HomeMy WebLinkAboutWQ0039552_Renewal Application_20220331Initial Review
Reviewer Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
Permit Number (IR) * WQ0039552
Applicant/Permittee Town of Mocksville
Applicant/Permittee Address 171 Clement Street, MoCksville, NC 27028
Is the owner in BIMS? Yes No Is the facility in BIMS?
Owner Type
Facility Name
County
Fee Category Minor
Is this a complete application?*
Yes No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Municipal
Town of Mocksville Class A Residuals Program
Davie
Does this need review by the hydrogeologist? * Yes No
Regional Office
CO Reviewer
Admin Reviewer
Yes No
Fee Amount $0
Complete App Date 03/31/2022
Below list any additional email address that need notification about a new project.
... ... ..
Email Address
Comments to be added to email notfication
Comments for Admin
Comments for RO
Comments for Reviewer
Comments for Applicant
Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Brent Collins
Email Address*
brent.collins@emaresourcesinc.com
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
336-399-3646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
Permit Number: *
WQ0039552
Has Current Existing permit number
Applicant/Permittee*
Town of Mocksville
Applicant/Permittee Address*
171 Clement Street, Mocksville, NC 27028
Facility Name*
Town of Mocksville Class A Residuals Program
Please provide comments/notes on your current submittal below.
High -Rate Infiltration
Reclaimed Water
Residuals
Other
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at nathaniel.thornburg@ncdenr.gov.
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Town of Mocksville WTP - Permit Renewal -
9.44MB
WQ0039552.pdf
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 3/30/2022
g
Inc.
Permit Renewal Application
For the Town of Mocksville WTP
WQ0039552
Distribution of Class A Water
Treatment Plant Residuals
Prepared By:
EMA Resources Inc.
755 Yadkinville Road
Mocksville, NC 27028
336-751-1441
March 30, 2022
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1617 Mail Services Center
Raleigh, NC 27699-1617
RE: Permit Modification — WQ0039552
To Whom it May Concern:
EMA Resources is submitting the included permit renewal for Town of Mocksville's
WTP Land Application Permit - WQ0039552. There are no modifications to the process
or the permit included.
If you have any questions concerning this renewal, please contact Brent Collins —
Director of Technical Services
Respectfully,
Brent Collins
Director of Technical Services
brent.collinsgemaresourcesinc.com
(336) 399-3646
Phone 336975191441 — Fax 336975191442
755 Yadkinville Rd — Mocksville, NC 27028
Table of Contents
1) DCAR Form
a) Current Permit
2) Program Information
3) RSC Form
a) Vicinity Map
b) Process Flow Diagram & Process Summary
c) Quantitative Justification
4) Residuals Quality Information
a) Laboratory Analytical Reports
b) Residuals Information Sheet
5) Operation & Maintenance Plan
1) DCAR Form
State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
L APPLICANT INFORMATION:
1. Applicant's name: Town of Mocksville WTP
Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership Privately -Owned Public Utility
FLI Federal ❑ State ® Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Ken Gamble Title: Town Manager
Applicant's mailing address: 171 Clement Street
City: Mocksville State: NC Zip: 27028- Vp
Telephone number: (336) 753-6701 Email Address: kgamble&mocksvillenc.gov
2. Consultant's name: Brent Collins License Number (for P.E.):
Affiliation: ❑ On Staff ® Retained (Firm: EMA Resources Inc.)
Consultant's mailing address: 755 Yadkinville Rd
City: Mocksville State: NC Zip: 27028-
Telephone number: (336) 399-3646 Email Address: brent.collinsA_emaresourcesinc.com
3. Fee submitted: $0 (See Instruction B)
IL PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00039552
Date of most -recently issued permit: 11/17/2017
Date of most -recently certified Attachment A (if different than the permit): 11/17/2017
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Town of Mocksville WTP
City: Mocksville State: NC Zip: 27028-_
Coordinates: Latitude: 35' 53' 22" Longitude: 80. 34' 43"
Datum: NAD83 Level of accuracy: Nearest Second
Method of measurement: GPS
County where facility is located: Davie
2. Facility contact (person familiar with residuals preparation):
Name: Justin Turbyfill Title: ORC
Mailing address: 771 Sanford Avenue
City: Mocksville State: NC
Telephone number: 3( 36) 751-2635
Zip: 27028-
E-mail address: mocksville cgenvirolink.com
FORM: DCAR 06-16 Page 1 of 3
3. Is the residual process facility also the generator? ® Yes; ❑ No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: 365 days (Note: the Division requires minimum 30 days storage in units that are separate
from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
® other (explain); Bulk liquid land application at agronomic rates
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials Amounts to be added
Der 1.0 dry ton of residuals (dry ton)
3. Approximate amounts of the residuals received and processed at the facility: 188 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 188 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): Two — 275,000 gallon residuals storage tanks equipped with floating decanter.
The residuals will be removed annually for a maximum of 365 days of storage prior to distribution
6. Does the facility have a stormwater management plan? ❑ Yes; ® No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: N/A
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
e
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of 3
Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes U No, Explain;
I, Ken Gamble Town Manager
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Town of Mocksville - WTP
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature:
Date:
FORM: DCAR 06-16 Page 3 of 3
la) Current Permit
Water Resources
ENVIRONMENTAL QUALITY
November 17, 2017
MARcus A. ABERNETHY — TOWN MANAGER
TOWN OF MOCKSVILLE
171 CLEMENT STREET
MOCKSVI LLE, NORTH CAROUNA 27028
Dear Mr. Abernethy:
ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
LINDA CULPEPPER
Interim Director
Subject: Permit No. WQ0039552
Town of Mocksville DCAR
Distribution of Class A Water
Treatment Plant Residuals
Davie County
In accordance with your permit application request received October 19, 2017, we are forwarding
herewith Permit No. WQ0039552 dated November 17, 2017, to the Town of Mocksville for the operation
of the subject residuals management program.
This permit shall be effective from the date of issuance until October 31, 2022, and shall be subject
to the conditions and limitations as specified therein. Please pay particular attention to the monitoring
requirements listed in Attachment A. Failure to establish an adequate system for collecting and maintaining
the required operational information shall result in future compliance problems.
If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding.
If you need additional information concerning this permit, please contact Troy Doby at (919) 807-
6336 or trgy.dohygnedetir.gov.
