NC0035173_Remission (Request)_20220323

March 23, 2022 Wieland
North Carolina Department of Environmental Quality
Water Sciences Section
Division of Water Resources Wieland Copper Products, LLC
3990 US 311 Hwy N
1621 Mail Service Center Pine Hall, NC 27042
Raleigh, NC 27699-1621 Phone: [phone]
Fax: [phone]
Subject: Request for Remission [e-mail]
Assessment of Civil Penalty for Violations of NC General Statute+&-Jr'"�sper.com
NPDES Permit No. NC0035173/003
Wieland Copper Products, LLC RECEIVED
Case No.TX-2022-0003 f 100
Stokes County MAR 2 8 2022
To Whom it May Concern: Wei& Sciences Section
On March 11,2022,Wieland Copper Products, LLC, received an Assessment of Civil Penalty for
Violations of NC General Statute 143-215.1(a)(6) Notice for violation of the discharge limits and
monitoring requirements of NPDES Permit No. NC0035173/003.
Wieland's toxicity self-monitoring reports revealed that the average chronic value for the fourth
quarter of 2021 to be 39.75%which is lower than the chronic limit for the facility(90%).The facility
has failed monthly toxicity testing since April 2021. In this letter I am requesting a remission of the
civil penalty because the violation was unintentional and inadvertent. In addition to incurring
significant costs to abate the toxicity failure in our effluent and return to compliance,Wieland has
spent considerable time and taken numerous actions to determine the root cause(s)of the failure.
While our actions have shown improvements to the discharge effluent,Wieland is still not meeting
the minimum 90%requirement.Wieland has also ensured NCDEQ was kept well informed of the
progress and has acted in good faith in our environmental protection efforts both historically and
during our mission to return to full compliance.
Summary of actions taken:
1. May 3, 2021,Wieland was notified by Pace Analytical that Outfall 003 failed Whole Effluent
Toxicity Testing for Q2 taken in the month of April.An investigation was started to
determine the root cause and to prevent the toxicity failure in the future.The Incident
Investigation Report shows the complete history of the major corrective/preventative
actions taken to date (See Attached). Note*The failure coincided with the sale and
transition of R&A Laboratory to Pace Analytical (who utilizes Meritech for lab testing) and
the removal of our outdated Water Tube product line and associated machinery.The effects
to the quality of the effluent are undetermined, but testing/sampiing hasn't revealed any
major changes.To our knowledge the new lab is testing as required, but I feel these major
changes are worthy of note.
2. Wieland has contracted Pace Analytical to perform toxicity, heavy metals,PPA, and tank
study sampling on the various cooling water systems,holding tanks,influent,and effluent
streams of the processes in an attempt to determine the source of the toxicity.Total cost to
date of$17,737.50. No red flags were discovered through testing that would indicate a
toxicity failure and the sampling results were similar to historical sampling results.
3. Wieland has contracted environmental remediation companies to empty and clean the
cooling water tanks and pits at a cost of$45,706.45.
4. Wieland has started adding bentonite clay and activated carbon to the process to absorb any
toxins and aid in flocculation.Cost$4,090.00.

5. Wieland is currently in the process constructing and installing an additional waste water
treatment plant which utilizes an ion exchange resin to remove copper at a cost of
$529,751.27.We are hoping that this system will eliminate the toxicity issue.(See Attached).
6. Closed all blow downs from machinery influents and instead pump to totes.Then send out
totes via tanker trucks to segregate the cooling water only in our WWTP and sample(no
changes,still failed toxicity).
7. Wieland has consulted with leading water treatment engineers in our area for help in
determining the source of the toxicity,and so far all are at a loss as to the cause.Wieland
has recently reached out to a Ph.D.Aquatic Toxicity Engineer with ERM Environmental to
further assist in analyzing the toxicity issue.
Wieland will continue to utilize all available resources to determine the source of the toxicity in
Outfall 003 so the proper corrective actions can be implemented.Wieland hopes NCDEQ is satisfied
with our actions taken and will approve our request for remission.
If you have any questions please feel free to call me at(336)445-4526.
rBes, egar f�pnnk e
Environmental &Facilities Supervisor

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENTAL QUALITY
COUNTY OF STOKES
IN THE MATTER OF ASSESSMENT ) WAIVER OF RIGHT TO AN
OF CIVIL PENALTIES AGAINST ) ADMINISTRATIVE HEARING AND
STIPULATION OF FACTS
Wieland Copper Products LLC
NPDES PERMIT NO. NCO035173 ) CASE NO. TX-2022-0003
I
Having been assessed civil penalties totaling$3.073.88 for violation(s) as set forth in the assessment document
of the Director of the Division of Water Resources dated March 11,2022,the undersigned, desiring to seek
remission of the civil penalties,does hereby waive the right to an administrative hearing in the above-stated
matter and does stipulate that the facts are as alleged in the assessment document. The undersigned further
understands that all evidence presented in support of remission of this civil penalty must be submitted to the
Director of the Division of Water Resources within 30 days of receipt of the notice of assessment. No new
evidence in support of a remission request will be allowed after 30 days from the receipt of the notice of
assessment. n n
This the day of 20-a.
?IATURE
ADDRE
990 05 31 hip✓
IJC , 276
RECEIVED TELEPHONE
MAR2 8 2022 � 7 .-V
Water Sciences Section

RECEIVED
MAR 2 S 2022
JUSTIFICATION FOR REMISSION REQUEST Water Sciences Section
Case Number: TX-2022-0003 County: Stokes
Assessed Party: Wieland Copper Products LLC
Permit No. (if applicable): NC0035173 Amount Assessed: $3,073.88
Please use this form when requesting remission of this civil penalty. You must also complete the
"Request For Remission. Waiver ought to an Administrative Hearing and Stipulation ofFacts"
form to request remission of this civil penalty. You should attach any documents that you believe
support your request and are necessary for the Director to consider in evaluating your request for
remission. Please be aware that a request for remission is limited to consideration of the five
factors listed below as they may relate to the reasonableness of the amount of the civil penalty
assessed. Requesting remission is not the proper procedure for contesting whether the violation(s)
occurred or the accuracy of any of the factual statements contained in the civil penalty assessment
document. Pursuant to N.C.G.S. § 14313-282.1(c), remission of a civil penalty maybe granted
only when one or more of the following five factors applies. Please check each factor that you
believe applies to your case and provide a detailed explanation, including copies of supporting
documents, as to why the factor applies (attach additional pages as needed).
(a) one or more ofthe civil penalty assessment factors in N.C.G.S. 1 4313-2 8 2.1(b)were
wrongfully applied to the detriment of the petitioner (the assessment factors are listed in
the civil penalty assessment document);
i/ (b) the violator promptly abated continuing environmental damage resulting from the
violation (i.e., explain the steps that you took to correct the violation and prevent future
occurrences);
(c) the violation was inadvertent or a result of an accident (i.e., explain why the
violation was unavoidable or something you could not prevent or prepare for);
(d) the violator had not been assessed civil penalties for any previous violations;
(e) payment of the civil penalty will prevent payment for the remaining necessary
remedial actions (i.e., explain how payment of the civil penalty will prevent you from
performing the activities necessary to achieve compliance).
EXPLANATION:

3/23122,2:54 PM Print Summary Distribution
RECEIVE,LD
Wieland Wieland Pine Hall MAR 282022
Ul/aiwr Scierces 5cctiorl
ALERT: Incident
INCIDENT DATE: Monday, May 3, 2021 12:30 AM
FACILITY: WCP Pine Hall, NC - Outfall #003
LOCATION DETAILS: -
INCIDENT ID: 42785
WHAT HAPPENED: WCP quarterly toxicity compliance sampling failed at 90% in violation of the NPDES
permit.
FINDINGS(ROOT CAUSE): a To prevent the overflow and volume in the catch pits,which then require an operator
or maintenance to pump out,a redesign is needed to the levels and shower drain.
The cooling water and waste sludge need to be separated and processed separately.
To limit labor, investigate how much the catch pits fill once the shower has been
separated and then set a contract with a waste disposal company to perform regular
pump outs. Level alarms will indicate if an abnormal condition occurs so WCP
personnel can respond in a timely fashion.
Corrective/Preventative Actions Assigned:
CORRECTIVE/PREVENTATIVE ACTIONS TARGET DATE COMPLETION DATE
Re-route diaphragm pumps to pump from catch pits to cooling system, 5/31/2021 5/27/2021
to catch pits to totes or other IBC.
Take a non-compliance grab sample and review results. 5/7/2021 5/10/2021
Install float and digital display in IH #2,#3 and main cooling pits. 5/31/2021 5/27/2021
Based on Outfall#003 results,clean out entire IH cooling systems. 5/31/2021 6/1/2021
If Jose approves the tanker have them pump out#3 IH. 5/31/2021 6/1/2021
Ensure actions are taken to prevent another occurrence in time for Junes 6/4/2021 5/14/2021
toxicity sampling.
Send out safety contact to notify of policy to pump catch pits into totes 6/4/2021 6/4/2021
only,and steps to take with new alarm installed.
Submit a list of all maintenance employees and IH workers to EHS. 6/4/2021 6/4/2021
Update the IH SOP to reflect the new alarm and steps to take.Also 6/11/2021 7/15/2021
include the steps to pump the catch pits our into tote and forbid
pumping into the cooling pits.
Clean out everything to ensure no contamination 6/28/2021 6/28/2021
Install mixer into tank to dose bentonite clay which acts as a binder for 6/28/2021 6/28/2021
hUps://go.sospes.com/ReportSummary?id=42785 1/3

3/23/22,2:54 PM Print Summary Distribution
the^coagulant,and also helps absorb metals,toxins,etc.
Pass monthly compliance sampling two consecutive months in row. 5/4/2022
Drain and clean 100k tanks 12/30/2021 1/7/2022
On 9/9/21,Pace Analytical Laboratories performed a complete analysis of 10/19/2021 10/19/2021
the water in the 100K tanks and the influent and effluent of the W WTP.
The analysis showed that the water did not contain any solvents,metals
were low,and the salts were not high enough to cause a toxicity issue.
(See Documentation)
On 9/22/21,Pace Analytical Laboratories performed Toxicity Analysis on 10/19/2021 10/19/2021
the following cooling water systems:Direct Cast 1-4,Annealing Furnaces
1&3,Bunch Coilers 1&2 Quenchwater,IH Shower Water.The results
showed that the Bunch Coilers and IH Water failed immediately.The
other systems failed slightly due the systems possibly being cycled up.
The corrective action that was implemented as follows:Eliminated the
Bunch Coiler and IH blowdowns and adjusted the Conductivity from 800
u/S to 600 u/S all other cooling systems.
SE Laboratories has performed testing on the Promoss and sent the 10/27/2021 10/27/2021
samples to Pace Laboratories for Toxicity Analysis.We are waiting on the
results in order to try to determine if corrective action is needed.
The results of the testing will determine our next course of action. 10/27/2023 11/9/2021
The results of the testing will determine our next course of action. 10/27/2022 1/7/2022
Ken Ridings of SE Laboratories conducted a second round of toxicity 11/22/2021 11/22/2021
testing on the Promoss because ProMoss failed toxicity on the first round
of testing.Ken seems to think that the failure was due to his lab
technician used a zinc coated paper clip and a dirty magnetic stirring
stone.The ProMoss passed the second round of toxicity testing at 100%.
The EHS Department of WCP has contracted Meritech Laboratories to
conduct toxicity testing on the ProMoss to confirm the results of SE
Laboratories testing.
SE Laboratories is contracted to provide WCP with cooling water 12/17/2021 12/9/2021
treatment utilizing Promoss instead of chemical treatment.On 10/27/21,
SE laboratories was notified by Meritech Laboratories that their first
round of toxicity testing failed.Ken Ridings of SE Laboratories thinks that
a zinc coated paperclip and a dirty magnetic stirring stone may be the
reason.On 11/17/21,SE Laboratories was notified by Meritech Laboratories
that their second round of testing passed at 100%.WCP has sent a
sample of the Promoss to Meritech Laboratories to do toxicity testing in
order to confirm whether or not the ProMoss is the cause of the toxicity
failures.Ken Ridings tested 0.1 of a gram of Promoss.I have asked
Meritech to follow Kens procedures but to conduct two tests using 0.1 of
a gram and 1 gram and to make sure that the Promoss is in full contact
with the water.
On March 1,2022,WCP contracted Pace Analytical to perform a Priority 3/23/2022 3/23/2022
Pollutant Analysis on the effluent of the Cooling Water Treatment Plant
the discharges into Outfall 003.This was to try to determine the source
of the toxicity.On March 17,2022,WCP received the results.The results
proved to be inconclusive.Could determine the source of the toxicity.
https://go.sospes.com/RepartSummary?id=42785 213

3/23/22,2:54 PM Print Summary Distribution
4
On-12/15/21,Activated Carbon was added to the treatment process 3/23/2022 3/23/2022
during toxicity testing.The results show great improvement with a failure
at 63.6%rather than an immediate failure of 11.25%.On 1/24/22 and
1/26/22,Activated Carbon was added to the treatment process with the
same results as 12/15/21.
https://go.sospes.mm/ReportSummary?id=42785 313

Copper Removal Proiect and Toxicity Evaluation Expenditures
MAR 2 S 2'U'V2
WaiarSciencvsuc
Copper Removal Project Estimated Cost $661,867 80
Copper Removal Project Cost(YTD) $517,271.27
Pipe Installation Labor $12,480.00
Total $529,751.27
Toxicity Issue Expenditures
Toxicity Evaluation Cost(Pace Laboratories) $17,737.50
100K Tank Cleaning $21,026.45
Direct Cast Cooling Water Pit Cleaning $10,290.00
Annealing Furnace Cooling Water Pit Cleaning $14,390.00
Activated Carbon $1,690.00
Bentonite Clay $2,400.00
Total $67,533.95
Copper Removal Project Cost(YTD) $629,751.27
Toxicity Issue Total (YTD) $67,533.95
Total (YTD) $597,285.22

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P+18474656785- [e-mail] e sCEFI
Wieland North America, Inc. 1 567 Northgate Parkway I Wheeling, IL 60090-2682 1 USA
Please consider the environment before printing this email UAR 2 8 202p
From:Tony Sprinkle<[e-mail]> WaierS
Sent: Friday, March 11, 2022 2:06 PM C)c'tjLBS ��'Ci10n
To:Catherine Babik<[e-mail]>
Cc:Jared Ranken<[e-mail]>
Subject:Waste Treatment Project Number 3700018.01
Good Afternoon Catherine,
Can you email me a print out on what we have paid out on the Water Treatment Project No. 3700018.01?
This is for NCDEQ.
Thanks,
Best regards I Freundliche Gruge,
Tony Sprinkle
Environmental Supervisor
P+13364454526- [e-mail]
Wieland Copper Products,LLC 13990 US 311 Hwy N I Pine Hall INC,NC 27042 1 USA
wieland.coin
Linkedln Twitter Facebook youtube Instagram
Please consider the environment before printing this email
2

