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/05/21 06:18 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/05/21 06:18 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/05/21 06:18 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/05/21 06:18 108-67-80.50 1 Vinyl chloride ND ug/L 11/05/21 06:18 75-01-41.0 1 m&p-Xylene ND ug/L 11/05/21 06:18 179601-23-11.0 1 o-Xylene ND ug/L 11/05/21 06:18 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)100 %11/05/21 06:18 17060-07-070-130 1 4-Bromofluorobenzene (S)99 %11/05/21 06:18 460-00-470-130 1 Toluene-d8 (S)105 %11/05/21 06:18 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 5.0 Std. Units 11/07/21 13:30 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate ND mg/L 11/04/21 23:19 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia ND mg/L 11/05/21 10:31 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 11/10/21 04:59 7727-37-911/09/21 19:390.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 18 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-6 Lab ID:92570488005 Collected:11/03/21 12:10 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 0.045 mg/L 11/04/21 00:010.040 1 Nitrogen, Nitrate 0.045 mg/L 11/04/21 00:01 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 11/04/21 00:01 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 19 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-7 Lab ID:92570488006 Collected:11/03/21 12:40 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 11/09/21 04:59 7440-38-211/05/21 10:0310.0 1 Barium 52.4 ug/L 11/09/21 04:59 7440-39-311/05/21 10:035.0 1 Chromium ND ug/L 11/09/21 04:59 7440-47-311/05/21 10:035.0 1 Iron ND ug/L 11/09/21 04:59 7439-89-611/05/21 10:0350.0 1 Lead ND ug/L 11/09/21 04:59 7439-92-111/05/21 10:035.0 1 Manganese ND ug/L 11/09/21 04:59 7439-96-511/05/21 10:035.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/05/21 06:36 71-43-20.50 1 Bromobenzene ND ug/L 11/05/21 06:36 108-86-10.50 1 Bromochloromethane ND ug/L 11/05/21 06:36 74-97-50.50 1 Bromodichloromethane ND ug/L 11/05/21 06:36 75-27-40.50 1 Bromoform ND ug/L 11/05/21 06:36 75-25-20.50 1 Bromomethane ND ug/L 11/05/21 06:36 74-83-95.0 1 n-Butylbenzene ND ug/L 11/05/21 06:36 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/05/21 06:36 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/05/21 06:36 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/05/21 06:36 56-23-50.50 1 Chlorobenzene ND ug/L 11/05/21 06:36 108-90-70.50 1 Chloroethane ND ug/L 11/05/21 06:36 75-00-31.0 1 Chloroform ND ug/L 11/05/21 06:36 67-66-30.50 1 Chloromethane ND ug/L 11/05/21 06:36 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/05/21 06:36 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/05/21 06:36 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/05/21 06:36 96-12-81.0 1 Dibromochloromethane ND ug/L 11/05/21 06:36 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/05/21 06:36 106-93-40.50 1 Dibromomethane ND ug/L 11/05/21 06:36 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/05/21 06:36 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/05/21 06:36 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/05/21 06:36 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/05/21 06:36 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/05/21 06:36 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/05/21 06:36 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/05/21 06:36 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/05/21 06:36 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/05/21 06:36 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/05/21 06:36 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/05/21 06:36 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/05/21 06:36 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/05/21 06:36 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/05/21 06:36 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/05/21 06:36 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/05/21 06:36 108-20-30.50 1 Ethylbenzene ND ug/L 11/05/21 06:36 