Sincerely,
,L,mda Culpepper, Interim Directo
a Division of Water Resources
cc: Davie County Health Department (Electronic Copy)
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Roy L. Whitaker -- EMA Resources, Inc. (Electronic Copy)
Digital Permit Archive (Electronic Copy)
Central Files
<'7 "Nothing Cornpares'�-,
State of North Carolina I Environmental Quality I Water Resources I Water Quality Permitting I Non -Discharge Permitting
1617 Mail Service Center G Raleigh, North Carolina 27699-1617
919-807-6332
NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
DISTRIBUTION OF CLASS A WATER TREATMENT PLANT RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
Town of Mocksville
Davie County
FOR THE
operation of a residuals management program for Town of Mocksville and consisting of the distribution of
Class A water treatment plant residuals generated by the approved facility listed in Attachment A with no
discharge of wastes to surface waters, pursuant to the application received October 19, 2017, and in
conformity with other supporting data subsequently filed and approved by the Department of
Environmental Quality and considered a part of this permit. The use and disposal of residuals are regulated
under Title 40 Code of Federal Regulations Part 257. This permit does not exempt the Permittee from
complying with the federal regulations.
This permit shall be effective from the date of issuance until October 31, 2022, and shall be subject to the
following specified conditions and limitations:
I. SCHEDULES
1. No later than six months prior to the expiration of this permit, the Permittee shall request renewal of
this permit on official Division forms. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will renew the permit for such period of
time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A
NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application.
[ 15A NCAC 02T .0108(b)(2), 02T .0105(d), 02T .0109]
H. PERFORMANCE STANDARDS
1. The subject residuals management program shall be effectively maintained and operated at all times so
there is no discharge to surface waters, nor any contravention of groundwater or surface water
standards. In the event the facilities fail to perform satisfactorily, including the creation of prolonged
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
distribution of residuals, contact the Winston-Salem Regional Office supervisor, and take any
immediate corrective actions. [G.S. 143-215.11
2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [I 5A NCAC 02B .0200,
02L .0100]
WQ0039552 Version 1.0 Shell Version 171103 Page 1 of 10
3. Only residuals generated by the facility listed in Attachment A are approved for distribution in
accordance with this permit. [G.S. 143-215.1]
4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed
the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis):
Parameter
Ceiling Concentration
(milligrams per kilogram)
Monthly Average
Concentration
(milligrams per kilogram)
Arsenic
75
41
Cadmium
85
39
Copper
4,300 HI
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
n/a
Nickel
420
420
Selenium
100
100
Zinc
7,500
2,800
[15A NCAC 02T. 1105]
5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T
.1106 (a) and (b)(2). Exceptions to this requirement shall be specified in Attachment A. [15A NCAC
02T .1106]
6. Setbacks for treatment and storage facilities shall be as follows:
Setback Description
Setback
feet
Habitable residence or place of public assembly under separate ownership or not to
be maintained as part of the project site
100
Property lines
50
Private or public water supply
100
Surface waters (streams — intermittent and perennial, perennial waterbodies, and
wetlands
50
Wells with exception to monitoring wells
100
[ 15A NCAC 02T. 11081
WQ0039552 Version 1.0 Shell Version 171103 Page 2 of 10
7. Setbacks for Class A land applied bulk residuals shall be as follows:
Setback by residual type
Setback Description
(feet)
Liquid
Cake'
Private or public water supply
100
100
Surface waters (streams — intermittent and perennial,
100
25
perennial waterbodies, and wetlands
Surface water diversions (ephemeral streams,
25
0
waterways, ditches
Groundwater lowering ditches (where the bottom of
25
0
the ditch intersects the SHWT
Wells with exception to monitoring wells
100
100
Bedrock outcrops
25
0
' Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported and
spread as a solid (e.g., using a backhoe, front end loader, slinger spreader, broadcast spreader or
other equipment designed for handling solid materials) without leaving any significant liquid
fraction behind.
[ 15A NCAC 02T .11081
8. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance
of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen
requirements based on the determined Realistic Yield Expectations (RYE) using any of the following
methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science h :/./nutrients.soil.ncsu.edu/yields/indg&.Vhp). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services; the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter 1
(bgp://www.ncaar.i4ov/SWC/tech/documents/9th Guidance_ Doc_ 100109.pdf).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards(ftp://ftp-fc.sc.egov.usda.gov/NHQ/practice-standards/standards/590.pdf).
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[15A NCAC 02T .1109(b)(1)(k)]
WQ0039552 Version 1.0 Shell Version 171103 Page 3 of 10
9. The Permittee shall not distribute Class A water treatment plant residuals that have a sodium adsorption
ratio (SAR) of 10 or higher without prior written Division approval. The Permittee may seek approval
by demonstrating that the entity accepting the residuals is: aware of the effects of a high SAR content;
has agreed on proper residual application rates; and has agreed to operational considerations to ensure
that the high SAR content will not adversely impact the receiving sites. Recommendations regarding
sodium application rate, soil amendments (e.g., gypsum, etc.) or a mechanism for maintaining site
integrity and conditions conducive to crop growth, can be obtained from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist. [15A NCAC 02T
A 108(b)(1)]
M. OPERATION AND MAINTENANCE REQUIREMENTS
The residuals management program shall be properly maintained and operated at all times. The
program shall be effectively maintained and operated as a non -discharge system to prevent any
contravention of surface water or groundwater standards. [15A NCAC 02T .1110]
2. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications
to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan,
at the minimum, shall include:
a. Operational functions;
b. Maintenance schedules;
c. Safety measures;
d. Spill response plan;
e. Inspection plan including the following information:
i. Names and/or titles of personnel responsible for conducting the inspections;
ii. Frequency and location of inspections, including those to be conducted by the ORC, and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
iii. Detailed description of inspection procedures including record beeping and actions to be taken
by the inspector in the event that noncompliance is observed pursuant to the noncompliance
notification requirements under the monitoring and reporting section of the permit;
f. Sampling and monitoring plan including the following information:
i. Names and/or titles of personnel responsible for conducting the sampling and monitoring;
ii. Detailed description of monitoring procedures including parameters to be monitored;
iii. Sampling frequency and procedures to assure that representative samples are being collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen reduction requirements (e.g. facilities that distribute multiple times per year but
have an annual sampling frequency, may need to sample during winter months when pathogen
reduction is most likely to be negatively affected by cold temperatures).
