WQ0001953_ AR_20220209

Town of Spindale
2021 Annual Report
Land Application Program
Permit No. WQ0001953

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit4: WQ0001953 County:
Facility Name (as shown on permit):
Land Application Operator:
Rutherford
Year: 2021
Town of Spindale
US Biosolids, Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
R1 Yes D No - if No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
6
Total number of fields utilized for land application during the year:
5
Total amount of dry tons applied during the year for all application sites:
115.43
Total number of acres utilizes for land application during the year
64.4
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. Q Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
I ) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .l 1 1 1 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of deviation, prior
authorisation was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accuratc,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Permittee Name and Titl� (type or print)
1-12- h 4, -Z2
Signature of Permittee Date
'-61-91,;d
Signature of Preparer* Date SigWature ol'Larrd Applier Date
(if different from Permittee) (ii'different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T.1 102 (26) DENR FORM ACF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale Total Dry Tons Applied (Annual): 8.70
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series: PaC2
Acres Used: 15.1 Acres Permitted: 15.1 Site #: M Field #: I
Residual Analysis Data (Heavy Metals and Total Phosphorus use me/ke, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
J
3/11/21
_2�
3
41
5 i
6
7
8
9
10
11r
12
% Solids
1.69
Arsenic
29.4
Cadmium
5.88
Copper
277
Chromium
42.9
Lead
32.4
Mercury
0.912
Molyb-
_dghum
14.7
Nickel
14.7
Selenium
29.4
Zinc
700
Total
Phos-
Chorus
11100
Annuat heavy ivietai rteta Loaames (L;aiculatea in Ibs/acre):
Total
1;
2.
31
4�
5
6
7
8
9N
10F
11
12i
App.
�.
y
Event
0.58
Arsenic
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.319
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.319
Chromium
0.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.049
Lead
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
denum
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Nickel
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Selenium
0,034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
7.inc
0.806 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.806
Total
Phos-
12.787
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
12.787
horus
t certtty, unuer penatty of iaw, that tnts document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
_ I - - -- --?-q�o�
Sii-ma re of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to he submitted in Annual Report
Facility Name: Town of Spindale Total Dry Tons Applied (Annual): 18.34
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series: PaC2
Acres Used: 15.5 Acres Permitted: 15.5 Site #: M Field #: 3
Recidit:il Analvcis nata (Heavv Metals and 'Total Phosnhorus use me/ka. % Solids use Raw Percent #):
Sample or
Com-
posite
Date
3/11/21
21
3. i
4
5!
6 !
7
8 !
9
10
11
12
% Solids
1.69
Arsenic
29.4
Cadmium
5.88
Copper
277
Chromium
42.9
Lead
32.4
Mercury
0.912
Molyb-
denum
14.7
Nickel
14.7
Selen ium
29.4
Zinc
700
Total
Phos-
horus
11100
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
1
2i
3�
4i
5!
6�
7:
8�
9!
10
11
12
-
---
--
J
DT/Ac./
o
App.
K
Event
1.18
Arsenic
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Cadmium
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.014
Copper
0.655
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.655
Chromium
0.102
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.102
Lead
0.077
0.000
0.000
0.000
0.000
0,000
0.000
0,000
0.000
0.000
0.000
0.000
0.077
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.035
denum
Nickel
0.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.035
Selenium
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Zinc
1.656
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
1.656
Total
Kos-
26.263
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
26.263
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
_. 7,6� )- �-� �a
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale Total Dry Tons Applied (Annual): 50.39
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series: PaC2
Acres Used: 17.1 Acres Permitted: 17.1 Site #: M Field #: 4
Residual Analvsis Data (Heavv Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
I L _1_,
3/11/21
2 ,
31
4
5
fi
7J
81,
9 ;
10 !
11 j
121
% Solids
1.69
Arsenic
29.4
Cadmium
5.88
Copper
277
Chromium
42.9
Lead
32.4
Mercury
0.912
Molyb-
enum
14.7
Nickel
14.7
Selenium
29.4
Zinc
700
Total
Phos-
horus
11100
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2;
31
4!
5 i
6
7
8
9
10
11
DT/Ac./
o
App-
Event
2.95
14
Arsenic
0.173
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.173
Cadmium
0.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.035
Copper
1.633
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.633
Chromium
0.253
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.253
Lead
0.191
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.191
Mercury
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.087
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.087
denum
Nickel
0.087
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.087
Selenium
0.173
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.173
Zinc
4.126
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.126
Total
Phos-
65.423
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
65.423
horus
"l Certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land pplier
a-9-;bn
Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale Total Dry Tons Applied (Annual):
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series:
Acres Used: 10.6 Acres Permitted: 10.6 Site #: M Field #:
26.11
CaB2
5
Residual Analysis Data (Heavy Metals and 'fotal Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
. 1
3/11/21
2J
L3J
4
5;
6
7
8
9^
10 1
11
12
% Solids
1.69
Arsenic
29.4
Cadmium
5.88
Copper
277
Chromium
42.9
Lead
32.4
Mercury
0.912
Molyb-
denum
14.7
Nickel
14.7
Selenium
29.4
Zinc
700
Total
Phos-
horus
11100
Annual Heavy Metal kield Loadinp-s (Calculated in Ibs/acre):
Total
1 1
2
3
4'
S
6
7'
8
9 i
10
11
12
DT/Ac.i
o
App.
H
Event
2.46
Arsenic
0.145
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
1 0.145
Cadmium
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Copper
1.365
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.365
Chromium
0.211
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.211
Lead
0.160
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.160
Mercury
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.004
Molyb-
denum
0.072
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.072
Nickel
0.072
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.072
Selenium
0.145
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.145
Zinc
3.448
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
3.448
Total
Phos-
54.679
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
54.679
horus
x ceruly, unuer penaHy of law, tnat tnts document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
9-4.?usk
Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Spindale
WQ0001953
John McFadden Owner:
6.1 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
John McFadden Predominant Soil Series:
6.1 Site #: M Field #:
CaB2
6
Recidtial Annlvvis Data (Heavv Metals and 'Total Phosphorus use ma/ka. % Solids use Raw Percent #):
le or
Com-
posite
Date
3/11121
2
3
4
5
781
_
9
10
11
12Sam
Solids
1.69
Arsenic
29.4
Cadmium
5.88
Copper
277
Chromium
42.9
Lead
32.4
Mercury
0.912
Molyb-
enum
14.7
Nickel
14.7
Selenium
29A
"Zinc
700
Total
Phos-
horus
11100
Annual Heavy Metal Field Loadintws (Calculated in lbs/acre):
Total
17
2
16�i
7
8
9
10 J
11 1
12
-
--
-
-
-
DT/Ac./
APp-
14
Event
1.95
Arsenic
0.115
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.115
Cadmium
0.023
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Copper
1.081
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.081
Chrorniurn
0.167
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.167
Lead
0.126
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.126
Mercury
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.057
denum
Nickel
0.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.057
Selenium
0.115
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.115
Zinc
2.733
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.733
Total
Phos-
43.334
0.000
0.000
0.000
0.000
0-000
0.000
0.000
0.000
0.000
0.000
0.000
43.334
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified Personnel properly gathered and evaluated the information submitted.
l am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
i-4.2 630
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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a

