NC0027103_NPDES Permit Renewal_20031120

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State of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
William G. Ross, Jr., Secretary
Alan W. Klimek, P.E., Director
November 20, 2003
Mr. McDuffie Cummings
Town of Pembroke
PO BOX 866
PEMBROKE NC 28372
CDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
Subject: NPDES Permit Renewal Application
Permit NC0027103 ..
Pembroke WWTP
Robeson County)
Dear Mr. Cummings:
The NPDES Unit received your permit renewal . application on November 17, 2003. Thank you for
submitting this package. The renewal request did not include a sludge: management plan. Please
submit a sludge management plan.
The permit renewal for this facility will be assigned to Dawn Jeffries. -Oils staff member will contact you
if further information is needed to complete the permit renewal. Please note that the NPDES Unit has
several vacant positions. This staff shortage has lasted for. over 4 years and is delaying all permit
renewals. Our remaining permit writers are currently reviewing Authorizations to Construct, speculative
limit requests, major permit modifications and 201 plan updates ahead! of permit renewals. This is
necessary due to a variety of factors, including mandatory deadlines in the statutes which govern our
program.
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If this staff shortage delays reissuance of NC0027103 the existing !requirements in your permit will
remain in effect until the permit is renewed (or the Division takes other action). We appreciate your
patience and understanding while we operate with a severely depleted staff. If you have any additional
questions concerning renewal of the subject permit, please contact Dawn Jeffries at [phone],
extension 595.
cc: Fayetteville Regional Office, Water Quality Section
NPDES_File--�
Central Files
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
VISIT US ON THE INTERNET @ http://h2o.enr.state.nc.us/NPDES,
Sincerely,
Valery Stephens
Point Source Branch
919 733-5083, extension 520 (fax) 919 733-0719
[e-mail]

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SUPPLEMENTAL APPLICATION INFORMATION:
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
FORM
2A
NPDES
APPLICATION OVERVIEW
PERMIT ACTION REQUESTED: RIVER BASIN:
Renewal Lumber
Form 2A has been developed in a modular format and consists of a "Basic Application Information" packet
and a "Supplemental Application Information" packet. The Basic Application Information packet is divided
into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or
equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental
Application Information packet. The following items explain which parts of Form 2A you must complete.
BASIC APPLICATION INFORMATION:
A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works
that discharges effluent to surface waters of the United States must also answer questions A'.9 through A.12.
Fr -a
B. Additional Application Information for Applicants with a Design Flow >_ 0.1� mgd. All treatment works thatLhave d—e�sign flows
greater than or equal to 0.1 million gallons per day must complete questions B.11through B.6.
C. Certification. All applicants must complete Part C (Certification). li ! ; f
il L� ', , NOV 1 7 2003
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D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface'waters;,of,the UnitedfStates and meets
one or more of the following criteria must complete Part D (Expanded Effluent Testing Data):
1. Has a design flow rate greater than or equal to 1 mgd,
2. Is required to have a pretreatment program (or has one in place), or
3. Is otherwise required by the permitting authority to provide the information.
E. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E (Toxicity Testing
Data):
1. Has a design flow rate greater than or equal to 1 mgd,
2. Is required to have a pretreatment program (or has one in place), or
3. Is otherwise required by the permitting authority to submit results of toxicity testing.
F. Industrial User Discharges and RCRA/CERCLA Wastes. A treatment works that accepts process wastewater from any
significant industrial users (SIUs) or receives RCRA or CERCLA wastes must complete Part F (Industrial User Discharges
and RCRA/CERCLA Wastes). SIUs are defined as:
1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations (CFR) 403.6 and
40 CFR Chapter I, Subchapter N (see instructions); and
2. Any other industrial user that:
a. Discharges an average of 25,000 gallons per day or more of process wastewater; to the treatment works (with certain
exclusions); or
b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic
capacity of the treatment plant; or
c. Is designated as an SIU by the control authority.
G. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G (Combined Sewer
Systems).
ALL APPLICANTS MUST COMPLETE PART C (CERTIFICATION)

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FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal ,'
RIVER BASIN:
Lumber
BASIC APPLICATIONS INFORMATION`
'..
'
`gym".
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PARTsA BASIC APPLICATIONrINFORMATION FOR ALL APPLICANTS
All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet.
A.1. Facility Information.
Facility Name Town of Pembroke
• i ,
Mailing Address Post Office Box 866
Pembroke, NC 28372
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Contact Person McDuffie Cummings
Title Manager
Telephone Number [phone]
Facility Address 8257 Deep Branch Road
(not P.O. Box) Pembroke, NC 28372
A.2. Applicant Information. If the applicant is different from the above, provide the following:
Applicant Name
!
Mailing Address
Contact Person
Title
I �
Telephone Number ( )
Is the applicant the owner or operator (or both) of the treatment works?
0 owner ❑ operator
Indicate whether correspondence regarding this permit should be directed
❑ facility ❑ applicant
A.3. Existing Environmental Permits. Provide the permit number of any
(include state -issued permits).
NPDES NC0027103
to the facility or the applicant'
existing environmental perm
PSD
Other
Other
and areas served by the
(combined vs. separate)
Type of Collection
Separate
is that have been issued to the treatment works
UIC
Collections WQ0013729
RCRA
,
A.4. Collection System Information. Provide information on municipalities
entity and, if known, provide information on the type of collection system
Name Population Served
Town of Pembroke 2,600
facility. Provide the name and population of each
and its ownership (municipal, private, etc.).
System Ownership
I ! Municipal
I
Total population served
—
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FACILITY NAME AND. PERMIT NUMBER:
Town of Pembroke,'NC0027103
P i
PERM IT ACTION REQUESTED:
Renewal "
RIVER BASIN:
Lumber
A.5. Indian Country.
a. Is the treatment works located in Indian Country?
❑ Yes ® No
b. Does the treatment works discharge to a receiving water that is,either in Indian Country or that id upstream from (and eventually flows
through) Indian Country?
0 Yes
® No
A.6. Flow. Indicate the design flow rate of the treatment plant (i.e., the wastewater flow rate that the plant was built to handle). Also provide the
average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period
with the 12s' month of "this year" occurring no more than three months prior to this application submittal.
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a. Design flow rate 1.33 mgd
Two Years Ago
Last Year This Year
b. Annual average daily flow rate .61 MGD .47 MGD .77MGD
c. Maximum daily flow rate
2.04 MGD
.97 MGD 2.30MGD
A.7. Collection System. Indicate the type(s) of collection system(s) used by the treatment plant. Check all that apply. Also estimate the percent
contribution (by miles) of each:
® Separate sanitary sewer 100
0 Combined storm.and sanitary sewer
A.8. Discharges and Other Disposal Methods.
a. Does the treatment works discharge effluent to waters of the U.S.?
® Yes
❑ No
If yes, list how many of each of the following types of discharge points the treatment works uses:
i. • Discharges of treated effluent
ii. Discharges of untreated or partially treated effluent
iii. Combined sewer overflow points
iv. Constructed emergency overflows (prior to the headworks)
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• N/A
N/A
N%A
v. Other NIA
b. Does the treatment works discharge effluent to basins, ponds, or other surface impoundments
that do not have outlets for discharge to waters of the U.S.? 0 Yes
If yes, provide the following for each surface impoundment:
Location: -
® No
Annual average daily volume discharge to surface impoundments)
Is discharge 0 continuous or 0 intermittent?
c. Does the treatment works land -apply treated wastewater?,
If yes, provide the following for each land application site:
Location:
Number of acres:
Annual average daily volume applied to site:
Is land application
mgd
❑ Yes ® No
0 continuous or 0 intermittent?
mgd
d. Doesthe treatment works discharge or transport treated or untreated wastewater to another
treatment works? I ❑ Yes ® No

PERMIT NUMBER: NC0027103
FACILITY NAME: Town of Pembroke - Pembroke WWTP
CITY: Pembroke
OUTFALL: 001
EFFLUENT
COUNTY: Robeson
PERIOD ENDING MONTH: 11 - 2002
REGION: Fayetteville
DMR 12 Month Calculated
PAGE 1 OF 3.
00010 '
deg c
Temperature,
Water Deg.
Centigrade
00300
mg/1
DO, Oxygen,
Dissolved
•
00310
lbs/day
BOD, 5-Day (20
Deg. C)
00310
mg/1
BOD, 5-Day (20
Deg. C)
00340
mg/1
COD, Oxygen -
Demand, Chem.
(High Level)
00400
su
pH
00500
mg/1
Solids, Total
00530
lbs/day -
Solids, Total
Suspended
125
18
125
19.85625
8.566667
5.222222
- -
6.7 - 7.5
-
1 - 02
125
18
__
15.918182
9.473333
4.478571
6.2 - .7
2-02
125
18
125
16.33
8.584615
4.684615
6.7 - 7.3
3-02•125
18
125
17.533333
8.425
4.741667
6.5 - 7.2
4-02.
125
18
125
21.052381
8.027692
5.338462
7.02 - 7.54
5-02
125
18
_
125
23.034783
7.65
4.914286
- -
6.24 - 7.51
6-02
125
18
125
25,57
7.05
3.95
6.16 - 7.19
7 - 02
125
18
125
27.486364
6.626667
3.6
(
6.21 - 7.45
-
8 - 02
125
18
125
27.745455
6.3
.
.2.425
-
6.77 - 7.25
9-02
125
18
125
26.66 •
6.458333
2.45
-
6.2 - 7.4
10-02
.125
18
125
23.491304
7.413333
2.646667
6.67 - 7.29
- -
11 - 02
125
18
125
20.522222
8.241667
2.283333
6.88 - 7.29

PERMIT NUMBER: NC0027103
FACILITY NAME: Town of Pembroke - Pembroke WWTP
CITY: Pembroke
COUNTY: Robeson
PERIOD ENDING MONTH: 11 - 2002
REGION: Fayetteville
DMR 12 Month Calculated
PAGE 2 OF 3
00530
mg/1,
Solids, Total
Suspended
00545
ml/1
Solids,
Settleable
00600
mg/1
Nitrogen,
Total (as N)
00610
mg/1
Nitrogen,
Ammonia Total
(as N)
00665
mg/1
Phosphorus,
Total (as P)
31616
#/100m1
Coliform,
Fecal MF, M-FC
Broth,44.5C
50050
mgd
Flow, in conduit
or thru
treatment plant
50060
ug/1
Chlorine,
Total Residual
12 - 01
20
12
1.33
6.855556
12
0
3
9.642616
0.367097
15.066667
1 - 02
20
12
1.33
7.557143--
9..1-
1.028571--
2.4 -
3.901226
0.506129
1.333333
2 - 02
20
. 12
1.33
6.192308
3.8
1.223077
2
2.723232
0.57
6.153846
3-02
20
12
1.33
6.95
8.8
1.05
2.6
1.541132
0.545484
3.333333
4 - 02
20
12
1.33
3.923077'
3.9
2.084615
1.8
4.384999
0.596
10.769231
5 - 02
20
12
1.33
6.492857
15
1.928571
2.4
2.378894
0.419355
15.714286
6 - 02
20
12
1.33
5.166667
15
0
2.3
2.262591
0.347667
15
•
7 - 02
20
12
1.33
4.32
15
0.086667
1.3
5.638218
0.339032
18.666667
8 - 02
20
12
1.33
4.8
13
0.016667
2.3
19.93294
0.377097
16.666667
9 - 02
20
12
1.33
4.683333
17
0.625
3.2
6.731761
0.413333
8.333333
10 - 02
20
12
1.33
5.013333
16
0.013333
2.8
40.569237
0.512258
13.333333
11 - 02
20
12
-
1.33
4.866667
12
0.308333
2.1
23.617189
0.703
13.333333

PERMIT NUMBER: NC0027103
FACILITY NAME: Town of. Pembroke - Pembroke WWTP
CITY: Pembroke
COUNTY: Robeson
71900
ug/1
Mercury, Total
(as Hg) -
TGP3B
pass/fail
P/F STATRE
7Day Chr
Ceriodaphnia
THP3B
percent
CHV STATRE
7Day CHR
Ceriodaphnia
12-01
- _1-02.
2-02
3-02
4-02
0
1
5-02
6-02
.
7-02
1
8-02
9-02
10-02
1
11-02
PERIOD ENDING MONTH: 11 - 2002 DMR 12 Month Calculated
PAGE 3 OF 3
REGION: Fayetteville

PERMIT NUMBER: NC0027103
FACILITY. NAME: Town of Pembroke- Pembroke WWTP
CITY: Pembroke
OUTFALL: 001
EFFLUENT
COUNTY: Robeson
PERIOD ENDING MONTH: 11 - 2003
REGION: Fayetteville
DMR 12 Month Calculated
• PAGE 1 OF 3
.
.
00010
deg c ,
Temperature,
Water Deg.
Centigrade
-
00300
mg/1-
DO, Oxygen, ''
Dissolved
00310
lbs/day
SOD, 5-Day (20
Deg. C)
00310
mg/1
-BOD, 5-Day '(20
Deg. C)
00340
mg/1
COD, Oxygen
Demand, Chem.
(High Level)
00400
su
'pH
-
00500
mg/1
Solids, Total
00530
lbs/day
Solids, Total
Suspended
-12 - 02-
125
18
-
-- ----- --
----- ----- ---
125
16.427778
9.154545 -
3.945455
_ - -- -
6.67 - = 7.22 -
- --
1 -03
125
18.,
125
15.038095
9:491667,
2.858333
6.53 - 7.31
2 - 03
125
18
125
14.555
9.658333
4.175
•6.49 - -7.47
3 - 03
125 '
18
125
16.6,19048
' 9.525 '
6.191667
6.13 .- 6.92
4-03
125'
18-
125
-19.1 -
8.792857
6.478571
"
- - --
6.38 -= 7.48,
5 - 03
125
18
'
125
21.680952
8.1 •
5.184615
6.61 - 7.42 .
6 - 03
•24.619048
125. ,
18
' 125
7.808333
2.55
6.93 - 7.27
7 - 03
125
18
,125
25.386364
7.126667
3.18
6.8 = 7.23
8 - 03
125
18' -
.125
26.971429 -
7.041667
2.95
6:32 - 7.57
9 - 03
125 • ..
98
125
•
26.233333
'
6.993333
3.557143
6.6 - 7.3
10-03
125
18
-
125
-
23.495652
7.653846
3.115385
6.74 - 7.39
11 - 03
125
18
125
22.394444
7.966667
6.283333
6.5 - 7.13'