[15A NCAC 02T .1100]
WQ0039552 Version 1.0 Shell Version 171103 Page 4 of 10
3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the facility, the Permittee shall designate and employ a certified operator in responsible
charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC
08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204,
or as specified in the most recently approved O&M plan (i.e., see Condition 111.2.), and shall comply
with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and
designation requirements, please contact the Division of Water Resources' Protection and Enforcement
Branch at (919) 707-9105. At the time of this permit issuance, a certified ORC is not required for the
subject Distribution of Class A Residuals program. [15A NCAC 02T .0117]
4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be
maintained at the land application sites during land application activities. [15A NCAC 02T
.0108(b)(1)]
5. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be
maintained in all residuals transport and application vehicles. [15A NCAC 02T .I 110]
b. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind
erosion and surface runoff from conveying residuals from the land application sites onto adjacent
properties or into surface waters. [G.S. 143-215.11
7. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land
application sites onto which residuals are applied, or application shall be in accordance with the crop
management plan outlined by the local Cooperative Extension Office, the Department of Agriculture
and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved
by the Division. [15A NCAC 02T .1109(b)(1)]
8. Bulk residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes prolonged nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or groundwater standards;
d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the
residuals would occur;
e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a
24-hour period following a residuals land application event;
f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than
18% for injected or incorporated bulk liquid residuals;
h. If the land does not have an established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in a
USDA no -till program shall be exempted from meeting this vegetative cover requirement;
i. If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
j. If the vertical separation of bedrock and the depth of residuals application is less than one foot;
k. Application exceeds agronomic rates.
[I5A NCAC 02T. 1109]
WQ0039552 Version 1.0 Shell Version 171103 Page 5 of 10
9. The Permittee shall notify all third -party entities receiving bulk distributed Class A water treatment
plant residuals that land application activities occurring on the third -parry's property shall meet the
requirements in 15A NCAC 02T .1108(b)(1) and 02T .1109(b) (i.e., Conditions 11.8. and III.8.,
respectively). [15A NCAC 02T .1103(5)]
10. All residuals shall be adequately stored to prevent untreated leachate runoff. The finished product may
be placed on a concrete pad, placed under shelter or physically covered until it is distributed to a third -
parry entity. If bulk residuals are to be applied, the residuals may be staged at the application site for
up to 30 days for biological residuals, and 60 days for non -biological residuals. If an alternate storage
site is used, approval must be obtained from the Division. [15A NCAC 02T .0108(b)(1)]
11. A label shall be affixed to the bag or other container in which residuals are sold or given away for land
application, or an information sheet shall be provided to the person who receives Class A residuals. At
a minimum, the label or information sheet shall contain the following:
a. The name and address of the person who prepared the residuals;
b. A statement that residual land application is prohibited except in accordance with the instructions
on the label or information sheet;
c. A statement identifying that this material shall be prevented from entering any public or private
water supply source (including wells) and any surface water (e.g., stream, lake, river, wetland, etc.);
d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use.
[I5A NCAC 02T. I 109(a)]
12. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals
contrary to the conditions of this permit. The Permittee shall report to the Winston-Salem Regional
Office as per reporting conditions under Condition IV.8. any person or entity known to be applying
residuals contrary to the condition of this permit. [15A NCAC 02T .I 103(a)]
WQ0039552 Version 1.0 Shell Version 171103 Page 6 of 10
W. MONITORING AND REPORTING REOUIREMENTS
1. Any Division -required monitoring (including groundwater, plant tissue, soil and surface water
analyses) necessary to ensure groundwater and surface water protection shall be established, and an
acceptable sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)]
2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation
and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste under 40
CFR Part 261 shall not be used or disposed under this permit. The analyses [corrosivity, ignitability,
reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed at the
frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of
five years. Any exceptions from the requirements in this condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1, 1 -Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
Chlorobenzene {100.0)
Heptachlor (and its hydroxide)
0 008
Toxaphene (0.5)
Chloroform (6.0)
Hexachloro-1,3-butadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200,0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle.
[15ANCAC 13A .0102(b), 02T .1101, 02T .1105]
WQ0039552 Version 1.0 Shell Version 171103 Page 7 of 10
3. An analysis shall be conducted on the residuals from each source generating facility at the frequency
specified in Attachment A, and the Permiee shall maintain the results for a minimum of five years.
The analysis shall include the following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[15A NCAC 02T. I 10 1]
4. Residuals shall be monitored for compliance with pathogen reduction requirements at the frequency
specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the
approved O&M plan. The required data shall be specific to the stabilization process utilized, and
sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC
02T .1106 (a) and (b)(2) shall be met. Any exceptions from the requirements in this condition shall be
specified in Attachment A. [15A NCAC 02T .1106, 02T .1107, 02T .1111(c)]
5. Laboratory parameter analyses shall be performed on the residuals as they are distributed, and shall be
in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B .05051
6. The Permiee shall maintain records tracking all bulk residual distribution or land application events
performed by the Permiee. At a minimum, these records shall include the following;
a. Source of residuals;
b. Date of distribution/land application;
c. Name and address of recipient of residuals;
d. Volume of residuals distributed to each recipient;
e. Intended use of residuals;
£ If land application events performed by the Permiee - Nitrogen Application Rate based on RYLs
(if using data obtained from the North Carolina State University Department of Soil Science
Website, the printout page shall be kept on file and reprinted every five years).
[15A NCAC 02T .0108(a)]
7. Three copies of an annual report shall be submitted on or before March 1". The annual report shall
meet the requirements described in the Instructions for Residuals Application Annual ReportingForms.
orms.