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Spindale
WWTP Name: Town of Spindale W WTP
Monitoring Period: From 1/1/2021
To
WQ Permit Number:
NPDES Number:
12/31 /2021
WQ0001953
NCO020664
13ot6nnnn D-A-nt.nn 11GA NICAC n7T I lnfl - PIPncP indiente level achieved and alternative nerformed:
Class A:
Alt` A (time/temp) ❑
Alt B (Alk Treatment)i]
Alt. C (Prior Testing)®
A1t.D (No Prior Test) © I
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Therniophilic. ❑
Beta Ray ❑
Gamma Ka y ❑
Pasteurization
Class B: jAlt.
(1) Fecal Density 21
Alt. (2) Process to i,Wnlfica11dy Reduce Patho ens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Com postinu ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Density en Pathog y
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
Ana ytica
Tech -
i clue
Minimum
Geo. Mean
Maximurn
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
5785
9745
16363
MPN/g
0
7
grab
sm9221 c
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry,
weight)
Vector Attraction Reduction t15A NCAE- U24 A 1U7) - Ylease indicate alternative pertormea:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑✓
Alt. 4 (Spec. O, uptake) J
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ©
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attrketion reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dennis Key US Biosolids, Inc.
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer*
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 21' .1102 (26)
DENR FORM PVRF 02T (1212006)

