NC0055786_Wasteload Allocation_19921005

NPDES DOCUHENT SCANNING COVER :SHEET
NPDES Permit:
NC0055786
Lexington Regional WWTP
Document Type:
Permit Issuance
Wasteload Allocation
Authorization to Construct (AtC)
Permit Modification
Complete File - Historical
Engineering Alternatives (EAA)
Correspondence
Owner Name Change
Instream Assessment (67b)
Speculative Limits
Environmental Assessment (EA)
Document Date:
October 5, 1992
This document is printed on reuse paper - ignore any
content on the reYerse side

DIVISION OF ENVIRONMENTAL MANAGEMENT
October 5, 1992
MEMORANDUM
TO: Randy Kepler
FROM: Susan A. Wilson),
THROUGH: Trevor Clement
Carla Sanderso
SUBJECT: Lexington WWTP
NC0055786
Davidson County
Technical Support cannot agree, at this time, to the City of Lexington's request to drop the
monitoring requirements for silver and cyanide, since both parameters are permitted
through the facility's industrial pretreatment program at levels which warrant monitoring.
However, Technical Support does recommend that the monitoring frequency be reduced to
once per quarter for both parameters in light of the effluent monitoring data provided by the
permittee.
cc: Steve Mauney, WSRO
Julia Storm, Pretreatment Unit

. R/23 AZ
09/23/92 ver 3.1 T 0 X I/ C S R E V I E W \
Facility: lexington coy, N. '� o t_ y 1
NPDES Permit No.: nc0055786 I �.1 JJJ/A�� D a� 1
Status (E, P, or M): e mom-0-1Ly M.oniITo2404 �oR •, . 41 �l IS Petit NOW
Permitted Flow: 5.5 mgd / V
Actual Average Flow: 2.7 mgd �i '' - 7/4 2-
Subbasin: '030707
Receiving Stream: abbotts I PRETREATMENT DATA I----EFLLUENT DATA---- 1
Stream Classification: WtI3.3 C. I ACTUAL PERMITTEDI
7Q10: 6.7 cfs I Ind. + Ind. + 1 FREQUENCY 1
IWC: 55.99 % I Domestic PERMITTED Domestic I OBSERVED of Chronic)
Stn'd / Bkg 1 Removal Domestic Act.Ind. Total Industrial Total I Eflluent Criteria 1
Pollutant AL Conc. I Eff. Load Load Load Load Load I Conc. Violations)
(ug/1) (ug/1) 1 % (#/d) (#/d) (#/d) (#/d) (#/d) 1 (ug/1) (#vio/#sam)1
Cadmium S 2.0 I 0% 1 I
Chromium S 50.0 1 0% I 1 I
Copper AL 7.0 I 0% 1 1 N
Nickel S -2 0 1 0% I 1 P
Lead S 25.0 I 0% 1 1 U
Zinc AL 50.0 1 0% I T
Cyanide S 5.0 1 59% 0.0 0.00 0.10001, 0.100 1 I
Mercury S 0.012 1 0% I 1 S
Silver AL 0.06 I 94%4 0.00 0.00081 0.001 I 1 E
Selenium S 5.00 1 0% 1 I C
Arsenic S 50.00 1 0% .,,:res. w�sll ,/.4_JJ I T
Phenols S 0.5 1 0% ace YAcwl or' )�� ;.''S?'1RF z(._cll, ',In.'v'tprno5 I I
NH3-N C 1 0% I 1 0
T.R.Chlor.AL 17.0 1 0% I 1 N
I
I
I
ALLOWABLE PRDCT'D PRDCT'D PRDCT'D MONITOR/LIMIT I--ADTN'L RECMMDTN'S--
1 Effluent Effluent Effluent Instream 1 Recomm'd
Conc. using using Conc. Based on Based on Based on 1 FREQUENCY INSTREAM
I Allowable CHRONIC ACTUAL PERMIT using ACTUAL PERMITTED OBSERVED 1 Eff. Mon. Monitor.
Pollutant 1 Load Criteria Influent Influent OBSERVED Influent Influent Effluent 1 based on Recomm'd ?
(#/d) (ug/l) (ug/1) (ug/1) (ug/i) Loading Loading Data 1 OBSERVED (YES/NO)
Cadmium S
Chromium S
Copper AL
Nickel 5
Lead S
Zinc AL
Cyanide S
Mercury S
Silver AL
Selenium S
Arsenic S
Phenols S
NH3-N C
T.R.Chlor.AL
0.12
2.94
0.41
1.47
1.47
2.94
0.72
0.00
0.06
0.29
2.94
0.03
3.572 0.000 0.000 0.00
89.296 0.000 0.000 0.00
12.501 0.000 0.000 0.00
44.648 0.000 0.000 0.00
44.648 0.000 0.000 0.00
89.296 0.000 0.000 0.00
8.930 0.000 1.606 0.00
0.021 0.000 0.000 0.00
0.107 0.000 0.002 0.00
8.930 0.000 0.000 0.00
89.296 0.000 0.000 0.00
0.893 0.000 0.000 0.00
0.000 0.00
30.361 0.00
Limit
Monitor
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DIVISION OF ENVIRONMENTAL MANAGEMENT
Permits and Engineering/ NPDES Unit
Memorandum
TO: Technical Support Branch
(Modelers and Pretreatment)
Through: Coleen Sullins (',j
FROM: Randy Kepler YJ v
SUBJECT:
pew
July 23, 1992 � �'. (AV-1
•�•r,!'.L?'4.1.41r n". Yl savr+f'MrbrOb'�,.'..r.
Er11VED
JUL 2 7 1992
TECHNICAL SUPPORT BRANCH
City of Lexington
Lexington Regional WWTP/NC0055786
Davidson County
The City of Lexington is requesting their Silver and Cyanide monitoring
requirements be removed from their NPDES permit referenced above.
Attached is a copy of their comments and the supporting monitoring data for
the respective characteristic. Please review and comment if this is acceptable.
If you have any questions I'm at 733-5083( x553).
Thank You
cc. Winston-Salem Regional Office
Lei
rteecl
rue.)
jowl ,
7it izeziA
tAff-
a s , ,teek—, e- -
ac�e.. �r�-
/7-9 -

