WI0600231_2021 Annual Report_20220128

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January 26, 2022
Mr. Mike Rogers
UIC Program
NCDEQ Division of Water Resources
1636 Mail Service Center
Raleigh, North Carolina 27699-1636

RE: 2021 Annual Report
Groundwater Remediation Permit No. WI0600231 (formerly WQ0014357)
Aberdeen Pesticide Dumps Site - Route 211 Area
Aberdeen, North Carolina

Dear Mr. Rogers:

On behalf of Syngenta Crop Protection, LLC and Olin Corporation, please find enclosed
one copy of the 2021 Annual Report for the groundwater extraction, treatment and
discharge system located at the Route 211 Area of the Aberdeen Pesticide Dumps Site.
Information provided in this letter report includes:
 Analytical monitoring requirements summary (Table 1);
 Influent and effluent analytical results summary (Tables 2 and 3);
 Monitoring well analytical results summary (Table 4);
 Groundwater monitoring locations and water levels (Figure 1);
 Laboratory analytical reports (Attachment 1), and
 Completed copies of NCDEQ Division of Water Resources GW-59 Forms
(Attachment 2).
The treatment system was inspected monthly, and influent and effluent samples were
collected semi-annually (June 28, 2021 and December 2, 2021) in accordance with the
permit. These results are summarized in Tables 2 and 3. The treatment system
performed as designed during 2021 and experienced minimal downtime. The system
operates 24 hours per day and a total of 797,680 gallons (based upon the monthly
inspection logs dated between December 4, 2020 to December 3, 2021) of groundwater
were treated.
2021 Annual Report – Groundwater Remediation Permit No. WI0600231
Aberdeen Pesticide Dumps Site – Route 211 Area
Aberdeen, North Carolina Page 2
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Groundwater extraction rates averaged approximately 2,185 gpd during the monitoring
period. The treatment system removal efficiency was greater than 95% (see Tables 2
and 3).

Pumping of extraction well RT-PW-01 continues to fulfill the closed-loop requirement
of the Site Groundwater Remediation Permit. Two sidegradient wells, MW-2 (05-MW-
01) and MW-3 (RT-MW-05), and one upgradient well, MW-1 (RT-MW-12), were
sampled on December 2, 2021 and analyzed for SW-846 8081A pesticides. Analytical
results are summarized in Table 4. Water levels were collected on December 2, 2021 and
are shown of Figure 1. Copies of the treatment system influent and effluent analytical
reports and the MW-1, MW-2 and MW-3 analytical report are included with the
completed GW-59 forms provided as attachments.

Information provided in this submittal is intended to fulfill the annual reporting
requirement described in Part V of the Site Groundwater Remediation Permit
WI0600231 issued December 7, 2021.

If you require additional copies of the enclosed materials or have any questions, please
contact me at [phone].

Sincerely,

Thomas A. Mann, P.E.
Project Manager
SynTerra Corporation

Attachment 1 - Laboratory Analytical Reports
Attachment 2 - NCDEQ Division of Water Resources Form GW-59

Electronic cc:
Jim Barber – NC DWR Fayetteville Dane Grimshaw – Olin
Doug Rumford – NCDEQ Michael Bogle, Esq. – WBD
John Nolen – USEPA Ted Volskay - SynTerra
Peter Jacobson - Syngenta
2021 Annual Report – Groundwater Remediation Permit No. WI0600231
Aberdeen Pesticide Dumps Site – Route 211 Area
Aberdeen, North Carolina

TABLES

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Reports\Semi & Annual Reports\2022\Annual\Tables\Table 1 - 2021 Sampling Requirements Table.doc

TABLE 1
ANALYTICAL MONITORING REQUIREMENTS
GROUNDWATER EXTRACTION AND TREATMENT SYSTEM
ROUTE 211 AREA ANNUAL OPERATING REPORT
ABERDEEN, NORTH CAROLINA

Location Analysis and Field
Parameters
Monitoring Frequency
(Permit No. WI0600231)
Influent (RT-PW-01) TCL Pesticides & pH Semi-annually
(Jan.-June, July- Dec.)
Effluent TCL Pesticides & pH Semi-annually
(Jan.-June, July- Dec.)
MW-1 (RT-MW-12) TCL Pesticides, pH
& Water Level Annually
MW-2 (05-MW-01) TCL Pesticides, pH
& Water Level Annually
MW-3 (RT-MW-05) TCL Pesticides, pH
& Water Level Annually
Prepared by: VTV Checked by: TAM
Monitoring Period
Sample Name Influent Effluent
Date Sampled 06/28/21 06/28/21
Pesticides (ug/L)
Aldrin <0.01 <0.0021
alpha-BHC <0.017 <0.0032
Chlordane 0.118 JP <0.011
beta-BHC 0.26 <0.0036
p,p-DDD <0.028 <0.0053
p,p-DDE <0.028 <0.0053
p,p-DDT <0.029 <0.0055
delta-BHC 0.83 <0.0036
Dieldrin <0.029 <0.0056
Endosulfan I <0.024 <0.0046
Endosulfan II <0.083 <0.016
Endosulfan Sulfate 0.10 J <0.0061
Endrin <0.045 <0.0086
Endrin Aldehyde <0.11 <0.021
gamma-BHC <0.011 <0.0021
Heptachlor <0.011 <0.0021
Heptachlor Epoxide <0.013 <0.0024
Methoxychlor <0.17 <0.032
Toxaphene <1.70 <0.32
Total Pesticides 2.46 0.0121
System Removal Efficiency:99.51%
Notes:
Influent pH was 5.85 s.u.
J-estimated value
P - RPD >40%
V - RPD >100%
Permit specified removal efficiency is 95%
January - June 2021
Where concentrations are ND, detection limit of constituent was divided by
half for use in calculation.
TABLE 2
TREATMENT SYSTEM MONITORING RESULTS AND
TREATMENT REMOVAL EFFICIENCY (JANUARY - JUNE 2021)
ROUTE 211 ANNUAL OPERATING REPORT
ABERDEEN, NORTH CAROLINA
TABLE 3
TREATMENT SYSTEM MONITORING RESULTS AND TREATMENT REMOVAL
EFFICIENCY (JULY - DECEMBER 2021)
ROUTE 211 AREA ANNUAL OPERATING REPORT
ABERDEEN, NORTH CAROLINA
Pesticides (ug/L)Note 1 Note 1
Aldrin <0.022 *1 cn <0.0022 *1 cn
alpha-BHC 0.021 J p *1 cn <0.0033 *1 cn
beta-BHC 1.7 cn <0.0037 cn
gamma-BHC (Lindane)0.013 J p *1 cn <0.0022 *1 cn
alpha-Chlordane 0.070 *1 cn <0.0033 *1 cn
gamma-Chlordane 0.037 J p *1 cn <0.0076 *1 cn
p,p-DDD 0.044 p *1 cn <0.0054 *1 cn
p,p-DDE 0.0070 J p *1 cn <0.0054 *1 cn
p,p-DDT 0.014 J p *1 cn <0.0056 *1 cn
delta-BHC 1.8 p *1 cn <0.0037 *1 cn
Dieldrin 0.0098 J p *1 cn <0.0057 *1 cn
Endosulfan I 0.040 *1 cn <0.0047 *1 cn
Endosulfan II 0.059 p *1 cn <0.016 *1 cn
Endosulfan Sulfate 0.095 cn <0.0063 cn
Endrin <0.0087 *1 cn <0.0088 *1 cn
Endrin Aldehyde 0.056 J p *1 cn <0.022 *1 cn
Endrin Ketone 0.053 cn <0.0054 *1 cn
Heptachlor <0.0022 cn <0.0022 cn
Heptachlor Epoxide 0.0072 J p *1 cn <0.0025 *1 cn
Methoxychlor 0.18 p cn <0.033 cn
Toxaphene 5.2 p cn <0.33 cn
9.406 0.233
System Removal Efficiency: (Notes 2 and 3)97.52%
Prepared by: VTV Checked by: TAM
Data Flags:
J - Estimated value.
p -
*1
cn -
1
2
3
Total Pesticides
Monitoring Period July - December 2021
Sample Name Influent Effluent
Date Sampled 12/02/21 12/02/21
Permit specified removal efficiency: 95%
Relative percent difference (RPD) >40%. The lower value has been reported.
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD) Relative Percent Difference
(RPD) exceeds control limits.
Surrogate recovery for laboratory control sample duplicate was outside the lower control limits. The
recoveries for the analytes of interest were within acceptable control limits. The data is reported.
Notes:
Influent pH was 4.61 Standard Units (su); Effluent pH was 4.93 su
System removal efficiency calculated only for constituents having concentrations greater than method
detection limit (MDL). One-half of the MDL is assumed for constituent concentrations that are less than the
MDL.
TABLE 4
MONITORING WELL ANALYTICAL RESULTS SUMMARY
ROUTE 211 AREA ANNUAL OPERATING REPORT
ABERDEEN, NORTH CAROLINA
Note 1 Note 1 Note 1
< 0.0021 *1 cn < 0.0021 *1 cn < 0.0021 *1 cn
< 0.0032 *1 cn < 0.0031 *1 cn < 0.0032 *1 cn
< 0.0036 cn 0.052 cn < 0.0036 cn
< 0.0021 *1 cn < 0.0021 *1 cn < 0.0021 *1 cn
< 0.0032 *1 cn 0.0035 J*1 cn < 0.0032 *1 cn
< 0.0074 *1 cn < 0.0073 *1 cn < 0.0074 *1 cn
< 0.0053 *1 cn < 0.0052 *1 cn < 0.0053 *1 cn
< 0.0053 *1 cn < 0.0052 *1 cn < 0.0053 *1 cn
< 0.0055 *1 cn < 0.0054 *1 cn < 0.0055 *1 cn
< 0.0036 *1 cn < 0.0035 *1 cn < 0.0036 *1 cn
< 0.0056 *1 cn < 0.0055 *1 cn < 0.0056 *1 cn
< 0.0045 *1 cn < 0.0045 *1 cn < 0.0046 *1 cn
< 0.016 *1 cn < 0.016 *1 cn < 0.016 *1 cn
< 0.0061 cn < 0.0060 cn < 0.0062 cn
< 0.0085 *1 cn < 0.0084 *1 cn < 0.0086 *1 cn
< 0.021 *1 cn < 0.021 *1 cn < 0.021 *1 cn
< 0.0053 *1 cn < 0.0052 *1 cn < 0.0053 *1 cn
< 0.0021 cn < 0.0021 cn < 0.0021 cn
< 0.0024 *1 cn < 0.0024 *1 cn < 0.0024 *1 cn
< 0.032 cn < 0.031 cn < 0.032 cn
< 0.32 cn 0.52 J cn < 0.32 cn
Prepared by: VTV Checked by: TAM
Data Flags:
J - Estimated value.
*1 -
cn -
1
Toxaphene
Laboratory Control Sample/Laboratory Control Sample Duplicate (LCS/LCSD) Relative Percent Difference (RPD)
exceeds control limits.
Endosulfan Sulfate
Endrin
Endrin Aldehyde
Surrogate recovery for laboratory control sample duplicate was outside the lower control limits. The recoveries
for the analytes of interest were within acceptable control limits. The data is reported.
Notes:
MW-1 ( pH = 3.55 Standard Units [su]); MW-2 (pH = 3.88 su); MW- 3 (pH = 4.05 su)
Endrin Ketone
Heptachlor
Heptachlor Epoxide
Methoxychlor
p,p-DDE
p,p-DDT
delta-BHC
Dieldrin
Endosulfan I
Endosulfan II
12/2/2021Date Sampled
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
p,p-DDD
Pesticides (ug/L)
Aldrin
alpha-BHC
beta-BHC
12/2/2021 12/2/2021
MW-1 (RT-MW-12) MW-2 (05-MW-01) MW-3 (RT-MW-05)Sample Name
Sample Event Annual Annual Annual
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Reports\Semi & Annual Reports\2022\Annual\Tables\Tables 2, 3 and 4 - 2022 Treatment Syst Annual Rpt
2021 Annual Report – Groundwater Remediation Permit No. WI0600231
Aberdeen Pesticide Dumps Site – Route 211 Area
Aberdeen, North Carolina