S'Ayffi'VAKM WANAMMOM . .......... a ......... - - -----
Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 03/1 V2021
Reported: 03/30/2021
For: Spindale
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210311-24-01 TCLP Spindale See Attached as Noted 03/12/2021 PACE
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 w Statesville, NC 28687 • 704/872/4697
Page 1 of 30

Pace Ana"cal Services, LLC
9M K9,06y Ave, Suite 100
/�ZAnalytcal Hunwit"WNC280'm
ANALYTICAL RESULTS
Protect. 210311-24-0
Pace Project No. 92527465
Sample: 210311-24-01 Lab 10. 9252746501 CcliadedOV11441 10,00 Received. GNI2r'21 D9,38 WtrP: WaW
Parameters Resuns unft Reporl Limit OF Propared Analyzed CAS No Oua;
Chkxlriatod H*M (GC) 8151A Analytical Method-W*8151A Preparation Melho4 6151A
Leachate Methii:00alw 1311, 03"8f21 11:03 Initial pH 7 43. Feral pH 4.92
Pace National - W. Juliet
2.4,5.TP (Sintex) NO mWL 0100200 1 03d2=11226 03LI3<l! 18:04 93-72-1
2,4-0 NO MW'L 0,00200 1 DWV2112:26 DY23121 18:04 94-75-7
swroval"
2,4-OC-AA (S)
661 %
140-158 1
MV21 1126 OU23121 W04 19719-26-9
M11 TCLP Pimficid" RYE
Analytica, Malhod EPA 80619 Preparabm Method: EPA 3510C
Leachaw MetricidDalo: EPA 1311 > 03el 511 15:29 WWI pK I anal PH 5
Pace Analytical Services - Chaildle
garnme, allr- (Ltrioane)
NO uWL
0,50 1
UlMl 09,52 03,117,71 16:18 58-89-9
chomene (Tedbiri"l)
ND Owl-
310 1
Ml 7�121 09,52 03/17r4i 1618 57-74-9
Erockin
NO 4L
0.50 t
03,117121 09,52 0311V21 1618 72-204
HapWcthlor
NO UWL
050 1
071 Tf2l 09 62 03117,71 16,18 76-44-8
Hepta0W apaxide
NO upIL
05c 1
03117!21 02:52 03117,11 16: 18 1024.57-3 L1
Mathawychiof
NO ug!L
1000 1
03E17.121 04:52 03117,11 16:18 72-23 5,
Toxaphane
NO ugll-
3,0 1
03117,2109:52 03F17f2l 16,18 SWI-35.2
sunwafts
Decac13i`wYi (S]
113 ci4
10-154 1
03,117121 (* 52 03r17,021 16,18 2051-24-3
Tatireialoro-rn-xVlatte (S)
99 %
10-184 1
MIMI 0952 03lI7#2I WIS 877-0"
6082 TCLP PCBs RYE
Ariaiytmr Mathctd: EPA SMA P"parsbw Mothod. EPA 3510C
Leacriale Melhod,`Daw EPA 1311: 03115121 1529 lriU'al pH, : FMRI pH. 5
Paco Artatitic-ii Services - Charlode
PCB- 10 16 ukoclor 1016)
NO kisit
low I
a1ri`21 1113 03MW21 13:03 12674-11-2
PM 1221 (Arad" I Z21)
NO uc ,pl-
1000 1
0317*1 1113 0311911 13:03 11104-28-2
PCB- 12,32 (Aroclor 1232)
No UWL
1000 1
031111TV 1123 03119121 1103 11141-16-5
PCa-1242 (Aroclor 12421
ND 16*WL
1000 1
03117,121 1113 03f1911 13,03 53469-21.9
PCB-1248 (Amclor 1248t
NO uwt-
1000 1
OW1711 11:23 03MOP21 11,03 12672-29.6
PCB-1254 (Aroclor 125C
No ugL
100(1 1
03tIT121 W23 0311W.11 1103 11097-69-1
PCB-12W (Arodor 126M
ND 09"L
1000 1
03117M 11:23 0Y19121 13:03 11096-112-5
(S)
65
10.181 1
0317121 11:23 03f19121 13:03 2051-24-3
6010 MET ICP, TCLP
Analytical Mel,,Dd. EPA 60100 Pnewrailkxn Methw-- EPA 3010A
Lwhate Method(t)ate EPA 13M 03.061'21 15,.53 Initial pK, Final pH, 2
Pact Aiiatyucai Serviceti - Asheville
Afww
NO MOIL
0. VA I
OW1611 1 G:24 03/21,112046 7440-39-2
Barium
NO rdwL
0.25 1
03,11811 1 G,:24 03,21/212046 7440-39-3
Cadmium
NO M9fL
0 0050 1
031I8121 10:24 03121,21 2V46 744043-9
Ginforrimm
NO rinqk
0.050 i
03118f2I 10:24 031112121046 7440-47- 3
Load
NO Molt
0 NIS 1
031I8i21 10:24 031`2 1 �21 20:46 7434-92-1
Solarilum
No M911-
0.10 1
03!I1gt21 1 G,24 WV21,121 20 46 7782-49.2
Silver
mg.'L
0,326 1
03118121 10,24 031211212046 7440-22.4
REPORT OF LABORATORY ANALYSIS
This report sh&I not be
eOmdUC&d, K.-Apt W 1W,
Date: 0373W2021 0104 PM
witni'm the gtMten � wnt of
P" Anwrylcui Se-mm, Ll C Page S 0127
PO Box 228 * Statesville, NC 28687 w 704/872/4697
Page 8 of 30

