NC0006254_Groundwater Monitoring Report March 2022_20220322

PO Box 604 ▪ Fletcher, NC 28732 ▪ Cell: 828-508-4510

March 22, 2022
Mr. Brett Laverty
NCDEQ Division of Water Resources
Asheville Regional Office
2090 US Highway 70
Swannanoa, NC 28778

RE: Groundwater Analytical Results – March 1, 2022
Blue Ridge Tissue Corporation
1427 Yadkin River Road
Patterson, North Carolina

Mr. Laverty:

On March 1, 2022, Singleton Environmental, Inc. (SEI) visited the Blue Ridge Tissue site located
at 1427 Yadkin River Road in Patterson, North Carolina, to collect groundwater samples from
monitoring wells MW-1, MW-2, MW-3, MW-4, MW-6, MW-7 and MW-8. The depth to
groundwater in the monitoring wells ranged from 5.27feet in MW-4 to 51.94 feet in MW-2. Refer
to Table 1 for all monitoring well groundwater depths and Figure 1 for all monitoring well
locations.

All groundwater samples, with the exception of MW-2 and MW-3, were collected using a
peristaltic pump connected to a Horiba U52-2 water quality meter with a flow through cell to
collect groundwater parameters (temperature, pH, specific conductivity, dissolved oxygen, ORP,
and turbidity). A groundwater sample MW-2 was not collected due to the water level being too
low for the pump or bailer to collect. Groundwater parameters in MW-3 did not stabilize prior to
sample collection due to the low groundwater level in the well causing it to purge dry after
multiple attempts. Later in the day a sample was collected after the well recharged just enough for
the pump to pull enough water to fill the sample containers.

The groundwater samples were submitted on ice to Pace Analytical for the analysis of 8-RCRA
Metals, pH, ammonia, TKN, sulfate, nitrogen, nitrite and nitrate. MW-3 was also analyzed for
total dissolved solids (TDS) using EPA Method SM 2540C. The groundwater parameters for all
samples are outlined in Table 2.

The laboratory analysis of groundwater sample MW-1 detected levels of total iron and total
manganese above the NCAC 2L groundwater standards, however, both compounds were lower
than the November 2022 sampling event.

A groundwater sample was not submitted for MW-2 due to the low groundwater elevation not
allowing either a bailer or pump to recover enough groundwater required for analysis.

The laboratory analysis of groundwater sample MW-3 detected levels of arsenic, total iron, total
manganese, and ammonia above the NCAC 2L groundwater standards. The total iron, arsenic, and
Singleton Environmental, Inc.
Singleton Environmental, Inc.
ammonia were detected at concentrations higher than the November 2022 event. The total
manganese was detected at a slightly lower concentration than November 2022 event.

The laboratory analysis of groundwater sample MW-4 detected levels of total iron and total
manganese above the NCAC 2L groundwater standards. The levels of total iron and total
manganese were significantly lower than the November 2022 event.

Laboratory analysis of groundwater samples MW-6, MW-7, and MW-8 did not detect any
compounds exceeding the NCAC 2L groundwater standards. The analytical results are shown on
attached Table 2 and the attached laboratory data sheets.

During the April 2017 groundwater sampling event, AECOM reported a possible sheen on the
groundwater in monitoring well MW-4. During the March 2022 event a sheen was not observed;
therefore, a VOC sample was not collected from the monitoring well.

The compound levels detected in the groundwater analysis for the March 2022 sampling event
detected relatively lower concentration levels of total iron and total manganese in monitoring wells
MW-1, MW-3, and MW-4. Monitoring well MW-3 did detect higher concentrations of total iron,
arsenic and ammonia.

Singleton Environmental, Inc. recommends sampling the monitoring wells again in July 2022 to
continue tracking the groundwater concentration and groundwater levels.

If you have any questions you can reach me at [phone].