THE CITY OF
NORTH
July 9. 1992
77.
t+_i : ?.lt.rjj 'f it •.�
rt�J 6��„'�1\ i.t •.r f f
tJ �� !1 C• t
.. • t . 1 1
92J1J
LEXINGTON
CAROLINA
DEPARTMENT OF WATER RESOURCES
"GROWING WITH THE PIEDMONT"
Mr. Don Safrit
Permits Section
N.C. DEHNR - DEM
P.O. Box 29533
Raleigh, N.C. 27626-0535
RE: Permit Nc. NC0055786
Lexington Regional Wastewater Treatment Plant
Davidson County
1) •
•
SUBJ: Request to Re -Evaluate the Silver and Cyanide Monitoring
Requirements
33
Dear Mr. Safrit:
Per the attached letter dated 12/19/90, I am requesting that the
monitoring requirements for silver and cyanide be dropped from cur
NPDES Permit (NC0055786). I am attaching influent and effluent
data for cyanide and effluent data for silver.
The only detectable levels of cyanide found were eventually
determined to be due to interference in the test by residual
chlorine in the effluent. Since the effluents were dechlorinated,
we have found no trace of cyanide in the plant's effluent.
Please refer any questions to my attention at [phone]
ext. 244.
Sincerely,
CITY OF LEXINGTON
TI4JC14(-.
Roger Spach
Superintendent
RS/kb
Attachments:
cc: Dennis Roberts
Gisele Hedrick
28 WEST CENTER STREET • LEXINGTON, NORTH CAROLINA 27292 • PH. 704-243-2489

*9 v meLe
C ry�_�
State of North Carolina Us / ' ` •
Department of Environment, Health, and Natural Resources iz
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
0
I.�-.s7- 90
r
James G. Ninth. Govemor
1MWam W. Cobey, Jr., Secretary
Mr. R. D. Whisenant, City Manager
City of Lexington
28 W. Center Street
Lexington, NC 27292
Dear Mr. Whisenant:
George T. Everett, Ph.D.
Director
December 19, 1990
Subject: Permit No. NC0055786
Lexington Regional WWTP
Davidson County
In accordance with your application for discharge permit received on December
21, 1988, we are forwarding herewith the subject State - NPDES permit. This permit is
issued pursuant to the requirements of North Carolina General Statute 143-215.1 and
the Memorandum of Agreement between North Carolina and the US Environmental Protection
Agency dated December 6, 1983. In addition to the parts, measurement frequencies and
sampling requirements set out in said permit the City of Lexington is required to
conduct additional effluent monitoring for the following metals:
Cyanide: Monthly monitoring at detection less than
0.01 mg/1;
Cadmium: Monitor weekly, using graphite furnace
technique at 2 ug/l.
Silver: Monthly monitoring using graphite furnace 7
(detection level .less than 5 ug/1)
DEM also agrees to reevaluate the Cyanide and Silver monitoring requirements
after one year of data have been submitted by the City of Lexington.
If any parts, measurement frequencies or sampling requirements contained in
this permit are unacceptable to you, you have the r.i.ght to an adjudicatory hearing
upon written request within thirty (30) days foll.owing receipt of this letter. This
request must be in the form of a written petition, conforming to Chapter 150B of the
North Carolina General Statutes, and filed with the Office of Administrative Hearings,
Post Office Drawer 11666, Raleigh, North Carolina 27604. Unless such demand is made,
this decision shall be final and binding.
Please take notice that this permit is not transferable. Part II, E.4
addresses the requirements to be followed in case of change in ownership or control of
this discharge.
Poiludon Prevendon Pays
P.O. Box 27687. Raleigh. North Carolina 27611-7687 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

