NC0005274_Correspondence_20150309

NPDES DOCIMENT 5CANNIN` COVER SHEET
NPDES Permit:
NC0005274
Document Type:
Permit Issuance
Wasteload Allocation
Authorization to Construct (AtC)
Permit Modification
Complete File - Historical
Engineering
Alternatives (EAA)
Correspondence t
Instream Assessment (67b)
Speculative Limits
Environmental Assessment (EA)
Permit
History
Document Date:
March 9, 2015
This document its printed on reuse paper - ignore any
content on the reirerse wide

Templeton, Mike
From: Tom McKittrick [[e-mail]]
Sent: Monday, March 09, 2015 2:56 PM
To: Templeton, Mike; Steve Hart
Subject: RE: Proposed Lowell Storm Water Plan
Follow Up Flag:
Flag Status:
Follow up
Completed
Categories: .Keep/File
Thank you Mike, we will proceed as outlined below.
Regards,
To m
Tom McKittrick
President
Forsite Development, Inc.
5320 Old Pineville Road
Charlotte, NC 28217
[phone] Direct
[phone] Office
[phone] Fax
[e-mail]
www.forsiteinc.com
www.reventurepark.com
Forsite
is Download vCard
From: Templeton, Mike [mailto:[e-mail]]
Sent: Monday, March 09, 2015 2:33 PM
To: Tom McKittrick
Cc: Belnick, Tom; Bateson, James; Eckard, Sharon; Poupart, Jeff; Steve Hart; Shannon Doster; Bell, Wes
Subject: RE: Proposed Lowell Storm Water Plan
Hi, Tom -
I have reviewed your request and discussed it with Wes Bell of our Mooresville Regional Office. Because the transfer as
proposed will not result in a discharge to surface waters, you may proceed at your convenience. Please notify both Wes
and me within two weeks after the work is completed and provide an updated copy of your Table 1, Wastewater Tank
Volume Estimates.
You do not need to request permission for future transfers so long as there is no release from the tanks. But, again, you
should notify us when those transfers occur and provide an updated table of tank volumes.
Let me know if you have any further questions.
- Mike Templeton
1/2

Michael E. Templeton, P.E.
Wastewater Branch
Water Quality Permitting Section
NCDENR • DWR Raleigh, NC
Tel: [phone]
Fax: [phone]
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties.
Original Message
From: Tom McKittrick [mailto:tom(aforsiteinc.com]
Sent: Monday, February 16, 2015 3:34 PM
To: Templeton, Mike
Cc: Belnick, Tom; Bateson, James; Eckard, Sharon; Poupart, Jeff; Steve Hart
Subject: Proposed Lowell Storm Water Plan
Hello Mike (et all)
Please find a letter regarding the storm water that has accumulated in various tanks at the
former Crompton & Knowles plant in Lowell, NC. The letter outlines our plans to move the
water from Tank 1 into another tank so that it does not discharge through a hole cut in Tank
1 by the previous owner.
We continue to work through the process with DENR to secure a BFA on the site and hopefully
sell the property to Gaston County for the expansion of a park that is contiguous to the
property.
Thanks in advance and please do not hesitate to call me if you would like to discuss further.
Tks
Tom
Tom McKittrick
President
Forsite Development, Inc.
5320 Old Pineville Road
Charlotte, NC 28217
[phone] Direct
[phone] Office
[phone] Fax
[e-mail]
www.forsiteinc.com
www.reventurepark.com
Original Message
From: [e-mail] [mailto:[e-mail]]
Sent: Monday, February 16, 2015 3:05 PM
To: Tom McKittrick; Shannon Doster
Subject:
TASKalfa 400ci
[00:c0:ee:4c:03:bd]
2/2

Templeton, Mike
From: Templeton, Mike
Sent: Monday, March 09, 2015 2:33 PM
To: Tom McKittrick
Cc: Belnick, Tom; Bateson, James; Eckard, Sharon; Poupart, Jeff; Steve Hart; [e-mail]; Bell,
Wes
Subject: RE: Proposed Lowell Storm Water Plan
Follow Up Flag:
Flag Status:
Follow up
Completed
Hi, Tom -
I have reviewed your request and discussed it with Wes Bell of our Mooresville Regional Office. Because the transfer as
proposed will not result in a discharge to surface waters, you may proceed at your convenience. Please notify both Wes
and me within two weeks after the work is completed and provide an updated copy of your Table 1, Wastewater Tank
Volume Estimates.
You do not need to request permission for future transfers so long as there is no release from the tanks. But, again, you
should notify us when those transfers occur and provide an updated table of tank volumes.
Let me know if you have any further questions.
- Mike Templeton
Michael E. Templeton, P.E.
Wastewater Branch
Water Quality Permitting Section
NCDENR • DWR Raleigh, NC
Tel: [phone]
Fax: [phone]
E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties.
Original Message
From: Tom McKittrick [mailto:tom(aforsiteinc.com]
Sent: Monday, February 16, 2015 3:34 PM
To: Templeton, Mike
Cc: Belnick, Tom; Bateson, James; Eckard, Sharon; Poupart, Jeff; Steve Hart
Subject: Proposed Lowell Storm Water Plan
Hello Mike (et all)
Please find a letter regarding the storm water that has accumulated in various tanks at the
former Crompton & Knowles plant in Lowell, NC. The letter outlines our plans to move the
water from Tank 1 into another tank so that it does not discharge through a hole cut in Tank
1 by the previous owner.
We continue to work through the process with DENR to secure a BFA on the site and hopefully
sell the property to Gaston County for the expansion of a park that is contiguous to the
property.
Thanks in advance and please do not hesitate to call me if you would like to discuss further.
Tks
Tom
1/2

Tom McKittrick
President
Forsite Development, Inc.
5320 Old Pineville Road
Charlotte, NC 28217
[phone] Direct
[phone] Office
[phone] Fax
[e-mail]
www.forsiteinc.com
www.reventurepark.com
Original Message
From: [e-mail] [mailto:[e-mail]]
Sent: Monday, February 16, 2015 3:05 PM
To: Tom McKittrick; Shannon Doster
Subject:
TASKalfa 400ci
[00:c0:ee:4c:03:bd]
2/2

AZPRISM
="7 LABORATORIES. INC.
Hart & Hickman (Charlotte)
Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Full -Service Analytical &
Environmental Solutions
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Project: IPP-001
Lab Submittal Date: 05/26/2010
Prism Work Order: 0060008
Case Narrative
06/16/2010
RECEIVEDIDENNDWR
Water Quality
Permitting Section
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the original laboratory report dated 6/15/10. (Client added Total
Chromium to Sludgecomp-1.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services Reviewed By
Data Qualifiers Key Reference:
A Could not run at lesser dilution due to sample matrix. Sample was analyzed as a waste dilution.
Aa Surrogate diluted out.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 1 of 40

/PRISM
e�"= =':rA°t- eoru*oRIE$ ING
Full -Service Analytical &
Environmental Solutions
Sample Receipt Summary
06/16/2010
Prism Work Order: 0060008
Client Sample ID
Lab Sample ID Matrix Date Sampled Date Received
SCSS-1 0060008-01 Solid 05/26/10 05/26/10
ETSS-1 0060008-02 Solid 05/26/10 05/26/10
ETSS-2 0060008-03 Solid 05/26/10 05/26/10
ETSS-3 0060008-04 Solid 05/26/10 05/26/10
PCSS-1 0060008-05 Solid 05/26/10 05/26/10
PCSS-2 0060008-06 Solid 05/26/10 05/26/10
ATSS-1 0060008-07 Solid 05/26/10 05/26/10
Sludgecomp-1 0060008-08 Solid 05/26/10 05/26/10
Sludgecomp-1 (TCLP List 8260/8270) 0060008-09 Solid 05/26/10 05/26/10
Samples received in good condition at 5.7 degrees C unless otherwise noted.
RECEIVEDIDENR/DWR
FEB 23 20 i5
Water Quality
Permitting Section
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 40

/.--PR
LABOMTOMES. LNG
Full -Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: I P P-001
Sample Matrix: Solid
Laboratory Report
06/16/2010
Client Sample ID: SCSS-1
Prism Sample ID: 0060008-01
Prism Work Order: 0060008
Time Collected: 05/26/10 13:15
Time Submitted: 05/26/10 15:20
Parameter
Result
Units Report
Limit
MDL Dilution Method Analysis Analyst
Factor Date/Time
Batch
ID
General Chemistry Parameters
Solids
Microbiological Parameters
6.59
% by
Weight
0.100 0.100 1 '5M2540 G 6/3/10 14:60
KCP
P0F0096
Fecal Coliforms
BRL
CFU/g dry 15000 100 'SM9222 D 5/27/10 12:38 KCP POF0060
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 40

Full -Service Analytical 8
Environmental Solutions
Laboratory Report
06/16/2010
® uponAromas. INC
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: IPP-001
Sample Matrix: Solid
Client Sample ID: ETSS-1
Prism Sample ID: 0060008-02
Prism Work Order: 0060008
Time Collected: 05/26/10 09:45
Time Submitted: 05/26/10 15:20
Parameter
Result
Units Report
Limit
MDL Dilution
Factor
Method Analysis Analyst Batch
Date/Time ID
General Chemistry Parameters
% Solids
Microbiological Parameters
25.0
% by
Weight
0.100 0.100 1 'SM2540 G 6/3/10 14:60 KCP POF0095
Fecal Coliforms
BRL
CFU/g dry 4000 100 'SM9222 D 5/27/10 12:38 KCP POF0060
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc,
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 40