Sincerely,

Chris Singleton, P.G.
Singleton Environmental, Inc.

cc: Dave Hallock, Blue Ridge Tissue Corporation

Attachments
@A
@A @A
@A
@A
@A
@A
@A
MW-2
MW-3
MW-4
MW-1
@A
MW-5
MW-7
MW-6
MW-8
1
2
8
0
12601
3
2
0
1340
1360
1380
124014201240
1420
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/AirbusDS, USDA, USGS, AEX, Getmapping, Aerogrid, IGN, IGP, swisstopo, and theGIS User Community
Figure
60540673
1
May 2017
§
0 200 400Feet
1 inch = 200 feet
Y
a
d
k
i
n

R
i
v
e
r

R
d
Whisnant RdYad
k
i
n

R
i
v
e
r
Yadkin
R
iver
Roby Martin Rd#0
Site Layout MapBlue Ridge Tissue CorporationPatterson, North Carolina
Legend
Property Boundary
Yadkin River Flow Direction
#Land Surface Elevation Contour (ft above mean sea level)
Monitoring Well Location
Abandoned Water Well#0@A
Well ID Date Installed Total Depth (feet
bls)
Screened Interval
(feet bls)
Top of Casing
Elevation (feet msl)
Date Water Level
Measured
Depth to Water (feet
BTOC)
Groundwater Elevation
(feet msl)
MW-1 02/08/11 11 6-11 1253.71 03/01/22 12.67 1,241.04
MW-2 08/12/09 50 40-50 1323.03 03/01/22 51.94 1,271.09
MW-3 08/13/09 20 10-20 1299.02 03/01/22 22.11 1,276.91
MW-4 08/13/09 15 5-15 1247.23 03/01/22 5.27 1,241.96
MW-5 08/16/11 21 11-21 1285.46 N/A N/A N/A
MW-6 08/06/14 29 19-29 1341.55 03/01/22 29.12 1,312.43
MW-7 08/06/14 24 14-24 1274.41 03/01/22 18.86 1,255.55
MW-8 08/06/14 20 10-20 1253.14 03/01/22 13.88 1,239.26
Notes:
bls - feet below land surface BTOC - below top of casing msl - above mean sea level NG - not gauged
AECOM
Table 1
Monitoring Well Construction and Groundwater Elevations
Blue Ridge Tissue Corporation
1427 Yadkin River Road
Patterson, North Carolina
Sample ID MW-1 MW-2*MW-3 MW-4 MW-6 MW-7 MW-8
Sample Date 03/01/22 03/01/22 03/01/22 03/01/22 03/01/22 03/01/22 03/01/22
Temperature (°C)NS 17.15 N/A N/A 22.22 19.30 24.70 19.10
pH (standard units)NS 5.99 N/A N/A 5.77 5.05 5.50 5.70
Specific Conductivity (mS/cm)NS 0.235 N/A N/A 0.277 0.051 0 0.164
Dissolved Oxygen (mg/L)NS 2.30 N/A N/A 0.42 4.80 7.04 4.90
ORP (mV)NS 17.0 N/A N/A 125.0 150.0 135.0 84.0
Turbidity (NTU)NS 5.2 N/A N/A 3.7 0 5.4 1.7
Gallons Pumped NS 2 N/A 1 3 1.5 2 2.5
Cloudy/Odor No/No No/No Cloudy/Odor Cloudy/Odor No/No No/No No/No No/No
Total Barium (ug/L)700 108 N/A 658 132 71 55.1 11.5
Total Iron (ug/L)300 13600 N/A 48700 1130 ND 71 ND
Total Manganese (ug/L)50 2100 N/A 4610 939 14.6 ND ND
Aresenic (ug/L)10 ND N/A 12 ND ND ND ND
Chromium (ug/L)10 ND N/A ND ND ND ND ND
Lead (ug/L)15 ND N/A ND ND ND ND ND
Sulfate N/A 1.6 N/A 21.4 36.4 ND 1.7 18
Ammonia (mg/L)1.5 0.29 N/A 14.8 1.5 ND ND ND
TKN (mg/L)N/A ND N/A 14.5 1.5 ND ND ND
Nitrogen NO2 plus NO3 (mg/L)N/A ND N/A ND 2.4 0.11 0.91 2.6
Nitrate (mg/L)10 ND N/A ND 2.3 0.11 0.91 2.6
Nitrite (mg/L)1 ND N/A 0.047 0.074 ND ND ND
pH (standard units)N/A 6.7 N/A 6.6 6.4 5.7 6.4 6.4
Total Disolved Solids (mg/L)N/A N/A N/A 356 N/A N/A N/A N/A
EPA Method 6200B for VOCs N/A N/A N/A N/A N/A N/A N/A N/A
Notes:
Samples analyzed for total and dissolved iron, barium and manganese by EPA Method 200.7
2L Standard - North Carolina groundwater quality standards established in Title 15A of the North Carolina Administrative Code, Subchapter 2L, Section 0.20
°C - degrees Celsius
µS/cm - microsiemens per centimeter
EPA - United States Environmental Protection Agency mg/L - milligrams per liter
mV - millivolt
NA - Not analyzed NS - No standard
NTU - Nephelometric Turbidity Unit
RCRA - Resource Conservation Recovery Act
Bold samples indicate concentrations above the 2L Standard
*MW-2 purged with disposable bailer, water quality parameters collected from same bail as sample.
2L
Standard
Field Parameters
Analytical Parameters
Table 2
Blue Ridge Tissue Corporation
1427 Yadkin River Road
Patterson, North Carolina
#=CL#
March 11, 2022
LIMS USE: FR - CHRIS SINGLETON
LIMS OBJECT ID: 92590781
92590781
Project:
Pace Project No.:
RE:
Chris Singleton
Singleton Environmental
105 Charlotte Highway