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 20 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-7 Lab ID:92570488006 Collected:11/03/21 12:40 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/05/21 06:36 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/05/21 06:36 98-82-80.50 1 Methylene Chloride ND ug/L 11/05/21 06:36 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/05/21 06:36 1634-04-40.50 1 Naphthalene ND ug/L 11/05/21 06:36 91-20-32.0 1 n-Propylbenzene ND ug/L 11/05/21 06:36 103-65-10.50 1 Styrene ND ug/L 11/05/21 06:36 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/05/21 06:36 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/05/21 06:36 79-34-50.50 1 Tetrachloroethene ND ug/L 11/05/21 06:36 127-18-40.50 1 Toluene ND ug/L 11/05/21 06:36 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/05/21 06:36 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/05/21 06:36 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/05/21 06:36 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/05/21 06:36 79-00-50.50 1 Trichloroethene ND ug/L 11/05/21 06:36 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/05/21 06:36 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/05/21 06:36 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/05/21 06:36 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/05/21 06:36 108-67-80.50 1 Vinyl chloride ND ug/L 11/05/21 06:36 75-01-41.0 1 m&p-Xylene ND ug/L 11/05/21 06:36 179601-23-11.0 1 o-Xylene ND ug/L 11/05/21 06:36 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)98 %11/05/21 06:36 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %11/05/21 06:36 460-00-470-130 1 Toluene-d8 (S)105 %11/05/21 06:36 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 5.9 Std. Units 11/07/21 13:36 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 1.6 mg/L 11/04/21 23:34 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia ND mg/L 11/05/21 10:32 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 11/10/21 05:03 7727-37-911/09/21 19:390.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 21 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-7 Lab ID:92570488006 Collected:11/03/21 12:40 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 1.1 mg/L 11/04/21 00:020.040 1 Nitrogen, Nitrate 1.1 mg/L 11/04/21 00:02 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 11/04/21 00:02 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 22 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-8 Lab ID:92570488007 Collected:11/03/21 11:40 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville 200.7 MET ICP Arsenic ND ug/L 11/09/21 05:02 7440-38-211/05/21 10:0310.0 1 Barium 13.9 ug/L 11/09/21 05:02 7440-39-311/05/21 10:035.0 1 Chromium ND ug/L 11/09/21 05:02 7440-47-311/05/21 10:035.0 1 Iron ND ug/L 11/09/21 05:02 7439-89-611/05/21 10:0350.0 1 Lead ND ug/L 11/09/21 05:02 7439-92-111/05/21 10:035.0 1 Manganese ND ug/L 11/09/21 05:02 7439-96-511/05/21 10:035.0 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/05/21 06:53 71-43-20.50 1 Bromobenzene ND ug/L 11/05/21 06:53 108-86-10.50 1 Bromochloromethane ND ug/L 11/05/21 06:53 74-97-50.50 1 Bromodichloromethane ND ug/L 11/05/21 06:53 75-27-40.50 1 Bromoform ND ug/L 11/05/21 06:53 75-25-20.50 1 Bromomethane ND ug/L 11/05/21 06:53 74-83-95.0 1 n-Butylbenzene ND ug/L 11/05/21 06:53 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/05/21 06:53 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/05/21 06:53 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/05/21 06:53 56-23-50.50 1 Chlorobenzene ND ug/L 11/05/21 06:53 108-90-70.50 1 Chloroethane ND ug/L 11/05/21 06:53 75-00-31.0 1 Chloroform ND ug/L 11/05/21 06:53 67-66-30.50 1 Chloromethane ND ug/L 11/05/21 06:53 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/05/21 06:53 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/05/21 06:53 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/05/21 06:53 96-12-81.0 1 Dibromochloromethane ND ug/L 11/05/21 06:53 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/05/21 06:53 106-93-40.50 1 