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HomeMy WebLinkAboutWQ0039552_Renewal Application_20220331Initial Review Reviewer Thornburg, Nathaniel D Is this submittal an application? (Excluding additional information.)* Yes No Permit Number (IR) * WQ0039552 Applicant/Permittee Town of Mocksville Applicant/Permittee Address 171 Clement Street, MoCksville, NC 27028 Is the owner in BIMS? Yes No Is the facility in BIMS? Owner Type Facility Name County Fee Category Minor Is this a complete application?* Yes No Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Municipal Town of Mocksville Class A Residuals Program Davie Does this need review by the hydrogeologist? * Yes No Regional Office CO Reviewer Admin Reviewer Yes No Fee Amount $0 Complete App Date 03/31/2022 Below list any additional email address that need notification about a new project. ... ... .. Email Address Comments to be added to email notfication Comments for Admin Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. ............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................ Name* Brent Collins Email Address* brent.collins@emaresourcesinc.com Project Information Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 336-399-3646 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type: * Wastewater Irrigation Other Wastewater Closed -Loop Recycle Single -Family Residence Wastewater Irrigation Permit Number: * WQ0039552 Has Current Existing permit number Applicant/Permittee* Town of Mocksville Applicant/Permittee Address* 171 Clement Street, Mocksville, NC 27028 Facility Name* Town of Mocksville Class A Residuals Program Please provide comments/notes on your current submittal below. High -Rate Infiltration Reclaimed Water Residuals Other At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) Town of Mocksville WTP - Permit Renewal - 9.44MB WQ0039552.pdf Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 3/30/2022 g Inc. Permit Renewal Application For the Town of Mocksville WTP WQ0039552 Distribution of Class A Water Treatment Plant Residuals Prepared By: EMA Resources Inc. 755 Yadkinville Road Mocksville, NC 27028 336-751-1441 March 30, 2022 Division of Water Resources Water Quality Permitting Section Non -Discharge Permitting Unit 1617 Mail Services Center Raleigh, NC 27699-1617 RE: Permit Modification — WQ0039552 To Whom it May Concern: EMA Resources is submitting the included permit renewal for Town of Mocksville's WTP Land Application Permit - WQ0039552. There are no modifications to the process or the permit included. If you have any questions concerning this renewal, please contact Brent Collins — Director of Technical Services Respectfully, Brent Collins Director of Technical Services brent.collinsgemaresourcesinc.com (336) 399-3646 Phone 336975191441 — Fax 336975191442 755 Yadkinville Rd — Mocksville, NC 27028 Table of Contents 1) DCAR Form a) Current Permit 2) Program Information 3) RSC Form a) Vicinity Map b) Process Flow Diagram & Process Summary c) Quantitative Justification 4) Residuals Quality Information a) Laboratory Analytical Reports b) Residuals Information Sheet 5) Operation & Maintenance Plan 1) DCAR Form State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS FORM: DCAR 06-16 L APPLICANT INFORMATION: 1. Applicant's name: Town of Mocksville WTP Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership Privately -Owned Public Utility FLI Federal ❑ State ® Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Ken Gamble Title: Town Manager Applicant's mailing address: 171 Clement Street City: Mocksville State: NC Zip: 27028- Vp Telephone number: (336) 753-6701 Email Address: kgamble&mocksvillenc.gov 2. Consultant's name: Brent Collins License Number (for P.E.): Affiliation: ❑ On Staff ® Retained (Firm: EMA Resources Inc.) Consultant's mailing address: 755 Yadkinville Rd City: Mocksville State: NC Zip: 27028- Telephone number: (336) 399-3646 Email Address: brent.collinsA_emaresourcesinc.com 3. Fee submitted: $0 (See Instruction B) IL PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00039552 Date of most -recently issued permit: 11/17/2017 Date of most -recently certified Attachment A (if different than the permit): 11/17/2017 III. FACILITY INFORMATION: 1. Name of residuals processing facility: Town of Mocksville WTP City: Mocksville State: NC Zip: 27028-_ Coordinates: Latitude: 35' 53' 22" Longitude: 80. 34' 43" Datum: NAD83 Level of accuracy: Nearest Second Method of measurement: GPS County where facility is located: Davie 2. Facility contact (person familiar with residuals preparation): Name: Justin Turbyfill Title: ORC Mailing address: 771 Sanford Avenue City: Mocksville State: NC Telephone number: 3( 36) 751-2635 Zip: 27028- E-mail address: mocksville cgenvirolink.com FORM: DCAR 06-16 Page 1 of 3 3. Is the residual process facility also the generator? ® Yes; ❑ No If No, please specify delivery frequency and quantity of residual to be processed: 4. Length of residuals storage at facility: 365 days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: 1. Specify how these residuals will be distributed: ❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk); ® other (explain); Bulk liquid land application at agronomic rates Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: Type of Materials Amounts to be added Der 1.0 dry ton of residuals (dry ton) 3. Approximate amounts of the residuals received and processed at the facility: 188 dry tons per year. 4. Approximate amounts of the final product (processed residuals) to be distributed: 188 dry tons per year. 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): Two — 275,000 gallon residuals storage tanks equipped with floating decanter. The residuals will be removed annually for a maximum of 365 days of storage prior to distribution 6. Does the facility have a stormwater management plan? ❑ Yes; ® No Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: N/A V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals Source Certification and all associated documentation. e RSC 06-16.doc FORM: DCAR 06-16 Page 2 of 3 Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units) attest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engineer's Seal, Signature, and Date: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. ® Yes U No, Explain; I, Ken Gamble Town Manager (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for Town of Mocksville - WTP (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: Date: FORM: DCAR 06-16 Page 3 of 3 la) Current Permit Water Resources ENVIRONMENTAL QUALITY November 17, 2017 MARcus A. ABERNETHY — TOWN MANAGER TOWN OF MOCKSVILLE 171 CLEMENT STREET MOCKSVI LLE, NORTH CAROUNA 27028 Dear Mr. Abernethy: ROY COOPER Governor MICHAEL S. REGAN Secretary LINDA CULPEPPER Interim Director Subject: Permit No. WQ0039552 Town of Mocksville DCAR Distribution of Class A Water Treatment Plant Residuals Davie County In accordance with your permit application request received October 19, 2017, we are forwarding herewith Permit No. WQ0039552 dated November 17, 2017, to the Town of Mocksville for the operation of the subject residuals management program. This permit shall be effective from the date of issuance until October 31, 2022, and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring requirements listed in Attachment A. Failure to establish an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee has the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding. If