310057_Lab Data_20220223

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
NCDENR-DWR
Date of Report: Mar 07, 2022
127 N. Cardinal Drive Ext.
Customer PO #:
Wilmington NC 28405
Customer ID: 09010049
Attention: Chad Coburn
Report #: 2022-03464
Project ID: Hog Waste (2nd sample)
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-08180 Site: Upstream
2/23/2022 3:50 PM Water Coburn/Ryan
Test
Method Results Date Analyzed
Fecal Coliform
SM 9222 D-2015 MF <20 Colonies/100mL 02/23/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-08181 Site: Upstream
2/23/2022 3:50 PM Water Coburn/Ryan
Test
Method Results Date Analyzed
Ammonia Nitrogen
EPA 350.1, Rev. 2.0,1993 0.6 mg/L 03/01/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1993 0.31 mg/L 02/28/2022
Total Phosphorus
SM 4500 P (F-H)-2011 < 0.04 mg/L 03/04/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0,1993 20.7 mg/L 03/02/2022
Total Nitrogen
Total Nitrogen 2 1. 0 mg/L 03/04/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-08182 Site: Waste Source
2/23/2022 3:25 PM Water Coburn/Ryan
Test
Method Results Date Analyzed
Fecal Coliform
SM 9222 D-2015 MF 6000 Colon ies/1 00m L 02/23/2022
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-08183 Site: Waste Source
2/23/2022 3:25 PM Water Coburn/Ryan
Test
Method Results Date Analyzed
Ammonia Nitrogen
EPA 350.1, Rev 2.0, 1993
210 mg/L
03/01/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1993
0.08 mg/L
02/28/2022
Total Phosphorus
SM 4500 P (F-H)-2011
1.20 mg/L
03/04/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0,1993
268 mg/L
03/02/2022
Total Nitrogen
Total Nitrogen
268 mg/L
03/04/2022
Report #.. 2022-03464 Page 1 of 2

[qlvirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
NCDENR-DWR Date of Report: Mar 07, 2022
127 N. Cardinal Drive Ext. Customer PO #:
Wilmington NC 28405 Customer ID: 09010049
Attention: Chad Coburn Report #: 2022-03464
Project ID: Hog Waste (2nd sample)
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-08184 Site: Downstream 2/23/2022 3:40 PM Water Coburn/Ryan
Test Method Results Date Analyzed
Fecal Coliform SM 9222 D-2015 MF 500 Colonies/100mL 02/23/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-08185 Site: Downstream 2/23/2022 3:40 PM Water Coburn/Ryan
Test
Method
Results
Date Analyzed
Ammonia Nitrogen EPA 350.1, Rev. 2.0,1993
26.6 mg/L
03/01/2022
Total Phosphorus SM 4500 P (F-H)-2011
0.13 mg/L
03/04/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993
5 1. 0 mg/L
03/02/2022
Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993
0.08 mg/L
02/28/2022
Total Nitrogen Total Nitrogen 51.1 mg/L 03/04/2022
Comment:
Reviewed by:
Report #:: 2022-03464 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392
Sample Receipt Checklist .0223
Client: I�1C,pt�7�J jZ— W���.rn,�N6MYDJP Z Z.
ate: Z --- _ Report Number: _ 2022- 03 (o
Receipt of sample: ECHEM Pickup ❑ Client Delivery UPS ❑
❑ YES ❑ NO FedEx ❑ Other ❑
N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
How temperature taken: ❑ Temperature Blank Against es 'C
IR Gun ID: Thomas Traceable S/N: 210835468 IR Gun Correcti nFactoB Ct10 0
❑ YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES ❑ NO 4. Were per custody procedures (relinquished/received) followed?
YES ❑ NO 5. Were sample ID's listed on the COC?
YES ❑ NO 6. Were samples ID's listed on sample containers?
YES ❑ NO 7. Were collection date and time listed on the COC?
YES ❑ NO 8. Were tests to be performed listed on the COC?
YES ❑ NO 9. Did samples arrive in proper containers for each test?
YES ❑ NO 10. Did samples arrive in a . qr�:'Lion
11:1 NO 11 'Alas adegUate sample volume available?' ----- -- - -!
YES ❑ NO 12. Were samples received within proper holding time for requested tests?
❑ YES NO 13. Were acid preserved samples received at a pH of <2?
❑ YES ❑ NO 14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volati'es are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sampie(s)ZZ-•0818( 081$3 &18S ,,,sere received incorrectly preserved and were adjusted accordingly
adding (circle one): ZSOHNO3 HCI NaOH
ITby
ime of preservation: Y "S
more than one preservative is needed, notate in comments below
Note: Notify customer service immediat ly for incorrectly preserved samples. obtain a new sample or
notify the state lab if directed to analyzed by the customer. who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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