RISM PI
Full -Service Analytical &
EnvivironmentalalSolutions
Laboratory Report
06/16/2010
�. LABORATORIES INC.
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: IPP-001
Sample Matrix: Solid
Client Sample ID: ETSS-2
Prism Sample ID: 0060008-03
Prism Work Order: 0060008
Time Collected: 05/26/10 09:55
Time Submitted: 05/26/10 15:20
Parameter
Result
Units Report
Limit
MDL Dilution Method Analysis Analyst
Factor Date/Time
Batch
ID
General Chemistry Parameters
% Solids
Microbiological Parameters
27.0
% by
Weight
0.100 0.100 1 "SM2540 G 6/3/10 14:50 KCP P0F0095
Fecal Coliforms
BRL
CFU/g dry 3700 100 'SM9222 D 5/27/10 12:38 KCP POF0060
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 5 of 40

Full -Service Analytical &
Environmental Solutions
Laboratory Report
06/16/2010
�. LABORATORIES IHG
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: IPP-001
Sample Matrix: Solid
Client Sample ID: ETSS-3
Prism Sample ID: 0060008-04
Prism Work Order: 0060008
Time Collected: 05/26/10 10:05
Time Submitted: 05/26/10 15:20
Parameter
Result
Units Report
Limit
MDL Dilution
Factor
Method Analysis Analyst Batch
Date/Time ID
General Chemistry Parameters
% Solids
Microbiological Parameters
23.1
by
Weight
0.100 0.100 1 'SM2540 G 6/3/10 14:50 KCP P0F0095
Fecal Coliforms
BRL
CFU/g dry 4300 100 'SM9222 D 5/27/10 12:38 KCP POF0060
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Spring brook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 6 of 40

/PRISM
LABORATORIES INC
Full -Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: IPP-001
Sample Matrix: Solid
Laboratory Report
06/16/2010
Client Sample ID: PCSS-1
Prism Sample ID: 0060008-05
Prism Work Order: 0060008
Time Collected: 05/26/10 11:05
Time Submitted: 05/26/10 15:20
Parameter
Result
Units Report
Limit
MDL Dilution Method Analysis Analyst
Factor Date/Time
Batch
ID
General Chemistry Parameters
% Solids
Microbiological Parameters
7.60
by
Weight
0.100 0.100 1 'SM2540 G 6/3/10 14:50 KCP P0F0095
Fecal Coliforms
BRL
CFU/g dry 13000 100 'SM9222 D 5/27/10 12:38 KCP POF0060
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 40

Full-Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: I P P-001
Sample Matrix: Solid
Laboratory Report
06/16/2010
Client Sample ID: PCSS-2
Prism Sample ID: 0060008-06
Prism Work Order: 0060008
Time Collected: 05/26/10 11:15
Time Submitted: 05/26/10 15:20
Parameter
Result
Units Report
Limit
MDL Dilution Method Analysis Analyst
Factor Date/Time
Batch
ID
General Chemistry Parameters
Solids
Microbiological Parameters
7.29
% by
Weight
0.100 0.100 1 "SM2540 G 6/3/10 14:50 KCP P0F0095
Fecal Coliforms
BRL
CFU/g dry 14000 100 "SM9222 D 5/27/10 12:38 KCP POF0060
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 8 of 40

/PRISMLAR
Full-Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: IPP-001
Sample Matrix: Solid
Laboratory Report
06/16/2010
Client Sample ID: ATSS-1
Prism Sample ID: 0060008-07
Prism Work Order: 0060008
Time Collected: 05/26/10 12:00
Time Submitted: 05/26/10 15:20
Parameter
Result
Units Report
Limit
MDL Dilution Method Analysis Analyst
Factor Date/me
Batch
ID
General Chemistry Parameters
% Solids
Microbiological Parameters
12.0
by
Weight
0.100 0.100 1 'SM2540 G 6/3/10 14:50 KCP P0F0095
Fecal Coliforms
BRL
CFU/g dry 8300 100 'SM9222 D 5/27/10 12:38 KCP P0F0060
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 9 of 40

/PRISM
iaeonnTOME ING
Full -Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: I P P-001
Sample Matrix: Solid
Laboratory Report
06/16/2010
Client Sample ID: Sludgecomp-1
Prism Sample ID: 0060008-08
Prism Work Order: 0060008
Time Collected: 05/26/10 13:45
Time Submitted: 05/26/10 15:20
Parameter
Result
Units Report MDL
Limit
Dilution
Factor
Method Analysis Analyst Batch
Datefrime ID
General Chemistry Parameters
% Solids
Corrosivity-pH
Nitrate/Nitrite as N
pH
Total Kjeldahl Nitrogen
Ammonia as N
14.1 % by 0.100 0.100 1 "SM2540 G 6/2/10 18:00 PJF P0F0067
Weight
6.7 pH Units 1 "9045D 6/3/10 11:24 AGS P0F0078
72 mg/kg dry 35 3.9 1 "SM4500-NO3 F 6/2/10 10:15 KBC POF0108
6.7 pH Units 1 '9045D 613/10 11:16 AGS P0F0076
49000 mg/kg dry 35000 1500 20 '351.2 6/8/10 13:03 CDE POF0180
290 mg/kg 2.5 0.31 1 'SM4500-NH3 H 6/4/10 9:43 KCP P0F0134
Semivolatile Organic Compounds by GC/MS
A
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2,4, 5-Trichlorophenal
2, 4, 6-Trich lorop h eno l
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophencl
2-Methylnaphthalene
2-Methylphenol
2-Nitroaniline
2-Nitrophenol
3, 3'-Dichlorobenzidi ne
3/4-Methylphenol
3-Nitroaniline
4, 6-D i n itro-2-methy l p h en oI
4-Bromophenyl phenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenyl phenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Azobenzene
Benzo(a)anthracene
Benzo(a)pyrene
BRL ug/kg dry 1200000 300000 1
BRL ug/kg dry 1200000 270000 1
BRL ug/kg dry 1200000 270000 1
BRL ug/kg dry 1200000 260000 1
BRL ug/kg dry 1200000 260000 1
BRL ug/kg dry 1200000 280000 1
BRL ug/kg dry 1200000 300000 1
BRL ug/kg dry 1200000 300000 1
BRL ug/kg dry 1200000 180000 1
BRL ug/kg dry 1200000 280000 1
BRL ug/kg dry 1200000 240000 1
BRL ug/kg dry 1200000 280000 1
BRL ug/kg dry 1200000 320000 1
BRL ug/kg dry 1200000 360000 1
BRL ug/kg dry 1200000 290000 1
BRL ug/kg dry 1200000 210000 1
BRL ug/kg dry 1200000 270000 1
BRL ug/kg dry 1200000 290000 1
BRL ug/kg dry 1200000 300000 1
BRL ug/kg dry 1200000 220000 1
BRL ug/kg dry 1200000 190000 1
BRL ug/kg dry 1200000 260000 1
BRL ug/kg dry 1200000 270000 1
BRL ug/kg dry 1200000 240000 1
BRL ug/kg dry 1200000 230000 1
BRL ug/kg dry 1200000 160000 1
BRL ug/kg dry 1200000 160000 1
BRL ug/kg dry 1200000 250000 1
BRL ug/kg dry 1200000 270000 1
BRL ug/kg dry 1200000 240000 1
BRL ug/kg dry 1200000 270000 1
BRL ug/kg dry 1200000 260000 1
BRL ug/kg dry 1200000 290000 1
BRL ug/kg dry 1200000 160000 1
'8270D
'8270D
*8270D
'8270D
"8270D
*8270D
'8270D
'8270D
*8270D
'8270D
'8270D
'8270D
'8270D
*8270D
"8270D
"8270D
*8270D
"8270D
"8270D
*8270D
*8270D
*8270D
'82700
'8270D
'8270D
'8270D
'8270D
*8270D
'8270D
"8270D
"8270D
'8270D
'8270D
'8270D
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
6/2/10 21:40 CGP POF0141
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 10 of 40

PRISM
LABORATORIES. INC.
Full -Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: I P P-001
Sample Matrix: Solid
Laboratory Report
06/16/2010
Client Sample ID: Sludgecomp-1
Prism Sample ID: 0060008-08
Prism Work Order: 0060008
Time Collected: 05/26/10 13:45
Time Submitted: 05/26/10 15:20
Parameter
Result
Units Report
Limit
MDL Dilution Method Analysis Analyst Batch
Factor Date/Time ID
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
b is(2-C h loroethoxy) meth a ne
Bis(2-Chloroethyl)ether
Bis(2-chloroisopropyl)ether
B is(2-Ethy lh exyl) phtha l ate
Butyl benzyl phthalate
Chrysene
Dibenzo(a,h)anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
H e x a ch to ro cy clo pe n t a d i e n e
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
N-N itroso-di-n-propylamine
N-N itrosod iphenyla mine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL uglkg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
BRL ug/kg dry 1200000
240000
210000
320000
300000
290000
310000
320000
310000
380000
350000
260000
270000
250000
290000
270000
390000
390000
310000
260000
260000
300000
230000
280000
300000
270000
310000
300000
260000
290000
320000
260000
320000
280000
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'82700
'8270D
"8270D
'8270D
'8270D
'8270D
'8270D
'8270D
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
POF0141
Surrogate
Recovery
Control Limits
2, 4,6-Tribrom op h en of
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d14
TCLP Extraction by EPA 1311
75 %
83 %
91 %
85 %
79 %
92 %
34-134
17-122
13-108
11-118
23-109
41-156
TCLP Extraction
TCLP Metals
Complete
N/A
1 "1311 6/3/10 8:05 JAB P0F0065
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 11 of 40