FIGURE

"M
&<
&<
&<
ABERDEEN&ROCKFISHRR
RT-MW-12 (MW-1)432.99
RT-MW-09430.57
RT-MW-05 (MW-3)429.94
05-MW-01 (MW-2)431.78
RT-PW-01
³
FIGURE 1MONITORING LOCATIONS AND POTENTIOMETRIC MAP-SURFICIAL AQUIFERROUTE 211 AREA
ABERDEEN PESTICIDE DUMPS SITEMOORE COUNTY, NORTH CARO LIN A
Groundwater levels and surface contour elevations expressed in feet,referenced to the North American Vertical Datum of 1988 (NAVD88).
Source: Water levels measured December 2021, MooreCounty 2007 aerial, and site surveys.4304
3
1
4
3
2
INFILTRATIONGALLERIES
4
304
3
1
Legend
&<MONITORING WELL
"M EXTRACTION WELL
GROUNDWATERSURFACE CONTOUR
GROUNDWATER FLOWDIRECTION
EFFLUENT DISCHARGELINE
FORMER SOURCE AREA
50 0 50 100GRAPHIC SCALE
DRAWN BY: C. WYATT
CHECKED BY: T. VOLSKAYREVISED BY: C. WYATT DATE: 12/22/2021
(IN FEET)
DATE: 12/22/2021
APPROVED BY: T. MANN
PROJECT MANAGER: T. MANN
DATE: 12/22/2021
DATE: 12/18/2021
www.synterracorp.com
FLOW
FLOW
This map is a product of SynTerra. Reasonable effortshave been made to ensure the accuracy of this map.SynTerra expressly disclaims any responsibility or liabilitywith regard to the use of this map, and promotes andrecommends the independent verification of any datacontained on this map by the user of this map product.
4
3
2
2021 Annual Report – Groundwater Remediation Permit No. WI0600231
Aberdeen Pesticide Dumps Site – Route 211 Area
Aberdeen, North Carolina