Instructions for reporting and annual report forms are available at
http://deq.ne.gov/about/divisions/water-resources/water-resources-permits/wastewater-branch/non-
discharge-permittin -ug nit/reportin -fg orms. or can be obtained by contacting the Non -Discharge
Permitting Unit directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
WQ0039552 Version 1.0 Shell Version 171103 Page 8 of 10
[15A NCAC 02T .1111(a)]
8. Noncompliance Notification
The Permittee shall report by telephone to the Winston-Salem Regional Office, telephone number (336)
776-9800, as soon as possible, but in no case more than 24 hours or on the next working day following
the occurrence or first knowledge of the occurrence of any of the following:
a. Distribution of residuals abnormal in quantity or characteristic.
b. Any failure of the distribution program resulting in a release of material to surface waters.
c. Any time self -monitoring indicates the facility has gone out of compliance with its permit
limitations.
d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of
adequate residual treatment.
e. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons
reporting such occurrences by telephone shall also file a written report in letter form within five days
following first knowledge of the occurrence. This report shall outline the actions taken or proposed to
betaken to ensure that the problem does not recur. [15A NCAC 02T .0105(1), 02T .0108(b)(1)]
V. INSPECTIONS
1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan. [15A NCAC 02T .0108(b)]
2. Prior to each bulk residuals distribution event, the Permittee or his designee sball inspect the residuals
storage, transport and distribution facilities to identify malfunctions, facility deterioration and operator
errors that could result in discharges to the environment, a threat to human health or a public nuisance.
The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of
inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee
shall maintain this inspection log for a period of five years from the date of inspection, and this log
shall be made available to the Division upon request. [15A NCAC 02T .0108(b)]
3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the distribution sites or facilities permitted herein at
any reasonable time for the purpose of determining compliance with this permit; may inspect or copy
any records required to be maintained under the terms and conditions of this permit; and may collect
groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)]
VI. GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an
enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to
143-215.6C, [G.S. 143-215.6A to 143-215.6C]
2. This permit shall become voidable if the residuals distribution events are not carried out in accordance
with the conditions of this permit. [ 15A NCAC 02T .0110]
3. This permit is effective only with respect to the nature and volume of residuals described in the permit
application and other supporting documentation. [G.S. 143-215.1]
WQ0039552 Version 1.0 Shell Version 171103 Page 9 of 10
4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies
(e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in
15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and
under the Division's General Permit NCGO 10000; any requirements pertaining to wetlands under 15A
NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter
143 of the General Statutes. [15A NCAC 02T .0105(c)(6)]
In the event the residuals program changes ownership or the Permittee changes his name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division forms, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary. The Permittee of record shall remain fully responsible for
maintaining and operating the residuals program permitted herein until a permit is issued to the new
owner. [15A NCAC 02T .0104]
6. This permit is subject to revocation or unilateral modification upon 60-day notice from the Division
Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. [ 15A NCAC 02T .0110]
7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained
herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b).
[15A NCAC 02T .0120]
8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay
the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T
.0105(e)(3)]
Permit issued this the 17' day of November 2017
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
Linda Culpepper, Interim Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0039552
WQ0039552 Version 1.0 Shell Version 171103 Page 10 of 10
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2) Program Information
Program Information
1. Provide a narrative explaining the following:
a. How will the materials be handled and transported from where the residuals were
produced?
The water plant residuals are strictly sediment which has settled in the sedimentation
basin and accumulated in the filters. The residuals are drawn off the bottom of the
sedimentation basins on a daily basis and pumped to the storage tanks. The filter wash
water is pumped to the storage tanks on a daily basis where any remaining residuals will
settle.
b. How will the residuals be processed/treated?
The residuals are thickened via decanting of the water which is discharged via an
NPDES permit.
c. How will leachate collection be handled?
There is no leachate in the system. The decant from the storage lagoon is discharged in accordance with
the NDPES permit.
d. Where will the residuals be stored until processing?
The thickened residuals will be stored in one of two — 275,000 gallon storage/decant tanks
e. How will the final product be distributed?
The residuals will be delivered to local farmers via 6,500 gallon tankers. Each load will be off-loaded
to a tractor pull tank spreader or pumper truck for application on a receiver site (grassland or row -
crop)
2. Attach a marketability statement detailing destinations and approximate amounts of the final product to
be distributed.
The residuals have limited major (N, P, K) nutrient value, but they have additional micro -nutrients that can
be utilized by crops for optimum crop growth. The program will recruit local farmers to participate in the
bulk land application program. They will be advised as to the limited nutrient value of the residuals, but
they will be offered up to one ton of agricultural lime for soil pH adjustment where soil analysis indicated
a need.
3. Provide either a label that shall be affixed to the bagged residuals or an information sheet that shall be
provided to the person who receives the processed residuals. The label or information sheet shall contain,
at a minimum, the following information.
Residuals will be distributed through bulk land application of liquid, managed by the contracted land
application firm. See attached information sheet.
3) RSC Form
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DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Mocksville WTP
2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: ).
3. Facility contact person and title: Justin Turbyfill
Complete mailing address: 771 Sanford Rd
City: Mocksville State: NC Zip: 27028-
Telephone number: (336) 751-2635 E-mail address: mocksvillegenvirolinkinc.com
4. Facility physical address: 771 Sanford Rd
City: Mocksville State: NC Zip: 27028-
Coordinates: Latitude: 35' 53' 22" Longitude: 80. 34' 43"
Datum: NAD83 Level of accuracy: Nearest Second
Method of measurement: GPS
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
® treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: __E % industrial and % domestic)
❑ other (explain: _ ).
6. Does the facility have an approved pretreatment program: ❑ Yes ® No
7. Facility permitted/design flow: 2 MGD and facility average daily flow: 0.9 MGD
8. Average amount of residuals being generated at this facility 188 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: Two — 275,000 gallon residuals storage tanks equipped with floating decanter.
Type and volume of residuals storage (i.e., outside of residuals treatment units): Same as above
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
❑ 40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
❑ Biological ® Non -Biological
FORM: RSC 06-16 Page 1 of 5
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well
as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical and Date of analysis: 01/24/22
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes ❑ no. Flashpoint: >200 OF (> 140°F)
Passed reactivity test: W yes Ono. HCN: <0.250 mg/kg (<250) & H2S: <25 mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
TCLP Parameter
Limit
(mgfi)
Result
(mgfi)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
ND
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
ND
Carbon Tetrachloride
0.5
ND
Lindane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1,1-Dichloroethylene
0.7
ND
2,4,5-Trichlorophenol
400.0
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
ND
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND
FORM: RSC 06-16 Page 2 of 5
4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate
the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical and Date of analysis: 01/24/22
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
7.58
Cadmium
85
39
<0.377
Copper
4,300
1,500
37.2
Lead
840
300
28.5
Mercury
57
17
<0.124
Molybdenum
75
n/a
<2.55
Nickel
420
420
28.1
Selenium
100
100
<6.04
Zinc
7,500
2,800
86.4
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of
5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 5.3 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analytical and Date of analysis: 01/24/22
Parameter
Result
(mg/kg)
Aluminum
89100
Ammonia -Nitrogen
2090
Calcium
1690
Magnesium
3960
Nitrate -Nitrite Nitrogen
<93.4
pH (Standard Unit)
6.5
Phosphorus
1580
Potassium
2960
Sodium
289
Total Kjeldahl Nitrogen
14600
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.20
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and
conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: - %. This rate
is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: The solids are considered
raw undigested with regards to mineralization.