�h
Tony Sprinkle
From: Anna Lazarz <[e-mail]>
Sent: Monday, March 14, 2022 1:24 PM
To: Tony Sprinkle
Cc: Catherine Babik,Jared Ranken
Subject: RE:Waste Treatment Project Number 3700018.01
Attachments: 7000000028.XLSX
Hello Tony,
This is what we have currently booked on this asset:
Asset ISub-number 1Assignment iFiscal Year ISequence Asset Value Date ,Amount Posted (Currency
II I Number I I
000000028 T K2021 2 6130/2021 117,373.91 USD
.1000000028 TO '2021 1 713112021. 146,828.98 USD
Ff000000028 '2'021 12 8/31/2021 B72.75 USD
000000028 T '2021 17 9/30/2021 139,795.19 USD
000000028 T 12022 12 11130/2021 0.00:USD
000000028 'b 12022 It 1213112021 76,055.71 USD
000000028 O '2022 12 1/3112022 36,344.73 USD
000000028 rD tG22 17 2/28/2022 0.00 USD
517,27127
Company Code 0037 Wieland Copper Products
Asset 17000000028 FO-1 Wastewater Treatment Capper Removal System
Fiscal year [1 z a
ned values=' Posted vakres Corrgraris�ns Parameters
— -_ —
Planned values GROUP GAAP in local currency USD
Value Fiscal year start Change Year-end Crcy
APC transactions 404,870.83 112,400.44 517,271.27 USD
Acquisition value 404,870.83 112,400.44 517,271.27 USD
Ordinary deprec. USD
Special depreciation USD
Unplanned dep. USD
Write-up USD
j Value adjustment USD
Net book value 404,970.83 112,400.44 517,271.27 USD
Dawn payments USD
E
Best regards I Freundliche GrURe,
Anna Lazarz
Senior Accountant
1

wieland
soances Section Wieland Copper Products, LLC
U�$tr 3990 US 311 Hwy.N.
PINE HALL NC 27042
USA
Shipping address:
W.J. Turpish & Co., Inc. Wieland Copper Products, LLC
439 Neisler Street 3990 US-311
Shelby NC 28152-5001 NC 27042
USA
Tel.No.
Fax No.
Department/Pers on responsib'e Phone Exlens on Fex(direct) Dz to Pzce
EX.PH/Vaulty [phone] 06/22/2021 1/ 2
tim.naulty®wieland.com
Techncal person msponsib'e Phone cxtens on Supplier No. Your ref. QLcte
30076270
Purchase Order No. 4509045887
CRDE R CONFIRMAIION MUST EE SENT TO tim.naulfyggwieland.cem
Goods and invoices will net he accepted withept der;very nets and unless cur PO No.is indicated on the bill of lading,deliveiy note and
invoice.Please send invoice in dcpl.'cate.
The latest revision cf the stands id shall to applied.Speelfications in addition 10 the siandaid shall be met.
QUOTATION - T 10-210602
Item Material number Delivery date Quantity U/M Fixed price
001 07/30/2021 4 PC 20,335.00 USD/l PC
RESIN TANK w/ 30CubicFeet MEDIA
FIBREGLASS TANK IN STEEL LIFTING FRAME 44"x44"x 103" TALL
30 CUBIC FEET OF PUROMET MTS9300 RESIN PER TANK
INSTALLED PER APPROVED DRAWING
Total fixed price without tax 81,340.00 USD
-------------------
Terry s cf c'el'�ery: EXW, Incoterms® 2020 Shelby
Truck
Pa ym ant terms: within 25 days Due net

RECEIVED
MAR 2 8 2022
ft'Scianc s Seciiun
CONCRITE - . . • ,
FINISHING
P.O.Box 4704
Eden,North Carolina 27289-4704 Date: April 28,2021
[e-mail]
www.wraysconcretefinishing.com Proposal# 10459
336-362-3630
Bill To: Wieland Copper Service To: Tony Sprinkle
3990 US 311,Pine Hall NC [e-mail]
Sales Rep Service Date Terms
Product ID Description Oly/Hours Unit Price Line Total
Dig a 6'dip pit near the waste water system.
Grade,form,pour,and finish a pad in the
bottom of the pit to support the block walls.
Concrete will be 4000psi and have 2 rebar
mats at 12"on center.Lay block and fill the
cells with concrete.The inside dimensions
of the block walls will be 6'X6'and 6'high.
Approximately one course of block will be
lout of the ground. 14,700.00
Subtotal 14,700.00
Notes: Discount% 0%
Thank you for considering Wray's Concrete for your Discount Amount
concrete needs.If we can be of further assistance please
let us knowl TOTAL14,700.00

RECEIVED
MAR 2 8 2022
Warr sciences saction
FINISHING
P.O.Box 4704
Eden,North Carolina 27289-4704 Date: April 29,2021
[e-mail]
www.wraysconcretefinishing.com Proposal# 10460
336-362-3630
Bill To: Wieland Copper Service To: Tony Sprinkle
3990 US 311, Pine Hall NC [e-mail]
Sales Rep Service Date Terms
Product ID Description Qty/Hours Unit Price Line Total
Lay block along the mechanical roam in the
pit to the elevation of the new concrete and
fill the cells.Place dean stone in the pit at A
bay to allow for concrete to be 6"above the
existing pedestal in the floor.Place 2 rebar
mats at 12"on center using#4 rebar.Form,
pour,and slick finish the area using 4000psi
concrete. 57,100.00
Subtotal 67,100.00
Notes: Discount% 0%
Thank you for considering Wray's Concrete for your Discount Amount 0.00
concrete needs.If we can be of further assistance please TOTAL 57,100.00
let us know!

Tony Sprinkle
From: [e-mail]
Sent: Wednesday, June 30, 2021 8:01 AM
To: Tony Sprinkle
Subject: RE:Vertical Turbine Pump Quotation
Attachments: Submittal -VT pump Wieland 6-28-21.pdf
CAUTION: This email originated from outside of the organization Wieland. Do not click links or open attachments unless
you recognize the sender and know the content is safe. Sender address is: [e-mail]
Tony,
Two options for the vertical turbine pump with 14' column.
National Pump (American Turbine), 1-61- 30 gpm at 300' Head, 5 HP, 1800 rpm,460v/3 14'-6"
column $19,882.00 each X - ^ A / G ; �
TACO SILLS, 30 gpm at 300' Head, 10 HP, v 3 14'-6"
column $12,600.00 each
Multipurpose valve, 2",TACO
MPV020 $ 365.75 each
Regards,
OR
William (Bill) Turpish, PE, PEM, CEA, CEM
W 7 Turpish and Company
704-484-3450 Office
704-473-0270 Cell
www.turi)ish.com
439 Neisler Street
Shelby, NC 28152-5001
t

2L*ft Ila 490c.
7B7/Lo- 46-1�
Okay to Pay Water Treatment Project No. 3700018.01
P.O. Box 4704
Eden, North Carolina 27289-4704 Date: August 3, 2021
[e-mail] Invoice# 90
www.wraysconcretefinishing.com
336-362-3630
Bill To: Wieland Copper Service To: Tony Sprinkle
3990 US 311, Pine Hall NC [e-mail]
Sales Rep Service Date Terms
Product ID Description Qty/Hours Unit Price Line Total
Clean,prime,and paint the 40X40 pit
walls including the hand rails around the
perimeter in A Bay. 5,175.00
Subtotal 5,175.00
Notes: Discount% 0%
THANK YOU,WE APPRECIATE YOUR BUSINESS, IF WE Discount Amount45,175.00
CAN ASSIST YOU WITH YOUR CONCRETE NEEDS IN THE
FUTURE, PLEASE GIVE US A CALL! TOTAL
PAID
TOTAL DUE

wieland
Wieland Copper Products, LLC
3990 US 311 Hwy.N.
PINE HALL NC 27042
USA
Shipping address:
Seegars Fence Company Wieland Copper Products, LLC
8220 Triad Drive 3990 US-311
Greensboro NC 27409 NC 27042
USA
Tel.No. 336-370-9797
Fax No.
Department/Person responsible Phone extension Fax(direct) Date Page
EX.PH/Naulty [phone] 11/02/2021 l/ 2
[e-mail]
Technical person responsible Phone extension Supplier No. Your ref. Quote
30080275
Purchase Order No. 4509075665
ORDER CONFIRMATION MUST BE SENT TO [e-mail]
Goods and invoices will not be accepted without delivery note and unless our PO No.is indicated on the bill of lading,delivery note and
invoice.Please send invoice in duplicate.
The latest revision of the standard shall be applied.Specifications in addition to the standard shall be met.
Item Material number Delivery date Quantity U/M Fixed price
001 11/29/2021 1 PC 15,234.90 USD/1 PC
RETENTION POND FENCE 226 LINEAR FEET
CHAIN LINK: 9 GAUGE x 1.2 OUNC
GATE POSTS 4" x ss40 TERMNAL POSTS 3" x ss40 1INE POSTS 2" x ss40
TOP RAIL 1-5/8" bRACED & TRUSSED
BOTTOM TENSION WIRE 7 GUAGE / 3 STANDS OF 12.5 GA. BARBWIRE
INCLUDES 3- 10' WIDE DRIVE GATES W/ 1 5/8" FRAME
GREEN BOTTOM LOCKING PRIVCY SLATS
002 11/29/2019 1 PC 1,911.50 USD/1 PC
WOOD BOARDER FENCE - 96 LINEAR FEET
WOOD POSTS - 6" x 6" SET IN CONCRETE
ROUGH SAWN RAIL BOARD 1" x 6"
Total fixed price without tax 17,146.40 USD

wieland
Wieland Copper Products, LLC
3990 US 311 Hwy.N.
PINE HALL NC 27042
USA
Company Date Page
Seegars Fence Company 11/02/2021 2/ 2
Terms of delivery: FOB, IncotermsO 2020
Truck
Payment terms: 30 days after receipt and acceptance of goods, net
Send all Invoices to: rrm
Please include our Purchase Order Number on your packing slip
Please send return confirmation by e-mail or fax to 336427-0491
INVOICE IN DUPLICATE
Parking 1 ist Must Arrnmp anY All Sh*nmonrs
WCP Purchase Order terms and conditions,revision dated 11-27.2006,are herein incorporated by reference
For all shipments that are not parcel group service:
Contact Glen Raven [e-mail] or 800-729-0081 unless otherwise
directed by WCP.Unauthorized deviations including excessive freight charges will result in a debit to your company.

GPS , M$ElHu ``may Quotation
�'CERiiF,IED'a'
GP SUPPLY COMPANY, LLC a �T... a0g... »eft..... ..
501 East Washing�tton Street 06/04/21 S151786
Greensboro NC 5401 ORDER TO: _ - -----
336-274-7615 Fax [phone] GP SUPPLY GGMPANY, u - -
501 Bast Washington stzeet
Gz....b .NC 21..1 1
336-274-7615 FaX [phone]
QUOTE TO: SHIP TO:
WIELAND COPPER PRODUCTS,LLC WIELAND COPPER PRODUCTS,LLC
3990 US 311 HWY N. 3990 US 311 HWY N.
PINE HALL, NC 27042 PINE HALL, NC 27042
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3851
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MIKE MCGOVERN 336-544-8089 UPS COLLECT Net Due 30 D 06/21/21 No
oxoca.:arr.::.;;;:..;:.;:.;:<.Baas:.:ma:,:.;:.:;.;.>:.::.::.>:.::.>:.;:.:;:.;;;;.... ;:.;:.;:.;:.;:.vEsxars r.. :;:::::.;:..::.;:.;:.;:.>:
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********* Shipping Instructions *** ******
* UPS ACCT # 28022X
*********************************** ******
2000ft 10040 2 S80 PVC PE PIPE 2 . 920 5840 .00
200ea 5335 2 S80 PVC COUPLING SXS 4 . 565 913 .00
20ea 5292 2 S80 PVC 90 ELL SXS 3 .667 73 .34
lea 93173 320Z PVC HD CLEAR CEMENT 31008 15 .933 15 . 93
OATEY
lea 749 320Z C720 PURPLE PLA PRIMER 10.105 10 .11
30758 / 55918
------------------- --------------—— -------------------------------------—----------------------------- --------------------- ?668 DUE TO THE ONGOING MARKET VOLATILITY. PRICES ARE IN EFFECT AT THE TINE OF QUOTATION SubtotalONLY AND MAY CHANGE AT ANYTIME WITHOUT NOTICE. Prices are based on entire quote of S&H CHGSmaterial and product availability. Please review the accuracy of quantity and -------------------_description. Availability of product is subject to change and may affect price and
freight charges. Orders are subject to credit and contract approval. Applicable taxes extra. Amount Due

YN 312 Crosstown Dr.Suite 188
Southern Val Peachtree City,GA 30269
& Service 704-900-9920
LI
June 28, 2021 REFCSIVED
MAR 2 E 20?
WIELAND Z
O US 311 Hwy N °? i'
Hall N.C.N.0 27284 USA Pine SCjc r Gs cC+fO
Attn.Jared Ranken Environmental, Health &Safety Director Wieland Group
Tony Sprinkle Environmental Supervisor Wieland Group
Dear Jared,Tony,
SOUTHERN VALVE&SERVICE,Inc is pleased to submit the following quotation for the new wastewater
treatment upgrade that will divert the domestic biological treatment outflow from the existing surface
water receiving stream into two large industrial wastewater equalization tanks.The treated domestic
water and the raw industrial wastewater will combine to flow through the current industrial physical-
chemical system as a single waste stream.The clear treated combined effluent will then be pumped
back into the main plant for final polishing to remove trace soluble copper.The Scope of the project is as
follows:
WASTEWATER EQUIPMENT
• N1 and N2 fiberglass mix tanks approx.4000 gals each constructed out of Derakane Signia
vinyl ester resin.
• Pumps 3 and 4 are GOULDS Model NPE 1.5 HP 3500 RPM 480V
• Fiberglass Tank Mixers are BRAWN BGMF300 3 HP 17SO RPM 480V with Dual 17" Impellers
Spaced 32"Apart
• SENSOREX pH Probe 1 Controls Acid Metering Pump
• SENSOREX pH Probe 2 Controls Acid Metering Pump
• SENSOREX pH Probe 3 Controls pH to Resin Train
• SENSOREX pH Probe 4 Controls Discharge Flow Totalizer
• Levels Controls 1 and 2 ARE NIVELCO
• TOSHIBA GF630 Flow Meter/Totalizer
• 2 SHELCO FILTERS 2 and 25 Micron
• 2 WALCHEM EHE SERIES METERING Pumps for Caustic and Acid Feed
Continued next page

312 Crosstown Dr. Suite 188
Southern ' Valve Peachtree City, GA 30269
& Service i„ 704-900-9920
SIEMENS PLC ELECTRICAL CONTROL CENTER
Siemens S7-1200 PLC with ProfiNET uplink to plant network will be used in this system. It will be
housed in a double—door free standing NEMA 12 enclosure.The micro PLC is capable of 6 analog
inputs,12 digital inputs,and 12 digital outputs.All motors will be controls by contactors in lieu of
VFD's.
Hardware
• NEMA12 Free—Standing Double—Door Enclosure (72x48x18)
• S7—1200 PLC with Associated 1/0 Modules
• 4—Motor Contactors
• 24VDC Power Supply
• Misc. terminal strip, wire,fusing, disconnect, etc.
Engineering& Design
• Panel layout drawings
• Electrical wiring diagrams
• System documentation package to include all drawings and equipment manuals.
INTERCONNECTING PIPING FOR NEW WASTEWATER EQUIPMENT IN EXISTING PIT ONLY.
DESGNED AND INSTALLED PRICE..............................................................$261,784.00
**In addition to the above price SV&S agrees to rebate the total of all Yd party invoiced installation
labor costs for controls,electrical and plumbing installation back to Wieland at''/:the difference in
price between the quoted job cost and the actual invoiced cost to SV&S,if the invoiced cost is less.
This is in an effort to help reduce total cost on the project. Total budgeted cost of these trades was
$57,800.00. Once invoiced we will credit any reduction in price at%the difference between
$57,800 and the actual invoiced cost.
Southern Valve and Service Terms and Condition of sale apply

312 Crosstown Dr.Suite 188
Southern !; Valve ,,, Peachtree City, GA 30269
& Service4
^ 704-900-9920
Continued next page
Exclusions& Exceptions
• SOUTHERN VALVE&SERVICE, INC will set system up based on parameters given to us by
WIELAND.
• SOUTHERN VALVE&SERVICE, INC is not responsible for outfall or sewer discharge limits.
• WIELAND agrees to any additional time for troubleshooting and parts found to be defective
beyond our original scope that affect the project startup time.Additions will be billed as a change
order to the base bid.
• WIELAND to provide 4 Turpish Canisters filled with Purlite 9300H Resin from their current vendor
and SOUTHERN VALVE&SERVICE will incorporate those parts into our system
• Ties into the existing plant pipes will be by WIELAND
Freight
• Equipment Freight to site not included and billed by separate invoice.
Payment Terms
• 50%with the PO
• 40% By Oct 1, 2021
• 10% at startup
Warranty
• Products manufactured, constructed, assembled by SOUTHERN VALVE&SERVICE, INC are
warranted for a period of 12 months from date or start-up against manufacturing defects
and workmanship which develop in the service for which they are designed, provided the
products are installed and used in accordance with any applicable instructions or limitations
issued by SOUTHERN VALVE&SERVICE,INC.
Limitation of Warranty
• Components used by SOUTHERN VALVE&SERVICE,INC. but manufactured by others, are
warrantied only to the extent of that manufacturer's warranty.This limited warranty shall
not apply if the product has been altered or repaired by others.SOUTHERN VALVE&
SERVICE, INC will make no allowances or credit for such repairs or alterations unless
authorized in writing by SOUTHERN VALVE&SERVICE, INC.