you need additional information concerning this permit, please contact Troy Doby at (919) 807- 6336 or trgy.dohygnedetir.gov. Sincerely, ,L,mda Culpepper, Interim Directo a Division of Water Resources cc: Davie County Health Department (Electronic Copy) Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy) Roy L. Whitaker -- EMA Resources, Inc. (Electronic Copy) Digital Permit Archive (Electronic Copy) Central Files <'7 "Nothing Cornpares'�-, State of North Carolina I Environmental Quality I Water Resources I Water Quality Permitting I Non -Discharge Permitting 1617 Mail Service Center G Raleigh, North Carolina 27699-1617 919-807-6332 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENTAL QUALITY RALEIGH DISTRIBUTION OF CLASS A WATER TREATMENT PLANT RESIDUALS PERMIT In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO Town of Mocksville Davie County FOR THE operation of a residuals management program for Town of Mocksville and consisting of the distribution of Class A water treatment plant residuals generated by the approved facility listed in Attachment A with no discharge of wastes to surface waters, pursuant to the application received October 19, 2017, and in conformity with other supporting data subsequently filed and approved by the Department of Environmental Quality and considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 257. This permit does not exempt the Permittee from complying with the federal regulations. This permit shall be effective from the date of issuance until October 31, 2022, and shall be subject to the following specified conditions and limitations: I. SCHEDULES 1. No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application. [ 15A NCAC 02T .0108(b)(2), 02T .0105(d), 02T .0109] H. PERFORMANCE STANDARDS 1. The subject residuals management program shall be effectively maintained and operated at all times so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards. In the event the facilities fail to perform satisfactorily, including the creation of prolonged nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease distribution of residuals, contact the Winston-Salem Regional Office supervisor, and take any immediate corrective actions. [G.S. 143-215.11 2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. [I 5A NCAC 02B .0200, 02L .0100] WQ0039552 Version 1.0 Shell Version 171103 Page 1 of 10 3. Only residuals generated by the facility listed in Attachment A are approved for distribution in accordance with this permit. [G.S. 143-215.1] 4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis): Parameter Ceiling Concentration (milligrams per kilogram) Monthly Average Concentration (milligrams per kilogram) Arsenic 75 41 Cadmium 85 39 Copper 4,300 HI 1,500 Lead 840 300 Mercury 57 17 Molybdenum 75 n/a Nickel 420 420 Selenium 100 100 Zinc 7,500 2,800 [15A NCAC 02T. 1105] 5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b)(2). Exceptions to this requirement shall be specified in Attachment A. [15A NCAC 02T .1106] 6. Setbacks for treatment and storage facilities shall be as follows: Setback Description Setback feet Habitable residence or place of public assembly under separate ownership or not to be maintained as part of the project site 100 Property lines 50 Private or public water supply 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and wetlands 50 Wells with exception to monitoring wells 100 [ 15A NCAC 02T. 11081 WQ0039552 Version 1.0 Shell Version 171103 Page 2 of 10 7. Setbacks for Class A land applied bulk residuals shall be as follows: Setback by residual type Setback Description (feet) Liquid Cake' Private or public water supply 100 100 Surface waters (streams — intermittent and perennial, 100 25 perennial waterbodies, and wetlands Surface water diversions (ephemeral streams, 25 0 waterways, ditches Groundwater lowering ditches (where the bottom of 25 0 the ditch intersects the SHWT Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 ' Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15% solids by weight and can be stacked without flowing, as well as can be handled, transported and spread as a solid (e.g., using a backhoe, front end loader, slinger spreader, broadcast spreader or other equipment designed for handling solid materials) without leaving any significant liquid fraction behind. [ 15A NCAC 02T .11081 8. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre -approved site specific historical data for specific crop or soil types by calculating the mean of the best three yields of the last five consecutive crop harvests for each field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science h :/./nutrients.soil.ncsu.edu/yields/indg&.Vhp). A copy shall be kept on file and reprinted every five years in accordance with Condition IV.6. c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE and appropriate nutrient application rates reported in any of the following documents: i. Crop management plan as outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services; the Natural Resource Conservation Service, or other agronomist. ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance Document: Chapter 1 (bgp://www.ncaar.i4ov/SWC/tech/documents/9th Guidance_ Doc_ 100109.pdf). iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management Standards(ftp://ftp-fc.sc.egov.usda.gov/NHQ/practice-standards/standards/590.pdf). d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall contact the Division to determine necessary action. [15A NCAC 02T .1109(b)(1)(k)] WQ0039552 Version 1.0 Shell Version 171103 Page 3 of 10 9. The Permittee shall not distribute Class A water treatment plant residuals that have a sodium adsorption ratio (SAR) of 10 or higher without prior written Division approval. The Permittee may seek approval by demonstrating that the entity accepting the residuals is: aware of the effects of a high SAR content; has agreed on proper residual application rates; and has agreed to operational considerations to ensure that the high SAR content will not adversely impact the receiving sites. Recommendations regarding sodium application rate, soil amendments (e.g., gypsum, etc.) or a mechanism for maintaining site integrity and conditions conducive to crop growth, can be obtained from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist. [15A NCAC 02T A 108(b)(1)] M. OPERATION AND MAINTENANCE REQUIREMENTS The residuals management program shall be properly maintained and operated at all times. The program shall be effectively maintained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. [15A NCAC 02T .1110] 2. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan, at the minimum, shall include: a. Operational functions; b. Maintenance schedules; c. Safety measures; d. Spill response plan; e. Inspection plan including the following information: i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record beeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f. Sampling and monitoring plan including the following information: i. Names and/or titles of personnel responsible for conducting the sampling and monitoring; ii. Detailed description of monitoring procedures including parameters to be monitored; iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen reduction requirements (e.g. facilities that distribute multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). [15A NCAC 02T .1100] WQ0039552 Version 1.0 Shell Version 171103 Page 4 of 10 3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification of the facility, the Permittee shall designate and employ a certified operator in responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC 08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204, or as specified in the most recently approved O&M plan (i.e., see Condition 111.2.), and shall comply with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and designation requirements, please contact the Division of Water Resources' Protection and Enforcement Branch at (919) 707-9105. At the time of this permit issuance, a certified ORC is not required for the subject Distribution of Class A Residuals program. [15A NCAC 02T .0117] 4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be maintained at the land application sites during land application activities. [15A NCAC 02T .0108(b)(1)] 5. