WQ0009267_Monitoring - 12-2021_20220131 (3)

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DWR - NonDischarge Monitoring Report Submittal
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NORTH CAROLINA
Enrlranmenlel QHaflly
Monitoring Report Submittal
..............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Permit Number#* WQ0009267
Name of Facility:* City of Jacksonville WWTF
Month:* December Year:* 2021
Report Information
..................................................................................................................................................................................................................................................................................................
Type* Upload Document*
GW-59 WQ0009267 December 2021 23.07MB
GW-59 MW Report,VOCs
attached.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1,NDAR-2,NDMLR,GW-59).
Confirmation Email Address:* [e-mail]
Name of Submitter:* Amy Palaschak
Signature:
I NdO
Date of submittal: 1/31/2022
This will be filled in automatically
Initial Review

Reviewer: Gerald,Wanda
Is the project number correct?* WQ0009267
Is the monitoring report accepted?* Yes No
Regional Office* Wilmington
Accepted Date: 3/16/2022

(1W-59A C'(.)MP!AAN(,I; REPORT FORM Permit II. WQ0009267
(Submit one each monitoring period with(,W-59 torrnry.)
1 Enter date monitoring results were due. (10/31/2021) Will this monitoring report(GW-59 and GW-59A) be YES NO
submitted after the established due date?
2 Was any required information missing on the GW-59 report forms? YES NO
IF the answer to question 1 or 2 is"YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3 Are any of the monitor wells in need of repair or maintenance(damaged casing,unlocked or missing cap,missing YES NO
identification plate,area overgrown,etc.)?If the answer is"Yes",contact the Regional Office for guidance.
4 Are any monitored constituents equal to or above the established standards? 4/11) NO
If the answer to question 4 is"NO", skip to section 8. If the answer to question 4 is"YES" list the affected wells
individually with constituent(s)and concentration(s) exceeding standards in the space provided below:
MW 10—TDS 633 mg/L
MW 2—Bromomethane 1.60 ug/L, Chloromethane 1.14 ug/L
MW 11 —Bromomethane 1.44ug/L Chloromethane 1.06 ug/I
5 For the constituents identified in question 4 above, have standards been exceeded previously for the same ® NO
constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is"NO", skip to section 8. If the answer to question 5 is"YES", list in the space
provided below, each well with constituent(s)exceeding standards, concentration(s) reported, and sample
collection date for each occurrence(for the last two years).
MW 10—all TDS—9/2019 (643 mg/L), 12/2019 (568.5 mg/L), 3/2020 (618 mg/L), 6/2020 (596.5 mg/L),
9/2020 (628 mg/L), 12/2020 (579 mg/L), 3/2021 (683 mg/L), 6/2021 (657 mg/L), 9/2021 (675)
MW 2—Chloromethane—1.90 ug/L(12/2020)
MW 11 —Chloromethane—1.22 ug/L(12/2020)
6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO
If the answer is"YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE
IMMEDIATELY FOR GUIDANCE. If the answer is"NO", monitoring wells may be improperly located; contact
the Regional Office.
Contacted Tom Tharrington and Helen Perez at NC DEQ Wilmington Regional Office to notify them of
the presence of VOCs (Chloromethane and Bromomethane) in MWs. Env. Specialist II, Helen Perez,
advised that we resample the wells positive for VOCs.
7 Is the permittee implementing previously approved actions required by the Division involving this groundwater 415 NO
quality problem?
If the answer to question 7 is"YES", describe those actions in the space provided below. If the answer to
question 7 is"NO", contact the Regional Office within 90 days; an evaluation may be required to determine the
impact the waste disposal system is having at the review and compliance boundaries surrounding this facility.
Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties.
MW10—high background TDS—noted in current permit
8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form
with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report(Compliance Report GW-59A)is true and complete to the best of my knowledge
11/ e. (/ 01-31-2021
Signature of Permittee(or Authorized Agent) Date
(:W-59A 12/8/200