ATTACHMENT 1

LABORATORY ANALYTICAL REPORTS

ANALYTICAL REPORT
Eurofins Lancaster Laboratories Env, LLC
2425 New Holland Pike
Lancaster, PA 17601
Tel: [phone]
Laboratory Job ID: 410-45293-1
Client Project/Site: Rte 211 Treatment System, NC
Sampling Event: Rte 211 Treatment System, NC
For:
SynTerra
148 River Street
Suite 220
Greenville, South Carolina 29601
Attn: Mr. Ted Volskay
Authorized for release by:
7/9/2021 11:27:39 AM
Marrissa Williams, Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Analytical test results meet all requirements of the associated regulatory program (e.g., NELAC (TNI), DoD,
and ISO 17025) unless otherwise noted under the individual analysis. Data qualifiers are applied to note
exceptions. Noncompliant quality control (QC) is further explained in narrative comments.
· QC results that exceed the upper limits and are associated with non-detect samples are qualified but further
narration is not required since the bias is high and does not change a non-detect result. Further narration is
also not required with QC blank detection when the associated sample concentration is non-detect or more
than ten times the level in the blank.
· Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD is performed, unless otherwise
specified in the method.
· Surrogate and/or isotope dilution analyte recoveries (if applicable) which are outside of the QC window are
confirmed unless attributed to a dilution or otherwise noted in the narrative.
Regulated compliance samples (e.g. SDWA, NPDES) must comply with the associated agency
requirements/permits.
Measurement uncertainty values, as applicable, are available upon request.
Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or
microbiological analysis is the collection of the sample. Unless the sample analyzed is truly representative of
the bulk of material involved, the test results will be meaningless. If you have questions regarding the proper
techniques of collecting samples, please contact us. We cannot be held responsible for sample integrity,
however, unless sampling has been performed by a member of our staff. Times are local to the area of activity.
Parameters listed in the 40 CFR Part 136 Table II as "analyze immediately" and tested in the laboratory are not
performed within 15 minutes of collection.
This report shall not be reproduced except in full, without the written approval of the laboratory.
WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results
for the sample as submitted. The foregoing express warranty is exclusive and is given in lieu of all other
warranties, expressed or implied, except as otherwise agreed. We disclaim any other warranties, expressed or
implied, including a warranty of fitness for particular purpose and warranty of merchantability. In no event shall
Eurofins Lancaster Laboratories Environmental, LLC be liable for indirect, special, consequential, or incidental
damages including, but not limited to, damages for loss of profit or goodwill regardless of (A) the negligence
(either sole or concurrent) of Eurofins Lancaster Laboratories Environmental and (B) whether Eurofins
Lancaster Laboratories Environmental has been informed of the possibility of such damages. We accept no
legal responsibility for the purposes for which the client uses the test results. Except as otherwise agreed, no
purchase order or other order for work shall be accepted by Eurofins Lancaster Laboratories Environmental
which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster
Laboratories Environmental hereby objects to any conflicting terms contained in any acceptance or order
submitted by client.
Marrissa Williams
Project Manager
7/9/2021 11:27:39 AM
Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Laboratory Job ID: 410-45293-1
Page 2 of 18 7/9/2021
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Table of Contents
Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Laboratory Job ID: 410-45293-1
Page 3 of 18
Eurofins Lancaster Laboratories Env, LLC
7/9/2021
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18
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Definitions/Glossary
Job ID: 410-45293-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Qualifiers
GC Semi VOA
Qualifier Description
*1 LCS/LCSD RPD exceeds control limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
1C Result is from the primary column on a dual-column method.
2C Result is from the confirmation column on a dual-column method.
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Lancaster Laboratories Env, LLC
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Case Narrative
Client: SynTerra Job ID: 410-45293-1
Project/Site: Rte 211 Treatment System, NC
Job ID: 410-45293-1
Laboratory: Eurofins Lancaster Laboratories Env, LLC
Narrative
Job Narrative
410-45293-1
Receipt
The samples were received on 6/29/2021 8:23 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 5.0°C
Pesticides
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Eurofins Lancaster Laboratories Env, LLC
Page 5 of 18 7/9/2021
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Detection Summary
Job ID: 410-45293-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Client Sample ID: Effluent Lab Sample ID: 410-45293-1
No Detections.
Client Sample ID: Influent Lab Sample ID: 410-45293-2
alpha-Chlordane (1C)
RL
0.11 ug/L
MDL
0.017
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA5J0.061 8081B
beta-BHC (1C)0.11 ug/L0.019 Total/NA50.26 8081B
delta-BHC (2C)0.11 ug/L0.019 Total/NA50.83 8081B
Endosulfan sulfate (2C)0.17 ug/L0.032 Total/NA50.10 J 8081B
gamma-Chlordane (1C)0.22 ug/L0.039 Total/NA50.057 J p 8081B
Eurofins Lancaster Laboratories Env, LLC
This Detection Summary does not include radiochemical test results.
Page 6 of 18 7/9/2021
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Client Sample Results
Job ID: 410-45293-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Lab Sample ID: 410-45293-1Client Sample ID: Effluent
Matrix: WaterDate Collected: 06/28/21 14:30
Date Received: 06/29/21 08:23
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
Aldrin (1C)ND *1 0.021 0.0021 ug/L 07/02/21 17:18 07/06/21 19:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.021 0.0032 ug/L 07/02/21 17:18 07/06/21 19:19 1alpha-BHC (1C)ND
0.021 0.0032 ug/L 07/02/21 17:18 07/06/21 19:19 1alpha-Chlordane (1C)ND
0.021 0.0036 ug/L 07/02/21 17:18 07/06/21 19:19 1beta-BHC (2C)ND
0.021 0.0036 ug/L 07/02/21 17:18 07/06/21 19:19 1delta-BHC (1C)ND
0.032 0.0056 ug/L 07/02/21 17:18 07/06/21 19:19 1Dieldrin (1C)ND
0.021 0.0046 ug/L 07/02/21 17:18 07/06/21 19:19 1Endosulfan I (1C)ND
0.042 0.016 ug/L 07/02/21 17:18 07/06/21 19:19 1Endosulfan II (1C)ND
0.032 0.0061 ug/L 07/02/21 17:18 07/06/21 19:19 1Endosulfan sulfate (1C)ND
0.032 0.0086 ug/L 07/02/21 17:18 07/06/21 19:19 1Endrin (1C)ND
0.11 0.021 ug/L 07/02/21 17:18 07/06/21 19:19 1Endrin aldehyde (1C)ND
0.032 0.0053 ug/L 07/02/21 17:18 07/06/21 19:19 1Endrin ketone (1C)ND
0.021 0.0021 ug/L 07/02/21 17:18 07/06/21 19:19 1gamma-BHC (Lindane) (1C)ND
0.042 0.0074 ug/L 07/02/21 17:18 07/06/21 19:19 1gamma-Chlordane (1C)ND
0.021 0.0021 ug/L 07/02/21 17:18 07/06/21 19:19 1Heptachlor (1C)ND
0.021 0.0024 ug/L 07/02/21 17:18 07/06/21 19:19 1Heptachlor epoxide (1C)ND
0.12 0.032 ug/L 07/02/21 17:18 07/06/21 19:19 1Methoxychlor (1C)ND
1.1 0.32 ug/L 07/02/21 17:18 07/06/21 19:19 1Toxaphene (1C)ND
0.032 0.0053 ug/L 07/02/21 17:18 07/06/21 19:19 1p,p'-DDD (1C)ND
0.032 0.0053 ug/L 07/02/21 17:18 07/06/21 19:19 1p,p'-DDE (1C)ND
0.032 0.0055 ug/L 07/02/21 17:18 07/06/21 19:19 1p,p'-DDT (1C)ND
DCB Decachlorobiphenyl (Surr) (1C)72 32 -149 07/02/21 17:18 07/06/21 19:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr) (2C)69 07/02/21 17:18 07/06/21 19:19 132-149
Tetrachloro-m-xylene (Surr) (1C)59 07/02/21 17:18 07/06/21 19:19 129-129
Tetrachloro-m-xylene (Surr) (2C)52 07/02/21 17:18 07/06/21 19:19 129-129
Lab Sample ID: 410-45293-2Client Sample ID: Influent
Matrix: WaterDate Collected: 06/28/21 14:35
Date Received: 06/29/21 08:23
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
Aldrin (2C)ND *1 0.11 0.011 ug/L 07/02/21 17:18 07/06/21 19:30 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.11 0.017 ug/L 07/02/21 17:18 07/06/21 19:30 5alpha-BHC (2C)ND
0.11 0.017 ug/L 07/02/21 17:18 07/06/21 19:30 5alpha-Chlordane (1C)0.061 J
0.11 0.019 ug/L 07/02/21 17:18 07/06/21 19:30 5beta-BHC (1C)0.26
0.11 0.019 ug/L 07/02/21 17:18 07/06/21 19:30 5delta-BHC (2C)0.83
0.17 0.029 ug/L 07/02/21 17:18 07/06/21 19:30 5Dieldrin (1C)ND
0.11 0.024 ug/L 07/02/21 17:18 07/06/21 19:30 5Endosulfan I (1C)ND
0.22 0.083 ug/L 07/02/21 17:18 07/06/21 19:30 5Endosulfan II (1C)ND
0.17 0.032 ug/L 07/02/21 17:18 07/06/21 19:30 5Endosulfan sulfate (2C)0.10 J
0.17 0.045 ug/L 07/02/21 17:18 07/06/21 19:30 5Endrin (1C)ND
0.56 0.11 ug/L 07/02/21 17:18 07/06/21 19:30 5Endrin aldehyde (1C)ND
0.17 0.028 ug/L 07/02/21 17:18 07/06/21 19:30 5Endrin ketone (1C)ND
0.11 0.011 ug/L 07/02/21 17:18 07/06/21 19:30 5gamma-BHC (Lindane) (1C)ND
0.22 0.039 ug/L 07/02/21 17:18 07/06/21 19:30 5gamma-Chlordane (1C)0.057 J p
0.11 0.011 ug/L 07/02/21 17:18 07/06/21 19:30 5Heptachlor (1C)ND
0.11 0.013 ug/L 07/02/21 17:18 07/06/21 19:30 5Heptachlor epoxide (1C)ND
Eurofins Lancaster Laboratories Env, LLC
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Client Sample Results
Job ID: 410-45293-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Lab Sample ID: 410-45293-2Client Sample ID: Influent
Matrix: WaterDate Collected: 06/28/21 14:35
Date Received: 06/29/21 08:23
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Methoxychlor (2C)ND 0.61 0.17 ug/L 07/02/21 17:18 07/06/21 19:30 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.6 1.7 ug/L 07/02/21 17:18 07/06/21 19:30 5Toxaphene (1C)ND
0.17 0.028 ug/L 07/02/21 17:18 07/06/21 19:30 5p,p'-DDD (2C)ND
0.17 0.028 ug/L 07/02/21 17:18 07/06/21 19:30 5p,p'-DDE (1C)ND
0.17 0.029 ug/L 07/02/21 17:18 07/06/21 19:30 5p,p'-DDT (1C)ND
DCB Decachlorobiphenyl (Surr) (1C)83 32 -149 07/02/21 17:18 07/06/21 19:30 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr) (2C)73 07/02/21 17:18 07/06/21 19:30 532-149
Tetrachloro-m-xylene (Surr) (1C)73 07/02/21 17:18 07/06/21 19:30 529-129
Tetrachloro-m-xylene (Surr) (2C)60 07/02/21 17:18 07/06/21 19:30 529-129
Eurofins Lancaster Laboratories Env, LLC
Page 8 of 18 7/9/2021
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Surrogate Summary
Job ID: 410-45293-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Method: 8081B - Organochlorine Pesticides (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (32-149)(32-149)(29-129)(29-129)
DCB1 DCB2 TCX1 TCX2
72 69 59 52410-45293-1
Percent Surrogate Recovery (Acceptance Limits)