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1st) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/kg)
Surface
2390
3140
Injection/Incorporation
3435
4185
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of
7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
❑ Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, 9 air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur
when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of
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Town of Mocksville -WTPDATE: 03.23.22 Land Application Program
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LU
LU
Z
z
LU
00
0
0
.N
o
�
0
0
0
0
Z
G3
m
o
V)
0
0
4L[0-3 ON 'OII ON - LLZBZ VNIIOHVO H1a0N
31L018VHO 3OVld S3NIS OOLOI
'ONI Sa33NION3 SIIIIM
3c) Quantitative Justification
Mocksville WTP
Quantitative Justification for Residuals Production Rate
The Town of Mocksville WTP currently thickens the residuals in two — 275,000
gallon storage/decant tanks. The solids build up in the storage tank and need to be
removed approximately every 2-3 years. The thickened residuals are pumped along
with high pressure water to wash the basin.
IDU,v vv x
„ /,' , n/C7 I ,
Z5.34 x v.un =
Dry lbs/ton Dry
375,300 - 2000 = 188
4a)Laboratory Analytical Reports
Waypointo
ANALYTICAL
2/2/2022
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 22-025-0020
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax 901.213.2440
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/25/2022 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
TNI
Page 1 of 9
Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901.213.2440
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2022
Arkansas
State Program
88-0650
02/07/2022
California
State Program
2904
06/30/2022
Florida
State Program
- NELAP
E871157
06/30/2022
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2022
Illinois
State Program
- NELAP
200078
10/10/2022
Kentucky
State Program
80215
06/30/2022
Kentucky
State Program
KY90047
12/31/2022
Louisiana
State Program
- NELAP
LA037
12/31/2022
Louisiana
State Program
- NELAP
04015
06/30/2022
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
415
12/31/2022
Pennsylvania
State Program
- NELAP
68-03195
05/31/2022
South Carolina
State Program
84002
06/30/2022
South Carolina
State Program
84002
06/30/2022
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2022
Virginia
State Program
00106
06/30/2022
Virginia
State Program
- NELAP
460181
09/14/2022
Page 1 of 1 00001/22-025-0020
Page 2 of 9
Waypoint
ANALYTICAL
Report Number: 22-025-0020
Client Project Description: Mocksville, NC
Lab No Client Sample ID
91577 Mocksville V TP
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax 901.213.2440
www.waypointanalytical.com
Sample Summary Table
Matrix Date Collected Date Received
Solids 01/24/2022 09:00 01/25/2022
Page 3 of 9
Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 22-025-0020
Date: 2/1 /2022
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax 901.213.2440
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 99187
Analyte: Aluminum
QC Batch No: 1-596771/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Calcium
QC Batch No: 1-597088/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Copper
QC Batch No: 1-596771/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Iron
QC Batch No: 1-596771/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Potassium
QC Batch No: 1-597000/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 99187
Analyte: Magnesium
QC Batch No: 1-597000/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Manganese
QC Batch No: 1-596771/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Page 4 of 9
Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax 901.213.2440
www.waypointanalytical.com
Analyte: Phosphorus
QC Batch No: 1-597000/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Lead
QC Batch No: 1-596771/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Sulfur
QC Batch No: 1-597000/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99187
Analyte: Zinc
QC Batch No: 1-596771/1-596454
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 9
Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number : 22-025-0020
Lab No : 91577
Sample ID : Mocksville WTP
Project Mocksville, NC
Information :
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax 901.213.2440
www.waypointanalytical.com
REPORT OFANALYSIS
Report Date : 02/02/2022
Received : 01/25/2022
Danyale Love
Project Manager
Matrix: Solids
Sampled: 1/24/2022 9:00
Test
Results
Units
MDL
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Moisture
94.7
%
0.010
1
01/26/2216:41
FMM
SW-DRYWT
Ammonia Nitrogen
2090
mg/Kg -
dry
302
1890
1
02/01/22 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<93.4
mg/Kg -
dry
93.4
93.4
1
02/01/22 14:46
ZBD
4500NO3F-2011
Organic N
12550
mg/Kg -
dry
301.9
1887
1
01/31/22 10:00
CALCULATION
pH
6.5
S.U.