312 Crosstown Dr.Suite 188
SoUt ern Valve Peachtree City,GA 30269
& Service`` 704-900-9920
u
Continued next page
Items not included in Scope of Supply.
• Any civil work,anchor bolts or concrete work,site preparation,building and or structure to
house equipment,landscaping,or painting.
• Any concrete pit/lift station
• Any concrete pad for equipment
• Influent utilities and process piping from the identified skids as specified in the proposal and
system drawings.
• Effluent utilities and process piping the identified skids to effluent point of connection as
specified in this proposal and system drawings.
• Equipment interconnecting piping,conduit and wiring between Southern Valve and Service,
Inc supplied system components as identified in the system drawings and the current
infrastructure. IE wastewater piping tie in and power tie ins from the plant electrical feeds.
• Any insurance at place of installation
• Equipment off-loading,storing,and placement.
• Any solids transfer piping,valves.
• Any pump alignment
• local permitting process
• Supply of all reagent chemicals and other consumables
• All other items unless otherwise specifically mentioned in this proposal.
Sales Tax: North Carolina State Tax is not included in the attached proposal and will be
added to the final invoice,with the exception of the following.
• Tax Exempt Status
• 1%Manufacturers Tax
• Shipment of parts/equipment outside the state of North Carolina
• Note: If Tax Exempt or 1% Manufactures Tax applies,a copy of N.C.Tax
Certificate issued to Southern Valve and Service, Inc. must be submitted with
purchase order and/or credit application.
If you have any questions or need for further information, please do not hesitate to call.
Best Regards,
John Rowe
President

312 Crosstown Dr.Suite 188
Southern = Valve Peachtree City, GA 30269
& Service'" 704-900-9920
END

Tony Sprinkle
From: Jared Ranken <[e-mail]>
Sent: Tuesday, June 29, 2021 1:40 PM
To: John Rowe; Paul Pelton; Tony Sprinkle
Cc: Tim Naulty;Van Powell; Neal Shinault
Subject: FW: Updated Quote
Attachments: Weiland_Quote 062821.pdf
Paul/John,
Thanks for revising.
We are pleased to announce that WCP has accepted your bid. It appears all terms (50%,at PO,40%after 10/1, and 10%
upon completion)and conditions(contractor rebate)are correct so I will send this over to our purchasing department.
We look forward to working with you further and appreciate the expedited response.We have already issued PO for the
resin tanks and are on track with our end of the project.
Van,
Please add this PO to the waste water project capex.
Best regards I Freundliche GrOge,
Jared Ranken
Environmental Health &Safety Director
Jared.RankenC&wieland.com
Wieland Copper Products,LLC 1 3990 US 311 Hwy N I Pine Hall NC, NC 27042 1 USA
wieland.com
Linkedln Twitter Facebook youtube Instagam
Please consider the environment before printing this email
From:John Rowe [mailto:[e-mail]]
Sent:Tuesday,June 29, 2021 12:51 PM
To:Jared Ranken <[e-mail]>;Tony Sprinkle<[e-mail]>
Cc: Paul Pelton <[e-mail]>
Subject: RE: Updated Quote
C AUTiON: This email originated from outside of the organization VVieland. Do not click links or open attachments unless
you recognize the sender and know the content is safe. Sender address is: iohnrowe((Dsouthernvalveservice.com
Please find the attached quote. In addition to the summary price change, note the paragraph after the price summary
for a potential rebate we have extended.
John Rowe
1

M
will be constantly agitated while the system is running the floats are likely to get beat up and not really where we would
suggest saving money. Same with several of the other parts, we can go and try to find cheaper components but we've
dealt with the companies we've suggested for many years and feel its not the cheapest but good quality items that will
last for years. If we need to look for other areas of saving we can certainly try and scale back on some of those items.
Items to remove from SVS scope
and become Wieland's scope Price from SVS
Control System Start up $ 12,000.00
Plumbing $ 17,000.00
Electrical $ 28,800.00
Total Labor $ 57,800.00
Parts Dollars remove/change
Replace Radar Probes with Floats $ 4,400.00
Controls to Honeywell vs Siemens $ 6,000.00
Discount on other parts $ 3,188.00
Total Parts $ 13,588.00
Total Dollars $ 71,388.00
Previous Quote $ 267,784.00
Updated Quote Amount $ 196,396.00
Please look this over and if its something you want to move forward with I will revise the quote and send it back to
you. I didn't want to make this many changes without discussing first as it gets a little complicated if we are pulling
items out and then putting them back in. Let me know how I can help further and please call Paul or myself with any
questions.
John Rowe
Southern Valve Et Service, Inc
Southern . Va/ane'
& Service
704-900-9920
312 Crosstown Dr. Suite 188
Peachtree City, Georgia 30269
http://www.southernvalveservice.com
3

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h1AR 2 2022
Effluent Aquatic Toxicity Report Form t Phase II Chronic Ceriodaphnia
Facility: Wieland NPDES:# NC00 35173 Pipe#: 003 County: Stokes
Laboratory Performing Test: Meritech, Inc. (Lab#NCO27) Comments:Test terminated on 10/22/21 due
v (� to 100% mortality in all test concentrations
_ -_within 48 hours of test initiation.
Signature of O.R.CIPhone#IE-mail Address Signature of Laboratory Supervisor
Sample Information Sample 1 Sample 2 Control r_asl. Start Date I End Date I Stad Time End Time
Collection Stan Dale
10/19/21 nmrmaror 10/20/21 10/22/21 12:22 PM 1!30 PM
snot Rw.l Renew2 Slart 110.1 Rw.2
Grab Treatment 100 % % % Control Contrd condor
Composite
(Ouraroni 10.7 pri Initial 7A4 8.05
Hardness(mgf) 48
pH Final 8.60 7.99
D.O.Initial 7.77 7.88
Spec,Cone.(pmhoslcm) 714 162 D.o.Final 6.99 7.07
Chlorine(mg/I) <0,1 emp.Instal 24.4 24.4
0 Sample temp.at receipt 0.2 C 0 C Temp.Final 24.3 24.4
Organism# Chronic Test Results
1 2 3 4 5 6 7 8 9 10 11 12 Mears Final Control Modality%
Control #Young 0 0 0 0 0 0 0 0 0 0 %Control 3rd brood
Adult L L L L L L L L L I L Control Repro CV
(L)Ive(D)ead 48 Hour Modality
Control two
1 2 3 4 5 6 7 8 9 10 11 12 Mean 0 of 10 10 of 10
Effluent'/° #Young 0 0 0 0 0 0 () 0 0 0 9
Si nifcanl7 Y N
Aadt D D D D D D D D D D Al
Final Mortality Significant Q
11.25 LJive(0)aad
1 t.25 °/ of No Conc.
1 2 3 4 5 6 7 8 9 10 Mea
Reproduction Analysis:
Effluent% #Young 0 0 0 0 0 0 0 0 0 0 Repro.LOEC= %; NOEC= %
yaw
22.5 Lpve Dead D D D D D D D D D D MCNoorrmalDisirb7_ Method
1 2 3 4 5 6 7 8 9 10 won statistic: Critical:
Effluent%
#Young � Equal Variances?_ Method:
0 0 0 0 0 0 0 0 0 0 Statistic critkal —
Atlult nnr°
45 L)ive(D)ead D D D D D D D D D D Non-Parametric Analysis(ifapDlicableh
Method:
1 2 3 4 5 6 7 8 9 10 Mean Effluent nt° Rank Sum Critical Sum
Effluent% #Young 0 0 0 0 0 0 0 0 0 0
Adult D D D D D D D D D DH
90 L)Ive(D)eatl
1 2 3 4 5 6 7 8 9 10 Meer
verall Analysis:
ENluent°!° #Yo
100 un O
9 0 0 0 0 0 0 0 0 0 0 Result=PASSIFAIL or
Aauit D D D D D D D D D D Aaw Test LOEC= 11.25 %; NOEC= <11.25 %
L)iw(D)caa
Chronic Value= <11.25 %
ATTt Water Sciences Stetson Should use highest test concentration or highest
MAIL Aquaucloxicology Breach concentration with D.O. 5.0 mgn
Division of\Paler Resources t Reeuomn from Comro1 Roprotl<nw Mean
T
Page 18 0125

h 71 � tSf CtSlnCa / h���lee.' C ON,' U/VI
Effluent Aquatic Toxicity Report Form/ Phase II Chronic Ceriodaphnia
Facility: Wieland NPDES:# NC00 35173 Pipe#: 003 County: Stokes
Laboratory Performing Test: Meritechh,,7lnc.(Lab#NCCJ027)/ Comments:
x x
Signature of O.R.C/Phone#/E-mail Address Signature of Laboratory Supervisor
Sample information Samples Sample Control Ifni Start Dale End Dale Stan Time End Time
Collection Start Date
12/13/21 12/15/21 "m°'i° 12/15/21 12I22/21 10:02AM 9:38AM
start Renewl Re.2 Sind Renews Remw2
Grab Treatment 100 % 100 % 100 % Control Control Control
Composite
(Nmunrl 24.0 24.0 pH Initial 8.19 7.97 8.17 7.97 8.01 7.90
Hardness(mgA) 46 46 pH Final 8.28 8.66 8.42 7.76 8.20 7.95
D.O,Initial B.42 8.21 8.03 8.37 7.93 8.19
Spec.Cond.(pmhoalcm) 569 60,9 159 165
O.O.Final 7.85 8.35 7.78 8.02 8.21 7.90
Chlorine(mgA) <0.1 <0.1 Temp.Initial 24.9 24.6 24.7 24.3 24.3 24,5
Sample temp.at receipt 0.3 dC 0.4 dC Temp,Final 24.9 24,6 25.0 24.7 24.4 24.8
Organism# Chronic Test Results
1 2 3 4 5 6 7 8 9 10 11 12 mean Final Control Mortality% 0
Control #Young %Control 3rd brootl 100
23 25 26 28 27 26 24 24 24 23 z5.o
Aanu L I L I L I L I L I L I L I L I L I L Control Repro CV 6.8
(L1ivo(0)ead 48 Hour Mortality
Conlrot IWC
1 2 3 4 5 6 7 8 9 10 11 12 mean 0 Of 10 0 of 10
Effluent% #Young 26 1 21 26 25 1 24 24 1 25 28 1 24 25 1 24.8 Significant? Y N
Adult 1111 Final Mortality Significant@
11.25 (L)ive(01ead L L L L L L L L L L 0e , or No Conc
1 2 3 4 5 6 7 8 9 10 mean Reoroduction Analysis:
Effluent% #Young 23 1 22 20 22 24 24 26 1 22 23 24 23.0 Repro..LOEC= 45 %; NOEL= 22.5 %
Adm1 L L L L L L L L L L ve`a Method ounneu's rest
22,5 (L)iva(Dlaad 6.0 Normal Distrib? YES Method Kolmogorov
1 2 3 4 5 6 7 8 9 10 Mean Statistic: 0.6250 Critical. 1.035
Effluent% #YoungEqual Variances? YES Method: earthen
24 21 23 23 22 22 22 23 22 22H22.4 statistic: 11.83= Cntiw T�0g-
Adull 45 (L)Ive(D)ead L L L L L L L L L L Non-Paramet cAnalvsis(if applicable)
Method:
1 2 3 4 5 6 7 8 9 10 Mean Effluent% Rank Sum Critical Sum
Effluent?/6 #Young 18 16 17 22 18 16 20 18 19 13ne0 17.7
Adult
90 L)ive(D)ead L L L L L L L L L L 2e2
1 2 3 4 5 6 7 8 9 10 Mean
Overall Analysts:
Effluent% #Young 7 7 5 10 11 10 14 11 7 7 8.9 Result=PASS/FAIL or
Aamt L L L D L D L L L D .n,a TestLOEC= 90 /; NOEL= 45 %
1l)f) (give(D)ead 644
Chronic Value- 63.6 %
ATT; Waler Sciences Seedon - Shovld use highest test concentration or highest
MAIL %quatic Toxicology Branch concentration with D.O.-5.0 mgn
Division fir\Yale•Resources 1 R°Cuenon h°m Ca41°1 R°yedv.ii°n moan
TO: 1621 Mail Semice Center Page 18 of 30
Itslcigb.N.C.27699.1621 DWO form AT-3 (8191)Rev.11195

arc• �/c �/ C,c./ern -j y} Pz-/"Ykli,4'7A�C7
.! � �4� i,C✓}yi.. f'`i1 / � `/i"'� � )� 1JF't'� ��(dl G"�� 1 - -S�l.����...r..- `�� SU4j--3
Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia (fir-LE_ /L/ C 4 j4� `
Facility: Wieland NPDES:# NC00 35173 Pipe#: 003 County: Stokes Ct,4-a'
Laboratory Performing Test: Meritech,Inc.(Lab#NCO27) Comments: Yl fr`
Signature of O.R.CIPhone WE-mail Address Signature of Laboratory Supervisor �n
Sample Information Sample 1 Sample 2 Control rest Start Date End Dale SlartTime End Time 'r .
Collection Start Date
1/24/22 1/26/22 Oars 1/26122 2/2/22 11:45AM 1002AM
sign Rur.l Ranen2 Start RanewI R..2
Grab Treatment too % too % 100 % Control Control Control
Composite
(Duration) 24.0 24.0 rill Initial 7.66 8A3 8.22 8.09 8.11 7.62
Hardness(mgn) 46 46 pit Final 8.30 8.50 8.44 7.99 8.06 7.98
D.O.Initial 8.50 8.49 8.49 8.35 8,18 8.01
Spec.Cond.(pmhoslcm)E2461 596 158 157D.O.Final BOi 8.27 8.03 8.10 8.24 8.12
Chlorine(mga) <0.1 temp.trival 24.4 24.7 24.9 24.8 24.7 24.7
Sample temp.at receipt 0.2 pC Temp.Final 242 24.2 24.3 24.3 24.3 25.0
Ornanlsm# Chronic Test Results
1 2 3 4 5 6 7 8 9 10 11 12 moan Final Control Mortality% 0
Control #Young 21 22 22 23 24 24 22 22 21 26 22.7 %Control 3rd brood 100
Admt Control Repro CV 6.9
(ume(D)ead L L L L L L L L L L 48 Hour Mortality
Control IWC
1 2 3 4 5 6 7 8 9 10 11 12 maw 0 of 10 0 of 10
Etnuent% #Young 20 20 22 22 23 24 23 24 24 23 H2. 9Si ntfcantl Y NAr Dt L L L L L L L L L L Final Mortality Significant@
give(D)ead
or No Conc
1 2 3 4 5 6 7 8 9 10 mom
Reproduction Analysis:
Effluent% #Young 23 21 23 22 24 1 23 24 24 25 23 23.2 Repro.LOEC= 90 %; NOEC= 45 %
Adult ' °a Method: Steel's Many-One Rank Test
22.5 (L)Ive(Diesel L L L L L L L L L L ,Y 2 Normal Dlslrib7 NO Method* Kotmo9orov
1 2 3 4 5 6 7 8 9 10 war, Statistic: 1.3204 CdGeal: 1.035
Effluent% #Young Equal Variances? NO Method: 83Nelt
16 23 19 23 20 18 19 22 23 22 20.5 Statistic: 54.46= cotiwc�3-
Adult Rm
45 yive(plead L L L L L L L L L L a l Non-Parametric Analysis(if aoplicableY
Method:Steel's Many-one Rank Test
1 2 3 4 5 6 7 8 9 10 moan Effluent% Rank Sum Critical Sum
11.25 106.5 75.0
Effluent% #Young 2 20 17 3 4 18 21 20 23 21 14.9 -2=
Adult n •^ 45 82. 75.0
90 (L)we(D)ead L L L D L L L L L L 3a 4 45 -63 5- 75o
1 2 3 4 5 6 7 8 9 10 moan 100 55.0 75.0
Effluent°/a #Yours Overall Analysis:
9 3 13 19 20 16 5 17 8 18 17 13.6 Result=PASSIFAIL or
Adult `"" Test LOEC- 90 %; NOEC- 45 %
100 L) a(0)eatl D L L L L L L L L L 4011 63.6 %
Chronic Value=
ATT: Water Sciences Section Should use highest lest concentration or highest
MAIL Aquatic'roxlcology Rranch concentration with D.O >5o moll
111vislne orWri(cr Resources r Radvclla,from Cwtrol R,,:rud crcn lean
TO: 1621\tail SciNlee Center Page 11 of 22
Raleigh,N.C.27699-1621 DWO form AT-3 (8191)Rev. 11195