Piece Anetytical Services. LLC
oo A,,,, • 98W Kinsey Ave. Suite 100
HuntenwYe, NC 28078
s�apdsla,Cee [phone]
ANALYTICAL RESULTS
Project: 210311-24-01
Pace Project No-: 92527465
Sample: 210311-24-01 Lan ID: 22527465001 Collected: 03/11/21 10:00 Received: 03/12121 0938 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
7470 Mercury, TCLP
Analytical Method EPA 7470A Preparation Method: EPA 7470A
Loachate Method/Date: EPA 1311, 03/16(21 '5:53
Iniial
pH. ; Final pH. 2
Pace Analytical Services - Asheville
Mercury
NO
nuYL
0.00020
1
03/1812111:12 03l19i2113:02 7439-97-8
8270E TCLP RVE
Analytical Method:
EPA 6270E Preparation
Method. EPA 3510C
Leachate Method/Date EPA 1311. 03115/21 1529
Initial pH: ; Final pH 5
Pace Analytical Services - Charlotte
14-Dichiorobenzene
NO
ug/L
50.0
1
03il 7121 11:37 0311812114:58 106.46-7
2,4-Dindrotoluene
NO
uglL
50.0
1
0311712111:37 03/1&2114:58 121-14-2
Hexachloro-1,3-butodiene
NO
ug/L
50.0
1
03117/2t 11:37 03/18/21 14:58 87-68-3
Hexachloroberizene
NO
up/L
50.0
1
03117f2111:37 03/1872114.58 118-74-1
Hexachloroethane
NO
ug/L
50.0
1
0311712111:37 03il&2114:58 67-72.1
2-Methylphenol(o-Cresoi)
NO
ug!L
50.0
t
0311712111:37 03118/21 14:58 95-48-7
394-Methylphenol(ri Cresol)
179
ug/L
50.0
1
03/17121 11:37 03/18f21 14:58 15831-10-4
N trobenzene
NO
ug/L
50.0
1
03/17/21 11:37 03118/21 14:58 W95-3
Pentachlorophenol
NO
uglL
100
1
0311712111.37 0311&12114:58 87-86-5
Pyridine
NO
ug7L
so.0
1
0311712111:37 0311812114:58 110-Wl
2,4,5-Tnchlorophenol
NO
uq/L
50.0
1
03/1712111:37 03118/2114:58 95-95-4
2.4.6-Trichlorophend
ND
ug1L
50.0
1
03117/21 11:37 03118l2114-58 88-06-2
Surreyatas
Nitrobenzene-05 (S)
79
%
10-144
1
03117/21 11.37 0311B121 14:58 4165-60-0
2-Flucrobephenyl (S)
66
%
10-130
1
03117/21 11:37 03/18/21 14:58 321-60-8
Terpheny"14 (S)
123
%
34-163
1
03117/21 11:37 03/18/21 1458 1718-51-0
Phenoi-d6 (S)
37
%
10-130
1
03,117121 11:37 03118f21 14:58 13127488-3
2-Flucrophenol(S)
51
%
10-130
1
03117/21 11.37 03/18/21 14.58 367-124
2,416-Tribrornophenol (S)
61
%
10-144
1
03/17121 11:37 03/18/21 14:58 118.79-6
8260D MSV TCLP
Analytical Method: EPA 82600 Leachate MethodlDate EPA 1311, 03/25/21 12:58
Pace Analytical Services - Charlotte
Benzene
ND
ug/L
100
20
03126/2112:15 71-43-2
2-autanone (MEK)
NO
ug7L
20C
20
03/26/21 12 15 78-93-3
Carbon tetrachloride
NO
ug7L
10C
20
03/26/21 12:15 56-23-5
ClNorobenzene
NO
ug/L
100
20
0312612112:15 108-90-7
Chloroform
NO
ug/L
10C
20
03126/21 12:15 67-66-3
1,4-Dichlorobenzene
NO
ug7L
10C
29
0312612112:15 106-46-7
1,2-Dichloroethane
NO
ug7L
100
20
03/2612112.15 107-06-2
1,1-Dichloroethene
ND
ug7L
10C
20
03/26/21 12 15 75-354
Tetra chlcroethene
ND
uglL
10C
20
0312612112:15 127-10-4
Tnchloroethene
ND
ug7L
100
20
0312W11215 79-01.6
Vinyl chlonde
NO
ug7L
100
20
03/26121 12:15 75-014
Surregafea
1,2-oichloroethane-04 (S)
108
%
70-130
20
03/26/21 12:15 17060.07-0
TolueneAll (S)
98
%
67-135
2D
03126/21 12:15 2037-26-5
4-Bromofluorobenzene (S)
104
%
70-130
20
03/2W1 1215 460-004
REPORT
OF LABORATORY
ANALYSIS
Ttvs report shell not be reproduced. except in
ru 1.
Date: 03i3012021 03:04 PM
without the wniten consent of
Pace Analytical
$*"WAS.
LLC
Page 6 of 27
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 9 of 30