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be maintained in all residuals transport and application vehicles. [15A NCAC 02T .I 110] b. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into surface waters. [G.S. 143-215.11 7. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land application sites onto which residuals are applied, or application shall be in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved by the Division. [15A NCAC 02T .1109(b)(1)] 8. Bulk residuals shall not be land applied under the following conditions: a. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. If the application causes prolonged nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards; d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur; e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following a residuals land application event; f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than 18% for injected or incorporated bulk liquid residuals; h. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a USDA no -till program shall be exempted from meeting this vegetative cover requirement; i. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot; j. If the vertical separation of bedrock and the depth of residuals application is less than one foot; k. Application exceeds agronomic rates. [I5A NCAC 02T. 1109] WQ0039552 Version 1.0 Shell Version 171103 Page 5 of 10 9. The Permittee shall notify all third -party entities receiving bulk distributed Class A water treatment plant residuals that land application activities occurring on the third -parry's property shall meet the requirements in 15A NCAC 02T .1108(b)(1) and 02T .1109(b) (i.e., Conditions 11.8. and III.8., respectively). [15A NCAC 02T .1103(5)] 10. All residuals shall be adequately stored to prevent untreated leachate runoff. The finished product may be placed on a concrete pad, placed under shelter or physically covered until it is distributed to a third - parry entity. If bulk residuals are to be applied, the residuals may be staged at the application site for up to 30 days for biological residuals, and 60 days for non -biological residuals. If an alternate storage site is used, approval must be obtained from the Division. [15A NCAC 02T .0108(b)(1)] 11. A label shall be affixed to the bag or other container in which residuals are sold or given away for land application, or an information sheet shall be provided to the person who receives Class A residuals. At a minimum, the label or information sheet shall contain the following: a. The name and address of the person who prepared the residuals; b. A statement that residual land application is prohibited except in accordance with the instructions on the label or information sheet; c. A statement identifying that this material shall be prevented from entering any public or private water supply source (including wells) and any surface water (e.g., stream, lake, river, wetland, etc.); d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its intended use. [I5A NCAC 02T. I 109(a)] 12. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals contrary to the conditions of this permit. The Permittee shall report to the Winston-Salem Regional Office as per reporting conditions under Condition IV.8. any person or entity known to be applying residuals contrary to the condition of this permit. [15A NCAC 02T .I 103(a)] WQ0039552 Version 1.0 Shell Version 171103 Page 6 of 10 W. MONITORING AND REPORTING REOUIREMENTS 1. Any Division -required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established, and an acceptable sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)] 2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be used or disposed under this permit. The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of five years. Any exceptions from the requirements in this condition shall be specified in Attachment A. The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1, 1 -Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene {100.0) Heptachlor (and its hydroxide) 0 008 Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200,0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) Once the residuals have been monitored for two years at the frequency specified in Attachment A, the Permittee may submit a permit modification request to reduce the frequency of this monitoring requirement. In no case shall the monitoring frequency be less than once per permit cycle. [15ANCAC 13A .0102(b), 02T .1101, 02T .1105] WQ0039552 Version 1.0 Shell Version 171103 Page 7 of 10 3. An analysis shall be conducted on the residuals from each source generating facility at the frequency specified in Attachment A, and the Permiee shall maintain the results for a minimum of five years. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) [15A NCAC 02T. I 10 1] 4. Residuals shall be monitored for compliance with pathogen reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b)(2) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. [15A NCAC 02T .1106, 02T .1107, 02T .1111(c)] 5. Laboratory parameter analyses shall be performed on the residuals as they are distributed, and shall be in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B .05051 6. The Permiee shall maintain records tracking all bulk residual distribution or land application events performed by the Permiee. At a minimum, these records shall include the following; a. Source of residuals; b. Date of distribution/land application; c. Name and address of recipient of residuals; d. Volume of residuals distributed to each recipient; e. Intended use of residuals; £ If land application events performed by the Permiee - Nitrogen Application Rate based on RYLs (if using data obtained from the North Carolina State University Department of Soil Science Website, the printout page shall be kept on file and reprinted every five years). [15A NCAC 02T .0108(a)] 7. Three copies of an annual report shall be submitted on or before March 1". The annual report shall meet the requirements described in the Instructions for Residuals Application Annual ReportingForms. orms. Instructions for reporting and annual report forms are available at http://deq.ne.gov/about/divisions/water-resources/water-resources-permits/wastewater-branch/non- discharge-permittin -ug nit/reportin -fg orms. or can be obtained by contacting the Non -Discharge Permitting Unit directly. The annual report shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 WQ0039552 Version 1.0 Shell Version 171103 Page 8 of 10 [15A NCAC 02T .1111(a)] 8. Noncompliance Notification The Permittee shall report by telephone