/PRISM
IAeoRAr DRIES Inc
Full -Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: IPP-001
Sample Matrix: Solid
Laboratory Report
06/16/2010
Client Sample ID: Sludgecomp-1
Prism Sample ID: 0060008-08
Prism Work Order: 0060008
Time Collected: 05/26/10 13:45
Time Submitted: 05/26/10 15:20
Parameter
Result
Units
Report
Limit
MDL Dilution
Factor
Method Analysis Analyst Batch
Date/Time ID
Mercury
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Total Metals
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
mg/L
mg/L
mglL
mg/L
mg/L
mg/L
mg/L
mg/L
0.010
0.050
5.0
0.025
0.25
0.050
0.10
0.25
0.0000084
0.0096
0.0032
0.00075
0.0026
0.0028
0.014
0.0018
'7470A
'6010C
'6010C
'6010C
'6010C
'6010C
'6010C
'6010C
6/4/10
6/9/10
6/9/10
6/9/10
6/9/10
6/9/10
6/9/10
6/9/10
10:35
3:47
3:47
3:47
3:47
3:47
3:47
3:47
RWF
DJS
DJS
DJS
DJS
DJS
DJS
DJS
P0F0086
POF0100
POF0100
POF0100
POF0100
POF0100
POF0100
POF0100
Mercury
Arsenic
Cadmium
Chromium
Copper
Lead
Molybdenum
Nickel
Selenium
Zinc
Volatile Organic Compounds by GC/MS
BRL
BRL
BRL
990
2400
12
BRL
19
BRL
110
mg/kg dry
mg/kg dry
mg/kg dry
mg/kg dry
mg/kg dry
mg/kg dry
mg/kg dry
mg/kg dry
mg/kg dry
mg/kg dry
0.14
3.5
1.7
17
35
1.7
3.5
6.9
3.5
17
0.0097 1
0.39 1
0.18 1
2.4 10
15 10
0.43 1
0.26 1
2.1 1
0.70 1
1.8 1
'7471B
'6010C
'6010C
'6010C
'6010C
'6010C
'6010C
*6010C
'6010C
"6010C
6/10/10 14:06 KCP
6/8/10 2:01 DJS
6/8/10 2:01 DJS
6/8/10 23:39 DJS
6/8/10 23:39 DJS
6/8/10 2:01 DJS
6/8/10 2:01 DJS
6/8/10 2:01 DJS
6/8/10 2:01 DJS
6/8/10 2:01 DJS
P0F0255
P0F0101
POF0101
POF0101
POF0101
POF0101
POF0101
POF0101
P0F0101
POF0101
A
1,1,1, 2-Tetrachloroethane
1,1,1-Trichloroethane
1,1, 2, 2-Tetrachloroethane
1,1, 2-Trichloroethane
1,1-Dichloroethane
1,1-Dich loroethylene
1,1-Dichloropropylene
1,2, 3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3, 5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chloroethyl Vinyl Ether
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BR L
BR L
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
820000 110000 10000
820000 300000 10000
820000 230000 10000
820000 110000 10000
820000 200000 10000
820000 350000 10000
820000 310000 10000
1600000 120000 10000
820000 95000 10000
1600000 140000 10000
820000 200000 10000
1600000 200000 10000
820000 76000 10000
820000 180000 10000
820000 120000 10000
820000 140000 10000
820000 270000 10000
820000 170000 10000
820000 92000 10000
820000 140000 10000
820000 320000 10000
820000 120000 10000
'8260B
'8260B
'8260B
'82608
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'82608
'8260B
'8260B
'8260B
'8260B
'8260B
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
6/8/10 22:46 KLA P0F0231
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 12 of 40

�] MI
I l I S n Full -Service al Solutions
s
r ' V' Environmental Solutions
LABORATORIES IRO
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: IPP-001
Sample Matrix: Solid
Laboratory Report
06/16/2010
Client Sample ID: Sludgecomp-1
Prism Sample ID: 0060008-08
Prism Work Order: 0060008
Time Collected: 05/26/10 13:45
Time Submitted: 05/26/10 15:20
Parameter
Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
2-Chlorotoluene
4-Chlorotoluene
4-Isopropyltoluene
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethylene
cis-1, 3-Dich loropropylene
Dibromochloromethane
Dibromomethane
D i ch t o ro d i fl u o ro m et h a n e
Ethylbenzene
Hexachlorobutadiene
Isopropyl Ether
lsopropylbenzene (Cumene)
m,p-Xylenes
Methyl Butyl Ketone (2-Hexanone)
Methyl Ethyl Ketone (2-Butanone)
Methyl Isobutyl Ketone
Methylene Chloride
Methyl-tert-Butyl Ether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethylene
Toluene
trans-1, 2-Dichloroethylene
trans-1, 3-Dichloropropylene
Trichloroethylene
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BR L
BRL
BRL
BRL
BRL
BR L
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
uglkg dry
uglkg dry
uglkg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
ug/kg dry
820000
820000
820000
3300000
820000
820000
820000
820000
820000
1600000
820000
820000
820000
1600000
820000
1600000
820000
820000
820000
820000
1600000
820000
1600000
820000
820000
1600000
3300000
3300000
3300000
820000
820000
1600000
820000
820000
820000
820000
820000
820000
820000
820000
820000
820000
820000
220000
170000
310000
120000
200000
160000
100000
150000
120000
430000
230000
210000
140000
300000
190000
230000
220000
150000
96000
98000
460000
210000
420000
170000
240000
410000
120000
210000
120000
180000
89000
120000
280000
240000
180000
320000
130000
260000
250000
230000
250000
110000
230000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
10000
'8260B
'8260B
'8260B
'8260B
*8260B
'8260B
'8260B
*8260B
'8260B
'82608
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
'8260B
*8260B
'8260B
'82608
*8260B
'8260B
'8260B
'8260B
'8260B
*8260B
'8260B
'8260B
'8260B
'8260B
*8260B
'8260B
'8260B
'8260B
'8260B
'82608
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
618/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
6/8/10 22:46
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
KLA
POF0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
P0F0231
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 13 of 40

PRISM
LABORATORIES INC
Full -Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: IPP-001
Sample Matrix: Solid
Laboratory Report
06/16/2010
Client Sample ID: Sludgecomp-1
Prism Sample ID: 0060008-08
Prism Work Order: 0060008
Time Collected: 05/26/10 13:45
Time Submitted: 05/26/10 15:20
Parameter
Result
Units Report
Limit
MDL Dilution Method Analysis Analyst
Factor Date/Time
Batch
ID
Trichlorofluoromethane
Vinyl chloride
BRL
BRL
ug/kg dry
ug/kg dry
1600000 500000 10000 `8260B 6/8/10 22:46
1600000 350000 10000 '8260B 6/8/10 22:46
KLA P0F0231
KLA P0F0231
Surrogate Recovery
Control Limits
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-d8
0%
0%
0%
70-130
70-130
70-130
Aa
Aa
Aa
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 14 of 40

PRISM
ueORATonIEs INC
Full -Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: I P P-001
Sample Matrix: Solid
Laboratory Report
06/16/2010
Client Sample ID: Sludgecomp-1 (TCLP List
Prism Sample ID: 0060008-09
Prism Work Order: 0060008
Time Collected: 05/26/10 13:45
Time Submitted: 05/26/10 15:20
Parameter
Result
Units Report
Limit
MDL Dilution Method Analysis Analyst
Factor Daterfine
Batch
ID
Semivolatile Organic Compounds by GC/MS
1,2-Dichlorobenzene
2,4, 5-Trichlorophenol
2,4,6-Trichlorophenal
2,4-Dinitrotoluene
2-Methylphenol
3/4-Methylphenol
Hexachlorobenzene
Hexachlorobutadiene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ug/kg wet
ug/kg wet
ug/kg wet
ug/kg wet
ug/kg wet
ug/kg wet
ug/kg wet
ug/kg wet
ug/kg wet
ug/kg wet
uglkg wet
ug/kg wet
160000
160000
160000
160000
160000
160000
160000
160000
160000
160000
160000
160000
37000
36000
39000
39000
41000
41000
36000
41000
38000
41000
44000
14000
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'8270D
'82700
612/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
6/2/10 21:40
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
CGP
A
POF0201
POF0201
POF0201
POF0201
POF0201
POF0201
POF0201
POF0201
POF0201
POF0201
POF0201
POF0201
Surrogate
Recovery
Control Limits
2,4,6-Tri bromoph enol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
Terphenyl-d14
Volatile Organic Compounds by GC/MS
75 %
83 %
91 %
85 %
79 %
92 %
34-134
17-122
13-108
11-118
23-109
41-156
A
1,1-Dichloroethylene
1,2-Dibromo-3-chloropropane
1,2-Dichloroethane
1,4-Dichlorobenzene
Benzene
Carbon Tetrachloride
Chlorobenzene
Chloroform
Ethylbenzene
m,p-Xylenes
Methyl Ethyl Ketone (2-Butanone)
o-Xylene
Tetrachloroethylene
Toluene
Trichloroethylene
Vinyl chloride
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
ug/kg wet 120000 49000 10000 '8260B 6/8/10 22:46 KLA
ug/kg wet 230000 28000 10000 *8260B 6/8/10 22:46 KLA
ug/kg wet 120000 17000 10000 '8260B 6/8/10 22:46 KLA
ug/kg wet 120000 20000 10000 `8260B 6/8/10 22:46 KLA
ug/kg wet 120000 28000 10000 `8260B 6/8/10 22:46 KLA
ug/kg wet 120000 30000 10000 '8260B 6/8/10 22:46 KLA
ug/kg wet 120000 19000 10000 `826013 6/8/10 22:46 KLA
ug/kg wet 120000 27000 10000 `8260B 6/8/10 22:46 KLA
ug/kg wet 120000 29000 10000 `8260B 6/8/10 22:46 KLA
ug/kg wet 230000 58000 10000 '8260B 6/8/10 22:46 KLA
ug/kg wet 470000 29000 10000 *8260B 6/8/10 22:46 KLA
ug/kg wet 120000 25000 10000 '8260B 6/8/10 22:46 KLA
ug/kg wet 120000 35000 10000 *8260B 6/8/10 22:46 KLA
ug/kg wet 120000 32000 10000 '8260B 6/8/10 22:46 KLA
ug/kg wet 120000 33000 10000 '82608 6/8/10 22:46 KLA
ug/kg wet 230000 49000 10000 '8260B 6/8/10 22:46 KLA
P0F0267
P0F0267
POF0267
P0F0267
POF0267
P0F0267
P0F0267
P0F0267
P0F0267
P0F0267
P0F0267
P0F0267
POF0267
P0F0267
P0F0267
P0F0267
Surrogate
Recovery
Control Limits
4-B ro mof l u orobenzen e
Dibromofluoromethane
Toluene-d8
0%
0%
0%
70-130
70-130
70-130
Aa
Aa
Aa
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 15 of 40