Mr. R. D. Whisenant
Page -2-
This permit does not affect the legal requirements Lo obtain other permits
which may be required by the Division of Environmental Management or permits required
by the Division of Land Resources, Coastal Area Management Act or any other Federal or
Local governmental permit that may be required.
If you have any questions concerning this permit, please contact Mr. Dale
Overcash at telephone number 919/733-5083.
cc: Mr. Jim Patrick, EPA
Winston-Salem Regional Office
Sin erely,
a..
a T.
lG

CYANIDE - INFLUENT
LEXINGTON REGIONAL WASTEWATER TREATMENT PLANT
DATE INFLUENT
CN- mg/1
1/14/91 40.01
2/19/91 40.01
3/13/91 <0.01
4/8/91 40.01
5/13/91 40.01
6/17/91 <0.01
7/8/91 <0.01
8/20/91 40.01.
9/18/91 40.01
10/14/91 <0.01
11/19/91 40.01
12/18/91 <0.01
3/24/92 <0.01
6/17/92 <0.01

CYANIDE — EFFLUENT
mg/1 --
DATE CN ug/ 1
1/14/91 40.01
2/19/91 40.01
3/13/91 0.012
4/8/91 0.04
5/13/91 0.048✓
6/17/91 0.013
9/18/91
10/14/91 0.01 /
11/19/91 40.01 *
12/18/91 z 0.01 *
1/27/92 40.01 * `-7
2/24/92 .0.01*
3/24/92 <0.01 *
4/21/92 <0.01 *
5/20/92 .0.01 *
6/17/92 L0.01 *
* Samples dechlorinated before analyses.
_,. 0102 - 0 7-'5
0.021✓
0��
04

DATE EFFLUENT
1/6/92 C5
1/13/92 <5
1/21/.92 45
1/27/92 45
2/3/92 45
2/10/92 < 5
2/17/92 45
2/24/92 45
3/2/92 4 5
3/9/92 45
3/16/92 c5
3/23/92 <5
3/30/92 45
4/6/92 45
4/13/92 45
4/20/92 45
4/27/92 <5
5/4/92 <5
5/11/92 <5
5/18/92 <5
5/26/92 45

Date Effluent
1/2/91
1/7/91
1/14/91
1/22/91
1/28/91
2/4/91
2/11/91
2/18/91
2/25
3/4/91
3/11/91
3/18/91
<5
<5
<5
<5
[5
<5
<5
<5
45
<5
G5
5
3/ 97 45
4/1/91 <5
4/8/91 45
4/15/91 <5
4/22/91 <5
A / 29/1 45.
5/6/91 <5
5/13/91 <5
-5/20/91 <5
55 / 28 L91
6/3/91 <5
6/10/91 <5
6/17/91 <5
6/24/91
<5
SILVER ug/1 - G.F.
Date
Effluent
7/1/91 < 5
7/8/91 45
7/15/91 45
7/22/91 <5
7129/91 <5 _
8/5/91 45
8/12/91 <5
8/19/91 <5
8/2-6/91
9/3/91 <5
9/9/91 <5
9/16/91 <5
9/23/91 <5
9/3nip►.-4Q 45-
10/7/91 45
10/14/91 <5
10/21/91 45
7 0/2/91
11/4/91
11/12/91 <5
11/18/91 <5
11/2fi/91 c5
12/2/91 _ 40
12/9/91
12/16/91
12/16/91
12/23/91
12/30/91
sue.
<5
<3
<5
45
<5
< 5
-\\r
‘p
Sk
)el\e"

IU NAME
IU#
PIPE #
FLOW LIMIT
MGD
CD LIMIT
MG/L
CD LOAD
LBS
CR LIMIT
MG/L
CR LOAD
LBS
CU LIMIT
MG/L
CU LOAD
LBS
LEXINGTON INDUSTRIES
6
1
0.1500
0.0075
0.1260
0.1550
CARDINAL STEEL DRUM COMPANY
1 0
1
0.0180
0.0230
1.1400
0.2850
DURACELL
11
1
0.0000
0.0000
0.0000
0.0000
DURACELL
11
2
0.0067
0.0000
0.0009
0.0000
DURACELL
11
3
0.0288
0.0000
0.0000
0.0000
COBLE DAIRY
21
1
0.1300
0.0330
0.0670
0.2500
0.0000
0.0000
0.0000
TOTAL ALLOWED FOR INDUSTRIES
ALLOW
CD 1.37
CR 21 .4Q
/.Y7
CU 668
TOTAL PERMITTED FOR INDUSTRIES
0.33
CD 0.06
CR 1 .33
CU 0.69
riTi I
STILL AVAILABLE FOR INDUSTRIES
LEFT
CD 1.31
CR 20.07
CU 5.99
C.;ze.)� /eeJ ��Guk0( 4//,,c,I,,,
o�a q
LEXINGTON IUP LOAD, 9/11/92, page 1