p�T �ce Pace Analytical Services,LLC
PaceAnaiyticai R pp..� �r f"1'� 1377 South Park Drive n W It= tl Kemersville,NC 27284
www.pacelabs.com MAR 2 8 2022 [phone]
Page 1 of 9
Wail r Sciences ydCf10p
Laboratory Report
Tony Sprinkle Report Date: 09/09/2021
Wieland Copper Products Date Received: 08/26/2021
3990 US 311 Hwy North
Pine Hall, NC 27042
Project: Wieland-Tank Study
Pace Project No.:92557925
Sample: Wleland Tanks(Top) Lab ID: 92557925001 Collected: 08/26/21 09:00 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 245.1 Mercury NO ug/L 0.20 09107/2113:34
EPA 200.7 Rev 4.4 1994 Antimony NO ug/L 5.0 09/0812120:36
EPA 200.7 Rev 4.41994 Arsenic NO ug/L 10.0 09/08/2120:36
EPA 200.7 Rev 4.41994 Barium 28.9 ug/L 5.0 09/0812120:35
EPA 200.7 Rev 4.41994 Beryllium NO ug/L 1.0 09/0812120:35
EPA 200.7 Rev 4.41994 Cadmium NO ug/L 1.0 09/0812120:35
EPA 200.7 Rev 4.41994 Chromium NO ug/L 5.0 09/08/2120:35
EPA 200.7 Rev 4.4 1994 Copper 116 ug/L 5.0 09108/21 20:35
EPA 200.7 Rev 4.41994 Iron 56.3 ug/L 50.0 09/08t2120:35
EPA 200.7 Rev 4.4 1994 Lead NO ug/L 5.0 09108121 20:35
EPA 200.7 Rev 4.41994 Manganese NO ug/L 5.0 09/0812120:36
EPA 200.7 Rev 4.41994 Nickel NO ug/L 5.0 09/0812120:36
EPA 200.7 Rev 4.41994 Selenium NO ug/L 10.0 09/0812120:36
EPA 200.7 Rev 4.41994 Silver NO ug/L 5.0 09/08/2120:35
EPA 200.7 Rev 4.41994 Sodium 40500 ug/L 5000 09/08/2120:35
EPA 200.7 Rev 4.41994 Thallium NO ug1L 10.0 09108/2120:35 BC
EPA 200.7 Rev 4.4 1994 Zinc 10.8 ug1L 10.0 09/08/21 20:35
EPA 8270E Acenaphlhene NO ug/L 10.0 08131/2114:12
EPA 8270E Acenaphthylene NO ug/L 10.0 08131/2114:12
EPA 8270E Aniline ND ug/L 10.0 08/31/2114:12
EPA 8270E Anthracene NO ug/L 10.0 08/3112114:12
EPA 8270E Benzo(a)anthracene NO ugli- 10.0 0813112114:12
EPA 8270E Benzo(a)pyrene NO ug1L 10.0 08/31/2114:12
EPA 8270E Benzo(b)Buoranthene NO ug1L 10.0 08/31/2114:12
EPA 8270E Benzo(g,h,i)perylene NO ug/L 10.0 0813112114:12
EPA 8270E Benzo(k)fiuoranthene NO ug/L 10.0 08/3112114:12
EPA 8270E Benzoic Acid NO ug/L 50.0 08/31/2114:12
EPA 8270E Benzyl alcohol NO ug/L 20.0 08/31121 14:12
EPA 8270E 4-Bromophenylphenyl ether NO ug/L 10.0 0813112114:12
EPA 8270E Bulylbenzylphlhalate NO ug/L 10.0 0813l/2114:12 v1
EPA 8270E 4-Chloro-3-melhylphenol NO ug/L 10.0 08/31/2114:12
EPA 8270E 4-Chloroaniline NO ug/L 20.0 08/31/2114:12
EPA 8270E bis(2-Chloroethoxy)methane NO ug/L 10.0 08/3112114:12
EPA 8270E bis(2-Chloroethyl)ether NO ug/L 10.0 0813112114:12
EPA 8270E 2-Chloronaphthalene NO ug/L 10.0 08/31/2114:12
EPA 8270E 2-Chlorophenol NO ug/L 10.0 08/3112114:12
EPA 8270E 4-Chlorophenylphenyl ether NO ug/L 10.0 0813112114:12
EPA 8270E Chrysene NO ug/L 10.0 0813112114:12
EPA 8270E Dibenz(a,h)anthracene NO ug/L 10.0 08/31/2114:12
EPA 8270E Dibenzofuran NO ug/L 10.0 08/31/2114:12
EPA 8270E 1,2-Dichlorobenzene NO ug/L 10.0 Dat3112114:12
EPA 8270E 1,3-Dichlorobenzene NO ug/L 10.0 08131/21 14:12 Page 1 of 18

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Sample: Wieland Tanks(Top) Lab ID: 92567925001 Collected: 08/26/21 09:00 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 8270E 1,4-Dichlorobenzene NO ug/L 10.0 011/31/2114:12
EPA 8270E 3,3'-Dichlorobenzidine NO ug/L 20.0 08/3112114:12
EPA 8270E 2,4-Dichlorophenol NO ug/L 10.0 08/31/2114:12
EPA 8270E Diethylphthalate NO ug/L 10.0 08/31/2114:12
EPA 8270E 2,4-Dimelhylphenol NO ug/L 10.0 08/31/2114:12
EPA 8270E Dimethylphlhalate NO ug/L 10.0 08/31/2114:12
EPA8270E Di-n-butylphthalate NO ug/L 10.0 08/3112114:12
EPA 8270E 4,6-Dinitro-2-methylphenol NO ug/L 20.0 08/31/2114:12
EPA 8270E 2,4-Dlnitrophenol NO ug/L 50.0 08/31/2114:12
EPA 8270E 2,4-Dinitrotoluene NO ug1L 10.0 08/31/2114:12
EPA 8270E 2,6-Dinitrotoluene NO ug/L 10.0 08131/2114:12
EPA 8270E Di-n-octylphthalate NO ug/L 10.0 OB/31/2114:12
EPA 8270E bis(2-Ethylhexyl)phthalate NO ug/L 6.0 08/31/2114:12
EPA 8270E Fluoranthene NO ug/L 10.0 08/3112114:12
EPA 8270E Fluorene NO ug/L 10.0 08/3112114:12
EPA 8270E Hexachloro-1,3-butadiene NO ug/L 10.0 08131/2114:12
EPA 8270E Hexachlorobenzene NO ug/L 10.0 0813112114:12
EPA 8270E Hexachlorocyclopentadiene NO ug/L 10.0 0813112114:12
EPA 8270E Hexachloroethane NO ug/L 10.0 08/31/2114:12
EPA 8270E Indeno(1,2,3-cd)pyrene NO ug/L 10.0 08/31/2114:12
EPA 8270E Isophorone NO ug/L 10.0 08131/2114:12
EPA 8270E 1-Methylnaphthalene NO ug/L 10.0 08/31/2114:12
EPA 8270E 2-Methylnaphthalene NO ug/L 10.0 08131/2114:12
EPA 8270E 2-Methylphenol(c-Cresol) NO ug/L 10.0 08131/2114:12
EPA 8270E 3&4-Methylphenol(m&p Cresol) NO ug/L 10.0 08131/2114:12
EPA 8270E Naphthalene NO ug/L 10.0 08131/2114:12
EPA 8270E 2-Nitroaniline NO ug/L 20.0 08131/2114:12
EPA 8270E 3-Nitroaniline NO ug/L 20.0 08/3112114:12
EPA 8270E 4-Nitroaniline NO ug/L 20.0 08131/2114:12
EPA 8270E Nitrobenzene NO ug/L 10.0 08131/2114:12
EPA 8270E 2-Nitrophenol NO ug/L 10.0 08131/2114:12
EPA 8270E 4-Nitrophenol NO ug/L 50.0 0813112114:12
EPA 8270E N-Nitrosodimethylamine NO ug/L 10.0 08/3112114:12
EPA 8270E N-Nilroso-di-n-propylamine NO ug/L 10.0 08/31/2114:12
EPA 8270E N-Nitrosodiphenylamine NO ug/L 10.0 08/31/2114:12
EPA 8270E 2,2'-Oxybis(1-chloropropane) ND ug/L 10.0 08/3112114:12
EPA 8270E Pentachlorophenol NO ug/L 20.0 08/3112114:12
EPA 8270E Phenanthrene NO ug/L 10.0 08/31/2114:12
EPA 8270E Phenol NO ug1L 10.0 08/31/2114:12
EPA 8270E Pyrene NO uglL 10.0 08131/2114:12
EPA 8270E 1,2,4-Trichlorobenzene NO ug/L 10.0 0813112114:12
EPA 8270E 2,4,5-Trichlorophenol NO ug/L 10.0 08/3112114:12
EPA 8270E 2,4,6-Trichlorophenol NO ug/L 10.0 08131/2114:12
EPA 8260D Acetone NO ug/L 25.0 08/31/2109:15
EPA 8260D Benzene NO ug/L 5.0 08131/2109:15
EPA 8260D Bromobenzene NO ug/L 5.0 08131/2109:15
EPA 8260D Bromochloromelhane NO ug/L 5.0 08131/2109:15
EPA 8260D Bromodichloromethane NO ug/L 5.0 08/3112109:16
EPA 8260D Bromoform NO ug/L 5.0 08/3112109:16
EPA 8260D Bromomethane NO ug/L 10.0 08/31/2109:15
EPA 8260D 2-Butanone(MEIQ NO ug/L 10.0 08/31/2109:15
EPA8260D tert-Butyl Alcohol NO ug/L 100 08/3112109:15
EPA 8260D n-Butylbenzene NO ug/L 5.0 08/31/2109:15
EPA 8260D sec-Butylbenzene NO ug/L 5.0 08131/2109:15
EPA 8260D tert-Butylbenzene NO ug/L 5.0 08131/2109:15
EPA 8260D Carbon tetrachloride NO ug/L 5.0 08131/2109:15
EPA 8260D Chlorobenzene NO ug/L 5.0 08/31/2109:15
EPA 8260D Chloroethane NO ug/L 10.0 08131/21 09:15 Page 2 of 18

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Sample: Wieland Tanks(Top) Lab ID: 92557925001 Collected: 08/26/21 09:00 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 8260D Chloroform ND ug/L 5.0 08131/2109:15
EPA 8260D Chloromethane ND ug/L 6.0 08/31/2109:15
EPA8260D 2-Chlorololuene ND ug/L 5.0 08/3112109:15
EPA8260D 4-Chlorololuene ND ug/L 5.0 08/31/2109:16
EPA 8260D 1,2-Dibromo-3-chloropropane ND ug/L 5.0 08131/2109:15
EPA 82600 Dibromochloromethane ND ug/L 5.0 08/31/2109:15
EPA 8260D 1,2-Dibromoethane(EDB) ND ug/L 5.0 08131/2109:15
EPA 8260D Dibromomelhane ND ug/L 5.0 08131/2109:15
EPA 8260D 1,2-Dichlorobenzene ND uglL 5.0 08/31/2109:15
EPA 8260D 1,3-Dichlorobenzene ND ug/L 5.0 08/3112109:15
EPA8260D 1,4-Dichlorobenzene ND ug/L 5.0 08/31/2109:15
EPA 8260D Dichlorodifluoromethane ND ug/L 5.0 08/31/2109:15
EPA 8260D 1,1-Dichloroethane ND ug/L 5.0 0513112109:15
EPA 8260D 1,2-Dichloroelhane ND ug/L 5.0 0813112109:15
EPA8260D 1,2-Dichloroelhene(Total) ND ug1L 5.0 08/3112109:15
EPA 8260D 1,1-Dichloroethene ND ug/L 5.0 08/3112109:15
EPA 8260D cis-1,2-Dichloroethene ND ug/L 5.0 08131/2109:15
EPA 8260D trans-1,2-Dichloroethene ND ug/L 5.0 08131/2109:15
EPA 8260D 1,2-Dichloropropane ND ug/L 5.0 08/31/2109:15
EPA 8260D 1,3-Dichloropropane ND ug/L 5.0 0813112109:15
EPA 8260D 2,2-Dichloropropane ND uglL 5.0 0813112109:15
EPA 8260D 1,1-Dichloropropene ND ug/L 5.0 0813112109:15
EPA 8260D cis-1,3-Dichloropropene ND ug/L 5.0 0813112109:15
EPA 8260D trans-1,3-Dichloropropene ND ug/L 5.0 08/31/2109:15
EPA8260D Diisopropyl ether ND ug/L 5.0 08/31121 09:15
EPA8260D Ethylbenzene ND uglL 5.0 08/31/2109:15
EPA 8260D Hexachloro-1,3-butadiene ND uglL 5.0 08/31/2109:15
EPA 8260D 2-Hexanone ND ug/L 10.0 0813112109:15
EPA 8260D Isopropylbenzene(Cumene) ND ug/L 5.0 08/31/2109:15
EPA 8260D p-Isopropylloluene ND ug/L 5.0 08/31/2109:15
EPA 8260D Methylene Chloride ND ug/L 5.0 08/31/2109:15
EPA 8260D 4-Methyl-2-pentanone(MIBK) ND ug/L 10.0 08/31/2109:15
EPA 8260D Methyl4ert-butyl ether ND ug/L 5.0 0813112109:15
EPA 82600 Naphthalene ND uglL 5.0 0813112109:15
EPA 82600 n-Propylbenzene ND ug1L 5.0 0813112109:15
EPA 8260D Styrene ND uglL 5.0 08/31/2109:15
EPA 8260D 1.1,1,2-Tetrachloroethane ND ug1L 5.0 08/31/2109:15
EPA 8260D 1,1,2,2-Tetrachloroethane ND ug/L 5.0 Oat3l/2109:15
EPA 8260D Tetrachloroethene ND ug/L 5.0 0813112109:15
EPA8260D Toluene ND ug/L 5.0 08/31/2109:15
EPA 8260D 1,2,3-Trichlorobenzene ND ug/L 5.0 08/31/2109:15
EPA8260D 1,2,4-Trichlorobenzene ND ug/L 5.0 08131/2109:15
EPA 8260D 1,1,1-Trichlorcethane ND ug/L 5.0 08131/2109:15
EPA 8260D 1,1,2-Trichloroelhane ND ug/L 5.0 0813112109:16
EPA 8260D Tichooroethene ND ug/L 5.0 08/3112109:15
EPA 8260D Trichlorofluoromethane ND ug/L 10.0 08/31/2109:16
EPA 8260D 1,2,3-Trichloropropane ND ug/L 5.0 OB/31/2109:15
EPA 8260D 1,2,4-Trimethylbenzene ND ug/L 5.0 08/3112109:15
EPA 8260D 1,3,5-Trimethylbenzene ND ug/L 5.0 08/31/2109:15
EPA8260D Vinyl acetate ND ug/L 10.0 08131/2109:15 v1
EPA 8260D Vinyl chloride ND ug/L 5.0 OW31/2109:15
EPA 8260D m&p-Xylene ND ug/L 10.0 08131/2109:15
EPA 8260D o-Xylene ND ug/L 5.0 08131/2109:15
SM 4500-H+B-2011 pH at 25 Degrees C 8.6 Sid Units 0.10 09/05/21 14:28 H3
EPA 300.0 Rev 2.1 1993 Chloride 17.9 mg/L 1.0 09/D4/21 02:32
EPA 300.0 Rev 2.1 1993 Fluoride 0.48 mg/L 0.10 09/04121 02:32
EPA 300.0 Rev 2.1 1993 Sulfate 11.6 mg/L 1.0 09/04121 02:32
SM 4500-CN-E-2011 Cyanide ND mg/L 0.0080 09/08121 13:15 Page 3 of 18