to the Winston-Salem Regional Office, telephone number (336) 776-9800, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Distribution of residuals abnormal in quantity or characteristic. b. Any failure of the distribution program resulting in a release of material to surface waters. c. Any time self -monitoring indicates the facility has gone out of compliance with its permit limitations. d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment. e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to betaken to ensure that the problem does not recur. [15A NCAC 02T .0105(1), 02T .0108(b)(1)] V. INSPECTIONS 1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan. [15A NCAC 02T .0108(b)] 2. Prior to each bulk residuals distribution event, the Permittee or his designee sball inspect the residuals storage, transport and distribution facilities to identify malfunctions, facility deterioration and operator errors that could result in discharges to the environment, a threat to human health or a public nuisance. The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. [15A NCAC 02T .0108(b)] 3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the distribution sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)] VI. GENERAL CONDITIONS 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to 143-215.6C, [G.S. 143-215.6A to 143-215.6C] 2. This permit shall become voidable if the residuals distribution events are not carried out in accordance with the conditions of this permit. [ 15A NCAC 02T .0110] 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation. [G.S. 143-215.1] WQ0039552 Version 1.0 Shell Version 171103 Page 9 of 10 4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes, rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCGO 10000; any requirements pertaining to wetlands under 15A NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. [15A NCAC 02T .0105(c)(6)] In the event the residuals program changes ownership or the Permittee changes his name, a formal permit modification request shall be submitted to the Division. This request shall be made on official Division forms, and shall include appropriate documentation from the parties involved and other supporting documentation as necessary. The Permittee of record shall remain fully responsible for maintaining and operating the residuals program permitted herein until a permit is issued to the new owner. [15A NCAC 02T .0104] 6. This permit is subject to revocation or unilateral modification upon 60-day notice from the Division Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. [ 15A NCAC 02T .0110] 7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b). [15A NCAC 02T .0120] 8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T .0105(e)(3)] Permit issued this the 17' day of November 2017 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION Linda Culpepper, Interim Director Division of Water Resources By Authority of the Environmental Management Commission Permit Number WQ0039552 WQ0039552 Version 1.0 Shell Version 171103 Page 10 of 10 i. M Q i � Y � � o cYa a w id C b� •� ^� Q L Cd i r. R g d o ayyi C so d �y 'O CV ° Y•� a � O N O N 4cr d p b C 9 0� C � � � cd m E Cd j H L U O L O O W C Q O O T+ y c Qd = Cm u uce Q03 y O O C Q cm a a3i ° o. V tL E v El = e y cd u + 43 C O ,C t� °y a b C C d w u L O bA tg tw v A w a 2) Program Information Program Information 1. Provide a narrative explaining the following: a. How will the materials be handled and transported from where the residuals were produced? The water plant residuals are strictly sediment which has settled in the sedimentation basin and accumulated in the filters. The residuals are drawn off the bottom of the sedimentation basins on a daily basis and pumped to the storage tanks. The filter wash water is pumped to the storage tanks on a daily basis where any remaining residuals will settle. b. How will the residuals be processed/treated? The residuals are thickened via decanting of the water which is discharged via an NPDES permit. c. How will leachate collection be handled? There is no leachate in the system. The decant from the storage lagoon is discharged in accordance with the NDPES permit. d. Where will the residuals be stored until processing? The thickened residuals will be stored in one of two — 275,000 gallon storage/decant tanks e. How will the final product be distributed? The residuals will be delivered to local farmers via 6,500 gallon tankers. Each load will be off-loaded to a tractor pull tank spreader or pumper truck for application on a receiver site (grassland or row - crop) 2. Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. The residuals have limited major (N, P, K) nutrient value, but they have additional micro -nutrients that can be utilized by crops for optimum crop growth. The program will recruit local farmers to participate in the bulk land application program. They will be advised as to the limited nutrient value of the residuals, but they will be offered up to one ton of agricultural lime for soil pH adjustment where soil analysis indicated a need. 3. Provide either a label that shall be affixed to the bagged residuals or an information sheet that shall be provided to the person who receives the processed residuals. The label or information sheet shall contain, at a minimum, the following information. Residuals will be distributed through bulk land application of liquid, managed by the contracted land application firm. See attached information sheet. 3) RSC Form � o � a a 0 0 E-� A � a Fr � z O M z a o U Q C� z •V U � w O L O w � o � �U .: DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Mocksville WTP 2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private. Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Justin Turbyfill Complete mailing address: 771 Sanford Rd City: Mocksville State: NC Zip: 27028- Telephone number: (336) 751-2635 E-mail address: mocksvillegenvirolinkinc.com 4. Facility physical address: 771 Sanford Rd City: Mocksville State: NC Zip: 27028- Coordinates: Latitude: 35' 53' 22" Longitude: 80. 34' 43" Datum: NAD83 Level of accuracy: Nearest Second Method of measurement: GPS 5. Purpose of the facility: ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ® treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: __E % industrial and % domestic) ❑ other (explain: _ ). 