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original $4`_ o 4 1, lit _ __ -�
GROUNDWATER QUALITY MONITORING: and 1 copy to \ `� �� . _ �
COMPLIANCE REPORT FORM •:1� .m -a•' t .__�� r 1
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name(if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
.acksonvhie NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
't` , _`' zrX Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-1 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-1 Date sample collected: 12/14/2021 FIELD ANALYSES: WAS
Well Depth: 16.6 ft, Well Diameter: 2 in. pH 00400: 5 units Temp. 000ic 17.8 °C DRY at
Depth to Water Level 82546: 9 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 3.2 ft. above land surface Relative M.P. Elevation: 5.8 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 3.65 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/14/2021 Laboratory Name: 1. Jacksonville 2, Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2) as N oasis <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.03 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
dissolved Solids:Total 70300 174 mg/L Al-Aluminum 01105 mg/L
pH (Lab)00403 5.01 units Ba-Barium 01007 ug/L
TOC 00680 13.1 mg/L Ca-Calcium oosls mg/L
Chloride 00940 48 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils oo552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron(nazis ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate oosas 14 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance(foss µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia o0s10 <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH,as N;Ammonia Nitrogen,Total) Mn- Manganese 010ss ug/L , method#
TKN as N o0625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
William E. Brown-ORC1,JG . 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original f m semis ' '�I I ` � -\���`
GROUNDWATER QUALITY MONITORING: 44 6 0A ► t
and I copy to ��-- 27 ,, -������� `, _
COMPLIANCE REPORT FORM : „� ��-1--,1�
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name(if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
''-'` X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-2 No,of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-2 Date sample collected: 12/14/2021 FIELD ANALYSES: WAS
Well Depth: 17.0 ft. Well Diameter: 2 in. pH 00400: 5.2 units Temp, 000ic 18.6 °C DRY at
Depth to Water Level 82546: 5.6 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 2.4 ft. above land surface Relative M.P. Elevation: 3.2 ft. Odor00085: check
Volume of water pumped/bailed before sampling: 5.47 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/14/2021 Laboratory Name: 1.Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 29 /100mL Nitrate(NO3)as N 00620 0.05 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 122 mg/L Al-Aluminum o11os mg/L
pH (Lab) 00403 5.15 units Ba-Barium o1007 ug/L
TOC 00680 4.2 mg/L Ca-Calcium oo91s mg/L
Chloride 00940 46 mg/L Cd-Cadmium 01027 ug/L
Arsenic©1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe- Iron oloas ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 <5 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No(0)
Specific Conductance 0009s µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia o0s10 <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese moss ug/L , method#
TKN as N oos25 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
/
William E. Brown ORC /y1 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev,8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original t =L�� `�1��' , ,� �� �, -��
GROUNDWATER QUALITY MONITORING: ® E --.,,� 1., �� e , -t� t.
and 1 copy to: li y� _ i ,-
COMPLIANCE REPORT FORM ti �,, ;L� „ ` —,
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name(if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
Cm,= ,ate
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-3 No,of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-3 Date sample collected: 12/13/2021 FIELD ANALYSES: WAS
Well Depth: 17.0 ft. Well Diameter: 2 in. pH o0400: 4,3 units Temp.000ic 18.8 °C DRY at
Depth to Water Level 82546: 11 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 3.2 ft. above land surface Relative M.P. Elevation: 8.1 ft. Odor'00085: check
Volume of water pumped/bailed before sampling: 2.74 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/13/2021 Laboratory Name: 1.Jacksonville 2. Environmental Chemists Certification No, 1, 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N oo615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P oosss <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
dissolved Solids:Total 70300 44 mg/L Al-Aluminum 01105 mg/L
pH (Lab)00403 4.29 units Ba-Barium 01007 ug/L
TOC 00680 1.4 mg/L Ca-Calcium on-is mg/L
Chloride 00940 12 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 17 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia o0s10 <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen:NH3 as N;Ammonia Nitrogen.Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
William E. Brown ORC / 7� G ? 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original ��'Y _ti®-1.�a , ,--- r a -- - s�
GROUNDWATER QUALITY MONITORING: ,°- ► � _
COMPLIANCE REPORT FORM and 1 copy >< �� ( k 4�
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name(if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonvilie NC 28540 County Onslow D Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-4 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-4 Date sample collected: 12/13/2021 FIELD ANALYSES: WAS
Well Depth: 16.0 ft. Well Diameter: 2 in. pH 00400: 4.8 units Temp. 000ic 16.8 °C DRY at
Depth to Water Level 82546: 2.5 ft. below measuring point Screened Interval: 5.8 ft. to 14 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 2.68 ft, above land surface Relative M.P. Elevation: -0.18 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 6.48 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/13/2021 Laboratory Name: 1.Jacksonville 2. Environmental Chemists Certification No. 1. 128 2,94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2)as N 00s1s <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3)as N ooszo <0.02 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P Doses <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 95 mg/L Al-Aluminum 011os mg/L
pH (Lab) 00403 4.83 units Ba-Barium 01007 ug/L
TOC 00680 1.2 mg/L Ca-Calcium 0091s mg/L
Chloride 00940 56 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 uglL Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 35 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No(0)
.pecific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia o0s10 <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese Dross ug/L , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
William E. Brown-ORC 7 7 / 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original ° I ` ° I am -_ -��
GROUNDWATER QUALITY MONITORING: �� a ®� ,. -� , ��-
COMPLIANCE REPORT FORM and 1 copy to: � � o :
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge W00009267 UIC
Permit Name(if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
vatn, Z r,
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-5 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-5 Date sample collected: 12/13/2021 FIELD ANALYSES: WAS
Well Depth: 18.1 ft. Well Diameter: 2 in. pH 00400: 5.5 units Temp. 000lc 17.9 °C DRY at
Depth to Water Level 82546: 9 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 2.57 ft. above land surface Relative M.P. Elevation: 6.43 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 4.37 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/13/2021 Laboratory Name: 1.Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2)as N oosls <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3)as N ooszo <0.02 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 0o665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 62 mg/L Al-Aluminum o11os mg/L
pH (Lab) 00403 5.48 units Ba-Barium 01007 ug/L
TOC 00680 <0.5 mg/L Ca-Calcium oosls mg/L
Chloride 00940 <5 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron o1045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 <5 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia ooslo <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen:NH3 as N:Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
• i
William E. Brown-ORC A ,,e-oi97-6-rij 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail orI ® �qe ._ , !t. ���
GROUNDWATER QUALITY MONITORING: g ��
COMPLIANCE REPORT FORM and 1 copy o -��� 1 - - _ �y ����
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name(if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksanvife NC 285d3 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
' `t'``= ❑ Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-6 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-6 Date sample collected: 12/15/2021 FIELD ANALYSES: WAS
Well Depth: 16.8 ft. Well Diameter: 2 in. pH 00400: 5.7 units Temp, 000lc 17.6 °C DRY at
Depth to Water Level 82546: 4.4 ft. below measuring point Screened Interval: 3.5 ft. to 14 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 2.65 ft. above land surface Relative M.P. Elevation: 1.75 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 5.95 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/15/2021 Laboratory Name: 1.Jacksonville 2. Environmental Chemists Certification No. 1. 128 2, 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2)as N oos15 0.16 mg/L Pb-Lead 01051 uglL
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 <0.02 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 231 mg/L Al-Aluminum 01105 mg/L
pH (Lab)00403 5.68 units Ba-Barium 01007 ug/L
TOC ooseo 7.1 mg/L Ca-Calcium oosss mg/L
Chloride 00940 23 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron o1045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 17 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos K- Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia ooseo <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen.Total) Mn-Manganese o1055 ug/L , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
A. r William E. Brown ORC " gi24ss 7 ♦' 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or tvoe Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original ,�� ��� -- = �� �i � ���
GROUNDWATER QUALITY MONITORING: t e �- 8 - tt
and 1 copy to .�� �- � -
i .,--- a � � 9 ��1��--t,'
COMPLIANCE REPORT FORM , �.� „ _�„ ��,"�, �� �
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name (if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-7 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-7 Date sample collected: 12/15/2021 FIELD ANALYSES: WAS
Well Depth: 15.0 ft. Well Diameter: 2 in. pH 00400: 4.5 units Temp. 000ic 15.4 °C DRY at
Depth to Water Level 82546: 8.4 ft, below measuring point Screened Interval: 2.5 ft. to 13 ft, Spec. Cond.00094: µMhos time of
sampling,
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: 5.4 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 3.17 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/15/2021 Laboratory Name: 1.Jacksonville 2, Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2) as N 00615 <0.02 mg/L Pb-Lead o1os1 ug/L
Coliform: MF Fecal 31616 3 /100mL Nitrate(NO3) as N ooszo <0.02 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P o0665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 159 mg/L Al-Aluminum o11os mg/L
pH (Lab)00403 4.46 units Ba-Barium 01007 ug/L
TOC 00680 7.1 mg/L Ca-Calcium o0916 mg/L
Chloride 00940 27 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe- Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 30 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia oosio <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen:NH3as N:Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
William E. Brown-ORC . / (,44,y/ 2 ,ti(,7.4./11 1/31/2022
Permittee for Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original ,':�• a g ie> ,-s
GROUNDWATER QUALITY MONITORING: W s- -� _ 'e -i i1-
and 1 copy to `,
COMPLIANCE REPORT FORM - .=� „ram - _
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name(if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
S'ate1 X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-8 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-8 Date sample collected: 12/16/2021 FIELD ANALYSES: WAS
Well Depth: 12.1 ft. Well Diameter: 2 in. pH 00400: units Temp.oo0to: °C DRY at
Depth to Water Level 82546: 10 ft. below measuring point Screened Interval: 3 ft. to 9 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: 7 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 1.01 gallons Appearance here:
Samples for metals were collected unfiltered: X YES El NO and field acidified: X YES El NO
V
LABORATORY INFORMATION
Date sample analyzed: 12/16/2021 Laboratory Name: 1.Jacksonville 2, Environmental Chemists Certification No. 1. 128 2.94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2)as N oos15 mg/L Pb-Lead otosi ug/L
Coliform: MF Fecal 31616 /100mL Nitrate (NO3)as N 00620 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P oo665 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Il issolved Solids:Total 70300 mg/L Al-Aluminum 01105 mg/L
pH (Lab)00403 units Ba-Barium 01007 ug/L
TOC 00680 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 mg/L Cd-Cadmium 01027 ug/L
Arsenic 0100z ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron oio45 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0)
specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia oosio mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH,as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N 0os25 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I°certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
William E. Brown-ORC / / i •- 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original . -•� r _ F4 a ®A : � -------
GROUNDWATER
QUALITY MONITORING: - it- 0
COMPLIANCE REPORT FORM and 1 copy to: _ z
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name(if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
r.-. e3Le 7,r=
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-9 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-9 Date sample collected: 12/16/2021 FIELD ANALYSES: WAS
Well Depth: 14.0 ft. Well Diameter: 2 in. pH 00400: 3.8 units Temp. 000ic 17.8 °C DRY at
Depth to Water Level 82546: 11 ft. below measuring point Screened Interval: 7 ft. to 11 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 2.55 ft. above land surface Relative M.P. Elevation: 8.75 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 1.30 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/16/2021 Laboratory Name: 1.Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2)as N oosi5 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3) as N oos2o <0.02 mg/L Zn-Zinc o1092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
dissolved Solids:Total 70300 184 mg/L Al-Aluminum o1105 mg/L
pH (Lab)00403 3,79 units Ba-Barium 01007 ug/L
TOC 00680 2.3 mg/L Ca-Calcium 00s1s mg/L
Chloride 00940 7 mg/L Cd-Cadmium 01027 ug/L
Arsenic olooz ug/L Chromium:Total 01034 ug/L
Grease and Oils o0552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 uglL Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 97 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No(0)
Specific Conductance 000s5 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia oos10 <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen:NH,as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
r
ir -
William E. Brown-ORC AIFf4/ ::, AP_-6i0n ' 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized gent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original P.- ' l •>_, z, 6 1`' e m, ��
� �
GROUNDWATER QUALITY MONITORING: `a Zs ,r �e _ ®� .� --
and 1 copy to
COMPLIANCE REPORT FORM _�`��� ��� � � � �▪ -- � rr -
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name (if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
` " X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-10 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-10 Date sample collected: 12/16/2021 FIELD ANALYSES: WAS
Well Depth: 30.1 ft. Well Diameter: 2 in. pH o0400: 6.4 units Temp. 000ic 16.5 °C DRY at
Depth to Water Level 82546: 12 ft. below measuring point Screened Interval: 17 ft. to 27 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 2.9 ft. above land surface Relative M.P. Elevation: 9.2 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 8.64 gallons Appearance here:
Samples for metals were collected unfiltered: X YES E NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/16/2021 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2) as N 00615 <0.02 mg/L Pb-Lead o1os1 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3) as N 00620 <0.02 mg/L Zn-Zinc 01o92 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P oo665 1.1 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 633 mg/L Al-Aluminum oiio5 mg/L
pH (Lab)00403 6.36 units Ba-Barium 01007 ug/L
TOC 00680 2 mg/L Ca-Calcium o0s1s mg/L
Chloride 00940 13 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron o1o4s ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 129 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia 00610 <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH,as N;Ammonia Nitrogen.Total) Mn-Manganese 01055 uglL , method#
TKN as N o0625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
William E. Brown ORC 16
0._..-4,07-e..4,7 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original - :'4' . - * t � `r� i,,•
GROUNDWATER QUALITY MONITORING: - �: $ t i�
and 1 copy to
COMPLIANCE REPORT FORM _ _,`,7 „„ � _„_
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name (if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Ja-cksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
.°` ^t_' X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-11 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-11 Date sample collected: 12/14/2021 FIELD ANALYSES: WAS
Well Depth: 22.2 ft. Well Diameter: 2 in. pH 00400: 4.8 units Temp. 000ic 18.3 °C DRY at
Depth to Water Level 82546: 13 ft, below measuring point Screened Interval: 5 ft. to 20 ft. Spec. Cond.00094: µMhos time of
sampling,
Measuring Point is 2.25 ft. above land surface Relative M.P. Elevation: 10.45 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 4.56 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/14/2021 Laboratory Name: 1.Jacksonville 2. Environmental Chemists Certification No. 1. 128 2, 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N o0s1s <0.02 mg/L Pb-Lead oiosi ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.28 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus;Total as P 00665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 45 mg/L Al-Aluminum o11os mg/L
pH (Lab)00403 4.75 units Ba-Barium 01007 ug/L
TOC 00680 <0.5 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 5 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1o0z ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe- Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 <5 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No(0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia ooslo <0.1 mg/L Mg- Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
1(-)/
1 r
William E. Brown-ORC LQrjyy� e ,f KGB 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original © = �
GROUNDWATER QUALITY MONITORING:
:6 ��
and1copyto tit `�
COMPLIANCE REPORT FORM 1t "a:-- = '�'
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name (if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
S.3P 'z c X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-12 No.of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-12 Date sample collected: 12/15/2021 FIELD ANALYSES: WAS
Well Depth: 18.3 ft. Well Diameter: 2 in. pH 00400: 5.4 units Temp.000ic 18 °C DRY at
Depth to Water Level 82546: 7.5 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 3.04 ft. above land surface Relative M.P. Elevation: 4.46 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 5.18 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/15/2021 Laboratory Name: 1,Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2) as N 00615 0.05 mg/L Pb-Lead olosi ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3)as N 00620 <0.02 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P oos65 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 105 mg/L Al-Aluminum o11os mg/L
pH (Lab)00403 5.44 units Ba-Barium 01007 ug/L
TOC 00680 26.2 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 <5 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe- Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 6 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia oos10 <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
William E. Brown-ORC 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original gam- � _ °L `'_�•: -
GROUNDWATER QUALITY MONITORING: and 1 copy to a 8 •-si
COMPLIANCE REPORT FORM 1 - _ - - -
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name(if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
uaccsonvil!e NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
u` X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-13 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-13 Date sample collected: 12/16/2021 FIELD ANALYSES: WAS
Well Depth: 23,2 ft. Well Diameter: 2 in. pH 00400: 4.6 units Temp. 000ic 18.9 °C DRY at
Depth to Water Level 82546: 17 ft. below measuring point Screened Interval: 10.5 ft. to 23.2 ft. Spec. Cond.00094: µMhos time of
sampling,
Measuring Point is 2.75 ft. above land surface Relative M.P. Elevation: 14.15 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 3.02 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/16/2021 Laboratory Name: 1.Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2) as N 00615 <0.02 mg/L Pb-Lead 01051 uglL
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3) as N 00620 <0.02 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P o0665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 40 mg/L Al-Aluminum 01105 mg/L
pH (Lab) 00403 4.6 units Ba- Barium 01007 ug/L
TOC 00680 0.8 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 16 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 uglL Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 uglL Fe-Iron 01045 uglL (Specify test and method#.ATTACH LAB REPORT.)
Sulfate oos45 <5 mg/L Hg-Mercury 71900 uglL Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia o0s10 0,2 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH,as N;Ammonia Nitrogen,Total)
Mn-Manganese 01055 uglL , method#
TKN as N 00625 mg/L Ni-Nickel 01067 uglL , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
William E. Brown-ORC / . . 40~ ,A1P-.-1-=eZzrY1 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: Mail original s ��'oaf m "�' 'i _� _ - �
and 1 copy to g _, - e g -�
COMPLIANCE REPORT FORM Vim'' �
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name (if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
,=:,' sEt°'' u, X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-14 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-14 Date sample collected: 12/16/2021 FIELD ANALYSES: WAS
Well Depth: 17.9 ft. Well Diameter: 2 in. pH 00400: 4.8 units Temp. 000ic 18.8 °C DRY at
Depth to Water Level azs4s: 13 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 3.2 ft. above land surface Relative M.P. Elevation: 9.4 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 2.54 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/16/2021 Laboratory Name: 1.Jacksonville 2. Environmental Chemists Certification No. 1. 128 2.94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2) as N Dods <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3) as N 00620 0.04 mg/L Zn-Zinc cmosz mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P 00665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 49 mg/L Al-Aluminum 01105 mg/L
pH (Lab)00403 4.75 units Ba-Barium 01007 ug/L
TOC 00680 12.6 mg/L Ca-Calcium oos16 mg/L
Chloride 00940 8 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils o0552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 <5 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia ooslo 1.26 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N ooszs mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
William E. Brown ORC ie..)
, ..........- 0
1/31/2022
Pemiittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
M• I •riginal��' : � k=e J�
GROUNDWATER QUALITY MONITORING: e ' e� =e' . -t,
and 1 copy to ��—
COMPLIANCE REPORT FORM a. s� '='., , r �' -----
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name (if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
``' X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-15 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-15 Date sample collected: 12/14/2021 FIELD ANALYSES: WAS
Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 4.7 units Temp. 000ic 17.4 °C DRY at
Depth to Water Level 82546: 3.7 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 2.9 ft. above land surface Relative M.P. Elevation: 0.8 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 5.42 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/14/2021 Laboratory Name: 1.Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2) as N 00615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3) as N 00620 2.68 mg/L Zn-Zinc oio92 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P o0665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 51 mg/L Al-Aluminum 011os mg/L
pH (Lab) 00403 4.74 units Ba-Barium 01007 ug/L
TOC 00680 0.7 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 41 mg/L Cd-Cadmium 01027 ug/L
Arsenic o1002 ug/L Chromium: Total 01034 ug!L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate o0945 <5 mg/L Hg Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia ooslo <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH,as N;Ammonia Nitrogen,Total) Mn-Manganese o1055 ug/L , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
•
William E. Brown-ORC �� 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original � � _
GROUNDWATER QUALITY MONITORING: i _ - e �� 1;1N
and 1 copy to: : :-,,�_ � a
COMPLIANCE REPORT FORM , ' �� , _ '�-
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name (if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
:t;s `6-ales "'r"
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-16 No. of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-16 Date sample collected: 12/14/2021 FIELD ANALYSES: WAS
Well Depth: 25 ft. Well Diameter: 2 in. pH 00400: 4.7 units Temp. 000ic 18.4 °C DRY at
Depth to Water Level 82546: 11 ft. below measuring point Screened Interval: 15 ft. to 20 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 2.4 ft. above land surface Relative M.P. Elevation: 8.3 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 6.86 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/14/2021 Laboratory Name: 1.Jacksonville 2, Environmental Chemists Certification No, 1. 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2)as N 00615 <0.02 mg/L Pb-Lead 01os1 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3)as N 00620 0.09 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P o0665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 75 mg/L Al-Aluminum o11os mg/L
pH (Lab) 00403 4.68 units Ba-Barium 01007 ug/L
TOC 00680 1.1 mg/L Ca-Calcium oos16 mg/L
Chloride 00940 29 mg/L Cd-Cadmium 01027 ug/L
Arsenic olooz ug/L Chromium:Total 01034 ug/L
Grease and Oils oo552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 6 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No(0)
Specific Conductance 000ss µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia 00610 <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn- Manganese 01055 ug/L , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
William E. Brown-ORC i '' '� 1' 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev,8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original s - e �* a-_ -�' = —_
GROUNDWATER QUALITY MONITORING: and 1 copy to e
COMPLIANCE REPORT FORM % 1 - �_ _� t -� , —•m. -K`r
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 4/30/2022
Facility Name: City of Jacksonville Land Treatment System Non-Discharge WQ0009267 UIC
Permit Name(if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC 28540 County Onslow ❑ Lagoon ❑ Remediation: Infiltration Gallery
'' °' X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-17 No.of wells to be sampled: 17 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): MW-17 Date sample collected: 12/14/2021 FIELD ANALYSES: WAS
Well Depth: 25 ft. Well Diameter: 2 in. pH 00400: 4.3 units Temp. 000ic 19 °C DRY at
Depth to Water Level 82546: 7.8 ft. below measuring point Screened Interval: 15 ft. to 20 ft. Spec. Cond. 00094: µMhos time of
sampling,
Measuring Point is 1.9 ft. above land surface Relative M.P. Elevation: 5.9 ft. Odor 00085: check
Volume of water pumped/bailed before sampling: 8.26 gallons Appearance here:
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/14/2021 Laboratory Name: 1.Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2) as N 00615 <0.02 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3) as N oo62o <0.02 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P oo665 <0.2 mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
dissolved Solids:Total 70300 116 mg/L Al-Aluminum 01105 mg/L
pH (Lab)00403 4.32 units Ba-Barium 01007 ug/L
TOC 00680 0.7 mg/L Ca-Calcium oosls mg/L
Chloride 00940 25 mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils o0552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 10 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance moss µMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200C
Total Ammonia oosio <0.1 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen;NH3 as N;Ammonia Nitrogen,Total) Mn-Manganese 01055 ug/L , method#
TKN as N o0625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of,fines and imprisonment for knowing violations.
William E. Brown-ORC •��m ^GAY( 1/31/2022
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee(or Authorized (Date)
GW-59 Rev.8/2013