Effluent
83 73 73 60410-45293-2 Influent
89 90 85 74LCS 410-144907/2-A Lab Control Sample
32 33 42 40LCSD 410-144907/3-A Lab Control Sample Dup
73 72 35 33MB 410-144907/1-A Method Blank
Surrogate Legend
DCB = DCB Decachlorobiphenyl (Surr)
TCX = Tetrachloro-m-xylene (Surr)
Eurofins Lancaster Laboratories Env, LLC
Page 9 of 18 7/9/2021
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QC Sample Results
Job ID: 410-45293-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Method: 8081B - Organochlorine Pesticides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-144907/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 146647 Prep Batch: 144907
RL MDL
Aldrin (1C)ND 0.020 0.0020 ug/L 07/02/21 17:18 07/09/21 08:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00300.020 ug/L 07/02/21 17:18 07/09/21 08:17 1alpha-BHC (1C)
ND 0.00300.020 ug/L 07/02/21 17:18 07/09/21 08:17 1alpha-Chlordane (1C)
ND 0.00340.020 ug/L 07/02/21 17:18 07/09/21 08:17 1beta-BHC (1C)
ND 0.00340.020 ug/L 07/02/21 17:18 07/09/21 08:17 1delta-BHC (1C)
ND 0.00530.030 ug/L 07/02/21 17:18 07/09/21 08:17 1Dieldrin (1C)
ND 0.00430.020 ug/L 07/02/21 17:18 07/09/21 08:17 1Endosulfan I (1C)
ND 0.0150.040 ug/L 07/02/21 17:18 07/09/21 08:17 1Endosulfan II (1C)
ND 0.00580.030 ug/L 07/02/21 17:18 07/09/21 08:17 1Endosulfan sulfate (1C)
ND 0.00810.030 ug/L 07/02/21 17:18 07/09/21 08:17 1Endrin (1C)
ND 0.0200.10 ug/L 07/02/21 17:18 07/09/21 08:17 1Endrin aldehyde (1C)
ND 0.00500.030 ug/L 07/02/21 17:18 07/09/21 08:17 1Endrin ketone (1C)
ND 0.00200.020 ug/L 07/02/21 17:18 07/09/21 08:17 1gamma-BHC (Lindane) (1C)
ND 0.00700.040 ug/L 07/02/21 17:18 07/09/21 08:17 1gamma-Chlordane (1C)
ND 0.00200.020 ug/L 07/02/21 17:18 07/09/21 08:17 1Heptachlor (2C)
ND 0.00230.020 ug/L 07/02/21 17:18 07/09/21 08:17 1Heptachlor epoxide (1C)
ND 0.0300.11 ug/L 07/02/21 17:18 07/09/21 08:17 1Methoxychlor (1C)
ND 0.301.0 ug/L 07/02/21 17:18 07/09/21 08:17 1Toxaphene (1C)
ND 0.00500.030 ug/L 07/02/21 17:18 07/09/21 08:17 1p,p'-DDD (1C)
ND 0.00500.030 ug/L 07/02/21 17:18 07/09/21 08:17 1p,p'-DDE (1C)
ND 0.00520.030 ug/L 07/02/21 17:18 07/09/21 08:17 1p,p'-DDT (1C)
DCB Decachlorobiphenyl (Surr) (1C)73 32 -149 07/09/21 08:17 1
MB MB
Surrogate
07/02/21 17:18
Dil FacPreparedAnalyzedQualifierLimits%Recovery
72 07/02/21 17:18 07/09/21 08:17 1DCB Decachlorobiphenyl (Surr) (2C)32 -149
35 07/02/21 17:18 07/09/21 08:17 1Tetrachloro-m-xylene (Surr) (1C)29 -129
33 07/02/21 17:18 07/09/21 08:17 1Tetrachloro-m-xylene (Surr) (2C)29 -129
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-144907/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 146028 Prep Batch: 144907
Aldrin (1C)0.101 0.0847 ug/L 84 28 -119
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
alpha-BHC (2C)0.101 0.101 ug/L 99 47 -132
beta-BHC (1C)0.100 0.114 ug/L 114 27 -143
delta-BHC (1C)0.100 0.110 ug/L 110 28 -141
Dieldrin (1C)0.200 0.201 ug/L 100 31 -145
Endosulfan I (1C)0.101 0.0931 ug/L 92 40 -138
Endosulfan II (1C)0.201 0.189 ug/L 94 27 -138
Endosulfan sulfate (2C)0.201 0.190 ug/L 94 41 -133
Endrin (1C)0.200 0.200 ug/L 100 35 -143
Endrin aldehyde (1C)0.201 0.148 ug/L 74 40 -135
Endrin ketone (1C)0.200 0.201 ug/L 100 44 -136
gamma-BHC (Lindane) (2C)0.100 0.0990 ug/L 99 29 -136
Heptachlor (2C)0.101 0.0763 ug/L 75 38 -135
Heptachlor epoxide (1C)0.100 0.0980 ug/L 98 28 -146
Methoxychlor (2C)1.01 1.11 ug/L 110 39 -143
Eurofins Lancaster Laboratories Env, LLC
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QC Sample Results
Job ID: 410-45293-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-144907/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 146028 Prep Batch: 144907
p,p'-DDD (1C)0.201 0.208 ug/L 103 42 -148
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
p,p'-DDE (1C)0.201 0.183 ug/L 91 22 -138
p,p'-DDT (1C)0.201 0.197 ug/L 98 40 -145
DCB Decachlorobiphenyl (Surr)
(1C)
32 -149
Surrogate
89
LCS LCS
Qualifier Limits%Recovery
90DCB Decachlorobiphenyl (Surr)
(2C)
32 -149
85Tetrachloro-m-xylene (Surr)
(1C)
29 -129
74Tetrachloro-m-xylene (Surr)
(2C)
29 -129
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-144907/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 146647 Prep Batch: 144907
Aldrin (1C)0.101 0.0505 *1 ug/L 50 28 -119 51 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
alpha-BHC (1C)0.101 0.0930 ug/L 92 47 -132 8 30
beta-BHC (1C)0.100 0.0969 ug/L 97 27 -143 16 30
delta-BHC (2C)0.100 0.100 ug/L 100 28 -141 10 30
Dieldrin (2C)0.200 0.189 ug/L 94 31 -145 6 30
Endosulfan I (2C)0.101 0.0878 ug/L 87 40 -138 6 30
Endosulfan II (2C)0.201 0.193 ug/L 96 27 -138 2 30
Endosulfan sulfate (1C)0.201 0.187 ug/L 93 41 -133 1 30
Endrin (1C)0.200 0.187 ug/L 93 35 -143 7 30
Endrin aldehyde (1C)0.201 0.177 ug/L 88 40 -135 18 20
Endrin ketone (1C)0.200 0.180 ug/L 90 44 -136 11 30
gamma-BHC (Lindane) (1C)0.100 0.0914 ug/L 91 29 -136 8 30
Heptachlor (1C)0.101 0.0580 ug/L 57 38 -135 27 30
Heptachlor epoxide (2C)0.100 0.0910 ug/L 91 28 -146 7 30
Methoxychlor (1C)1.01 0.972 ug/L 96 39 -143 13 30
p,p'-DDD (2C)0.201 0.184 ug/L 91 42 -148 12 30
p,p'-DDE (1C)0.201 0.137 ug/L 68 22 -138 29 30
p,p'-DDT (1C)0.201 0.164 ug/L 82 40 -145 18 30
DCB Decachlorobiphenyl (Surr)
(1C)
32 -149
Surrogate
32
LCSD LCSD
Qualifier Limits%Recovery
33DCB Decachlorobiphenyl (Surr)
(2C)
32 -149
42Tetrachloro-m-xylene (Surr)
(1C)
29 -129
40Tetrachloro-m-xylene (Surr)
(2C)
29 -129
Eurofins Lancaster Laboratories Env, LLC
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QC Association Summary
Job ID: 410-45293-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
GC Semi VOA
Prep Batch: 144907
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C410-45293-1 Effluent Total/NA
Water 3510C410-45293-2 Influent Total/NA
Water 3510CMB 410-144907/1-A Method Blank Total/NA
Water 3510CLCS 410-144907/2-A Lab Control Sample Total/NA
Water 3510CLCSD 410-144907/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 145510
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8081B 144907410-45293-1 Effluent Total/NA
Water 8081B 144907410-45293-2 Influent Total/NA
Analysis Batch: 146028
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8081B 144907LCS 410-144907/2-A Lab Control Sample Total/NA
Analysis Batch: 146647
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8081B 144907MB 410-144907/1-A Method Blank Total/NA
Water 8081B 144907LCSD 410-144907/3-A Lab Control Sample Dup Total/NA
Eurofins Lancaster Laboratories Env, LLC
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Lab Chronicle
Client: SynTerra Job ID: 410-45293-1
Project/Site: Rte 211 Treatment System, NC
Client Sample ID: Effluent Lab Sample ID: 410-45293-1
Matrix: WaterDate Collected: 06/28/21 14:30
Date Received: 06/29/21 08:23
Prep 3510C 07/02/21 17:18 QQ3P144907 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8081B 1 145510 07/06/21 19:19 ZO3C ELLETotal/NA
Client Sample ID: Influent Lab Sample ID: 410-45293-2
Matrix: WaterDate Collected: 06/28/21 14:35
Date Received: 06/29/21 08:23
Prep 3510C 07/02/21 17:18 QQ3P144907 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8081B 5 145510 07/06/21 19:30 ZO3C ELLETotal/NA
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Lancaster Laboratories Env, LLC
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Accreditation/Certification Summary
Client: SynTerra Job ID: 410-45293-1
Project/Site: Rte 211 Treatment System, NC
Laboratory: Eurofins Lancaster Laboratories Env, LLC
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (DW)42705State 07-31-21
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification .
Analysis Method Prep Method Matrix Analyte
8081B 3510C Water Aldrin (1C)
8081B 3510C Water Aldrin (2C)
8081B 3510C Water alpha-BHC (1C)
8081B 3510C Water alpha-BHC (2C)
8081B 3510C Water alpha-Chlordane (1C)
8081B 3510C Water beta-BHC (1C)
8081B 3510C Water beta-BHC (2C)
8081B 3510C Water delta-BHC (1C)
8081B 3510C Water delta-BHC (2C)
8081B 3510C Water Dieldrin (1C)
8081B 3510C Water Endosulfan I (1C)
8081B 3510C Water Endosulfan II (1C)
8081B 3510C Water Endosulfan sulfate (1C)
8081B 3510C Water Endosulfan sulfate (2C)
8081B 3510C Water Endrin (1C)
8081B 3510C Water Endrin aldehyde (1C)
8081B 3510C Water Endrin ketone (1C)
8081B 3510C Water gamma-BHC (Lindane) (1C)
8081B 3510C Water gamma-Chlordane (1C)
8081B 3510C Water Heptachlor (1C)
8081B 3510C Water Heptachlor epoxide (1C)
8081B 3510C Water Methoxychlor (1C)
8081B 3510C Water Methoxychlor (2C)
8081B 3510C Water p,p'-DDD (1C)
8081B 3510C Water p,p'-DDD (2C)
8081B 3510C Water p,p'-DDE (1C)
8081B 3510C Water p,p'-DDT (1C)
8081B 3510C Water Toxaphene (1C)
Eurofins Lancaster Laboratories Env, LLC
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Method Summary
Job ID: 410-45293-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Method Method Description LaboratoryProtocol
SW8468081BOrganochlorine Pesticides (GC)ELLE
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)ELLE
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Lancaster Laboratories Env, LLC
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Sample Summary
Job ID: 410-45293-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
410-45293-1 Effluent Water 06/28/21 14:30 06/29/21 08:23
410-45293-2 Influent Water 06/28/21 14:35 06/29/21 08:23
Eurofins Lancaster Laboratories Env, LLC
Page 16 of 18 7/9/2021
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Login Sample Receipt Checklist
Client: SynTerra Job Number: 410-45293-1
Login Number: 45293
Question Answer Comment
Creator: Lugardo, Tamara
List Source: Eurofins Lancaster Laboratories Env, LLC
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
TrueMultiphasic samples are not present.
N/ASamples do not require splitting or compositing.
TrueIs the Field Sampler's name present on COC?
N/ASample Preservation Verified.
N/AResidual Chlorine Checked.
N/ASample custody seals are intact.
Eurofins Lancaster Laboratories Env, LLC
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ANALYTICAL REPORT
Eurofins Lancaster Laboratories Env, LLC
2425 New Holland Pike
Lancaster, PA 17601
Tel: [phone]
Laboratory Job ID: 410-65475-1
Client Project/Site: Rte 211 Treatment System, NC
Sampling Event: Rte 211 Treatment System, NC
For:
SynTerra
148 River Street
Suite 220
Greenville, South Carolina 29601
Attn: Cheryl Glenn
Authorized for release by:
12/9/2021 9:02:30 PM
Marrissa Williams, Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Analytical test results meet all requirements of the associated regulatory program (e.g., NELAC (TNI), DoD,
and ISO 17025) unless otherwise noted under the individual analysis. Data qualifiers are applied to note
exceptions. Noncompliant quality control (QC) is further explained in narrative comments.