PERMIT NUMBER: NC0027103
FACILITY NAME: Town of Pembroke - Pembroke WWTP
CITY: Pembroke
COUNTY: Robeson
PERIOD ENDING MONTH: 11 - 2003
REGION: Fayetteville
DMR 12 Month Calculated
PAGE 2 OF 3
00530
mg/1
Solids, Total
Suspended
00545
ml/1
Solids,
Settleable
00600
mg/1
Nitrogen, '
Total (as N)
00610
mg/1
Nitrogen,
Ammonia Total
(as N)
00665
mg/1
Phosphorus,
Total (as P)
31616
#/100m1
Coliform,
Fecal MF, M-FC
Broth,44.5C
50050
mgd
Flow, in conduit
or thru
treatment plant
50060
ug/1
Chlorine,
Total Residual
12-02
20
12
1.33
4.490909
3.7
0
1.2
15.028716
0.646452
10.666667
1 - 03
20
- -
12 -
- -
1.33
-
3.9
9.5
0.223333
0.8
4.53481
0.65
8.333333
2 - 03
20
12
1.33
6.166667
8.2
0.883333 '
1.2
1.799372
0.758929
15 -
3-03
20
12
1.33
10.233333
9.2
0.425
2.6
14.835689
1.218065
15
4 - 03
20
12
1.33
11.507143
4
2.357143
2.2
3.01052
0.975667
4.285714
5 - 03
20
12
1.33
8.130769
7.2
1.676923
2
17.693628
1.094
7.692308
6-03
20
12
1.33
3.5
2.6
0.075
0.1
12.65654
0.709333
1.666667
7-03
20
12
1.33
5.206667
4.8
0.16
0.95
44.131258
0.847097
5.333333
8 - 03
20
-
12
1.33
7.966667
6.8
0.6
0.81
35.024332
0.788065
11.666667
9 - 03
20
12
1.33
4.757143
6.4
0.371429
3.3
49.683317
0.729
3.75
10 - 03
20
12
1.33
4.953846
11
1.262308
2.2
20.070383
0.718387
7.692308
11 - 03
20
12
1.33
10.25
9.6
0.26
1.5
8.831247
0.765
1.666667

PERMIT NUMBER: NC0027103
FACILITY NAME: Town of Pembroke - Pembroke WWTP
CITY: Pembroke
COUNTY: Robeson
71900
ug/1
Mercury, Total
(as Hg)
TGP3B
pass/fail
P/F STATRE
7Day Chr
Ceriodaphnia
THP3B
percent
CHV STATRE
7Day CHR
Ceriodaphnia
12-02
1 -03
2-03
3-03
4-03
1
5-03
6-03
7-03
0
1
8-03
•
9-03
10-03
1
11-03
-
PERIOD ENDING MONTH: 11 - 2003 DMR 12 Month Calculated
PAGE 3 OF 3
REGION: Fayetteville

. MONITORING REPORT(MR) VIOLATIONS for:
PERMIT: NC0027103
FACILITY: Town of Pembroke - Pembroke WWTP
COUNTY: Robeson
Report Date: 01/08/04
Page: 1 of 1
REGION: Fayetteville
Limit Violation
MONITORING OUTFALL
REPORT /PPI
LOCATION PARAMETER
-09 - 2003 001 Effluent - Coliform, Fecal MF, M-FC _
Broth,44.5C
VIOLATION UNIT OF CALCULATED
DATE FREQUENCY MEASURE LIMIT VALUE VIOLATION TYPE VIOLATION ACTION
-09/06/03 3 X week
- #/100m1 400 761.07 - Weekly Geometric_Mean _- - Proceed to NOV
Exceeded

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FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED
Renewal
RIVER BASIN:
Lumber
_ If yes, describe the mean(s) by which the wastewater from the treatment works is discharged or transported to the other treatment works
(e.g., tank truck, pipe). - 1
If transport is by a party other than the applicant, provide:
Transporter Name
Mailing Address
Contact Person
Title
Telephone Number ( )
For each treatment works that receives this discharge, provide the following:
Name
Mailing Address
Contact Person
Title
Telephone Number ( )
If known, provide the NPDES permit number of the treatment works that receives this discharge
Provide the average daily flow rate from the treatment works into the receiving facility.
e. Does the treatment works discharge or dispose of its wastewater in a manner not included
in A.8. through A.8.d above (e.g., underground percolation, well injection):
If yes, provide the following for each disposal method:
Description of method (including location and size of site(s) if applicable):
mgd
❑; Yes ®No
Annual daily volume disposed by this method:
Is disposal through this method ❑ continuous or ❑ intermittent?

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FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED
Renewal iI:
RIVER BASIN:
Lumber
WASTEWATER DISCHARGES:
If you answered "Yes" to question A.8.a, complete questions A.9 through A.12 once for each outfall (including bypass points) through
which effluent is discharged. Do not include information on combined sewer overflows in this section. If you answered "No" toquestion
A.8.a, go to Part B, "Additional Application Information.for Applicants with a Design Flow Greater than or Equal to 0.1 mgd."
A.9. Description of Outfall.
a. Outfall number 001
b. - Location Pembroke
(City or town, if applicable)
Robeson
28372
(Zip Code)
NC
(County)
34°39'55"
(Latitude)
c. Distance from shore (if applicable)
d. Depth below surface (if applicable)
e Average daily flow rate
•
•
f. Does this outfall have either an intermittent or a periodic discharge?
If yes, provide the following information:
Number f times per year discharge occurs:
Average duration of each discharge:
Average flow per discharge:
Months in which discharge occurs:
g. Is outfall equipped with a diffuser?
A.10. Description of Receiving Waters.
a. Name of receiving water Lumber River
b. Name of watershed (if known) Lumber
0.5.
❑ Yes
(State)
79°12'00"
(Longitude)
ft.
ft.
mgd
® No (go to A.9.g.)
❑ Yes ®! No
United States Soil Conservation Service 14-digit watershed code (if known):
c. Name: of State Management/River Basin (if known):Lumber
United States Geological Survey 8-digit hydrologic cataloging unit code (if known):
mgd
d. Critical low flow of receiving stream (if applicable)
acute cfs chronic cfs
e. Total hardness of receiving stream at critical low flow (if applicable): { mg/I of CaCOa

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FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
A.11. Description of Treatment
a. What level of treatment are provided? Check all that apply.
El Primary El Secondary ,
❑ Advanced ❑ Other. Describe:
b. Indicate the following removal rates (as applicable):
Design BOD5 removal or Design CBOD5 removal 91 1 %
•
Design SS removal 90 I %
Design P removal N/A
Design N removal 60 %
Other
c. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season', please describe:
Chlorination
I'
If disinfection is by chlorination is dechlorination used for this outfall? ® Yes I ' ❑ No
Does the treatment plant have post aeration? El Yes 1 ❑ No
A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following
parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is
discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data
collected through analysis conducted using 40 CFR Part 136 methods. In addition, this dataymust comply with QA/QC requirements of
40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a
minimum, effluent testing data must be based on at least three samples and must be no more than four and one-half years apart.
Outfall number: 001
PARAMETER
MAXIMUM DAILY VALUE
AVERAGE; DAILY VALUE
P J.-..
Value
Units
Value
Units
Number of Samples
pH (Minimum)
7.23
s.u.
;.
pH (Maximum)
6.80
s.u.
IP
....°
Flow Rate
2.30 .
MGD
0.78
MGD
365
Temperature (Winter)
16.0
°C
15.0
°C
31
Temperature (Summer)
27.0
°C
25.4
I °C
31
* For pH please report a minimum and a maximum daily value
POLLUTANT
MAXIMUM DAILY
DISCHARGE
I ,;
AVERAGE DAILY DISCHARGE '1
�
-., ANALYTICAL
METHOD
MUMDL
Conc.
Units
Conc.
Units
Number of :1
Samples ';
CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS
BIOCHEMICAL OXYGEN
DEMAND (Report one)
BOD5
10.3
Mg/L
3.7
Mg/L
1561 ' • 1
5210B
2.0 Mg/L
CBOD5
FECALCOLIFORM
>1200
CoI/100mL
13.5
Col/100
1
156, 1
9222D(MF)
lcol/100m1
TOTAL SUSPENDED SOLIDS (TSS)
20.5
Mg!L
6.0
Mg/L
156,
2540(D)
1.0 Mg/L
END OF PART A.
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE
OF FORM 2A YOU MUST COMPLETE,
WHICH OTHER PARTS

U
it
LJ
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
BASIC APPLICATION INFORMATION
PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR
EQUAL TO 0.1 MGD (100`,000 gallons per day). I :i
All applicants with a design flow rate z 0.1 mgd must answer questions B.1 through B.6. All others go to Part C (Certification).
B.1. Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration.
10,0000 gpd
i '
Briefly explain any steps underway or planned to minimize inflow and infiltration.
Pembroke has completed an I/1 study as well as an optimization study to target/prio'ritize problem areas.
B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This
map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire
area.)
a. The area surrounding the treatment plant, including all unit processes. -
b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which
treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping; if applicable.
i 1
c. Each well where wastewater from the treatment plant is injected underground.
1
d. Wells, springs, other surface water bodies, and drinking water wells that are: 1) within''/< mile of the; property boundaries of the treatment
works, and 2) listed in public record or otherwise known to the applicant.
e. Any areas where the sewagesludge produced by the treatment works is stored, treated, or disposed.
f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act (RCRA) by truck, rail,
or special pipe, show on the map where the hazardous waste enters the treatment works and where' it is treated, stored, and/or disposed.
B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant, including all bypass piping and all
backup power sources or redunancy in the system. Also provide a water balance showing all treatment units, including disinfection (e.g.,
chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow
rates between treatment units. Include a brief narrative description of the diagram.
B.4. Operation/Maintenance Performed by Contractor(s).
Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a
contractor? 0 Yes ® No
If yes, list the name, address, telephone number, and status of each contractor and describe the contractor's responsibilities (attach additional
pages if necessary).
Name:
Mailing Address:
Telephone Number: ( )
Responsibilities of Contractor:
B.5. Scheduled improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or
uncompleted plans for improvements that will affect the wastewater treatment, effluent quality, or design' capacity of the treatment works. If the
treatment works has several different implementation schedules or is planning several improvements, submit separate responses to question B.5
for each. (If none, go to question B.6.)
a. List the outfall number (assigned in question A.9) for each outfall that is covered by this implementation schedule.
b. Indicate whether the planned improvements or implementation schedule are required by local, State, or Federal agencies.
0 Yes ❑ No 1 '

u
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal ,,
RIVER BASIN:
Lumber
c. If the. answer to B.5.b is "Yes," briefly describe, including new maximum daily inflow rate (if applicable .
d. Provide dates imposed
applicable. For improvements
applicable. Indicate
Implementation Stage
- Begin Construction
- End Construction
- Begin Discharge
- Attain Operational
e. Have appropriate
Describe briefly:
by any compliance schedule
planned independently
dates as accurately as possible.
Level
permits/clearances concerning
or any actual dates of completion
of local, State, or Federal agencies,
Schedule
MM/DD/YYYY
for the
indicate
been obtained?
implementation steps listed
planned or actual completion
Actual Completion
MM/DD/YYYY
below, as
dates, as
Yes ❑ No
/ /
/ /
/ /
i / /
/ /
1 / /
/ /
/ /
other Federal/State requirements
❑
i
B.6. EFFLUENT TESTING DATA (GREATER THAN 0.1 MGD
Applicants that discharge to waters of the US must
effluent testing required by the permitting authority
on combine sewer overflows in this section. All information
using 40 CFR Part 136 methods. In addition, this data
QA/QC requirements for standard methods for analytes
based on at least three pollutant scans and must be
Outfall Number: 001
ONLY). j
provide effluent testing data for the following parameters. Provide
for each outfall through which effluent is discharged. Do not include
the indicated
information
conducted
other appropriate
data must be
reported must be based on data collected through analysis
must comply with QA/QCrequirements of 40 CFR Part 136 and
not addressed by 40 CFR Part 136.I At a minimum effluent testing
no more than four and on -half years old.
I
POLLUTANT
MAXIMUM DAILY
DISCHARGE
AVERAGE DAILY DISCHARGE
f'
ANALYTICAL
METHOD
6•
ML/MDL
Conc.
Units
Conc.
Units
Number of (M
Samples r,
CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS
AMMONIA (as N)
8.8
MG/L
.65
MG/L
156,
4500(NH3) F.
0.2 MG/L
CHLORINE (TOTAL
RESIDUAL, TRC)
20
UG/L
20
UG/L
156 '
i
4500(Cl2) G.
20 UG/L
DISSOLVED OXYGEN
10.5
MG/L
8.13
MG/L
156!'
4500(0) C.
1.0 MG/L
TOTAL KJELDAHL
NITROGEN (TKN) -
7.2
MG/L
1.78
MG/L
12
351.2
0.5 MG/L
NITRATE PLUS NITRITE
NITROGEN
15.0
MG/L
..
8.41
MG/L
12
I
I
353.2
0.1 MG/L
OIL and GREASE
8.5
MG/L
4.4
MG/L
3
5520B
1.0 MG/L
PHOSPHORUS (Total)
15.0
MG/L
1.97
MG/L
121 !
365.2
0.1 MG/L
( TOTAL DISSOLVED SOLIDS
DS
184
MG/L
147
MG/L
3 j •
2540C
1.0 MG/L
OTHER
END OF PART B. ;, "
REFER TO THE APPLICATION OVERVIEW (PAGE 1) TO DETERMINE WHICH OTHER PARTS
OF FORM 2A YOU MUST COMPLETE- 1
lJ

FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, _NC0027103
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
BASIC APPLICATION INFORMATI o N t�
PART O. CERTIFICATION'~
All applicants must complete the Certification Section. Refer to instructions to determine who is an
certification. All applicants must complete all applicable sections of Form 2A, as explained in the
parts of Form 2A you have completed and are submitting. By signing this certification statement,
Form 2A and have completed all sections that apply to the facility for which this application is submitted.
officer for the purposes of this
Application Overview. Indicate below which
applicants confirm that they have reviewed
Indicate which parts of Form 2A you have completed and are submitting:
�I Basic Application Information packet Supplemental Application Information packet:
El Part D (Expanded Effluent Testing
® Part E (Toxicity Testing: Biomonitoring
❑ Part F (Industrial User Discharges
❑ Part G (Combined Sewer Systems)
1
Data)
Data)
1
and RCRA/CERCLA Wastes)
'
ALL APPLICANTS MUST COMPLETE. THE FOLLOWING CERTIFICATION.
}
I certify under penalty of law that this document and all attachments were prepared under my direction or
designed to assure that qualified personnel properly gather and evaluate the information submitted. Based
manage the system or those persons directly responsible for the information, the information is,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including
for knowing violations.
Name and official title McDuffie Cummings
t
supervision in accordance with a system ,
on'my inquiry of the person or persons who
to the best of my knowledge and belief, true,
the possibility of fine and imprisonment
,
Signature ,nce ,i-eeo
Telephone number (910) 5 - 85
Date signed ff _ /I 3
I'
Upon request of the permitting authority, you must submit any other information necessary to"assure wastewater
works or identify appropriate permitting requirements.
treatment practices at the treatment
SEND COMPLETED FORMS TO:
NCDENR/ DWQ
Attn: NPDES Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

U
J
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal '; i
RIVER BASIN:
Lumber
SUPPLEMENTAL APPLICATIONINF.ORMATION� +'
1
+
PART D zEXPANDED EFFLUENT .�TESTING DATA`
�` ems' K. .:
fit.• r
'
Refer to the directions on the cover page to determine whether this section applies to the treatment works.
Effluent Testing: 1.0 mgd and PretreatmentWorks. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has (or is required
to have) a pretreatmentprogram, or is otherwise required by the permitting authority to provide the data, tlen provide effluent testing data for the following
pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which
effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected
through analyses conducted using 40 CFR Part 136 methods. In addition, these data must comply with QA/QC
other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part
any data you may have on pollutants not specifically listed in this form. At a minimum, effluent testing data
scans and must be no more than four and one-half years old.
Outfall number: 001=See Additional Info. (Complete once for each outfall discharging effluent to waters
requirements of 40 CFR Part 136 and
06. I Indicate in the blank rows provided below
must be based on at least three pollutant
of the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
'°
A ME HOD L
MUMDL
Conc.
Units
Mass
Units
Conc.
Units
Mass
s
Units
Number
' z..of
Samples
METALS (TOTAL RECOVERABLE), CYANIDE,
PHENOLS,
AND HARDNESS.
ANTIMONY
ARSENIC
BERYLLIUM
CADMIUM
CHROMIUM
.
COPPER
LEAD
MERCURY
NICKEL
SELENIUM
SILVER
THALLIUM
-
ZINC
+
CYANIDE
TOTAL PHENOLIC
COMPOUNDS
HARDNESS (as CaCO3)
Use this space (or a separate sheet) to provide information on other metals requested by the permit writer {,
j;
•

U
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal 1
RIVER BASIN:
Lumber
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MUMDL
Conc.
Units
Mass
Units
Conc.
Units
Mass
Units
Number
11 of
Samples
VOLATILE ORGANIC COMPOUNDS
ACROLEIN •
ACRYLONITRILE
BENZENE
BROMOFORM
CARBON
TETRACHLORIDE
CHLOROBENZENE
CHLORODIBROMO-•
METHANE
CHLOROETHANE
2-CHLOROETHYLVINYL
ETHER
CHLOROFORM
DICHLOROBROMO-
METHANE
1,1-DICHLOROETHANE
1,2-DICHLOROETHANE
TRANS-1,2-DICHLORO-
ETHYLENE
1,1-DICHLORO--
ETHYLENE
i„
1,2-DICHLOROPROPANE
1,3-DICHLORO-
PROPYLENE
ETHYLBENZENE
METHYL BROMIDE
METHYL CHLORIDE
METHYLENE CHLORIDE
1,1,2,2-TETRA-
CHLOROETHANE
I'
TETRACHLORO-
ETHYLENE
TOLUENE
I,

U
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103 -
PERMIT ACTION REQUESTED:
Renewal .
RIVER BASIN:
Lumber
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE' •.
ANALYTICAL
METHOD
MUMDL
Conc.
Units
Mass
Units
Conc.
Units
Mass
Units
Number
i
Samples
of
1,1,1-
TRICHLOROETHANE
1,1,2-
TRICHLOROETHANE
TRICHLOROETHYLENE
VINYL CHLORIDE
1
I
Use this space (or a separate sheet) to
provide information
on
other volatile organic
compounds
requested
by the permit
writer
I
ACID -EXTRACTABLE COMPOUNDS
P-CHLORO-M-CRESOL
2-CHLOROPHENOL
2,4-DICHLOROPHENOL
2,4-DIMETHYLPHENOL
4,6-DINITRO-O-CRESOL
2,4-DINITROPHENOL
2-NITROPHENOL
4-NITROPHENOL
PENTACHLOROPHENOL
PHENOL
1
2,4,6-
TRICHLOROPHENOL
•
I
Use this space (or a separate sheet) to
provide information
on
other acid -extractable
compounds
requested
by the permit
writer
BASE -NEUTRAL COMPOUNDS
ACENAPHTHENE
1
ACENAPHTHYLENE
i
.
ANTHRACENE
I
BENZIDINE
I
BENZO(A)ANTHRACENE
BENZO(A)PYRENE

FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal ,
RIVER BASIN:
Lumber
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of;the United States.)
POLLUTANT
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MUMDL
Conc.
Units
Mass
Units
Conc.
Units
Mass
Units
`
Number
1l';_'of
Samples
3,4 BENZO-
FLUORANTHENE
BENZO(GHI)PERYLENE
BENZO(K)
FLUORANTHENE
•
,
BIS (2-CHLOROETHOXY)
METHANE
BIS (2-CHLOROETHYL)-
ETHER
BIS (2-CHLOROISO-
PROPYL) ETHER
BIS (2-ETHYLHEXYL)
PHTHALATE
4-BROMOPHENYL
PHENYL ETHER
BUTYL BENZYL
PHTHALATE
2-CHLORO-
NAPHTHALENE
4-CHLORPHENYL
PHENYL ETHER
CHRYSENE
DI-N-BUTYL PHTHALATE
DI-N-OCTYL PHTHALATE
DIBENZO(A,H)
ANTHRACENE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
3,3-DICHLORO-
BENZIDINE
•
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
2,4-DINITROTOLUENE
f �
2,6-DINITROTOLUENE
1,2-DIPHENYL-
HYDRAZINE

u
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
Outfall number: 001 (Complete once for each outfall discharging effluent to waters of the United States.)
" POLLUTANT '
MAXIMUM DAILY DISCHARGE
AVERAGE DAILY DISCHARGE
ANALYTICAL
METHOD
MIJMDL
Conc.
Units
Mass
Units
Conc.
Units
Mass
`-
Units
Number
It: •of
Samples
FLUORANTHENE
l;
FLUORENE
'
HEXACHLOROBENZENE
,I
HEXACHLORO-
BUTADIENE
I'
1
HEXACHLOROCYCLO-.
PENTADIENE
l
I
HEXACHLOROETHANE
1
INDENO(1,2,3-CD)
PYRENE
1
ISOPHORONE
NAPHTHALENE
NITROBENZENE
N-NITROSODI-N-
PROPYLAMINE
N-NITROSODI-
METHYLAMINE
N-NITROSODI-
PHENYLAMINE
PHENANTHRENE
-
Ii
PYRENE
1,2,4-
TRICHLOROBENZENE
I'
Use this space (or a separate sheet) to
provide information
on
other base -neutral compounds
requested
by
the permit
writer
i
,
Use this space (or a separate sheet) to provide information on other pollutants (e.g., pesticides requested by the permit writer
i
END OF, PARTD.
REFER TO THE APPLICATION OVERVIEW (PAGE` 1) TO_DETERMINE
' OF -FORM `2A YOU MUST COMPLETEK
WHICH OTHER PARTS
' ° "

LJ
Li
FACILITY NAME AND PERMIT NUMBER: • '
,
Town of Pembroke, NC00271.03
PERMIT ACTION REQUESTED':
1
Renewal . i
, .
RIVER BASIN:
Lumber
1
SUPPLEMENTAL APPLICATION INFORMATION ,
i _
PART E. TOXICITY TESTING DATA ,
POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests
facility's discharge points: 1) POTWs with a design flow rate greater than or equal to 1.0 mgd; 2) POTVV,
required to have one under 40 CFR Part 403); or 3) POTWs required by the permitting authority to submit
-
• At a minimum, these results must include quarterly testing for a 12-month period within the past
species), or the results from four tests performed at least annually in the four and one-half years',
show no appreciable toxicity, and testing for acute and/or chronic toxicity, depending on the range
information on combined sewer overflows in this section. All information reported must be based
using 40 CFR Part 136 methods. In addition, this data must comply with QA/QC requirements of
requirements for standard methods for analytes not addressed by 40 CFR Part 136.
• In addition, submit the results of any other whole effluent toxicity tests from the past four and one-half,
conducted during the past four and one-half years revealed toxicity, provide any information on
toxicity reduction evaluation, if one was conducted.
• If you have already submitted any of the information requested in Part E, you need not submit it
requested in question E.4 for previously submitted information. If EPA methods were not used,
If test summaries are available that contain all of the information requested below, they may be
If no biomonitoring data is required, do not complete Part E. Refer to the Application Overview for directions
complete.
i 1
for acute or chronic toxicity for each of the
with la pretreatment program (or those that are
data for these parameters.
I I
,1 year using multiple species (minimum of two
prioli to the application, provided the results
of receiving water dilution. Do not include
on data collected through analysis conducted
40 CFR Part 136 and other appropriate QA/QC
!
!
years. If a whole effluent toxicity test
the cause of the toxicity or any results of a
I I
'again. Rather, provide the information
report the reasons for using altemate methods.
submitted in place of Part E.
I 1
on which other sections of the form to
I I
E.1. Required Tests.
Indicate the number of whole effluent
• IZI, chronic El acute
E.2. Individual Test Data. Complete
column per test (where each species
toxicity tests conducted in the past four and one-half years. ! 1
!
1
t i
the following chart for each whole effluent toxicity test conducted in the last four and one-half years. Allow one
constitutes a test). Copy this page
Test number
if
more than three tests are
Test number
being reported.
Test number:
a. Test information.
Test Species & test method number
.
Age at initiation of test
'
Ouffall number
Dates sample collected
Date test started
Duration -
b. Give toxicity test methods followed.
Manual title
.
Edition number and year of publication
Page number(s)
t .
c. Give the sample collection method(s) used. For multiple grab samples, indicate the number ofigrab samples used.
24-Hour composite
Grab
.
d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. ,
Before disinfection
After disinfection
!
After dechlorination
X

Li
I
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
I 1
Renewal ,, ;
RIVER BASIN:
Lumber
Test number: Test number: ' : Test number:
e. Describe the point in the treatment process at which the sample was collected. ! ,
Sample was collected:
. ,
f. For each test, include whether the test was intended to assess chronic toxicity, acute toxicity, or
both '
Chronic toxicity
Acute toxicity
g. Provide the type of test performed.
Static
1
Static -renewal
Flow -through
h. Source of dilution water. If laboratory water, specify type; if receiving water, specify source.
Laboratory water
Receiving water
i. Type of dilution water. If salt water, specify "natural" or type of artificial sea salts or brine used.
Fresh water ,
Salt water
j. Give the percentage effluent used for all concentrations in the test series. i '
I
.
.
, .
.
, .
k. Parameters measured during the test. (State whether parameter meets test method specifications)
pH
Salinity
Temperature
Ammonia
Dissolved oxygen
I. Test Results.
Acute:
_ Percent survival in 100%
effluent
%
. %
%
LC50
95% C.I.
.
% ',
%
Control percent survival
%
% ,
.
%
Other (describe)

u
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke; NC0027103
PERMIT ACTION REQUESTED:
Renewal !
RIVER BASIN:
Lumber
Chronic:
NOEC
%
% . '
%
IC25
%
%
'' ;
%
Control percent survival
%
%
Other (describe)
m. Quality Control/Quality Assurance.
Is reference toxicant data available?
Was reference toxicant test within
acceptable bounds?
What date was reference toxicant test
run (MM/DD/YYYY)?
/ /
/ /
/ /
Other (describe)
E.3. Toxicity Reduction Evaluation.
❑ Yes ® No
Is the treatment works involved in a Toxicity Reduction Evaluation?
If yes, describe:
E.4. Summary of Submitted Biomonitoring Test Information. If you have
cause of toxicity, within the past four and one-half years, provide the dates
of the results.
Date submitted: 11/13/03 (MM/DD/YYYY)
submitted biomonitoring test
the information was submittedito
2003) passed
i
information, or information regarding the
the permitting authority and a summary
at 1.7%. Chronic Fat Head
Summary of results: (see instructions)
Chronic ceriodaphnia dubia results submitted quarterly (Jan.,Apr.,July,Oct.
Minnow analyzed July and October 2003, Jan. and April 2004 results will be forward.
SEND OFq PART E
..�r+ Yx� d+. �. +'S`4,`il"sse.M. b 4
REFER TO;THE�APPL`IC�ATION OVERVIEW (PAGE 1) TOEDE�TERMINE
OFFORM2A11'OU MUST`COMPLETE
Y
S thT .i �£:3i7i
WHICH -OTHER PART=S x