6. Does the facility have an approved pretreatment program: ❑ Yes ® No 7. Facility permitted/design flow: 2 MGD and facility average daily flow: 0.9 MGD 8. Average amount of residuals being generated at this facility 188 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Two — 275,000 gallon residuals storage tanks equipped with floating decanter. Type and volume of residuals storage (i.e., outside of residuals treatment units): Same as above II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ❑ 40 CFR Part 503 or ® 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ❑ Biological ® Non -Biological FORM: RSC 06-16 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Pace Analytical and Date of analysis: 01/24/22 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: >200 OF (> 140°F) Passed reactivity test: W yes Ono. HCN: <0.250 mg/kg (<250) & H2S: <25 mg/kg (<500) TCLP Parameter Limit (mgfi) Result (mgfi) TCLP Parameter Limit (mgfi) Result (mgfi) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1,1-Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 01/24/22 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 7.58 Cadmium 85 39 <0.377 Copper 4,300 1,500 37.2 Lead 840 300 28.5 Mercury 57 17 <0.124 Molybdenum 75 n/a <2.55 Nickel 420 420 28.1 Selenium 100 100 <6.04 Zinc 7,500 2,800 86.4 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 5.3 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: 01/24/22 Parameter Result (mg/kg) Aluminum 89100 Ammonia -Nitrogen 2090 Calcium 1690 Magnesium 3960 Nitrate -Nitrite Nitrogen <93.4 pH (Standard Unit) 6.5 Phosphorus 1580 Potassium 2960 Sodium 289 Total Kjeldahl Nitrogen 14600 c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.20 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: - %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: The solids are considered raw undigested with regards to mineralization. e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1st) Year PAN Five -Year Maximum Adjusted PAN (mg/kg) (mg/kg) Surface 2390 3140 Injection/Incorporation 3435 4185 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(13)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T. 1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: ❑ Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, 9 air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.I107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. ® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 3a) Vicinity Map k ,t x { e r 1r 1 41 +.'S,F i` •,1'' � •'►. �� i � � � � i Y�. � � ' �y .� t ��� r b i � T R 7 +t4 'F � � i i�. + r1. a i 'M �•.t t J 1` 1 �•1r �� a F i ce. Mr \ • v, r �,► N ' A VIN wf ; , Yi„A 1Nk S o tip rSanford Avenue n i _ - r� • i yi j Y ��.# _ t",.J • 1. Source: Esri, M ar, GeoE�ye, E rths'tar Property Boundary USDA, USGS AeroGKv Iga, ndthe ■�■+ SCALE: ,.,%._,.,\ FIGURE NO. 1 "=440' �' EdIAMA Town of Mocksville -WTPDATE: 03.23.22 Land Application Program DRAWN BY: BC .Resources, Inc. 2 PROJECT NO: %A1nnn`zatiti0 Mocksville WTP 3b) Process Flow Diagram & Process Summary 2�AG mE%7 - - - EXISTING WASH WATER DRAIN x 1.0 MG EXISTING WATER x CLEARWELL TREATMENT PLANT x ❑ E80 x x�i x WTP x - I TO STATESVILLE LV i FLOW MONITOR - x - IARK N0, 2 C 9TANK N0. 1 / ' NEW GRAVEL ACCESS ROAD NEW FENCE --NEW 6" RJ DIP WATER LINE. SEE SHEET 2 SEE EXISTING 12" NOTE 3 TPVC WATER LINE V o� - _ EXISTING S" AC WATER LINE --�� CIEI I AREA PLAN w owm CAWjr GJW wK K AMA 5°' 0 50' 100, WINS ENGINEERS TOW WATEF ofnn JCS J N d O Oco V Ul w O1 b O m i Z Z 0 m �O b CL Z m w Q Z 0 a F J o 0 2 W z z LLI 3 X z 3 LJ :D J w J tiLLI v o Y 00000 o g w Q La o LJ c�i Z Z LL- o W O Q 0 LU LU Z z LU 00 0 0 .N o � 0 0 0 0 Z G3 m o V) 0 0 4L[0-3 ON 'OII ON - LLZBZ VNIIOHVO H1a0N 31L018VHO 3OVld S3NIS OOLOI 'ONI Sa33NION3 SIIIIM 3c) Quantitative Justification Mocksville WTP Quantitative Justification for Residuals Production Rate The Town of Mocksville WTP currently thickens the residuals in two — 275,000 gallon storage/decant tanks. The solids build up in the storage tank and need to be removed approximately every 2-3 years. The thickened residuals are pumped along with high pressure water to wash the basin. IDU,v vv x „ /,' , n/C7 I , Z5.34 x v.un = Dry lbs/ton Dry 375,300 - 2000 = 188 4a)Laboratory Analytical Reports Waypointo ANALYTICAL 2/2/2022 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 22-025-0020 Client Project Description: Mocksville, NC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 1/25/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. TNI Page 1 of 9 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2022 Florida State Program - NELAP E871157 06/30/2022 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2022 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2022 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2022 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2022 South Carolina State Program 84002 06/30/2022 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2022 Virginia State Program - NELAP 460181 09/14/2022 Page 1 of 1 00001/22-025-0020 Page 2 of 9 Waypoint ANALYTICAL Report Number: 22-025-0020 Client Project Description: Mocksville, NC Lab No Client Sample ID 91577 Mocksville V TP 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample Summary Table Matrix Date Collected Date Received Solids 01/24/2022 09:00 01/25/2022 Page 3 of 9 Waypointo ANALYTICAL Client: EMA Resources Inc Project: Mocksville, NC Lab Report Number: 22-025-0020 Date: 2/1 /2022 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 601 OD Sample 99187 Analyte: Aluminum QC Batch No: 1-596771/1-596454 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99187 Analyte: Calcium QC Batch No: 1-597088/1-596454 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99187 Analyte: Copper QC Batch No: 1-596771/1-596454 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99187 Analyte: Iron QC Batch No: 1-596771/1-596454 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99187 Analyte: Potassium QC Batch No: 1-597000/1-596454 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99187 Analyte: Magnesium QC Batch No: 1-597000/1-596454 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99187 Analyte: Manganese QC Batch No: 1-596771/1-596454 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99187 Page 4 of 9 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com Analyte: Phosphorus QC Batch No: 1-597000/1-596454 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99187 Analyte: Lead QC Batch No: 1-596771/1-596454 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99187 Analyte: Sulfur QC Batch No: 1-597000/1-596454 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 99187 Analyte: Zinc QC Batch No: 1-596771/1-596454 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 9 Waypointo ANALYTICAL 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number : 22-025-0020 Lab No : 91577 Sample ID : Mocksville WTP Project Mocksville, NC Information : 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com REPORT OFANALYSIS Report Date : 02/02/2022 Received : 01/25/2022 Danyale Love Project Manager Matrix: Solids Sampled: 1/24/2022 9:00 Test Results Units MDL MQL DF Date / Time Analyzed By Analytical Method Moisture 94.7 % 0.010 1 01/26/2216:41 FMM SW-DRYWT Ammonia Nitrogen 2090 mg/Kg - dry 302 1890 1 02/01/22 14:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N <93.4 mg/Kg - dry 93.4 93.4 1 02/01/22 14:46 ZBD 4500NO3F-2011 Organic N 12550 mg/Kg - dry 301.9 1887 1 01/31/22 10:00 CALCULATION pH 6.5 S.U. 1 01/31/2215:39 DRS 9045D Total Solids 5.30 % 0.010 0.010 1 01/26/22 16:41 FMM 2540G-2011 Total Kjeldahl Nitrogen 14600 mg/Kg - dry 189 4720 1 01/31/22 10:00 JPJ ;M-4500-NH3C-TKl` Phosphorus 1580 mg/Kg - dry 52.1 94.3 1 01/28/22 05:34 EAL 6010D Aluminum 89100 mg/Kg - dry 87.2 94.3 1 01/28/22 05:34 EAL 6010D Arsenic 7.583 mg/Kg - dry 4.53 9.43 1 01/28/22 05:34 EAL 6010D Cadmium <0.377 mg/Kg - dry 0.377 1.89 1 01/28/22 05:34 EAL 6010D Calcium 1690 mg/Kg - dry 730 943 1 01/28/22 05:34 EAL 6010D Chromium 71.5 mg/Kg - dry 4.45 4.72 1 01/28/22 05:34 EAL 6010D Copper 37.2 mg/Kg - dry 5.85 9.43 1 01/28/22 05:34 EAL 6010D Iron 42300 mg/Kg - dry 161 189 1 01/28/22 05:34 EAL 6010D Lead 28.5 mg/Kg - dry 3.40 5.66 1 01/28/22 05:34 EAL 6010D Magnesium 3960 mg/Kg - dry 48.7 94.3 1 01/28/22 05:34 EAL 6010D Manganese 1000 mg/Kg - dry 6.13 9.43 1 01/28/22 05:34 EAL 6010D Mercury <0.124 mg/Kg - dry 0.124 0.285 1 01/26/22 17:15 JW2 7471A Molybdenum <2.55 mg/Kg - dry 2.55 4.72 1 01/28/22 05:34 EAL 6010D Nickel 28.1 mg/Kg - dry 2.26 4.72 1 