/PRISM
n
Full-Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Level II QC Report
6/16/10
Project: IPP-001 Prism Work Order: 0060008
Time Submitted: 5/26/10 3:20:OOPM
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P0F0231 - 5035
Blank (P0F0231-BLK1) Prepared & Analyzed: 06/08/10
1,1-Dichloroethylene BRL 250 ug/kg wet
1,2-Dibromoethane BRL 250 ug/kg wet
1,4-Dichlorobenzene BRL 250 ug/kg wet
Benzene BRL 250 ug/kg wet
Carbon Tetrachloride BRL 250 ug/kg wet
Chlorobenzene BRL 250 ug/kg wet
Chloroform BRL 250 ug/kg wet
Methyl Ethyl Ketone (2-Butanone) BRL 1000 ug/kg wet
Tetrachloroethylene BRL 250 ug/kg wet
Trichloroethylene BRL 250 ug/kg wet
Vinyl chloride BRL 500 ug/kg wet
Surrogate: 4-Bromofluorobenzene 2220 ug/kg wet 2500 89 70.130
Surrogate: Dibromotluoromethane 2360 ug/kg wet 2500 94 70-130
Surrogate: Toluene-d8 2170 ug/kg wet 2500 87 70-130
LCS (P0F0231-BS1) Prepared & Analyzed: 06/08/10
1,1-Dichloroethylene 2280 250 ug/kg wet 2500 91 70-130
Benzene 2340 250 ug/kg wet 2500 94 70-130
Chlorobenzene 2320 250 ug/kg wet 2500 93 70-130
Trichloroethylene 2330 250 ug/kg wet 2500 93 70-130
Surrogate: 4-Bromofluorobenzene 2040 ug/kg wet 2500 81 70-130
Surrogate: Dibromotluoromethane 2220 ug/kg wet 2500 89 70-130
Surrogate: Toluene-d8 2080 ug/kg wet 2500 83 70-130
LCS Dup (P0F0231-BSD1) Prepared & Analyzed: 06/08/10
1,1-Dichloroethylene 2600 250 ug/kg wet 2500 104 70-130 13
Benzene 2620 250 ug/kg wet 2500 105 70-130 11
Chlorobenzene 2570 250 ug/kg wet 2500 103 70-130 10
Trichloroethylene 2630 250 ug/kg wet 2500 105 70-130 12
Surrogate: 4-Bromofluorobenzene 2220 ug/kg wet 2500 89 70-130
Surrogate: Dibromofluoromethane 2420 ug/kg wet 2500 97 70-130
Surrogate: Toluene-d8 2340 ug/kg wet 2500 94 70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 16 of 40

/PRISM
---- ueonArome5 we
Full -Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Level II QC Report
6/16/10
Project: IPP-001 Prism Work Order: 0060008
Time Submitted: 5/26/10 3:20:OOPM
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P0F0267 - 5035
Blank (P0F0267-BLK1) Prepared & Analyzed: 06/08/10
1,1-Dichloroethylene BRL 250 ug/kg wet
1,2-Dibromoethane BRL 250 ug/kg wet
1,4-Dichlorobenzene BRL 250 ug/kg wet
Benzene BRL 250 ug/kg wet
Carbon Tetrachloride BRL 250 ug/kg wet
Chlorobenzene BRL 250 ug/kg wet
Chloroform BRL 250 ug/kg wet
Methyl Ethyl Ketone (2-Butanone) BRL 1000 ug/kg wet
Tetrachloroethylene BRL 250 ug/kg wet
Trichloroethylene BRL 250 ug/kg wet
Vinyl chloride BRL 500 ug/kg wet
Surrogate: 4-Bromofluorobenzene 2220 ug/kg wet 2500 89 70-130
Surrogate: Dibromofluoromethane 2360 ug/kg wet 2500 94 70-130
Surrogate: Toluene-d8 2170 ug/kg wet 2500 87 70-130
LCS (P0F0267-BS1) Prepared & Analyzed: 06/08/10
1,1-Dichloroethylene 2280 250 ug/kg wet 2500 91 70-130
Benzene 2340 250 ug/kg wet 2500 94 70-130
Chlorobenzene 2320 250 ug/kg wet 2500 93 70-130
Trichloroethylene 2330 250 ug/kg wet 2500 93 70-130
Surrogate: 4-Bromofluorobenzene 2040 ug/kg wet 2500 81 70-130
Surrogate: Dibromofluoromethane 2220 ug/kg wet 2500 89 70-130
Surrogate: Toluene-d8 2080 ug/kg wet 2500 83 70-130
LCS Dup (P0F0267-BSD1) Prepared & Analyzed: 06/08/10
1,1-Dichloroethylene 2600 250 ug/kg wet 2500 104 70-130 13
Benzene 2620 250 ug/kg wet 2500 105 70-130 11
Chlorobenzene 2570 250 ug/kg wet 2500 103 70-130 10
Trichloroethylene 2630 250 ug/kg wet 2500 105 70-130 12
Surrogate: 4-Bromofluorobenzene 2220 ug/kg wet 2500 89 70-130
Surrogate: Dibromolluoromethane 2420 ug/kg wet 2500 97 70-130
Surrogate: Toluene-d8 2340 ug/kg wet 2500 94 70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 17 of 40

PRISM
Full -Service Analytical 8
Environmental Solutions
Level II QC Report
6/16/10
unonnroalFS. Inc
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: IPP-001 Prism Work Order: 0060008
Time Submitted: 5/26/10 3:20:OOPM
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POF0141 - 3580A
Blank (P0F0141-BLK1) Prepared & Analyzed: 06/02/10
1,2,4-Trichlorobenzene BRL 200000 ug/kg wet
1,2-Dichlorobenzene BRL 200000 ug/kg wet
1,3-Dichlorobenzene BRL 200000 ug/kg wet
1,4-Dichlorobenzene BRL 200000 ug/kg wet
2,4,5-Trichlorophenol BRL 200000 ug/kg wet
2,4,6-Trichlorophenol BRL 200000 ug/kg wet
2,4-Dichlorophenol BRL 200000 ug/kg wet
2,4-Dimethylphenol BRL 200000 ug/kg wet
2,4-Dinitrophenol BRL 200000 ug/kg wet
2,4-Dinitrotoluene BRL 200000 ug/kg wet
2,6-Dinitrotoluene BRL 200000 ug/kg wet
2-Chloronaphthalene BRL 200000 ug/kg wet
2-Chlorophenol BRL 200000 ug/kg wet
2-Methylnaphthalene BRL 200000 ug/kg wet
2-Methylphenol BRL 200000 ug/kg wet
2-Nitroaniline BRL 200000 ug/kg wet
2-Nitrophenol BRL 200000 ug/kg wet
3,3'-Dichlorobenzidine BRL 200000 ug/kg wet
3/4-Methylphenol BRL 200000 ug/kg wet
3-Nitroaniline BRL 200000 ug/kg wet
4,6-Dinitro-2-methylphenol BRL 200000 ug/kg wet
4-Bromophenyl phenyl ether BRL 200000 ug/kg wet
4-Chloro-3-methylphenol BRL 200000 ug/kg wet
4-Chloroaniline BRL 200000 uglkg wet
4-Chlorophenyl phenyl ether BRL 200000 ug/kg wet
4-Nitroaniline BRL 200000 ug/kg wet
4-Nitrophenol BRL 200000 ug/kg wet
Acenaphthene BRL 200000 ug/kg wet
Acenaphthylene BRL 200000 ug/kg wet
Aniline BRL 200000 ug/kg wet
Anthracene BRL 200000 uglkg wet
Azobenzene BRL 200000 uglkg wet
Benzo(a)anthracene BRL 200000 uglkg wet
Benzo(a)pyrene BRL 200000 ug/kg wet
Benzo(b)fluoranthene BRL 200000 ug/kg wet
Benzo(g,h,i)perylene BRL 200000 ug/kg wet
Benzo(k)fluoranthene BRL 200000 ug/kg wet
Benzoic Acid BRL 200000 uglkg wet
Benzyl alcohol BRL 200000 uglkg wet
bis(2-Chloroethoxy)methane BRL 200000 ug/kg wet
Bis(2-Chloroethyl)ether BRL 200000 ug/kg wet
Bis(2-chloroisopropyl)ether BRL 200000 ug/kg wet
Bis(2-Ethylhexyl)phthalate BRL 200000 ug/kg wet
Butyl benzyl phthalate BRL 200000 ug/kg wet
Chrysene BRL 200000 ug/kg wet
Dibenzo(a,h)anthracene BRL 200000 ug/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 18 of 40

/.411.1.1:1129A1300.ATORIES. I S M Full -Service vironmen Analytical
Environmental Solutions
INC.
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Level II QC Report
6/16/10
Project: IPP-001 Prism Work Order: 0060008
Time Submitted: 5/26/10 3:20:OOPM
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POF0141 - 3580A
Blank (P0F0141-BLK1) Prepared & Analyzed: 06/02/10
Dibenzofuran BRL 200000 ug/kg wet
Diethyl phthalate BRL 200000 ug/kg wet
Dimethyl phthalate BRL 200000 ug/kg wet
Di-n-butyl phthalate BRL 200000 ug/kg wet
Di-n-octyl phthalate BRL 200000 ug/kg wet
Fluoranthene BRL 200000 ug/kg wet
Fluorene BRL 200000 ug/kg wet
Hexachlorobenzene BRL 200000 ug/kg wet
Hexachlorobutadiene BRL 200000 ug/kg wet
Hexachlorocyclopentadiene BRL 200000 ug/kg wet
Hexachloroethane BRL 200000 ug/kg wet
Indeno(1,2,3-cd)pyrene BRL 200000 ug/kg wet
Isophorone BRL 200000 ug/kg wet
Naphthalene BRL 200000 ug/kg wet
Nitrobenzene BRL 200000 ug/kg wet
N-Nitroso-di-n-propylamine BRL 200000 ug/kg wet
N-Nitrosodiphenylamine BRL 200000 ug/kg wet
Pentachlorophenol BRL 200000 ug/kg wet
Phenanthrene BRL 200000 ug/kg wet
Phenol BRL 200000 ug/kg wet
Pyrene BRL 200000 ug/kg wet
Surrogate: 2,4,6-Tribromophenol 818000 ug/kg wet 1200000 68 34-134
Surrogate: 2-Fluorobipheny! 505000 ug/kg wet 600000 84 17-122
Surrogate: 2-Fluorophenol 1100000 ug/kg wet 1200000 91 13-108
Surrogate: Nitrobenzene-d5 513000 ug/kg wet 600000 86 11-118
Surrogate: Phenol-d5 1000000 ug/kg wet 1200000 84 23-109
Surrogate: Terphenyl-d14 561000 ug/kg wet 600000 93 41-156
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 19 of 40