U
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
SUPPLEMENTAL APPLICATION;INFORMATION
PART F.INDIJSTRIAL USER DISCHARGES AND RCRAICERCLA WASTES
a {'
All treatment works receiving discharges from significant industrial users or which receive RCRA
complete part F.
GENERAL INFORMATION:
F.1. Pretreatment program. Does the treatment works have, or is subject to, an approved pretreatment
❑ Yes ® No
F.2. Number of Significant Industrial Users (SIUs) and Categorical Industrial Users (CIUs). Provide
industrial users that discharge to the treatment works.
a. Number of non -categorical Sills.
CERCLA, or other remedial wastes must
program?
the number of each of the following types of
copy questions F.3 through F.8 and
b. Number of ClUs.
SIGNIFICANT INDUSTRIAL USER INFORMATION:
Supply the following information for each SIU. If more than one SIU discharges to the treatment works,
provide the information requested for each SIU.
F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages
as necessary.
I
Name:
Mailing Address:
F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge.
F.5. Principal Product(s) and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's
discharge.
Principal product(s):
Raw material(s):
F.6. Flow Rate.
a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge
day (gpd) and whether the discharge is continuous or intermittent.
gpd ( continuous or intermittent)
into the collection system in gallons per
1
flow discharged into the collection system
4
il
b. Non -process wastewater flow rate. Indicate the average daily volume of non -process wastewater,
in gallons per day (gpd) and whether the discharge is continuous or intermittent.
gpd ( continuous or intermittent)
F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following:
a. Local limits ❑ Yes 0 No
b. Categorical pretreatment standards ❑ Yes ❑ No
If subject to categorical pretreatment standards, which category and subcategory?

FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal '
RIVER BASIN:
Lumber
F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU., Has the SIU
upsets, interference) at the treatment works in the past three years?
I;
❑ Yes 0 No If yes, describe each episode.
caused or contributed to any problems (e.g.,
'
1
RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL, OR DEDICATED PIPELINE:
,
F.9. RCRA Waste. Does the treatment works receive or has it in the past three
❑ Yes ❑ No (go to F.12)
F.10. Waste transport. Method by which RCRA waste is received (check all
years received RCRA hazardous
-
that apply):
(volume or mass, specify units).
waste by truck, rail or dedicated pipe?
,
, -
I Units
■ Truck ❑ Rail 0 Dedicated Pipe
F.11. Waste Description. Give EPA hazardous waste number and amount
EPA Hazardous Waste Number Amount
I
CERCLA (SUPERFUND) WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION
WASTEWATER, AND OTHER REMEDIAL ACTIVITYWASTEWATER:
I
F.12. Remediation Waste. Does the treatment works currently (or has it been notified that it will) receive
❑ Yes (complete F.13 through F.15.) ❑ No
F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial
the next five years).
waste from remedial activities?
'
waste originates (or is excepted to origniate in
f
1
F.14. Pollutants. List the hazardous constituents that are received (or are expected to be received). Include
known. (Attach additional sheets if necessary.)
data on volume and concentration, if
;
F.15. Waste Treatment.
a. Is this waste treated (or will be treated) prior to entering the treatment works?
❑ Yes ❑ No
If yes, describe the treatment (provide information about the removal efficiency):
b. Is the discharge (or will the discharge be) continuous or intermittent? •
❑ Continuous ❑ Intermittent If intermittent, describe discharge schedule.
�, _END
PARTF �' �Y�' r
/ P11` TO DETERMINE WHICH OTHER PARTS
,...., t,.i. /�y '
,... 's ,A:_,- i _,
-} APPLICATION OVERVIEW(
FORM 2AYOUCOMRLETE
- : 'MUST
x+e• � 3'

U
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal
RIVER BASIN:
Lumber
SUPPLEMENTAL APPLICATION INFORMATION f.
4
I,.
PART G. COMBINED SEWER SYSTEMS
If the treatment works has a combined sewer system, complete Part G. i
G.1. System Map. Provide a map indicating the following: (may be included with Basic Application Information)
a. All CSO discharge points.
b. Sensitive use areas potentially affected by CSOs (e.g., beaches, drinking water supplies, shellfish beds, sensitive aquatic ecosystems, and
outstanding natural resource waters).
c. Waters that support threatened and endangered species potentially affected by CSOs.
G.2. System Diagram. Provide a diagram, either in the map provided in G.1 or on a separate drawing, of the combined sewer collection system that
includes the following information.
a. Location of major sewer trunk lines, both combined and separate sanitary.
b. Locations of points where separate sanitary sewers feed into the combined sewer system.
c. Locations of in -line and off-line storage structures.
d. Locations of flow -regulating devices.
e. Locations of pump stations.
CSO OUTFALLS:
Complete questions G.3 through G.6 once for each CSO discharge point.
G.3. Description of Outfall.
a. Outfall number
i,
b. Location
(City or town, if applicable) (Zip Code)
(County) (State)
(Latitude) (Longitude)
c. Distance from shore (if applicable) ft.
d. Depth below surface (if applicable) ft.
e. Which of the following were monitored during the last year for this
0 Rainfall 0 CSO pollutant concentrations
❑ CSO flow volume 0 Receiving water quality
f. How many storm events were monitored during the last year?
G.4. CSO Events.
a. Give the number of CSO events in the last year.
events (❑ actual or 0 approx.)
CSO?
0 CSO frequency
b. Give the average duration per CSO event.
hours (❑ actual or ❑ approx.)

U
FACILITY NAME AND PERMIT NUMBER:
Town of Pembroke, NC0027103
PERMIT ACTION REQUESTED:
Renewal ' '
RIVER BASIN:
Lumber
G.5.
G.6.
c. Give the average volume per CSO event.
million gallons (❑ actual or ❑ approx.)
d. Give the minimum rainfall that caused a CSO event in the last year
Inches of rainfall
Description of Receiving Waters.
a. Name of receiving water:
b. Name of watershed/river/stream system:
United State Soil Conservation Service 14-digit watershed code
c. Name of State Management/River Basin:
(if known):
United States Geological Survey 8-digit hydrologic cataloging unit code (if known):
CSO Operations.
Describe any known water quality impacts on the receiving water caused by this CSO (e.g., permanent
intermittent shell fish bed closings, fish kills, fish advisories, other recreational loss, or violation of any
di intermittent beach closings, permanent or
applicable State water quality standard).
I
i
END OF PART G.
REFER TO THE APPLICATION OVERVIEW. (PAGE 1) TO. DETERMINE
OF FORM 2A YOU MUST COMPLETE
WHICH OTHER PARTS
'`

U
Additional information, if provided, will appear on the following pages.
1
4
NPDES FORM 2A Additional Information

LJ
Additional Information:
Town of Pembroke Outfall 001
NC0027103
Part B2. Topographic Map

U
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.
_ . � �- rCem •
�? `!=— :`�; T' �-
t� - _ -.-iy
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it
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7
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md5•
Ye �? DrOKe ;
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Town of Pembroke
Town ; of Pembroke WWTP
NC0027103
Discharge Point:
Latitude: 34°39'55"
Longitude: 79°12'00"
•a
•
"••.`".:.

u
Additional Information:
Town of Pembroke Outfall 001
NC0027103
B.3 Process Flow Diagram
Generator
1,76
Mechanical
Screening
D)Flt�h !
Waste Sludge
Influent Flow
.5MGD
Return Activated Sludge
3-45Hp 44_
Pumps
Influent
Pump Station
Digester
Return
Line
Chlorine Contact
Lumber River

Additional Information:
Town of Pembroke Outfall 001
NC0027103
Part D. Expanded Effluent Testing Data
Pollutants for July 2003 and October 2003 enclosed, January and Apri12OO4 results will
forward upon completion.

U
In
_I
-
ENVIRONMENTAL
S C I ENCE CORP .
REPORT OF ANALYSIS
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone] '
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
d
July 21, 20.03
I.
ESC Sample # : L120688-01.
Date Received July 11, 2003
Description 13139 - Town of Pembroke
Site ID
Sample ID EFFLUENT• , -
Project # : TBL-13139
Collected By 1
Collection Date : 07/09/03 08:20 '
Parameter Result. Det. Limit -Units Methl d Date Dil.
Cyanide BDL 0.0050 mg/1 335.13 07/16/03 1 -
Hardness,calcium 27,. mg/1 Calc. .07/17/03 1
Total Phenol by.4AAP BDL 0.040 mg/1 420.2 07/16/03 1
Mercury BDL 0.00020 mg/1 245.1 07/17/03 1
Antimony BDL 0.0050 mg/1 200.7 07/16/03 . 1
Arsenic BDL 0.010 mg/1 200.7 07/16/03 1
Beryllium BDL 0.0020 mg/1 200.7 07/16/03 1
Cadmium BDL ,. 0.0050 mg/1 200.7 07/16/03 1
Chromium BDL 0.010 mg/1 200.7 07/16/03 1
Copper 0.057 0.010 mg/1 20047 07/16/03 1
Lead 0.0062 0.0050 •mg/1 200.7 07/16/03 1
Nickel - BDL 0.010 mg/1 200.7 07/16/03 1.
Selenium BDL 0.010 mg/1 200.7 07/16/03 1
Silver BDL . 0.0050 mg/1. 200.7 07/17/03 1
Thallium BDL 0.010 mg/1 200.7 07/16/03 1
Zinc 0.36 0.030 mg/1' 200,7 07/16/03 1
Volatile Organics
Benzene • - BDL 0.0010 mg/1 624 f; 07/18/03 1
Bromodichloromethane BDL .0.0010_ mg/1 624 ; 07/18/03 1
Bromoform BDL -0.0010 mg/1 624.i 07/18/03 1
Bromomethane BDL 0-0010 mg/1 624 , 07/18/03 1
"Carbon tetrachloride BDL 0.0010 mg/1 624 i 07/18/03 1 "
Chlorobenzene BDL 0.0010 mg/1 , 624 .. 07/18/03 . 1
Chlorodibromomethane BDL 0.0010 mg/1 624 07/18/03 1
Chloroethane BDL 0.0010 mg/1 624 ' 07/18/03 1
2-Chloroethyl vinyl ether BDL 0.050 mg/1 624 . 07/18/03 1
Chloroform BDL 0.0050 ..mg/1 624' 07/18/03 1
Chloromethane -BDL 0.0010 mg/1 624,, .•07/18/03 1
1-,2-Dichlorobenzene BDL 0.0010 mg/1 624 ' - 07/18/03 1
1,3-Dichlorobenzene BDL 0.0010 mg/1 624 07/18/03 1
1,4-Dichlorobenzene BDL 0.0010 mg/1 624 07/18/03 1
Dichlorodifluoromethane BDL 0.0010 mg/1 624 07/18/03 1
1,1-Dichloroethane BDL 0.0010- - Mg/1 624 07/18/03 1
1,2-Dichloroethane BDL 0.0010 mg/1 624 07/18/03 1
1
BDL - Below Detection Limit -
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
MLA"- 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN C-TN-01
KY 7 90010, KYUST - 0016, NC' ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 .
Page 1 of 6

ENVIRONMENTAL
SCIENCE CORP.
REPORT OF ANALYSIS
Pam Hester July 21, 2003
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received •July - 11, 2003
Description •13139 - Town of Pembroke
Sample ID EFFLUENT
Collected By
Collection Date : 07/09/03 08:20
12065 Lebanon -Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax .(615), 758-5859
Tax I.D. 62-0814289
Est. 1970
ESC Sample # : L120688-01
Site ID
Project # : TBL-13139
I
Parameter .• Result Det. Limit' Units Method •Date Dil.
1,1-Dichloroethene BDL 0.0010 mg/1 1624• 07/18/03 1.'
trans-1,2-Dichloroethene BDL 0.0010 mg/1 424, 0.7/18/03. 1
1;2-Dichloropropane .. - BDL 0.0010 mg/1 624; 07/18/03 1
cis-1,3;-Dichloropropene- BDL 0.0010 .mg/1 624, 07/18/03 1
trans-1,3-Dichloropropene BDL 0.0010 mg/1 624; 07/18/03 1
Ethylbenzene BDL 0.0010. mg/1 624) 07/18/03 1 •
Methylene Chloride BDL 0.0050 mg/1 624 07/18/03 1
1,1,2,2-Tetrachloroethane BDL _ •0.0010 mg/1 624! 07/18/03 1
Tetrachloroethene• BDL '0.0010 mg/1 624. 07/18/03 1
Toluene BDL 0:0050 mg/1 624 07/18/03 1
1,1,1-Trichloroethane BDL 0.0010 mg/1 624, 07/18/03 1
1,1,2-Trichloroethane BDL 0.0010 `mg/1 624' 07/18/03 1
Trichloroethene • BDL 0.0010 mg/1 624) 07/18/03 1
Trichlorofluoromethane BDL 0.0010 mg/1 624 07/18/03 1 •
Vinyl chloride BDL 0.0010 mg/1 624, 07/18/03 1
Surrogate Recovery . •
--; Toluene-d8 94. . % Rec. 624_' 07/18/03 1
Dibromofluoromethane . 100 % Rec. 6241 07/18/03 1
4-Bromofluorobenzerie '72. % Rec. 624. 07/18/03 1
625 Base/Neutrals.w/ TIC
Acenaphthene BDL 0.010, . mg/1 625 07/18/03 1
Acenaphthylene BDL 0.010 mg/1 625 07/18/03 1:
Anthracene BDL 0:010 mg/1 625. 07/18/03 1
Benzidine BDL 0.050 mg/1 625, 07/18/03 1
Benzo(a)anthracene BDL 0.010 mg/1 625; 07/18/03 1
Benzo(b)fluoranthene BDL 0.010 mg/1 - 625 07/18/03 1
Benzo(k)fluoranthene . BDL 0.010 mg/1 625', 07/18/03 1
Benzo(g,h,i)perylene BDL 0.010 mg/1 625; 07/18/63 1
Benzo(a)pyrene BDL 0.010' mg/1 625! 07/18/03 1
Bis(2-chlorethoxy)methane •BDL 0.010 mg/1 625 07/18/03 1
Bis(2-chloroethyl)ether - ..BDL 0.010 mg/1 625 ' 07/18/03 1
Bis(2-chloroisopropyl)ether • BDL 0.010 mg/1 625! 07/18/03 1
4-Bromophenyl-phenylether BDL 0.010, mg/1 625 ' 07/18/03 1
2-Chloronaphthalene BDL 0.010 mg/1 625' 07/18/03 1
4-Chlorophenyl-phenylether BDL 0.010 mg/1 625 ' 07/18/03 1
Chrysene BDL 0.010 mg/1. 625 ; 07/18/03 1
Dibenz(a,h)anthracene BDL 0.010 mg/1 625,' 07/18/03 1
3,3-Dichlorobenzidine BDL 0.010 mg/I • 625,! *07/18/03 1
BDL - Below'Detection.Limit
Det. Limit -' Estimated Quantitation Limit(EQL).
Laboratory Certification Numbers: 1' •f
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL 4.E8,7487, GA - 923, IN - C-TN-01
• KY - 90010,'KYUST-'0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN-'2006, VA--00109; WV - 233
Page 2 of 6