01/28/22 05:34 EAL 6010D Potassium 2960 mg/Kg - dry 117 189 1 01/28/22 21:48 EAL 6010D Selenium <6.04 mg/Kg - dry 6.04 9.43 1 01/28/22 21:48 EAL 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Page 6 of 9 • Waypoint 27090 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalyiical.com 46245 EMA Resources Inc Project Mocksville, NC Mr. Brent Collins Report Date : 02/02/2022 755 Yadkinville Rd Information : Received : 01/25/2022 Mocksville , NC 27028 Danyale Love Report Number : 22-025-0020 REPORT OFANALYSIS Project Manager Lab No : 91577 Matrix: Solids Sample ID : Mocksville WTP Sampled: 1/24/2022 9:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Sodium 2893 mg/Kg - dry 245 472 1 01/28/22 05:34 EAL 6010D Zinc 86.4 mg/Kg - dry 15.3 23.6 1 01/28/22 05:34 EAL 6010D Sulfur 1340 mg/Kg - dry 97.7 189 1 01/28/22 05:34 EAL 6010D Sodium Absorption Ratio 0.203 Ratio 0.01 0.01 1 01/28/22 05:34 CALCULATION Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit J Estimated value Page 7 of 9 s WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133 21.2440 Main 901.213.240fl °Fax 901.213.2440 N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 22-025-0020 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: T137 Shipping container/cooler uncompromised? * Yes 0 No Number of coolers/boxes received F-71 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: IMakayla Weaver Date & Time: 01/25/2022 09:00:55 Page 8 of 9 l rn LL a E E N n co ry \ N o o E U Z `2 =-ssNa� vemaM= ii Q LJ 7 V U x 2 2 2 2 S L/ Q 0 i r U on C2.�L1 I Lo z Z z z a a'�— DA T t yytvz ~ y m d d d 2 - _ a u ff u 121 J 7 VJ V N Ly ��,a ❑` 'l7 o m SInn ,� m E iz E E Hd t7 L N 5PHOS lelo1 m c 0 T aCIL c N oiuebAO/8leA!N m (D [ � ,o m ° C d a � PIUOW V/N>fl G � W � d o (0o1o9) 51e19W a z QU ur V t��1� C7 l7 z l'} r � a❑ Q6 a;ISodtuo{])3o geltE>j (Aa)i o; .Ja}atlf xis;eery c a E a - c sjauie;uo:) p jagwnti y V am a r V7 A Y � x a D v 0 r w Q a a` c a a a CL E E w J co ° U N (,] O 1.i •� O M < d' M T 0 N a+ r V 0i Q 7z pa Q P O [] C LC] Y v LijLn eaye y Ui y ace Analytical ' ANALYTICAL REPORT February 07, 2022 EMA Resources Sample Delivery Group: L1454554 Samples Received: 01/25/2022 Project Number: Description: Sludge Report To: Mr. Brent Collins 755 Yadkinville Road Mocksville, NC 27028 Entire Report Reviewed By: , �- Justin Carr Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. N � T ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1454554 02/07/22 16:05 1 of 21 TABLE OF CONTENTS Cp: Cover Page Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 MOCKSVILLE WTP L1454554-01 5 Qc: Quality Control Summary 7 Wet Chemistry by Method 9012 B 7 Wet Chemistry by Method 9034-9030B 8 Wet Chemistry by Method 9045D 9 Wet Chemistry by Method D93/1010A 10 Mercury by Method 7470A 11 Metals (ICP) by Method 6010D 12 Volatile Organic Compounds (GC/MS) by Method 8260D 13 Chlorinated Acid Herbicides (GC) by Method 8151A 15 Pesticides (GC) by Method 8081B 16 Semi Volatile Organic Compounds (GC/MS) by Method 8270E 17 GI: Glossary of Terms 19 al: Accreditations & Locations 20 Sc: Sample Chain of Custody 21 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1454554 02/07/22 16:05 2 of 21 MOCKSVILLE WTP L1454554-01 Waste Method Preparation by Method 1311 Preparation by Method 1311 Wet Chemistry by Method 9012 B Wet Chemistry by Method 9034-9030B Wet Chemistry by Method 9045D Wet Chemistry by Method D93/1010A Mercury by Method 7470A Metals (ICP) by Method 6010D Volatile Organic Compounds (GC/MS) by Method 8260D Chlorinated Acid Herbicides (GC) by Method 8151A Pesticides (GC) by Method 8081B Semi Volatile Organic Compounds (GC/MS) by Method 8270E SAMPLE SUMMARY Collected by Brent Collins Batch WG1808840 WG1809554 WG1808566 WG1809680 WG1808419 WG1812928 WG1810317 WG1810384 WG1810127 WG1811223 WG1809205 WG1809535 Collected date/time Received date/time 01/24/22 09:00 01/25/22 09:15 C P Dilution Preparation Analysis date/time date/time 1 01/27/2210:39 01/27/2210:39 1 01/28/2212:49 01/28/2212:49 1 01/30/221127 02/01/2214:39 1 01/31/2216:00 02/01/22 22:00 1 01/26/2214:00 01/27/22 09:00 1 02/04/22 0108 02/04/22 0108 1 01/30/22 09:32 01/31/22 09:41 1 02/01/22 00:24 02/01/22 23:50 1 01/29/2216:27 01/29/2216:27 1 02/02/22 08:09 02/03/221159 1 02/03/22 06:33 02/03/2215:56 1 01/30/2216:30 01/31/22 06:11 Analyst JWS CJ W LDT SAC GI WOS MRW CCE JAH AO AO JNJ Location FC Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Fn Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Fr Mt. Juliet, TN Mt. Juliet, TN Rc Mt. Juliet, TN Mt. Juliet, TN GI F RC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1454554 02/07/22 16:05 3 of 21 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the FP appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. 0 Fr Rc GI Justin Carr [Al Project Manager RC Project Narrative All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B. All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1454554 02/07/22 16:05 4 of 21 SAMPLE RESULTS - 01 L1454554 MOCKSVILLE WTP Collected date/time: 01/24/22 09:00 Preparation by Method 1311 Result Qualifier Prep Batch Analyte date / time TCLP Extraction 1/27/202210:39:54 AM WG1808840 TCLP ZHE Extraction - 1/28/202212:49:36 PM WG1809554 Fluid 1 1/27/202210:39:54AM WG1808840 Initial pH 6.60 1/27/202210:39:54AM WG1808840 Final pH 4.98 1/27/202210:39:54 AM WG1808840 Wet Chemistry by Method 9012 B Result Qualifier RDL Analyte mg/kg mg/kg Reactive Cyanide ND 0.250 Wet Chemistry by Method 9034-9030B Result Qualifier RDL Analyte mg/kg mg/kg Reactive Sulfide ND 25.0 Wet Chemistry by Method 9045D Dilution Analysis Batch date / time 1 02/01/202214:39 WG1808566 Dilution Analysis Batch date / time 1 02/01/2022 22:00 WG1809680 Result Qualifier Dilution Analysis Batch Analyte su date / time Corrosivity by pH 6.64 T8 1 01/27/2022 09:00 WG1808419 Sample Narrative: L1454554-01 WG1808419: 6.64 at18C Wet Chemistry by Method D93/1010A Result Analyte Deg. F Ignitability DNI at200 Mercury by Method 7470A Qualifier Dilution Analysis Batch date / time 1 02/04/2022 0108 WG1812928 Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Mercury ND 0.0100 0.20 Metals (ICP) by Method 6010D Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Arsenic ND 0.100 5 Barium ND 0.100 100 Cadmium ND 0.100 1 Chromium ND 0.100 5 Lead ND 0.100 5 Selenium ND 0.100 1 Silver ND 0.100 5 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Benzene ND 0.0500 0.50 Carbon tetrachloride ND 0.0500 0.50 Chlorobenzene ND 0.0500 100 Chloroform ND 0.250 6 ACCOUNT: PROJECT: EMA Resources Dilution Analysis Batch date / time 1 01/31/2022 09:41 WG1810317 Dilution Analysis Batch date / time 1 02/01/2022 23:50 WG1810384 1 02/01/2022 23:50 WG1810384 1 02/01/2022 23:50 WG1810384 1 02/01/2022 23:50 WG1810384 1 02/01/2022 23:50 WG1810384 1 02/01/2022 23:50 WG1810384 1 02/01/2022 23:50 WG1810384 Dilution Analysis Batch date / time 1 01/29/202216:27 WG1810127 1 01/29/202216:27 WG1810127 1 01/29/202216:27 WG1810127 1 01/29/202216:27 WG1810127 SDG: DATE/TIME: PAGE: L1454554 02/07/22 16:05 5 of 21 MOCKSVILLE WTP SAMPLE RESULTS - 01 Collected date/time: 01/24/22 09:00 L1454554 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier RDL Limit Dilution Analysis Analyte mg/I mg/I mg/I date/time 1,2-Dichloroethane ND 0.0500 0.50 1 01/29/202216:27 1,1-Dichloroethene ND 0.0500 0.70 1 01/29/202216:27 2-Butanone (MEK) ND 0.500 200 1 01/29/202216:27 Tetrachloroethene ND 0.0500 0.70 1 01/29/202216:27 Trichloroethene ND 0.0500 0.50 1 01/29/202216:27 