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ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22063
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-55316 Site: MW-3 12/13/2021 1:09 PM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev 2 1,1993 17 mg/L 12/16/2021
Total Organic Carbon (TOC) SM 5310 B-2014 1.4 mg/L 12/15/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2-Chiorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#:: 2021-22063 Page 1 of 9

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111111111111111111111111111111v1v111111111:111011101vi maw 0 1111111111111111010 IM000 6602 Windmill Way,Wilmington,NC 28405 0 910.392.0223 Lab 6 910.392.4424 Fax
710 liowsertown Road,Monte°,NC 27954 0 252.473.5702 Lab/Fax
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11140000000nm 255 A Wilmington Highway,Jacksonville,NC 28540 0 910.347.5843 Lab/Fax
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ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22063
Project ID: Monitoring Wells
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Isopropylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 12/18/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
n-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
p-lsopropyltoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Styrene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Toluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#:: 2021-22063 Page 2 of 9

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710 Bowsertown Road,Manteo,NC 27954 0 252.473.5702 Lab/Fax
milloomploo
NI IlVihoolosolosi
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255-A IATilmiri:ton Highway, Jacksonville,NC 28540 6 910.347.5843 Lab/Fax
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ANALYTICAL&CONSULTING CHEMISTS info@environmentalehemists corn
City of of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22063
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloride SM4500 Cl E-2011 12 mg/L 12/17/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/14/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/15/2021
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/28/2021
Report#. 2021-22063 Page 3019

II 11111111111111111111111holill111111111111111111111,111
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710 Bowsertown Road,Manteo,NC 27954 * 252,473.5702 Lab/Fax
VI
"4 255••A Wilmington Highway,Jacksonville,NC 28540 a 910,347.58431Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22063
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-55317 Site: MW-4 12/13/2021 12:33 PM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2.1,1993 35 mg/L 12/16/2021
Total Organic Carbon (TOC) SM 5310 B-2014 1.2 mg/L 12/15/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Tiichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#:: 2021-22063 Page 4 of 9

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&602 Windmill Way,Wilmington,NC284Q5 ° 91.0.392.0223 1.,a6 ~ 9I8.392.4424 Fax
' 71.8Bowaert:ovpn,Road B���0�� ���7�5� w 252.473.5702�mb/Fax
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, Z55`���omio���.��i��wayjecksortville,NC28540 m 91.8.347.5043Lsb/Fax
ANALYTICAL&CONSULTING CHEMISTS im0m@envimonomentmtohemmimtsoaom
_______
City of Jacksonville Date of Report: Jan O5. 2O23
Post Office Box 138 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: AmyPa|aochak Report#: 2021-22083
Project ID: Monitoring Wells
Bromobenzene mw«u» u-2011 < O.5Opg/L 12/18/2021
Bromoohloronnethane uMnu«»c'u»11 < 0.50pg/L 12/18/2021
Bnomodich|onmmethane amau»«o'u»11 < 0.50pg/L 12/18/2021
BnOmnoform sm«u»»c'c»11 « 0.50pg/L 12/18/2021
Bnomomethane awoo»»c-2»11 < 0.50pg/L 12/18/2021
Carbon tetrachloride oMeu»»o'u»11 < O.5Opg/L 12/18/2021
Ch|orobenzene omou»o«'u»11 < O.5Opg/L 12/18/2021
Ch|oroethane smnu»»c-2»11 < 0.50pg/L 12/18/2021
Chloroform amse»«c'o»11 < O.5Opg/L 12/18/2021
Ch|onomethane am«o»»o'e«11 < 0.50pg/L 12/18/2021
cis-1.2-Dioh|oroathene amau»»c-2»11 < O.5Opg/L 12/18/2021
cis-1.3-Dinh|onopropena aws»»»u'u»11 < 0.50pg/L 12/18/2031
Dibromoch|onomethana am»u»»o'u«11 < 0.50pg/L 12/18/2021
Dibromomethene aMnu»»c'u«11 < 0.50pg/L 12/18/2021
Dich|onmdifluonomathone amoc»oo-2»11 x 0.50pg/L 12/18/2021
Ethy|benzene awsoo»c'u»11 < 0.50VD/L 12/18/2021
Hewooh|orobubadiene ownu»»c-2»11 < 0.50pg/L 13/18/2021
|oopnopy|benzene am«u»»o'u»11 < 0.50pg/L 12/18/2021
K8+P}(y|ene om«»»oo'co11 < 1.00pg/L 12/18/2031
Methylene chloride sw«o»»c-2«`1 < 0.50pQ/L 12/18/2021
Naphthalene mweu»»c'u»11 < 0.50pQ/L 12/18/2021
n-Buh//banrene SMoo»»c'»«11 < 0.50pg/L 12/18/2021
n-Propy|benzene aw«oo»o'o»11 < 0.50pg/L 12/18/2021
ortho-Xy|ene smeuo»o'u»11 < O.5OAg/L 12/18/2021
p-|sopropy|to/uene oMnu»»«-2«11 < O.5Opg/L 13/18/2021
sec-Butyl benzene oMnoo»o'u»11 < O.5Opg/L 12/18/2021
Styrene aw««»«o-2»11 < O.5Opg/L 12/18/2021
teMt-Butylbenzena smeo»»c'u»11 < O.5OpQ/L 12/18/3021
Tetnach|oroethane ownu»»c-2n11 < 0.60pg/L 12/18/2021
Toluene om«o»»c'oo11 < O.5OpQ/L 13/18/2021

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7 i 0 Bowsertown Road,Manteo,NC 27954 * 252.4'73.5'02 T,ab,/Fax
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ANALYTICAL&CONSULTING CHEMISTS [e-mail]
, ..... .. 22
.. ..
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22063
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichloroethene SM 6200 C-2011 <0.50 pg/L 12/18/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Vinyl chloride SM 6200 C-2011 <0.50 pg/L 12/18/2021
Chloride SM4500 CI E-2011 56 mg/L 12/17/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2 0,1993 < 0.02 mg/L 12/14/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/15/2021
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/28/2021
Report#:: 2021-22063 Page 6019

•
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evil,„motto..Hmome 111101 II Heil ii I, III fil 11 ������ 6602 Windmill Way,Wilmington,NC 284.05 * 910.392..0223 Lab * 910.392..4424 Fax
Ivo 710 Bowser town Road,Manteo,NC 27954 * 252.473.5702 Lab/Fax
III woonium
iii ," 255-A Wilmington Highway,Jacksonville,NC 28540 * 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(a)environmentalchemists.com.
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22063
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-55318 Site: MW-5 12/13/2021 10:00 AM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2.1,1993 <5 mg/L 12/16/2021
Total Organic Carbon (TOC) SM 5310 B-2014 <0.5 mg/L 12/15/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,1-Trichioroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#:: 2021-22063 Page 7 of 9

I �. =��
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6602Wirwdmill Way,Wilmington,NC28485 91.0.392.0225Lab w 91.0.892.4j'24Faz
7I8Bavvaertmvvn Road,Maoteo,NC27954 ° 252.473.57021.,ab/Fmx
=" 255-AWilmmin.gtorillighm/ayjecksorivi.ile,NC20540 * 91.0.347.5043Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan O5. 2O22
Post Office Box 128 Customer PO#:
Jacksonville WC 28541 Customer ID: 08110015
Attention: AmnyPe|aochoh Reponk#: 2031-22063
Project ID: Monitoring VVa||s
Bnomobenzene mweo» »-2011 < O.5Opg/L 12/18/2021
Bromooh|onomethane oMso»»o'»»11 < 0.50pQ/L 13/18/2021
Bromodich|onomathana sMeu»»o'o»11 < O.5Opg/L 12/18/3021
Bnomofmrm aw»o»»o'c»11 < D.5Opg/L 12/18/2021
Bromomethane aMsu«»o-2»11 < O.5Opg/L 12/18/2021
Carbon tetrachloride ow»uo«o'»»11 < 0.50pg/L 12/18/2021
Ch|onobenzena amsu»oc'o»11 < D.5Opg/L 12/18/2021
Ch|oroethone om«u«»«-2»11 < O.5Opg/L 12/18C3021
Chloroform awoo»««'co11 < O.5Opg/L 12/18/2021
[|h|oromethane omau»»c-2»11 < O.5OpQ/L 12/18/3021
cis-1.2-Dioh|oroethene oMnu»»o'u«11 < 0.50pg/L 12/18/2021
cis-1.3-Dioh|oropropmne am«c«»«'o»11 < O.5Opg/L 12/18/2021
Oibromooh|orommthane aMou»»«-2»11 < O.SOpg/L 13/18/2021
Oibnornomethane aw«n»»o'u»11 < 0.50pg/L 12/18/2021
[Jich!onodifluorornethane awn«»»c-2»11 < O.5Dpg/L 12/18/2021
Ethy|benzene Vwoc»oc'««11 « O.5Opg/L 12/18/2021
Hexach|onobutadiene ow«n»oo'u»11 < O.5Opg/L 12/18/2031
|eopnopy|benzene mmau«»o-2«11 < O.5Opg/L 12/18/2021
K0+pXy|ene amauo»o-2»11 « 1.00pQ/L 12/18/2021
Methylene chloride awn»»»c'»»11 < 0.50pg/L 12/18/2021
Naphthalene ama»»»c-2»11 < O.5OVQ/L 12/18/2021
n-Buhy|bonoene aw«o»»u-2«11 < O.5Opg/L 12/18/2021
n-Propy|bonzene amsn»ou'u»11 < 0.50VQ/L 13/18/2021
odho-Xy|ene awo»»»o-2»11 < O.5Opg/L 12/18/2021
p-|eopnopy|ho|uene aM*u»»c-2»11 < O.5Opg/L 12/18/2021
Geo-Buty|benzene em«»»»o'o»11 < O.5Opg/L 12/18/2021
Styrene amuu«»o'u»11 < 0.50pg/L 12/18/2021
baMt-Buh/|benzene mmou»»o-2»11 < O.5Opg/L 12/18/2021
Tetnaoh|oroethene awnu»oo-2»11 < O.5OVg/L 12/18/2021
Toluene swn»»»o'»»11 « 0.50pg/L 12/18/2031

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6602 Windmill Way Wilmington,NC 28405 61 910392.0223 Lab 6 910 392_4424 Fax
amosOlY 1
"""111101111,11111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111
710 Bowsertown Road,Manteo,NC 27954 * 282 473.5702 Lab/Fax
611116111611111111111111.00a111111111111111111111111111111111111111111111"11111n111111111111110 ,,IVII
111 1111111olillo11111111 111111:illil 1 IIVOilhhhh
255-A Wilmington f figlhway,Jacksonville,NC 28540 * 910347.5843 Lab/Fax
6,166111111111661$111111111111111111111
Hill
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22063
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloride SM4500 CI E-2011 < 5 mg/L 12/17/2021
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2,Rev 2 0,1993 < 0.02 mg/L 12/14/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev 2 0 1993 < 0.02 mg/L 12/15/2021
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/28/2021
Comment: ro 1,
Reviewed by: 1,10i:,:ka,,, \I\I i.„,),,,,,, ,- \
Report#:: 2021-22063 Page 9 of 9

Environmental Chemist,
, _�__ G6O2 Windmill Way
Wilmington, NC 38405
910.39I0223
Sample Receipt Checklist
Cl ient: �_~� ��~r \ ON��| /\D\Cate: | \+ Report Nunnber:_ 2[)21-
11 YES 0 NO
,�4 N/A I. Were custody seals present on the'c'ooler?'
11 YES 0 NO 12 If custody seals were present, were they inta ct/un broken?
Original temperature upon receipt C Corrected temperature upon receipt C,
,How temperature taken: 13 Temperature Blank Against Bottles
X YES
El NO 3. If temperature of cooler exceeded 6*C, was Project Mgr./QA notified?
X YES 0 NO 4. Were proper custody procedures (relinquished/received) followed?
YES 0 NO 5. Were sample ID's listed on the COC?
YES El NO 6. Were samples ID's listed on sample containers?
-74 YES 0 NO 8. Were tests to be performed listed on the COC?
NO 9, D�d sarnp�es arr�ve �n proper conta�ners for,each test'?
M. YES 0 NO 10. Did samples arrive in good condition for each test?
YES El NO 11 Was adequate sample volume availableT
04 YES 11 NO 12. Were samples received within proper holding time for reque"sted test s?
b YES El NO 14. Were cyanide samples re'ceived at a pH>12?
YES El NO 15. Were sulfide samples received at a pH >9?
44 21 16. Were NH3/TKN/Pheno"l received at a chlorine residual of<0'.5 m/L?
El YES 0 NO 17. Were Sulfide/Cyan,ide recei..ved at a chlorine residual of<0.5 m/L?
El YES 11 NO 18, Were ortho"phosphate samples filtered in the' field with'i..—.n15 minutes? -—------------.....
�* TO[/VoYa0es are pH checked at time ofana�ys�is and recorded mn the benchsheet. `
'** Bacteria samples are checked for CNodne at Vme of anaiysis and recorded on the benchsheet. �
Sample Preservation: (Must be completed for any sampie/x1 incorrectly preserved or with headspace)
Sample(s) were received incorrectly
accordingly�y
by adding (circle one): H2SO4 HNCL HC/ NaOH
- '�-- --'-'^^~ ~`^~'~'^' '
Time ofpreservation: — /f more than one preservative is needed,inotate /n comments below �
Note:Noffy customer service�mmediate[y for/ncorrecVy preserved samp�s.Obtain a new sample or
notify the state lab ifd/ectedtoana�yzedby the customer.Who was notifled,date and t�mei____
Vo/atUesSamp(e/s> were received with heads ace ----
-
COMMENTS:

ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington,NC 28405
OFFICE:910-392-0223 FAX [phone]
NCDENR: DWQ CERTIFICATION#94 NCDHHS: DLS CERTIFICATION#37729
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
CLIENT: City of Jacksonville PROJECT NAME: Monitoring Wells (Jacksonville LTS) REPORT NO: 2,1 — 2-2Z7 4, 3
ADDRESS: PO Box 128 CONTACT NAME: PO NO: 225042
Jacksonville, NC 28540 REPORT TO: Amy Palaschak PHONE/FAX:
COPY TO: E-MAIL: [e-mail]
Sampled By: ,,i 8 SAMPLE TYPE: I=Influent, E= Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection PRESERVATION
1E-
Sample Identification `2 itl IZ hi-) 8 if, 0 Es ANALYSIS REQUESTED
Date Time emp o
cn I— g o go. .cE 4..5, m 0 2 ,p, < - ,..=
c.) o z z z I z o
1,211313i 13°9 le 13 P TOC, Sulfate, Nitrate,
MW %•• W G G 0 311° X X X Chloride, VOC (SM 6200 C)
1,211 31.21 i gSS i b.c2) P TOC, Sulfate, Nitrate,
1 MW 4 W G G 553 i 1 X X X Chloride, VOC (SM 6200 C)
ialislal tc010 1--A.c1 _ . P TOC, Sulfate, Nitrate,
MW W G G 5534 x x X Chloride, VOC (SM 6200 C)
P TOC, Sulfate, Nitrate,
MW W G G X X X Chloride, VOC (SM 6200 C)
P TOC, Sulfate, Nitrate,
MW W G G X X X Chloride, VOC (SM 6200 C)
P TOC, Sulfate, Nitrate,
MW W G G X X X Chloride, VOC (SM 6200 C)
P TOC, Sulfate, Nitrate,
MW
_ _ _ W G G X X X _ Chloride, VOC (SM 6200 C)
_ . _
P TOC, Sulfate, Nitrate,
MW W G G X X X _ Chloride, VOC (SM 6200 C)
P TOC, Sulfate, Nitrate,
MW W G G X X X _ Chloride, VOC (SM 6200 C)
P TOC, Sulfate, Nitrate,
MW W G G X X X Chloride, VOC (SM 6200 C)
NOTICE-DECHLORINATION: Samples for Ammonia,TKN,Cyanide,Phenol and Bacteria must be dechlorinated(0.2 ppm or less)in the field at the time of collection. See reverse for instructions
Transfer pelin hed By: Date/Ti e Received By: Date/Time
. 1
1. • 1,9-114 tcA IOC°
2. --
Temperature when Received: 3 3 Accepted: Rejected: Resample Requested:
Delivered By: Received By: 7c4.--.. Date: a-M- Zi Time: kq'-50
Comments: TURNAROUND:

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6602 Windmill Way,Wilmington,NC 28405 a 910.392.0223 Lab a 910.392.4424 Fax
NI 01000001011
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710 Bowsertown Road,Manteo,NC 27954 & 252.473.5702 Lab/Fax
1011111111
255-A Wilmington Highway,Jacksonville,NC 28540 a 910.347.5843 Lab/Fax
1,110 III
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vivivivivimoo
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-55749 Site: MW-1 12/14/2021 11:11 AM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2 1,1993 14 mg/L 12/16/2021
Total Organic Carbon (TOC) SM 5310 B-2014 13.1 mg/L 12/15/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloroethane sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#:: 2021-22250 Page 1 of 18

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omoyouN
V pl 6602 Win mill Way,Wilmington,NC 28405 * 910.392.02231Lab * 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 * 252.473.5702 Lab/Fax
5"�' 255-A Wilmington l-highway,Jacksonville,NC 28540 * 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info@environmentaichemists..com
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50IJg/L 12/18/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Isopropylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 12/18/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
n-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
p-Isopropyltoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Styrene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Toluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#:: 2021-22250 Page 2 of 18

„IIIIIIIIIIIIIIIIINI101,11,011,111,11,0110101010101,,,,,,,,,,,,,,0101 0101010101 1111 7 I I 1 III1 1111 1 16 .1.1 11 ILI I .. 1 1 1.4:4 1 ' j.MM.1 0
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710 Bowset town Road,Man leo,NC 27954 * 252.473.5702 Lab/Fax
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255-A Wilmington Highway,Jacksonville,NC 28540 6 910.347 5843 L,ab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloride SM4500 Cl E-2011 48 mg/L 12/20/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev 2 0,1993 < 0.02 mg/L 12/15/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev 2 0,1993 0.03 mg/L 12/16/2021
Nitrate Nitrogen Subtraction Method 0.03 mg/L 12/28/2021
Report#: 2021-22250 Page 3 of 18

60O2 Windmill Way,Wilmington,NC 28405 ° 91.0.392.02251.*b ° 910392.4424 Fax
710Bowoertown Road,&�nteo,NC'27954 ° 252.4:73.5702 Lab/Fax
Wilrm�gton.1i'ligbvvay,juckoonvll�.NC28540 ° 9I0.347.5843Lmlb/Far
ANALYTICAL&CONSULTING CHEMISTS inGm@eovimanmmemtaUobeooiats.00mn
___
City mfJacksonville Date ofReport: Jan O5. 2O22
Post Office Box 138 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: AnnyPa|oachoh Report#: 2021-22250
Project ID: Monitoring Wells
Lab ID Sample ID: CoQeckDmte/Timmw Matrix Sampled by
21'65750 Sitw: N1N-2 12/14/2021 12:09PK8 VVotar NB
Test Method Fkemm|tw Date Analyzed
Sulfate EPA uo»4 Rev.x.1'1»oo <5mng/L 12/18/2021
Total Organic Carbon (TOC) am»»1»o-2»1* 4.2rng/L 12/15/2021
1.1.1.2-Tetnooh|onoathona sMnu»«c'»o11 < O.5Opg/L 12/18/2021
1.1.1-Trinh|onoothano omau«»c-2»11 < D.5OUg/L 12/18/2021
1.1.2.2-Totneoh|omoathana am«u»»c'u»11 <O.5OUg/L 12/10/2021
1.1.2-Triohlonoethane oma««»c-2«11 < O.5Opg/L 12/18/2021
1.1'Oich|onoethune omo:»»c'u»11 < 0.50pg/L 12/18/2021
1.1-Dich|onoethene om«o«»o-2»11 « O.GOpg/L 12/18/2021
1.1-Dich|onopnopene smnu»»c'u»11 < O.5OUg/L 12/18C2021
1.2.3-Trioh|onobanzmno oms»»»c-2»11 < O.SOpg/L 12/18/2021
1.2.3'Trioh|onopvopona uM»o»»c'u»11 < 0.50pg/L 12/18/2021
1.2.4-Trioh|onmbenzono amnu«»o-2»11 < O.5Opg/L 12/18/2021
1.2.4-Tri methyl benzene »me»»ou'u»11 < O.5OpQ/L 12/18/2031
1.2'Dibnomo-3'Ch|onopnopone amou»»u-2»11 < O.5Opg/L 12/18/2021
1.2'Oibnomoothuna amau»»c'x»11 « O.5OpQ/L 13/18/2021
1.2-Oiohlonobanzane sMno«»«'u«11 < O.6OUg/L 12/18/2021
1.2-Oiuh|oroethana ameu«»c'e«11 < 0.50pg/L 12/18/2021
1.2-Dioh|oropropono amuuo«u-2»11 < O.5Opg/L 12/18C2021
1.3.5-Tri methyl benzene omac»»o'»»11 < 0.50pQ/L 12/18/2021
1.3'Dioh|onobenzana amso»»c':»11 < O.6O;g/L 12/18/2021
1.3-Oioh}onopnopona sM»»«»u'x«11 < 0.50pg/L 12/18/2021
1.4-Dioh|onobenzono oM»u»»u'u»11 < 0.50pg/L 12/18/2021
2.2-Dich|onopnopane om«o»»u'»»11 < O.5Opg/L 12/18/2021
2-Ch|onoho|uena omsu»»o'u»11 < 0.50pg/L 12/18/2021
4-Ch|oroto|uene um«»»»u-2«11 « O.5Opg/L 12/18/2021
Benzene amnu»»c'u«11 < O.5Dpg/L 12/18/2021
manux#�: 2021-22250 Page 4m10

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6602 Windmill Way,Wilmington,NC20405 w 918.392.0223 Lab = 91.0.392.4424 Fax
M 471QBovveaotown Road,B�anweo,NCZ7954 a 252.473.5702Lob/Fax
"- ="� 2S5�A Wilmington Ifighwa�Jacksonville,NC2854Q a 91.0.347.5843Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan O5. 2O22
Post Office Box 128 Customer PO#:
Jacksonville MC 28541 Customer ID: 08110015
Attention: AnnyPa|aochoh Report#: 2021-22250
Project ID: Monitoring Wells
Bromobenzena ammm»o-2m11 < O.5Opg/L 12Y18/2021
Bnomooh|onornethane awsu»»u-u»11 < 0.50pg/L 12/18/2021
Bpomodioh|oromethane aw«o»»«'u«11 < O.5Opg/L 12/18/2021
Bromoform ameo»»o'u»11 < 0.50pg/L 12/18/2021
Bponnomethene aw«u»»u-2»11 1.80pQ/L 12/18/2021
Carbon tetrachloride om«»»»c'u»11 < O.5OpQ/L 12/18/2021
Ch|orobenzene em«u»»«-2»11 < O.5Opg/L 12/18/2021
Ch|ormethane swn»o»o-2»11 < O.5Dpg/L 12/18/2021
Chloroform amsu»»o'c«11 < 0.50pg/L 12/18/2021
Ch|oromethane aM«u»oo-2»11 1.14pg/L 13/18/3021
cis-1.2-Dich|oroethene amsuo»o'u»11 < O.5Opg/L 12/18/2021
cis-1.3-Dich|omopropene sm»u»»o-2«11 < 0.50pg/L 12/18/2021
Oibnomooh|oromethane mm000»«'uo11 < 0.50pg/L 12/18/2021
Dibronnommethone am*«»»o-2»11 < O.5Opg/L 12/18X3031
Dioh|orodif|uoronnethone amn»»»c'»»11 < 0.50pg/L 13/10/2021
Ethy|benzeno awao»»c-2»11 < O.5Opg/L 12/18/2021
Haxeohlorobutadiene am*o»»o-2o11 < O.5Opg/L 12/18/2021
|ooppopy|benzene ameu»»c-2»11 < O.5Opg/L 12/18/2021
W1+PXy|ene eMo»«»o'o»11 < 1.00pg/L 12/18/2021
Methylene chloride awnc»»c-2»11 < 0.50pg/L 12/18/2021
Naphthalene ewnuo»«'u«11 < O.5OpQ/L 12/18/2021
n-Buty|benzene am«c»»c'»»11 < O.5Opg/L 12/18/2021
n-Propy|benzeng smeu»»u-2o11 < D.5Opg/L 12/18/2021
odho-Xy|ene nmn»»»c'u«11 < O.50pg/L 12/18/2021
p-|mopnopy|bo|uene aMec»oo-2»11 < O.5OpQ/L 12/18/2021
eec-Buty|benzene am«u»»u'o»11 < O.5Opg/L 12/18/2021
Styrene awnc»«o-2»11 < O.5Opg/L 12/18/2021
tedt-Butylbenzone awsu»»u'u»11 < D.5Opg/L 12/18/2021
7-etnaoh|oroethene eweo»»o'u»11 « 0.50pg/L 12/18/2021
Toluene amoco»«-2»11 < O.5Opg/L 12/18/2021
Rennrtw:: 2021'22250 Page am10

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710 Bowsertown Road,Monte°,NC 27954 * 252.473.5702 1,ab/Fox
11111111111111111111111111111111111111,11,1111111111111111111111111111IIIIIIIIIIIIIII0OIIIIII ° 5M 255-A Wilmington Highway,Jacksonville,NC 28540 0 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 <0.50 pg/L 12/18/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloride SM4500 Cl E-2011 46 mg/L 12/20/2021
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/15/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.05 mg/L 12/16/2021
Nitrate Nitrogen Subtraction Method 0.05 mg/L 12/28/2021
Report#:: 2021-22250 Page 6 of 18

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710 Bowser town Road,Monte°,NC 27954 0 252.473.5702 Lab/Fax
6616°1111111111111111111111!111111111
iltoss11111 1 P'4 255-A Wilmington Highway,Jacksonville,NC 28540 0 910 347 5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-55751 Site: MW-11 12/14/2021 10:18 AM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2.1,1993 <5 mg/L 12/16/2021
Total Organic Carbon (TOC) SM 5310 B-2014 <0.5 mg/L 12/15/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#:: 2021-22250 Page 7 of 18