IU#
CN LIMIT
MG/L
CN LOAD
LBS
PB LIMIT
MG/L
PB LOAD
LBS
HG LIMIT
MG/L
HG LOAD
LBS
Mn LIMIT
MG/L
Mn LOAD
LBS
NI LIMIT
MG/L
NI LOAD
LBS
AG LIMIT
MG/L
AG LOAD
LBS
6
0.1020
0.1230
0.0008
0.0000
0.0525
0.0000
1 0
0.0000
3.2000
0.0008
0.0000
0.3800
0.0000
1 1
0.0000
0.0000
0.0150
0.0000
0.0000
0.0000
11
,
0005
`-)
0.0000
0.0005
0.0045
0.0053
(_0.0008
1 1
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
21
0.0000
0.1700
0.0050
0.0000
0.2500
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
0.0000
ALLOW
CN
0.50
FB
6.17
I-G
0.10
Mn
13.01
NI
1.69
AG
/•92_
ROO
I1_1Iv1
ON
0.10
FB
3.49
I-G
0.02
Mn
0.00
NI
0.69
AG
0.00
LEFT
CN
0.40
FB
2.68
I-G
0.08
Mn
13.01
NI
1.00
AG
2.30
LEXINGTON IUP LOAD, 9/11/92, page 2

IU#
ZN LIMIT
MG/L
ZN LOAD
LBS
O&G LIMIT
MG/L
O&G LOAD
LBS
NH3 LIMIT
MG/L
NH3 LOAD
LBS
BOD LIMIT
MG/L
BOD LOAD
LBS
TSS LIMIT
MG/L
TSS LOAD
LBS
6
0.4380
100
125.10
0.0000
585.00
120.00
10
2.2000
135.00
0.0000
1050.00
462.00
11
0.0000
0.00
0.0000
0.00
0.00
11
0.0030
0.00
0.0000
0.00
0.00
11
0.0000
0.00
0.0000
0.00
0.00
21
0.6100
100
108.42
0.0000
9900.00
1975.00
0.0000
0.00
0.0000
0.00
0.00
ALLOW
ZN
11.-19
O&G
NH3
2498.00
BOO
107,75.00
TSS
5187-._00
ZN
3.25
O&G
368.52
NH3
0.00
BOD
11535.00
TSS
2557,00
FT fv1
LEFT
ZN
7.94
O&G
-368.52
NH3
2498.00
BOD
-760.00
TSS
2630.00
LEXINGTON IUP LOAD, 9/11/92, page 3

1
FILE COI
State of North Carolina
Department of Environment, Health and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27604 ;t
James G. Martin, Governor,,
William W. Cobey, Jr., Secretary
Regional Offices ` ` r' s
Asheville t`
704/251-6208 Gi'se 1e� •Hedrz. ck
Industrial Waste Chemist
Fayetteville City oof.' Lexington*
919/486-1541 283`West:s Center Street
Lexington; N. C. 27291
Mooresville • :_ {
704/663-1699 Subject:_ Headworks Analysis
City of Lexington
Raleigh Davidson County
9 1 9/571-4700
Dear Ms. Hedrick:
Washington
June 1
, 1992
Review
George T. Everett, Ph.D
= Director
;2
919/946-6481 The pretreatment staff of the Division of Environmental
Management has reviewed the revised headworks analysis submitted
Wilmington by the City of Lexington for the Regional Wastewater Treatment '
919/395-3900 PlanOnd received by the Division on May 12 , 1992 The Division
concurs with your calculated allowable industrial loading rates
Winston-Salem for BOD, TSS, ammonia, cadmium, chromium, copper, cyanide, lead,
919/896-7007 nickel, silver and zinc. Therefore, when the Division reviews
the pretreatment permits issued to significant industrial users
discharging to the Lexington Regional WWTP, we will approve
permit limits which do not exceed your established allowable
loading rates. These rates are as follows:
Parameter
•
Allowable industrial loading
rates (lb/day)
- BOD 9767
TSS 4874
NH3 1883
Cd 0.98
Cr 8.15
Cu 1.47
CN 0.41
Pb 1.99
Ag 1.92
Zn 1.02
Pollution Prevention Pays
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone]
An Equal Opportunity Affirmative Action Employer •

1
Burlington
Resea rch
ANNUAL POLLUTANT ANALYSIS
LEXINGTON REGIONAL WWTP
NPDES# NC0055786
JUNE 1992
Burlington Research, Inc. • P. O. Box 2481 • Burlington, NC 27215 • Telephone [phone]

ANNUAL POLLUTANT ANALYSIS MONITORING REQUIREMENT
REPORTING FORM A
(Revised June 1990) •
1. Factlity Information!
NPDES Permit No: NC0055786 Discharge (Pipe) No: 001 Year: 1992
Facility Name: Lexington Regional WWTP Class: IV County: Davidson
Person(s) Collecting Samples: Gisela Hendrick
Status of facility wastewater treatment operation on day of sampling: Typical : Yes_ No
If no, explain briefly:
Analytical Laboratory: Burlington Research. Inc. (WO# 92-06-291)
II. Sampling
24 hr ;composite for main sample/grab sample for purgeable fraction
Date Sampled: (composite sample)
Sampling begun (date, tiara): Tuesday. June 16. 1992: 00:00 AM
Sampling finished (date, time): Wednesday. June 17. 1992: 00:00 AM
Date and time sampled (grab sample): Wednesday. June 17. 1992: 00:00 AM
Corresponding sample taken for toxicity testing:
Yes (BRI WO# 92-06-292 & 92-06-367) No
Page 1 of 13