/PRISMo
Full-Service Analytical &
Environmental Solutions
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Level II QC Report
6/16/10
Project: IPP-001 Prism Work Order: 0060008
Time Submitted: 5/26/10 3:20:OOPM
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POF0201 - 3580A
Blank (POF0201-BLK1) Prepared & Analyzed: 06/02/10
1,2,4-Trichlorobenzene BRL 200000 uglkg wet
1,2-Dichlorobenzene BRL 200000 ug/kg wet
1,3-Dichlorobenzene BRL 200000 ug/kg wet
1,4-Dichlorobenzene BRL 200000 ug/kg wet
2,4,5-Trichlorophenol BRL 200000 ug/kg wet
2,4,6-Trichlorophenol BRL 200000 ug/kg wet
2,4-Dichlorophenol BRL 200000 ug/kg wet
2,4-Dimethylphenol BRL 200000 ug/kg wet
2,4-Dinitrophenol BRL 200000 ug/kg wet
2,4-Dinitrotoluene BRL 200000 uglkg wet
2,6-Dinitrotoluene BRL 200000 ug/kg wet
2-Chloronaphthalene BRL 200000 ug/kg wet
2-Chlorophenol BRL 200000 ug/kg wet
2-Methylnaphthalene BRL 200000 uglkg wet
2-Methylphenol BRL 200000 ug/kg wet
2-Nitroaniline BRL 200000 ug/kg wet
2-Nitrophenol BRL 200000 ug/kg wet
3,3'-Dichlorobenzidine BRL 200000 ug/kg wet
3/4-Methylphenol BRL 200000 ug/kg wet
3-Nitroaniline BRL 200000 ug/kg wet
4,6-Dinitro-2-methylphenol BRL 200000 ug/kg wet
4-Bromophenyl phenyl ether BRL 200000 ug/kg wet
4-Chloro-3-methylphenol BRL 200000 uglkg wet
4-Chloroaniline BRL 200000 uglkg wet
4-Chlorophenyl phenyl ether BRL 200000 uglkg wet
4-Nitroaniline BRL 200000 ug/kg wet
4-Nitrophenol BRL 200000 uglkg wet
Acenaphthene BRL 200000 ug/kg wet
Acenaphthylene BRL 200000 ug/kg wet
Aniline BRL 200000 ug/kg wet
Anthracene BRL 200000 ug/kg wet
Azobenzene BRL 200000 ug/kg wet
Benzo(a)anthracene BRL 200000 ug/kg wet
Benzo(a)pyrene BRL 200000 ug/kg wet
Benzo(b)fluoranthene BRL 200000 ug/kg wet
Benzo(g,h,i)perylene BRL 200000 ug/kg wet
Benzo(k)fluoranthene BRL 200000 ug/kg wet
Benzoic Acid BRL 200000 ug/kg wet
Benzyl alcohol BRL 200000 ug/kg wet
bis(2-Chloroethoxy)methane BRL 200000 ug/kg wet
Bis(2-Chloroethyl)ether BRL 200000 ug/kg wet
Bis(2-chloroisopropyl)ether BRL 200000 ug/kg wet
Bis(2-Ethylhexyl)phthalate BRL 200000 ug/kg wet
Butyl benzyl phthalate BRL 200000 ug/kg wet
Chrysene BRL 200000 ug/kg wet
Dibenzo(a,h)anthracene BRL 200000 ug/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 20 of 40

ER I S MI
FullService Analytical &
Enivronmental Solutions
LABORATORIES, INC.
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Level II QC Report
6/16/10
Project: IPP-001 Prism Work Order: 0060008
Time Submitted: 5/26/10 3:20:OOPM
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POF0201 - 3580A
Blank (POF0201-BLK1) Prepared & Analyzed: 06/02/10
Dibenzofuran BRL 200000 ug/kg wet
Diethyl phthalate BRL 200000 ug/kg wet
Dimethyl phthalate BRL 200000 ug/kg wet
Di-n-butyl phthalate BRL 200000 ug/kg wet
Di-n-octyl phthalate BRL 200000 ug/kg wet
Fluoranthene BRL 200000 ug/kg wet
Fluorene BRL 200000 ug/kg wet
Hexachlorobenzene BRL 200000 ug/kg wet
Hexachlorobutadiene BRL 200000 ug/kg wet
Hexachlorocyclopentadiene BRL 200000 ug/kg wet
Hexachloroethane BRL 200000 ug/kg wet
Indeno(1,2,3-cd)pyrene BRL 200000 ug/kg wet
Isophorone BRL 200000 ug/kg wet
Naphthalene BRL 200000 ug/kg wet
Nitrobenzene BRL 200000 ug/kg wet
N-Nitroso-di-n-propylamine BRL 200000 ug/kg wet
N-Nitrosodiphenylamine BRL 200000 ug/kg wet
Pentachlorophenol BRL 200000 ug/kg wet
Phenanthrene BRL 200000 ug/kg wet
Phenol BRL 200000 ug/kg wet
Pyrene BRL 200000 ug/kg wet
Pyridine BRL 200000 ug/kg wet
Surrogate: 2,4,6-Tribromophenol 818000 ug/kg wet 1200000 68 34-134
Surrogate: 2-Fluorobiphenyl 505000 ug/kg wet 600000 84 17-122
Surrogate: 2-Fluorophenol 1100000 ug/kg wet 1200000 91 13-108
Surrogate: Nitrobenzene-d5 513000 ug/kg wet 600000 86 11-118
Surrogate: Phenol-d5 1000000 ug/kg wet 1200000 84 23-109
Surrogate: Terphenyl-d14 561000 ug/kg wet 600000 93 41-156
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 21 of 40

PRISM Full -Service Analytical
Environmental Solutions
IiIIMIMMEL LAnORATORIE$ INO
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Total Metals - Quality Control
Level II QC Report
6/16/10
Project: IPP-001 Prism Work Order: 0060008
Time Submitted: 5/26/10 3:20:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POF0101 - 3050B
Blank (P0F0101-BLK1) Prepared: 06/03/10 Analyzed: 06/08/10
Arsenic BRL 0.50 mg/kg wet
Cadmium BRL 0.25 mg/kg wet
Chromium BRL 0.25 mg/kg wet
Copper BRL 0.50 mg/kg wet
Lead BRL 0.25 mg/kg wet
Molybdenum BRL 0.50 mg/kg wet
Nickel BRL 1.0 mg/kg wet
Selenium BRL 0.50 mg/kg wet
Zinc BRL 2.5 mg/kg wet
LCS (POF0101-BS1) Prepared: 06/03/10 Analyzed: 06/08/10
Arsenic 25.2 0.50 mg/kg wet 25.0 101 80-120
Cadmium 24.6 0.25 mg/kg wet 25.0 98 80-120
Chromium 26.2 0.25 mg/kg wet 25.0 105 80-120
Copper 26.6 0.50 mg/kg wet 25.0 106 80-120
Lead 24.9 0.25 mg/kg wet 25.0 100 80-120
Molybdenum 27.5 0.50 mg/kg wet 25.0 110 80-120
Nickel 25.6 1.0 mg/kg wet 25.0 103 80-120
Selenium 24.4 0.50 mg/kg wet 25.0 98 80-120
Zinc 25.5 2.5 mg/kg wet 25.0 102 80-120
Batch P0F0255 - 7471B
Blank (P0F0255-BLK1) Prepared & Analyzed: 06/10/10
Mercury
BRL 0.020 mg/kg wet
LCS (P0F0255-BS1) Prepared & Analyzed: 06/10/10
Mercury
0.421 0.020 mg/kg wet 0.417 101 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 22 of 40

IERISM
-ti LABORATORIES INC
Full -Service Analytical 8
Environmental Solutions
Level II QC Report
6/16/10
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
TCLP Metals - Quality Control
Project: IPP-001 Prism Work Order: 0060008
Time Submitted: 5/26/10 3:20:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P0F0086 - 7470A
Blank (P0F0086-BLK1) Prepared: 06/03/10 Analyzed: 06/04/10
Mercury BRL 0.010 mg/L
LCS (P0F0086-BS1)
Prepared: 06/03/10 Analyzed: 06/04/10
Mercury 0.00865 0.010 mg/L 0.00938 92 80-120
Batch POF0100 - 3010A
Blank (P0F0100-BLK1) Prepared: 06/03/10 Analyzed: 06/09/10
Arsenic BRL 0.050 mg/L
Barium BRL 5.0 mg/L
Cadmium BRL 0.025 mg/L
Chromium BRL 0.25 mg/L
Lead BRL 0.050 mg/L
Selenium BRL 0.10 mg/L
Silver BRL 0.25 mg/L
LCS (P0F0100-BS1) Prepared: 06/03/10 Analyzed: 06/09/10
Arsenic 1.20 0.050 mg/L 1.25 96 80-120
Barium 1.27 5.0 mg/L 1.25 102 80-120
Cadmium 1.23 0.025 mg/L 1.25 98 80-120
Chromium 1.26 0.25 mg/L 1.25 101 80-120
Lead 1.25 0.050 mglL 1.25 100 80-120
Selenium 1.18 0.10 mglL 1.25 95 80-120
Silver 1.22 0.25 mg/L 1.25 98 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
I Page 23 of 40 I