· QC results that exceed the upper limits and are associated with non-detect samples are qualified but further
narration is not required since the bias is high and does not change a non-detect result. Further narration is
also not required with QC blank detection when the associated sample concentration is non-detect or more
than ten times the level in the blank.
· Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD is performed, unless otherwise
specified in the method.
· Surrogate and/or isotope dilution analyte recoveries (if applicable) which are outside of the QC window are
confirmed unless attributed to a dilution or otherwise noted in the narrative.
Regulated compliance samples (e.g. SDWA, NPDES) must comply with the associated agency
requirements/permits.
Measurement uncertainty values, as applicable, are available upon request.
Test results relate only to the sample tested. Clients should be aware that a critical step in a chemical or
microbiological analysis is the collection of the sample. Unless the sample analyzed is truly representative of
the bulk of material involved, the test results will be meaningless. If you have questions regarding the proper
techniques of collecting samples, please contact us. We cannot be held responsible for sample integrity,
however, unless sampling has been performed by a member of our staff. Times are local to the area of activity.
Parameters listed in the 40 CFR Part 136 Table II as "analyze immediately" and tested in the laboratory are not
performed within 15 minutes of collection.
This report shall not be reproduced except in full, without the written approval of the laboratory.
WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results
for the sample as submitted. The foregoing express warranty is exclusive and is given in lieu of all other
warranties, expressed or implied, except as otherwise agreed. We disclaim any other warranties, expressed or
implied, including a warranty of fitness for particular purpose and warranty of merchantability. In no event shall
Eurofins Lancaster Laboratories Environmental, LLC be liable for indirect, special, consequential, or incidental
damages including, but not limited to, damages for loss of profit or goodwill regardless of (A) the negligence
(either sole or concurrent) of Eurofins Lancaster Laboratories Environmental and (B) whether Eurofins
Lancaster Laboratories Environmental has been informed of the possibility of such damages. We accept no
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purchase order or other order for work shall be accepted by Eurofins Lancaster Laboratories Environmental
which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster
Laboratories Environmental hereby objects to any conflicting terms contained in any acceptance or order
submitted by client.
Marrissa Williams
Project Manager
12/9/2021 9:02:30 PM
Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Laboratory Job ID: 410-65475-1
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Table of Contents
Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Laboratory Job ID: 410-65475-1
Page 3 of 20
Eurofins Lancaster Laboratories Env, LLC
12/9/2021
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
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Definitions/Glossary
Job ID: 410-65475-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Qualifiers
GC Semi VOA
Qualifier Description
*1 LCS/LCSD RPD exceeds control limits.
Qualifier
cn Refer to Case Narrative for further detail
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
S1-Surrogate recovery exceeds control limits, low biased.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
1C Result is from the primary column on a dual-column method.
2C Result is from the confirmation column on a dual-column method.
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Lancaster Laboratories Env, LLC
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Case Narrative
Client: SynTerra Job ID: 410-65475-1
Project/Site: Rte 211 Treatment System, NC
Job ID: 410-65475-1
Laboratory: Eurofins Lancaster Laboratories Env, LLC
Narrative
Job Narrative
410-65475-1
Receipt
The samples were received on 12/3/2021 11:06 AM. Unless otherwise noted below, the samples arrived in good condition, and, where
required, properly preserved and on ice. The temperature of the cooler at receipt time was 0.8°C
Pesticides
Method 8081B: The DCB Decachlorobiphenyl surrogate recovery for laboratory control sample duplicate (LCSD) associated with
preparation batch 410-202747 and analytical batch 410-203188 was outside the lower control limits. The recoveries for the analytes of
interest were within acceptable control limits. The data is reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
Eurofins Lancaster Laboratories Env, LLC
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Detection Summary
Job ID: 410-65475-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Client Sample ID: Effluent Lab Sample ID: 410-65475-1
No Detections.
Client Sample ID: MW-1 (RT-MW-12)Lab Sample ID: 410-65475-2
No Detections.
Client Sample ID: RT-MW-05 (MW-3)Lab Sample ID: 410-65475-3
No Detections.
Client Sample ID: MW-2 (05-MW-01)Lab Sample ID: 410-65475-4
alpha-Chlordane (2C)
RL
0.021 ug/L
MDL
0.0031
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J *1 cn0.0035 8081B
beta-BHC (1C)0.021 ug/L0.0035 Total/NA10.052 cn 8081B
Toxaphene (1C)1.0 ug/L0.31 Total/NA10.52 J cn 8081B
Client Sample ID: Influent Lab Sample ID: 410-65475-5
alpha-BHC (2C)
RL
0.022 ug/L
MDL
0.0032
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J p *1 cn0.021 8081B
alpha-Chlordane (2C)0.022 ug/L0.0032 Total/NA10.070 *1 cn 8081B
Dieldrin (2C)0.032 ug/L0.0057 Total/NA10.0098 J p *1 cn 8081B
Endosulfan I (2C)0.022 ug/L0.0046 Total/NA10.040 *1 cn 8081B
Endosulfan II (2C)0.043 ug/L0.016 Total/NA10.059 p *1 cn 8081B
Endosulfan sulfate (1C)0.032 ug/L0.0063 Total/NA10.095 cn 8081B
Endrin aldehyde (2C)0.11 ug/L0.022 Total/NA10.056 J p *1 cn 8081B
Endrin ketone (2C)0.032 ug/L0.0054 Total/NA10.053 cn 8081B
gamma-BHC (Lindane) (2C)0.022 ug/L0.0022 Total/NA10.013 J p *1 cn 8081B
gamma-Chlordane (1C)0.043 ug/L0.0075 Total/NA10.037 J p *1 cn 8081B
Heptachlor epoxide (2C)0.022 ug/L0.0025 Total/NA10.0072 J p *1 cn 8081B
Methoxychlor (2C)0.12 ug/L0.032 Total/NA10.18 p cn 8081B
Toxaphene (2C)1.1 ug/L0.32 Total/NA15.2 p cn 8081B
p,p'-DDD (2C)0.032 ug/L0.0054 Total/NA10.044 p *1 cn 8081B
p,p'-DDE (2C)0.032 ug/L0.0054 Total/NA10.0070 J p *1 cn 8081B
p,p'-DDT (2C)0.032 ug/L0.0056 Total/NA10.014 J p *1 cn 8081B
beta-BHC (1C) - DL 0.22 ug/L0.037 Total/NA101.7 cn 8081B
delta-BHC (1C) - DL 0.22 ug/L0.037 Total/NA101.8 p *1 cn 8081B
Eurofins Lancaster Laboratories Env, LLC
This Detection Summary does not include radiochemical test results.
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Client Sample Results
Job ID: 410-65475-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Lab Sample ID: 410-65475-1Client Sample ID: Effluent
Matrix: WaterDate Collected: 12/02/21 14:20
Date Received: 12/03/21 11:06
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
Aldrin (2C)ND *1 cn 0.022 0.0022 ug/L 12/08/21 08:43 12/09/21 10:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.022 0.0033 ug/L 12/08/21 08:43 12/09/21 10:44 1alpha-BHC (1C)ND *1 cn
0.022 0.0033 ug/L 12/08/21 08:43 12/09/21 10:44 1alpha-Chlordane (1C)ND *1 cn
0.022 0.0037 ug/L 12/08/21 08:43 12/09/21 10:44 1beta-BHC (1C)ND cn
0.022 0.0037 ug/L 12/08/21 08:43 12/09/21 10:44 1delta-BHC (1C)ND *1 cn
0.033 0.0057 ug/L 12/08/21 08:43 12/09/21 10:44 1Dieldrin (1C)ND *1 cn
0.022 0.0047 ug/L 12/08/21 08:43 12/09/21 10:44 1Endosulfan I (1C)ND *1 cn
0.043 0.016 ug/L 12/08/21 08:43 12/09/21 10:44 1Endosulfan II (1C)ND *1 cn
0.033 0.0063 ug/L 12/08/21 08:43 12/09/21 10:44 1Endosulfan sulfate (1C)ND cn
0.033 0.0088 ug/L 12/08/21 08:43 12/09/21 10:44 1Endrin (1C)ND *1 cn
0.11 0.022 ug/L 12/08/21 08:43 12/09/21 10:44 1Endrin aldehyde (1C)ND *1 cn
0.033 0.0054 ug/L 12/08/21 08:43 12/09/21 10:44 1Endrin ketone (1C)ND *1 cn
0.022 0.0022 ug/L 12/08/21 08:43 12/09/21 10:44 1gamma-BHC (Lindane) (2C)ND *1 cn
0.043 0.0076 ug/L 12/08/21 08:43 12/09/21 10:44 1gamma-Chlordane (1C)ND *1 cn
0.022 0.0022 ug/L 12/08/21 08:43 12/09/21 10:44 1Heptachlor (1C)ND cn
0.022 0.0025 ug/L 12/08/21 08:43 12/09/21 10:44 1Heptachlor epoxide (1C)ND *1 cn
0.12 0.033 ug/L 12/08/21 08:43 12/09/21 10:44 1Methoxychlor (1C)ND cn
1.1 0.33 ug/L 12/08/21 08:43 12/09/21 10:44 1Toxaphene (1C)ND cn
0.033 0.0054 ug/L 12/08/21 08:43 12/09/21 10:44 1p,p'-DDD (1C)ND *1 cn
0.033 0.0054 ug/L 12/08/21 08:43 12/09/21 10:44 1p,p'-DDE (1C)ND *1 cn
0.033 0.0056 ug/L 12/08/21 08:43 12/09/21 10:44 1p,p'-DDT (1C)ND *1 cn
DCB Decachlorobiphenyl (Surr) (1C)84 cn 20 -149 12/08/21 08:43 12/09/21 10:44 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr) (2C)77 cn 12/08/21 08:43 12/09/21 10:44 120-149
Tetrachloro-m-xylene (Surr) (1C)79 cn 12/08/21 08:43 12/09/21 10:44 120-129
Tetrachloro-m-xylene (Surr) (2C)69 cn 12/08/21 08:43 12/09/21 10:44 120-129
Lab Sample ID: 410-65475-2Client Sample ID: MW-1 (RT-MW-12)
Matrix: WaterDate Collected: 12/02/21 11:05
Date Received: 12/03/21 11:06
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
Aldrin (1C)ND *1 cn 0.021 0.0021 ug/L 12/08/21 08:43 12/09/21 10:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.021 0.0032 ug/L 12/08/21 08:43 12/09/21 10:56 1alpha-BHC (1C)ND *1 cn
0.021 0.0032 ug/L 12/08/21 08:43 12/09/21 10:56 1alpha-Chlordane (1C)ND *1 cn
0.021 0.0036 ug/L 12/08/21 08:43 12/09/21 10:56 1beta-BHC (1C)ND cn
0.021 0.0036 ug/L 12/08/21 08:43 12/09/21 10:56 1delta-BHC (1C)ND *1 cn
0.032 0.0056 ug/L 12/08/21 08:43 12/09/21 10:56 1Dieldrin (1C)ND *1 cn
0.021 0.0045 ug/L 12/08/21 08:43 12/09/21 10:56 1Endosulfan I (1C)ND *1 cn
0.042 0.016 ug/L 12/08/21 08:43 12/09/21 10:56 1Endosulfan II (1C)ND *1 cn
0.032 0.0061 ug/L 12/08/21 08:43 12/09/21 10:56 1Endosulfan sulfate (1C)ND cn
0.032 0.0085 ug/L 12/08/21 08:43 12/09/21 10:56 1Endrin (1C)ND *1 cn
0.11 0.021 ug/L 12/08/21 08:43 12/09/21 10:56 1Endrin aldehyde (1C)ND *1 cn
0.032 0.0053 ug/L 12/08/21 08:43 12/09/21 10:56 1Endrin ketone (1C)ND *1 cn
0.021 0.0021 ug/L 12/08/21 08:43 12/09/21 10:56 1gamma-BHC (Lindane) (1C)ND *1 cn
0.042 0.0074 ug/L 12/08/21 08:43 12/09/21 10:56 1gamma-Chlordane (1C)ND *1 cn
0.021 0.0021 ug/L 12/08/21 08:43 12/09/21 10:56 1Heptachlor (1C)ND cn
0.021 0.0024 ug/L 12/08/21 08:43 12/09/21 10:56 1Heptachlor epoxide (1C)ND *1 cn
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Client Sample Results
Job ID: 410-65475-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Lab Sample ID: 410-65475-2Client Sample ID: MW-1 (RT-MW-12)