•
ZAnaoical
awsSo4Msa
ANALYTICAL RESULTS
Pace Analytfeal Semis, LLC
980D Kincey Ave. Suile 100
HcnlereviNe. NC 28078
[phone]
Pwi 210311-24-01
Pace Pro}ect No.: 92527465
Sample: 210311-24-01
Lab 10: 92527465001 Collected: 03/11/21 10.00 Received: 03/12121 D9:38 Matrix: Water
Parameters
Results Units Report Limit OF Prepared Analyzed CAS No. Qual
1010 FiashpoiM,Closed Cup
Analytical Method: EPA 1010E
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 1 03/25l21 12:10
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.9 Sid. Units 010 1 03/21121 18:33 H3
9095 Paint Filter Uqu4d Test
Analytical Method EPA 9095B
Pace Analytical Services - Asheville
Free Liquids
Fall 1.0 1 03119/21 16:19
733C S Reacllve Cyanide
Analytical Method: EPA 9014 Preparation Method. SW-846 T3.3.2
Pace Analytical Services - Greensburg
Cyanide, Reactive
NO mg/kg 52.1 1 03/16/21 19:28 03117/21 18:46
7345 Reactive Sulfide
Analytical Method. SM 4500S2F-2011 Preparation Method SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive
NO mg1kg 521 1 03/16/21 19:28 03/16/21 19:31
Sample: 210311-24-01
Parameters
Lab lD: 92527465002 Collected: 03M V21 10 00
Results Units Report Limit OF
Received: 03/12/21 09:38 Matrix: Water
Prepared Analyzed CAS No. Qual
8082 GCS PCB RVE
Analytical Method. EPA 8082A Preparation Method EPA 351 DC
Pace Analytical Services - Charlotte
PCB-1016 (Amclor 1016)
NO ug/L
2.5
1
03/26/21 1253 0312W21 15:52 12874-11-2
PCB-1221 (Aroclor 1221)
NO ug1L
2 5
1
03126/21 12:53 03129/21 15:52 11104.28.2
PCB-1232 (Aroclor 1232)
NO ug'L
2.5
1
03126121 12:53 03/29J21 15:52 11141-16-5
PCB-1242 (Aroclor 1242)
NO u91L
2.5
1
03126121 12,53 03,i29.21 15:52 53469-21.9
PCB-1248 (Aroclor 1248)
NO ug1L
2 5
1
03121 121 12:53 03129.r21 15:52 12672-2M
PCB-1254 (Aroclor 1254)
NO uglL
2 5
1
03IM21 12:53 03/29/21 15:52 11097-69-1
PCB-1260 (Aroclor 1260)
NO ug'L
2.5
1
0126121 12:53 03129t2l 16:52 11096-82-5
Surmptes
Decachlorotrphenyl (S)
73 %
10-181
1
03/26/21 12:53 03129.121 15:52 2051-24-3
REPORT OF LABORATORY ANALYSIS
Thia report shot! not he reprodueeo, exrept it tilt.
Date: 03/3C/2021 03:04 PM without the wrmen �nsent of Pace Analytical Services. LLC. Page 7 of 27
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 10 of 30