AlaRISM
ueoanraaies, iMc
Full•Service Analytical &
Environmental Solutions
Level II QC Report
6/16/10
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
General Chemistry Parameters - Quality Control
Analyte
Project: IPP-001 Prism Work Order: 0060008
Time Submitted: 5/26/10 3:20:OOPM
Result
Reporting Spike Source %REC RPD
Limit Units Level Result %REC Limits RPD Limit Notes
Batch P0F0076 - NO PREP
LCS (P0F0076-BS1)
Prepared & Analyzed: 06/03/10
pH
Duplicate (P0F0076-DUP1)
6.86 pH Units 6.86 100 99-101
Source: 0060008-08 Prepared & Analyzed: 06/03/10
pH
Batch P0F0078 - NO PREP
6.72 pH Units 6.68 0.6 20
LCS (P0F0078-BS1)
Prepared & Analyzed: 06/03/10
Corrosivity-pH
Duplicate (P0F0078-DUP1)
0.00 pH Units 99-101
Source: 0060008-08 Prepared & Analyzed: 06/03/10
Corrosivity-pH
Batch POF0108 - NO PREP
0.00 pH Units 6.68
10
Blank (POF0108-BLK1)
Prepared & Analyzed: 06/02/10
Nitrate/Nitrite as N
LCS (POF0108-BS1)
Nitrate/Nitrite as N
Matrix Spike (POF0108-MS1)
Nitrate/Nitrite as N
Matrix Spike Dup (POF0108-MSD1)
Nitrate/Nitrite as N
BRL 5.0 mg/kg wet
Prepared & Analyzed: 06/02/10
49.4 5.0 mg/kg wet 50.0 99 80-120
Source: 0060008-08 Prepared & Analyzed: 06/02/10
351 35 mg/kg dry 354 71.6 79 80-120
Source: 0060008-08 Prepared & Analyzed: 06/02/10
MI
351 35 mg/kg dry 354 71.6 79 80-120 0.1 20 MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 24 of 40

R I S IVI I Full -Service Analytical &
Environmental Solutions
LAOORATONIE& INC.
Level II QC Report
6/16/10
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
General Chemistry Parameters - Quality Control
Analyte
Project: IPP-001
Result
Reporting
Limit Units
Prism Work Order: 0060008
Time Submitted: 5/26/10 3:20:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P0F0134 - NO PREP
Blank (P0F0134-BLK1)
Prepared & Analyzed: 06/04/10
Ammonia as N
LCS (P0F0134-BS1)
BRL 2.5 mg/kg
Prepared & Analyzed: 06/04/10
Ammonia as N
Matrix Spike (P0F0134-MS1)
Ammonia as N
Matrix Spike Dup (P0F0134-MSD1)
Ammonia as N
Batch POF0180 - 351.2
2.41 0.050 mg/kg 2.50 97 80-120
Source: 0060008-08 Prepared & Analyzed: 06/04/10
382 2.4 mg/kg 121 288 77 80-120
Source: 0060008-08 Prepared & Analyzed: 06/04/10
MI
384 2.4 mg/kg 121 288 79 80-120 0.6 20 MI
Blank (POF0180-BLK1)
Prepared: 06/07/10 Analyzed: 06/08/10
Total Kjeldahl Nitrogen
BRL 25 mg/kgwet
LCS (POF0180-BS1) Prepared: 06/07/10
Total Kjeldahl Nitrogen
Matrix Spike (POF0180-MS1)
125 25 mg/kg wet 125
Analyzed: 06/08/10
100 90-110
Source: 0060008-08 Prepared: 06/07/10 Analyzed: 06/08/10
Total Kjeldahl Nitrogen
Matrix Spike Dup (POF0180-MSD1)
Total Kjeldahl Nitrogen
125000 35000 mg/kg dry 70900 48900 107 90-110
Source: 0060008-08 Prepared: 06/07/10 Analyzed: 06/08/10
122000 35000 mg/kg dry 70900 48900 103 90-110 2 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 25 of 40

PJRJSM
epngTOMES INC
Full -Service Analytical &
Environmental Solutions
Level II QC Report
6/16/10
Hart & Hickman (Charlotte)
Attn: Steve Hart
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Microbiological Parameters - Quality Control
Project: IPP-001 Prism Work Order: 0060008
Time Submitted: 5/26/10 3:20:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch POF0060 - NO PREP
Blank (P0F0060-BLK1) Prepared & Analyzed: 05/27/10
Fecal Coliforms
Duplicate (P0F0060-DUP1)
BRL 1000 CFU/g wet
Source: 0060008-01 Prepared & Analyzed: 05/27/10
Fecal Coliforms
BRL 15000 CFU/g dry 0.00
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
I Page 26 of 40 I

Sample Extraction Data
Prep Method: 361.2
Lab Number Batch
Initial
Final Date
0060008-08
NO PREP
Lab Number
POF0180 0.05 g 25 mL 06/07/10
Batch Initial Final Date
0060008-01 P0F0095 30 g 30 mL 08/03/10
0060008-02 POF0095 30 g 30 mL 06/03/10
0060008-03 P0F0095 30 g 30 mL 06/03/10
0060008-04 P0F0095 30 g 30 mL 06/03/10
0060008-05 POF0095 30 g 30 mL 06/03/10
0060008-06 P0F0095 30 g 30 mL 06/03/10
0060008-07 P0F0095 30 g 30 mL 06/03/10
0060008-08 P0F0067 30 g 30 mL 08/02/10
0060008-08 P0F0078 50 g 50 mL 06/03/10
0060008-08 P0F0076 20 g 20 mL 06/03/10
0060008-08 P0F0134 1.02 g 50 mL 06/04/10
0060008-08 POF0108 1.001 g 50 mL 06/02/10
NO PREP
Lab Number
Batch Initial Final Date
0060008-01 POF0060 1.012 g 100 mL 05/27/10
0060008-02 POF0060 1.003 g 100 mL 05/27/10
0060008-03 POFOO6O 0.991 g 100 mL 05/27/10
0060008-04 POF0060 1.015 g 100 mL 05/27/10
0080008-05 POF0060 1.004 g 100 mL 05/27/10
0060008-06 POF0060 1.006 g 100 mL 05/27/10
0060008-07 POF0060 1.004 g 100 mL 05/27/10
Prep Method: 3580A
Lab Number Batch Initial Final Date
0060008-08 POF0141
0060008-09 POF0201
0.6 g
0.61 g
10 mL 06/02/10
10 mL 06/02/10
Prep Method: 1311
Lab Number Batch Initial Final Date
0060008-08
Prep Method: 3010A
Lab Number
P0F0065 100 g 2000 mL 06/02/10
Batch initial Final Date
0060008-08
Prep Method: 7470A
Lab Number
POF0100 10 mL 50 mL 06/03/10
Batch Initial Final Date
0060008-08
Prep Method: 3050E
Lab Number
P0F0086 20 mL 30 mL 06/03/10
Batch Initial Final Date
0060008-08 POF0101 2.05 g 50 mL 06/03/10
0060008-08 POF0101 2.05 g 50 mL 06/03/10
0060008-08 POF0101 2.05 g 50 mL 06/03/10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-800/529-6364 - Fax: [phone]
Page 27 of 40

Sample Extraction Data
Prep Method: 7471B
Lab Number
Batch
Initial
Final Date
0060008-08
Prep Method: 6036
P0F0255 0.6131 g 50 mL 06/10/10
Lab Number Batch Initial Final Date
0060008-08 P0F0231
0060008-09 P0F0267
2.15 g
2.15 g
5 mL
5 mL
Subcontracted Analyses
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab Number Analysis
06/08/10
06/08/10
0060008-08 lgnitability
0060008-08 Reactivity, Cyanide (Sub)
0060008-08 Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone]
Page 28 of 40

LikAAR I M
Y LABORATORIES INC.
Full -Service Analytical &
Environmental Solutions
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543
Phone: [phone] • Fax: 704�/ 40/9
Client Company Name: / % crt / '
Report To/Contact Name: 5-7it/e /i'w
Reportingri
Address: .,1" 2?
Cc r47it, /VC 47-?
Phone. �y'-5FC— 7Fax (Yes)y
Emai (Ye ) (No),E ail Address.r4a•,^`t(e' cc �i«,�y�alxyr,
EDD Type: PDF)C Excel Other
Site Location Name:
Site Location Phy 'cal Address:
A/C
CLIENT
SAMPLE DESCRIPTION
Sampler's Signature
DATE
COLLECTED
\%.
Upon relinquishing, this Chain
submitted in writing to the Pris
Relinquished By: (Signature)
Relinquished By: (Signature)
Relinquished By: (Signature)
. TIME
COLLECTED
MILITARY
HOURS
MATRIX
. (SOIL,
WATER OR
SLUDGE)
✓vac:
CH IN OF CUSTODY RECORD
PAGE�F QUOTE # TO ENSURE PROPER BILLING.
P
Project Name. .-�r
Short Hold Analysis:
(Yes)
(No) UST Project: (Yes)((No
*Please ATTACH any pI'bjeLrt specific reporting (QC LEVEL 1 1i llilV)
provisions and/or Requirements roe
Invoice To* sTI /at �ii%B/%-
Address
amp10INTACl upon arrivah
ecelved ON:WET IO0 Temp J 1 '
ROPER PRESERVATIVES indicated
eoahkd WITHI r(f HOLDINGTIMES2
UST, ODY,SEALS 1NTACT1
OLATILES r-ec d W/OU,T HEADSPACE'r.
T�QPER CONiAIN�R$:u'sed?
rcthase Order No./Billing Reference
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days Days
"Working Days" p 6-9 Days 0 Standard 10 days ❑ Pre Appor Must Be
Samples received after 15:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) ]�+
SAMPLE CONTAINER4646
*TYPE
SEE BELOW
NO.
SiZE
PRESERVA-
TIVES
ANALYS
�V
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNE7
Certification: NELAC USACE FL NC
SC OTHER N/A
Water Chlorinated: YES NO, <
Sample Iced Upon Collection. YES
EQU STED
tr.
t to \
S
net
PRISM
LAB
ID NO.
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1
1/
-57 x X Y_X
6$
Sampled By (Print Name) LO C afO�ilxtLr
Affiliation _,/`T r`1
ustody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
rrject Manager. There will be charges for any changes after analyses have been initialized.
Received By: (Signature)
Date Military/Hours
Date
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEA - OR TRANSPORTATION TO THE LABORATORY. C Oro/kg
is--2
S LES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
0 Fed Ex 0 UPS and -delivered 0 Prism Field Service 0 Other •
PRESS DOWN FIRMLY - 3 COPIES
Additional Comments:
* Glass f3
�vra/ySif
a� Ah 44,c / ets 'tr
/'%. Pravrc•�e
-4C7r scL�r o/es
PRISM USE ONLY
ate Arrival?line;:
Bite: Departure;Tiilie
Field Tech Fee:i
1Nileage::;
DdC, e,On Q 1
NPDES: UST: GROUNDWATER:RCRA:
o NC ❑ SC o NC ❑ SC la NC ❑ SCT U NCI❑ SC ATER: SOLID NC El SC WASTE:^ 0 NC 0 SC U NC L❑ SC D NC LANDFILL❑ SC O NC ❑ SC fl r / a/off ta4l5+'
cvra/yt
•CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) J s?7.ie�
SEE REVERSE FOR
TERMS & CONDITIONS
ORIGINAL