1
01/31/2215:39
DRS
9045D
Total Solids
5.30
%
0.010
0.010
1
01/26/22 16:41
FMM
2540G-2011
Total Kjeldahl Nitrogen
14600
mg/Kg -
dry
189
4720
1
01/31/22 10:00
JPJ
;M-4500-NH3C-TKl`
Phosphorus
1580
mg/Kg -
dry
52.1
94.3
1
01/28/22 05:34
EAL
6010D
Aluminum
89100
mg/Kg -
dry
87.2
94.3
1
01/28/22 05:34
EAL
6010D
Arsenic
7.583
mg/Kg -
dry
4.53
9.43
1
01/28/22 05:34
EAL
6010D
Cadmium
<0.377
mg/Kg -
dry
0.377
1.89
1
01/28/22 05:34
EAL
6010D
Calcium
1690
mg/Kg -
dry
730
943
1
01/28/22 05:34
EAL
6010D
Chromium
71.5
mg/Kg -
dry
4.45
4.72
1
01/28/22 05:34
EAL
6010D
Copper
37.2
mg/Kg -
dry
5.85
9.43
1
01/28/22 05:34
EAL
6010D
Iron
42300
mg/Kg -
dry
161
189
1
01/28/22 05:34
EAL
6010D
Lead
28.5
mg/Kg -
dry
3.40
5.66
1
01/28/22 05:34
EAL
6010D
Magnesium
3960
mg/Kg -
dry
48.7
94.3
1
01/28/22 05:34
EAL
6010D
Manganese
1000
mg/Kg -
dry
6.13
9.43
1
01/28/22 05:34
EAL
6010D
Mercury
<0.124
mg/Kg -
dry
0.124
0.285
1
01/26/22 17:15
JW2
7471A
Molybdenum
<2.55
mg/Kg -
dry
2.55
4.72
1
01/28/22 05:34
EAL
6010D
Nickel
28.1
mg/Kg -
dry
2.26
4.72
1
01/28/22 05:34
EAL
6010D
Potassium
2960
mg/Kg -
dry
117
189
1
01/28/22 21:48
EAL
6010D
Selenium
<6.04
mg/Kg -
dry
6.04
9.43
1
01/28/22 21:48
EAL
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 6 of 9
•
Waypoint
27090 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 ° Fax 901.213.2440
ANALYTICAL
www.waypointanalyiical.com
46245
EMA Resources Inc
Project
Mocksville, NC
Mr. Brent Collins
Report Date : 02/02/2022
755 Yadkinville Rd
Information :
Received : 01/25/2022
Mocksville , NC 27028
Danyale Love
Report Number : 22-025-0020
REPORT OFANALYSIS
Project Manager
Lab No : 91577
Matrix: Solids
Sample ID : Mocksville WTP
Sampled: 1/24/2022 9:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
2893
mg/Kg - dry
245
472 1 01/28/22 05:34 EAL 6010D
Zinc
86.4
mg/Kg - dry
15.3
23.6 1 01/28/22 05:34 EAL 6010D
Sulfur
1340
mg/Kg - dry
97.7
189 1 01/28/22 05:34 EAL 6010D
Sodium Absorption Ratio
0.203
Ratio
0.01
0.01 1 01/28/22 05:34 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 7 of 9
s
WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133
21.2440
Main 901.213.240fl °Fax 901.213.2440
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 22-025-0020
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T137
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IMakayla Weaver Date & Time: 01/25/2022 09:00:55
Page 8 of 9
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ace Analytical ' ANALYTICAL REPORT
February 07, 2022
EMA Resources
Sample Delivery Group: L1454554
Samples Received: 01/25/2022
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By: , �-
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
N
� T
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1454554 02/07/22 16:05 1 of 21
TABLE OF CONTENTS
Cp: Cover Page
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
MOCKSVILLE WTP L1454554-01
5
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
Wet Chemistry by Method D93/1010A
10
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
Volatile Organic Compounds (GC/MS) by Method 8260D
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
17
GI: Glossary of Terms
19
al: Accreditations & Locations
20
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
EMA Resources L1454554
02/07/22 16:05 2 of 21
MOCKSVILLE WTP L1454554-01 Waste
Method
Preparation by Method 1311
Preparation by Method 1311
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
Volatile Organic Compounds (GC/MS) by Method 8260D
Chlorinated Acid Herbicides (GC) by Method 8151A
Pesticides (GC) by Method 8081B
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
SAMPLE SUMMARY
Collected by
Brent Collins
Batch
WG1808840
WG1809554
WG1808566
WG1809680
WG1808419
WG1812928
WG1810317
WG1810384
WG1810127
WG1811223
WG1809205
WG1809535
Collected date/time Received date/time
01/24/22 09:00 01/25/22 09:15 C
P
Dilution Preparation
Analysis
date/time
date/time
1 01/27/2210:39
01/27/2210:39
1 01/28/2212:49
01/28/2212:49
1 01/30/221127
02/01/2214:39
1 01/31/2216:00
02/01/22 22:00
1 01/26/2214:00
01/27/22 09:00
1 02/04/22 0108
02/04/22 0108
1 01/30/22 09:32
01/31/22 09:41
1 02/01/22 00:24
02/01/22 23:50
1 01/29/2216:27
01/29/2216:27
1 02/02/22 08:09
02/03/221159
1 02/03/22 06:33
02/03/2215:56
1 01/30/2216:30
01/31/22 06:11
Analyst
JWS
CJ W
LDT
SAC
GI
WOS
MRW
CCE
JAH
AO
AO
JNJ
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
Rc
Mt. Juliet, TN
Mt. Juliet, TN
GI
F
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1454554 02/07/22 16:05 3 of 21
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the FP
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data. 0
Fr
Rc
GI
Justin Carr [Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1454554 02/07/22 16:05 4 of 21
SAMPLE RESULTS - 01
L1454554
MOCKSVILLE WTP
Collected date/time: 01/24/22 09:00
Preparation by Method 1311
Result Qualifier Prep
Batch
Analyte
date / time
TCLP Extraction
1/27/202210:39:54 AM
WG1808840
TCLP ZHE Extraction
- 1/28/202212:49:36 PM
WG1809554
Fluid
1 1/27/202210:39:54AM
WG1808840
Initial pH
6.60 1/27/202210:39:54AM
WG1808840
Final pH
4.98 1/27/202210:39:54 AM
WG1808840
Wet Chemistry by Method 9012 B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Cyanide ND 0.250
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Sulfide ND 25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 02/01/202214:39 WG1808566
Dilution Analysis Batch
date / time
1 02/01/2022 22:00 WG1809680
Result Qualifier Dilution Analysis Batch
Analyte su date / time
Corrosivity by pH 6.64 T8 1 01/27/2022 09:00 WG1808419
Sample Narrative:
L1454554-01 WG1808419: 6.64 at18C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at200
Mercury by Method 7470A
Qualifier Dilution Analysis Batch
date / time
1 02/04/2022 0108 WG1812928
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
ND
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.0500
0.50
Carbon tetrachloride
ND
0.0500
0.50
Chlorobenzene
ND
0.0500
100
Chloroform
ND
0.250
6
ACCOUNT:
PROJECT:
EMA Resources
Dilution Analysis Batch
date / time
1 01/31/2022 09:41 WG1810317
Dilution Analysis
Batch
date / time
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
1 02/01/2022 23:50
WG1810384
Dilution Analysis
Batch
date / time
1 01/29/202216:27
WG1810127
1 01/29/202216:27
WG1810127
1 01/29/202216:27