INSTRUCTIONS
The purpose of this document cnd the NC DEHNR memo of October 30, 1990 (Tedder)/mailing of December 1990 is to standard-
ize the sampling, analysis and reporting procedures to be used for the Annual Pollutant Analysis Monitoring (APAM) Require-
ment as described in the permit.
1 - Take a 24-hour composite sample from the final effluent during mid -week (Wednesday through Friday). Collect a grab
sample for the volatile organic fraction when collection of the 24-hour composite sample is completed. Follow any other
sampling instructions provided by the laboratory performing the analysis.
2 - Indicate in the space provided on Page 1 of 13 this page whether a corresponding sample for toxicity testing was taken.
3 - Make note of any unusual wastewater treatment operating conditions occurring on the day of sampling in the apace pro-
vided on Page 1 of 13.
. ls
4 - Analyze the effluent for pollutants listed on the APAM form, including those to be identified and approximately quan-
tified under the 10 significant peaks rule, using appropriate EPA -approved methods for each of the analytic fractions.
Other analytical methods can be substituted only with prior, written approval of the Director of the Division of Environmen-
tal Management (DEN). Read and distribute to the laboratory performing the analysis the accompanying m.mo (Tedder, October
1990) clarifying analytical requirements.
5 - Identify chemicals to be analyzed for according to the 10 significant peaks rule (as described in Item 2 of the Annual
Pollutant Analysis Monitoring Requirement in the permit) using a GC/MS library search. Tentative identification is all that
is required; confirmation by standard injection is not necessary. Estimate the concentration of each based on an internal
standard having the closest retention time.
Bsoorr=
6 - Quantitation Limit Targets that should be met are listed on this Revised APAM Reporting Form A. Report the use of any
higher quantition limit and an explanation as to why the listed quantitation limit target could not be met. Examples of
acceptable reasons for not meeting a quantitation limit target could be high background concentrations in a sample, or the
necessity for sample fraction dilution to bring a chemical to within a quantifiable concentration. List any quantitation
limit different (whether higher or lower) from the target in the column provided for the purpose.
7 - If a chemical is found to be below the quantitation limit, report the concentration detected as less than (or '<o) the
quantitation limit in the appropriate space. Provide a concentration estimate for chemicals detected in concentrations
greater than the detection limit and less than the quantitation limit. Enter the detection limit in parentheses beside the
estimate. Chemicals detected in concentrations above the quantitation limits must be quantified. Quantitation limit and
detection limit are defined in the NC DEHNR memo (Tedder, October 1990). Enter the total number of peaks detected in
each analytic fraction in the appropriate space on this Revised APAM Form A. Report all concentrations in units of micro-
grams per liter (ug/L) and metals as total recoverable metal. If no peaks to be identified under the 10 significant peaks
rule are observed, enter "none" in the space provided for "other" compounds in each appropriate analytic fraction section.
Provide the concentration estimate and retention time for "unknowns" as welt as for "significant peaks" fa' which a struc-
tural assignment can be made.
8 - If "significant peaks" are found, provide probable molecular weight, library match probability, retention time, ident-
ification basis, and MS scan number each. In addition, list internal otandards and their retention times.
9 - In the section labeled NOrganic Analytical Information", (Page 11 of 13) include for each organic fraction the method,
extraction technique, GC operatin.; conditions, end surrogate recovery. Report the size of the GC/i4S library b:in:g utilized
in the appropriate space.
10 - Use copies of this Annual Pollutant Analysis Monitoring Revised Form A to report the results of the analysis. Both
the analytical laboratory representative and the facility operator in responsible charge should sign cceptetad forms
(last page).
11 - Mail two completed copies of the form (and the laboratory report, if submitted to the facility on a different form)
to: ATTN: Central Files, Division of Environmental Management, NC DEHNR, P.O. Box 27687, Raleigh,' NC 27611. Mail the APAM
form separately from Discharge Monitoring Reports,
Page 2 of 13