Dibromomethane ND ug/L 11/05/21 06:53 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/05/21 06:53 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/05/21 06:53 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/05/21 06:53 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/05/21 06:53 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/05/21 06:53 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/05/21 06:53 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/05/21 06:53 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/05/21 06:53 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/05/21 06:53 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/05/21 06:53 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/05/21 06:53 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/05/21 06:53 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/05/21 06:53 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/05/21 06:53 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/05/21 06:53 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/05/21 06:53 108-20-30.50 1 Ethylbenzene ND ug/L 11/05/21 06:53 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 23 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-8 Lab ID:92570488007 Collected:11/03/21 11:40 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/05/21 06:53 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/05/21 06:53 98-82-80.50 1 Methylene Chloride ND ug/L 11/05/21 06:53 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/05/21 06:53 1634-04-40.50 1 Naphthalene ND ug/L 11/05/21 06:53 91-20-32.0 1 n-Propylbenzene ND ug/L 11/05/21 06:53 103-65-10.50 1 Styrene ND ug/L 11/05/21 06:53 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/05/21 06:53 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/05/21 06:53 79-34-50.50 1 Tetrachloroethene ND ug/L 11/05/21 06:53 127-18-40.50 1 Toluene ND ug/L 11/05/21 06:53 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/05/21 06:53 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/05/21 06:53 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/05/21 06:53 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/05/21 06:53 79-00-50.50 1 Trichloroethene ND ug/L 11/05/21 06:53 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/05/21 06:53 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/05/21 06:53 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/05/21 06:53 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/05/21 06:53 108-67-80.50 1 Vinyl chloride ND ug/L 11/05/21 06:53 75-01-41.0 1 m&p-Xylene ND ug/L 11/05/21 06:53 179601-23-11.0 1 o-Xylene ND ug/L 11/05/21 06:53 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)102 %11/05/21 06:53 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %11/05/21 06:53 460-00-470-130 1 Toluene-d8 (S)103 %11/05/21 06:53 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 5.5 Std. Units 11/07/21 13:25 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 17.6 mg/L 11/05/21 00:19 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia ND mg/L 11/05/21 10:34 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 11/10/21 05:04 7727-37-911/09/21 19:390.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 24 of 44 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Sample:MW-8 Lab ID:92570488007 Collected:11/03/21 11:40 Received:11/03/21 15:09 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 2.4 mg/L 11/04/21 00:000.040 1 Nitrogen, Nitrate 2.4 mg/L 11/04/21 00:00 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 11/04/21 00:00 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 25 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 657760 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 200.7 MET Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3447891 Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Matrix:Water Analyzed Arsenic ug/L ND 10.0 11/09/21 03:58 Barium ug/L ND 5.0 11/09/21 03:58 Chromium ug/L ND 5.0 11/09/21 03:58 Iron ug/L ND 50.0 11/09/21 03:58 Lead ug/L ND 5.0 11/09/21 03:58 Manganese ug/L ND 5.0 11/09/21 03:58 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3447892LABORATORY CONTROL SAMPLE: LCSSpike Arsenic ug/L 500500 100 85-115 Barium ug/L 508500 102 85-115 Chromium ug/L 507500 101 85-115 Iron ug/L 50705000 101 85-115 Lead ug/L 510500 102 85-115 Manganese ug/L 522500 104 85-115 Parameter Units MS Result % Rec Limits Qual% RecConc. 