WG1810127
1 01/29/202216:27
WG1810127
SDG:
DATE/TIME: PAGE:
L1454554
02/07/22 16:05 5 of 21
MOCKSVILLE WTP
SAMPLE RESULTS
- 01
Collected date/time: 01/24/22 09:00
L1454554
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL Limit Dilution
Analysis
Analyte
mg/I
mg/I mg/I
date/time
1,2-Dichloroethane
ND
0.0500 0.50 1
01/29/202216:27
1,1-Dichloroethene
ND
0.0500 0.70 1
01/29/202216:27
2-Butanone (MEK)
ND
0.500 200 1
01/29/202216:27
Tetrachloroethene
ND
0.0500 0.70 1
01/29/202216:27
Trichloroethene
ND
0.0500 0.50 1
01/29/202216:27
Vinyl chloride
ND
0.0500 0.20 1
01/29/202216:27
(S) Toluene-dH
93.6
80.0-120
011291202216.27
(S) 4-Bromofluorobenzene
102
77.0-126
011291202216.27
(S) 1,2-Dichloroethane-d4
90.6
70.0-130
011291202216.27
Chlorinated Acid Herbicides (GC)
by Method 8151A
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S) Z4-Dichlorophenyl Acetic Acid 77.H
Pesticides (GC) by Method 8081B
Batch
WG1810127
WG1810127
WG1810127
WG1810127
WG1810127
WG1810127
WG1810127
WG1810127
WG1810127
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
date / time
0.00200
1
1 02/03/20221159
WG1811223
0.00200
10
1 02/03/20221159
WG1811223
14.0-158
021031202211.59
WG1811223
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Chlordane
ND
0.00500
0.03
Endrin
ND
0.00500
0.02
Heptachlor
ND
0.00500
0.0080
Heptachlor epoxide
ND
0.00500
0.0080
Lindane
ND
0.00500
0.40
Methoxychlor
ND
0.00500
10
Toxaphene
ND
0.0100
0.50
(S) Decochlorobiphenyl
93.8
10.0-128
(S) Tetrochloro-m-xylene
93.0
10.0-127
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Analyte
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-Fluorobiphenyl
(S) Z4, 6-Tribromophenol
(S) p-Terphenyl-d14
ACCOUNT:
EMA Resources
Dilution Analysis
date / time
1 02/03/2022 15:56
1 02/03/2022 15:56
1 02/03/2022 15:56
1 02/03/2022 15:56
1 02/03/2022 15:56
1 02/03/2022 15:56
1 02/03/2022 15:56
0210312022 15.56
0210312022 15.56
Batch
WG1809205
WG1809205
WG1809205
WG1809205
WG1809205
WG1809205
WG1809205
WG1809205
WG1809205
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
mg/I
mg/I
mg/I
date/time
ND
0.100
7.50
1 01/31/2022 0611
WG1809535
ND
0.100
0.13
1 01/31/2022 06:11
WG1809535
ND
0.100
0.13
1 01/31/2022 06:11
WG1809535
ND
0.100
0.50
1 01/31/2022 06:11
WG1809535
ND
0.100
3
1 01/31/2022 06:11
WG1809535
ND
0.100
2
1 01/31/2022 06:11
WG1809535
ND
0.100
5
1 01/31/2022 06:11
WG1809535
ND
0.100
400
1 01/31/2022 06:11
WG1809535
ND
0.100
200
1 01/31/2022 06:11
WG1809535
ND
0.100
100
1 01/31/2022 06:11
WG1809535
ND
0.100
400
1 01/31/2022 06:11
WG1809535
ND
0.100
2
1 01/31/2022 06:11
WG1809535
52.0
10.0-120
0113112022 06.11
WG1809535
31.0
10.0-120
0113112022 06.11
WG1809535
78.0
10.0-127
0113112022 06.11
WG1809535
72.3
10.0-130
0113112022 06.11
WG1809535
74.0
10.0-155
0113112022 06.11
WG1809535
85.9
10.0-128
0113112022 06.11
WG1809535
PROJECT:
SDG:
DATE/TIME: PAGE:
L1454554
02/07/22 16:05 6 of 21
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
Fn
RDL
Reported Detection Limit.
Rec.
Recovery.
Fr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
F
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
F
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Rc
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix interfered with the ability to make any accurate determination, spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1454554 02/07/22 16:05 19 of 21
ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1454554 02/07/22 16:05
PAGE:
20 of 21
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4b) Residuals Information Sheet
Residuals Information Sheet
Generator: Town of Mocksville-WTP
Facility:
Mocksville WTP
Address:
771 Sanford Rd
Mocksville, NC 27028
Phone:
336-751-2635
Contact:
Justin Turbyfill
Land Application Contractor: EMA Resources Inc.
755 Yadkinville Rd
Mocksville, NC 27028
Phone: 336-751-1441
Contact: Brent Collins
Please Note: The application of these residuals is only allowed in accordance with subject permit.
(WQ0039552)
All applicable setbacks in accordance with 15A NCAC 02T .1108(b) will be adhered and is the
responsibility of the land application contractor.
Application rates shall be applied at agronomic rates for intended uses.
No residuals shall be applied to any site that is flooded, frozen, or snow covered.
Adequate procedures will be implemented to prevent surface runoff of residuals in any surface waters.
The attached residuals analysis report is a summary of major and micro -nutrients available in the
residuals.
If you have any questions concerning this information, you may contact EMA Resources Inc, at the
number listed above.
5) Operation & Maintenance Plan
Standard Operating Procedure and Operation
and Maintenance Plan for the Town of Mocksville
WTP- Land Application Program
1. Purpose
a. Ensure the requirements of the Town of Mocksville, NC Non -Discharge
Perm it#WQ0039552 are met.
2. Personnel
a. The following is a list of personnel in order they are to be contacted when
information needs to be shared.
i. EMA Resources inc.
1. Jeff Thompson — Project Manager 336-477-4078
2. Roy Whitaker — Director of Bus.Dvlpmt./Ops. 336-909-1718
3. Brent Collins — Director of Technical Services 336-399-3646
ii. Town of Mocksville, NC
1. Ken Gamble — Town Manager 336-753-6701
2. Justin Turbyfill — WTP-ORC 336-751-2635 (EnviroLink)
3. Operational Functions
a. The operational function of this project it going to involves transporting the
thickened liquid residuals via tanker trailers to a staging area in the receiver
sites. The liquid residuals will be off-loaded into tractor/pull tank spreader
or pumper truck and land applied in a uniform application. It is going to be
spread at agronomic rates that are determined using the Realistic Yield
Expectations (RYE) as outlined in the permit, the amount of other nutrient
sources the landowner and operator has applied, and the residuals nutrient
and metal sample that is current for that monitoring period. The material is
going to be land applied on fields that have a crop growing on them that
are going to either be grazed or cut for animal feed or row crops for feed
or fiber. Application rates will be reduced by 25% on fields that are primarily
used for grazing in accordance with USDA-NRCS 590. Grazed fields will be
determined by the farmers and EMA project managers.