A. Purgeable (Volatile organic) Fraction, EPA Method 624
Number of chemicals detected in Fraction 1
Fraction STORET Number 84085
STORET
Number Compound
Quantitation
Limit Target
Quantitation
Limit*
Concentration
Detected
GC/kS
Corfirmation?
1. Pollutants to be analyzed for:
(ug/L)
(ug/L)
(u8/L)
'es
No
1
Acro o n
100
2.5
ND
..-vii-
15-
Acrylonitrile
100
2.5
ND-
-
—Ur
34030
-MT-
Benzene
5
9.
-32TUr
Bromodichloromethane
5
1
ND
---va.---
Bromoform
5
1
ND
Yes
Bromomethane
10
1
Tp
..,.-
--"-fps"—
---
32102
Carbon tetrachloride
5
1
ND
34301
Chlorobenzene
6
1
ND
—
---In_
"`-
34311
Chloraetaane
10
1
N
3 76
2-Chloroethyl vinyl ether
10
1
ND
Yes
32TW
-S410$-
Chloroform
5
1
2.0
Yes
Chloromethane
10
';,
u
32105
Dibromochloromethane
5
" yes
9
-34531-
1,1-Dichloroetliane
5
1
""Yss
—Tr—a
---
-3450f
1,2•Dichloroethane
5
1
`,
1,1-Dich[oroethy(ene
5
ND
as
W
`34341-
trans-1,2-Dich(oroethylene
5
1
ND
Yeses
1,2-Dichloropropana
6
1
ND
"' "'
34704
cis 1,3•Dichloropropene
5
1
ND
Yeses
)6699
-31371-
trans 1,3-Dichtoroprapene
5
1
NO
.. YQa
3 3-
Ethylbenzene
8
1
ss—
Nothy[ene chloride
5
1
ND
yes
'•' fcs
•"'4'ea--
`es
-------
34516
-UM-
1,1,2,2•Totrac%[oroehtane
7
1
ND
Tstrach[oroethylene
5
1
ND
0
'SO06
-
Tolusne
6
1
ND
1,1,1-Trichloroethane
5
1
ND
Yes
3
-39180
1,1,2•Trichloroethene
5
1
ND
Trichloroethylene
5
1
ND
---f' `
lair
9175-
-1-17-2
Trich[orofluromethane
10
1
ND
Yes
Vinyl chloride
10
1
MD
—Yoa"
fferent from auantitetien limit tarawt_
ND'None Detected. < and < > : As per instructions.
Page 3 of 13

A2. Other Purgeables (up to 10 highest peaks).
Compound
Probable
Molecular
Wight
Est.
Conc.
(ug/L)
-"
Library Match
Probability
(%)
Retention
Time (RT)
(Min)
ldentification 1aie
(Chock all that epplyf
Scan
Number
Library
Match
Manual
Interpretation
RT
None
-
-
IINNI
Complete only if non -targeted compounds are present:
Internal Standard
1,4 - Dif Cuorobenzene
Chlorobenzene - dS
Retention
Time
(Min)
19.57
27.03
Page 4 of 13

B. Acid Extractable Fraction, .:.r.. Method
Number of chemicals detected in Fraction
Fraction STOREY Number 45582
625
2
STORE?
Number Compound
Quantitation
Limit Target
Guantitation
Limit*
Concentration
Detected
GC/MS
Confirmation?
1. Pollutants to be analyzed for:
(ug/L)
(ug/L)
(ug/L)
'es
No
-US'—"
-C oro- -met y • eno
10
ND
W
2-Chloropheno[
10
iD
"" -.
-341603-
2,4-Dicl►olorophenol
10
ND
"'Yes
2,4-Dimethylphenol
10
ND
Yes
Yeses
114037
-3465T
"3
2,4-Dinitrophenol
50
ND
2-Nethyl-4,6-dinitrophenol
50
ND
""'Tes
9f
2-Nitrophenol
10
ND
— e
1-7
4-Nitrophenol
50
ND-
-
39032-
Pentachlorophenol
50
RD
Phenol
10
ND
Ys
-w-Tra
2,4,6-Trichlorophenol
10
ND
—lir-
fferent from auantitatinn limit
tarait�'-
ND=None Detected. < and < > : As per instructions.
Page 5 of 13

W. Other Acid Extractebles (up to 10 highest peaks).
Compound
Probable
Molecular
Weight
Est.
Conc.
(ug/L)
-'18
Library Match
Probability
(%)
Retention
Time (RT)
(Min)
identification Sgsi•
(Check el that apply)
Scan
Number
Library
Match
Manual
Interpretation
CT
Hexadecenoic Acid
3-Hexadccanol
256
76
24.64
X
—
326
-4—
242
11—
40
35.42
—
Complete only if non•targeted compounds are present:
Internal Standard
1,4 - Dichtorcbentene - d4
Naphthalene - d8
Retention
Time
(Min)
10.35
Acenaphthene - d10
Phenanthrene - d10
Chrysene - d1f
Perylene - dFZ
14.07
19.63
24.30
32.90
40.22
Page 6 of 13