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710 Bowsertown Road, , ,NC Manteo 27954 * 252A711,5702 Lab/Fax
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11111 IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIMmally110111011 m. " II F I a facksonville,NC 2.8540 6 91 0341.,5843 Lab/Fax
255 A Wilmington rig lw,y,
ANALYTICAL&CONSULTING CHEMISTS info@eavironmentalchernist&com
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromochioromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromomethane SM 6200 C-2011 1.44 pg/L 12/18/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloromethane SM 6200 C-2011 1.06 pg/L 12/18/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
lsopropylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 12/18/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
n-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
p-Isopropyltoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Styrene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Toluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#: 2021-22250 Page 8 of 18

1,11111111111111111111111111111111111111111111111\11111\1111111111111111111111111111111111,j1 11111111111111 111111111111111111111111111111
1111111111111nere 1111111111 1 I $ 1 .1111 1 mil I 1 1111 1 .111 1 1*
1111111111111111111111.1111114011
11101111161l 6602 Windmill Way,Wilmington,NC 28405 e 910 392.022;3 Lab * 910 392A424 Fax
no80011111,1111111111111111011010011144,11114,11111111400i4,119 ,4191u5,6,111111111411111111111111111111111111111111111111111111111111111111111111111111111111111
""11111:1111111111111111111THIsg*;;;; 1* 1111101111111110110000mi 11 1
1111111111111111111111111111111111111111111Foommo 710 flowsertown Road,Manteo,NC 27954 * 252.475 5702 11,ab/Fax
11 0118111111 M
11 1111111111111111 sahlrilinnomos 2'.)5-A Wilmington Highway,Jacksonville,NC 2.8540 4 910.347.58431,ab/Fax
woololololoomp
1 *somoomommommol0000000000000
ANALYTICAL&CONSULTING CHEMISTS in fo@environnlentalckemists COrn
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloride 5M4500 CI E-2011 5 mg/L 12/20/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/15/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.28 mg/L 12/16/2021
Nitrate Nitrogen Subtraction Method 0.28 mg/L 12/28/2021
Report#:: 2021-22250 Page 9 of 18

UW!
111111111111111111111111111111 6 l I� 16I ll' T 1 1 A d f l i, I I!iii` 11111 .
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ai 11„100000000
I, oennioll 6602.Windmill Way,Wilmington,NC 28405 a 91.0392.0223 Lab m 910.392.4424 Fax
710 1Lowsertown Road,Manteo,NC 2.7954 4' 2.52..473.5702 Lab/Fax
111111111111111111111111111 111 P ;�M; 2.55-A Wilmington Flighnway,Jacksonville,NC 28540 a 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-55752 Site: MW-15 12/14/2021 12:59 PM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2.1,1993 <5 mg/L 12/16/2021
Total Organic Carbon (TOC) SM 5310 B-2014 0.7 mg/L 12/15/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#.. 2021-22250 .�...- Page 10 of 18

1,11,111,111,11,11,11,11,11,111111111111111111111111111111111111111111111111111111111111111111111116*IIIIIIII , 1 1 I I 1 I 1 I 1 H aw .1 Imil 1 ,1 .11 .
11111111111111111111111 10.1.1.1.01Not 11.11,111,11,11,111
11.0titirot 1.11111111111011111 .volfitill11111111 6602 Windmill Way,Wilmington,NC 28405 * 910392.0223 Lab 0 910.392 4424 Fax
11:11111111111111111111111111,0NINibier II e
001,100000;011111 weeejlembe
710 Bowsertown Road,Manteo,NC 27954 .0 252.473.5702 Lab/Fax
1111111111111111111111%behiNiiiii!:111111111111111111111111111111111111111000 ,,m
11 255•.A Wilmington Highway,Jacksonville,NC 28540 * 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
lsopropylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 12/18/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
n-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
p-lsopropyltoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Styrene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Toluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report# 2021-22250 Page 11 of 18

1.1111111,111,10„„„11,1,111111111 11111,111111111111111111111111111111111111111111111,,,,,,,,,,11100,
1 111111111_-1111,4411111111,1,1,1,1,1,1,1,1,1,1,1,,,,,,,,,!,0010101010101,,,,,,,,00,111111111
1.111111110mir 0 101401011Billl.111 6602 Windmill Way,Wilmington,NC 28405 0 9.10.392.0223 Lab * 910392A424 Fax
mosBoosh1111111111111111111111.1
710 Bowsertown Road,Manteo,NC 27954 * 252473.5702 Lab/Fax
1111111111!1L* *11111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111110111111**111
255•-A Wilmington Highway,Jacksonville,NC 28540 * 910.347.5843 Lab/I'Iax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
sz .
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene sm 6200 C-2011 < 0.50 pg/L 12/18/2021
Trans-1,3-dichloropropene sm 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichlorofluoromethane sm 6200 C-2011 < 0.50 pg/L 12/18/2021
Vinyl chloride sm 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloride SM4500 CI E-2011 41 mg/L 12/20/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/15/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 2.68 mg/L 12/16/2021
Nitrate Nitrogen Subtraction Method 2.68 mg/L 12/28/2021
Report#. 2021-22250 Page 12 0118

RRRNkN h
11-1010tv 0 III,,,,vivliv,,,,,IIIIIIIIIIIH11,;HolIVIIVI;l'illoivill11111110111V PONININ111110101011111111111111111111111111111111
lip I ' 6602 Windmill Way,Wilmington,NC 28405 ' 910.392.0223 Lab * 9110.392.4 24 Fax
1110111111111 11111111111111111 moll moo ill
710 43owsertown Road,Manteo,NC 27954 * 252.473.5702 Lab/Fax
255.A Wilmington Highway,Jacksonville,NC 28540 * 910.347.58413 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info@,environmentalchemnusts.corm
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention:. Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-55753 Site: MW-16 12/14/2021 2:50 PM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2.1,1993 6 mg/L 12/16/2021
Total Organic Carbon (TOC) SM 5310 B-2014 1.1 mg/L 12/15/2021
1,1,1,2-Tetrachloroethane sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,1-Trichloroethane sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2,2-Tetrachloroethane sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2-Trichloroethane sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethene sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloropropene sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichlorobenzene sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichloropropane sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trichlorobenzene sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trimethylbenzene sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromoethane sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichlorobenzene sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichlorobenzene sM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,4-Dichlorobenzene sM 6200 C-2011 < 0.50 pg/L 12/18/2021
2,2-Dichloropropane sM 6200 C-2011 < 0.50 pg/L 12/18/2021
2-Chiorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
4-Chlorotoluene sM 6200 C-2011 < 0.50 pg/L 12/18/2021
Benzene sM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#:: 2021-22250 Page 13 of 16

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6602Windzmill Way,Wilmington,NC20405 ° 910.392,0223 Lab ° 918.S9144.24 Fax
-� �1QBowaeztmvvn Road,B�anteo,��C27954 ° 252.473.5702Lab/Fax
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255-.A Wilmington Flighway.,Jacksonville,NC2854U = 910,347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS im0o@envirmnmmemtalchemoimm.00mm
City of Jacksonville Date ofReport: Jan D5. 2D22
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: AnnyPe|amcheh Report#: 2021-22250
Project ID: Monitoring Wells
Bromobenzene smeo»»c-2m11 < O.5OpQ/L 13/18/2021
Bromnoch|onomethane mwee»«C-2»11 < O.5Dpg/L 13/18/2021
Bnomodioh|ononmethane awsu«»c'u»11 < 0.50pQ/L 12/18/2021
Bpomnofornn swouo»u'«»11 < O.5OpQ/L 12/18/2021
Bromomethane amsuo»n-2»11 < D.5Opg/L 12/18/2021
Carbon tetrachloride amnu«»u'o»11 < O.5Opg/L 12/18/2021
Ch|onobenzene amnu»«o-u»11 < O.5Opg/L 12/18/2031
Ch!omoethone amoo»»o'u»11 < O.5Opg/L 12/18/2021
Chloroform aw«u»«n'u»11 < 0.50pg/L 12/18/2021
Ch|oromathene amno»»u-2»11 < 0.50pg/L 12/18/2021
cis-1.2-Dich|onoethene omao»»u-2»11 < O.5Opg/L 12/18/3021
cis-1.3-Dioh|onopropene aws»»»o'o»11 < O.5Opg/L 12/18/2031
Dibnomoch|onomethane amno»»c'««11 < O.5Opg/L 12/18/2021
[)ibronnonnethane amoo»»o'c»11 < D.5Opg/L 12/18C2021
Dioh|orodiOuonomathane emou»»c'«o11 < D.5Opg/L 12/18/2021
Ethy|banzene ameo»«o'»»11 < O.5OpQ/L 12/18/3021
Hexaoh{onobutadiene amuu»»c'»»11 < 0.50pQ/L 12/18/2021
|eopnopy|benzene amau»on-2»11 < O.5OpQ/L 12/18/2021
M+P|4y|one smoo»ou-2»11 < 1.00pg/L 12/18/2031
Methylene chloride aM«»«»o'z»11 « 0.50pg/L 12/18/2021
Naphthalene Swe»»»«-2»11 < 0.50pg/L 13/18C2021
n-Buty|benzene Smou»»o-2»11 < O.5Opg/L 12/18/2021
n-Propy|banzene aw«u»»o-2»11 < O.5OpQ/L 12/18/2021
ortho-Xy|ene aw«u»»o'o»11 < O.5Opg/L 12/18/2021
p-|eopropyito|uane aw*««»c-2»11 < 0.50pg/L 12/18/2021
aeo-Buty|benzene sm*o»»c'o»11 < O.5Opg/L 12/18/2021
Styrene aM»u«»u-2o11 < O.5Opg/L 12/18/2021
hert-Buty|benzene Sm«c»»o-2»11 < O.5Opg/L 12/18/2021
Tetnanh|omoethane awez»oo'c»11 < O.5OpQ/L 12/18/2021
Toluene am«u«»o'o»11 < O.5Qp0/L 12/18/2021
Report#:: 2021'22250 Page 1*of 18

,11111111111114111111111111111114 111111111,111111 11111..1111111111
111111111111111111111111111111111111111111111111111111111141111111111111111111111111111111111111111111111111111111ii:1111Hoolloolloo 1111
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11111111111111,1111100107110 olio 0 oi 1111 1111 oil lillIhIqh 6602 Windmill Way,Wilmington,NC 28405 * 910.392 0223 Lab * 910.392.4424 Fax
9111,001:111:1111:1111:1111111111111111111111111111111111111111111111111111111111001
IVIVil000NtmovolygIIIII4itvvMg9Thpl9** C.R4 710 Bowsertown Road,'Wandler),NC 27954 * 252.473.5702 Lab/Fax
255 A Wilriiin:ton Highway,Jacksonville,NC 28540 * 910.347 5843 Lab/Fax
11111111iiilividiviVirovidoloolorgl1111111111111111
ANALYTICAL&CONSULTING CHEMISTS infogenvirohmentalchemists.coin
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichioroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloride SM4500 CI E-2011 29 mg/L 12/20/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev 2 0 1993 < 0.02 mg/L 12/15/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev 2 0,1993 0.09 mg/L 12/16/2021
Nitrate Nitrogen Subtraction Method 0.09 mg/L 12/28/2021
Report#. 2021-22250 Page 15 of 18

r III I 111111411111111111,
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o,. ' % ,I .,1l,.I.i � I„pJ / f.a 1,,,,, ,l�%,Ji,,, /'!a W.. i�I,,,, 41
,fl toommos 41i I I I' 6602 Windmill Way,Wilmington,NC 28405 ' 910.392.0223➢ab ' 910.392.4424 Fax
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IIIwo 7:10 Bowsertown.Road,Manteo,NC 27954 ' 252.473.5'7021Lab/Fax
�; 255--A Wilmington aoksonville,NC 28540 ' 910.347.5843 Lab/Fax
➢� Highway,h gwaY U
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-55754 Site: MW-17 12/14/2021 2:03 PM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2 1,1993 10 mg/L 12/16/2021
Total Organic Carbon (TOC) SM 5310 B-2014 0.7 mg/L 12/15/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 <0.50 pg/L 12/18/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#:: 2021-22250 Page 16 of 18

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6602 Windmill Way,Wilmington,NC 28405 '''' 910.392,0223 Lab * 910,392 4424 Fax
III moodoso,11,11111111111111*
1111
IIIIIIIIII*110111111111114101111111,111,1111111111111111111111,0141161,11,11,11,11,1011
voNsoomeg1h111111111111111111111111111111111111111111111112111 m
NIIIIIIIIIIIIIIIIIIIigulli011111111
710 Bowsertown Road,Manteo,NC 27954 0 252 473.5702 Lab/Fax
111'211111111110morn1fl1g11111111111111111111111111111111111101111111111111110100010101010101 &
I,* 1111111111
255 A Wilmington Highway,Jacksonville,NC 28540 * 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
lsopropylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 12/18/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
n-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
p-Isopropyltoluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Styrene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Toluene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Report#:: 2021-22250 Page 17 of 18