Analytical Results SITATESY I LLE
A N' I "" I " ALYI LAL
U.S. Bicisolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date:
Reported:
For:
Comments:
Sample Number
0410112021
04/05/2021
Spirdale
GEOMETRIC MEAN: 9745 MPNIO
Parameter Sample ID Result
Unit
Method
Analyzed
Analyst
210401-18-01
Fecal Collforms
S1
12687
MPN/g
SM922"CE 2006
044112021
MD
210401 - I a-01
Percent Solids
S1
443
%
SM25406-2c",
041011'2021
MD
210401-18-02
Fecal ColiforMs
S2
12360
MPNIg
5M92,210E 2006
04101/2021
MD
210401-18-02
Percent Solids
S2
3,47
%
SM2554W-2011
04/01,2021
MD
210401-18-03
Fecal Coliforms
S3
5785
MPNIg
SM9221CF—'"
04/01/2021
MD
21 G401-18-03
Percent Solids
S3
4.33
%
$WfA.W-r, I ,
04101/2021
MD
210401-18-04
Fecal Coliforms
S4
7558
MPN/q
SM92210E-AW
04101,12021
MD
210401-18-04
Percent Solids
S4
5,19
%
SV125AM201 i
0410 112021
MD
210401-18-05
Fecal Coliforms
S5
7602
MPN/g
SM92210E-2"
0410112021
MID
210401-118-05
Percent Solids
S5
53
%
Sk*2W8-n 11
04101/2021
IVID
21 D401-18-06
Fecal Colifamis
S6
9 717 0
MPN/g
SM92210E 2X6
04/01/2021
MD
210401-18-06
Percent Solids
S6
435
%
spa WS-201, 1
0410112021
MD
210401-18-07
Fecal Coliforms
S7
16363
MPNig
SMOVICE—IX6
0410112021
MD
210401-18-07
Percent Solids
S7
50
%
SM254013-22I 1
04t01/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert 9440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 * Statesville, NC 28687 * 704/872/4697
Page 1 Of 4