ACCESS
A ►ALY I
ANALYTICAL REPORT
CLIENT
Prism Laboratories, Inc.
PO BOX 240543
Charlotte, NC 28224
ATTENTION
Angie Overcash
PROJECT ID
0060008
LABORATORY REPORT NUMBER
210060325
DATE
06/10/2010
Primary Data Review By Secondary Data Review By
Curtis Ekker
Data Validation Manager, GCAL
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL), 7979 GSRI
Rd. Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955, NELAP
certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a representative of
GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access
Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Page 30 of 40

NELAP CERTIFICATE NUMBER 01955
ANALYTICAL RESULTS
PERFORMED BY
GULF COAST ANALYTICAL LABORATORIES, INC.
7979 GSRI Rd.
Baton Rouge, LA 70820
Report Date 06/10/2010
GCAL Report 210060325
IIllIflhI pIII 0IIIIIIIII I II1II
Deliver To Prism Laboratories, Inc.
PO BOX 240543
Charlotte, NC 28224
706-529-6364
Attn Angie Overcash
Project 0060008
Page 31 of 40

CASE NARRATIVE
Client: Prism Laboratories, Inc. Report: 210060325
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the sample cross-reference page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
CONVENTIONALS
The Flashpoint analysis for sample 21006032501 (SLUDGE COMP 1) was performed by SW-846 Method
1010. The matrix is identified as a solid; while solid samples do not fall within the scope of this method, this
sample is a liquid.
Page 32 of 40

Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the
Environmental Protection Agency or other recognized agencies. The samples and their corresponding
extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention
period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.
Common Abbreviations Utilized in this Report
ND ndicates the result was Not Detected at the specified RDL
DO ndicates the result was Diluted Out
MI ndicates the result was subject to Matrix Interference
TNTC ndicates the result was Too Numerous To Count
SUBC ndicates the analysis was Sub -Contracted
FLD ndicates the analysis was performed in the Field
PQL Practical Quantitation Limit
MDL Method Detection Limit
RDL Reporting Detection Limit
00:00 Reported as a time equivalent to 12:00 AM
Reporting Flags Utilized in this Report
J Indicates an estimated value
U Indicates the compound was analyzed for but not detected
B (ORGANICS) Indicates the analyte was detected in the associated Method Blank
B (INORGANICS) Indicates the result is between the RDL and MDL
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with
NELAC, this report shall be reproduced only in full and with the written permission of GCAL. The results
contained within this report relate only to the samples reported. The documented results are presented
within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as
a permanent record thereof. The results contained within this report are intended for the use of the client.
Any unauthorized use of the information contained in this report is prohibited.
certify that this data package is in compliance with the NELAC standard and terms and conditions of the
contract and Statement of Work both technically and for completeness, for other than the conditions in the
case narrative. Release of the data . contained in this hardcopy data package and in the
computer -readable data submitted has been authorized by the Quality Assurance Manager or his/her
designee, as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the
DOD QSM as specified in the contract if applicable.
Int
■
ign
Robyn Migues
Technical Director
GCAL REPORT 210060325
InteSig
THIS REPORT CONTAINS lit PAGES.
Page 33 of 40

Report Sample Summary
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
21006032501 SLUDGE COMP 1 Solid 05/26/2010 13:45 06/03/2010 08:50
GCAL Report 210060325
Page 34 of 40

Summary of Compounds Detected
There were no detects
GCAt. Report 210060325.
Page 35 of 40

:GCAL ID
2100603250
Client ID`
SLUDGE'COMI
atrb
ollect Datefrlme
5//26/201013:45
Receive=Datefrima
06/03/2010 08:50 ,.
SW-846 1010 Flashpoint
Prep Date Prep Batch
Prep Method
Dilution Analyzed By Analytical Batch
1 06/03/2010 10:30 DJH 433502
CAS# Parameter
000000-01-3 FlashPoint
SW-846 9012A Reactivity CN
Result
>170
RDL
50
MDL
50
Units
Deg F
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
06/04/2010 13:00 433485 7.3.3.2 1 06/04/2010 15:48 DJH 433685
CAS#
Parameter
57-12-5R Reactivity Cyanide
SW-846 9034 Reactivity Sulfide
Result
250U
RDL
250
MDL
250
Units
mg/kg
Prep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
06/04/2010 13:00 433486 Sec 7.3.4.2 1 06/04/2010 15:10 JEM 433682
CAS#
Parameter
18496-25-8R Reactivity Sulfide
RESULTS REPORTED ON A WET WEIGHT BASIS
Result
80U
RDL
80
MDL
80
Units
mg/kg
GCAL Report 210060325
Page 36 of 40

CD
CO
w
V
0
41.
General Chemistry Quality Control Summary
Analytical Batch 433502
Prep Batch N/A
Client 1D
GCAL 1D
Sample Type
Analytical Date
Matrix
LCS433502
840310
LCS
06/03/2010 10:30
Solid
SW-846 1010 Flashpoint
p
Spike
Added
Result
% R
Control
Limits °% R
000000-01-3 FlashPoint
90
91
101
97.8 -102.2
GCAL Report 210080325

MNIER
0)
CO
CD
W
CO
0
41,
General Chemistry Quality Control Summary
Analytical Batch 433685
Prep Batch 433485
Prep Method 7.3.3.2
Client ID
GCAL ID
Sample Type
Prep Date
Analytical Date
Matrix
MB433485 _
839016
Method Blank
06/04/2010 13:00
06/04/2010 15:40
Solid
LCS433485
839017
LCS
06/04/2010 13:00
06/04/2010 15:40
Solid
SW-846 9012A Reactivity CN
Units mg/kg
Result
Spike
Rgttided
Result
_
% R
Control
Limits % R
57-12-5R Reactivity Cyanide
250U 250
250
24.3
10
1 - 25
Analytical Batch 433685
Prep Batch 433485
Prep Method 7.3.3.2
Client ID
GCAL ID
Sample Type
Prep Date
Analytical Date
Matrix
MC #1
21006031001
SAMPLE
06/04/201013:00
06/04/2010 15:44
Solid
838914DUP
839018
DUP
06/04/2010 13:00
08/04/2010 15:45
Solid
SW-846 9012A Reactivity CN
Units mg/kg
Result RDL
Result
RPD
D
Limit
57-12-5R Reactivity Cyanide
0.0000 250
0.0000
0
25
GCAL Report 210060325

0V I0 6£ 86ed
General Chemistry Quality Control Summary
Analytical Batch 433682
Prep Batch 433486
Prep Method Sec 7.3.4.2
Client ID
GCAL ID
Sample Type
Prep Date
Analytical Date
Matrix
M6433486
839020
Method Blank
06/04/2010 13:00
06/04/2010 15:10
Solid
LCS433486
839021
LCS
06/04/2010 13:00
06/04/2010 15:10
Solid
SW-846 9034 Reactivity Sulfide
Units mglkg
Result
Spike
Mklded
Result
% R
Control
Limits % R
18496-25-8R Reactivity Sulfide
80U
80
1000
646
64.6
20 - 114
Analytical Batch 433682
Prep Batch 433486
Prep Method Sec 7.3.4.2
Client ID
GCAL ID
Sample Type
Prep Date
Analytical Date
Matrix
MC #1
21008031001
SAMPLE
06/04/2010 13:00
08/04/2010 15:10
Solid
838914DUP
839022
DUP
06/04/201013:00
08/04/2010 15:10
Solid
SW-846 9034 Reactivity Sulfide
Units
Result
mg/kg
RDL
Result
RPD
RPD
Limit
18498-25-8R Reactivity Sulfide
0
80
0
0
25
GCAL Report 210060325