4. Maintenance Schedule
a. EMA Resources Inc. will follow the maintenance schedule as recommended
by the EMA Resources EHS&T Director for the equipment necessary to
complete the job.
S. Safety Measures
a. The Town of Mocksville and EMA Resources Inc. believe in operating in a
safety conscious manner and all employees participate in safety training that
is designed to help employees recognize safety issues and take steps to
prevent accidents from occurring. In addition, EMA Resources employees
have the authority to stop operations if they think any aspect of the
operation is going to cause environmental or personal harm.
6. Spill Response Plan
a. In the unlikely event of a spill, the following action shall be taken
immediately.
i. Management of Spill Clean-up Activities: The EMA Resources
Project Manager shall take immediate charge and initiate clean-up
activities. EMA Resources labor and equipment is to be utilized. In
the event additional labor and equipment is required, assistance may
be requested from the Town of Mocksville, The NC Department of
Transportation, and other private contractors as necessary.
ii. Halt the Source of the Spill: Such as a ruptured container or
damaged transport unit.
iii. Contain the Spill: Form a barrier. Sufficient quantities of straw shall
be used for such purposes. Earthen barriers may be constructed to
augment the straw bale containment area of the spill. The
Operations Manager or the person in charge on the spill site will be
advise the clean-up personnel where to get the straw, lime, and other
items necessary to complete the clean-up operation. ie. local farmers,
farm supply centers, nurseries.
iv. Initial Clean -Up: Employ front-end loaders, vacuum equipment,
sludge application vehicles, and/or local septic tank service to
remove as much of the spilled material as possible. Straw and/or
sand should be scattered in the spill area to soak up the remaining
material. The straw and sand soaked material will be collected and
removed to a disposal area approved by representatives of the state
regulatory agency.
v. Final Clean-up: Employ rotary brush sweeper if needed and apply
lime to the spill area upon the approval of the clean-up efforts by the
state regulatory representative. If the event occurs on private
property, the clean-up will be completed to the satisfactory of the
property owner and state regulatory representatives. The ultimate
goal will be restore the spill area to its original condition if possible.
vi. Notification: As soon as possible after the spill occurs, the EMA
Resources Project Manager or designee will notify the Town of
Mocksville and the EMA Resources main office. EMA Resources
office staff is then responsible for notifying other key EMA Resources
personnel.
vii. Reporting_ EMA Resources staff will notify the Winston-Salem
regional office of the NCDENR by telephone (336) 776-9800 as soon
as possible, but not more than 24 hours after, or on the next working
day following the occurrence. The EMA Project Manager shall
provide a written report with 48 hours of the spill to the EMA
Resources Director of Technical Services and the Town of Mocksville
staff. The report shall list all relative information and actions taken.
With the assistance of EMA Resources personnel, and the Town of
Mocksville personnel, a written report will be filed with the Winston-
Salem regional office within 5 days of the occurrence. For after-hours
reporting, the Division's emergency number shall be called to report
all incidences (800) 662-7956.
7. Inspection Plan
a. Inspection for the land application of residuals will conducted on a
minimum of a weekly basis at the land application site during land
application activities. The inspection frequency is based on the time frame
that it is going to take to complete the project and the amount of dry tons
to be land applied from this facility. The inspections will consist of
inspecting a current field that is being applied as well as inspecting random
fields that have been completed. Inspections will be conducted by Jeff
Thompson — Project Manager. These inspections will consist of the
following:
i. Verifying the application rates for each field that plan on receiving
material.
ii. Checking the calculated loads to ensure the correct amount of
residuals are being land applied.
iii. Ensure that all manned equipment has a copy of the permit and the
operation and maintenance plan.
iv. Ensure that the field has been flagged properly and that all buffers
are being adhered to.
v. Ensure proper signage has been posted
vi. Verify that the proper number of samples of the residuals have been
taken and that it meets the criteria for land application.
vii. The records will be kept in the EMA Resources project files in the
main office. Copies of all analyses and records will be forwarded to
the Town of Hillsborough and kept on file.
viii. EMA Resources and the Town of Mocksville staff will immediately
inform the other party if any of the following conditions are noted.
1. Any occurrence with the distribution program resulting in the
land application of significant amounts of material that is
abnormal in quantity or characteristics.
2. Any failure of the distribution system that results in the release
to surface waters.
3. Any time that self -monitoring indicates that the facility has
gone out of compliance with the permit.
4. Any process failure that results in the system not adequately
treating the residuals.
5. Any spill or discharge from a vehicle or piping system during
residuals transportation.
6. Any release that requires immediate reporting outside normal
business hours shall be called in by EMA Resources staff to
DENR at (800) 662-7956. This number is to be called in the
event of a release to surface waters or imminent failure of a
storage system when the event occurs outside of normal
business hours.
8. Sampling and Monitoring Plan
a. Sampling for this project consists of sampling the residuals prior to land
application occurring in order to ensure that the residuals are suitable for
land application.
b. The samples will be collected from the two storage tanks that holds the
thickened residuals
c. Roy Whitaker, Brent Collins, or other designee will be responsible for sample
collection for nutrient and metal and TCLP.
d. Nutrient, metal and TCLP sample aliquots will be collected randomly and
consist of at least 7 individual aliquots mixed together in order to get the
composite sample for these parameters.
e. The residuals will be sampled annually for TCLP including the RClls.
f. Metal and nutrient parameters will be collected and analyzed based on the
requested dry ton numbers in the permit application.
9. Environmental Impacts
a. The environmental impacts for residuals may be affected by this procedure.
b. This procedure helps assure that land application is conducted in a safe and
efficient manner while ensuring compliance with the laws and regulations
and to minimize exposure, negative environmental impacts and public
relation concerns.