Asheville, NC 28803
Blue Ridge Tissue Corp
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on March 01, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Dyson for
[e-mail]
Project Manager
Lorri Patton
1(828)254-7176
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 24
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92590781001 MW-1 EPA 200.7 Rev 4.4 1994 6 PASI-ADS
SM 4500-H+B-2011 1 PASI-AYEG
EPA 300.0 Rev 2.1 1993 1 PASI-AJCM
EPA 350.1 Rev 2.0 1993 1 PASI-ASMS
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
92590781002 MW-3 EPA 200.7 Rev 4.4 1994 6 PASI-ADS
SM 2540C-2011 1 PASI-AMAB2
SM 4500-H+B-2011 1 PASI-AYEG
EPA 300.0 Rev 2.1 1993 1 PASI-AJCM
EPA 350.1 Rev 2.0 1993 1 PASI-ASMS
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
92590781003 MW-4 EPA 200.7 Rev 4.4 1994 6 PASI-ADS
SM 4500-H+B-2011 1 PASI-AYEG
EPA 300.0 Rev 2.1 1993 1 PASI-AJCM
EPA 350.1 Rev 2.0 1993 1 PASI-ASMS
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
92590781004 MW-6 EPA 200.7 Rev 4.4 1994 6 PASI-ADS
SM 4500-H+B-2011 1 PASI-AYEG
EPA 300.0 Rev 2.1 1993 1 PASI-AJCM
EPA 350.1 Rev 2.0 1993 1 PASI-ASMS
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
92590781005 MW-7 EPA 200.7 Rev 4.4 1994 6 PASI-ADS
SM 4500-H+B-2011 1 PASI-AYEG
EPA 300.0 Rev 2.1 1993 1 PASI-AJCM
EPA 350.1 Rev 2.0 1993 1 PASI-ASMS
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
92590781006 MW-8 EPA 200.7 Rev 4.4 1994 6 PASI-ADS
SM 4500-H+B-2011 1 PASI-AYEG
EPA 300.0 Rev 2.1 1993 1 PASI-AJCM
EPA 350.1 Rev 2.0 1993 1 PASI-ASMS
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 24
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
PASI-A = Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Sample:MW-1 Lab ID:92590781001 Collected:03/01/22 10:25 Received:03/01/22 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 03/10/22 13:17 7440-38-203/09/22 02:0010.0 1
Barium 108 ug/L 03/10/22 13:17 7440-39-303/09/22 02:005.0 1
Chromium ND ug/L 03/10/22 13:17 7440-47-303/09/22 02:005.0 1
Iron 13600 ug/L 03/10/22 13:17 7439-89-603/09/22 02:0050.0 1
Lead ND ug/L 03/10/22 13:17 7439-92-103/09/22 02:005.0 1
Manganese 2100 ug/L 03/10/22 13:17 7439-96-503/09/22 02:005.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 6.7 Std. Units 03/04/22 09:59 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 1.6 mg/L 03/02/22 21:07 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 0.29 mg/L 03/04/22 13:39 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 03/09/22 03:08 7727-37-903/08/22 05:210.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 ND mg/L 03/01/22 23:540.040 1
Nitrogen, Nitrate ND mg/L 03/01/22 23:54 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 03/01/22 23:54 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 5 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Sample:MW-3 Lab ID:92590781002 Collected:03/01/22 13:00 Received:03/01/22 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic 12.0 ug/L 03/10/22 13:20 7440-38-203/09/22 02:0010.0 1
Barium 658 ug/L 03/10/22 13:20 7440-39-303/09/22 02:005.0 1
Chromium ND ug/L 03/10/22 13:20 7440-47-303/09/22 02:005.0 1
Iron 48700 ug/L 03/10/22 13:20 7439-89-603/09/22 02:0050.0 1
Lead ND ug/L 03/10/22 13:20 7439-92-103/09/22 02:005.0 1
Manganese 4610 ug/L 03/10/22 13:20 7439-96-503/09/22 02:005.0 1
Analytical Method: SM 2540C-2011
Pace Analytical Services - Asheville
2540C Total Dissolved Solids
Total Dissolved Solids 356 mg/L 03/04/22 11:3050.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 6.6 Std. Units 03/04/22 10:18 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 21.4 mg/L 03/02/22 21:21 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 14.8 mg/L 03/04/22 13:40 7664-41-70.20 2
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 14.5 mg/L 03/09/22 03:09 7727-37-903/08/22 05:210.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 ND mg/L 03/01/22 23:590.040 1