SUBCONTRACT ORDER
Prisms Laboratories, Inc.
0060008
A ec,ee s/k s` Sl2roral, tl';2c/6, tato
SENDING LABORATORY:
Prism Laboratories, Inc.
P. O. Box 240543
Charlotte, NC 28224-0543
Phone:800-529=6364
Fax: [phone]
Project Manager: Angela D. Overcast'
RECEIVING LABORATORY:
Gulf Coast Analytical Labs, Inc.
7979 GSRI Avenue
Baton Rouge, LA 70820
Phone :[phone]
Fax: [phone]
Analysis Due
Expires
Laboratory ID Comments
Sample ID: 0060008-08 Solid
Reactivity (Sub)
Ignitability
Containers Supplied::
Sampied:05/26/10 13:45
06/02/10 15:00
06/02/10 15:00
06/02/10 13:45
06/23/10 13:45
(
Releasecf13y
S-1
6-I -Jo
Date
eX b-Z-1�
Released By Date
rc.�ct (o-S. 40 gz.
Received By Datc
Received 13y Date
/72
Page 1 of 1
Page 40 of 40

Table 1
Summary of Wastewater Tank Volume Estimates
Former Crompton & Knowles Facility
Lowell, NC
H&H Project No. FDP-033
RECEIVED/DENR/DWR
FEB t 3 2G.t
Water Quality
Permitting Sectior
Tank
Diameter
(ft)
Hei ht ft
g ()
Total Capacity
(ft3)
Total Capacity wl
2' freeboard (ft3)
Current Water
Volume (ft3)
Current Sludge
Volume (ft3)
Total Water and
Sludge Volume (ft3)
Total Excess
Capacity (ft3)
1'
60
6.5
18400
"
8700
8000
16700
1700
2
50
11
21600
20600
10000
0
10000
10600
3
60
13
36700
31100
17000
9300
26300
4800
4
70
25.5
98100
90400
17000
0
17000
73400
5
60
26
73500
67800
9000
17800
26800
41000
6
20
20
6300
5700
1500
450
1950
3750
Notes:
- Tank has a hole cut on side of tank so measurements are from hole.
" - Due to limited height of tank, no freeboard used in calculation for Tank 1

la 2015 Google
TITLE
WASTEWATER TANK LOCATIONS
PROJECT FORMER CROMPTON & KNOWLES FACILITY
LOWELL, NC
hart hickman
Ow -
SMARTER ENVIRONMENTAL SOLUTIONS
DATE: 2-13-15
JOB NO: FDP-035
2923 South Tryon Srrccr-Suitc 100
Charlotte, North Carolina 28203
704-586-0007 (p) 704-586-0373 (1)
REVISION NO: 0
FIGURE: 1

Stormwater/Sludge in Wastewater Tanks
Due to the presence of stormwater getting close to the bottom of the cut out section of Tank 1, on
February 3, 2015, Hart & Hickman, PC measured the total volume capacity, existing water and
sludge volume, and remaining capacity in each tank. Remaining capacity was calculated assuming
a 2 ft freeboard in each tank except for Tank 1. A summary of these measurements is provided in
the attached table. The locations of the tanks and their designations is provided in the attached
figure.
Based upon the above, Lowell Investments I is proposing to pump stormwater in Tank 1 to Tank
4. The approximate volume of water in Tank 1 is 8,700 cubic ft (65,000 gallons) and the current
excess capacity in Tank 4 is 73,400 cubic ft (550,000 gallons). These values are highlighted in the
attached table. Prior to pumping the water, we will sample the water in Tank 1 for volatile organic
compounds by EPA Method 8260, for semi-VOCs by EPA Method 8270, and for RCRA metals.
In addition, a composite sample will be collected from the remainder of the tanks for analysis of
the same parameters to provide updated analytical data for the tanks. These data will be provided
to you before the water is transferred from Tank 1 to Tank 4.
We also understand that DENR has requested sludge analytical data from the tanks. In May 2010,
Hart & Hickman collected samples of the sludge from the tanks. Seven grab samples were
collected for analysis of fecal coliform, and one composite sludge sample from all of the tanks was
collected and analyzed for pH (corrosivity), ignitability, reactivity, nitrate/nitrite, total Kjeldahl
nitrogen, ammonia, VOCs, SVOCs, metals, and toxicity characteristic leaching procedure (TCLP)
VOCs, SVOCs, and metals. The data are attached. Because there has been no wastewater
treatment since that time and the sludge was not removed after the samples were collected in 2010,
we believe that these data are representative of the current condition of the sludge. Therefore, we
do not believe that additional sampling of the sludge is warranted at this time.

'LOWELL INVESTMENTS I, LLC
5320 Old Pineville Road, Charlotte, NC 28217
Tel [phone]
February 16, 2015
Mr. Michael E. Templeton, P.E.
NCDENR/ Division of Water Resources
Water Quality Permitting Section/ Wastewater Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVEDIDENRIDWR
�? F X.U'i'
RE: NPDES Permit NC0005274 - Former Crompton and Knowles Plant — Lowell, NC
Mr. Templeton;
Water Quality
Permitting Sectio,
This letter is to provide you with an update on the above referenced NPDES Permit and related development plans
pertaining to the site. Additionally this letter addresses our plans for storing the storm water that has accumulated
in Tank 1.
Summary of Current Redevelopment Plan for the Site:
• NC DENR is in possession of $3+mm dollars received from the Crompton & Knowles bankruptcy
proceedings to be utilized towards the site remediation.
• I have entered into conversations with Gaston County officials regarding the County purchasing the site
from me to expand Poston Park which is contiguous on two sides.
• We have agreed in principle on a price and general terms, however, nothing definitive.
• The plan is for the County to purchase the site from me, and then work with DENR to establish a Brownfield
appropriate scope of work and how the bankruptcy funds could be utilized for the sites remediation and
potentially for some limited redevelopment / restoration work.
• Part of the purchase price would include the nutrient allocation from the existing NPDES Permit.
• The Carolina Thread Trail would connect along the water frontage (a key connection).
• A few of the buildings would likely remain as public works, park and other municipal outbuildings (likely not
full office build out).
Regarding the existing NPDES Permit, Twin Rivers Utilities (Gaston County) has expressed an interest in acquiring
the nutrient allocation as part of the transaction. While the allocation is not currently needed, Twin Rivers is desirous
of protecting the allocation for allocation future growth and potentially stricter nutrient rules. The nutrient allocation
is one of the key assets associated with the site and its continued protection is critical.
Plan for Accumulated Storm Water in Tank 1
As the current owner of the site, Lowell Investments I, LLC has not had any discharges from the facility. There are

various tanks (outlined below) that have sludge that will eventually need to be removed. Prior to taking title, the
previous owner Kings Mountain Venture # 1, LLC received permission from DENR to drain the water in these tanks.
Since we acquired the site in December of 2013, rain water has filled these tanks again.
Due to the presence of storm water getting close to the bottom of the cut out section of Tank 1, on February 3, 2015,
Hart & Hickman, PC measured the total volume capacity, existing water and sludge volume, and remaining capacity
in each tank. Remaining capacity was calculated assuming a 2 ft. freeboard in each tank except for Tank 1. A
summary of these measurements is provided in the attached table. The locations of the tanks and their designations
is provided in the attached figure.
Based upon the above, Lowell Investments I is proposing to pump storm water in Tank 1 to Tank 4. The approximate
volume of water in Tank 1 is 8,700 cubic ft. (65,000 gallons) and the current excess capacity in Tank 4 is 73,400
cubic ft. (550,000 gallons). These values are highlighted in the attached table. Prior to pumping the water, we will
sample the water in Tank 1 for volatile organic compounds by EPA Method 8260, for semi-VOCs by EPA Method
8270, and for RCRA metals. In addition, a composite sample will be collected from the remainder of the tanks for
analysis of the same parameters to provide updated analytical data for the tanks. This data will be provided to you
before the water is transferred from Tank 1 to Tank 4.
We also understand that DENR has requested sludge analytical data from the tanks. In May 2010, Hart & Hickman
collected samples of the sludge from the tanks. Seven grab samples were collected for analysis of fecal coliform,
and one composite sludge sample from all of the tanks was collected and analyzed for pH (corrosivity), ignitability,
reactivity, nitrate/nitrite, total Kjeldahl nitrogen, ammonia, VOCs, SVOCs, metals, and toxicity characteristic leaching
procedure (TCLP) VOCs, SVOCs, and metals. The data is attached. Because there has been no wastewater
treatment since that time and the sludge was not removed after the samples were collected in 2010, we believe
that this data is representative of the current condition of the sludge. Therefore, we do not believe that additional
sampling of the sl .ge is warranted at this time.
Lowell In
adva
McKitt c
anager
Lowell Investments I, LLC
I, LLC is requesting permission from DENR to proceed with plan as outlined above. Thanks in
consideration and we will continue to keep DENR informed as plans for the site progress.
Cc: Jeff Poupart - DENR
Tom Belnick — DENR
Jim Bateson — DENR
Sharon Eckard - DENR
Steve Hart — Hart & Hickman
Page 2

Belnick, Tom
From: Tom McKittrick [[e-mail]]
Sent: Monday, February 16, 201.5 3:34 PM
To: Templeton, Mike
Cc: Belnick, Tom; Bateson, James; Eckard, Sharon; Poupart, Jeff; Steve Hart
Subject: Proposed Lowell Storm Water Plan
Attachments: doc20150216150519.pdf
Hello Mike (et all)
Please find a letter regarding the storm water that has accumulated in various tanks at the
former Crompton & Knowles plant in Lowell, NC. The letter outlines our plans to move the
water from Tank 1 into another tank so that it does not discharge through a hole cut in Tank
1 by the previous owner.
We continue to work through the process with DENR to secure a BFA on the site and hopefully
sell the property to Gaston County for the expansion of a park that is contiguous to the
property.
Thanks in advance and please do not hesitate to call me if you would like to discuss further.
Tks
Tom
Tom McKittrick
President
Forsite Development, Inc.
5320 Old Pineville Road
Charlotte, NC 28217
[phone] Direct
[phone] Office
[phone] Fax
tomfforsiteinc .com
www.forsiteinc.com
www.reventurepark.com
Original Message
From: [e-mail] [mailto:copierOforstieinc.com]
Sent: Monday, February 16, 2015 3:05 PM
To: Tom McKittrick; Shannon Doster
Subject:
TASKalfa 400ci
[00:c0:ee:4c:03:bd]