Shallotte Sampling for 3-5-22 spill

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,Znvirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Shallotte Date of Report: Mar 07, 2022
P.O. Box 2287 Customer PO #:
Shallotte NC 28459 Customer ID: 09010021
Attention: Randy Long Report #: 2022-04085
Project ID: Sewer Spill
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-09750 Site: 4950 Main Street 3/6/2022 10:56 AM Water C. Little
Test Method Results Date Analyzed
Enterococci Enterolert IDEXX 20 MPN/100ml 03/06/2022
Fecal Coliform SM 9222 D-2015 MF 220 Colonies/100mL 03/06/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-09751 Site: 693 Lightwood, Lane 3/6/2022 11:10 AM Water C. Little
Test
Method
Results Date Analyzed
Enterococci Enterolert IDEXX 10 MPN/100ml 03/06/2022
Fecal Coliform SM 9222 D-2015 MF 19 Colonies/100mL 03/06/2022
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-09752 Site: 158 Wall Street 3/6/2022 11:23 AM Water C. Little
Test Method Results Date Analyzed
Enterococci
Fecal Coliform
Comment:
Reviewed by:
Enterolert IDEXX
SM 9222 D-2015 MF
10 MPN/100ml 03/06/2022
270 Colonies/100mL 03/06/2022
Report #:: 2022-04085 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910 392 0
Sample Receipt Checklist • 223
ClienLUAl PIVE —I-D " 3 ICP%C-)N
Date: Report Number: _ 2022- 408
Receipt of sample: ECHEM Pickup ❑ Client Delivery
UPS ❑
❑ NO
RO�nYESTEOJ
FedEx ❑ Other ❑
N/A 1. Were custody seals present on the cooler?
NO
Original temperature upon
V N/A 2. If custody seals were present, were they intact/unbroken?
receipt °C
Corrected temperature upon receipt How temperature taken: ❑ Temperature Blank
Against Bottles
IR Gun ID: Thomas Traceable S/N: 210835468 IR Gun Correction Factor °C: 0.0
❑ YES ❑ NO
YES ❑
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
NO
YES ❑
4. Were proper custody procedures (relinquished/received) followed?
NO
5. Were sample ID's listed on the COC?
YES ❑ NO
6. Were samples ID's listed on sample containers?
YES ❑ NO
7. Were collection date and time listed on the COC?
YES ❑ NO
8. Were tests to be performed listed on the COC?
YES ❑ NO
9. Did samples arrive in proper containers for each test?
YES I ❑ Nn
YFS ❑ NO
I�n n +�,� i-,- .•
r -� tUJi L011uiii0n for each test?
YES ❑
Ill Was adequate sample volume al,ailab!e?'
NO
12. Were samples received within proper holding time for requested tests?
YES ❑ NO
13. Were acid preserved samples received at a pH of <2?
YES ❑ NO
14. Were cyanide samples received at a pH >12?
YES ❑ NO
15. Were sulfide samples received at a pH >9?
YES ❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
YES ❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
YES ❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
bample(s) were received incorrectly preserved and were adjusted accordingly
y adding (circle one): Hz504 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrect:y preserved samples. Obtain a new sample or
Doti i the state lab if directed to analyzed by the customer. who was notified, date and time:
✓olatiles Sample(s) were received with headspace
COMMENTS:
°C
DOC. QA.002 Rev 1

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