Waypoint.
0
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401' Fox 804-271.6445
ANALYTICAL
www.waypointanalytical.com
46381
US Biosolids Inc
Project
Spindale
Dennis Key
Report Date: 03/25/2021
958 Hoots Road
Information :
Received: 03/ 15/2021
Roaring River , NC 28669
roc
Pauric Mc Groary Ph.D., Caapp
Report Number : 21-074-0008
RE�RTOFANALYSIS Agronomist
Lab No : 75440
Matrix: Solids
Sample ID : Spindale
Sampled: 3/11/202i 16:00
Test
Results
Units
MQL OF Date / Time By Analytical
Analyzed Method
Moisture
98.3
%
0.010 1 03/18/2116:48 FMM SM-2540G
Test
Results
Units
MQL DF Date 1 Time By Analytical
Analyzed Method
Ammonia Nitrogen
14600
mg/Kg - dry
5880
1
03/22/21 14:30
JP]
SM-4500-NH3C
Nitrate+Nitrite-N
<292
mg/Kg - dry
292
1
03/19/21 14:49
ZBD
4500NO3F-2011
Organic N
58800
mg/Kg - dry
14700
1
03/22/21 10:00
CALCULATION
pH
6.8
s.u.
1
03/19/2117:06
ADM
9045D
Total Solids
i
1.69
%
0.010
1
03/18/21 16:48
FMM
SM-254OG
Total Kjeldahl Nitrogen
735M
mg/Kg - dry
14700
1
03/22/21 10:00
JP] ')M-4500-NH3C-TKP
Phosphorus
11100
mg/Kg - dry
294
1
03/20/21 04:04
JTR
6010D
Aluminum
15000
mg/Kg - dry
294
1
03/20/21 04:04
JTR
6010D
Arsenic
<29.4
mg/Kg - dry
29.4
1
03/23/21 22:45
TADS
6010D
Calcium
8470
mg/Kg - dry
2940
1
03/20/21 D4:04
JTR
6010D
Cadmium
<5.88
mg/Kg - dry
5.88
1
03/20/21 04:04
JTR
6010D
Chromium
42.9
mg/Kg - dry
14.7
1
03/23/21 22:45
]ADS
6010D
Copper
277
mg/Kg - dry
29.4
1
03/20/21 04:04
JTR
6010D
Iron
11400
mg/Kg - dry
588
1
03/20/21 04:04
JTR
6010D
Lead
32.4
mg/Kg - dry
17.6
1
03/20/21 04:04
JTR
60101)
Magnesium
2180
mg/Kg - dry
294
1
03/20/21 04:04
JTR
6010D
Manganese
368
mg/Kg - dry
29.4
1
03/20/21 04:04
JTR
6010D
Qualifiers/ OF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quandtation Limit
Page 3 of 7

0
7621 Whitepine Road, Richmond, VA 23237
Waypoint Main 804-743.9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46381
US Biosolids Inc Project Spindale
Dennis Key Report Date : 03/25/2021
958 Hoots Road Information : Received : 03/15/2021
Roaring River , NC 28669 qp
Tew( iAc Freon✓
Report Number: 21-074-0008 REPOR T OF A NA4 YSTS Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No: 75"0 Matrix: Solids
Sample ID: Spindale Sampled: 3/11/2021 10:00
Teat Results Units MQL DF Date / Time By Analytical
Analyzed Method
Mercury
<0.912
mg/Kg - dry
0.912
1
03/18/21 11:13
DDB
SW-7471B
Molybdenum
<14.7
mg/Kg - dry
14.7
1
03/20/21 04:04
JTR
6010D
Nickel
<14.7
mg/Kg - dry
14.7
1
03/20/21 04:04
JTR
6010D
Potassium
5250
mg/Kg - dry
588
1
03/20/21 04:04
JTR
6010D
Selenium
<29.4
mg/Kg - dry
29.4
1
03/20/21 04:04
-TR
6010D
Sodium
11000
mg/Kg - dry
1470
1
03/20/21 04:04
JTR
6010D
Zinc
700
mg/Kg - dry
73.5
1
03/20/21 04:04
JTR
6010D
Sulfur
5710
mg/Kg - dry
588
1
03/20/21 04:04
JTR
6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 7