1]
ENVIRONMENTAL
SCIENCE CORP .
REPORT OF ANALYSIS
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC=28359
Date Received July 11, 2003
Description 13139 - Town of Pembroke
Sample ID
Collected By
Collection Date :
EFFLUENT
- 12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax.[phone]
Tax I.D. 62-0814289
Est. 1970
July 21, 2003
,
ESC Sample # : L120688-01
Site ID
1
Project # : TBL-13139
07/09/03 08:20 i
Parameter Result Det. Limit Units Method Date Dil.
1
2,4-Dinitrotoluene BDL 0.010 mg/1 625; 07/18/03 1
2,6-Dinitrotoluene BDL 0.010 mg/1 '625' 07/18/03 1
Fluoranthene BDL 0.010 mg/1 1625 07/18/03 1
Fluorene .BDL 0.010 mg/1 i625 07/18/03 1
Hexachlorobenzene BDL 0.010 mg/1 625, 07/18/03 1
Hexachloro-1,3-butadiene BDL 0.010 mg/1 625 07/18/03 1
Hexachlorocyclopentadiene BDL 0.010 mg/1 625 07/18/03 1
Hexachloroethane BDL 0.010 mg/1 625 07/18/03 1
Indeno(1,2,3-cd)pyrene BDL 0.010 mg/1 625 07/18/03 1
Isophorone BDL 0.010 mg/1 625, 07/18/03 1
Naphthalene BDL 0.010 mg/1 '625 07/18/03 1
Nitrobenzene BDL 0.010 mg/1 625' 07/18/03 1
n-Nitrosodimethylamine BDL 0.010 mg/1 625 07/18/03 1
n-Nitrosodiphenylamine BDL 0.010 mg/1 625: 07/18/03 1
n-Nitrosodi-n-propylamine BDL 0.010 mg/1 625' 07/18/03 1
Phenanthrene BDL 0.010 mg/1 625, 07/18/03 1
Benzylbutyl phthalate . BDL 0.010 mg/1 6251 07/18/03 1
Bis(2-ethylhexyl)phthalate 0.010 0.010 mg/1 625, 07/18/03 1
Di-n-butyl phthalate BDL 0.010 mg/1 625 07/18/03 1
Diethyl phthalate BDL 0.010 mg/1 625. 07/18/03 1
Dimethyl phthalate BDL 0.010 mg/1 625 07/18/03 1
Di-n-octyl phthalate BDL 0.010 mg/1 625, 07/18/03 1
Pyrene BDL 0.010 mg/1 625 07/18/03 1
1,2,4-Trichlorobenzene BDL 0.010 mg/1 625' 07/18/03 1
Acid Extractables j
4-Chloro-3-methylphenol BDL 0.010 mg/1 6251 07/18/03 1
2-Chlorophenol BDL 0.010 mg/1 625 07/18/03 1
2,4-Dichlorophenol BDL 0.010 mg/1 625 07/18/03 1
2,4-Dimethylphenol BDL 0.010 mg/1 625' 07/18/03 1
4,6-Dinitro-2-methylphenol BDL 0.010 mg/1 625: 07/18/03 1
2,4-Dinitrophenol BDL 0.010 mg/1 625' 07/18/03 A.
2-Nitrophenol BDL 0.010 mg/1 625, 07/18/03 1
4-Nitrophenol BDL 0.010 mg/1 625 07/18/03 1
Pentachlorophenol BDL 0.010 mg/1 625 07/18/03 1
Phenol BDL 0.010 mg/1 625, 07/18/03 1
2,4,6-Trichlorophenol BDL 0.010 mg/1 6251 07/18/03 1
Surrogate Recovery 1 1
Nitrobenzene-d5 17. % Rec. 625i 07/18/03 1
2-Fluorobiphenyl 23. % Rec. 625 07/18/03 1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
. Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660., CA - 1-2327, CT- PH-0197, FL
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004,
-'E87487, GA - 923, IN - C-TN-01
TM 2006, VA - 00109, WV -,233
Page 3 of 6

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ENVIRONMENTAL
SCIENCE CORP .
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received
Description
REPORT OF ANALYSIS
July , 11, 2003
13139 - Town of Pembroke
Sample ID EFFLUENT
Collected By
Collection Date : 07/09/03 08:20
Parameter Result
p-Terphenyl-d14
Phenol-d5
2-Fluorophenol
2,4,6-Tribromophenol'
55.
16.
21.
54.
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA -
KY - 90010,.KYUST - 0016, NC - ENV375,DW21704,
Note:
The reported analytical results relate only to
This report shall not be_reproduced, except. in
Reported: 07/21/03 12:25 Printed:.07/21/03 12:26
' 12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
July'21, 2003
ESC Sample # : L120688-01
S Ite ID .
Project # : TBL-13139
Det. Limit Units Method
Rec. 1625
;% Rec. 625,
% Rec. 6251
% Rec. 625
• I 1
Date Dil.
07/18/03 ' 1
07/18/03 1
07/18/03 1
07/18/03 1
Cheli Boucher, ESC Representative
•
Certification Numbers:
I-2327, CT- PH-0197, FL E87487, GA - 923, IN - C-TN-01•
ND - R-140, SC - 84004, TN-12006, VA - 00109, WV - 233
the sample submitted.
full, without the written approval from ESC.
I
Page 4 of 6

...Attachment A
List of Analytes with QC Qualifiers
Sample #
L120688-01
Analyte Qualifier,
Nitrobenzene-d5 J2
2-Fluorobiphenyi J2
2-Fluorophenol J2
• 2-Chloroethyl vinyl ether J4
Page 5 of 6

Attachment B
Explanation of QC Qualifier Codes
-�
Qualifier
Meaning
J2 Surrogate recovery limits have been exceeded; values are outside lower
control limits
J4 The associated batch QC was outside the established' quality control range
for accuracy. 1
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier.explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
unless qualified as 'R' (Rejected). I I
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
I
Surrogate - Organic compounds. that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added:to the
sample and carried through all stages of preparation and analyses.
Control Limits ,
2-Fluorophenol 31-119' Nitrobenzene-d5 43-118 ' Dibromfluoromethane 72-125
Phenol-d5 12-134 2-Fluorobiphenyl 45-128 Toluene-d8 I 79-120
2,4,6-Tribromophenol 51-141 Terphenyl-d14 43-137 4-Bromofluorobenzene 66-131
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 6 of 6

LJ
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ENVIRONMENTAL
SCIENCE CORP .
REPORT OF ANALYSIS
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received October 10, 2003
Description 13437 - Town of Pembroke
Sample ID EFFLUENT
Collected By
Collection Date : 10/09/03 10:25
Parameter Result
Cyanide BDL 0.0050 mg/1
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
I ,
October 23, 2003
ESC Sample # : L130795-01
Site ID .
Project # : TBL-13437
1,
Det. Limit Units ; Method
335.3
Hardness,calcium 35. mg/1 Calc.
Total Phenol by 4AAP BDL 0.040 mg/1 420.2
Mercury BDL 0.00020 mg/1 245.1
Antimony BDL 0.0050 mg/1
Arsenic BDL 0.010 mg/1
Beryllium BDL 0.0020 mg/1
Cadmium BDL 0.0050 mg/1
Calcium 14. 0.50 mg/1
Chromium BDL 0.010 mg/1
Copper 0.016 0.010 mg/1
Lead 0.0053 0.0050 mg/1
Nickel BDL 0.010 mg/1
Selenium BDL 0.010 mg/1
Silver BDL 0.0050 mg/1
Thallium BDL 0.010 mg/1
Zinc 0.10 0.030 mg/1
Volatile Organics
Benzene
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
BDL 0.0010 mg/1
BDL 0.0010 mg/1
BDL 0.0010 mg/1
BDL 0.0010 mg/1
BDL 0.0010 mg/1
BDL 0.0010 mg/1
BDL 0.0010 mg/1
BDL 0.0010 mg/1
BDL 0.050 mg/1
BDL 0.0050 mg/1
BDL 0.0010 mg/1
BDL 0.0010 mg/1
BDL 0.0010 mg/1
BDL 0.0010 mg/1
BDL 0.0010 mg/1
BDL 0.0010 mg/1
200.7
200.7
200.7
200.7
200.7
200.7
200.7
200.7
200.7
200.7
200.7
200.7
200.7
Date Dil.
10/17/03 1
10/16/03 1
10/16/03 1
10/14/03 1
10/14/03 1
10/14/03 1
10/14/03 1
10/14/03 1
10/14/03 1
10/14/03 1
10/14/03 1
10/16/03 1
10/14/03 1
10/14/03 1
10/14/03 1
10/14/03 1
10/15/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL1- E87487, GA - 923, IN - C-TN-01
1 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
1 L130795-01 (SV625TIC) - No extra bottles, cannot be re -extracted
Page 1 of 6

LJ
ENVIRONMENTAL
S C I ENCE CORP .
REPORT OF ANALYSIS
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received October 10, 2003
Description 13437 - Town of Pembroke
Sample ID EFFLUENT -
Collected By
Collection Date : 10/09/03 10:25
Parameter Result
1;2-Dichloroethane BDL
1,1-Dichloroethene BDL
trans-1,2-Dichloroethene BDL
1,2-Dichloropropane BDL
cis-1,3-Dichloropropene BDL
trans-1,3-Dichloropropene BDL
Ethylbenzene BDL
Methylene Chloride BDL
1,1,2,2-Tetrachloroethane BDL
Tetrachloroethene BDL
Toluene BDL
1,1,1-Trichloroethane BDL
1,1,2-Trichloroethane BDL
Trichloroethene BDL
Trichlorofluoromethane BDL
Vinyl chloride BDL
Surrogate Recovery
Toluene-d8 100
Dibromofluoromethane 110
4-Bromofluorobenzene 97.
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
October 23, 2003-
I
.ESC Sample #-: L130795-01
•Site ID .
Project # : TBL-13437
Det. Limit Unit's Method
f
0.00.10 mg/l
0.0010 mg/1
0.0010 mg/1
0.0010 mg/1
0.0010 mg/3
0.0010 mg/1
0.0010' mg/1
0.0050 mg/1,
0.0010 mg/1
0.0010 mg/1
0.0050 mg/1
0:0010 mg/1
0.0010 mg/1
0.0010 mg/l
0.0010 mg/1
0.0010 mg/I
Rec.
96 Rec.
s Rec.
Date Dil.
624 10/14/03 1
' 624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
1 624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
624 10/14/03 1
.I
625 Base/Neutrals w/ TIC ,
Acenaphthene BDL 0.010 mg/1 625 10/15/03 1
Acenaphthylene BDL 0.010 mg/1 : 625 10/15/03 1
Anthracene BDL 0.010 mg/1 , 625 10/15/03 1
Benzidine BDL 0.050 mg/1 ! 625 10/15/03 1
Benzo(a)anthracene BDL 0.010 mg/1 1 625 10/15/03 1
Benzo(b)fluoranthene BDL 0.010 mg/1 625 10/15/03 1
Benzo(k)fluoranthene BDL 0.010 mg/1 �625 10/15/03 1
Benzo(g,h,i)perylene BDL 0.010 mg/1 1625 10/15/03 1
Benzo(a)pyrene BDL 0.010 mg/1 1625 10/15/03 1
Bis(2-chlorethoxy)methane BDL 0.010 mg/1 1625 10/15/03 1
Bis(2-chloroethyl)ether BDL 0.010 mg/1 ' 625 10/15/03 1
Bis(2-chloroisopropyl)ether BDL 0.010 mg/I ; 625 10/15/03 1
4-Bromophenyl-phenylether BDL 0.010 mg/1 625 10/15/03 1
2-Chloronaphthalene BDL 0.010 mg/1 ; 625 10/15/03 1
4-Chlorophenyl-phenylether BDL 0.010 mg/I , 625 10/15/03 1
Chrysene BDL 0.010 mg/1 625 10/15/03 1
Dibenz(a,h)anthracene BDL 0.010 mg/1 1 625 10/15/03 1
BDL - Below Detection Limit I I
Det. Limit - Estimated Quantitation Limit(EQL) 1
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-01971 FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 8400.1,1 TN - 2006, VA - 00109, WV - 233
L130795-01 (SV625TIC) - No extra bottles, cannot be re -extracted I
Page 2 of 6