Vinyl chloride ND 0.0500 0.20 1 01/29/202216:27 (S) Toluene-dH 93.6 80.0-120 011291202216.27 (S) 4-Bromofluorobenzene 102 77.0-126 011291202216.27 (S) 1,2-Dichloroethane-d4 90.6 70.0-130 011291202216.27 Chlorinated Acid Herbicides (GC) by Method 8151A Result Analyte mg/I 2,4,5-TP (Silvex) ND 2,4-D ND (S) Z4-Dichlorophenyl Acetic Acid 77.H Pesticides (GC) by Method 8081B Batch WG1810127 WG1810127 WG1810127 WG1810127 WG1810127 WG1810127 WG1810127 WG1810127 WG1810127 Qualifier RDL Limit Dilution Analysis Batch mg/I mg/I date / time 0.00200 1 1 02/03/20221159 WG1811223 0.00200 10 1 02/03/20221159 WG1811223 14.0-158 021031202211.59 WG1811223 Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Chlordane ND 0.00500 0.03 Endrin ND 0.00500 0.02 Heptachlor ND 0.00500 0.0080 Heptachlor epoxide ND 0.00500 0.0080 Lindane ND 0.00500 0.40 Methoxychlor ND 0.00500 10 Toxaphene ND 0.0100 0.50 (S) Decochlorobiphenyl 93.8 10.0-128 (S) Tetrochloro-m-xylene 93.0 10.0-127 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Analyte 1,4-Dichlorobenzene 2,4-Dinitrotoluene Hexachlorobenzene Hexachloro-1,3-butadiene Hexachloroethane Nitrobenzene Pyridine 3&4-Methyl Phenol 2-Methylphenol Pentachlorophenol 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol (S) 2-Fluorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Z4, 6-Tribromophenol (S) p-Terphenyl-d14 ACCOUNT: EMA Resources Dilution Analysis date / time 1 02/03/2022 15:56 1 02/03/2022 15:56 1 02/03/2022 15:56 1 02/03/2022 15:56 1 02/03/2022 15:56 1 02/03/2022 15:56 1 02/03/2022 15:56 0210312022 15.56 0210312022 15.56 Batch WG1809205 WG1809205 WG1809205 WG1809205 WG1809205 WG1809205 WG1809205 WG1809205 WG1809205 Result Qualifier RDL Limit Dilution Analysis Batch mg/I mg/I mg/I date/time ND 0.100 7.50 1 01/31/2022 0611 WG1809535 ND 0.100 0.13 1 01/31/2022 06:11 WG1809535 ND 0.100 0.13 1 01/31/2022 06:11 WG1809535 ND 0.100 0.50 1 01/31/2022 06:11 WG1809535 ND 0.100 3 1 01/31/2022 06:11 WG1809535 ND 0.100 2 1 01/31/2022 06:11 WG1809535 ND 0.100 5 1 01/31/2022 06:11 WG1809535 ND 0.100 400 1 01/31/2022 06:11 WG1809535 ND 0.100 200 1 01/31/2022 06:11 WG1809535 ND 0.100 100 1 01/31/2022 06:11 WG1809535 ND 0.100 400 1 01/31/2022 06:11 WG1809535 ND 0.100 2 1 01/31/2022 06:11 WG1809535 52.0 10.0-120 0113112022 06.11 WG1809535 31.0 10.0-120 0113112022 06.11 WG1809535 78.0 10.0-127 0113112022 06.11 WG1809535 72.3 10.0-130 0113112022 06.11 WG1809535 74.0 10.0-155 0113112022 06.11 WG1809535 85.9 10.0-128 0113112022 06.11 WG1809535 PROJECT: SDG: DATE/TIME: PAGE: L1454554 02/07/22 16:05 6 of 21 EEEEZEEZE g . t ƒ D g c \ ID e 2 u ƒ D _ _ / \ Cf) k O e _ \ / M , % E = 3 \ .g Q RLO / _ 6 LO rl ƒ co # - \ EEEEZEEZE 0 /[1 T PI .. 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This is not intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions u Fc Fss] MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). Fn RDL Reported Detection Limit. Rec. Recovery. Fr RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and F (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the F Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Rc These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe samples from the time of collection until delivery to the laboratory for analysis. This section ofyour report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J3 The associated batch QC was outside the established quality control range for precision. J5 The sample matrix interfered with the ability to make any accurate determination, spike value is high. J6 The sample matrix interfered with the ability to make any accurate determination, spike value is low. T8 Sample(s) received past/too close to holding time expiration. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1454554 02/07/22 16:05 19 of 21 ACCREDITATIONS & LOCATIONS Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska N E-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TNO02 California 2932 New Mexico TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina' DW21704 _ Georgia NELAP North Carolina 3 41 Georgia' 923 North Dakota R-140 Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky' 6 KY90010 South Carolina 84004002 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee'" 2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas5 LABO152 Maryland 324 Utah TN000032021-11 Massachusetts M-TNO03 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2 LA A2LA— ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2 LA — ISO 17025 5 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TN00003 Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. Rc ACCOUNT: PROJECT: SDG: DATE/TIME: EMA Resources L1454554 02/07/22 16:05 PAGE: 20 of 21 a x E f U£ a m " LL a Z g ' U -CL �3 a qwy a -1 O O � E LL C c c ;✓: �& .@ L9 c n E o coa m t — T V � U U o a f- E a u C � � a co U 3 �j� Q o L N - — A o o o U° c Ud y c C a r y m m Ln CC a C13 d d L OD o a 0 a Z in LA } C Ql u M a 4 z w Y — N v 'O? o O ran O ULLI n sOMONAO-ll III} - dlDl X saIdON-JIJ-11 ASa3 X o 7-.F1 N a a a Z a E M V .. N a a ~o 0 o � r a � T r T C a T '. O d T a � o m > o 0 Ill a � o > �n L zlz zl z17I21 O Q a o � a c u U U 41 m � U L o N •U `� � Q a a d ->i .� > a m c a l v b m m yy N N .-1 01 •� W N 41 V1 a! 4a UUa+uw al [L (UO�C `J a o u OV m u vi N K V � E L } o E 4) p .. 00 F- or Y = O a — w N m n w pi 7 � cc CE m �P c � ,,p in in � d d y � a a H OC K Q . d E E E_ N H H W ' _ N � b u T rti � ai 1 ci a G � � w d m n % 1 _ a u n a� a E Y u u Eo T LL m N C OD N �0 C C oA �6 a to y Q O o c C C � �.. L f O cr Cc cc 4b) Residuals Information Sheet Residuals Information Sheet Generator: Town of Mocksville-WTP Facility: Mocksville WTP Address: 771 Sanford Rd Mocksville, NC 27028 Phone: 336-751-2635 Contact: Justin Turbyfill Land Application Contractor: EMA Resources Inc. 755 Yadkinville Rd Mocksville, NC 27028 Phone: 336-751-1441 Contact: Brent Collins Please Note: The application of these residuals is only allowed in accordance with subject permit. (WQ0039552) All applicable setbacks in accordance with 15A NCAC 02T .1108(b) will be adhered and is the responsibility of the land application contractor. Application rates shall be applied at agronomic rates for intended uses. No residuals shall be applied to any site that is flooded, frozen, or snow covered. Adequate procedures will be implemented to prevent surface runoff of residuals in any surface waters. The attached residuals analysis report is a summary of major and micro -nutrients available in the residuals. If you have any questions concerning this information, you may contact EMA Resources Inc, at the number listed above. 5) Operation & Maintenance Plan Standard Operating Procedure and Operation and Maintenance Plan for the Town of Mocksville WTP- Land Application Program 1. Purpose a. Ensure the requirements of the Town of Mocksville, NC Non -Discharge Perm it#WQ0039552 are met. 2. Personnel a. The following is a list of personnel in order they are to be contacted when information needs to be shared. i. EMA Resources inc. 1. Jeff Thompson — Project Manager 336-477-4078 2. Roy Whitaker — Director of Bus.Dvlpmt./Ops. 336-909-1718 3. Brent Collins — Director of Technical Services 336-399-3646 ii. Town of Mocksville, NC 1. Ken Gamble — Town Manager 336-753-6701 2. Justin Turbyfill — WTP-ORC 336-751-2635 (EnviroLink) 3. Operational Functions a. The operational function of this project it going to involves transporting the thickened liquid residuals via tanker trailers to a staging area in the receiver sites. The liquid residuals will be off-loaded into tractor/pull tank spreader or pumper truck and land applied in a uniform application. It is going to be spread at agronomic rates that are determined using the Realistic Yield Expectations (RYE) as outlined in the permit, the amount of other nutrient sources the landowner and operator has applied, and the residuals nutrient and metal sample that is current for that monitoring period. The material is going to be land applied on fields that have a crop growing on them that are going to either be grazed or cut for animal feed or row crops for feed or fiber. Application rates will be reduced by 25% on fields that are primarily used for grazing in accordance with USDA-NRCS 590. Grazed fields will be determined by the farmers and EMA project managers. 