Nitrogen, Nitrate ND mg/L 03/01/22 23:59 14797-55-80.040 1
Nitrogen, Nitrite 0.047 mg/L 03/01/22 23:59 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 6 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Sample:MW-4 Lab ID:92590781003 Collected:03/01/22 14:00 Received:03/01/22 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 03/10/22 13:46 7440-38-203/09/22 02:0010.0 1
Barium 132 ug/L 03/10/22 13:46 7440-39-303/09/22 02:005.0 1
Chromium ND ug/L 03/10/22 13:46 7440-47-303/09/22 02:005.0 1
Iron 1130 ug/L 03/10/22 13:46 7439-89-603/09/22 02:0050.0 1
Lead ND ug/L 03/10/22 13:46 7439-92-103/09/22 02:005.0 1
Manganese 939 ug/L 03/10/22 13:46 7439-96-503/09/22 02:005.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 6.4 Std. Units 03/04/22 10:26 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 36.4 mg/L 03/02/22 21:35 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia 1.5 mg/L 03/04/22 13:42 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 1.5 mg/L 03/09/22 03:10 7727-37-903/08/22 05:210.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 2.4 mg/L 03/02/22 00:010.040 1
Nitrogen, Nitrate 2.3 mg/L 03/02/22 00:01 14797-55-80.040 1
Nitrogen, Nitrite 0.074 mg/L 03/02/22 00:01 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 7 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Sample:MW-6 Lab ID:92590781004 Collected:03/01/22 12:30 Received:03/01/22 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 03/10/22 13:50 7440-38-203/09/22 02:0010.0 1
Barium 71.0 ug/L 03/10/22 13:50 7440-39-303/09/22 02:005.0 1
Chromium ND ug/L 03/10/22 13:50 7440-47-303/09/22 02:005.0 1
Iron ND ug/L 03/10/22 13:50 7439-89-603/09/22 02:0050.0 1
Lead ND ug/L 03/10/22 13:50 7439-92-103/09/22 02:005.0 1
Manganese 14.6 ug/L 03/10/22 13:50 7439-96-503/09/22 02:005.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 5.7 Std. Units 03/04/22 10:13 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate ND mg/L 03/02/22 23:27 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 03/04/22 13:43 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 03/09/22 03:11 7727-37-903/08/22 05:210.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 0.11 mg/L 03/01/22 23:560.040 1
Nitrogen, Nitrate 0.11 mg/L 03/01/22 23:56 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 03/01/22 23:56 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Sample:MW-7 Lab ID:92590781005 Collected:03/01/22 13:15 Received:03/01/22 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 03/10/22 13:53 7440-38-203/09/22 02:0010.0 1
Barium 55.1 ug/L 03/10/22 13:53 7440-39-303/09/22 02:005.0 1
Chromium ND ug/L 03/10/22 13:53 7440-47-303/09/22 02:005.0 1
Iron 71.0 ug/L 03/10/22 13:53 7439-89-603/09/22 02:0050.0 1
Lead ND ug/L 03/10/22 13:53 7439-92-103/09/22 02:005.0 1
Manganese ND ug/L 03/10/22 13:53 7439-96-503/09/22 02:005.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 6.4 Std. Units 03/04/22 10:22 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 1.7 mg/L 03/02/22 23:41 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 03/04/22 13:44 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 03/09/22 03:12 7727-37-903/08/22 05:210.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 0.91 mg/L 03/02/22 00:000.040 1
Nitrogen, Nitrate 0.91 mg/L 03/02/22 00:00 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 03/02/22 00:00 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 24
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Sample:MW-8 Lab ID:92590781006 Collected:03/01/22 12:00 Received:03/01/22 16:00 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
200.7 MET ICP
Arsenic ND ug/L 03/10/22 13:56 7440-38-203/09/22 02:0010.0 1
Barium 11.5 ug/L 03/10/22 13:56 7440-39-303/09/22 02:005.0 1
Chromium ND ug/L 03/10/22 13:56 7440-47-303/09/22 02:005.0 1
Iron ND ug/L 03/10/22 13:56 7439-89-603/09/22 02:0050.0 1
Lead ND ug/L 03/10/22 13:56 7439-92-103/09/22 02:005.0 1