U
ENVIRONMENTAL
S C I ENCE CORP .
REPORT OF ANALYSIS
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received October 10, 2003
Description 13437 - Town of Pembroke
Sample ID EFFLUENT
Collected By .
Collection Date : 10/09/03 10:25
Parameter
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine
Phenanthrene
Benzylbutyl phthalate
Bis(2-ethylhexyl)phthalate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
Acid Extractables
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
Surrogate Recovery
Nitrobenzene-d5
BDL - Below
Det. Limit
A2LA - 1461
KY - 90010
L130795-01
Detection Limit
- Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
(SV625TIC) - No extra bottles, cannot be re -extracted
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
October 23, 2003
I
ESC Sample # : L130795-01
Site ID .
Project # : TBL-13437
Result Det. Limit Units Method Date Dil.
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
BDL 0.010 mg/1 625 10/15/03 1
36. % Rec 625 10/15/03 1
1
Page 3 of 6

Ak
ENVIRONMENTAL
SCIENCE CORP .
REPORT OF ANALYSIS
Pam Hester
TBL Laboratory
P.O. Box 589
Lumberton, NC 28359
Date Received October 10, 2003
Description 13437 - Town of Pembroke
Sample ID EFFLUENT
Collected By
Collection Date : 10/09/03 10:25
Parameter
Result Det. Limit Units
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
October 23, 2003
ESC Sample # : L130795-01
Site ID .
Piroject # : TBL-13437
Method
Date Dil.
2-Fluorobiphenyl 40.
p-Terphenyl-d14 100
Phenol-d5 25.
2-Fluorophenol 34.
2,4,6-Tribromophenol 63.
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FLI - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004,117— 2006, VA - 00109, WV - 233
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 10/17/03 16:00 Printed: 10/23/03 15:20
L130795-01 (SV625TIC) - No extra bottles, cannot be re -extracted
or o\ or or o'
Rec.
Rec.
Rec.
Rec.
Rec.
625 10/15/03 1
625 10/15/03 1
625 10/15/03 1
625 10/15/03 1
625 10/15/03 1
CheliiBoucher, ESC Representative
Page 4 of 6

U
Attachment A
List of Analytes with QC Qualifiers
Sample #
L130795-01
Analyte Qualifier
Acenaphthene J4J3
Acenaphthylene J4J3
Benzo(b)fluoranthene V3
Benzo(k)fluoranthene V3
Benzo(g,h,i)perylene V3
Benzo(a)pyrene V3
Bis(2-chlorethoxy)methane J4J3
Bis(2-chloroethyl)ether J4J3
Bis(2-chloroisopropyl)ether J4J3
4-Bromophenyl-phenylether J4
2-Chloronaphthalene J4J3
4-Chlorophenyl-phenylether J4
Dibenz(a,h)anthracene V3
2,6-Dinitrotoluene J4
Fluorene J4J3
Hexachloro-1,3-butadiene J3
Hexachlorocyclopentadiene J3
Hexachloroethane J4J3
Indeno(1,2,3-cd)pyrene V3
Isophorone J4J3
Naphthalene J4J3
Nitrobenzene J4J3
n-Nitrosodiphenylamine J4
n-Nitrosodi-n-propylamine J4J3
Di-n-butyl phthalate J4
Diethyl phthalate J4
Dimethyl phthalate J4
1,2,4-Trichlorobenzene J4J3
4-Chloro-3-methylphenol J4
2-Chlorophenol J4
2,4-Dichlorophenol J4J3
2,4-Dimethylphenol J4J3
2-Nitrophenol J4
Phenol J4
2,4,6-Trichlorophenol J3
Nitrobenzene-d5 J2
2-Fluorobiphenyl J2
Zinc J4
Page 5 of 6

U
Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J2 Surrogate recovery limits have been exceeded; values are outside lower
control limits
J3
J4
V3
The associated batch QC was outside the established quality control range
for precision.
The associated batch QC was outside the established quality control range
for accuracy.
(ESC) - Additional QC Info: The internal standardlexhibited poor recovery
due to sample matrix interference. The analytical results will be biased
high. BDL results will be unaffected.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as !either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
unless qualified as 'R' (Rejected).
Definitions j
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc. 1
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition,' extraction,
and chromotography to analytes of interest. The surrogateslare used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
Control Limits
2-Fluorophenol 31-119 Nitrobenzene-d5 43-118 Dibromfluoromethane 79-126 83-119
Phenol-d5 12-134 2-Fluorobiphenyl 45-128 Toluene-d8 81-114 82-116
2,4,6-Tribromophenol 51-141 Terphenyl-d14 43-137 4-Bromofluorobenzene 65-129 72-126
TIC
- Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 6 of 6

Summary of RemarksForSamples Printed
10/23/03 at 15:21:07
TSR Signing Reports: 070
R5 - Desired TAT
Sample: L130795-01 Account: TBLLAB Received: 10/10/03 09:00 Due Date: 10/17/03 00:00 RPT Date: 10/17/03 16:00

Additional information:
Town of Pembroke Outfall 001
NC0027103"
Part E. Toxicity Test Data
Chronic Fathead Minnow for July 2003 and October 2003 enclosed, January and April
2004 results will forward upon completion.

LJ L
Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test
-li
Facility: Town of Pemb oke
tPDES # NC0027103 Pi
pe # 001
(L)L "-
Date:10/22/2003
County: •
[Control
x
Laboratory: Meriteci, Inc.
Signature of 0
x
Ct-flW1.�.�
in Responsible Charge
Signature of Labffrato
upervisor
Comments
MAIL ORIGINAL TO:
Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Test Initiation Date/Time 10/7/2003
% Eff. Repi.
Surviving #
Original #
Wt/original (mg)
0.43
Surviving #
Original #
Wt/original (mg)
0.85
Surviving #
Original #
Wt/original (mg)
1.7
Surviving #
' Original #
Wt/original (mg)
3.4
Surviving #
Original #
Wt/original (mg)
6.8
Surviving #
Original #
Wt/original (mg)
Water Quality Data
Control
pH (SU) Init/Fin
DO (mg/L) Init/Fin
Temp (C) Init/Fin
High Concentration
pH (SU) Init/Fin
DO (mg/L) Init/Fin
Temp (C) Init/Fin
Sample
Collection Start Date
Grab
Composite (Duration)
Conductivity (umhos/cm)
Chlorine(mg/L)
Temp. at Receipt (°C)
Test Organisms
1
/ 12.30 pm
2 3
Avg Wt/Surv. Control
10-
10
10
10
10
10
10
10
0.501
0.547
0.520
0.466
10
10
10
10
10
10
10•
10
0.449
0.411
0.499
0.600
10
10
10
10
10
10
10
10
0.467
0.462
0.480
0.425
10
10
10
10
10
10
10
10
0.450
0.515
0.513
0.562
10
10
10
10 _
10
10
10
10
0.556
0.541
0.453
0.398
10
10
10
10
10
10
.10
10
0.531
0.555
0.534
.0.479
Day
% Survival
Avg Wt (mg)
% Survival
Avg Wt (mg)
% Survival
Avg Wt (mg)
% Survival
Avg Wt (mg)
% Survival
Avg Wt (mg)
% Survival
Avg Wt (mg)
0.509
100.0
0.509
100.0
0.490
1 00.0
0.459
100.0
0.510
1 ; 0 0 . 0
0.487
1'00,01
0.525
0
1
3
4
51
7
8.10 / 8.02
8.08 / 8.04
8.05 / 8.03
8.06/ 8.03
8.05 / 8.01
8.03 / 8.02
8.02 / 8.02
7.50 / 7.10
7.51 / 7.08
7.60 / 7.07
7.63 / 7.06
7.80 / 7.09
7.76 / 7.08
7.78 / 7.09
25.0 / 24.9
25.0 / 24.9
25.0 / 24.8
25.0 / 24.8
25.0 / 24.9
25.0 / 24.8
25.0 / 24.8
1
51
7
7.99 / 7.96
8.00 / 7.98
7.99 ' / 7.79
7.97 / 7.81
8.03 / ,7.88
8.02 / 7.90
8.02 / 7.93
7.36 / _6.99
7.38 / 7.00
7.52 / 6.85
7.54 / 6.88
7.93 ,/ 6.95
7.95 / 6.93
7.94 / 6.97
25.0 / 24.7
25.0 / 24.8
25.0 / 24.7
25.0 / 24.7
25.0 / 24.8
25.0 / 24.8
25.0 / 24.7
1
2
10/5/2003
10/6/2003
10/9/2003
24.00
23.00
22.50
294
270
262
<0.1
<0.1
<0.1
0.3
0.1
0.3
Cultured In -House ; .•
Outside Supplier
Hatch Date/Time s 10/6/2003. / 200 pm
Normal jlr•I
Hom. Var. Fi] 1([ ,
NOEL 6.8 6.6
Survival Growth
Fr,
LOEC >6.8 I >68
ChV >6.8 I >6.8
Method _ . 1Dunnett
Crit t/rsum 12.4,,1
Conc. Calc t/rsum
0.43% 0.4961
0.85%
1.70%
3.40%
6.80%
I1.3229
-0.0397,
1-0.0265
-0.4299"
Result
Pass
Fail ChV
>6.8
DWQ Form AT-5 (8/03)

MIERITECH'
Chronic Fathead Minnow Benchsheet
Transfer and -Feeding Dates and Times
Test Initiation Data:
• Start Date: to -A-- o
Start Time:
Initials/Signature:
Date/Time Fed I c;i1)0,�.
Date/Time Born f L);:tzw., v,.
CQ l�l]` PtV S`i t %Li `'i c: 9 o' Z.4e_
, Q Zo ('i 1-38
Transfer
Date Time Initials
Day 1 t--e,-0>
Day 2 to ---
Day 3 do-i,P -p's
&D A,.A (rag st_
Day 4 1;.-+t c�� kc;:a h 11rL:£.St�
- Day-5 to,17.:-vc--- Itk51
Day 6 10-�?,
Test Termination Data:
Initials/Signature: _6'4__.-
End Date:
End Time: ]'(10
# of Organisms per Chamber: 10
Test Vessel Size: ?..5Tj -y !
Test Solution Volume: 2:0D0,9-
Temp. of Stock: 25..0'�
# of Reps: LA
Date, Time 1
Day 0 10- :)-•-0:', gum --
Day 1 i�1 5Z5 1r�
Day 2
Facility' OL,)
NPDES # i`it.t`--ac`^,?� `2
Dilution Water: S\v, 4-i,;w;-
Randomization: EYES NO
Incubator #:
Feeding
Initials Time 2 Initials Time 3 Initials,
Day 3 1CJ- tra•-c:"Yt F E-10 ILI°
Day 4 4i'i-`'v?, it'Sa-,t• '� `^_
Day 5 io•-tic- :‘,
Day 6 i 0-t }—D".;
I
rL.
S t Zoo 9, 5 c_ 11.3o S t�

L
MEW TECi.,-;
Chethiclal and Phy.s i
Facility tuo- of Pass4s,stt, NPDES .#
Test Time: Start End irk-siy—
TeSt Dates :
Test Organism: f Analyst
S ta:rt ;0:093 End
' • . Day
Conc. . n
• 1
2
3
4
. 5
6
/ .
,
Remarks
Temp. Initial
ZE3-c)
25,o
17,-. D
.8.,
Ts -A>
ac,ID
7,\.5.7,)
(
.
Final
b-iPi
N.R
1.49'.
',...wa
2A 5"
Ic.).:„.5,
'akka
1
i
D.O. initial
4-.50.
-1E; i
;4$0.
3i-ko3
1s%0
.44.7
:WZ
•
'
.
- rinal
4,Io
4.M
4o71--
-h-A,
•'..04=,,
pH In1 tl al
io
IrZ.CYS
ccrs
atly
i c4; t) 5
10?3
S-01-
•
' F i nal
ere m
q, ,. ri - i t
TY2s
gal
qr.) % '
57itiA
21241
,
Algal inity
..
-),50
',42
CAK
.
• •
Ha rdne Ss
k---(.--
_
Conduct . Tniti al
2:014, *
Z..ca
-a..., ,
4-el-Zo-.5.•
?ri-:.,--
Et) ls
e.:kOkst.
34:a
Final
PA
2,K.X,
2_03
2.-d2-
7_S .
a-,-ci3
:-...),C0-4.
Rs. Chlorine -
4,a i.
i .:z) 4
A.) A
'
1
71-kalinity r r ]
Hardness 1 .1
Condiact, . I? D Iaori I 86 1 c1,0
Final PA°, I? 1QC) I
-Chlorine It;, 14s> k. IL3:1,-( 141P-
1 ! 1
Day
Conc. r•-.).;;,41 1 1- • I / i 3 . 4 1 b. . I b i / 1 ; 1 Remarks
Tamp . Initial I/ stD ii.c.r) I Ir-t) 7,CC,--, I ti-i) I 31.-17 to
' Final: 1?16' 17:4,4 12:>6‹ 1 64,N 1 a4-7.5 1,A43- 1 1 '
D • 0 • In i ti al 1--).Lit; Il-t3F.4. I . -..f.,,-0 I 7. 92-1 4-80 ilY3-=',. 1
Final, 1)1;6 I `-‘/-.0% I :;°;1-..il .T-'-d,..,- I V., -1 :11-5.'4.-
I
Pi1H In iti al 1 I 1 Roq P--riLi 7. 9 7--12101G7 -.A-0•0 1 I '
Final 1*n; ccrn I 9-0? P)r) i :4 0E; 1'4-'115 1),'-':1 to 1
1 • •
! ;
!Determinations
I
83
ez
140- k. I 4_0-( I ;
. I
Conc. 0 26‹ 1 1 I 2 I - 3
Temp- Initial I Z.S7-0 I /v.,:
Final I 7,1(...:1- 17,0- I 2,Q11-
D.O. Initial 1 4LJA 1701m.
inal
pH i i I
I 4c4.71. 1:7-1e4Eg. 4c-tk4.
- Final
Day
4
1.0qc;
Rag
5
NO
0I.:.
Sb-z-
0
4P1
.)17)
ED:).
01->4
1 !
/ • 1 1
',A,sk.7,• 1
g-D'a 1
r•A 1
k-efri a r ks
_Alkalinity
Hardness 1• I.
Conduct .:_rn ti 12_04 ] aD% Hgcl
Final h q L;W,- 11
N•les2-
1
a to 1 KT< .1