3447893MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570795003 3447894 MSD Result MSD % Rec RPD MSDMS Spike Conc. Arsenic ug/L 500 103 70-13096 7500ND515479 Barium ug/L 500 101 70-13093 750021.0 526 488 Chromium ug/L 500 104 70-13094 95005.4 523 476 Iron ug/L 5000 105 70-13095 85000123064605980 Lead ug/L 500 103 70-13094 850027.5 543 499 Manganese ug/L 500 104 70-13095 950036.1 558 511 Parameter Units MS Result % Rec Limits Qual% RecConc. 3447895MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570488005 3447896 MSD Result MSD % Rec RPD MSDMS Spike Conc. Arsenic ug/L 500 99 70-13097 2500ND497485 Barium ug/L 500 97 70-13096 150073.2 557 552 Chromium ug/L 500 101 70-13099 2500ND505495 Iron ug/L 5000 100 70-13099 25000ND50604970 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 26 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3447895MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570488005 3447896 MSD Result MSD % Rec RPD MSDMS Spike Conc. Lead ug/L 500 100 70-13098 3500ND504490 Manganese ug/L 500 103 70-130100 250014.8 529 516 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 27 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 657633 SM 6200B SM 6200B 6200B MSV Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3447341 Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/05/21 03:22 1,1,1-Trichloroethane ug/L ND 0.50 11/05/21 03:22 1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/05/21 03:22 1,1,2-Trichloroethane ug/L ND 0.50 11/05/21 03:22 1,1-Dichloroethane ug/L ND 0.50 11/05/21 03:22 1,1-Dichloroethene ug/L ND 0.50 11/05/21 03:22 1,1-Dichloropropene ug/L ND 0.50 11/05/21 03:22 1,2,3-Trichlorobenzene ug/L ND 2.0 11/05/21 03:22 1,2,3-Trichloropropane ug/L ND 0.50 11/05/21 03:22 1,2,4-Trichlorobenzene ug/L ND 2.0 11/05/21 03:22 1,2,4-Trimethylbenzene ug/L ND 0.50 11/05/21 03:22 1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/05/21 03:22 1,2-Dibromoethane (EDB)ug/L ND 0.50 11/05/21 03:22 1,2-Dichlorobenzene ug/L ND 0.50 11/05/21 03:22 1,2-Dichloroethane ug/L ND 0.50 11/05/21 03:22 1,2-Dichloropropane ug/L ND 0.50 11/05/21 03:22 1,3,5-Trimethylbenzene ug/L ND 0.50 11/05/21 03:22 1,3-Dichlorobenzene ug/L ND 0.50 11/05/21 03:22 1,3-Dichloropropane ug/L ND 0.50 11/05/21 03:22 1,4-Dichlorobenzene ug/L ND 0.50 11/05/21 03:22 2,2-Dichloropropane ug/L ND 0.50 11/05/21 03:22 2-Chlorotoluene ug/L ND 0.50 11/05/21 03:22 4-Chlorotoluene ug/L ND 0.50 11/05/21 03:22 Benzene ug/L ND 0.50 11/05/21 03:22 Bromobenzene ug/L ND 0.50 11/05/21 03:22 Bromochloromethane ug/L ND 0.50 11/05/21 03:22 Bromodichloromethane ug/L ND 0.50 11/05/21 03:22 Bromoform ug/L ND 0.50 11/05/21 03:22 Bromomethane ug/L ND 5.0 11/05/21 03:22 Carbon tetrachloride ug/L ND 0.50 11/05/21 03:22 Chlorobenzene ug/L ND 0.50 11/05/21 03:22 Chloroethane ug/L ND 1.0 11/05/21 03:22 Chloroform ug/L ND 0.50 11/05/21 03:22 Chloromethane ug/L ND 1.0 11/05/21 03:22 cis-1,2-Dichloroethene ug/L ND 0.50 11/05/21 03:22 cis-1,3-Dichloropropene ug/L ND 0.50 11/05/21 03:22 Dibromochloromethane ug/L ND 0.50 11/05/21 03:22 Dibromomethane ug/L ND 0.50 11/05/21 03:22 Dichlorodifluoromethane ug/L ND 0.50 11/05/21 03:22 Diisopropyl ether ug/L ND 0.50 11/05/21 03:22 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 28 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3447341 Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Matrix:Water Analyzed Ethylbenzene ug/L ND 0.50 11/05/21 03:22 Hexachloro-1,3-butadiene ug/L ND 2.0 11/05/21 03:22 Isopropylbenzene (Cumene)ug/L ND 0.50 11/05/21 03:22 m&p-Xylene ug/L ND 1.0 11/05/21 03:22 Methyl-tert-butyl ether ug/L ND 0.50 11/05/21 03:22 Methylene Chloride ug/L ND 2.0 11/05/21 03:22 n-Butylbenzene ug/L ND 0.50 11/05/21 03:22 n-Propylbenzene ug/L ND 0.50 11/05/21 