Manganese ND ug/L 03/10/22 13:56 7439-96-503/09/22 02:005.0 1
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
4500H+ pH, Electrometric
pH at 25 Degrees C 6.4 Std. Units 03/04/22 10:08 H30.10 1
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
300.0 IC Anions 28 Days
Sulfate 18.0 mg/L 03/02/22 23:55 14808-79-81.0 1
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/L 03/07/22 12:49 7664-41-70.10 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total ND mg/L 03/09/22 03:16 7727-37-903/08/22 05:210.50 1
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, NO2 plus NO3 2.6 mg/L 03/01/22 23:550.040 1
Nitrogen, Nitrate 2.6 mg/L 03/01/22 23:55 14797-55-80.040 1
Nitrogen, Nitrite ND mg/L 03/01/22 23:55 14797-65-00.040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 10 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
682857
EPA 200.7 Rev 4.4 1994
EPA 200.7 Rev 4.4 1994
200.7 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92590781001, 92590781002, 92590781003, 92590781004, 92590781005, 92590781006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3571751
Associated Lab Samples:92590781001, 92590781002, 92590781003, 92590781004, 92590781005, 92590781006
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 03/10/22 12:03
Barium ug/L ND 5.0 03/10/22 12:03
Chromium ug/L ND 5.0 03/10/22 12:03
Iron ug/L ND 50.0 03/10/22 12:03
Lead ug/L ND 5.0 03/10/22 12:03
Manganese ug/L ND 5.0 03/10/22 12:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3571752LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 486500 97 85-115
Barium ug/L 516500 103 85-115
Chromium ug/L 463500 93 85-115
Iron ug/L 49005000 98 85-115
Lead ug/L 472500 94 85-115
Manganese ug/L 482500 96 85-115
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3571753MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92589394001
3571754
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 100 70-13098 2500ND501493
Barium ug/L 500 101 70-130100 150079.1 585 581
Chromium ug/L 500 91 70-13090 1500ND454449
Iron ug/L 5000 96 70-13096 05000ND47904790
Lead ug/L 500 92 70-13089 3500ND465452
Manganese ug/L 500 94 70-13093 1500ND470467
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3571755MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92589888001
3571756
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 104 70-130105 1500ND523526
Barium ug/L 500 102 70-130102 0500ND511512
Chromium ug/L 500 88 70-13089 150012.4 452 457
Iron ug/L 5000 95 70-13095 1500018249604920
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 11 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3571755MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92589888001
3571756
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Lead ug/L 500 87 70-13086 0500ND434432
Manganese ug/L 500 92 70-13093 150014.0 474 477
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 12 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
682447
SM 2540C-2011
SM 2540C-2011
2540C Total Dissolved Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92590781002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3569612
Associated Lab Samples:92590781002
Matrix:Water
Analyzed
Total Dissolved Solids mg/L ND 25.0 03/04/22 11:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3569613LABORATORY CONTROL SAMPLE:
LCSSpike
Total Dissolved Solids mg/L 252250 101 90-110
Parameter Units
Dup
Result QualifiersRPDResult
92590714002
3569614SAMPLE DUPLICATE:
Total Dissolved Solids mg/L 97.0 H3198.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 13 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
682427
SM 4500-H+B-2011
SM 4500-H+B-2011
4500H+B pH
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92590781001, 92590781002, 92590781003, 92590781004, 92590781005, 92590781006
Parameter Units
Dup
Result QualifiersRPDResult
92590781001