Ohethicl aid Phygical Determinapions
. _
161-6?, pfr,d.
Facility NPDES Test Dates StartEnd
:
Test 'Organism: 0. oft,-,.,—ks, AnalystS,, Test Till:nal: Start 11%-0...- End
3
Conc.
Temp. Initial 2c1. Zs-- 0
q
.0. Lnit.1 al evvs.,
1- Ina]
PH .tn T-1 a
•I- n a AL -
AiKa I init.
Harcines
Conduct.. Initial
Final - rd?
Res. Chlorine r5k
Jay
4-
2N,Y.,-
-4S. 709D
CALI. Pot.)
2c'z I
C)...C. • 1-R a
D
kci 1,;`;•,-.c" • 5
tg GS I f< rLo
A.„/
Day
• conc. . -,; I Z 1
TeITIP , ini tia.1 9_1-.0 I 2.C,D
Finals ei-iii 1?W9l ifk-i.c• lz.4.--
D.I n 1 ti a .-4-?;1„ 1 '>_,Ac,
laq
- P.H iflltia F.CID?_ .IT;D:!-, gCb >ri' ¶J4 Wfc ., 'ol 11
r nal
-A- V, a I i n 1 ty
Hardness 1
1. ii
prmduct. Ti-,:, t-i a.-1 A•5A-- I 1,0)- icao 1 WI 163( iRg" 1 gt',9 II
re"." 'tf.'.) IR 7i
Re_s . Chlorine_
,
,
Conc. 1 _C•
Temp. Init:ial
Final
D.J. Initial
-)napH
t.-1 a
inai
Hardness
Final
Condutt.Tni-ial
marks
D / rtemarks
Da I
I I . 3 4 1 h emarks •
-f.b. I )c-i--i I R--o '1Z •lif'i -o, • Sc I„).s..-D II
2)4,',..e Z:Liq I 24,1,-_ 7_44. 2J4,12, 'APP. 171.4:-\-
.-t I. • . 3. IS•a. -1-6PA-ii -7, (13 •)-q5 'N't')V1-k I!
tte,Ci. 71-* I ' 90- 5 Lo9P- LAS' i ,,-(-:;), koc1.74 l'
II
.-.q.i, 1-n. I-. -4-gt c).•P '')-C)rc) I W:4N
I' 50. _
- , I I;
1AS I LA i? 50 .I I [
....) I i5`:. ck" tqA lq ) •Po 1 e. k II
.11 1/!tt
,..c›,

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J
MERITECH INC.
FISH LARVAL SURVIVAL/GROWTH DATA SHEET
CHRONIC FATHEAD MINNOW
FACILITYTrotzk‘ Peark.kviv_e_
NPDES #: Zo3
DATE OF TEST: to1z4ict,-
•DATE WEIGHEDT1-1:51,-'-'---;75--7;
ORGANISM: pc
PAGE: OF
• OUTFALL: 00k
•
CONC
REP.
FOIL WT.
(Mg)
FOIL WT. +
ORQ. (mg)
WT. OF
ORG. (mg')
# OR.
1
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MERITECH INC.
•
FISH LARVAL SURVIVAL/GROWTH DATA SHEET
CHRONIC FATHEAD MINNOW
FACILITY:i 04-
NPDES #: ICO2:4- tti-DZ,
DATE OF TEST: (b t tut.
DATE WEIGHED: )0.-
ORGANISM:
PAGE L OF -1.,-
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CONC
REP..
FOIL-WT. '
(Mg)
FOIL WT. ÷
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•MER1TECH
Mortality Data: Chronic Fathead Test
Start Date/Time Concentration CD-dift,
Day 0 Dayl Day 2
Rep #1 n 0 0
Rep #2
Rep #3
Rep #4 0
Concentration
End Date/Time
Day 3 Pay 4 Day5i Day6 bay 7
0 ;
0
0 0 -
' !
Day 0 Day 1 Day 2 Day 3 Day 4 Da 5 I
Rep #1 ,6 0 0 .6)
Rep #2 0 0 CD - 0
Day 6
Rep #3 .0 CD c) 0.C.) .9
Rep #4 0 D
• Concentration ri
Day 0 •Day 1 Day 2 • Day 3 Day 4 Day
Rep #1 0 c)
Rep #2 • 1 0 0 CD
Rep #3 - •,
Rep #4.
0
C7
Day 7
5 Day6 Day 7

MERITECH
Mortality Data: Chronic Fathead Test
Start Date/Time ie-1 i-73 1 iv '' End Date/Time iI dr y;;
Concentration'
Rep #1
Rep #2
Rep #3
Rep #4
Day0 , Day1 Day2 Day3 Day4 Days: Day6 Day7
.0 0 0 0
0 ().
0 0 4 c
I2 0
Concentration 3,4
r7
Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 Day 7
Rep #1 CDC
Rep #2 tc.) /C2)
Rep #3 0 C I
Rep #4 O 0 C C7, 0
Concentration C_ 1
Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 1 Day 6 Day 7
Rep #1 b 0 0 i 0 • n Li C1
Rep #2 0 (3 0 0 a
Rep #3 a ' 0 0 0
Rep #4 0 0 0

U
Title: pembroke
File: pembroke Transform: NO TRANSFORMATION
Kolmogorov Test for Normality
D = 0.1920 (p-value = ' , 0.0224)
D*-= 0.9718
Critical D* = 1.035 (alpha = 0.01 , N = 24)
= 0.895 (alpha = .0.05 , N = 24)�
Data PASS normality test (alpha =. 0.01). Continue analysis.
U

Title:, pembroke
File: pembroke Transform: NO TRANSFORMATION
Bartlett's Test for Homogeneity of Variance
Calculated Bl statistic = 6.1797 (p value = 0.2891)
Data PASS Bl homogeneity test at 0.01 level. Continue analysis:
Critical B = 15.0863 (alpha = 0.01, df = 5)
= 11.0705. (alpha = 0.05, df = 5)
J.
L3

•
Title: pembroke
File: pembroke Transform: NO TRANSFORMATION
ANOVA Table
SOURCE
DF SS MS F
Between
5 0.0108
Within (Error) 18
0.0514
0.0022 0.7566
0.0029
Total
23 0.0622
(p-value = 0.5924)
Critical F = 4.2479 (alpha = 0.01, df = 5,18)
= 2.7729 (alpha = 0.05, df = 5,18)
Since F < Critical F FAIL TO REJECT Ho: All equal (alpha = 0.05)
n

Title: pembroke
File: pembroke Transform: 1 NO TRANSFORMATION
Dunnett's Test - TABLE 1 OF 2 Ho:Control<Treatment
TRANSFORMED MEAN CALCULATED IN SIG
GROUP IDENTIFICATION MEAN ORIGINAL UNITS T STAT 0.05
1
2
3
4
5
6
control 0.5085 0 5085
Q•.43 % 0.4898 0 '4898
0.85% 0.4585 0.4585
1.7% 0.5100 0:5100
3.4% 0.5095 0:5095
6.8% 0.5248 0.5248
0.4961
1.3229
- 0.0397
-0.0265
- 0.4299
Dunnett critical value = 2.4100 (1 Tailed, alpha = 0.05, df = 5,18)
Title: pembroke
File: pembroke
Transform:
Dunnett's Test - TABLE 2 OF 2
NO TRANSFORMATION
Ho: Control<Treatment
NUM OF MIN SIG DIFF % OF DIFFERENCE
GROUP IDENTIFICATION REPS (IN ORIG. UNITS)I CONTROL FROM CONTROL
1
2
3
4
5
6
control 4
0.43% 4 0.0911
0.85% 4 0.0911
1.7% 4 0.0911
3.4% 4 0.0911
6.8% 4 0.0911
17.9
17.9
17.9
17.9
17.9
0.0187
0.0500
-0.0015
-0.0010
-0.0163

Title: pembroke
File: pembroke Transform: NO TRANSFORMATION
Summary Statistics on Data TABLE 1 of 2
GRP IDENTIFICATION N MIN MAX
MEAN
1 control 4 0.4660 0.5470 0.5085
2 •0.43% 4 0.4110 0.6000 0.4898
3 0.85% 4 0.4250 0.480i0 0.4585
4 1.7% 4 0.4500 0.562'p 0.5100
5 3.4% 4 0.3980 0.55610 0.5095
6 6.8% 4 0.4790 0.555'p 0.5248
Title: pembroke
File: pembroke
Transform:
NO TRANSFORMATION
Summary Statistics on Data TABLE 2 of 2
GRP IDENTIFICATION VARIANCE SD
SEM C.V. %
1 control 0.0012 0.0340
2 0.43% 0.0067 0.0819
3 0.85% 0.0006 0.0236
4 1.7% 0.0021 0.0460
5 3.4% 0.0056 0.0746
6 6.8% 0.0010 0.0323
0.0170
0.0409
0.0118
0.0230
0.0373
0.0162
6.6950.
16.7145
5.1443
9.0125
14.6477
6.1581

L. P 111.—I
NW' umEN MIN
Test Initiation Data:
Start Date: '1- ; .
Start Time:
Initials/Signature: St-
Date/Time Fed 'i•-'2--
-� •1tao
Date/Time
Born .�.• . c,_Lt•Prv+
Ic. /. Cc,:idoCa,,.ial G
Transfer
Date Time Initials
Day 1=c-v3.
MERITECH
Chronic Fathead Minnow Benchsheet
Transfer and Feeding Dates and Times
i,q. c3D 4,I 1;
G 4i •� % '
[t Uu .SL n v�
Day. 2PDT •5i n1�t
Day 3 tti.. c3
rm_ Z.5\
Day 4. '�-x?=1• _; ��•�
_ -Day 5-.., ,"_ 1_C�_M riLd ,�vt
Day 6 :1-- Loa{) c
Test Termination Data:
Initials/Signature: at - /
End Date:
End Time: /�i.�ic •
# of Organisms per Chamber: ID
Test Vessel Size:�r�Q
Test Solution Volume: 2
Temp. of Stock: %.S.D%C:
# of Reps: (-4
-Date
Day 0 it)t) ..
Day 1 ) •-q `' 3 `) Zen
Day 2
CS
Facility -iU
NPDES # 11; -1
Dilution Waters-;�i�,,;tz1
Randomization. Y.ES'i . NO
Incubator #:
Feeding
Time 1 Initials Time 2 Initials Time 3
5a.
Day 3 _—
- -- Day 4•
Day. 5 :1a,:s-•;,:�
Day 6 :��;,;.,.;�,•y,
Lac r�
S (. S
Initials
IS b

Li
Cheinioaa and:
Faci1it NPDES # t
Test Organism:Pa.p„..if,- AnalystR._ Test
------
, •
Dates:
1
11tly
Conc. 121314151-67. I Remarks
Temp. Initia1j� Ii •I 2.5%-n 12.c..(-) 1 Zi-v I 2v, 3
1
• final 16-t.E.: 1?-4-ES I .6.-kA I Lirt-..e- I L22..v 4_ II
1). 0 . intia1 I-144 19--SS 1
na I 110,.C'zi. I Lc;.3 11-T›s- 1.4:0? 1 ;-t,i I I '
pH initial I asPr IBG" Ig.13 1!
F i nal Ig-11 laik 152,.(2_1(LA 1
Alkalinity . I I Cu I' • I !.
Hardnes-s Rio I - I AO I ,f(-10. 1 • I !
Conduct- Initial I ?.24 I ?Ail- lz. 12t4 I 1 Lt.)°, jZt c'• I
Fi nal ? .•1 2.1S i
Res. cal orine If. ILr k.o 1 Lo‘t Icc I Lr_a. k 1
St a-r lc., End. 4
Start End
I ' Day 1
Conc. .(5.LAI 1 1 I • 2 - [ 1 4 *I-blb1/1 i-Zeinarks
Trcip. Initial 16.0. 1;!..F.:- 0 Vli---.1-% I Z.c---C.) 1 2..S.-. 12s- I. 2c---o I
Final. I Z)L1-.R: !?Ii.k 1254 (?: . I-14.1- I a-t-i. S. 12.9 12.LL 9-, 1
D.O. In 1 ti al 111-,L4ca, 1.I,sc, I Lic, I-4-Ail. 1-4..t.4- . .)...s.', 11-.(er> 1
-inal
to_-,',i. (,,gi.,,, I '41-.7,A 1-, 14._(-)S 4- 1.- --(NS. I
pH initial IRAs 1 ---'3 i..1. I 'L',i'''.- 1 .i--c,i 1 iS•12:. lar4 •2, I
i-ina.: 1_,,i-:..c 1:9, I cits lep-,_ I P.-:i t, I E-1.1.3 E. I \
-Alkalinity
1
1
1* ' 1
1 ! 1 . 1 . 1 .
Ha rdn1 ess ' . 1 .1 1 1 1 • ' '1
Conduct. Initial I OA I 0.2* Iso. 1,.....".4.",;-,!_* LI ? _ I 230 I? 1 1
Final 12.1`c_= 1D.5 . 1 2_R_. I a_ii_3 I 222.) 1?-18. 12,1c I
Rs. Chi cp--i n= izio A • If._0:i : - I ?...c.%4 Ito . . I Lo• i I / o-i 1 1-b-i I
I Da I
Conc. (--._,,---,T-111213,14 5 1 - b . 1 / 1 k ema rks
TeMp- ' Initial 12).s.-L--:, i ,....C1 :-..,) 1 ›s- 7-:, '1?C',7-% 1 2.C. - I ?A'..'t)
7,-; n=1 . 11M-.1- -12471- .I ?LE. I 2-- I N.re. I L-i.ta 12i.t.5.- 1
D.O. initial N-Qto. tl-LA- 1 1-)7,-4‘ I-+ k.-(4,(- 1-.6,1 I
i-Inal 1(rA 1 16,51":,'. 14.(-_-.:;- I 1 t-i,..-' 14.05 1'4- to 1i 1
pH In i ti al 19. ik - 1c!, C..) ft:_t:c=r 1,S.11-: I RI k 1511 lc\ A 1
,.,
rina 1 'IYA-f-sk•- 1 P>i , • 1 P. Ca 1 R.t,ck 1p,m few Igic, I
A)kalinity • 1 1 : 1 1 1 . .1. . 1 .1
HP rdness . I 1 • 1 ' 1 • 1. . • 1 1 I
ponduct .7.:1; tj.7--1 PAS 1"?.i.iS 1 ./_...-%..-; 1 '402; 12.IL\ I 2.1 tz 122.0 . 1
.Final I:Li 5 I 2. i i, . • I 2.--1)... I ?....vt I ?Zr--, I 2:2-g 12-2-. I
Res. 'Chi or in e. I (A-:*.,1 I 1.-.0,i I .e.'-i:!.- I I ..-:.c.? - i IL.b-t. Lo. k 14_0,, 1