03:22 Naphthalene ug/L ND 2.0 11/05/21 03:22 o-Xylene ug/L ND 0.50 11/05/21 03:22 sec-Butylbenzene ug/L ND 0.50 11/05/21 03:22 Styrene ug/L ND 0.50 11/05/21 03:22 tert-Butylbenzene ug/L ND 0.50 11/05/21 03:22 Tetrachloroethene ug/L ND 0.50 11/05/21 03:22 Toluene ug/L ND 0.50 11/05/21 03:22 trans-1,2-Dichloroethene ug/L ND 0.50 11/05/21 03:22 trans-1,3-Dichloropropene ug/L ND 0.50 11/05/21 03:22 Trichloroethene ug/L ND 0.50 11/05/21 03:22 Trichlorofluoromethane ug/L ND 1.0 11/05/21 03:22 Vinyl chloride ug/L ND 1.0 11/05/21 03:22 1,2-Dichloroethane-d4 (S)%96 70-130 11/05/21 03:22 4-Bromofluorobenzene (S)%99 70-130 11/05/21 03:22 Toluene-d8 (S)%106 70-130 11/05/21 03:22 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3447342LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 48.950 98 60-140 1,1,1-Trichloroethane ug/L 54.350 109 60-140 1,1,2,2-Tetrachloroethane ug/L 47.650 95 60-140 1,1,2-Trichloroethane ug/L 52.250 104 60-140 1,1-Dichloroethane ug/L 50.650 101 60-140 1,1-Dichloroethene ug/L 51.750 103 60-140 1,1-Dichloropropene ug/L 53.450 107 60-140 1,2,3-Trichlorobenzene ug/L 49.550 99 60-140 1,2,3-Trichloropropane ug/L 46.050 92 60-140 1,2,4-Trichlorobenzene ug/L 49.550 99 60-140 1,2,4-Trimethylbenzene ug/L 46.450 93 60-140 1,2-Dibromo-3-chloropropane ug/L 51.450 103 60-140 1,2-Dibromoethane (EDB)ug/L 50.350 101 60-140 1,2-Dichlorobenzene ug/L 45.250 90 60-140 1,2-Dichloroethane ug/L 50.850 102 60-140 1,2-Dichloropropane ug/L 51.650 103 60-140 1,3,5-Trimethylbenzene ug/L 47.650 95 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 29 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3447342LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichlorobenzene ug/L 46.350 93 60-140 1,3-Dichloropropane ug/L 49.450 99 60-140 1,4-Dichlorobenzene ug/L 46.450 93 60-140 2,2-Dichloropropane ug/L 50.350 101 60-140 2-Chlorotoluene ug/L 46.450 93 60-140 4-Chlorotoluene ug/L 45.150 90 60-140 Benzene ug/L 49.450 99 60-140 Bromobenzene ug/L 47.450 95 60-140 Bromochloromethane ug/L 52.250 104 60-140 Bromodichloromethane ug/L 50.250 100 60-140 Bromoform ug/L 50.450 101 60-140 Bromomethane ug/L 55.050 110 60-140 Carbon tetrachloride ug/L 53.850 108 60-140 Chlorobenzene ug/L 45.750 91 60-140 Chloroethane ug/L 48.650 97 60-140 Chloroform ug/L 50.250 100 60-140 Chloromethane ug/L 51.750 103 60-140 cis-1,2-Dichloroethene ug/L 49.150 98 60-140 cis-1,3-Dichloropropene ug/L 52.250 104 60-140 Dibromochloromethane ug/L 51.550 103 60-140 Dibromomethane ug/L 50.150 100 60-140 Dichlorodifluoromethane ug/L 54.350 109 60-140 Diisopropyl ether ug/L 52.950 106 60-140 Ethylbenzene ug/L 46.850 94 60-140 Hexachloro-1,3-butadiene ug/L 50.650 101 60-140 Isopropylbenzene (Cumene)ug/L 48.550 97 60-140 m&p-Xylene ug/L 93.9100 94 60-140 Methyl-tert-butyl ether ug/L 54.150 108 60-140 Methylene Chloride ug/L 49.550 99 60-140 n-Butylbenzene ug/L 47.250 94 60-140 n-Propylbenzene ug/L 46.650 93 60-140 Naphthalene ug/L 49.750 99 60-140 o-Xylene ug/L 47.150 94 60-140 sec-Butylbenzene ug/L 46.350 93 60-140 Styrene ug/L 48.850 98 60-140 tert-Butylbenzene ug/L 39.150 78 60-140 Tetrachloroethene ug/L 47.050 94 60-140 Toluene ug/L 46.950 94 60-140 trans-1,2-Dichloroethene ug/L 51.250 102 60-140 trans-1,3-Dichloropropene ug/L 51.050 102 60-140 Trichloroethene ug/L 50.650 101 60-140 Trichlorofluoromethane ug/L 47.350 95 60-140 Vinyl chloride ug/L 50.050 100 60-140 1,2-Dichloroethane-d4 (S)%96 70-130 4-Bromofluorobenzene (S)%100 70-130 Toluene-d8 (S)%99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 30 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3447343MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570540001 3447344 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 108 60-140103 520ND21.6 20.5 1,1,1-Trichloroethane ug/L 20 120 60-140122 220ND24.1 24.5 1,1,2,2-Tetrachloroethane ug/L 20 107 60-140104 420ND21.5 20.7 1,1,2-Trichloroethane ug/L 20 119 60-140117 120ND23.7 23.4 1,1-Dichloroethane ug/L 20 116 60-140116 020ND23.1 23.2 1,1-Dichloroethene ug/L 20 120 60-140121 120ND24.1 24.2 1,1-Dichloropropene ug/L 20 122 60-140126 320ND24.3 25.1 