3569561SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 6.7 H316.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 14 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
682050
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92590781001, 92590781002, 92590781003, 92590781004, 92590781005, 92590781006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3567851
Associated Lab Samples:92590781001, 92590781002, 92590781003, 92590781004, 92590781005, 92590781006
Matrix:Water
Analyzed
Sulfate mg/L ND 1.0 03/02/22 19:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3567852LABORATORY CONTROL SAMPLE:
LCSSpike
Sulfate mg/L 50.450 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3567853MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92590770001
3567854
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L M15010690-110111 5501.9 54.8 57.5
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3567855MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92590742002
3567856
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Sulfate mg/L M15010990-110111 1501.7 56.2 57.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 15 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
682452
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
350.1 Ammonia
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92590781001, 92590781002, 92590781003, 92590781004, 92590781005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3569619
Associated Lab Samples:92590781001, 92590781002, 92590781003, 92590781004, 92590781005
Matrix:Water
Analyzed
Nitrogen, Ammonia mg/L ND 0.10 03/04/22 12:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3569620LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/L 5.25 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3569621MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92590866001
3569622
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L M158290-11078 1524.6 28.7 28.5
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3569623MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92590866002
3569624
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 108 90-110108 050.14 5.6 5.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 16 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
682762
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
350.1 Ammonia
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92590781006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3571359
Associated Lab Samples:92590781006
Matrix:Water
Analyzed
Nitrogen, Ammonia mg/L ND 0.10 03/07/22 12:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3571360LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/L 5.25 104 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3571361MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92590781006
3571362
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 99 90-11098 15ND4.9 4.9
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3571363MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92591348001
3571364
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/L 5 109 90-110109 15ND5.5 5.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 17 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
683001
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92590781001, 92590781002, 92590781003, 92590781004, 92590781005, 92590781006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3572670
Associated Lab Samples:92590781001, 92590781002, 92590781003, 92590781004, 92590781005, 92590781006
Matrix:Water
Analyzed
Nitrogen, Kjeldahl, Total mg/L ND 0.50 03/09/22 02:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3572671LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/L 9.510 95 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3572672MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92590110005
3572673
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L M1108890-11088 0104.6 13.3 13.4