1
1
1
1
J
Chemical a:1d. Physical De%ernin i.3.ons
•
FaClllt Y D
iTa?rcici.—. NPDES .fi,,); i; ?i-tii Test Dates :, Start
Test Organism: _1_�( End 11,: (�.
r �,"i�.; Analyst, Test Tune_ Start.a g End1i::c,,•.—
z..
Du
Conc. 1.4- i l 1 2 I ,3 1 e) • 5 I 6 1 j
Tern. ini i,ia? -.? -,,' I:=-y, ftf t I ZS•C I-t .s
Pi Dal i ;:t 143.1:s I ?,k, 2 12442-, I Z(-4.;- 12_t I,
J.U. in i ti a i 14 - 11.$) 14:3 r 1 ; I
I- inaI 1;. �, I,c:;� I ;: I-��.�� 14-t,a- 1-4. i,2_ I a.to
i l��.itr I`�.�� i �--�� I'
pH nit.al I Ii) 1=::1t i2.::i... I _ 1 alb Io p. i %-ii. I
Final ! D: R':=';:,.
:,r, 1. It.•Ci
,r--i-- I 9ti . I Rt�
Alkalinity 1 1 . 1 1• I -1 g.ii)
Aika1 1
-
flardness i i . I , l 1 i I
conduct. Initiai I2�4• Iat3- I ini;i I4,0e 1ZI`t ItA* I a1G, I
i22-I
Final 1L?4� 1:'2:-', 1L.1:`• 1 �l� Z,3D 1ZZ� I 1
Res. Cniorine 1'-•:... 1 )._ . 1 ,.V{ 1.:`r., iLo:t IL�,t I!c-1 i 1
Conc.
Temp.
Remarks
I Day I I
3.:.( I F 1 .2 1 .i 1.4 1 .5 1 6. 1/ I Remarks
ini;,iai 11...S.-o I?5- 125-i: 12S.C: I?5!.1....-� I•zi• 0 I
Finai 1 .;. ', I?q.'> 1 <:t':. 1-,;.,.=�- 124 �z4- 0 12_fS I
0 ..0 . - Initial 1.. t-iA Ih;i i I =N-Li 1 ? i- 1 -( I)- 6i: 11-1, )- 1
Final Itt t i {.e,t› I r s I")- 14-05 ! -.D 1•4-tv I
pi Tinitial 1?„.Q Ig!' • I8 Igo? I'€.t-I �a I,i�� 1
rlpal let.:5 lPc I4-' 18b1 1 ;s-t Imo t •I oac, I
Alkalinity I' - I 1 1 I I' i 1
Hardness I 1 1 .1 1 1 I I
, Conduct. Initial lati✓ • I2X 1 Li t I -4.-&_ 12-1,; I21 te- j ?._l5 I
. Final
na? I Li 3 1 --:-e I "<.ef; . i : I n \ i 23c, 122_° -
Res. Cni.ori ne kc,i. • I Zo. l 1L0,i I
Day
Cont.'. td•s' 11 1 2 1 3 i 4I b .1 6 1 i 1 Remarks
- • Temp. Initia, l? :�• 12 •c• I ri-, Izt izsD • 12t• Izi-..I
Final IVLt_ 2i. 2�tL
3t 1 i'•:t I t - -1 i t; •:.. 12m.4 • 1 2L1. 0 114 P. 1
13.O. initial Is -St 1.).Lt-c 1-- 1-rs.11)& I;-, I'*.F-t I
Final It,�3 It; .t 1')—oLt 1.h-ca 1'4_6* Iq .,1`4-bI
pH initial Isis 1siL IE.(i.E Iabto Ivr, I;;ba 1 ,tR 1
iZ CA I ,,.\ I..qi- I Rc-- I on Ieoul. I
Alkalinity i I. IS I 1St 1. -1 I
Hardness Izi'i. i I iy. i i tili 1 1 1
Conduct.;.31;4ia1IG•i4 I Z.it Ilte,:. 1itc:1..t I215 12.1(-4 I2_t3- I
Final TL.i t 12-i14 I =iCo 1?___i1=. 1 �i'.. I2LL. lac I
Res. Cili o- i rib 1 lr' 1i_[';• i I Lc.).,. 1i c.. 1 I /_0. 1 L. e. 9 kQ 1
1
Final

u
PAGE. OF
OUTFALL:;' -
INITIALS: d'` -
MERITECH, INC.
FISH LARVAL SURVIVAL/GROWTH DATA SHEET
. CHRONIC FATHEAD MINNOW
FACILITY: Pe.-om),, cj y
NPDES #: 6
DATE OF TEST: _ 0 17 _ / -_O?
DATE WEIGHED: - 7-11,,
ORGANISM:_

1
i
1
MERITECH
Mortality Data: Chronic Fathead Test
Start Date/Time_
Concentration
Day 0
Rep #1 t'c�
Day 1 Day 2
0 - l%
Rep #2 c)
Rep #3 V
Rep #4 • 0 c.)
Concentration 0. qa
Rep #1
Rep#2 0 0
Rep #3 0 i _I� :_
Day 3
cv
End Date/Time
Diay 5 Day 6 Day 7
c
Day 4.
O
C2
v
Day 0 Day 1 Day 2 Day 3' Day 4 Day 5
�II ' Rep #4
Concentration 0,
Rep #1
L.)
c ) C} .
Day 0 Day 1 Day 2 Day 3 Day 4 Day 5
Rep #2 (_.)
Rep #3 O) c.
Rep #4
U
Day 6
Day 6
f J
CD •
G
Day7
Day 7

1
1
J
MERITECH
Mortality Data: Chrdnic Fathead Test
Start Date/Time I I ily7,--- End Date/Time )-iic--r,t ( iCrwc—..' .
Cbncentration -
... Day 0 Day 1 Day 2 Day 3 Day 4 Day 5 Day 6 ' Day 7
Rep #1
Rep #2 C.-) cl) ,------,
%....x •-f3
i
Rep #3 -. -0' ---- b ,--0 c.,) C:2 c...) . • c.--_-)
Rep #4
Concentration
0
D.
• Day 0 Day 1 Day 2 Day 3 Day-4 Da 5 • Day 6 Day-7
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Rep #3
Rep #4
Concentration 61 g
Day 0 Day 1 Day 2 Day 3 Day 4 Day 5
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Rep #2
Rep #3
Rep #4
(-D D
0
0
0
Day 6 Day 7

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Title: PEMBROKE
File: PEMBROKE Transform: NO TRANSFORMATION
Kolmogorov Test - for Normality
D=
D* _
0.1459
0.7385
Critical D*
(p-value > 1 0 . 100 )
= 1.035 (alpha = 0.01 , N = 24)
= 0.895 (alpha = 0.05 , N = 24)
Data PASS normality test (alpha = 0.01). Continue analysis.

Title: PEMBROKE
File:
PEMBROKE
Transform: NO TRANSFORMATION
Bartlett's Test for Homogeneity ofVariance
Calculated Bi statistic = 9..2263.
Data PASS B1 homogeneity test at 0•.01 level.
(p-value = 0.1004)
Continue analysis.
Critical B = 15 ,0863- (alpha = 0.01, df = 5)
11.0705 (alpha = 0.05, df = 5)

Title: PEMBROKE
'File: PEMBROKE
Transform:
Summary Statistics on Data
NO TRANSFORMATION
TABLE 1 of 2
GRP IDENTIFICATION N MIN
MAXI
MEAN
1 'CONTROL 4 0.3550 .0.420 0.3917
2 0.43% 4 0..3100 0.4160 0.3660
3 0.85% 4 0.2740 0.3690 0.3220
4 1.7% 4 0.3980 0.4150 0.4088
5 3.4% 4 0.2800 0.4400 0.3455
6 6.8% 4 0.3660 0.4720 0.3950
Title: PEMBROKE
File: PEMBROKE Transform:'
Summary Statistics on .Data
NO TRANSFORMATION
TABLE 2 of 2
GRP IDENTIFICATION. VARIANCE SD- 'SEM
1 CONTROL 0.0010 0.0320
2 0.43% 0.0021 •0.0456
3 0.85% 0.0017 0.0413
4 1.7%' 0.0001 0.0075.
5 3.4% 0.0052 0.0719
6 6.8% 0.0027 .0.0515
'0.0160
0.0228
0.0207-
0.0037
0.0360
0.0257
C.V. % 0
8.1721
12.4529
12.8373
1.8240
20.8132
13.0357

I
L'
Title-: PEMBROKE
File: PEMBROKE
Dunnett's Test
Transform:
TABLE l OF 2
NO TRANSFORMATION
Ho:Control<Treatment
GROUP IDENTIFICATION
1
2
3
4
5
6
CONTROL
0.43 %
0.85%
1.7%
3.4%
6.80
TRANSFORMED
MEAN
0.3917
0.3660
0.3220
0.4088
0.3455
0.3950
MEAN CALCULATED IN SIG
ORIGINAL UNITS T STAT 0.05
0,. 3.917
O',.3660
01 3220
O'.4088
0 3455
0.3950 -
0.7919
2.1450
-0.5228
1.4223
-0.0999
Dunnett»critical value = 2.4100
Title: PEMBROKE
File: PEMBROKE
Dunnett's Test
(1 Tailed, alpha
'Transform:
- TABLE 2 OF 2.
=, 0. 05; df = 5,18) •
NO TRANSFORMATION
Ho:Control<Treatment
GROUP IDENTIFICATION
1
2
3
4
5
6
CONTROL
0.43%
0.85%
1.7%
3.4%
6.8%
NUM OF
REPS
4
4
4
4
4
4
MIN SIG DIFF % OF DIFFERENCE
(IN ORIG. UNITS)! CONTROL' FROM CONTROL
0.0784
0.0784
0.0784
0.0784
0.0784
20.0
20.0
20.0
20.0
20.0
0.0257
0.0697
- 0.0170
0.0462
- 0.00.33

Title: PEMBROKE
File: PEMBROKE Transform: NO TRANSFORMATION
Dunnett's Test
- TABLE 1 OF 2 Ho:Control<Treatment
GROUP
TRANSFORMED MEAN CALCULATED IN SIG
IDENTIFICATION MEAN ORIGINAL UNITS T STAT 0.0E
1 CONTROL 0.3917
2 0.43% 0.3660
3 0.85% 0.3220
4 1.7% 0.4088
5 3.4% 0.3455
6 6.8% 0.3950
0.3917
0.3660 •
0.;3220
0.4088
0:3455
0.3950
0. 7919
2.1450
-0.5228
1.4223
-0.0999
Dunnett critical value = 2.4100 (1 Tailed, alpha
Title: PEMBROKE
File: PEMBROKE
Dunnett's Test
Transform:
TABLE 2 OF 2
= 0.05, df = 5,18)
NO TRANSFORMATION
Ho :Control<Treatment
NUM OF MIN SIG DIFF % OF DIFFERENCE
GROUP IDENTIFICATION REPS (IN ORIG. UNITS). CONTROL FROM CONTROL
1 CONTROL 4
2 0.43% 4 0.0784 20.0 0.0257
3 0.85% 4 0.0784 20.0 0.0697
4 1.7% 4 0.0784 20.0-0.0170
5 3.4% 4
6 0.0784 1 � 20.0 0.0462
6.8% 4 0.0784
20.0-0.0033

Title: PEMBROKE
File: PEMBROKE Transform: NO TRANSFORMATION
ANOVA Table
SOURCE
DF SS MS F
I ,
Between
5 0.0220
Within (Error) 18
0.0381
0.0044 2.0830
0.0021
Total
23 .0.0601
(p-value = 0.1149)
Critical F = 4.2479 (alpha = 0.01, df = 5,18)
= 2..7729 (alpha = 0.05, df = 518)
Since F < Critical F FAIL TO REJECT Ho:' All equal (alpha = 0.05)