4. Maintenance Schedule a. EMA Resources Inc. will follow the maintenance schedule as recommended by the EMA Resources EHS&T Director for the equipment necessary to complete the job. S. Safety Measures a. The Town of Mocksville and EMA Resources Inc. believe in operating in a safety conscious manner and all employees participate in safety training that is designed to help employees recognize safety issues and take steps to prevent accidents from occurring. In addition, EMA Resources employees have the authority to stop operations if they think any aspect of the operation is going to cause environmental or personal harm. 6. Spill Response Plan a. In the unlikely event of a spill, the following action shall be taken immediately. i. Management of Spill Clean-up Activities: The EMA Resources Project Manager shall take immediate charge and initiate clean-up activities. EMA Resources labor and equipment is to be utilized. In the event additional labor and equipment is required, assistance may be requested from the Town of Mocksville, The NC Department of Transportation, and other private contractors as necessary. ii. Halt the Source of the Spill: Such as a ruptured container or damaged transport unit. iii. Contain the Spill: Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The Operations Manager or the person in charge on the spill site will be advise the clean-up personnel where to get the straw, lime, and other items necessary to complete the clean-up operation. ie. local farmers, farm supply centers, nurseries. iv. Initial Clean -Up: Employ front-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw and sand soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. v. Final Clean-up: Employ rotary brush sweeper if needed and apply lime to the spill area upon the approval of the clean-up efforts by the state regulatory representative. If the event occurs on private property, the clean-up will be completed to the satisfactory of the property owner and state regulatory representatives. The ultimate goal will be restore the spill area to its original condition if possible. vi. Notification: As soon as possible after the spill occurs, the EMA Resources Project Manager or designee will notify the Town of Mocksville and the EMA Resources main office. EMA Resources office staff is then responsible for notifying other key EMA Resources personnel. vii. Reporting_ EMA Resources staff will notify the Winston-Salem regional office of the NCDENR by telephone (336) 776-9800 as soon as possible, but not more than 24 hours after, or on the next working day following the occurrence. The EMA Project Manager shall provide a written report with 48 hours of the spill to the EMA Resources Director of Technical Services and the Town of Mocksville staff. The report shall list all relative information and actions taken. With the assistance of EMA Resources personnel, and the Town of Mocksville personnel, a written report will be filed with the Winston- Salem regional office within 5 days of the occurrence. For after-hours reporting, the Division's emergency number shall be called to report all incidences (800) 662-7956. 7. Inspection Plan a. Inspection for the land application of residuals will conducted on a minimum of a weekly basis at the land application site during land application activities. The inspection frequency is based on the time frame that it is going to take to complete the project and the amount of dry tons to be land applied from this facility. The inspections will consist of inspecting a current field that is being applied as well as inspecting random fields that have been completed. Inspections will be conducted by Jeff Thompson — Project Manager. These inspections will consist of the following: i. Verifying the application rates for each field that plan on receiving material. ii. Checking the calculated loads to ensure the correct amount of residuals are being land applied. iii. Ensure that all manned equipment has a copy of the permit and the operation and maintenance plan. iv. Ensure that the field has been flagged properly and that all buffers are being adhered to. v. Ensure proper signage has been posted vi. Verify that the proper number of samples of the residuals have been taken and that it meets the criteria for land application. vii. The records will be kept in the EMA Resources project files in the main office. Copies of all analyses and records will be forwarded to the Town of Hillsborough and kept on file. viii. EMA Resources and the Town of Mocksville staff will immediately inform the other party if any of the following conditions are noted. 1. Any occurrence with the distribution program resulting in the land application of significant amounts of material that is abnormal in quantity or characteristics. 2. Any failure of the distribution system that results in the release to surface waters. 3. Any time that self -monitoring indicates that the facility has gone out of compliance with the permit. 4. Any process failure that results in the system not adequately treating the residuals. 5. Any spill or discharge from a vehicle or piping system during residuals transportation. 6. Any release that requires immediate reporting outside normal business hours shall be called in by EMA Resources staff to DENR at (800) 662-7956. This number is to be called in the event of a release to surface waters or imminent failure of a storage system when the event occurs outside of normal business hours. 8. Sampling and Monitoring Plan a. Sampling for this project consists of sampling the residuals prior to land application occurring in order to ensure that the residuals are suitable for land application. b. The samples will be collected from the two storage tanks that holds the thickened residuals c. Roy Whitaker, Brent Collins, or other designee will be responsible for sample collection for nutrient and metal and TCLP. d. Nutrient, metal and TCLP sample aliquots will be collected randomly and consist of at least 7 individual aliquots mixed together in order to get the composite sample for these parameters. e. The residuals will be sampled annually for TCLP including the RClls. f. Metal and nutrient parameters will be collected and analyzed based on the requested dry ton numbers in the permit application. 9. Environmental Impacts a. The environmental impacts for residuals may be affected by this procedure. b. This procedure helps assure that land application is conducted in a safe and efficient manner while ensuring compliance with the laws and regulations and to minimize exposure, negative environmental impacts and public relation concerns.