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3572674MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92590781005
3572675
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/L 10 100 90-110101 110ND1010.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 18 of 24
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
681780
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite, Unpres.
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92590781001, 92590781002, 92590781003, 92590781004, 92590781005, 92590781006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3566355
Associated Lab Samples:92590781001, 92590781002, 92590781003, 92590781004, 92590781005, 92590781006
Matrix:Water
Analyzed
Nitrogen, Nitrate mg/L ND 0.040 03/01/22 23:46
Nitrogen, Nitrite mg/L ND 0.040 03/01/22 23:46
Nitrogen, NO2 plus NO3 mg/L ND 0.040 03/01/22 23:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3566356LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/L 1.51.5 99 90-110
Nitrogen, Nitrite mg/L 0.991 99 90-110
Nitrogen, NO2 plus NO3 mg/L 2.52.5 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3566357MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92590731001
3566358
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/L 1.5 -10 90-11040 41.520.9 20.7 21.5
Nitrogen, Nitrite mg/L 1 102 90-110102 01ND1.0 1.0
Nitrogen, NO2 plus NO3 mg/L M12.5 35 90-11065 32.520.9 21.8 22.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 19 of 24
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 20 of 24
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92590781
Blue Ridge Tissue Corp
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92590781001 682857 683335MW-1 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92590781002 682857 683335MW-3 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92590781003 682857 683335MW-4 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92590781004 682857 683335MW-6 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92590781005 682857 683335MW-7 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92590781006 682857 683335MW-8 EPA 200.7 Rev 4.4 1994 EPA 200.7 Rev 4.4 1994
92590781002 682447MW-3 SM 2540C-2011
92590781001 682427MW-1 SM 4500-H+B-2011
92590781002 682427MW-3 SM 4500-H+B-2011
92590781003 682427MW-4 SM 4500-H+B-2011
92590781004 682427MW-6 SM 4500-H+B-2011
92590781005 682427MW-7 SM 4500-H+B-2011
92590781006 682427MW-8 SM 4500-H+B-2011
92590781001 682050MW-1 EPA 300.0 Rev 2.1 1993
92590781002 682050MW-3 EPA 300.0 Rev 2.1 1993
92590781003 682050MW-4 EPA 300.0 Rev 2.1 1993
92590781004 682050MW-6 EPA 300.0 Rev 2.1 1993
92590781005 682050MW-7 EPA 300.0 Rev 2.1 1993
92590781006 682050MW-8 EPA 300.0 Rev 2.1 1993
92590781001 682452MW-1 EPA 350.1 Rev 2.0 1993
92590781002 682452MW-3 EPA 350.1 Rev 2.0 1993
92590781003 682452MW-4 EPA 350.1 Rev 2.0 1993
92590781004 682452MW-6 EPA 350.1 Rev 2.0 1993
92590781005 682452MW-7 EPA 350.1 Rev 2.0 1993
92590781006 682762MW-8 EPA 350.1 Rev 2.0 1993
92590781001 683001 683327MW-1 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92590781002 683001 683327MW-3 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92590781003 683001 683327MW-4 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92590781004 683001 683327MW-6 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92590781005 683001 683327MW-7 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92590781006 683001 683327MW-8 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92590781001 681780MW-1 EPA 353.2 Rev 2.0 1993
92590781002 681780MW-3 EPA 353.2 Rev 2.0 1993
92590781003 681780MW-4 EPA 353.2 Rev 2.0 1993
92590781004 681780MW-6 EPA 353.2 Rev 2.0 1993
92590781005 681780MW-7 EPA 353.2 Rev 2.0 1993
92590781006 681780MW-8 EPA 353.2 Rev 2.0 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/11/2022 09:16 AM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 21 of 24
Page 22 of 24
Page 23 of 24
Page 24 of 24