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Page 4 of 9
Sample: Wieland Influent Lab ID: 92557925002 Collected: 08(26121 09:30 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 245.1 Mercury NO ug/L 0.20 09/0712113:45
EPA 200.7 Rev 4.41994 Antimony NO ug/L 5.0 09/0812120:38
EPA 200.7 Rev 4.41994 Arsenic NO ug/L 10.0 09/08/2120:38
EPA 200.7 Rev 4.41994 Barium 5.3 ug/L 5.0 09/08/2120:38
EPA 200.7 Rev 4.41994 Beryllium NO ug/L 1.0 09/0812120:38
EPA 200.7 Rev 4.41994 Cadmium NO ug/L 1.0 09/0812120:38
EPA 200.7 Rev 4.41994 Chromium NO ug/L 5.0 09/0812120:38
EPA 200.7 Rev 4.41994 Copper 44.1 ug/L 5.0 09/0812120:38
EPA 200.7 Rev 4.41994 Iron 236 ug/L 50.0 09/08/2120:38
EPA 200.7 Rev 4.41994 Lead NO ug/L 5.0 09/0812120:38
EPA 200.7 Rev 4.41994 Manganese NO ug/L 5.0 09/0812120:38
EPA 200.7 Rev 4.41994 Nickel NO ug/L 5.0 09/0812120:38
EPA 200.7 Rev 4.41994 Selenium NO ug/L 10.0 09/08/2120:38
EPA 200.7 Rev 4.41994 Silver NO ug/L 5.0 09/0812120:38
EPA 200.7 Rev 4.41994 Sodium 67200 ug/L 5000 09/08/2120:38
EPA 200.7 Rev 4.4 1994 Thallium NO ug/L 10.0 09/0812120:38 BC
EPA 200.7 Rev 4.4 1994 Zinc 23.8 ug/L 10.0 09/08/21 20:38
EPA 8270E Acenaphthene NO ug/L 9.1 08/31/2114:38
EPA 8270E Acenaphthylene NO ug/L 9.1 08/31/2114:38
EPA 8270E Aniline NO ug/L 9.1 08/31121 14:38
EPA 8270E Anthracene NO ug/L 9.1 08/31121 14:38
EPA 8270E Benzo(a)anthracene NO ug/L 9.1 08/31/2114:38
EPA 8270E Benzo(a)pyrene NO ug/L 9.1 08/31/2114:38
EPA 8270E Benzo(b)fluoranthene NO ug/L 9.1 08/31/2114:38
EPA 8270E Benzo(g,h,i)perylene NO ug/L 9.1 08/31121 14:38
EPA 8270E Benzo(k)fluoranthene NO ug/L 9.1 0813112114:38
EPA 8270E Benzoic Acid NO ug/L 45.5 0813112114:38
EPA 8270E Benzyl alcohol NO ug/L 18.2 08131/2114:38
EPA 8270E 4-Bromophenylphenyl ether NO ug/L 9.1 08/31121 14:38
EPA 8270E Butylbenzylphlhalate NO ug/L 9.1 OS/3112114:38 v1
EPA 8270E 4-Chloro-3-methylphenol NO ug/L 9.1 OB/3112114:38
EPA 8270E 4-Chloroaniline NO ug/L 18.2 08/31121 14:38
EPA 8270E bis(2-Chloroethoxy)methane NO ug/L 9.1 08/31121 14:38
EPA 8270E bis(2-Chloroethyl)ether NO ug/L 9.1 08/31/2114:38
EPA 8270E 2-Chloronaphthalene NO ug/L 9.1 08131/2114:38
EPA 8270E 2-Chlorophenol NO ug/L 9.1 08131/2114:38
EPA 8270E 4-Chlorophenylphenyl ether NO ug/L 9.1 08131/2114:38
EPA 8270E Chrysene NO ug/L 9.1 08131/2114:38
EPA 8270E Dibenz(a,h)anthracene NO ug/L 9.1 08/31/2114:38
EPA 8270E Dlbenzofuran NO ug/L 9.1 08/31/2114:38
EPA 8270E 1,2-Dichlorobenzene NO ug/L 9.1 0013112114:38
EPA 8270E 1,3-Dichlorobenzene NO ug/L 9.1 0813112114:38
EPA8270E 1,4-Dichlorobenzene NO ug/L 9.1 08/31/2114:38
EPA 8270E 3,3'-Dichlorobenzidine NO ug/L 18.2 08131/2114:38
EPA 8270E 2,4-Dichlorophenol ND ug/L 9.1 08/31/2114:38
EPA 8270E Diethylphthalate NO ug/L 9.1 08/31/2114:38
EPA 8270E 2,4-Dimethylphenol NO ug/L 9.1 08131/2114:38
EPA 8270E Dimelhylphthalate NO ug/L 9.1 08131/2114:38
EPA 8270E Di-n-butylphthalate NO ug/L 9.1 08/31/2114:38
EPA 8270E 4,6-Dinitro-2-methylphenol NO ug/L 18.2 08/31/2114:38
EPA 8270E 2,4-Dinitrophenol NO ug/L 45.5 08/31121 14:38
EPA 8270E 2,4-Dinitrotoluene NO ug/L 9.1 08/31121 14:38
EPA 8270E 2,6-Dinitrotoluene NO ug/L 9.1 08/31121 14:38
EPA 8270E DI-n-octylphthalate NO ug/L 9.1 08/31121 14:38
EPA 8270E bis(2-Ethylhexyl)phthalate NO ug/L 5.5 0813112114:38
EPA 8270E Fluorarlthene NO ug/L 9.1 08/31121 14:38
EPA 8270E Fluorene NO ug/L 9.1 08/31/2'114:38
EPA 8270E Hexachloro-1,3-butadiene NO ug/L 9.1 01313112114:38 Page of 18

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Sample: Wieland Influent Lab ID: 92557925002 Collected: 08/26/21 09:30 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 8270E Hexachlorobenzene NO ug/L 9.1 06/3112114:38
EPA 8270E Hezachlorocyclopentadiene NO ug/L 9.1 08/3112114:38
EPA 8270E Hexachloroethane NO ug/L 9.1 08131/2114:38
EPA8270E Indeno(1,2,3-cd)pyrene NO ug/L 9.1 08131/2114:38
EPA 8270E Isophorone NO ug/L 9.1 08/3112114:38
EPA 8270E 1-Melhylnaphthalene NO ug/L 9.1 08/31/2114:38
EPA8270E 2-Methylnaphthalene NO ug/L 9.1 0813112114:38
EPA 8270E 2-Methylphenol(o-Cresol) NO ug/L 9.1 08131/2114:38
EPA 8270E 3&4-Methylphenol(m&p Cresol) NO ug/L 9.1 0813112114:38
EPA 8270E Naphthalene NO ug/L 9.1 0813112114:38
EPA 8270E 2-Nitroaniline NO ug/L 18.2 08/3112114:38
EPA 8270E 3-Nitroaniline NO ug/L 18.2 08/3112114:38
EPA 8270E 4-Nitroaniline NO ug/L 18.2 08/3112114:38
EPA 8270E Nitrobenzene NO ug/L 9.1 08/3112114:38
EPA 8270E 2-Nltrophenol NO ug/L 9.1 08/3l/2114:38
EPA 8270E 4-Nitrophenol NO ug/L 45.5 08/31/2114:38
EPA 8270E N-Nitrosodimethylamine NO ug/L 9.1 08131/2114:38
EPA 8270E N-Nitroso-di-n-propylamine NO ug/L 9.1 08/3112114:38
EPA 8270E N-Nitrosodiphenylamine NO ug/L 9.1 0813112114:38
EPA 8270E 2,2'-Oxybis(1-chloropropane) NO ug/L 9.1 08/31/2114:38
EPA 8270E Pentachlorophenol NO ug/L 18.2 08131/2114:38
EPA 8270E Phenanthrene NO ug/L 9.1 0813112114:38
EPA 8270E Phenol NO ug/L 9.1 08/3112114:38
EPA 8270E Pyrene NO ug/L 9.1 08/3112114:38
EPA8270E 1,2,4-Trichlorobenzene NO ug/L 9.1 08/3112114:38
EPA8270E 2,4,5-Trichlorophenol NO ug/L 9.1 08131/2114:38
EPA 8270E 2,4,6-Trichlorophenol NO ug/L 9.1 08131/2114:38
EPA 8260D Acetone NO ug/L 25.0 08131/2109:33
EPA 8260D Benzene NO ug/L 5.0 08131/2109:33
EPA 8260D Bromobenzene NO ug/L 5.0 08/31/2109:33
EPA8260D Bromochloromethane NO ug/L 5.0 08131/2109:33
EPA 8260D Bromodichloromethane NO ug/L 6.0 0813112109:33
EPA 8260D Bromoform NO ug/L 5.0 08131/2109:33
EPA 8260D Bromomethane NO ug/L 10.0 08/3112109:33
EPA8260D 2-Butanone(MEK) NO ug/L 10.0 0813112109:33
EPA8260D tert-Butyl Alcohol NO ug/L 100 08131/2109:33
EPA 82600 n-Butylbenzene NO ug/L 5.0 08131/2109:33
EPA 8260D sec-Butylbenzene NO ug/L 5.0 0813112109:33
EPA 8260D tert-Butylbenzene NO ug/L 5.0 08/3112109:33
EPA 8260D Carbon tetrachloride NO ug/L 5.0 08131/2109:33
EPA 8260D Chlorobenzene NO ug/L 5.0 0813112109:33
EPA 8260D Chloroethane NO ug/L 10.0 08/31/2109:33
EPA 8260D Chloroform NO ug/L 5.0 08/3112109:33
EPA 8260D Chloromethane NO ug/L 5.0 08/31/2109:33
EPA 8260D 2-Chlorotoluene NO ug/L 5.0 OB131/2109:33
EPA 8260D 4-Chlorotoluene NO ug/L 5.0 08131/2109:33
EPA 8260D 1,2-Dibromo-3-chloropropane NO ug/L 5.0 08/31/2109:33
EPA 8260D Dibromochloromethane NO ug/L 5.0 08131/2109:33
EPA 8260D 1,2-Dibromoethane(EDB) NO ug/L 5.0 08/31/2109:33
EPA 8260D Dibromomethane NO ug/L 5.0 08/31/2109:33
EPA8260D 1,2-Dichlorobenzene NO ug/L 5.0 08/3112109:33
EPA8260D 1,3-Dichlorobenzene NO ug/L 5.0 08131/2109:33
EPA 8260D 1,4-Dichlorobenzene NO ug/L 5.0 08131/2109:33
EPA8260D Dichlorodifluoromethane NO ug/L 5.0 08131/2109:33
EPA 8260D 1,1-Dichloroethane NO ug/L 5.0 08/3112109:33
EPA8260D 1,2-Dichloroethane NO ug/L 5.0 08131/2109:33
EPA 8260D 1,2-Dichloroethene(Total) NO ug/L 5.0 0813112109:33
EPA 8260D 1,1-Dichloroethene NO ug/L 5.0 08/31/21 09:33 Page 5 of 18

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Page 6 of 9
Sample: Wieland Influent Lab ID: 92557925002 Collected: 08/26/21 09:30 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA8260D cis-1,2-Dichloroethene ND ug/L 5.0 08131/2109:33
EPA 8260D trans-1,2-Dichloroethene ND ug/L 5.0 0813112109:33
EPA 8260D 1,2-Dichloropropane NO ug/L 5.0 08131/2109:33
EPA8260D 1,3-Dichloropropane NO ug/L 5.0 08/31/2109:33
EPA 8260D 2,2-Dichloropropane NO ug/L 5.0 08131/21 09:33
EPA 8260D 11-Dichloropropene NO ug/L 5.0 08/3112109:33
EPA 8260D cis-1,3-Dichloropropene NO ug/L 5.0 08131/2109:33
EPA 8260D trans-1,3-Dichloropropene NO ug/L 5.0 08/31/2109:33
EPA 8260D Diisopropyl ether NO ug/L 5.0 08/31/2109:33
EPA8260D Ethylbenzene NO ug/L 5.0 08131/2109:33
EPA 8260D Hexachloro-1,3-butadiene NO ug/L 5.0 08131/2109:33
EPA 8260D 2-Hexanone NO ug/L 10.D 0813112109:33
EPA 8260D Isopropylbenzene(Cumene) NO ug/L 5.0 08/31/2109:33
EPA 8260D p-Isopropyltoluene NO ug/L 5.0 08/31/2109:33
EPA 8260D Methylene Chloride NO ug/L 5.0 08/31/2109:33
EPA 8260D 4-Methyl-2-pentanone(MIBK) NO ug/L 10.0 08/31/2109:33
EPA 8260D Methyl-tert-butyl ether NO ug/L 5.0 08(31/2109:33
EPA 8260D Naphthalene NO ug/L 5A 08/31/2109:33
EPA 8260D n-Propylbenzene NO ug/L 5.0 08131/2109:33
EPA 8260D Styrene NO ug/L 5.0 08/3112109:33
EPA 8260D 1,1,1,2-Tetrachloroethane NO ug/L 5.0 08/31I2109:33
EPA 8260D 1,1,2,2-Tetrachloroethane ND ug/L 5.0 08/3112109:33
EPA 8260D Tetrachloroethene NO ug/L 5.0 0813112109:33
EPA 8260D Toluene NO ug/L 5.0 0813112109:33
EPA 8260D 1,2,3-Tdchlorobenzene NO ug/L 5.0 OB/31I2109:33
EPA 8260D 1,2,4-Trichlorobenzene NO ug/L 5.0 0813112109:33
EPA 8260D 1,1,1-Tdchloroethane NO ug/L 5.0 08131/2109:33
EPA 8260D 1,1,2-Trchloroethane ND ug/L 5.0 08131/2109:33
EPA 8260D Trichloroethene ND ug/L 5.0 08/31/2109:33
EPA 8260D Trichlorofluoromethane NO ug/L 10.0 08/3112109:33
EPA 8260D 1,2,3-Trichloropropane NO ug/L 5.0 08/3112109:33
EPA 8260D 1,2,4-Tdmethylbenzene NO ug/L 5.0 08/3112109:33
EPA 8260D 1,3,5-Trimethylbenzene NO ug/L 5.0 08/3112109:33
EPA 8260D Vinyl acetate NO ug/L 10.0 08/31/2109:33 v1
EPA 8260D Vinyl chloride NO ug/L 5.0 08/312109:33
EPA 8260D m&p-Xylene NO ug/L 10.0 08/31/2109:33
EPA 8260D o-Xylene NO ug/L 5.0 08131/2109:33
SM 4500-H+B-2011 pH at 25 Degrees C 8.6 Std.Units 0.10 09/05/21 14:34 H3
EPA 300.0 Rev 2.1 1993 Chloride 17.6 mg/L 1.0 09104121 02:47
EPA 300.0 Rev 2.1 1993 Fluoride 0.46 mg/L 0.10 09I0421 02:47
EPA 300.0 Rev 2.1 1993 Sulfate 10.8 mg/L 1.0 09/04121 02:47
SM 4500-CN-E-2011 Cyanide NO mg/L 0.0080 09/08121 13:16
Sample: Wieland Effluent Lab ID: 92557925003 Collected: 08126/21 10:00 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 245.1 Mercury NO ug/L 0.20 09107/2113:48
EPA 200.7 Rev 4.41994 Antimony NO ug/L 5.0 09/08/2120:42
EPA 200.7 Rev 4.41994 Arsenic NO ug/L 10.0 09/0812120:42
EPA 200.7 Rev 4.41994 Barium 26.1 ug/L 5.0 09/08/2120:42
EPA 200.7 Rev 4.41994 Beryllium NO ug/L 1.0 09/0812120:42
EPA 200.7 Rev 4.41994 Cadmium ND ug/L 1.0 09/0812120:42
EPA 200.7 Rev 4.41994 Chromium ND ug/L 5.0 09/0812120:42
EPA 200.7 Rev 4.4 1994 Copper 127 ug/L 5.0 09100121 20:42
EPA 200.7 Rev 4.41994 Iron 104 ug/L 50.0 0910812120:42
EPA 200.7 Rev 4.4 1994 Lead NO ug/L 5.0 09108121 20:42
EPA 200.7 Rev 4.4 1994 Manganese ND ug/L 5.0 09/08/21 20:42
EPA 200.7 Rev 4.41994 Nickel NO ug/L 5.0 09/082120:42
EPA 200.7 Rev 4.4 1994 Selenium NO ug/L 10.0 09/0821 20:42 Page 6 of 18