1,2,3-Trichlorobenzene ug/L 20 111 60-140113 220ND22.2 22.6 1,2,3-Trichloropropane ug/L 20 106 60-14097 920ND21.2 19.4 1,2,4-Trichlorobenzene ug/L 20 110 60-140109 120ND22.1 21.8 1,2,4-Trimethylbenzene ug/L 20 106 60-140106 020ND21.2 21.1 1,2-Dibromo-3-chloropropane ug/L 20 112 60-140109 320ND22.4 21.8 1,2-Dibromoethane (EDB)ug/L 20 112 60-140107 520ND22.4 21.4 1,2-Dichlorobenzene ug/L 20 104 60-140101 320ND20.8 20.3 1,2-Dichloroethane ug/L 20 112 60-140112 120ND22.3 22.5 1,2-Dichloropropane ug/L 20 118 60-140115 220ND23.6 23.1 1,3,5-Trimethylbenzene ug/L 20 108 60-140108 020ND21.6 21.7 1,3-Dichlorobenzene ug/L 20 104 60-140105 120ND20.9 21.0 1,3-Dichloropropane ug/L 20 111 60-140107 420ND22.3 21.4 1,4-Dichlorobenzene ug/L 20 106 60-140104 220ND21.3 20.9 2,2-Dichloropropane ug/L 20 125 60-140127 220ND25.0 25.4 2-Chlorotoluene ug/L 20 106 60-140106 120ND21.1 21.3 4-Chlorotoluene ug/L 20 102 60-140103 020ND20.5 20.5 Benzene ug/L 20 117 60-140114 320ND23.5 22.8 Bromobenzene ug/L 20 110 60-140110 020ND22.0 22.0 Bromochloromethane ug/L 20 119 60-140118 120ND23.9 23.7 Bromodichloromethane ug/L 20 111 60-140110 120ND22.2 22.0 Bromoform ug/L 20 105 60-140105 120ND21.1 20.9 Bromomethane ug/L 20 125 60-140129 320ND24.9 25.8 Carbon tetrachloride ug/L 20 127 60-140124 320ND25.4 24.8 Chlorobenzene ug/L 20 107 60-140104 220ND21.3 20.9 Chloroethane ug/L 20 124 60-140120 420ND24.8 23.9 Chloroform ug/L 20 115 60-140115 020ND23.0 23.0 Chloromethane ug/L 20 99 60-140100 120ND19.9 20.1 cis-1,2-Dichloroethene ug/L 20 114 60-140114 020ND22.7 22.8 cis-1,3-Dichloropropene ug/L 20 116 60-140114 220ND23.2 22.7 Dibromochloromethane ug/L 20 113 60-140108 420ND22.6 21.7 Dibromomethane ug/L 20 112 60-140112 020ND22.4 22.3 Dichlorodifluoromethane ug/L 20 115 60-140116 120ND23.0 23.1 Diisopropyl ether ug/L 20 114 60-140115 120ND22.7 23.0 Ethylbenzene ug/L 20 108 60-140106 120ND21.6 21.3 Hexachloro-1,3-butadiene ug/L 20 130 60-140131 020ND26.0 26.1 Isopropylbenzene (Cumene)ug/L 20 112 60-140107 420ND22.3 21.4 m&p-Xylene ug/L 40 106 60-140104 240ND42.5 41.5 Methyl-tert-butyl ether ug/L 20 117 60-140117 020ND23.4 23.3 Methylene Chloride ug/L 20 109 60-140110 120ND21.8 22.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 31 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3447343MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570540001 3447344 MSD Result MSD % Rec RPD MSDMS Spike Conc. n-Butylbenzene ug/L 20 112 60-140111 120ND22.4 22.2 n-Propylbenzene ug/L 20 109 60-140109 020ND21.8 21.8 Naphthalene ug/L 20 104 60-140105 020ND20.8 20.9 o-Xylene ug/L 20 104 60-140103 120ND20.8 20.6 sec-Butylbenzene ug/L 20 108 60-140107 220ND21.7 21.3 Styrene ug/L 20 108 60-140108 120ND21.6 21.5 tert-Butylbenzene ug/L 20 91 60-14090 120ND18.2 18.1 Tetrachloroethene ug/L 20 110 60-140104 520ND22.0 20.9 Toluene ug/L 20 111 60-140108 320ND22.2 21.5 trans-1,2-Dichloroethene ug/L 20 120 60-140122 120ND24.0 24.3 trans-1,3-Dichloropropene ug/L 20 113 60-140111 220ND22.6 22.2 Trichloroethene ug/L 20 118 60-140118 020ND23.7 23.6 Trichlorofluoromethane ug/L 20 110 60-140111 020ND22.1 22.1 Vinyl chloride ug/L 20 113 60-140115 220ND22.5 23.0 1,2-Dichloroethane-d4 (S)%95 70-13095 4-Bromofluorobenzene (S)%98 70-13098 Toluene-d8 (S)%100 70-13098 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 32 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 657951 SM 2540C-2015 SM 2540C-2015 2540C Total Dissolved Solids Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92570488002 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3448874 Associated Lab Samples:92570488002 Matrix:Water Analyzed Total Dissolved Solids mg/L ND 25.0 11/05/21 16:59 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3448875LABORATORY CONTROL SAMPLE: LCSSpike Total Dissolved Solids mg/L 254250 102 90-110 Parameter Units Dup Result QualifiersRPDResult 92570458031 3448876SAMPLE DUPLICATE: Total Dissolved Solids mg/L 255 0256 Parameter Units Dup Result QualifiersRPDResult 92570462001 3448877SAMPLE DUPLICATE: Total Dissolved Solids mg/L 366 0366 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 33 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 658098 SM 4500-H+B-2011 SM 4500-H+B-2011 4500H+B pH Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Parameter Units Dup Result QualifiersRPDResult 92570191001 3449532SAMPLE DUPLICATE: pH at 25 Degrees C Std. Units 6.0 D6,H346.3 Parameter Units Dup Result QualifiersRPDResult 92568941002 3449533SAMPLE DUPLICATE: pH at 25 Degrees C Std. Units 7.1 H307.