Matrix: WaterDate Collected: 12/02/21 11:05
Date Received: 12/03/21 11:06
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
Methoxychlor (1C)ND cn 0.12 0.032 ug/L 12/08/21 08:43 12/09/21 10:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.1 0.32 ug/L 12/08/21 08:43 12/09/21 10:56 1Toxaphene (1C)ND cn
0.032 0.0053 ug/L 12/08/21 08:43 12/09/21 10:56 1p,p'-DDD (1C)ND *1 cn
0.032 0.0053 ug/L 12/08/21 08:43 12/09/21 10:56 1p,p'-DDE (1C)ND *1 cn
0.032 0.0055 ug/L 12/08/21 08:43 12/09/21 10:56 1p,p'-DDT (1C)ND *1 cn
DCB Decachlorobiphenyl (Surr) (1C)73 cn 20 -149 12/08/21 08:43 12/09/21 10:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr) (2C)65 cn 12/08/21 08:43 12/09/21 10:56 120-149
Tetrachloro-m-xylene (Surr) (1C)75 cn 12/08/21 08:43 12/09/21 10:56 120-129
Tetrachloro-m-xylene (Surr) (2C)65 cn 12/08/21 08:43 12/09/21 10:56 120-129
Lab Sample ID: 410-65475-3Client Sample ID: RT-MW-05 (MW-3)
Matrix: WaterDate Collected: 12/02/21 12:22
Date Received: 12/03/21 11:06
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
Aldrin (1C)ND *1 cn 0.021 0.0021 ug/L 12/08/21 08:43 12/09/21 11:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.021 0.0032 ug/L 12/08/21 08:43 12/09/21 11:09 1alpha-BHC (1C)ND *1 cn
0.021 0.0032 ug/L 12/08/21 08:43 12/09/21 11:09 1alpha-Chlordane (1C)ND *1 cn
0.021 0.0036 ug/L 12/08/21 08:43 12/09/21 11:09 1beta-BHC (1C)ND cn
0.021 0.0036 ug/L 12/08/21 08:43 12/09/21 11:09 1delta-BHC (1C)ND *1 cn
0.032 0.0056 ug/L 12/08/21 08:43 12/09/21 11:09 1Dieldrin (1C)ND *1 cn
0.021 0.0046 ug/L 12/08/21 08:43 12/09/21 11:09 1Endosulfan I (1C)ND *1 cn
0.042 0.016 ug/L 12/08/21 08:43 12/09/21 11:09 1Endosulfan II (1C)ND *1 cn
0.032 0.0062 ug/L 12/08/21 08:43 12/09/21 11:09 1Endosulfan sulfate (1C)ND cn
0.032 0.0086 ug/L 12/08/21 08:43 12/09/21 11:09 1Endrin (1C)ND *1 cn
0.11 0.021 ug/L 12/08/21 08:43 12/09/21 11:09 1Endrin aldehyde (1C)ND *1 cn
0.032 0.0053 ug/L 12/08/21 08:43 12/09/21 11:09 1Endrin ketone (1C)ND *1 cn
0.021 0.0021 ug/L 12/08/21 08:43 12/09/21 11:09 1gamma-BHC (Lindane) (1C)ND *1 cn
0.042 0.0074 ug/L 12/08/21 08:43 12/09/21 11:09 1gamma-Chlordane (1C)ND *1 cn
0.021 0.0021 ug/L 12/08/21 08:43 12/09/21 11:09 1Heptachlor (1C)ND cn
0.021 0.0024 ug/L 12/08/21 08:43 12/09/21 11:09 1Heptachlor epoxide (1C)ND *1 cn
0.12 0.032 ug/L 12/08/21 08:43 12/09/21 11:09 1Methoxychlor (1C)ND cn
1.1 0.32 ug/L 12/08/21 08:43 12/09/21 11:09 1Toxaphene (1C)ND cn
0.032 0.0053 ug/L 12/08/21 08:43 12/09/21 11:09 1p,p'-DDD (1C)ND *1 cn
0.032 0.0053 ug/L 12/08/21 08:43 12/09/21 11:09 1p,p'-DDE (1C)ND *1 cn
0.032 0.0055 ug/L 12/08/21 08:43 12/09/21 11:09 1p,p'-DDT (1C)ND *1 cn
DCB Decachlorobiphenyl (Surr) (1C)73 cn 20 -149 12/08/21 08:43 12/09/21 11:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr) (2C)65 cn 12/08/21 08:43 12/09/21 11:09 120-149
Tetrachloro-m-xylene (Surr) (1C)73 cn 12/08/21 08:43 12/09/21 11:09 120-129
Tetrachloro-m-xylene (Surr) (2C)62 cn 12/08/21 08:43 12/09/21 11:09 120-129
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Client Sample Results
Job ID: 410-65475-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Lab Sample ID: 410-65475-4Client Sample ID: MW-2 (05-MW-01)
Matrix: WaterDate Collected: 12/02/21 10:27
Date Received: 12/03/21 11:06
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
Aldrin (1C)ND *1 cn 0.021 0.0021 ug/L 12/08/21 08:43 12/09/21 11:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.021 0.0031 ug/L 12/08/21 08:43 12/09/21 11:21 1alpha-BHC (1C)ND *1 cn
0.021 0.0031 ug/L 12/08/21 08:43 12/09/21 11:21 1alpha-Chlordane (2C)0.0035 J *1 cn
0.021 0.0035 ug/L 12/08/21 08:43 12/09/21 11:21 1beta-BHC (1C)0.052 cn
0.021 0.0035 ug/L 12/08/21 08:43 12/09/21 11:21 1delta-BHC (1C)ND *1 cn
0.031 0.0055 ug/L 12/08/21 08:43 12/09/21 11:21 1Dieldrin (1C)ND *1 cn
0.021 0.0045 ug/L 12/08/21 08:43 12/09/21 11:21 1Endosulfan I (1C)ND *1 cn
0.042 0.016 ug/L 12/08/21 08:43 12/09/21 11:21 1Endosulfan II (2C)ND *1 cn
0.031 0.0060 ug/L 12/08/21 08:43 12/09/21 11:21 1Endosulfan sulfate (1C)ND cn
0.031 0.0084 ug/L 12/08/21 08:43 12/09/21 11:21 1Endrin (1C)ND *1 cn
0.10 0.021 ug/L 12/08/21 08:43 12/09/21 11:21 1Endrin aldehyde (1C)ND *1 cn
0.031 0.0052 ug/L 12/08/21 08:43 12/09/21 11:21 1Endrin ketone (1C)ND *1 cn
0.021 0.0021 ug/L 12/08/21 08:43 12/09/21 11:21 1gamma-BHC (Lindane) (1C)ND *1 cn
0.042 0.0073 ug/L 12/08/21 08:43 12/09/21 11:21 1gamma-Chlordane (1C)ND *1 cn
0.021 0.0021 ug/L 12/08/21 08:43 12/09/21 11:21 1Heptachlor (1C)ND cn
0.021 0.0024 ug/L 12/08/21 08:43 12/09/21 11:21 1Heptachlor epoxide (1C)ND *1 cn
0.11 0.031 ug/L 12/08/21 08:43 12/09/21 11:21 1Methoxychlor (1C)ND cn
1.0 0.31 ug/L 12/08/21 08:43 12/09/21 11:21 1Toxaphene (1C)0.52 J cn
0.031 0.0052 ug/L 12/08/21 08:43 12/09/21 11:21 1p,p'-DDD (2C)ND *1 cn
0.031 0.0052 ug/L 12/08/21 08:43 12/09/21 11:21 1p,p'-DDE (1C)ND *1 cn
0.031 0.0054 ug/L 12/08/21 08:43 12/09/21 11:21 1p,p'-DDT (1C)ND *1 cn
DCB Decachlorobiphenyl (Surr) (1C)79 cn 20 -149 12/08/21 08:43 12/09/21 11:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr) (2C)72 cn 12/08/21 08:43 12/09/21 11:21 120-149
Tetrachloro-m-xylene (Surr) (1C)80 cn 12/08/21 08:43 12/09/21 11:21 120-129
Tetrachloro-m-xylene (Surr) (2C)71 cn 12/08/21 08:43 12/09/21 11:21 120-129
Lab Sample ID: 410-65475-5Client Sample ID: Influent
Matrix: WaterDate Collected: 12/02/21 14:30
Date Received: 12/03/21 11:06
Method: 8081B - Organochlorine Pesticides (GC)
RL MDL
alpha-BHC (2C)0.021 J p *1 cn 0.022 0.0032 ug/L 12/08/21 08:43 12/09/21 11:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.022 0.0032 ug/L 12/08/21 08:43 12/09/21 11:33 1alpha-Chlordane (2C)0.070 *1 cn
0.032 0.0057 ug/L 12/08/21 08:43 12/09/21 11:33 1Dieldrin (2C)0.0098 J p *1 cn
0.022 0.0046 ug/L 12/08/21 08:43 12/09/21 11:33 1Endosulfan I (2C)0.040 *1 cn
0.043 0.016 ug/L 12/08/21 08:43 12/09/21 11:33 1Endosulfan II (2C)0.059 p *1 cn
0.032 0.0063 ug/L 12/08/21 08:43 12/09/21 11:33 1Endosulfan sulfate (1C)0.095 cn
0.032 0.0087 ug/L 12/08/21 08:43 12/09/21 11:33 1Endrin (2C)ND *1 cn
0.11 0.022 ug/L 12/08/21 08:43 12/09/21 11:33 1Endrin aldehyde (2C)0.056 J p *1 cn
0.032 0.0054 ug/L 12/08/21 08:43 12/09/21 11:33 1Endrin ketone (2C)0.053 cn
0.022 0.0022 ug/L 12/08/21 08:43 12/09/21 11:33 1gamma-BHC (Lindane) (2C)0.013 J p *1 cn
0.043 0.0075 ug/L 12/08/21 08:43 12/09/21 11:33 1gamma-Chlordane (1C)0.037 J p *1 cn
0.022 0.0022 ug/L 12/08/21 08:43 12/09/21 11:33 1Heptachlor (1C)ND cn
0.022 0.0025 ug/L 12/08/21 08:43 12/09/21 11:33 1Heptachlor epoxide (2C)0.0072 J p *1 cn
0.12 0.032 ug/L 12/08/21 08:43 12/09/21 11:33 1Methoxychlor (2C)0.18 p cn
1.1 0.32 ug/L 12/08/21 08:43 12/09/21 11:33 1Toxaphene (2C)5.2 p cn
0.032 0.0054 ug/L 12/08/21 08:43 12/09/21 11:33 1p,p'-DDD (2C)0.044 p *1 cn
Eurofins Lancaster Laboratories Env, LLC
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Client Sample Results
Job ID: 410-65475-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Lab Sample ID: 410-65475-5Client Sample ID: Influent
Matrix: WaterDate Collected: 12/02/21 14:30
Date Received: 12/03/21 11:06
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
RL MDL
p,p'-DDE (2C)0.0070 J p *1 cn 0.032 0.0054 ug/L 12/08/21 08:43 12/09/21 11:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.032 0.0056 ug/L 12/08/21 08:43 12/09/21 11:33 1p,p'-DDT (2C)0.014 J p *1 cn
DCB Decachlorobiphenyl (Surr) (1C)84 cn 20 -149 12/08/21 08:43 12/09/21 11:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr) (2C)76 cn 12/08/21 08:43 12/09/21 11:33 120-149
Tetrachloro-m-xylene (Surr) (1C)77 cn 12/08/21 08:43 12/09/21 11:33 120-129
Tetrachloro-m-xylene (Surr) (2C)64 cn 12/08/21 08:43 12/09/21 11:33 120-129
Method: 8081B - Organochlorine Pesticides (GC) - DL
RL MDL
Aldrin (2C)ND *1 cn 0.22 0.022 ug/L 12/08/21 08:43 12/09/21 13:09 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.22 0.037 ug/L 12/08/21 08:43 12/09/21 13:09 10beta-BHC (1C)1.7 cn
0.22 0.037 ug/L 12/08/21 08:43 12/09/21 13:09 10delta-BHC (1C)1.8 p *1 cn
DCB Decachlorobiphenyl (Surr) (1C)112 cn 20 -149 12/08/21 08:43 12/09/21 13:09 10
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
DCB Decachlorobiphenyl (Surr) (2C)93 cn 12/08/21 08:43 12/09/21 13:09 1020-149
Tetrachloro-m-xylene (Surr) (1C)87 cn 12/08/21 08:43 12/09/21 13:09 1020-129
Tetrachloro-m-xylene (Surr) (2C)66 cn 12/08/21 08:43 12/09/21 13:09 1020-129
Eurofins Lancaster Laboratories Env, LLC
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Surrogate Summary
Job ID: 410-65475-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Method: 8081B - Organochlorine Pesticides (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (20-149)(20-149)(20-129)(20-129)
DCB1 DCB2 TCX1 TCX2
84 cn 77 cn 79 cn 69 cn410-65475-1
Percent Surrogate Recovery (Acceptance Limits)
Effluent
73 cn 65 cn 75 cn 65 cn410-65475-2 MW-1 (RT-MW-12)
73 cn 65 cn 73 cn 62 cn410-65475-3 RT-MW-05 (MW-3)
79 cn 72 cn 80 cn 71 cn410-65475-4 MW-2 (05-MW-01)
84 cn 76 cn 77 cn 64 cn410-65475-5 Influent
112 cn 93 cn 87 cn 66 cn410-65475-5 - DL Influent
87 80 82 72LCS 410-202747/2-A Lab Control Sample
12 S1-11 S1-56 51LCSD 410-202747/3-A Lab Control Sample Dup
85 80 85 75MB 410-202747/1-A Method Blank
Surrogate Legend
DCB = DCB Decachlorobiphenyl (Surr)
TCX = Tetrachloro-m-xylene (Surr)
Eurofins Lancaster Laboratories Env, LLC
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QC Sample Results
Job ID: 410-65475-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Method: 8081B - Organochlorine Pesticides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 410-202747/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 203188 Prep Batch: 202747
RL MDL
Aldrin (1C)ND 0.020 0.0020 ug/L 12/08/21 08:43 12/09/21 06:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00300.020 ug/L 12/08/21 08:43 12/09/21 06:53 1alpha-BHC (1C)
ND 0.00300.020 ug/L 12/08/21 08:43 12/09/21 06:53 1alpha-Chlordane (1C)
ND 0.00340.020 ug/L 12/08/21 08:43 12/09/21 06:53 1beta-BHC (1C)
ND 0.00340.020 ug/L 12/08/21 08:43 12/09/21 06:53 1delta-BHC (1C)
ND 0.00530.030 ug/L 12/08/21 08:43 12/09/21 06:53 1Dieldrin (1C)
ND 0.00430.020 ug/L 12/08/21 08:43 12/09/21 06:53 1Endosulfan I (1C)
ND 0.0150.040 ug/L 12/08/21 08:43 12/09/21 06:53 1Endosulfan II (1C)
ND 0.00580.030 ug/L 12/08/21 08:43 12/09/21 06:53 1Endosulfan sulfate (1C)
ND 0.00810.030 ug/L 12/08/21 08:43 12/09/21 06:53 1Endrin (1C)
ND 0.0200.10 ug/L 12/08/21 08:43 12/09/21 06:53 1Endrin aldehyde (1C)
ND 0.00500.030 ug/L 12/08/21 08:43 12/09/21 06:53 1Endrin ketone (1C)
ND 0.00200.020 ug/L 12/08/21 08:43 12/09/21 06:53 1gamma-BHC (Lindane) (1C)
ND 0.00700.040 ug/L 12/08/21 08:43 12/09/21 06:53 1gamma-Chlordane (1C)
ND 0.00200.020 ug/L 12/08/21 08:43 12/09/21 06:53 1Heptachlor (1C)