Pace Analytical Services,LLC
aceAnalytical 1377 South Park Drive
Kemersville,NC 27284
www.pacelabs.cam [phone]
Page 7 of 9
Sample: Wieland Effluent Lab ID: 92557925003 Collected: 08126/21 10:00 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 200.7 Rev 4.41994 Silver ND ug/L 5.0 09/08/2120;42
EPA 200.7 Rev 4.4 1994 Sodium 39500 ug/L 5000 09/08121 20:42
EPA 200.7 Rev 4.41994 Thallium ND ug/L 10.0 09/08/2120:42 BC
EPA 200.7 Rev 4.41994 Zinc ND ug/L 10.0 09/08/21 20:42
EPA 8270E Acenaphthene ND ug/L 8.3 08/31/2115:05
EPA 8270E Acenaphlhylene ND ug/L 8.3 08/3112115:05
EPA 8270E Aniline ND ug/L 8.3 08/31/2115:05
EPA 8270E Anthracene ND ug/L 8.3 08131/2115:05
EPA 8270E Benzo(a)anthracene ND ug/L 8.3 0813112115:05
EPA 8270E Benzo(a)pyrene ND ug/L 8.3 08/3112115:05
EPA8270E Benzo(b)Suoranthene ND ug/L 8.3 0813112115:05
EPA 8270E Benzo(g,h,i)perylene ND ug/L 8.3 08/31/2115:05
EPA 8270E Benzo(k)Buoranthene ND ug/L 8.3 0813112115:05
EPA8270E Benzoic Acid ND ug/L 41.7 08/3112115:05
EPA 8270E Benzyl alcohol ND ug/L 16.7 08131/2115:05
EPA 8270E 4-Bromophenylphenyl ether ND ug/L 8.3 08131/2115:05
EPA 8270E Butylbenzylphlhalate ND ug/L 8.3 08/31/2115:05 v1
EPA 8270E 4-Chloro-3-melhylphenol ND ug/L 8.3 08/31/2116:06
EPA 8270E 4-Chloroaniline ND ug/L 16.7 08/31/2115:05
EPA 8270E bis(2-Chloroethoxy)methane ND uglL 8.3 0813112115:05
EPA 8270E bis(2-Chloroethyl)ether ND ug/L 8.3 08131/2115:05
EPA 8270E 2-Chloronaphthalene ND ug/L 8.3 08131/2115:05
EPA 8270E 2-Chlorophenol ND ug/L 8.3 0813112115:05
EPA 8270E 4-Chlorophenylphenyl ether ND ug/L 8.3 08131/2115:05
EPA8270E Chrysene ND ug/L 8.3 08/31/2115:05
EPA 8270E Dibenz(a,h)anthracene ND ug/L 8.3 08/31/2116:05
EPA 8270E Dibenzofuran ND uglL 8.3 0813112115:06
EPA 8270E 1,2-Dichlorobenzene ND ug/L 8.3 OB131/2115:05
EPA8270E 1,3-Dichlorobenzene ND ug/L 8.3 08131/2115:05
EPA8270E 1,4-Dichlorobenzene ND ug/L 8.3 0813112115:05
EPA 8270E 3,3'-Dichlorobenzidine ND ug/L 16.7 08131/2115:05
EPA 8270E. 2,4-Dichlorophenol ND ug/L 8.3 08/31/2115:05
EPA 8270E Diethylphthalate ND ug/L 8.3 08/3112115:05
EPA 8270E 2,4-Dimelhylphenol ND uglL 8.3 08/31/2115:05
EPA 8270E Dimethylphthalate ND ug/L 8.3 08/3112115:05
EPA 8270E Di-n-bulylphthalate ND ug/L 8.3 08/31/2115:05
EPA 8270E 4,6-Dinitro-2-methylphenol ND ug/L 16.7 08131/2115:05
EPA8270E 2,4-Dinitrophenol ND ug/L 41.7 0813112115:05
EPA827GE 2,4-Dinitrotoluene ND ug/L 8.3 08/31/2115:05
EPA 8270E 2,6-Dinitrotoluene ND ug/L 8.3 08131/2115:05
EPA 8270E Di-n-octylphthalale ND ug/L 8.3 0813112115:05
EPA 8270E bis(2-Ethylhexyl)phthalate ND ug/L 5.0 0813112115:05
EPA 8270E Fluoranthene ND ug/L 8.3 08131/2115:05
EPA 8270E Fluorene ND ug/L 8.3 0813112115:05
EPA 8270E Hexachloro-1,3-butadiene ND ug/L 8.3 08/31/2115:05
EPA 8270E Hexachlorobenzene ND ug/L 8.3 08/31/2115:05
EPA 8270E Hexachlorocyclopentadiene ND ug/L 8.3 0813112115:05
EPA 8270E Hexachloroethane ND ug/L 8.3 08131/2116:06
EPA 8270E Indeno(1,2,3-cd)pyrene ND ug/L 8.3 00131/2115:05
EPA 8270E Isophorone ND ug/L 8.3 08131/21 15:05
EPA 8270E 1-Melhylnaphthalene ND ug/L 8.3 08/3112115:05
EPA 8270E 2-Methylnaphlhalene ND ug/L 8.3 08/31/2115:06
EPA 8270E 2-Methylphenol(o-Cresol) ND ug/L 8.3 08/3112115:05
EPA 8270E 3&4-Methylphenol(m&p Cresol) ND ug/L 8.3 0813112116:05
EPA 8270E Naphthalene ND ug/L 8.3 08131/2115:05
EPA 8270E 2-Nitroaniline ND ug/L 16.7 08131/2115:05
EPA8270E 3-Nitroaniline ND ug/L 16.7 0813112115:05
EPA 8270E 4-Nitroaniline ND ug/L 16.7 08131/21 15:05 Page 7 of 18

Pace Analytical Services,LLC
ace '" 1377 South Park Drive
Analytical m Keeisville,NC 27284
III ww.paceas.ccm
' lb [phone]
Page 8 of 9
Sample: Wieland Effluent Lab ID: 92557925003 Collected: 08/26/21 10:00 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 8270E Nitrobenzene NO ug/L 8.3 0813112115:05
EPA 8270E 2-Nilrophenol NO ug/L 8.3 08131/2116:05
EPA 8270E 4-Nilrophenol NO ug/L 41.7 08131/2116:06
EPA 8270E N-Nilrosodimethylamine NO ug/L 8.3 0813112115:05
EPA 8270E N-Nilroso-di-n-propylamine NO ug/L 8.3 08131/2116:05
EPA 8270E N-Nilrosodiphenylamine NO ug/L 8.3 08/3112115:05
EPA 8270E 2,2'-Oxybis(1-chloropropane) NO ug/L 8.3 08/3112116:05
EPA 8270E Pentachlorophenol NO ug/L 16.7 08/31121 15:05
EPA 8270E Phenanthrene NO ug/L 8.3 08/3112116:06
EPA 8270E Phenol NO ug/L 8.3 08/3l/2115:05
EPA 8270E Pyrene NO ug/L 8.3 08/31I2115:05
EPA 8270E 1,2,4-Tdchlorobenzene NO ug/L 8.3 08131/2115:05
EPA 8270E 2,4,5-Trichlorophenol NO ug/L 8.3 08/31/2115:06
EPA 8270E 2,4,6-Trichlorophenol NO ug/L 8.3 08131/2116:06
EPA 8260D Acetone NO ug/L 25.0 08131/2109:61
EPA 8260D Benzene NO ug/L 5.0 0813112109;51
EPA8260D Bromobenzene NO ug/L 5.0 08131/2109:51
EPA 8260D Bromochloromethane NO ug/L 5.0 0a/3112109:51
EPA 8260D Bromodichloromethane NO ug/L 5.0 08/3112109:51
EPA 8260D Bromoform NO ug1L 5.0 0813112109:51
EPA 8260D Bromomelhane NO ug/L 10.0 08/31I2109:51
EPA8260D 2-Butanone(MEK) NO ug/L 10.0 08131/2109:51
EPA8260D tert-Butyl Alcohol NO ug/L 100 0813l/2109:51
EPA 8260D n-Butylbenzene NO ug/L 5.0 0813l/2109:51
EPA 8260D sec-Butylbenzene NO ug/L 5.0 08/31/2109:51
EPA 8260D tert-Buylbenzene NO ug/L 5.0 08131/2109:51
EPA 8260D Carbon tetrachloride NO ug/L 6.0 0813112109:51
EPA 8260D Chlorobenzene NO ug/L 5.0 08/3112109:51
EPA 8260D Chloroethane NO ug/L 10.0 08/31/2109:51
EPA 8260D Chloroform NO ug/L 5.0 0813112109:51
EPA 8260D Chloromethane NO ug/L 5.0 0813l/2109:51
EPA 8260D 2-Chlorotoluene NO ug/L 5.0 08/31I2109:61
EPA 8260D 4-Chlorotoluene NO ug/L 5.0 0813l/2109:51
EPA 8260D 1,2-Dibromo-3-chloropropane NO ug/L 5.0 08131/2109:51
EPA 8260D Dibromochloromethane NO ug/L 5.0 08131/2109:51
EPA8260D 1,2-Dibromoethane(EDB) NO ug/L 5.0 08131/2109:51
EPA 8260D Dibromomethane NO ug/L 5.0 08f31t2l 09:51
EPA 8260D 1,2-Dlchlorobenzene NO ug/L 5.0 08/31009:51
EPA 8260D 1,3-Dlchlorobenzene NO ug/L 5.0 08/31/2109:51
EPA 8260D 1,4-Dichlorobenzene NO ug/L 5.0 08(31/2109:51
EPA 8260D Dichlorodifluoromethane NO ug/L 5.0 08/31/2109:51
EPA 8260D 1,1-Dichloroethane NO ug/L 5.0 08/31/2109:51
EPA 8260D 1,2-Dichloroethane NO ug/L 5.0 08131/2109:51
EPA8260D 1,2-Dichloroethene(Total) NO ug/L 5.0 08/31/2109:61
EPA 8260D 1,1-Dichloroethene NO ug/L 5.0 08/31/2109:51
EPA 8260D cis-1,2-Dichloroethene NO ug/L 5.0 08/31/2109:61
EPA 8260D trans-1,2-Dichloroethene NO ug/L 5.0 O8/3l/2109:51
EPA8260D 1,2-Dichloropropane NO ug/L 5.0 OBI31I2109:51
EPA8260D 1,3-Dichloropropane NO ug/L 5.0 08131/2109:51
EPA 8260D 2,2-Dichloropropane NO ug/L 5.0 08131/2109:51
EPA 8260D 1,1-Dichloropropene NO ug/L 5.0 08131/2109:51
EPA8260D cis-1,3-Dichloropropene NO ug/L 5.0 08131/2109:51
EPA 8260D trans-1,3-Dichloropropene NO ug/L 5.0 08/31/2109:51
EPA 8260D Diisopropyl ether NO ug/L 5.0 08/3112109:51
EPA 8260D Ethylbenzene NO ug/L 5.0 08131/2109:51
EPA 8260D Hexachloro-1,3-butadiene NO ug/L 5.0 08/31/2109:51
EPA8260D 2-Hexanone NO ug/L 10.0 080/2109:51
EPA 82600 Isopropylbenzene(Cumene) NO ug/L 6.0 08131/21 09:51 Page 8 of 18

Pace Analytical Services,LLC
,aceAnalytical 377 South Park Drive
Kemersv7 27284
www.DBcolabS.com (704)97977-0981
Page 9 of 9
Sample: Wieland Effluent Lab ID: 92557925003 Collected: 08126/21 10:00 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 8260D p-Isopropyltoluene NO ug/L 5.0 08/3112109:51
EPA 8260D Methylene Chloride NO ug/L 5.0 08131/21 09:51
EPA 8260D 4-Methyl-2-pentanone(MIBK) NO ug/L 10.0 08/31/2109:61
EPA8260D Methyl-tert-butyl ether NO ug/L 5.0 08/3112109:51
EPA 8260D Naphthalene NO ug/L 5.0 08/31/2109:51
EPA 82600 n-Propylbenzene NO ug/L 5.0 0813112109:51
EPA 8260D Styrene NO ug/L 5.0 08/31/2109:61
EPA 82600 1,1,1,2-Tetrachloroethane NO ug/L 5.0 08/31/2109:51
EPA 8260D 1,1,2,2-Tetrachloroelhane NO ug/L 5.0 08/3112109:51
EPA 8260D Tetrachloroethene NO ug/L 5.0 08131/2109:51
EPA 8260D Toluene NO ug/L 5.0 08/31/2109:51
EPA 8260D 1,2,3-Trichlorobenzene NO ug/L 5.0 0813112109:51
EPA 8260D 1,2,4-Trichlorobenzene NO ug/L 5.0 0813112109:51
EPA8260D 1.1.1-Trichloroethane ND ug/L 5.0 08/3112109:61
EPA8260D 1.1,2-Trichloroethane NO ug/L 5.0 08/31/2109:61
EPA 8260D Trichloroethene NO ug/L 5.0 08131/2109:51
EPA 8260D Trichloro8uoromethane NO ug/L 10.0 0813112109:51
EPA 8260D 1,2,3-Trichloropropane NO ug/L 5.0 0813112109:51
EPA 8260D 1,2,4-Trimethylbenzene NO ug/L 5.0 08/31/2109:51
EPA8260D 1,3,5-Trimethylbenzene NO ug/L 5.0 08/3112109:51
EPA 8260D Vinyl acetate NO ug/L 10.0 08/3l/2109:51 vt
EPA 8260D Vinyl chloride NO ug/L 5.0 OW31121 09:51
EPA 8260D m&p-Xylene NO ug/L 10.0 08/31/2109:51
EPA8260D o-Xylene NO ug/L 5.0 08/31/2109:51
SM 4500-H+B-2011 pH at 25 Degrees C 8.2 Sid.Units 0.10 09105/21 14:40 06,1-13
EPA 300.0 Rev 2.1 1993 Chloride 54.8 mg/L 1.0 09/04/21 03:02
EPA 300.0 Rev 2.1 1993 Fluoride 0.40 mg/L 0.10 09104/21 03:02
EPA 300.0 Rev 2.1 1993 Sulfate 11.1 mg/L 1.0 09/04/21 03:02
SM 4500-CN-E-2011 Cyanide NO mg/L 0.0080 09/08/21 13:17
ANALYTE QUALIFIERS
BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
vl The continuing calibration verification was above the method acceptance limit.Any detection for the analyte in the
associated samples may have a high bias.
Reviewed by:
Stephanie Knott
704-977-0981
[e-mail]
Pace Analytical Services Charlotte
9800 Kincey Ave.Ste 100,Hunlersville,NC 28078 South Carolina Certification#:99006001
Louisiana/NELAP Certification#LA170028 Florida/NELAP Certification#:E87627
North Carolina Drinking Water Certification#:37706 Kentucky UST Certification#:84
North Carolina Field Services Certification#:5342 Virginia/VELAP Certification#:460221
North Carolina Wastewater Certification#:12
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 North Carolina Wastewater Certification#:40
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 VlrginialVELAP Certification#:460222
Pace Analytical Services Peachtree Corners
110 Technology Pkwy,Peachtree Corners,GA 30092 North Carolina Certification#:381
Florida DOH Certification#:E87315 South Carolina Certification#:98011001 Page 9 of 18
Georgia DW Inorganics Certification#:812