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 34 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 657704 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 300.0 IC Anions Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3447750 Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Matrix:Water Analyzed Sulfate mg/L ND 1.0 11/04/21 21:19 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3447751LABORATORY CONTROL SAMPLE: LCSSpike Sulfate mg/L 47.450 95 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3447752MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570488001 3447753 MSD Result MSD % Rec RPD MSDMS Spike Conc. Sulfate mg/L 50 96 90-11099 350ND48.4 49.7 Parameter Units MS Result % Rec Limits Qual% RecConc. 3447754MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92569918004 3447755 MSD Result MSD % Rec RPD MSDMS Spike Conc. Sulfate mg/L 50 97 90-110100 3502.5 50.9 52.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 35 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 657750 EPA 350.1 Rev 2.0 1993 EPA 350.1 Rev 2.0 1993 350.1 Ammonia Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3447854 Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Matrix:Water Analyzed Nitrogen, Ammonia mg/L ND 0.10 11/05/21 10:03 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3447855LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Ammonia mg/L 5.05 101 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3447856MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570216003 3447857 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Ammonia mg/L 5 98 90-11098 05ND4.9 4.9 Parameter Units MS Result % Rec Limits Qual% RecConc. 3447858MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570425001 3447859 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Ammonia mg/L 5 102 90-110102 05ND5.1 5.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 36 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 658515 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 351.2 TKN Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3451393 Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Matrix:Water Analyzed Nitrogen, Kjeldahl, Total mg/L ND 0.50 11/10/21 04:39 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3451394LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Kjeldahl, Total mg/L 10.310 103 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3451395MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570215001 3451396 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Kjeldahl, Total mg/L M11012790-110129 2101.4 14.1 14.3 Parameter Units MS Result % Rec Limits Qual% RecConc. 3451397MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570215002 3451398 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Kjeldahl, Total mg/L M11012490-110118 510ND12.9 12.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 37 of 44 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 657377 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 353.2 Nitrate + Nitrite, Unpres. Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3446082 Associated Lab Samples:92570488001, 92570488002, 92570488003, 92570488004, 92570488005, 92570488006, 92570488007 Matrix:Water Analyzed Nitrogen, Nitrate mg/L ND 0.040 11/03/21 23:40 Nitrogen, Nitrite mg/L ND 0.040 11/03/21 23:40 Nitrogen, NO2 plus NO3 mg/L ND 0.040 11/03/21 23:40 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3446083LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Nitrate mg/L 1.51.5 102 90-110 Nitrogen, Nitrite mg/L 1.01 100 90-110 Nitrogen, NO2 plus NO3 mg/L 2.52.5 101 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3446084MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570265001 3446085 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Nitrate mg/L 1.5 123 90-110149 41.58.6 10.4 10.8 Nitrogen, Nitrite mg/L 1 103 90-110104 11ND1.0 1.0 Nitrogen, NO2 plus NO3 mg/L M12.5 115 90-110131 32.58.6 11.5 11.9 Parameter Units MS Result % Rec Limits Qual% RecConc. 