o
c
cci
A
0
0
V,
o
C7
X
N
Y
Y
cn
(n
Q7
N
E
II
II
11
II
N
O
O
X
Y
on
E
Z
Q
a
N
O
O
X
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x
E
p
N
O00
O
a�
d�
a_
a-
o
c
v
d
m
d ..
�
c

l-U I
Sodium Absorption Ratio
Na : Sodium (Mg/L) Equivalent weight; 23
Ca : Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight: 12
Milli Equivalent = Mg/L / Equivalent weight
Na M IL Ca M /L M M /L
185.9 143.14 32.48
Na (ME)
Ca (ME
Mac. JMEA
8.082609
I 7.157
I 2.706667
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 3.639547 (From Mg/L entered above)
SAR= 3.637205 1 (From ME entered below)
Na (ME)
Ca (ME)
Ma (fNE))
8.08
1 7.16
1 2.71
The amour
amount of i
Permitting

Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
STATESVILLE
X ANALYTICAL
Receive Date, 03/11/2021
Reported, 04115/2021
For. Spindale
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210311-23-01 30 Day Benchecale Spindale 101 % 0311112021 MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NCO0909
PO Box 228 a Statesville, NC 28687 9 704/872/4697
Page I of 5

11 q7&T-7,-, ,i, , c
Analytical Results
US BIOSOLIDS For: SPINDALE
958 HOOTS RD
ROARING RIVER, NC 28669
Entered: 3/11/21
Reported: 4/15/21
Sample ID: 210311-23-01
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids
Vglotile Solids
% Volatile Solids
Leek _1 1.79
1.19
0,6648
Week 2 37
1.16
0.6554
Week 3 1.76
1.15
0.6534
WCO 4 1.68
1.10
0,6548
Week 5 1.71
1.10
0.6433
Week 6 1.58
1.01
0.6392
Volatile Solids Reduction: 0.6648 - 0.6392 X 100 = 10.7 %
0.6648 - (0.6648 X (1.6392)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.# 44ONC
PO Box 228 - Statesville, NC 28687 • 704/872/4697
Page 4 of 5

30 Day Bench Worksheet
Sample ID # 210311-23-91
WEEK 1
Samples
Total Solids
Volatile Solids % Volatile Fraction
1
1.80
1.20
2
1.79
1.19
3
1.79
1.19
Avera e:
; 1.79
1.19 0.6649
WEEK 2
Samples
I Total Solids
Volatile Solids
% Volatile Fraction
1
1.77
1.17
2
1.77
1.16
1.76
1.16
_3
Average:
1.77
1.16
0.6554
WEEK 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.76
1.16
2
1.76
1.15
3
1.75
1.15
Avera e:
1.76
1.15
0,6534
WEEK 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.70
1.12
2
1.68
1.10
3
1.66
1.09
Average:
1.68
1.10
0.6548
WEEK 5
Samples
I Total Solids
Volatile Solids
% Volatile Fraction
1
1.7
1.09
2
1.71
1.10
3
1.71
1.10
Average:
1.71
1.10
0.6433
WEEK 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.56
1.00
2
1.6
1.03
3
1.57
1.01
Average: 1.58
1.01
0.6392
Van Kleeck Reduction: 0.6648 - 0.6392 X 100 %
0.660 - (0.6648 X 0,6392)
Final Result: 10.7%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 5

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