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— Page 11 of 18

Sample Receipt Form
Pace Analytical Services, LLC (�5ace Analytical
Charlotte www.yaceleb.cam
Login Summary
Workorder: 92557925 Client Work ID: Wieland-Tank Study
Report Version: SHRT Client: Wieland Copper
Min Sample Due: 09/10/2021 19:00 Profile: 14597
Max Sample Due: 09/10/2021 19:00 Profile Desc: Waste Water
Report
Lab ID Sample ID Collected Received Matrix Properties Location Due Date
92557925001 Wieland Tanks(Top) 08/26/21 09:00 08/26/21 15:08 WT PTR NC 09/10/21
92557925002 Wieland Influent 08/26/21 09:30 08/26/21 15:08 WT PTR NC 09/10/21
92557925003 Wieland Effluent 08/26/21 10:00 08/26/21 15:08 WT PTR NC 09/10/21
Pay
ag
Thursday,August 26,2021 3:55:25 PM e 1 of 7

Sample Receipt Form
Pace Analytical Services, LLC aceAnalj&al®
Charlotte mvi pcmabssam
Charge Summary
Workorder: 92557925 Bill To: Accounts Payable
Client PO: 4509020553 Wieland Copper Products LLC
A/R Acct: 92-620434 3990 US 311 Hwy North
Tax Status: Nonexempt,Sales Tax May Apply Pine Hall,NC 27042
Invoice CC:
Text to appear on Invoice:
Oty Unit Description Cmps Method Matrix Price Total
3 Ea 200.7 ICP Metals 16 EPA 200.7 Rev 4.4 Water $100.00 $300.00
3 Ea 245.1 Mercury 1 EPA 245.1 Rev 3.0 Water $25.00 $75.00
3Ea 300.0 IC Anions 4 EPA 300.0 Rev 2.1 Water $50.00 $150.00
3 Ea 4500CNE Cyanide,Total 1 SM 4500-CN-E-2011 Water $40.00 $120.00
3 Ea 4500H+B pH,Electrometric 1 SM 4500-H+8-2011 Water $12.50 $37.50
3 Ea 8260D MSV 68 EPA 8260D Water $110.00 $330.00
3 Ea 8270E RVE 68 EPA8270E Water $226.00 $675.00
Total before Taxes: $1,687.50
Estimated Tax(0.00%): $0.00
Grand Total: $1,687.50
Thursday,August 26,2021 3:55:25 PM age 200

Sample Receipt Form
Pace Analytical Services, LLC (!1a'ceAna1yfica1'
Charlotte wuw.racelataxam
Sample Acknowledgement Recipients: Bill to:
Wieland Copper Products Wieland Copper Products LLC
Tony Sprinkle Accounts Payable
3990 US 311 Hwy North 3990 US 311 Hwy North
Pine Hall,NC 27042 Pine Hall,NC 27042
Email:[e-mail] Email:[e-mail]
Wieland Copper Products LLC Final Report Recipients:
Accounts Payable Wieland Copper Products
3990 US 311 Hwy North Tony Sprinkle(Primary)
North
Pine Hall,NC 27042 Pine al 311 Hwy 42
Email:[e-mail] Pine Hall, ,s 27042
Email:[e-mail]
Cliff Cain Wieland Copper Products LLC
Accounts Payable
3990 US 311 Hwy North
Pine Hail,NC 27042
Email:[e-mail]
Email:[e-mail]
Cliff Cain
Email:[e-mail]
Line Item Descriptions:
[10)Tank Study
Client P O No: 4509020553 Lab Project No: 92557925
Phone: [phone] Project Deliverables Type: Standard Report
Project Manager. Stephanie Knott Project Report Due Date: 09/10/21
Client Project to: Wieland-Tank Study Profile: 14597(Autoreleased)
Automated EDD
EDD* FR Only no EDD(0) -
Publish or Review?: Publish(P)
Email Client?: Yes(Y)
Include FR?: Yes(Y)
Auto Invoice: No,do not auto invoice(N)
Email Invoice?: No,do not auto email(N)
Print Final Invoice7: No,do not print invoice(N)
Multiple EDD#2: FR Only no EDD(0)
Multiple EDD#3: FR Only no EDD(0)
Multiple EDD#4: FR Only no EDD(0)
Multiple EDD#5: FR Only no EDD(0)
Lab Smp 10: 92657926001 Client Smp ID: Wieland Tanks(Top) Collected: 08/26121 09:00
Proj Smp No: 1 Matrix:Water Type: PS Line Item: 10 Lab: Received: 08/26/21 15:08
Location: NC
PARAMETER METHOD EARLIEST HOLD UNIT PRICE WR SPL %
2007 W-200.7 ICP Metals EPA 200.7 Rev 4.4 02/22/22 23:59 $100.00
COMPOUND MDL ID PQL ID UNITS
Antimony 3 87692 5 9310 ug/L
Arsenic 4.7 87692 10 9310 ug/L
Barium 3.4791 87692 5 9310 ug/L
Beryllium 0.7027 87692 1 9310 ug/L
Cadmium 0.4 87692 1 9310 ug/L
Chromium 3.6585 87692 5 9310 ug/L
Copper 4.2552 87692 5 9310 ug/L
Thursday,August 26,2021 3:55:26 PM age 3 of

Sample Receipt Form
y (�15'ceAnalytical
Pace Analytical Services, LLC
Charlotte www.penlitimam
PARAMETER METHOD EARLIEST HOLD UNIT PRICE WR SPL %
COMPOUND MDL ID PQL ID UNITS
Iron 41.5142 87692 50 9310 ug/L
Lead 4.5325 87692 5 9310 ug/L
Manganese 3.4313 87692 5 9310 ug/L
Nickel 3.467 87692 5 9310 ug/L
Selenium 4.7 87692 10 9310 ug/L
Silver 2.5 87692 5 9310 ug/L
Sodium 610.6842 87692 5000 9310 ug/L
Thallium 8.1465 87692 10 9310 ug/L
Zinc 9.4505 87692 10 9310 ug/L
Compound Count: 16
2451 W92.245.1 Mercury EPA 245.1 Rev 3.0 09/23/21 23:59 $25.00
Compound Count: 1
3000 W28-300.0 IC Anions EPA 300.0 Rev 2.1 09/23/21 23:59 $50.00
Compound Count: 4
450OCNEWZ-4500CNE Cyanide,Total SM 4500-CN-E-2011 09/09/21 23:59 $40.00
Compound Count: 1
4500H+B-4500H+B pH,Electrometric SM 4500-H+B-2011 08126/21 09:15 $12.50
Compound Count 1
8260D W-8260D MSV EPA8260D 09/09/21 23:59 $110.00
Compound Count: 68
8270E RV-8270E RVE EPA 8270E 09/02/21 23:59 $225.00
Compound Count: 68
Sub Total-Sample 3375811 $562.50
Lab Smp ID: 92567925002 Client Smp ID: Wieland Influent Collected:08/26/21 09:30
Prol Smp No: 2 Matrix:Water Type: PS Line Item: 10 Lab: Received:08/26/21 15:08
Location: NC
PARAMETER METHOD EARLIEST HOLD UNIT PRICE WR SPL %
2007 W-200.7 ICP Metals EPA 200.7 Rev 4.4 OZ22/22 23:59 $100,00
COMPOUND MDL ID PQL ID UNITS
Antimony 3 87692 5 9310 ug/L
Arsenic 4.7 87692 10 9310 ug/L
Barium 3.4791 87692 5 9310 ug/L
Beryllium 0.7027 87692 1 9310 ug/L
Cadmium 0.4 87692 1 9310 ug/L
Chromium 3.6585 87692 5 9310 ug/L
Copper 4.2552 87692 5 9310 ug/L
Iron 41.5142 87692 50 9310 ug/L
Lead 4.5325 87692 5 9310 ug/L
Manganese 3.4313 87692 5 9310 ug/L
Nickel 3,467 87692 5 9310 ug/L
Selenium 4.7 87692 10 9310 ug/L
Silver 2.5 87692 5 9310 ug/L
Sodium 610.6842 87692 5000 9310 ug/L
Thallium 8.1465 87692 10 9310 ug/L
Zinc 9.4505 87692 10 9310 ug/L
Compound Count: 16
2451 W92-245.1 Mercury EPA 245.1 Rev 3.0 09/23/21 23:59 $25.00
Thursday,August 26,2021 3:55:26 PM 54 of e

Sample Receipt Form
Pace Analytical Services, LLC aceAnalytical
Charlotte www.vaedaba.com
PARAMETER METHOD EARLIEST HOLD UNIT PRICE WR SPL %
Compound Count: 1
3000 W28-300.01C Anions EPA 300.0 Rev 2.1 0912312123:59 $50.00
Compound Count: 4
4500CNEW2-4500CNE Cyanide,Total SM 4500-CN-E-2011 09/09/21 23:59 $40.00
Compound Count: 1
4500H+B-4500H+B pH,Electrometric SM 4500-H+B-2011 08/26/21 09:45 $12.50
Compound Count: 1 -,
8260D W-8260D MSV EPA 8260D 09/09/21 23:59 $110.00
Compound Count: 68
8270E RV-8270E RVE EPA 8270E 09/02/21 23:59 $225.00
Compound Count: 68
Sub Total-Sample 3376814 $562.50
Lab Smp ID: 92557925003 Client Smp ID: Wieland Effluent Collected:08/26/21 10:00
Proj Smp No: 3 Matrix:Water Type: PS Line Item: 10 Lab: Received:08/26/21 15:08
Location: NC
PARAMETER METHOD EARLIEST HOLD UNIT PRICE WR SPL %
2007 W-200.7 ICP Metals EPA 200.7 Rev 4.4 02/22/22 23:59 $100.00
COMPOUND MDL ID PQL ID UNITS
Antimony 3 87692 5 9310 ug/L
Arsenic 4.7 87692 10 9310 ug/L
Barium 3.4791 87692 5 9310 ug/L
Beryllium 0.7027 87692 1 9310 ug/L
Cadmium 0.4 87692 1 9310 ug/L
Chromium 3.6585 87692 5 9310 ug/L
Copper 4.2552 87692 5 9310 ug/L
Iron 41.5142 87692 50 9310 ug/L
Lead 4.5325 87692 5 9310 ug/L
Manganese 3.4313 87692 5 9310 ug/L
Nickel 3.467 87692 5 9310 ug/L
Selenium 4.7 87692 10 9310 ug/L
Silver 2.5 87692 5 9310 ug/L
Sodium 610.6842 87692 5000 9310 ug/L
Thallium 8.1465 87692 10 9310 ug/L
Zinc 9.4505 87692 10 9310 ug/L
Compound Count: 16
2451 W92-245.1 Mercury EPA 245.1 Rev 3.0 09/23/21 23:59 $25.00
Compound Count: 1
3000 W28-300.0 IC Anions EPA 300.0 Rev 2.1 09/23121 23:59 $50.00
Compound Count: 4
4500CNEW2-4600CNE Cyanide,Total SM 4500-CN-E-2011 09/09/21 23:59 $40.00
Compound Count: 1
4500H+B-4500H+B pH,Electrometric SM 4500-H+B-2011 08/26121 10:15 $12.50
Compound Count: 1
8260D W-8260D MSV EPA 8260D 09/09/21 23:59 $110,00
Compound Count: 68
8270E RV-8270E RVE EPA 8270E 09/02/21 23:59 $225.00 aq
Thursday,August 26,2021 3:55:29 PM Page 5 of 7

Sample Receipt Form
Pace Analytical Services, LLC aceAnalXieal
Charlotte www.pacelebs.eum
PARAMETER METHOD EARLIEST HOLD UNIT PRICE WR SPL %
Compound Count: 68
Sub Total-Sample 3375815 $562.50
Total Before Taxes-Project $1.687.50
Estimated Tax(0.00%) $0.00
Unit Pricing above does not reflect associated shipping,bottle,sample disposal and other miscellaneous charges. Prices
are subject to change without notice. Contact your Project Manager for further information.
P% e76 ffif
Thursday,August 26,2021 3:55:33 PM 9

Sample Receipt Forma
Pace Analytical Services, LLC aceAnalytical
Charlotte Y riY.p8C9109920 9
Containers
Lab ID Container ID Type Location Utilization
92567925001 92557925001 AGOU1/2 AGOU Charlotte 8270E RV
92557925001 AGOU2/2 AGOU Charlotte
92557926001 BPIUI/1 BP1U Asheville 3000 W28,4500H+B
92557925001 BP3N1/2 BP3N Asheville 2007 W
92557925001 BP3N2/2 BP3N Asheville 2451 W
92557926001 BP4C111 BP4C Asheville 450OCNEW2
92557925001 DG91-11/3 DG91-1 Charlotte 8260D W
92557925001 DG9H2/3 DG9H Charlotte
92657925001 DG9H3/3 DG9H Charlotte
92557925002 92557925002 AGOU1/2 AGOU Charlotte 8270E RV
92557925002 AGOU2/2 AGOU Charlotte
92557925002 BPI U111 BP1U Asheville 3000W28,4500H+B
92557925002 BP3N1/2 BP3N Asheville 2007 W
92557925002 BP3N2/2 BP3N Asheville 2451 W
92557925002 BP4C1/1 BP4C Asheville 450OCNEW2
92557925002 DG91-1113 DG91-1 Charlotte 8260D W
92557925002 DG91-12/3 DG91-1 Charlotte
92657925002 DG91-13/3 DG91-1 Charlotte
92557925003 92557925003AGOU12 AGOU Charlotte 8270E RV
92557925003 AGOU22 AGOU Charlotte
92557925003 BPI U1/1 BP11J Asheville 3000 W28,4500H+B
92557925003 BP3N1/2 BP3N Asheville 2007 W
92557925003 BP3N2/2 BP3N Asheville 2451 W
92567925003 BP4C1/1 BP4C Asheville 450OCNEW2
92557925003 DG9H1/3 DG9H Charlotte 8260D W
92557925003 DG91-12/3 DG9H Charlotte
92557925003 DG9H3/3 DG9H Charlotte
Thursday,August 26,2021 3:55:33 PM gage 7oof