ND 0.00230.020 ug/L 12/08/21 08:43 12/09/21 06:53 1Heptachlor epoxide (1C)
ND 0.0300.11 ug/L 12/08/21 08:43 12/09/21 06:53 1Methoxychlor (1C)
ND 0.301.0 ug/L 12/08/21 08:43 12/09/21 06:53 1Toxaphene (1C)
ND 0.00500.030 ug/L 12/08/21 08:43 12/09/21 06:53 1p,p'-DDD (1C)
ND 0.00500.030 ug/L 12/08/21 08:43 12/09/21 06:53 1p,p'-DDE (1C)
ND 0.00520.030 ug/L 12/08/21 08:43 12/09/21 06:53 1p,p'-DDT (1C)
DCB Decachlorobiphenyl (Surr) (1C)85 20 -149 12/09/21 06:53 1
MB MB
Surrogate
12/08/21 08:43
Dil FacPreparedAnalyzedQualifierLimits%Recovery
80 12/08/21 08:43 12/09/21 06:53 1DCB Decachlorobiphenyl (Surr) (2C)20 -149
85 12/08/21 08:43 12/09/21 06:53 1Tetrachloro-m-xylene (Surr) (1C)20 -129
75 12/08/21 08:43 12/09/21 06:53 1Tetrachloro-m-xylene (Surr) (2C)20 -129
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-202747/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 203188 Prep Batch: 202747
Aldrin (1C)0.101 0.0983 ug/L 97 10 -148
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
alpha-BHC (1C)0.101 0.110 ug/L 109 47 -132
beta-BHC (1C)0.100 0.112 ug/L 112 65 -139
delta-BHC (1C)0.100 0.111 ug/L 111 56 -141
Dieldrin (1C)0.200 0.237 ug/L 118 58 -145
Endosulfan I (1C)0.101 0.109 ug/L 107 40 -138
Endosulfan II (1C)0.201 0.226 ug/L 113 61 -138
Endosulfan sulfate (1C)0.201 0.226 ug/L 112 41 -133
Endrin (1C)0.200 0.249 ug/L 124 63 -131
Endrin aldehyde (1C)0.201 0.208 ug/L 103 57 -135
Endrin ketone (1C)0.200 0.228 ug/L 114 67 -136
gamma-BHC (Lindane) (1C)0.100 0.106 ug/L 106 61 -139
Heptachlor (1C)0.101 0.107 ug/L 105 35 -136
Heptachlor epoxide (1C)0.100 0.114 ug/L 114 59 -146
Methoxychlor (1C)1.01 1.32 ug/L 131 66 -148
Eurofins Lancaster Laboratories Env, LLC
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QC Sample Results
Job ID: 410-65475-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Method: 8081B - Organochlorine Pesticides (GC) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 410-202747/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 203188 Prep Batch: 202747
p,p'-DDD (1C)0.201 0.234 ug/L 116 42 -148
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
p,p'-DDE (1C)0.201 0.218 ug/L 108 20 -140
p,p'-DDT (1C)0.201 0.266 ug/L 132 40 -145
DCB Decachlorobiphenyl (Surr)
(1C)
20 -149
Surrogate
87
LCS LCS
Qualifier Limits%Recovery
80DCB Decachlorobiphenyl (Surr)
(2C)
20 -149
82Tetrachloro-m-xylene (Surr)
(1C)
20 -129
72Tetrachloro-m-xylene (Surr)
(2C)
20 -129
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 410-202747/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 203188 Prep Batch: 202747
Aldrin (1C)0.101 0.0686 *1 ug/L 68 10 -148 36 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
alpha-BHC (1C)0.101 0.0782 *1 ug/L 77 47 -132 34 30
beta-BHC (1C)0.100 0.101 ug/L 101 65 -139 10 30
delta-BHC (1C)0.100 0.0806 *1 ug/L 81 56 -141 31 30
Dieldrin (1C)0.200 0.172 *1 ug/L 86 58 -145 32 30
Endosulfan I (1C)0.101 0.0769 *1 ug/L 76 40 -138 34 30
Endosulfan II (1C)0.201 0.166 *1 ug/L 82 61 -138 31 30
Endosulfan sulfate (1C)0.201 0.168 ug/L 84 41 -133 29 30
Endrin (1C)0.200 0.181 *1 ug/L 91 63 -131 31 30
Endrin aldehyde (1C)0.201 0.166 *1 ug/L 83 57 -135 22 20
Endrin ketone (1C)0.200 0.165 *1 ug/L 83 67 -136 32 30
gamma-BHC (Lindane) (1C)0.100 0.0770 *1 ug/L 77 61 -139 32 30
Heptachlor (1C)0.101 0.0786 ug/L 78 35 -136 30 30
Heptachlor epoxide (1C)0.100 0.0795 *1 ug/L 80 59 -146 35 30
Methoxychlor (1C)1.01 1.01 ug/L 100 66 -148 27 30
p,p'-DDD (1C)0.201 0.170 *1 ug/L 84 42 -148 32 30
p,p'-DDE (1C)0.201 0.152 *1 ug/L 76 20 -140 36 30
p,p'-DDT (1C)0.201 0.195 *1 ug/L 97 40 -145 31 30
DCB Decachlorobiphenyl (Surr)
(1C)
S1-20 -149
Surrogate
12
LCSD LCSD
Qualifier Limits%Recovery
11 S1-DCB Decachlorobiphenyl (Surr)
(2C)
20 -149
56Tetrachloro-m-xylene (Surr)
(1C)
20 -129
51Tetrachloro-m-xylene (Surr)
(2C)
20 -129
Eurofins Lancaster Laboratories Env, LLC
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QC Association Summary
Job ID: 410-65475-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
GC Semi VOA
Prep Batch: 202747
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C410-65475-1 Effluent Total/NA
Water 3510C410-65475-2 MW-1 (RT-MW-12)Total/NA
Water 3510C410-65475-3 RT-MW-05 (MW-3)Total/NA
Water 3510C410-65475-4 MW-2 (05-MW-01)Total/NA
Water 3510C410-65475-5 Influent Total/NA
Water 3510C410-65475-5 - DL Influent Total/NA
Water 3510CMB 410-202747/1-A Method Blank Total/NA
Water 3510CLCS 410-202747/2-A Lab Control Sample Total/NA
Water 3510CLCSD 410-202747/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 203188
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8081B 202747410-65475-1 Effluent Total/NA
Water 8081B 202747410-65475-2 MW-1 (RT-MW-12)Total/NA
Water 8081B 202747410-65475-3 RT-MW-05 (MW-3)Total/NA
Water 8081B 202747410-65475-4 MW-2 (05-MW-01)Total/NA
Water 8081B 202747410-65475-5 Influent Total/NA
Water 8081B 202747410-65475-5 - DL Influent Total/NA
Water 8081B 202747MB 410-202747/1-A Method Blank Total/NA
Water 8081B 202747LCS 410-202747/2-A Lab Control Sample Total/NA
Water 8081B 202747LCSD 410-202747/3-A Lab Control Sample Dup Total/NA
Eurofins Lancaster Laboratories Env, LLC
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Lab Chronicle
Client: SynTerra Job ID: 410-65475-1
Project/Site: Rte 211 Treatment System, NC
Client Sample ID: Effluent Lab Sample ID: 410-65475-1
Matrix: WaterDate Collected: 12/02/21 14:20
Date Received: 12/03/21 11:06
Prep 3510C 12/08/21 08:43 BLX5202747 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8081B 1 203188 12/09/21 10:44 WN7O ELLETotal/NA
Client Sample ID: MW-1 (RT-MW-12)Lab Sample ID: 410-65475-2
Matrix: WaterDate Collected: 12/02/21 11:05
Date Received: 12/03/21 11:06
Prep 3510C 12/08/21 08:43 BLX5202747 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8081B 1 203188 12/09/21 10:56 WN7O ELLETotal/NA
Client Sample ID: RT-MW-05 (MW-3)Lab Sample ID: 410-65475-3
Matrix: WaterDate Collected: 12/02/21 12:22
Date Received: 12/03/21 11:06
Prep 3510C 12/08/21 08:43 BLX5202747 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8081B 1 203188 12/09/21 11:09 WN7O ELLETotal/NA
Client Sample ID: MW-2 (05-MW-01)Lab Sample ID: 410-65475-4
Matrix: WaterDate Collected: 12/02/21 10:27
Date Received: 12/03/21 11:06
Prep 3510C 12/08/21 08:43 BLX5202747 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8081B 1 203188 12/09/21 11:21 WN7O ELLETotal/NA
Client Sample ID: Influent Lab Sample ID: 410-65475-5
Matrix: WaterDate Collected: 12/02/21 14:30
Date Received: 12/03/21 11:06
Prep 3510C 12/08/21 08:43 BLX5202747 ELLE
Type
Batch Batch
MethodPrep Type LabAnalystRun
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis 8081B 1 203188 12/09/21 11:33 WN7O ELLETotal/NA
Prep 3510C DL 202747 12/08/21 08:43 BLX5 ELLETotal/NA
Analysis 8081B DL 10 203188 12/09/21 13:09 WN7O ELLETotal/NA
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Lancaster Laboratories Env, LLC
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Accreditation/Certification Summary
Client: SynTerra Job ID: 410-65475-1
Project/Site: Rte 211 Treatment System, NC
Laboratory: Eurofins Lancaster Laboratories Env, LLC
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (DW)State 42705 07-31-22
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification .
Analysis Method Prep Method Matrix Analyte
8081B 3510C Water Aldrin (1C)
8081B 3510C Water Aldrin (2C)
8081B 3510C Water alpha-BHC (1C)
8081B 3510C Water alpha-BHC (2C)
8081B 3510C Water alpha-Chlordane (1C)
8081B 3510C Water alpha-Chlordane (2C)
8081B 3510C Water beta-BHC (1C)
8081B 3510C Water delta-BHC (1C)
8081B 3510C Water Dieldrin (1C)
8081B 3510C Water Dieldrin (2C)
8081B 3510C Water Endosulfan I (1C)
8081B 3510C Water Endosulfan I (2C)
8081B 3510C Water Endosulfan II (1C)
8081B 3510C Water Endosulfan II (2C)
8081B 3510C Water Endosulfan sulfate (1C)
8081B 3510C Water Endrin (1C)
8081B 3510C Water Endrin (2C)
8081B 3510C Water Endrin aldehyde (1C)
8081B 3510C Water Endrin aldehyde (2C)
8081B 3510C Water Endrin ketone (1C)
8081B 3510C Water Endrin ketone (2C)
8081B 3510C Water gamma-BHC (Lindane) (1C)
8081B 3510C Water gamma-BHC (Lindane) (2C)
8081B 3510C Water gamma-Chlordane (1C)
8081B 3510C Water Heptachlor (1C)
8081B 3510C Water Heptachlor epoxide (1C)
8081B 3510C Water Heptachlor epoxide (2C)
8081B 3510C Water Methoxychlor (1C)
8081B 3510C Water Methoxychlor (2C)
8081B 3510C Water p,p'-DDD (1C)
8081B 3510C Water p,p'-DDD (2C)
8081B 3510C Water p,p'-DDE (1C)
8081B 3510C Water p,p'-DDE (2C)
8081B 3510C Water p,p'-DDT (1C)
8081B 3510C Water p,p'-DDT (2C)
8081B 3510C Water Toxaphene (1C)
8081B 3510C Water Toxaphene (2C)
Eurofins Lancaster Laboratories Env, LLC
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Method Summary
Job ID: 410-65475-1Client: SynTerra
Project/Site: Rte 211 Treatment System, NC
Method Method Description LaboratoryProtocol
SW8468081BOrganochlorine Pesticides (GC)ELLE
SW8463510CLiquid-Liquid Extraction (Separatory Funnel)ELLE
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
ELLE = Eurofins Lancaster Laboratories Env, LLC, 2425 New Holland Pike, Lancaster, PA 17601, TEL [phone]
Eurofins Lancaster Laboratories Env, LLC
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Sample Summary
Client: SynTerra Job ID: 410-65475-1
Project/Site: Rte 211 Treatment System, NC
Lab Sample ID Client Sample ID Matrix Collected Received
410-65475-1 Effluent Water 12/02/21 14:20 12/03/21 11:06
410-65475-2 MW-1 (RT-MW-12)Water 12/02/21 11:05 12/03/21 11:06
410-65475-3 RT-MW-05 (MW-3)Water 12/02/21 12:22 12/03/21 11:06
410-65475-4 MW-2 (05-MW-01)Water 12/02/21 10:27 12/03/21 11:06
410-65475-5 Influent Water 12/02/21 14:30 12/03/21 11:06
Eurofins Lancaster Laboratories Env, LLC
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Login Sample Receipt Checklist
Client: SynTerra Job Number: 410-65475-1
Login Number: 65475
Question Answer Comment
Creator: Cunningham, Abigail
List Source: Eurofins Lancaster Laboratories Env, LLC
List Number: 1
TrueThe cooler's custody seal is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable (</=6C, not frozen).
TrueCooler Temperature is recorded.
N/AWV: Container Temperature is acceptable (</=6C, not frozen).
N/AWV: Container Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueThere are no discrepancies between the containers received and the COC.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueThere is sufficient vol. for all requested analyses.
TrueIs the Field Sampler's name present on COC?
N/ASample custody seals are intact.
Eurofins Lancaster Laboratories Env, LLC
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2021 Annual Report – Groundwater Remediation Permit No. WI0600231
Aberdeen Pesticide Dumps Site – Route 211 Area
Aberdeen, North Carolina