C. Base/Neutral Fraction, EPA Method 5
Number of chemicals detected in Fraction
Fraction STORET Number 45583
STORET
Number Compound
Quantitation
Limit Target
Quantitation
Limit*
Ccncentration
Detected
GC/MS
• Confirmation?
1. Pollutants
to be analyzed for:
(ug/L)
(ug/L)
(ug/L)
'es
No
f 1
Acena• t ene
10
ND
—T!3-
34200
Acenaphthylene
10
ND
—'Ye—
3Z225'
Anthracene
10
ND
des
30Y20
"33-
Benzidine
50
NO-
`3426T
Benz (a) anthracene
10
ND
—lir-
Benzo (a) pyrene
10
NO
--lii___
34230
Basso (b) fluoranthene
10
ND
`des "`
34521
Benzo (ghi) perylene
10
ND
---m-- -
34242
Benzo (k) fluoranthene
1b
NO
34278-
-3C273-
Bis(2-chloroethoxy) methane
10
$0
-"'-
Bis(2-chloroehyl) ether
10
ND
-'-'Y--
—li
3C233-
Bis(2-chloroisapropyl) ether
10
ND
39100
Bis(2-ethylhexyl) phthalate
10
ND
—var.—
4-Bromophenyl phenyl ether
'
10
ND
—Y"es`
34292'
Butyl benzyl phthalate
10
ND
•es
3458i'
2-Chloronaphthalene
10
ND
r
4-Chlorophenyl phenyl ether
10
RD
--
Chrysene
10
ND
mat
3-
Dibenz (a,h) anthracene
10
kD
e;
3036
1,2-Dichlorobenzene
10
ND
-" es
63-
1,3-DicF.lorobenzene
10
ND
34571-
1,4-Dlchlorobenzene
10
ND
`Yes
34631
3,3-Dichloroberzidine
20
N0
Yes
34336
Diethyl phthalate
10
ND
---Yes
—'
Dimethyl phthalate
-
10
ND
---rts—
39110
Di-n-butyl phthalate
10
ND
--—
2,4-Oinitrotoluene
10
pD
'-
-"'P.m...
2,6-Dinitrotoluene
10
ND
___
39
Di-n-octyl phthalate
10
"'rx"-
""-
3W
3076
-3438v
Clent7;umd_
1,2-Diphenylhydrazine
30
'es
Fluoranthene
10
---fie—
Fluorene
ensue,... na.e.....A , ....r .
10
, .. ... -------••--=---
`',
a
�.....�.._.
�_
•
•
Page 7 of 13

C. Base/Neutral Fraction (Continued)
STORET
Number
Compound
1. Pollutants to be analyzed for:
Hexac or•• nzene
M91 Hexachlorobutadiene
386 Hexachlorocyclopentadiene
34396 Hoxachloroethane
34403 Indeno(1,2,3-cd) pyrene
I sopinorone
74303- Naphthalene
Nitrobenzene
N-nitrosodimethylamine
34428 N-nitroso-di-n-propylamine
N-nitrosodiphenylamfne
31 Phenanthrene
Pyrene
-raw- 1,2,4-Trichlorabenzene
0uantitation
Limit Target
(ug/L)
i0
10
10
10
10
10
10
10
10
10
10
10
10
10
—TM-different from quantitation target.
ND•None Detected. < and < > Is As per instructions.
0uantitation
Limit*
(ug/L)
Page 8 of 13
Concentration
Detected
(ug/L)
ND
NO
NO
ND
ND
ND
ND
ND
ND
ND
ND
NO
N0
GC/HS
Confirmation?
Yes
No

C2. Other.Base/Neutrals (up to 10 highest peaks).
Compound
2-Butyl
Probable
Molecular
Weight
Est.
Conc.
(ug/L)
—'—
Library Match
Probability
(%)
Retention
Time (RT)
(Min)
Identification id •
(Check all that ly)
Scan
Number
Library
Match
Manuel
Interpretation
PI
—"
Tetrahydro-furan
28
46
19.50
—`
- '"
4,8,12-Trimethyl-3,7-11-Tridecatrienoic
264
24—
b8
36.29
'— -'-'
—
3575
Acid, Methyl Ester•
•
•
Complete only if non -targeted compounds are present:
Internal Standard
1,4 - Dichlorobenzene - d4
Naphthalene - d8
Retention
Time
(Min)
10.35
Acenaphthene - d10
Phenanthrene
Chrysene - d12
Perylene - d12
14.07
19.03
24.30
32.90
40.22
Page 9 of 13

D. 0rganochlorine/Organophosphcsus Pesticides and PCB's
Number of chemicals detected in Fraction 0
Fraction STORET Kurber 00188
STORET
Number
Compound
Quantitation Quantitation
Limit Target Limit*
1. Pollutants to be analysed for: (ug/L)
Organochlorine Pesticides/PCB's: EPA Method 8080
A •r n
▪ 337- alpha-6HC
- 330 B• eta-BHC
- 3Z250- D• elta-BHC
39340 Gamma-BHC (Lindane)
39350 Chlordane
39310 4,4'-DDD
39320 4,4'-DDE
39300 4,4'-DDT
- 30355- Dieldrin
-3Z36T Endosulfan 1 (alpha)
- 0 E• ndosulfan 11 (beta)
-MST- Endosulfan sulfate
-30305- Endrin
34366 Endrin aldehyde
39410 Heptachlor
39420 Heptachlor epoxide
94150- - Methoxychlor
• 755- M• irex
- - Toxaphene
PCB 1016
IO$0 PCB 1221
39492 PCB 1232
39496 PCB 1242
- 0 PCB 1248
PCB 1254
08 PCB 1260
(ug/L)
0.05 0.25
0.05 0.25
0.05 0.25
0.1 0.25
0.05 0.25
0.2 0.25
0.1 0.25
0.1 0.25
0.1 0.25
0.02 0.25
0.1 0.25
0.1 0.25
0.7 0.25
0.06 0.25
0.2 0.25
0.05 0.25
0.8 0.25
0.5 0.25
0.2 0.25
2.4 2.5
0.5 1.0
0.5 1.0
0.5 1.0
0.5 1.0
0.5 1.0
1.0 1.0
1.0 1.0
Concentrbtion
Detected
(ug/L)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Confirmation?
Dual"Col. GC/MS
es No
ND
ND
ND
tiD
NO
ND
ND
ND
ND
ND
ND
Np
ND
ND
ND=None Detected. < and < > a As per instructions.
* Values listed are quantitation limits consistently achievable in wastewater matrices.
Page 10 of 13
ND
•
w
Yes
4.111.10
411,
No