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11111111111111111111111111111111111111111111111111111111111,1111,1111,1111,1111,11111,1111,1111,1111,1111,1111,1111,1111,1111,1010orrol s.
710 Bowsertown Road,Manteo,NC 27954 * 252.473 5702 Fab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 * 910 347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22250
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/18/2021
Chloride SM4500 CI E-2011 25 mg/L 12/20/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/15/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/16/2021
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/28/2021
Comment:
Reviewed by:
Report#:: 2021-22250 Page ladf 15

Environmental Chemist,
, 6GO2 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
/ ^ / | /
U~ |
Oient� � 1--L~ /\ t' / \//U[Date� / /1 |��|7 / Report �[>��--7-� ��c�r�
_ / � �-^-^-c_a._)
Receipt ofsample: ECHEK8Pickupx Client Delivery[] /UP3 [] FedEx [7 Other[]
0YES NO N/A VVerecustody sea�present o ^the coo|er?
0 YES IEl NO Ncin. 0/A /f custody seals xverepresenLwere they intact/unbroken?
Original temperature upon receipt ) I
"[ [nrrec�edtenn t. temperature
H +
How [] Temperature ��
Blank � Against8ott/es
/R Gun ID:Thomas Traceable S/N 192511657 /R Gun Correction Factor"[: 0.0
-X YES [] NO 3. If temperature of cooler exceeded VC, was Project Mgr./QA notified?
YES O NO
per custody procedures (relinquished/received) followed?
YES O NO 5. Were sample ID's listed on the COC?
� YES El NO 6. Were samples ID's listed on sample containers?
YES [] NO 7. Were collection date and time listed on the COC?
�J YES [] NO
uw YES [] NO 9. Did samples arrive in proper containers for each test?
;5 YES [] NO Did samples arrive in good condition for each test?
80 YES [] NO 11. Was adequate sample volume available?'
0U YES [] NO 12. Were samples received within proper holding time for requested tests?
YES [] NO 13. Were acid preserved samples received atapHof<J? *
[] YES [] NO 14. Were cyanide samples received ata pH >12?
�
YES [] NO 15. Were sulfide samples received atapH»9?
[] YES [] NO 16. Were NH3/TKN/Pheno/ received ata chlorine residual of«O5mn/L? **
0YES [] NO 17. VVeneSu/� Ode/[yanidereceiveda�ach/orineres/dua| of� 5'mn/`^?
[] YES [] NO /18. Were orthophosphate samples filtered in the field within '5 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
�* Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any samp|e(s) incorrectly preservedorvithheadspace'Samp|e(s) were received incorrectly preserved and were adjusted according
/ybyadding /circ(eone\: H2SO4 HNO3 HO NaOH
Time ofpreservation: |f more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Vo|a1i/es5amp/e(s) were received with headspace
COMMENTS:
DO[ QA.002 Rev 1

,__.„...,...,
,e_iteirmakw ENVIRONMENTAL CHEMISTS INC 6602 Windmill Way Wilmington,NC 28405
OFFICE:910-392-0223 FAX [phone]
NCDENR: DWQ CERTIFICATION#94 NCDHHS: DLS CERTIFICATION#37729
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
CLIENT: City of Jacksonville PROJECT NAME: Monitoring Wells (Jacksonville LTS) REPORT NO:
ADDRESS: PO Box 128 CONTACT NAME: PO NO: 225042
Jacksonville, NC 28540 REPORT TO: Amy Palaschak PHONE/FAX:
COPY TO: E-MAIL: [e-mail]
Sampled By:I* SAMPLE TYPE: I=Influent, E=Effluent,W=Well,ST=Stream,SO=Soil, SL=Sludge, Other:
Collection A, "a a W PRESERVATION
Iii• 0, 0, .0 .. Lli .E. ...1 2 w
Sample Identification 1—gg-, a ' tE a•
l'i '8 ti lib Da 1 w _, 8 - = 0 ,T, ANALYSIS REQUESTED
(13 F ° E •Ici = g 0 0) 2 .c) E x
U3 6 0 (-3 Z Z i '1 x
a e Time Temp
aliLi ;i Int P TOC, Sulfate, Nitrate,
MW 1-4.fa W G G ,(17-119 X X X 42- Chloride, VOC (SM 6200 C)
9-051 19, 1, P
L.,--)4-1- TOC, Sulfate, Nitrate,
MW )--, I u, v-' W G G 3-7----z:1 X X X 1-1' Chloride,VOC (SM 6200 C)
1M P TOC, Sulfate, Nitrate,
ILS
MW \ t W G G SS ,-) x x x L2-PL/ Chloride, VOC (SM 6200 C)
13,Gel tl L4 P TOC, Sulfate, Nitrate,
MW 1 G. W G G 5 -1:,1:-2-. X X X 47-fl— Chloride, VOC (SM 6200 C)
MW RD IL5O 1V*4 P
W G G b-S7 5- x x x '-'7--# TOC, Sulfate, Nitrate,
Chloride, VOC (SM 6200 C)
0 P TOC, Sulfate, Nitrate,
MW 11 NJ 0-103 1 Gi
W G G t- 1 511 x x x '2'6-
Chloride, VOC (SM 6200 C)
P TOC, Sulfate, Nitrate,
MW W G G X X X Chloride, VOC (SM 6200 C)
P TOC, Sulfate, Nitrate,
MW W G G X X X Chloride, VOC (SM 6200 C)
P TOC, Sulfate, Nitrate,
MW W G G X X X Chloride, VOC (SM 6200 C)
_ P TOC, Sulfate, Nitrate,
_
MW W G G X X X Chloride, VOC (SM 6200 C)
NOTICE-DECHLORINATION: Samples for Ammonia,TKN,Cyanide,Phenol and Bacteria must be dechlorinated(0.2 ppm or less)in the field at the time of collection. See reverse for instructions
Transfer Relinquished By: ate/Time Received By: Date/Time
a11111:21 - 1530
2.
Temperature when Received: \ . , ,t)C---- Accepted: / R jected: Resample Re uested:
Delivered By: Received By: .A l - Date: 17-115 2) Time: •
Comments: i TURNAROUND:

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II
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lo III -July*l� „I ( , , n QI 6602 Windmill Way,Wilmington,NC 28405 ° 910.392.0223 Lab * 910.392.4424 Fax
710 Bowsertown.Road,Manteo,NC 27954 0 252.473.5702 Lain/.Fax
" "nt" h 255-A Wilmington Highway,Jacksonville,NC 28540 ° 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56049 Site: MW-6 12/15/2021 12:24 PM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2.1,1993 17 mg/L 12/17/2021
Total Organic Carbon (TOC) SM 5310 B-2014 7.1 mg/L 12/21/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 ig/L 12/19/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Report#:: 2021-22386 Page 1 of 21

'Ily '''''''''"°11'1111'11111111111110""""""imil 1111111111111111111111111
11111111111:111111I iiimo1111111111111111111111111001"1111.111111 1 11 111111. 111 11. 1111
080016#10111191111101h401 ol „II 1111111111111f 6602 Windmill Way,Wilmington,NC 28405 * 910.392.0223 Lab * 910.392A424 Fax
1111111111111111111111111 1111111111111111110111111101010111110111IIIIIIIIVIIIIIIIIIIIIM I 1111111
IIIIIIIIIIIIIIIIIIIIIIIIII11111111111111111111111111111 1 'ovl 710 Bowsertown Road,Manteo,NC 27954 * 252.473.5702 Lab/Fax
255•-A Wilmington Highway,Jacksonville,NC 28540 "" 910.3475843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infogenviromnentalchemists.com
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Isopropylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 12/19/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
n-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
p-lsopropyltoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Styrene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Toluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Report#:: 2021-22386 Page 2 of 21

1,11 0111100111111111111111111 11111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111116 „ ,„„J,1 ,1 11 1 1 1111 1 1 1 1 1 1 '1 111 1 1 1111 la 1 .1 1 1 1111 lb.,. „ „„ 1111 11 0
1 014,, 011111111111111011111111;1111111111VIVIV1111111111111111111111111111111111111111111111e111;;;11111111101111111111111111111111111111111111111111111111111010
11111111VVVVVVII0 111 11 11111 113 1 1111 1 101 11 11 NI 111111011l$h 6607 Windmill Way,Wilmington,NC 28405 "' 910.392.0223 Lab ' 910.392.4424 Fax
11111"111111111111111111111111010!IILIIIIIIIII111,10101010100011„
710 Bowsertown Road,Manteo,NC 27954 * 252.473 5707 Lab/Fax
000010111l01111010001
11111111111111111111111111111111111111IIII1111101010111 255•-A Wilmington Highway,Jacksonville,NC 28540 " 910347 5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloride SM4500 CI E-2011 23 mg/L 12/20/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353 2,Rev.2.0,1993 0.16 mg/L 12/17/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.05 mg/L 12/20/2021
Nitrate Nitrogen Subtraction Method <0.02 mg/L 01/03/2022
Report#. 2021-22356 Page 3 of 21

I (D i I.I.. GI 1111 l(f ,ll,r„
J �1
1 nNI 6602 Windmill Way,Wilmington,NC 28405 m 910 392 0223 Lab m 91.0.392. ±.24 Fax
IIIIIIIIIIIIIII��� �' 255-A Wiimington Highway,Jacksonville,NC 28540 * 910.347.5843
Lax
1111111111111111111 11 71013owsertown Road,Manteo,NC 27954 2,52.473.5702 L..,a
Illo
41..a11T/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56050 Site: MW-7 12/15/2021 9:47 AM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2 1,1993 30 mg/L 12/17/2021
Total Organic Carbon (TOC) SM 5310 B-2014 7.1 mg/L 12/21/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Report# 2021-22386 Page 4 of 21

F�O��� N� k� �~ � ^�� ������ �
0602 Windmill Way,Wilmington,NC28405 ° 910.392.0223Lab ° 9.10.392.4424Fox
7I8Bowsertnwn Road,Manveo'NC2795@ a 252.473.5702Lab/Fax
255-AWilnzinghmnlligbwayjackoonville'.NC28540 ° 91.0.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS inOm(geoviremmaentaUci.ieoa�ato.conm
City pfJacksonville Date of Report: Jan OS. 2O22
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: AnnyPa/aoohak Report#: 2021-22388
Project ID: Monitoring Wells
8romobanzena amn:»»c-2«11 < O.5Opg/L 12/19/2021
Bnomoch|onornothone um«uu u-2011 < D.5Opg/L 12/19/2021
Bromodioh|onomathane oMao»»c-2»11 < O.5Opg/L 12/18/2021
8nomoformn »m«u»»«'x»11 « 0.50Ug/L 12/19/2021
Bromomedhone »M«»»»c-2»11 <D.5OUg/L 13/19C3021
Carbon tetrachloride omn:«««'e«11 < O.5Opg/L 12/19/2021
Ch|orobanzena am«u»oo'u»11 < O.5DUg/L 12/19/2021
Ch|onoethane smsu»»«'u«11 < O.5Opg/L 12/19/2021
Chloroform oM«u»««'u»11 < O.SOpg/L 12/18/2021
Ch|onomethana »m«e»»u-2«11 « O.5OUg/L 12/19/2021
cis-1.2-Diohloroothena »m«u««u'o»11 < O.5Opg/L 12/18/2021
cis-1.3-Dioh|oropnopene ama»»»«'u«11 <O.6Dpg/L 12/19/2021
Oibnomooh|opomethane ameu««o'u»11 < O.5Opg/L 12/19/2021
Oibnomornothana om«u«»«':»11 < O.5Opg/L 12/19/2021
Dioh|orodifluoronnethane sm«eo»u'o«11 < O.5Opg/L 12/19/2021
Ethy|benzano om«c«»«'»»11 < O.5Opg/L 12/19/2021
Hexach|onobubsdieno smno»»u'c»11 < O.5Opg/L 12/18/2021
|sopnopy|benzene ow«u«»u'u»11 = O.6Dpg/L 12/18/2021
K8+PXy|ene ow»u»«u'u»11 < 1.00pg/L 12/18/2021
Methylene chloride om«uo»c'»»11 < 0.50pg/L 12/18/2021
Naphthalene oM«x»»o-2»11 <0.50pg/L 12/19/2021
n-Buhy!benzano om»x«»u'«»11 < 0.50pg/L 12/19/2021
n-Propylbanzene omuu»«o'u»11 <O.SOpQ/L 12/19/2021
ortho'Xy|ono om«u«»u-2«11 < 0.50pg/L 12/19/2021
p-|oopnopy|to|uono om«o»»c'»»11 < O.5Opg/L 13/19/2021
oeu'Buty|benzene om««»«c'u«11 < 0.50pg/L 12/19/2021
Styrene sw«o«o«-2«11 < O.5Opg/L 12/19/2021
hed-Buty|benzene sm«u»»u'u»11 < O.5Opg/L 12/19/2021
Tatroch|onoathena ownc»»u'o»11 < 0.50pg/L 12/19/3021
Toluene «m«u«»c-2«11 < 0.50pg/L 12/19/2021
Report#. 2021'22386 Page smu1

r I IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII1 o
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1 1011,111111111111110****13$11111111110111111111111111111114 1
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2111111118111 101010101,11,110000#11111111111111111111111101111111
1111111111111111111111111,!04111181:111r00 11611* 111 1110011111111111111111111 6602 Windmill Way,Wilmington,NC 28405 * 910.392.0223 Lab 0 910.392 4424 Fax
710 Bowsertown Road,Mantco,NC 27954 6 252.473.5702 Lab/Fax
115080011 oiloomo
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movvvylviololo,0111111111111111111111111111 cohohoomm w
10100000000 III 11111111
255-A Wilmington Highway,Jacksonville,NC 28540 * 910.347.5843 i,ab/Fax
111111111111111111111111111111
ANAL'YTICAL&CONSULTING CHEMISTS [e-mail]
11 11111 locohy
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloride SM4500 Cl E-2011 27 mg/L 12/20/2021
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/17/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/20/2021
Nitrate Nitrogen Subtraction Method <0.02 mg/L 01/03/2022
Report#: 2021-22386 Page 6 0121