ATTACHMENT 2

NCDEQ DIVISION OF WATER RESOURCES
GW-59 FORMS
SUBMIT FORM ON YELLOW PAPER ONLY
GW-59 Rev. 06-07-2018
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:Expiration Date:
Facility Name:Non-Discharge UIC
Permit Name (if different):NPDES Other
Facility Address:TYPE OF PERMITTED OPERATION BEING MONITORED
County Lagoon
(City) (State) (Zip)Spray Field
Contact Person:Telephone#:Rotary Distributor
Well Location/Site Name:No. of wells to be sampled:Water Source Heat Pump
Remediation: Infiltration Gallery
Remediation:
Land Application of Sludge
Other:
(from Permit)
SAMPLING INFORMATION
WELL ID NUMBER (from Permit):Date sample collected:FIELD ANALYSES:
Well Depth:ft.Well Diameter:in.pH 00400: units Temp. 00010: oC
Depth to Water Level 82546: ft. below measuring point Screened Interval:ft.to ft.Spec. Cond. 00094:µMhos
Measuring Point is ft. above land surface Relative M.P. Elevation:ft.Odor 00085:
Volume of water pumped/bailed before sampling:gallons Appearance
Samples for metals were collected unfiltered:YES NO and field acidified:YES NO
LABORATORY INFORMATION
Laboratory Name:Certification No.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L
(Note: Use MPN method for highly turbid samples)Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L
pH (Lab) 00403 units Ba - Barium 01007 ug/L
TOC 00680 mg/L Ca - Calcium 00916 mg/L
Chloride 00940 mg/L Cd - Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium: Total 01034 ug/L
Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached?Yes (1)No (0)
Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 , method #
Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L , method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)Mn - Manganese 01055 ug/L , method #
TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method #
For Remediation Systems Only (Attach Lab Reports):Influent Total VOCs:mg/L Effluent Total VOCs:mg/L VOC Removal%
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent)(Date)
Date sample analyzed:
If WELL
WAS
DRY at
time of
sampling,
check
here:
Mail original
and 1 copy to:
(Street)
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
SUBMIT FORM ON YELLOW PAPER ONLY
GW-59 Rev. 06-07-2018
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:Expiration Date:
Facility Name:Non-Discharge UIC
Permit Name (if different):NPDES Other
Facility Address:TYPE OF PERMITTED OPERATION BEING MONITORED
County Lagoon
(City) (State) (Zip)Spray Field
Contact Person:Telephone#:Rotary Distributor
Well Location/Site Name:No. of wells to be sampled:Water Source Heat Pump
Remediation: Infiltration Gallery
Remediation:
Land Application of Sludge
Other:
(from Permit)
SAMPLING INFORMATION
WELL ID NUMBER (from Permit):Date sample collected:FIELD ANALYSES:
Well Depth:ft.Well Diameter:in.pH 00400: units Temp. 00010: oC
Depth to Water Level 82546: ft. below measuring point Screened Interval:ft.to ft.Spec. Cond. 00094:µMhos
Measuring Point is ft. above land surface Relative M.P. Elevation:ft.Odor 00085:
Volume of water pumped/bailed before sampling:gallons Appearance
Samples for metals were collected unfiltered:YES NO and field acidified:YES NO
LABORATORY INFORMATION
Laboratory Name:Certification No.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L
(Note: Use MPN method for highly turbid samples)Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L
pH (Lab) 00403 units Ba - Barium 01007 ug/L
TOC 00680 mg/L Ca - Calcium 00916 mg/L
Chloride 00940 mg/L Cd - Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium: Total 01034 ug/L
Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached?Yes (1)No (0)
Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 , method #
Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L , method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)Mn - Manganese 01055 ug/L , method #
TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method #
For Remediation Systems Only (Attach Lab Reports):Influent Total VOCs:mg/L Effluent Total VOCs:mg/L VOC Removal%
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent)(Date)
Date sample analyzed:
If WELL
WAS
DRY at
time of
sampling,
check
here:
Mail original
and 1 copy to:
(Street)
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
SUBMIT FORM ON YELLOW PAPER ONLY
GW-59 Rev. 06-07-2018
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:Expiration Date:
Facility Name:Non-Discharge UIC
Permit Name (if different):NPDES Other
Facility Address:TYPE OF PERMITTED OPERATION BEING MONITORED
County Lagoon
(City) (State) (Zip)Spray Field
Contact Person:Telephone#:Rotary Distributor
Well Location/Site Name:No. of wells to be sampled:Water Source Heat Pump
Remediation: Infiltration Gallery
Remediation:
Land Application of Sludge
Other:
(from Permit)
SAMPLING INFORMATION
WELL ID NUMBER (from Permit):Date sample collected:FIELD ANALYSES:
Well Depth:ft.Well Diameter:in.pH 00400: units Temp. 00010: oC
Depth to Water Level 82546: ft. below measuring point Screened Interval:ft.to ft.Spec. Cond. 00094:µMhos
Measuring Point is ft. above land surface Relative M.P. Elevation:ft.Odor 00085:
Volume of water pumped/bailed before sampling:gallons Appearance
Samples for metals were collected unfiltered:YES NO and field acidified:YES NO
LABORATORY INFORMATION
Laboratory Name:Certification No.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L
(Note: Use MPN method for highly turbid samples)Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L
pH (Lab) 00403 units Ba - Barium 01007 ug/L
TOC 00680 mg/L Ca - Calcium 00916 mg/L
Chloride 00940 mg/L Cd - Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium: Total 01034 ug/L
Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached?Yes (1)No (0)
Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 , method #
Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L , method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)Mn - Manganese 01055 ug/L , method #
TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method #
For Remediation Systems Only (Attach Lab Reports):Influent Total VOCs:mg/L Effluent Total VOCs:mg/L VOC Removal%
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent)(Date)
Date sample analyzed:
If WELL
WAS
DRY at
time of
sampling,
check
here:
Mail original
and 1 copy to:
(Street)
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
SUBMIT FORM ON YELLOW PAPER ONLY
GW-59 Rev. 06-07-2018
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:Expiration Date:
Facility Name:Non-Discharge UIC
Permit Name (if different):NPDES Other
Facility Address:TYPE OF PERMITTED OPERATION BEING MONITORED
County Lagoon
(City) (State) (Zip)Spray Field
Contact Person:Telephone#:Rotary Distributor
Well Location/Site Name:No. of wells to be sampled:Water Source Heat Pump
Remediation: Infiltration Gallery
Remediation:
Land Application of Sludge
Other:
(from Permit)
SAMPLING INFORMATION
WELL ID NUMBER (from Permit):Date sample collected:FIELD ANALYSES:
Well Depth:ft.Well Diameter:in.pH 00400: units Temp. 00010: oC
Depth to Water Level 82546: ft. below measuring point Screened Interval:ft.to ft.Spec. Cond. 00094:µMhos
Measuring Point is ft. above land surface Relative M.P. Elevation:ft.Odor 00085:
Volume of water pumped/bailed before sampling:gallons Appearance
Samples for metals were collected unfiltered:YES NO and field acidified:YES NO
LABORATORY INFORMATION
Laboratory Name:Certification No.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L
(Note: Use MPN method for highly turbid samples)Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L
pH (Lab) 00403 units Ba - Barium 01007 ug/L
TOC 00680 mg/L Ca - Calcium 00916 mg/L
Chloride 00940 mg/L Cd - Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium: Total 01034 ug/L
Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached?Yes (1)No (0)
Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 , method #
Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L , method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)Mn - Manganese 01055 ug/L , method #
TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method #
For Remediation Systems Only (Attach Lab Reports):Influent Total VOCs:mg/L Effluent Total VOCs:mg/L VOC Removal%
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent)(Date)
Date sample analyzed:
If WELL
WAS
DRY at
time of
sampling,
check
here:
Mail original
and 1 copy to:
(Street)
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
SUBMIT FORM ON YELLOW PAPER ONLY
GW-59 Rev. 06-07-2018
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number:Expiration Date:
Facility Name:Non-Discharge UIC
Permit Name (if different):NPDES Other
Facility Address:TYPE OF PERMITTED OPERATION BEING MONITORED
County Lagoon
(City) (State) (Zip)Spray Field
Contact Person:Telephone#:Rotary Distributor
Well Location/Site Name:No. of wells to be sampled:Water Source Heat Pump
Remediation: Infiltration Gallery
Remediation:
Land Application of Sludge
Other:
(from Permit)
SAMPLING INFORMATION
WELL ID NUMBER (from Permit):Date sample collected:FIELD ANALYSES:
Well Depth:ft.Well Diameter:in.pH 00400: units Temp. 00010: oC
Depth to Water Level 82546: ft. below measuring point Screened Interval:ft.to ft.Spec. Cond. 00094:µMhos
Measuring Point is ft. above land surface Relative M.P. Elevation:ft.Odor 00085:
Volume of water pumped/bailed before sampling:gallons Appearance
Samples for metals were collected unfiltered:YES NO and field acidified:YES NO
LABORATORY INFORMATION
Laboratory Name:Certification No.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L
(Note: Use MPN method for highly turbid samples)Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L
pH (Lab) 00403 units Ba - Barium 01007 ug/L
TOC 00680 mg/L Ca - Calcium 00916 mg/L
Chloride 00940 mg/L Cd - Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium: Total 01034 ug/L
Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached?Yes (1)No (0)
Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 , method #
Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L , method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)Mn - Manganese 01055 ug/L , method #
TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method #
For Remediation Systems Only (Attach Lab Reports):Influent Total VOCs:mg/L Effluent Total VOCs:mg/L VOC Removal%
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent)(Date)
Date sample analyzed:
If WELL
WAS
DRY at
time of
sampling,
check
here:
Mail original
and 1 copy to:
(Street)
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617