D. Pesticides (Continued).
STORET Compound
Number
Quatitation
Limit Target
Quantitation
Limit*
Concentration
Detected
Confirmation?
Dual Col.
GC/MS
1. Pollutants
0rganophosphorus
to be analyzed for:
Pesticides: EPA Method
(ug/L)
625/8080
(ug/L)
(ug/L)
VIM
-Q—
No
Yes
Y
--
No
--
—
39560
Denton
2.5
ND
—
0
Parathion (ethyl)
0.6
ND
E. Herbicides, EPA Method 8150
Number of chemicals detectedin Fraction 0
Fraction STORET Number 00148
STORET
Number Compound
- Quantitation -
Limit Target
Quantitation
Limit*
Concentration
Detected
Ccnfirmation?
Cual Column
1. Pollutants
to be analyzed for:
(ug/L)
(ug/L)
(ug/L)
Yes
No
39730
2,4-D
12
0.2
*0
'—'--
No
39045
Silvex
2
0.2
Np10745-
No
2,4,5-T
few auantitatinn unlit
2
0.2
N
,_____
-""No
1Tdtfferent
ND=None Detectable.
< and < > . As per instructions.
Organic Analytical Information:
Organic Fraction
Method
Extraction
GC Operating Conditions
Column Description
Surrogates (Spikes)
Batch
Continuous
Length X ID, Film Thickness,
Column Type, Carrier Gas & Flow
Rate, Temperature Program
Compound
Recovery
X
Purgeable
N/A
75m x 0.53mn,3.0mm, DB-624
Bromofluorobenzene
195
_
He, 5cc/min. 36° C (9 Min).
1,2-Dichloroethano.d4
230
180°C 0 6°C/min. 2Q0°C, 10°C/min.
Toluene-d8
` T—
Acid Extractable
X
30m x 0.32mm, 1.0mm, DB-5
2-Fluorophenol
He, 2cc/min., 40°C (4 min)
Phenol -cis
320° C, 8 C/min.
2,4,6-Tribre enol
33
Base/Neutral Ext.
X
30m x 0.32mm, 1.0mm, DB-5,
2-Fluorobiphenyl
-737
He, 2cc/min., 40"C (4min)
Nitrobenzene-d5
245
320° 0, 8° t/min.
4-Terphenyl-d14
144
Example:
Acid Extractable
625
X
30m x 0.25mm, 0.21un, DB-5,
He, 30 cmmsec, 4g C (4 min) -
270 C, 10 /min
d5-Phenol I
GC/MS Library size (number of reference spectra):
42.222
Page 11 of 13

F. Metals and Other Chemicals
Number of Metals and Other Chemicals (as listed below) detected in Sample 6
Fraction STORET Number 78240
STORET
Number
Compound
1. Pollutants to be analyzed for:
A uminum
0- 107- Antimony
01002 Arsenic
01012 Beryllium
01027 Cadmium
- 36 Chromium
0orr Copper
'0105f" Lead
ligUr Mercury
11o67 Nickel
0i 7- Selenium
3fi077- Silver
2 Zinc
2. Other Inorganics:
Quantitation
Limit Target
(u9/L)
50
50
10
25
2
5
2
10
0.2
10
5
5
10
Quantitation
Limit*
(ug/L)
10**
5**
5**
5**
0.5**
5**
2**
5**
0.2
5**
5**
5**
5
Concentration
Detected
(ug/L)
280
BDL
RL
ebL
2
BOL
BBL
6
' BDL
BOL
52
01007
Barium
506
100
B$L _
00940
-00720
Chior fde
1000
50050
Cyanide
20
5
,e�__--
—7If-different
Fluoride
100
100
830
from nuantitetien limit
tnrnat
•* Lowest Quantitation Limit attainable by Graphite Furnace AA. Mercury analyzed by Cold Vapor Method. Ziiic and
Barium analyzed by Flame ;.
liDL As Below Detection Limit
Page 12 of 13

•
Analytical laboratory Rcpresantsti>'eo:
41
tJ,
Steven G. Yocklovich
Director, Chromatography Services
Richard A. Diehl
Director, Environmental Services
ToLm &3, L-ae`. Date
Facility Operator in Responsible Charge (ORC):
/11,64„//i /Klie. it
1 certify that th,,s,port is accurate nd complete to the best of my knowledge:
Signed:
r"?
Page 13 of 13
Date:
'7 a 9a