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,,,, ,,,,,,,,wol" 0110112L1111111::„„ 9 6
6602 Windmill Way,Wilmington,NC 28405 a 910392.,0223 Lab a 910 392 4424 Fax
ilt606 it to 1111111 11.61106
710 Bowsertown Road,Manteo NC 27954 252.473T5702 Lab/Fax
0006600666 11111111 IDIDIDIDIDIDIDIDIDIDIDIDIDIIIIIIIIII0
1111111" lay010101000000L11111,11111111111 ,,,,,m
255-A Wilmington Highway,Jacksonville,c NC 28540 a 910347,5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info@environmenialehemisttcom
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56051 Site: MW-12 12/15/2021 10:41 AM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300 0,Rev.2 1,1993 6 mg/L 12/17/2021
Total Organic Carbon (TOC) SM 5310 B-2014 26.2 mg/L 12/21/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dibromo-3-Chloropropane SM szoo c-zoli < 0.50 pg/L 12/19/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Report# 2021-22386 Page 7 of 21

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6602 Windmill Way,Wilmington,NC 28405 * 910.392.0223 Lab * 910.392.4424 Fax
��� 11111
710 Bowsertown.Roa d,Manteo,NC 27954 * 252.4'73.5702 Lab/]F'ax
255-.A Wilmington Highway,Jacksonville,NC 28540 0 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Isopropylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 12/19/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
n-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
p-lsopropyltoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Styrene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Toluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Report#:: 2021-22386 Page 8 of 21

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710 Bowsertown Road,Monte°,NC 27954 * 252.473.5702 Lab/Fax
11111111 1101 iv
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255 A Wilmington Highway,Jacksonville,NC 28540 a 910.347 5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS inib@covii onm entalchemists.coin
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloride SM4500 CI E-2011 < 5 mg/L 12/20/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 0.05 mg/L 12/17/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.03 mg/L 12/20/2021
Nitrate Nitrogen Subtraction Method <0.02 mg/L 01/03/2022
Report#,: 2021-22386 Page 9 of 21

vvolollhy41121:1111111:1111111111111 0000000000000000040o
vivivigooili41
o0 1A111111111 6602 Windmill Way,Wilmington,NC 28405 6 910,392.0223 Lab ii 910.391,414 24 Fax
111111111116000 1 iii111111111111111111,11,11,11,11,11040011
710 Bowspritown Road,Manic°,NC 27954 ok 252.473.5702 Lab/Fax
oligglimigoir _
"111 1111110,11,110411111111141111111111111111111111111,111,11,11,411111111111111111111111111111,111,111,111,1,1,1,11,11,11,11,1,1,1,1,1,1,1,1,1,1,11111111011iiiiiiilloillosiiii
iiiiiililililiIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII,ggill""IIIIIII'll'Ill'Il 00 '''" 255-A Wilmington Highway,Jacksonville,NC 28540 6 910347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56052 Site: MW-9 12/16/2021 8:43 AM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2 1,1993 97 mg/L 12/17/2021
Total Organic Carbon (TOC) SM 5310 B-2014 2.3 mg/L 12/21/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Report#.: 2021-22386 Page 10 of 21

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ANALYTICAL&CONSULTING CHEMISTS [e-mail]�clicoists.cwnm
City mfJacksonville Date ofReport: Jan O5. 2O22
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: AnnyPa|aachak Report#: 2021'22388
Project |D: Monitoring VVeUo
Bnomobanzane smum»c-2m11 < O.5Opg/L 13/19/2021
8romochlononnathana omsu»»o'u»11 < O.SOpg/L 12/19/2021
Bnomodioh|oromathmne om«u«»u'o»11 < 0.50Ug/L 12/19/2021
Bnomoform amse»»«-2»11 < D.SOpg/L 12/19/2031
8romoma{hane om«u»»u'u«11 < O.6Opg/L 13/19/2021
Carbon tetrachloride um«««««'u«11 < 0.50pg/L 12/19/2021
Ch|opobenoone aM«u«»«'««11 < D.SOpg/L 12/19/2021
Ch|onoothane »m«u»««'»»11 < 0.50pg/L 12/18/2021
Chloroform amsu«»u'u«11 < D.5Dpg/L 12/10/2021
Ch|oromethane sm«o»««'u»11 < O.5Opg/L 12/18/2021
cis-1.2-0oh|onoethane sM»o«»«'u«11 < O.5Dpg/L 12/19/2021
cis-1.3-Oich|onopnopane »m«u»»c'u»11 < 0.50pg/L 12/19/2021
Oibromooh|onomethana »m»o»»«'x«11 < O.5Opg/L 12/10/2021
Oibnomomethuno sm«e««o'c»11 < 0.50pg/L 12/19/2021
Dioh1onodifluononnathone amsu»»u'»»11 < O.5DUg/L 12/19/2021
Ethy|banzene aM«u««u'u«11 < O.5Dpg/L 12/19/2021
Hanach/onobutadiene aMsu»»c'x«11 < O.5OUg/L 12/19/2021
|eopnopy|banzena ow«««»u'o»11 < O.5Opg/L 12/18/2021
WY+pXy/eno am«u»»c'u«11 < 1.00pg/L 12/10/2021
Methylene chloride am«»«««'o»11 < O.5Opg/L 12/19/2021
Naphthalene »m«u»»c'u»11 < O.5Opg/L 12/19/2021
n-Buty|benzena om««««o'u»11 < O.5Opg/L 12/19/2021
n-PnoAy|benzena amoo«»«'«»11 < O.50pg/L 12/19/2021
ortho-Xy|ona om«u»«o-2»11 < O.5OUg/L 12/10/2021
p-|oopnopy|to|uene sm«u»»c'o»11 < 0.50pg/L 12/19/2021
sec-Buty|benzeno omou»»c'u»11 < O.SOpg/L 12/19/2021
Sb/nana smnu««c'»»11 < O.5Opg/L 12/19/2021
tart-Butylbenzene um»c«»«'u«11 < O.5Dpg/L 12/19/2021
Tetrach|onoethena »m«u««c'u»11 < 0.50pQ/L 13/18/2021
Toluene oMo:»»«'u«11 < O.5OUg/L 12/19/2021

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6602 Windmill Way,Wilmington,NC 28405 6 910.392,0223 Lab 't 910.392.4424 Fax
111 1111111111111111111111111111111111111111111111111111111111151;11111110 Oil 9 m 7.10 Bowsertown Road,Manteo,NC 27954 6 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 a 910347 5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloride SM4500 CI E-2011 7 mg/L 12/20/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev 2 0,1993 < 0.02 mg/L 12/17/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev 2 0 1993 < 0.02 mg/L 12/20/2021
Nitrate Nitrogen Subtraction Method <0.02 mg/L 01/03/2022
Report#. 2021-22386 Page 12 of 21

1,111111,11mosoloiiii1101111011hhi111o;1110111114111111111111111111111111111;i0 oolo!iiirri.
6602 Windmill Way,Wilmington,NC 28405 * 910392.02231Lab * 910.392.4424 Fax
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710 Bowsertown Road,Manteo,NC.27954 * 252473.5702 Lab/]Fax
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ANALYTICAL&CONSULTING CHEMISTS ini'[e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56053 Site: MW-10 12/16/2021 9:16 AM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2.1,1993 129 mg/L 12/17/2021
Total Organic Carbon (TOC) SM 5310 B-2014 2.0 mg/L 12/21/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,1-Trichioroethane SM 6200 c-2011 < 0.50 pg/L 12/19/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloropropane SM 6200 c-2011 < 0.50 pg/L 12/19/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
2,2-Dichloropropane SM 6200 c-2011 < 0.50 pg/L 12/19/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Benzene SM 6200 c-2011 < 0.50 pg/L 12/19/2021
Report#:: 2021-22386 Page 13 of 21

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710 Bowsertown Road,Manteo,NC 27954 g 252A73.5702 Lab/Fax
11111111' wwwwwwwe bl,
255•A.Wilmington Highway,Jacksonville,NC 28540 a 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Isopropylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 12/19/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
n-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
p-Isopropyltoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Styrene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Toluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
,.... .
Report#:: 2021-22386 Page 14 of 21

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11111111111""""" 111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111111110001061010 111 1 6602 Windmill Way,Wilmington,NC 28405 * 910.392.0223 Lab 0 910.392.4424 Fax
111111M111111111114°$$111111111111111111111111111111111 ihoompill sm 710 Bowsertown Road,Manteo,NC 27954 B 251473.5702 Lab/Fax
Imindioggiood 1 255-A Wilmington Highway,Jacksonville,NC 28540 0 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloride SM4500 CI E-2011 13 mg/L 12/20/2021
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/17/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/20/2021
Nitrate Nitrogen Subtraction Method <0.02 mg/L 01/03/2022
Report#:: 2021-22386 Page 15 of 21

Ulltiiiv��� ����� �
0602 Windmill Way,Wilmington,NC28405 * 91.0.392.0223�ab ^ 9I0392�".24 Fax
' 71.0 Bowsertow ���ao� �27� ~ 252.473.5702Lab/�x
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2��������Highway,Jacksonville,NC 28540 ° 910.347.5043L,ab/Fax
ANALYTICAL&CONSULTING CHEMISTS imfo@eovimommmea«x|cheoaiets.cmzm
City mfJacksonville Date mfReport: Jan D5. 2D22
Post Office Box 138 Customer PO#:
Jacksonville NC 28641 Customer ID: 08110015
Attention: Amy Palonchak Fkeport#: 2021-22306
Project ID: Monitoring Wells
Lab |D Sample U0: Collect Date/Time Matrix Sampled by
21'58054 Site: MN-13 12/16/2021 8:15 AM VVobar NB
Test D8mdbod Results Date Analyzed
Sulfate EPA o»«4 Rev.u.1'1»»» <5nng/L 12/17/2021
Total Organic Carbon (T<]C) sm«o1»o'u»14 0.8rng/L 12/21/2021
1.1.1.2-Tetnaoh|oroathone aM«u«»u'u«11 < 0.50Ug/L 12/18/2021
1.1.1-Trioh|onoethana oM«u»»o-2»11 < O.5Dpg/L 12/19/2021
1.1.2.2-Tetnaoh/onoothmna um«u««o'e»11 < D.SOpg/L 12/18/2021
1.1.2-Trich|oroothone om«o«»o'u«11 < 0.50pg/L 12/19/2021
1.1-Dich|onoethana »Mox»»o'u»11 < 0.50pg/L 12/19/2021
1.1-Dich|unoothane sm«««»c'u«11 < O.5Opg/L 12/10/2031
1.1-Dioh|oropnopane smu»»»o'u»11 < 0.50pg/L 12/19/2021
1.2.3-Thch|orobonzana omu»«»o'o»11 < O.6Opg/L 12/19/2021
1.2.3-Trinh/oropnopone oM«u»»c'x»11 < O.5Opg/L 12/18/2021
1.2.4-Trioh|onobenzene omsu»«u-2»11 < 0.50pg/L 12/19/2021
1.2.4-Trimethy|benzene »m«u»»u'u»11 = O.5Opg/L 12/18/2021
1.2-Dibnomo-3-Ch|onopnopane om«o»»u-2«11 < 0.50pg/L 12/19/2021
1.2-0bnomoothone sm»x»»«'uo11 < O.5Opg/L 12/19/2021
1.2-Dioh|orobonzono sm«u»»u'u«11 < 0.50pg/L 12/18/2021
1.2-Diohioroathana am«u»«c-2»11 < 0.50pg/L 12/19/2021
1.2-Oioh|onopnopmne am««««c'u»11 < O.5Dpg/L 12/18/2021
1.3.5-Trinnothy|benzene aM«u»»u'u«11 < O.5OUg/L 12/19/2021
1.3-[)ich|onobanzano oMsu»»c'oo11 < O.5Opg/L 13/19/2021
1.3-Dioh|oropnopone »m«o«»o'u»11 < O.5Opg/L 12/19/2021
1.4-Dioh|orobenzene sMoo«»c'««11 < O.5Opg/L 12/18/2021
2.2-0nh|onopnopono sm»»»»u-2«11 < 0.50pg/L 12/18/2031
2-Ch|oudoluano um«»»«o'e»11 < 0.60Ug/L 12/19/3021
4-Ch|onoho|uona am«o»»u'u»11 < O.5Opg/L 12/19/2021
Benzene sM«o»«u'u»11 < O.5Opg/L 12/18/2021
na»urt#.. 2021-22386 Page 1ouru1