RECEIVED Pace Analytical Services,LLC
1377 South Park Drive
.,/l•-.,FaceAnalytical Kemeraville,NC 27294
i wmpecelabs.com MAR 2 S 2022 [phone]
Page 1 of 3
�nlcf�Ci2flr�'9S Soctivn
Laboratory Report
Tony Sprinkle Report Date: 03/17/2022
Wieland Copper Products Date Received: 03/03/2022
3990 US 311 Hwy North
Pine Hall, NC 27042
Project: Wieland-PPA
Pace Project No.:92591318
Sample: 003-Comp Lab ID: 92591318001 Collected: 03102/2205:00 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
SM 254OC-2011 Total Dissolved Solids 308 mg/L 25.0 03/07/22 13:01
EPA 350.1 Rev 2.0 1993 Nitrogen,Ammonia 0.16 mg/L 0.10 03/10/22 10:45
EPA 200.7 Rev 4.4 1994 Hardness,Total(SM 2340B) 152000 ug/L 662 03/15/22 11:43
EPA 200.8 Rev 5.4 Antimony NO ug/L 1.0 03/15/22 20:38
EPA 200.8 Rev 5.4 Arsenic 1.2 ug/L 1.0 03/15/22 20:38
EPA 200.8 Rev 5.4 Beryllium NO ug/L 0.10 03/15/22 20:38
EPA 200.8 Rev 5.4 Cadmium NO ug/L 0.20 03/15/22 20:38
EPA 200.8 Rev 5.4 Chromium NO ug/L 1.0 03/16/22 20:38
EPA 200.8 Rev 5.4 Copper 11.6 ug/L 2.0 03/15/22 20:38
EPA 200.8 Rev 5.4 Lead NO ug/L 1.0 03/15/22 20:38
EPA 200.8 Rev 5.4 Nickel 1.0 ug/L 1.0 03/15/22 20:38
EPA 200.8 Rev 5.4 Selenium NO ug/L 2.0 03/15/22 20:38
EPA 200.8 Rev 5.4 Silver NO ug/L 0.40 03/15/22 20:38
EPA 200.8 Rev 5.4 Thallium NO ug/L 0.47 03/15/22 20:38
EPA 200.8 Rev 5.4 Zinc 15.2 ug/L 10.0 03/15/22 20:38
EPA 351.2 Rev 2.0 1993 Nitrogen,IGeldahl,Total ND mg/L 0.50 03/16/22 03:47
EPA 353.2 Rev 2.0 1993 Nitrogen,NO2 plus NO3 0.28 mg/L 0.040 03/16/22 15:00
EPA 365.1 Rev 2.01993 Phosphorus 1.3 mg/L 0.050 03115/2212:10
Sample: 003-Grab Lab ID: 92591318002 Collected: 03/02/22 13:10 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 1664B Oil and Grease NO mg/L 5.0 03107/22 09:23
EPA 625.1 Acenaphthene NO ug/L 4.2 03110/2202:38
EPA 625.1 Acenaphlhylene NO ug/L 4.2 03/10/2202:38
EPA 625.1 Arlthracene NO ug/L 4.2 03110/2202:38
EPA 625.1 Benzidine NO ug/L 41.7 03/102202:38 IL
EPA 625.1 Benzo(a)anthracene NO ug/L 4.2 0311012202:38
EPA 625.1 Benzo(a)pyrene NO ug/L 4.2 0311012202:38
EPA 625.1 Benzo(b)fluoranthene ND ug/L 4.2 03110/2202:38
EPA 625.1 Benzo(g,h,i)perylene NO ug/L 4.2 03110/2202:38
EPA 625.1 Benzo(k)fluoranthene NO ug/L 4.2 03110/2202:38
EPA 625.1 4-Bromophenylphenyl ether NO ug/L 4.2 03/10122 02:38
EPA 625.1 Butylbenzylphthalate NO ug/L 4.2 03/102202:38
EPA 625.1 4-Chloro-3-melhylphenol NO ug/L 4.2 031102202:38
EPA 625.1 bis(2-Chioroethoxy)methane NO ug/L 8.3 03/102202:38
EPA 625.1 bis(2-Chloroethyl)ether NO ug/L 4.2 0311012202:38
EPA625.1 2-Chloronaphthalene NO ug/L 4.2 03110/2202:38
EPA 625.1 2-Chlorophenol NO ug/L 4.2 03110/2202:38
EPA625.1 4-Chlorophenylphenyl ether NO ug/L 4.2 03/10/2202:38
EPA625.1 Chrysene NO ug/L 4.2 03/10/2202:38
EPA625.1 Dibenz(a,h)anthracene NO ug/L 4.2 03/10/22 02:38 page 1 of 6
EPA 625.1 1,2-Dichlorobenzene NO ug/L 4.2 03M 0/2202:38

Pace AnaWicel Services,LLC
q�Q 1377 South Park Drys
An�
P D I'-I 'yh'cdl Kemersville,NC 27284
www.pacelabsxom
[phone]
Page 2 of 3
Sample: 003-Grab Lab ID: 92591318002 Collected: 0310212213:10 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA625.1 1,3-Dichlorobenzene ND ug/L 4.2 03110/2202:38
EPA625.1 1,4-Dichlorobenzene ND ug/L 4.2 03110/2202:38
EPA625.1 3,3'-Dichlorobenzidine ND ug/L 8.3 03110/2202:38
EPA 625.1 2,4-Dichlorophenol ND ug/L 4.2 03110/2202:38
EPA 625.1 Diethylphthalate ND ug/L 4.2 03/1012202:38
EPA 625.1 2,4-Dimethylphenol ND ug/L 8.3 03/10/2202:38
EPA 625.1 Dimethylphthalate ND ug/L 4.2 03/10/2202:38
EPA 625.1 Di-n-butyiphthalale ND ug/L 4.2 03/10/2202:38
EPA 625.1 4,6-Dinitro-2-methylphenol ND ug/L 8.3 03/10/2202:38
EPA 625.1 2,4-Dinitrophenol ND ug/L 41.7 03M 0/2202:38
EPA 625.1 2,4-Dinitrotoluene ND ug/L 4.2 03/10/2202:38
EPA 625.1 2,6-Dinitrotoluene ND ug/L 4.2 03/10/2202:38
EPA 626.1 Di-n-octylphthalate ND ug/L 4.2 03/10/2202:38
EPA 625.1 1,2-Diphenylhydrazine ND ug/L 4.2 03/1012202:38
EPA 625.1 bis(2-Ethylhexyl)phthalate ND ug/L 4.2 03/10/2202:38
EPA 625.1 Fluoranthene ND ug/L 4.2 03110/2202:38
EPA 625.1 Fluorene ND ug/L 4.2 03/1012202:38
EPA 625.1 Hexachloro-1,3-butadiene ND ug/L 4.2 03/1012202:38
EPA 625.1 Hexachlorobenzene ND ug/L 4.2 03110/2202:38
EPA625.1 Hexachlorocyclopentadiene ND ug/L 8.3 03/10/2202:38
EPA625.1 Hexachloroethane ND ug/L 4.2 03110/2202:38
EPA625.1 Indeno(1,2,3-cd)pyrene ND ug/L 4.2 03110/2202:38
EPA625.1 Isophorone ND ug/L 8.3 03/10/2202:38
EPA625.1 Naphthalene ND ug/L 4.2 03110/2202:38
EPA625.1 Nitrobenzene ND ug/L 4.2 03110/2202:38
EPA625.1 2-Nitrophenol - ND ug/L 4.2 03110/2202:38
EPA625.1 4-Nitrophenol ND ug/L 8.3 03110/2202:38
EPA625.1 N-Nilrosodimethylamine ND ug/L 4.2 03/10/2202:38
EPA625.1 N-Nitroso-di-n-propylamine ND ug/L 4.2 03/10/2202:38
EPA625.1 N-Nilrosodiphenylamine ND ug/L 8.3 03/10/2202:38
EPA 625.1 2,2'-Oxybis(1-chloropropane) ND ug/L 4.2 03/10/2202:38
EPA625.1 Pentachlorophenol ND ug/L 8.3 03/10/2202:38
EPA 626.1 Phenanthrene ND ug/L 4.2 03/1012202:38
EPA 625.1 Phenol ND ug/L 4.2 03110/2202:38
EPA 625.1 Pyrene ND ug/L 4.2 03/10/2202:38
EPA 625.1 1,2,4-Trichlorobenzene ND ug/L 4.2 03/10/2202:38
EPA 625.1 2,4,6-Trichlorophenol ND ug/L 8.3 03/10/2202:38
EPA 624.1 Acrolein ND ug/L 5.0 03/04/2216:38 Mt
EPA 624.1 Acrylonitrile ND ug/L 5.0 03/04/2216:38
EPA 624.1 Benzene ND ug/L 1.0 03/04/2216:38
EPA 624.1 Bromodichloromelhane ND ug/L 2.0 03/04/2216:38
EPA624.1 Bromofonn ND ug/L 2.0 03/04/2216:38
EPA624.1 Bromomethane ND ug/L 2.0 03/04/2216:38
EPA624.1 Carbon tetrachloride ND ug/L 2.0 03104/2216:38 R1
EPA624.1 Chlorobenzene ND ug/L 2.0 03/04/2216:38
EPA624.1 Chloroelhane ND ug/L 2.0 03/04/2216:38
EPA624.1 Chloroform ND ug/L 2.0 03/04/2216:38
EPA624.1 Chloromethane ND ug/L 2.0 03104/2216:38 RI
EPA624.1 Dibromochloromelhane ND ug/L 2.0 03/04/2216:38
EPA624.1 1,2-Dichlorobenzene ND ug/L 2.0 03104/2216:38
EPA624.1 1,3-Dichlorobenzene ND ug/L 2.0 03/04/22 16:38
EPA624.1 1,4-Dichlorobenzene ND ug/L 2.0 03/0412216:38
EPA 624.1 1,1-Dichloroethane ND ug/L 2.0 03104/2216:38
EPA 624.1 1,2-Dichloroethane ND ug/L 2.0 03104/2216:38
EPA 624.1 1,1-Dichloroethene ND ug/L 2.0 03104/2216:38
EPA 624.1 cis-1,2-Dichloroethene ND ug/L 2.0 03104/2216:38 Rt
EPA624.1 trans-1,2-Dichloroethene ND ug/L 2.0 03104/2216:38
EPA 624.1 1,2-Dichloropropane ND ug/L 2.0 03/04/22 16:38 Page 2 of 6

Y Pace Analytical Services,LLC
• A r 1377 South Perk Drive
11 acie 'nalyficaIl Kemersville,NC 27284
www.pacelabsxam
� [phone]
Page 3 of 3
Sample: 003-Grab Lab ID: 92591318002 Collected: 03/02/22 13:10 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 624.1 cis-1,3-Dichloropropene ND ug/L 2.0 0310412216:38
EPA 624.1 trans-1,3-Dichloropropene ND ug/L 2.0 03104/2216:38
EPA 624.1 Ethylbenzene ND uglL 1.0 03/04/2216:38
EPA 624.1 Methylene Chloride ND ug/L 2.0 03104/2216:38 M1
EPA 624.1 1,1,2,2-Tetrachloroethane ND ug/L 2.0 03/04/2216:38
EPA 624.1 Tebachloroelhene ND ug/L 2.0 0310412216:38
EPA 624.1 Toluene ND ug/L 1.0 03/04/2216:38
EPA 624.1 1,1,1-Trichloroethane ND ug/L 2.0 03/04/2216:38
EPA 624.1 1,1,2-Trichloroethane ND ug/L 2.0 03/04/2216:38
EPA 624.1 Trichloroethene ND ug/L 2.0 03104/2216:38
EPA 624.1 Trichlorofiuoromethane ND ug/L 2.0 0310412216:38
EPA 624.1 Vinyl chloride ND ug/L 2.0 03/0412216:38 R1
EPA 420.4 Rev 1.0 1993 Phenolics,Total Recoverable ND mg/L 0.020 03/16/22 08:52 MI
SM 4500-CN-E-2011 Cyanide ND mg/L 0.0080 03/08/22 23:53
Sample: 003-LL Hg Lab ID: 92591318003 Collected: 03/02/22 12:50 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 1631E Mercury 2.52 ng/L 0.50 03/16/2214:38
Sample: 003-LL Hg-Field Blank Lab ID: 92691318004 Collected: 03/02/22 12:50 Matrix: Water
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 1631E Mercury ND ng/L 0.50 03/i6/2212:46
ANALYTE QUALIFIERS
IL This analyte exceeded secondary source verification criteria low for the initial calibration.The reported results should be
considered an estimated value.
MI Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
RI �cRgP�D'value was outside control limits.
Reviewed by:
Stephanie Knott
704-977-0981
[e-mail]
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cart.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification*E87627
North Carolina Field Services Certification M 5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water*LA029
South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 288D4 South Carolina Laboratory ID:99030
Florida/NELAP Certification#:E87648 South Carolina Certification M 99030001
North Carolina Drinking Water Certification#:37712 VirginialVELAP Certification#:460222
North Carolina Wastewater Certification#:40
Pace Analytical Services Eden
205 East Meadow Road Suite A,Eden,NC 27288 North Carolina Wastewater Certification#:633
North Carolina Drinking Water Certification#:37738 Virginia/VELAP Certification#:460025
Page 3 of 6

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a No C]WA 2
Shan gafd TtsrleArW h(<72 hr.J7
n rcv We S,
Rush Turn Naund lima Retuested?
tl No N/A A.
SuRldencValume? '
Yes Ab QN/A S.
COmat Cvmalners Used? ��((
-Pace Canufnem Used? is=Sa9 ONO QNIA S.
e /q
Containers lMd(47 re Mt N/A 7.
Dtssafreda SIC Sam sFlekl lagerad7 Elva Na
Sample taheh Match CCC7 /A N.
a ONO a/A 9.
i
•mdudes Date/tune/ID/Anal It "or �
Heads ace in VOA orals p5-Dmm17
es rco a !
Tnp ggnk 10.Present? au ONO A Lt.
p Ggnk[usta S TM Gait/cesanlT
a Na /0.
COMMt"ISAMPtt 01SCAVANCY
INfa Dam aequkrdn QYn� Na
NBdT NO7KtCITION/pg50tUlpN tot 10 Of SO Cantalli ; i
I
Person contacted: Oate/ftma: j
Protein Managar SCURF gdwaw: Osta:
. . Protect Manager SRF Rsvlew: Drte
Page 5 of 6

DOCWn I
Sam re to an Nam, DaamenfUftd:rNNWIY 7,1018
ld! I
Oaatunei[xo.: tafuhgAWparNy:
Rev.OP pry CAMOUS Qu
OhYa
°U1ak mark tap hall otbax N pH and/or dechlarina Nerffkaf and wdbin the acceptance ran ffe-fir pr tfun ie Pm*t
°sampkx etendon l
11a•We1MtAC'VOA.Caarayy iOC,Od and Greese,OA4/8015 Iwateq DD4 Ulf,Sodom hall of box)t to list number of bottle
1 r
Cb—
z of
' 3o �y g
1
1 9 � � � $� d � � d 3 ` � � _ � � d � $ � $ adOfYy( � � �• � 8 � � � i i
2 Y CC
I
3
a !
s
6
7
a
I
9 � '
i
30
11
12
I '
I
samPAa In l pH Adjustment Log for preserved Samples
Ype of prmarvaaw Pn apan MCI Deh prerem0dn mtwyd tgrh
pfermallea Awenoltreurvetlw letN
ad(eead added !
i
i
I
I :
NPtP: Whe tlprehrd4oepanq if 14.0, NPrthCardlne campdance eamPlaa,arcPy Pr M.Mrm wid to antbihe rvonl Grmina OEHNI Cerufintbn0(flce he. !
Oot of hold,4¢ 't Prturvatlul Pol of[emP.incarc i ett tontlinarz
Page 6 of 6