3446086MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92570472002 3446087 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Nitrate mg/L 1.5 104 90-110103 11.5126 ug/L 1.7 1.7 Nitrogen, Nitrite mg/L 1 104 90-110104 01ND1.0 1.0 Nitrogen, NO2 plus NO3 mg/L 2.5 104 90-110104 02.50.13 2.7 2.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 38 of 44 #=QL# QUALIFIERS Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3 The precision between the sample and sample duplicate exceeded laboratory control limits.D6 Sample was received or analysis requested beyond the recognized method holding time.H3 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 39 of 44 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92570488001 657760 657898MW-1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92570488002 657760 657898MW-2 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92570488003 657760 657898MW-3 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92570488004 657760 657898MW-4 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92570488005 657760 657898MW-6 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92570488006 657760 657898MW-7 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92570488007 657760 657898MW-8 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994 92570488001 657633MW-1 SM 6200B 92570488002 657633MW-2 SM 6200B 92570488003 657633MW-3 SM 6200B 92570488004 657633MW-4 SM 6200B 92570488005 657633MW-6 SM 6200B 92570488006 657633MW-7 SM 6200B 92570488007 657633MW-8 SM 6200B 92570488002 657951MW-2 SM 2540C-2015 92570488001 658098MW-1 SM 4500-H+B-2011 92570488002 658098MW-2 SM 4500-H+B-2011 92570488003 658098MW-3 SM 4500-H+B-2011 92570488004 658098MW-4 SM 4500-H+B-2011 92570488005 658098MW-6 SM 4500-H+B-2011 92570488006 658098MW-7 SM 4500-H+B-2011 92570488007 658098MW-8 SM 4500-H+B-2011 92570488001 657704MW-1 EPA 300.0 Rev 2.1 1993 92570488002 657704MW-2 EPA 300.0 Rev 2.1 1993 92570488003 657704MW-3 EPA 300.0 Rev 2.1 1993 92570488004 657704MW-4 EPA 300.0 Rev 2.1 1993 92570488005 657704MW-6 EPA 300.0 Rev 2.1 1993 92570488006 657704MW-7 EPA 300.0 Rev 2.1 1993 92570488007 657704MW-8 EPA 300.0 Rev 2.1 1993 92570488001 657750MW-1 EPA 350.1 Rev 2.0 1993 92570488002 657750MW-2 EPA 350.1 Rev 2.0 1993 92570488003 657750MW-3 EPA 350.1 Rev 2.0 1993 92570488004 657750MW-4 EPA 350.1 Rev 2.0 1993 92570488005 657750MW-6 EPA 350.1 Rev 2.0 1993 92570488006 657750MW-7 EPA 350.1 Rev 2.0 1993 92570488007 657750MW-8 EPA 350.1 Rev 2.0 1993 92570488001 658515 658665MW-1 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92570488002 658515 658665MW-2 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92570488003 658515 658665MW-3 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92570488004 658515 658665MW-4 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92570488005 658515 658665MW-6 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92570488006 658515 658665MW-7 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92570488007 658515 658665MW-8 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92570488001 657377MW-1 EPA 353.2 Rev 2.0 1993 92570488002 657377MW-2 EPA 353.2 Rev 2.0 1993 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 40 of 44 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92570488 Blue Ridge Tissue Corp 11/3 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92570488003 657377MW-3 EPA 353.2 Rev 2.0 1993 92570488004 657377MW-4 EPA 353.2 Rev 2.0 1993 92570488005 657377MW-6 EPA 353.2 Rev 2.0 1993 92570488006 657377MW-7 EPA 353.2 Rev 2.0 1993 92570488007 657377MW-8 EPA 353.2 Rev 2.0 1993 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/11/2021 02:47 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 41 of 44 Page 42 of 44 Page 43 of 44 Page 44 of 44