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iii„1111111111111011111 oclit . 0410060111111111111111111 6602 Windmill Way,Wilmington, NC 28405 * 910.392.0223 Lab a 910.392.4424 Fax
11,111,11,1„11,1j11,111,11,11,11,11,11,11 1111111111111111
710 Bowsertown Road,Manteo,NC 27954 '''' 252 473.5702 Lab/Fax
11 255-A Wilmington Highway,Jacksonville,NC 28540 * 910347.5843 Lab/Fax
, 1
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ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Bromobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromodichloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromoform SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Bromomethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Carbon tetrachloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloroform SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
cis-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
cis-1,3-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dibromochloromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dibromomethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Dichlorodifluoromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Ethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Hexachlorobutadiene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
lsopropylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
M+P Xylene SM 6200 C-2011 < 1.00 pg/L 12/19/2021
Methylene chloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Naphthalene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
n-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
n-Propylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
ortho-Xylene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
p-lsopropyltoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
sec-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Styrene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
tert-Butylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Tetrachloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Toluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Report#:: 2021-22386 Page 17 of 21

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411111 6602 Windmill Way,Wilmington,NC 28405 * 910.392.0223 Lab ,'', 910392.4424 Fax
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255 A Wilmington I Iighway,Jacksonville,NC 28540 * 910.347.5843 Lab/Fax
11111111111111111111111111111111111111 11111111111111111,11111111111
ANALYTICAL&CONSULTING CHEMISTS in fo@enviren m CD lalchemists corn
....... _
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloride 5M4500 Cl E-2011 16 mg/L 12/20/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/17/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 < 0.02 mg/L 12/20/2021
Nitrate Nitrogen Subtraction Method <0.02 mg/L 01/03/2022
Report a:: 2021-22386 Page 18 of 21

phi1:10111,1111111111111471111111111111111111111111111t1111111111111111111111 1,00110111111111111111111112111° atoll 6602 Windmill Way,Wilmington,NC 28405 �a 910392.0223 Lab 0i 910.392.' 24 Fax
�� ������ 710 Bowsertown Road,Manteo,NC 27954 % 252.473.5702 Lab/Fax
255••.A Wilmington Highway,Jacksonville,NC 28540 A 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info@environmenta➢chemists.com
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56055 Site: MW-14 12/16/2021 8:00 AM Water NB
Test Method Results Date Analyzed
Sulfate EPA 300.0,Rev.2 1,1993 <5 mg/L 12/17/2021
Total Organic Carbon (TOC) SM 5310 B-2014 12.6 mg/L 12/21/2021
1,1,1,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,1-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,2,2-Tetrachloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1,2-Trichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,1-Dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,3-Trichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2,4-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dibromo-3-Chloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dibromoethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloroethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3,5-Trimethylbenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,3-Dichlorobenzene SM 6200 C-2011 < 0.50 lg/L 12/19/2021
1,3-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
1,4-Dichlorobenzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
2,2-Dichloropropane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
2-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
4-Chlorotoluene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Benzene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Report#.: 2021-22386 Page 19 of 21

6602Windmmill Way,Wilmington,NC 28405 ° 910.392.0223 Lab " 910.392.4424 Fax
' 710 Bowaer&mwn Road,B�a�k�m ��2��5� w 252.473.5702Lmb/Fax
,
255�����ub��tm������wey,Jacksonville,NC28540 * 910.347.5043Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS i [e-mail]
City of Jacksonville Date of Report: Jan O5. 2O32
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer|D: 08110015
Attention: Amy Pa|amohah Report#: 2021-22386
Project ID: Monitoring Wells
Bnomobenzene mm««»»o-2»11 « O.5OVg/L 12/18/2021
Brornoch|oromathane amno»»o'u»11 < 0.50pg/L 12/19/2021
Bromodich|oromathane sMau»»o'u«11 < 0.50pg/L 12/18/2021
Bromnoformn awn»«»o-2»11 < O.5Opg/L 12/19/2021
Bnomomethang ameu»oc'o»11 < O.50pg/L 12/19/2021
Carbon tetrachloride awno»»c-2»11 < 0.50pQ/L 12/19/2021
Ch|orobenzena amoc»»c'u»11 < 0.50pg/L 12/19/2021
Ch/opoethane am«»«»o'u»11 < 0.50pg/L 12/19/2021
Chloroform aMn»»»o-»»11 < O.5Opg/L 12/19/2021
Ch|oromethone mwno»oo-2»11 < O.GOpQ/L 12/19/2021
cis-1.2-Dich|onoethene ameu»»u'u»11 < O.5Opg/L 12/19/2021
cis-1.3-Dich|mnopropena aweu»»o-2»11 < O.5Opg/L 12/19/2021
OibnonnocNoromethene amou»»o'o»11 < 0.50pg/L 12/19/2021
Dibromomethono awn»»»c-2»11 < 0.50pg/L 12/19/2021
Dioh|onodif|uoromathene aMe»o»o-2»11 < 0.50Vg/L 12/19/2021
Ethy|benzene aw«u«»o'o»11 < O.50pg/L 12/19/2021
Hexach|onobutodieng awoo»»o-2»11 < O.5Opg/L 13/19/2021
|oopropy|benzene Smuu»»c'«»11 < 0.50pg/L 12/19/2021
K8+P)(y|ene omoo»»c'««11 < 1.00pg/L 12/19/2021
Methylene chloride amsu»»n-2»11 < O.SOpg/L 12/18/2021
Naphthalene sws»»»c'u»11 < O.50pg/L 12/19/2021
n-Buty|benzene amou«»«'cm1 < 0.50pg/L 12/19/2021
n-Pnopy|benzene owsu»»u'«o11 < O.5Opg/L 12/19/2031
odho-Xyleno am«o«»o-2»11 < 0.50pg/L 12/19/2021
p-|eopropy|bo|uene aw*u«»c'u»11 < 0.50pg/L 12/18/2021
mec-Buty|benzene swan»»o-2«11 < O.5Opg/L 12/18/2021
Gh/nane uM«c»»o'c»11 < 0.50pD/L 12/18/2021
hod-Buty|benzene mmoo«»c'««11 < 0.50Ug/L 12/19/3021
Tetrach|oroethene em«u»»o-2»11 < O.5Opg/L 12/19/2021
Toluene nmso»oc'o»11 < 0.50pg/L 12/19/2021

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IIIIIIIIIIIIIIIIIIIIITtrli 1 1111111 1 'No11.111111 1 41141411111101 6602 Wiridnull Way,Wilmington,NC 28405 1 910.39'2 0223 Lab * 910.392.4424 Fax
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IIIIIIIIIIIIIIIIIIIIIIIIh000mo m 25, A710 Bowser town Road,Monte°,NC 27954 . 252A73.5702 Lab/Fax
111111111111111111111IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIII
. 3 Wilmington Highway,Jacksonville,NC 28540 * 910.347.5843 Lab/Lax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Jan 05, 2022
Post Office Box 128 Customer PO#:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Amy Palaschak Report#: 2021-22386
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trans-1,3-dichloropropene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichloroethene SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Trichlorofluoromethane SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Vinyl chloride SM 6200 C-2011 < 0.50 pg/L 12/19/2021
Chloride SM4500 CI E-2011 8 mg/L 12/20/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353 2,Rev.2.0,1993 < 0.02 mg/L 12/17/2021
Nitrate+Nitrite-Nitrogen EPA 353.2,Rev.2.0,1993 0.04 mg/L 12/20/2021
Nitrate Nitrogen Subtraction Method 0.04 mg/L 01/03/2022
Comment: , n
Reviewed by: Ro I., , ill'av),,
Report#.: 2021-22386 Page 21 of 21

Environmental Chemist, Inc., Wiln'in�� �[ ����_ G6O2 Windmill Way
Wilmington, NC 28405
Sa|npKe Receipt Checklist 910.3920223
Client: c - (L[L(~- "'�'
LU�° Date: l Z� `L~ 2-l
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'ES U NO N/A Were custody seals present on the cooler?YES [ NO ---/A /2� /f custodyeabwereprespn� were they/ntact/unbroken? ----[-]--
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ere
proper
-- ---' �� YES O
YES [ - - ' ~^ ^^^ CO^'
YES ] vu samples /D�/�t�e"don sample conta[ne �T YES [ NOL7. WerecoUecbondateandbme /oteUon the CO[?YES retests tobe performed / / dontheCO[? ---
11 NO
YB L] NO 9. Did samples arrive in proper containers
/
|
'
|for each test? --
/�F' YES |O NO ||10. Did samples arrive /n good condition for each test? -
'7 YES |[] NO �1I.
�asadpquatesamp(evo/umeevaUab/e?'
---I'M YES ] N0 12� Were samples rece�edw�himproper hoN i»8bmeforrequestedtests?yES ] NO 13. i
Were acid preserved oamp/esreceivedatapHof<Z? �
[] YES ![] NO l4. Were cyanide samples received aLapH >13?
|[] YES |[] NO |�15. Were sulfide samples received atapH»9? '
!|[] YES
[ NO _- | 15. Were NH3/TKN/Phe'no/ received ata chlorine residual of<O'Sno-1?YE5 ) ] NO 17. Were Su(fide/[. n/ erecekedatach/ohneresid«a/ of«O.Sm/L/yE3 [ NO 18 Were orthophosphate / U /n the �eNv �hinI5 minutes?
*
!'
TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
|
- Bacteria samples are checked for Chlorine at time of analysis and recorded on thebenchsheeL
Sample Preservation: (��u� becomp�ted for any somp/p/dinco�ectk/pre�prvedorwidhhead�pace) |
Sample(s) � .
byad'in� (ckz/eone)� H2SO4werenece�ndinconect|Yp�sen�dandw«snpaoUusteda accordingly
, � MN[� H[/ NaOH ~`
Time of `�=..�um^� - /f more than one preservative is needed, notate hn comments below��Note:Notify customer service immediate for incorrectly presemed samples,Obtain a new sample or
�notify the state lab if directed toanalyzdbythecustomec'Whowssnmified,date andti
me:
UVo/atUesSamp/e(s)
were received with headspace ' ^
__� �
[��W%HENTS: --
__ DO[ QAOOJ Rev 1

tit-t-viri5e-mixt: ENVIRONMENTAL CHEMISTS INC 6602 Windmill Way Wilmington,NC 28405
OFFICE:910-392-0223 FAX [phone]
NCDENR: DWQ CERTIFICATION#94 NCDHHS: DLS CERTIFICATION#37729
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
CLIENT: City of Jacksonville PROJECT NAME: Monitoring Wells (Jacksonville LTS) REPORT NO: r;il -a-a-?_,-,g
ADDRESS: PO Box 128 CONTACT NAME: PO NO: 225042
Jacksonville, NC 28540 REPORT TO: Amy Palaschak PHONE/FAX:
COPY TO: E-MAIL: [e-mail]
Sampled By:OE) SAMPLE TYPE: I=Influent, E= Effluent,W=Well,ST=Stream, SO=Soil, SL=Sludge, Other:
Collection g. - . PRESERVATION
., 2 6 .E _1 2 iTi
Sample Identification D. Itg 13= 'a re1.13 8 2 ANALYSIS REQUESTED
pa e Time Temp
co 0 x ,,
0 (-) z Z x x z 1- 0
0
12.6 11 Val-I 4 (t
1
P TOC, Sulfate, Nitrate,
(0 MW i , ' W G G 514;Dri X X XI 290 Chloride, VOC (SM 6200 C)
04-N ÷ 1 Li P TOC, Sulfate, Nitrate,
MW 4. 1--P 1 W G G S(cOSO X X X ' 14 Chloride, VOC (SM 6200 C)
l MW \ V 104 \ 19 r) P u — W G G 5L-Ccxxx '.-2e Chloride,TOC, Sulfate, Nitrate,
loride, VOC (SM 6200 C)
P TOC, Sulfate, Nitrate,
MW W G G X X X Chloride, VOC (SM 6200 C)
1 ,111#\ C2I-15 _ P TOC, Sulfate, Nitrate,
MW CI \-+Z W G G . 1t).52- X X X 4-LAI Chloride, VOC (SM 6200 C)
CA I U P TOC, Sulfate, Nitrate,
MW 10 10.5 W G G 51COS3 X X X '2,)11 Chloride, VOC (SM 6200 C)
_
1' 015- , P
W G G SU/Y-1 X X X'7f71 TOC, Sulfate, Nitrate,
MW 3 0i
Chloride, VOC (SM 6200 C)
CAO b , g g P TOC, Sulfate, Nitrate,
MW \LA % •
W G G SaSs- x x x -7t'cv Chloride, VOC (SM 6200 C)
-
P TOC, Sulfate, Nitrate,
MW W G G X X X Chloride, VOC (SM 6200 C)
P TOC, Sulfate, Nitrate,
MW W G G X X X Chloride, VOC (SM 6200 C)
NOTICE-DECHLORINATION: Samples for Ammonia,TKN,Cyanide,Phenol and Bacteria must be dechlorinated(0.2 ppm or less)in the field at the time of collection. See reverse for instructions
Transfer ,Relinquished By: Date/Time Received By: Date/Time
- .
,
I
I"
06191— CP SO
2.
Temperature when Received: , , lc C Accepted: v jected: Resample Requested:
Delivered By: Received By. -1/) C-71/ C-\.— Date: 1141 id il Time: 1
Comments: TUR AROUND: