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HomeMy WebLinkAboutNC0005274_Permit (Issuance)_20121217NPDES DOCUMENT SCANNING COVER SWEET NPDES Permit: NC0005274 Document Type: ,� Permit Issuance - T Wasteload Allocation Authorization to Construct (AtC) Permit Modification Complete File - Historical Engineering Alternatives (EAA) Correspondence Instream Assessment (67b) Speculative Limits Environmental Assessment (EA) Permit History Document Date: December 17, 2012 This document is printed on reuse paper - ignore arty - content on the reszerse side ATA NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Charles Wakild, P. E. Dee Freeman Governor Director • Secretary December 17, 2012 Mr. Tony Chiarella, Director of Operations Kings Mountain Venture #1, LLC 17 A Marlen Drive Hamilton, NJ 08691 Subject: Issuance of NPDES Permit NC0005274 Kings Mountain Venture #1 Gaston County Dear Mr. Chiarella: Division personnel have reviewed and approved your application for renewal of the subject permit. Accordingly, we are forwarding the attached NPDES discharge permit. This permit is issued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the U.S. Environmental Protection Agency dated October 15, 2007 (or as subsequently amended). The following changes have been incorporated into this permit renewal: • This permit will expire on December 31, 2013 - one year after the permit becomes effective. Kings Mountain Venture is expected to remove, seal and /or eliminate Outfall 001 after wastewaters from tanks AT 1, PC 2, ET 3, and SC 4 are transferred to the 400,000 gallon storage tank and discharge is completed. • Sections A.(1.) OCPSF Subpart I monitoring and A.(4.) Nutrient Special Condition (BMP Evaluation) were removed from the permit since textile dye operations at the facility have been terminated. • All the sample types have been changed to grab samples. Effluent samples shall be representative and taken after aeration or completion of treatment. It is recommended that samples be taken from the middle level of the center column of the storage tank. • Special condition, A. (3) Color Permitting Requirements, has been modified to clarify that effluent and stream samples be taken during discharge periods. 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Location: 512 N. Salisbury St Raleigh, North Carolina 27604 Phone: 919-807-63001 FAX: 919-807-6492 Internet: www.ncwaterqualitv.orq An Equal Opportunity 1 Affirmative Action Employer None Carolina aturu!ly Page 2 of 3 • Effluent monitoring for Total Phenolics, PAHs, Sulfates, Chlorides, Total Phosphorus, Total Nitrogen, and Color have been increased to daily or whenever a discharge occurs. • Upstream and downstream monitoring have been reduced to 1/week during discharge periods. • The Supplement to Permit Cover Sheet has been modified to identify the transfer of wastewaters to the 400,000 gallon storage tank for treatment and discharge to South Fork Catawba River. It also states that the pumping of wastewaters from the four tanks to the 400,000 gallon storage tank shall cease at 1-2 feet above the sludge level. • In Section A.(1.) the permitted flow has been reduced to 0.20 MGD and the flow measurement changed to instantaneous. Since the effluent will be pumped to Outfall 001 the pumping rate along with documentation on the duration of time wastewaters are pumped can be used to determine the daily flow volume reported on the Discharge Monitoring Reports (DMRs). Note that the Permittee may use a recording device if preferred. • Wastewaters shall not be discharged until 24 hour aute toxicity tests using (1)Ceriodaphnia dubia and (2) Fathead Minnow (Pimephales promelas) are performed on each treated batch of wastewater and no significant acute mortality at 90% is shown. See Section A. (2.) ACUTE TOXICITY MONITORING (Episodic) in the permit. The Permittee is required to notify the DWQ/Surface Water Protection Section at the Mooresville Regional Office 48 hours prior to discharge to allow for their inspection or observation of the wastewater discharge. Suggested contacts are Wes Bell or Michael Parker at 704-663-1699. Acute toxicity test results shall be made available to the Regional personnel upon request and submitted with monthly Discharge Monitoring Reports. All sludge and wastewaters associated with the sludge will be disposed of in accordance with state and federal regulations. Wastewaters as part of sludge dewatering will not be discharged via Outfall 001. Please note that the receiving stream is listed as an impaired waterbody on the North Carolina 303(d) Impaired Waters List. Addressing impaired waters is a high priority with the Division, and instream data will continue to be evaluated. If there is noncompliance with permitted effluent limits and stream impairment can be attributed to your facility, then mitigative measures may be required. If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30) days following receipt of this letter. This request must be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings (6714 Mail Service Center, Raleigh, North Carolina 27699- 6714). Unless such demand is made, this decision shall be final and binding. Please note that this permit is not transferable except after notice to the Division. The Division may require modification or revocation and reissuance of the permit. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Water Quality or permits required by the Division of Land Resources, the Coastal Area Management Act or any other Federal or Local governmental permit that may be required. Page 3 of 3 If you have any questions concerning this permit, please contact Julie Grzyb by email (julie.grzyb@ncdenr.gov) or phone at (919) 807-6389. Sincerely, 6$1( arles Wakild P.E. Enclosure: NPDES Permit NC0005274 cc: NPDES Unit Central Files Mooresville Regional Office / Surface Water Protection Section e-copy: Aquatic Toxicology Unit Stephen Timm, Safety/Environmental Director, safetytraining@rcn.com EPA Region 4 Permit NC0005274 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY PERMIT TO DISCHARGE WASTEWATER UNDER THE NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, the Kings Mountain Venture #1, LLC is hereby authorized to discharge wastewater from a facility located at the Kings Mountain Venture #1, LLC 1602 Main Street Gaston County to receiving waters designated as South Fork Catawba River in the Catawba River Basin in accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III, and IV hereof. This permit shall become effective January 1, 2013. This permit and authorization to discharge shall expire at midnight on December 31, 2013. Signed this day December 17, 2012. for T arles Wakild, P.E., Director Division of Water Quality By Authority of the Environmental Management Commission Permit NC0005274 SUPPLEMENT TO PERMIT COVER SHEET All previous NPDES Permits issued to this faciliO, whether for operation or discharge are hereby revoked. As of this permit issuance, any previously issued permit bearing this number is no longer effective. Therefore, the exclusive authority to operate and discharge from this faciliy arises under the permit conditions, requirements, terms, and provisions included herein. Kings Mountain Venture #1, LLC is hereby authorized to: 1. Transfer remaining wastewaters in tanks AT-1, PC-2, ET-3, and SC-4 to a 400,000 storage tank for treatment (aeration). Pumping of wastewaters from the tanks to the 400,000 gallon storage tank shall cease at approximately 1-2 feet above the sludge level in each of the four tanks located at the Kings Mountain Venture facility (1602 Main Street, Lowell, Gaston County). 2. Discharge from said treatment works (via Outfall 001) into South Fork Catawba River, classified WS-V waters in the Catawba River Basin, at the location specified on the attached map. County: Gaston Quad# F14SE Stream Class: WS-V Subbasin/ 8-Digit HUC: 30836 / 03050102 Receiving Stream: South Fork Catawba River Latitiude: 35°17' 13" Longitude: 81°06'13" Permit NC0005274 A'(1.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS (001) Beginning on the effective date of this permit and lasting until expiration, the Permittee is authorized to discharge treated wastewater from outfall 001. Such discharges shall be limited and monitored by the Permittee as specified below: EFFLUENT. CHARACTERISTICS 4t EFFLUENT LIMITATIONS MONITORING REQUIREMENTS Monthly } . , Average,..' .. Daily Maximum , . Measurement .Frequency, Sample . ,Type ",= .= Sample Location' `' ,_ f Flow 0.20 MGD Instantaneous2 Estimate Effluent BOD, 5-day, 20°C 123 pounds/day 329 pounds/day Daily Grab Effluent Total Suspended Solids 156 pounds/day 501 pounds/day Daily Grab Effluent Total Phenolics 1.67 pounds/day Daily Grab Effluent PAHs3 0.012 pounds/day 3.6 Hg/I Daily Grab Effluent Sulfates Daily Grab Effluent Chlorides • Daily Grab Effluent Acute Toxicity4 See footnote (4) Grab Effluent Total Phosphorus 7.6 pounds/day Daily Grab Effluent Total Nitrogen (NO2+NO3+TKN) 144 poundslday Daily Grab Effluent Dissolved Oxygen • Daily Grab Effluent Temperatures Daily Grab Effluent PH6 Daily Grab Effluent Color? Daily Grab Effluent Color (April -October)? Monthly Grab Upstream & Downstream Temperatures 1/Week8 Grab Upstream & Downstream Dissolved Oxygen$ 1/Week8 Grab Upstream & Downstream Conductivity$ 1/Week8 Grab Upstream & Downstream Notes: 1. Upstream = approximately 2.2 miles upstream at the Stanley/Spencer Mountain Road bridge. Downstream = approximately 2.6 miles downstream at the riverbank near the Lowell WWTP. 2. The duration of discharge must be recorded in order to calculate the total discharge quantity per day. 3. PAHs applies to total PAHs present and includes: benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene, benzo(k)fluoranthene, chrysene, dibenz(a,h)anthracene, indeno(1,2,3-cd)pyrene. 4. Toxicity tests, 24 hour acute pass/fail at 90% effluent using 1)Ceriodaphnia dubia and 2)Fathead Minnow (Pimephales promelar) (see Special Condition A (2.)). 5. The temperature of the effluent shall not cause an increase in the receiving stream of more than 2.8°C, and in no case cause the receiving stream temperature to exceed 32°C. 6. The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units. 7. Refer to Color Permitting Requirements (see Special Condition A (3.)). 8. Instream sampling shall be 1/Week during a discharge period. There shall be no discharge of floating solids or visible foam in other than trace amounts. Permit NC0005274 A. (2.) ACUTE TOXICITY MONITORING (Episodic) The permittee shall conduct acute toxicity tests on each batch of treated wastewater transferred from tanks AT-1, PC-2, ET-3, and SC-4 to the 400,000 gallon storage tank, after treatment but prior to discharge. Toxicity tests shall be performed using protocols defined in the North Carolina Procedure Document entitled "Pass/Fail Methodology For Determining Acute Toxicity In A Single Effluent Concentration" (Revised December 2010 or subsequent versions). Two twenty-four hour acute pass/fail monitoring tests shall be performed on each batch prior to discharge using (1) Ceriodaphnia dubia and (2) Fathead Minnow (Pimephales promelas). For example, if the 400,000 gallon storage tank is filled 7 times, then 14 tests (7 using Ceriodaphnia dubia and 7 using Fathead Minnow) would be required. The effluent concentration at which there may be at no time significant acute mortality is 90% (defined as treatment two in the procedure document). Effluent samples for self -monitoring purposes should be obtained from the middle level of the center column of the 400,000 gallon storage tank after treatment is completed. Wastewaters shall not be discharged until both the Ceriodaphnia dubia and Fathead Minnow (Pimephales promelas) toxicity tests, performed on each treated batch of wastewater, demonstrate no significant acute mortality at 90%. The parameter code for Pimephalespromelas is TGE6C. The parameter code for Ceriodaphnia dubia is TGP3B. All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Form (MR-1) for the month and day in which it was performed, using the appropriate parameter code. Additionally, DWQ Form AT-2 (original) is to be sent to the following address: Attention: North Carolina Division of Water Quality Environmental Sciences Section 1621 Mail Service Center Raleigh, N.C. 27699-1621 Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Section no later than 30 days after the end of the reporting period for which the report is made. Test data shall be complete and accurate and include all supporting chemical/physical measurements performed in association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should there be no discharge of flow from the facility during any month in which toxicity monitoring is required, the permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the facility name, permit number, pipe number, county, and the month/year of the report with the notation of "No Flow" in the comment area of the form. The report shall be submitted to the Environmental Sciences Section at the address cited above. Should any test data from either these monitoring requirements or tests performed by the North Carolina Division of Water Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include alternate monitoring requirements or limits. If the Permittee monitors any pollutant more frequently then required by this permit, the results of such monitoring shall be induded in the calculation & reporting of the data submitted on the DMR & all AT Form submitted. NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival and appropriate environmental controls, shall constitute an invalid test and will require immediate follow-up testing to be completed no later than the last day of the month following the month of the initial monitoring. Permit NC0005274 A (3.) COLOR PERMITTING REQUIREMENTS The permittee will conduct color monitoring of instream stations (upstream, downstream) once a month during the discharge of treated wastewaters. The permittee will record whether a color plume was observed around the outfall pipe during the monthly instream sampling events, and include that information on the monthly discharge monitoring report. Effluent samples will be collected daily for color on a year-round basis during any day that a wastewater discharge occurs. Color samples will be analyzed for ADMI color at natural pH. Samples shall be analyzed by a state certified laboratory. NCDENR / DWQ Final FACT SHEET FOR NPDES PERMIT DEVELOPMENT Kings Mountain Venture #1, LLC NC0005274 Facility Information Facility Name: Kings Mountain Venture #1, LLC (formerly Yorkshire Americas, Inc.) Permitted Flow,MGD: 0.15 — 0.20 MGD 002-eliminated County: Gaston Facility Class: No rating Regional Office: Mooresville Facility Status: Existing USGS Topo Quad: F14SE Permit Status: Temporary Renewal Stream Characteristics Receiving Stream/ Basin: South Fork Catawba River / Catawba River Basin Subbasin / 8-Digit HUC: 030836 / 03050102 Drainage Area (mi2): 628 Stream Index No.: 11-129-(15.5) Summer 7Q10 (cfs) 123 Stream Class: WS-V Winter 7Q10 (cfs): 200 303(d) 2010 List: Turbidity & low pH 30Q2 (cfs): 310 303(d) 2012 List: Turbidity Average Flow (cfs): 798 Use Support: IWC (%): <0.3% Background Kings Mountain Venture is a Brownfield site which previously operated as Yorkshire Americas, a textile dye manufacturer. Yorkshire Americas, Inc. had purchased the facility from Crompton & Knowles on 12/17/99. A permit modification reflecting the change of ownership from Yorkshire Americas to King Mountain Venture (KMV) was issued on 1/12/2007. Operations at the facility were terminated under KMV. As a textile dye manufacturer the facility was classified as a primary industry based on specialty organic chemical production. It was subject to the Organic Chemicals, Plastics, and Synthetic Fibers (OCPSF) Federal Effluent Guidelines and discharged treated process wastewater via Outfall 001, and non -contact cooling water via Outfall 002. All domestic wastewater was treated by an onsite septic system. Dewatered sludge was disposed at the BFI landfill. In 1995 a new 0.4 MGD biological wastewater treatment system was installed, replacing an old lagoon treatment system. The facility is located on a 42-acre tract with 14 acres fenced around the plant. The facility is also bordered on the southeast by the Catawba River. During late August 2009, OSC Ken Rhame conducted a site inspection with NC DENR and local authorities and discovered hundreds of drums of dye and dye intermediates in various conditions as well as several above ground storage tanks which contained residual caustic and acids. In October 2009, KM Ventures agreed to an Administrative Order with EPA Region 4 which included a scope of work to conduct the clean up. Discharge of process wastewaters ceased in September 2009. In December 2009, Kings Mountain Venture (KMV) submitted an application for a permit renewal to discharge the remaining stormwater/ process wastewater contained in four of the treatment system basins. The application lacked enough data to proceed with the renewal so the Permittee was requested to sample each of the basins for a range of pollutants, to identify the volume of wastewater to be discharged and at what rate, and to estimate sludge volumes and disposal procedures. The facility's permit expired on June 30, 2009. NPDES PERMIT FACT SHEET Kings Mountain Venture #1, LLC - Page 2 NPDES No. NC0005274 Due to the closing of the plant and the elimination of all industrial activities associated with the site, stormwater was collected and tested to determine if a NPDES stormwater permit was necessary. In Feb. 2010 the Stormwater Permitting Unit stated that the results indicated no problems and since manufacturing operations were terminated and the site cleaned, a NPDES SW permit was not required. As part of that process, KMV eliminated Outfall 002. Mr. Stephen Timm of Safe-T-raining and Environmental Services, and the consultant for Kings Mountain Venture, proceeded to investigate the possibility of discharging the wastewaters to the local WWTP. In August 2011, the DWQ Pretreatment Unit evaluated the wastewaters and determined it was treatable within the City of Lowell's wastewater treatment plant. However, Mr. Ben Blackburn, City Manager for Lowell denied KMV's request to discharge wastewaters to the Lowell WWTP stating that their first responsibility was to protect the WWTP from potential damage and noncompliance and that their cost recovery was not sufficient. Mr. Timm then proceeded with additional testing of the wastewaters and completetion of a NPDES WW permit application. A complete application for permit renewal was received at DWQ on May 11, 2012. Wastewaters from the facility are discharged to the South Fork Catawba River (SFCR), which forms the headwaters of Lake Wylie. The previous permit for the manufacturing facility had a permitted design flow of 0.4 MGD and the facility's discharge represented 0.5% of the instrearn flow under summer 7Q10 low flow conditions. The receiving stream is listed as impaired for turbidity in the 2012 303(d) list and turbidity and low pH in the 2010 303(d) listing. Permit Application KMV's application is for a temporary permit to discharge 2.5 million gallons of the remaining wastewater/ stormwater contained in 4 different tanks throughout the abandoned treatment system. It should be noted that the biological treatment system is not a functioning system since it has been abandoned, dismantled and vandalized on occasion. The consultant for KMV has proposed to transfer wastewaters from the following tanks to a 400,000 gallon storage tank, provide treatment(aeration) if necessary, and discharge the treated wastewaters at the following rates: AT 1 -Discharge rate of 200,000 gallons/day with a volume of approximately 750,000 gallons PC 2 -Discharge rate of 150,000 gallons/day with a volume of approximately 564,000 gallons ET 3 -Discharge rate of 200,000 gallons/day with a volume of approximately 994,000 gallons SC 4 -Discharge rate of 150,000 gallons/day with a volume of approximately 205,000 gallons Once the aeration is completed and a dissolved oxygen of greater then 5.0 mg/L is reached, the wastewaters will be discharged. The consultant estimates that the discharge will continue for approximately 120 days based on proposed flow rates, water transfer activities from tank to tank and the aeration process. The consultant estimates that the four tanks contain 1,500 cubic yards of sludge. After the wastewaters are discharged, the sludge will be tested and disposed of in accordance with applicable regulations. Sludge levels in each tank were estimated to be 1 foot deep in tanks, AT- 1, ET-3, and SC-4, and 6.5 feet deep in PC-2. Permit Limit Development In January 2010 the consultant performed testing for pollutants believed to be present on the 2C list plus 4-Methyl 2-pentanone, Acetone, Carbon disulfide, M,P xylenes, and 3 & 4 Methylphenol in each tank. Samples were taken from the upper, middle and lower columns of each tank and analyzed. All the data was compared to NC water quality based standards and Page 2 Version: December 3, 2012 NPDES PERMIT FACT SHEET Kings Mountain Venture #1, LLC Page 3 NPDES No. NC0005274 no reasonable potential to violate standards was found. A summary table of the analysis results and the RPA are attached. Since this will be a batch discharge with an In -stream Wastewater Concentration of about 0.20 to 0.25 % the Aquatic Toxicity Unit (ATU) determined that whole effluent acute toxicity testing would be more applicable than chronic testing. The Aquatic Toxicity Unit reviewed the data and recommended that the permittee perform 24 hr acute pass/fail tests at 90% effluent on each batch to be discharged using (1) Ceriodaphnia dubia and (2) Fathead minnow (Pimephales promelas). In addition, ATU recommended that the tests be conducted on the effluent after aeration and prior to discharge. Therefore, each time the wastewaters are transferred to the storage tank for treatment, after the wastewaters are aerated, two acute toxicity tests: one using Ceriodaphnia dubia and a second using Fathead minnow (Pimephales promelas), are to be perfomed. Each batch of wastewaters can be discharged via Outfall 001, if a passing test results for both acute tests (ie. wastewaters show no significant acute mortality at 90(Yo effluent for invertebrates and vertebrates). The limitations in the previous permit were determined by choosing the more stringent TBEL or WQBEL limitation for each parameter. These effluent limitations were maintained along with daily monitoring for each parameter of concern. It is expected that each batch will be sampled, everyday, until the storage tank is emptied. Then, the transfer of wastewaters from one of the four tanks in the treatment system to the storage tank will proceed again, with the process of aerating, toxicity testing, and effluent sampling being repeated. The permitted flow was reduced from 0.4 MGD to 0.20 MGD as proposed by the consultant. Proposed changes to the permit: • The permit will be issued for a period of one year. Kings Mountain Venture is expected to remove, seal and /or eliminate Outfall 001 after wastewaters from tanks AT 1, PC 2, ET 3, and SC 4 are transferred to the 400,000 gallon storage tank and discharge is completed. • Sections A.(1.) OCPSF Subpart I monitoring and A.(4.) Nutrient Special Condition (BMP Evaluation) were removed from the permit since textile dye operations at the facility have been terminated. • All the sample types have been changed to grab samples. Effluent samples shall be representative and taken after aeration or completion of treatment. It is recommended that samples be taken from the middle level of the center column of the storage tank. • Special condition, A. (3) Color Permitting Requirements, has been modified to clarify that effluent and stream samples be taken during discharge periods. • Effluent monitoring for Total Phenolics, PAHs, Sulfates, Chlorides, Total Phosphorus, Total Nitrogen, and Color have been increased to daily or whenever a discharge occurs. • Upstream and downstream monitoring has been reduced to 1/week during discharge periods. • The Supplement to Permit Cover Sheet has been modified to identify the transfer of wastewaters to the 400,000 gallon storage tank for treatment and discharge to South Fork Catawba River. • Flow measurement was changed to instantaneous. Since the effluent will be pumped to Outfall 001 the pumping rate along with documentation on the duration of time wastewaters are pumped can be used to determine Flow volume reported on the Discharge Monitoring Reports (DMRs). Note that the Permittee may use a recording device if perferred. • After the wastewaters are aerated, two 24 hour acute toxicity tests: one using Ceriodaphnia dubia and a second using Fathead minnow (Pimephales promelas), shall be performed. Each batch of wastewater can be discharged via Outfall 001, if both tests pass, demonstrating no significant acute mortality at 90% effluent for invertebrates and vertebrates. See Section A. (2.) ACUTE TOXICITY MONITORING in the permit. • Pumping of wastewaters from the tanks to the 400,000 gallon storage tank shall cease at 1- 2 feet above the sludge level in all four tanks. Page 3 Version: December 3, 2012 NPDES PERMIT FACT SHEET Kings Mountain Venture #1, LLC Page 4 NPDES No. NC0005274 The Permittee will be required to notify the DWQ/Surface Water Protection Section at the Mooresville Regional Office 48 hours prior to discharge to allow for their inspection or observation of the wastewater discharge. All sludge and wastewaters associated with the sludge will be disposed of in accordance with state and federal regulations. Any wastewaters resulting from sludge dewatering will not be discharged via Outfall 001. Proposed Schedule for Permit Issuance Draft Permit to Public Notice: October 24, 2012 (est.) Permit Scheduled to Issue: December 17, 2012 (est.) State Contact If you have any questions on any of the above information or on the attached permit, please contact Julie Grzyb at (919) 807-6389. NAME: DATE: 4e2 — K. -/pi, Regional Office Comments MRO No comments - Wes asked to have consultant give him a call AGENCY REVIEWS & COMMENTS NO COMMENTS RECEIVED, US EPA REGION IV CONCURRENCE FROM BRITT SETZER, DWR RECEIVED ON 10-29-2012 Page 4 Version: December 3, 2012 VI4 L/ 15-d .7 PUBLIC NOTICE AFFIDAVIT OF INSERTION OF ADVERTISMENT North Carolina Environ- mental Management Commission/NPDES Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Notice of Intent to Issue a NPDES Wastewater Permit The North Carolina Envi- rcnmental Management Commission proposes to issue a NPDES waste- water discharge permit to the person(s) listed below. Written comments regard- ing the proposed permit will be accepted until 30 days after the publish date of this notice. The Director of the NC Division of Water Quality (DWQ) may hold a public hearing should there be a signifi- cant degree of public inter- est. Please mail comments and/or information re- quests to DWQ at the above address. Interested persons may visit the DWQ at 512 N. Salisbury Street, Raleigh, NC to re- view information on file. Additional information on NPDES permits and this notice may be found on our w e b s i t e. http://portal.ncdenr.org/we or by caging (919) 807-6390. Kings Mountain Venture #1, LLC requested renewal of permit NC0005274 for its facility in Gaston County; this permitted dis- charge is treated process/ stormwater to South Fork Catawba River, Catawba River Basin. The Gaston Gazette Gastonia, N.C. 3aston County the Gaston Gazette does certify that the advertisement for: NOTICE OF INTENT TO ISSUE NPDES WASTEWATER PERMIT: Kings Mountain ✓enture #1, LLC Vleasuring 5.94 inches appeared in The Gaston Gazette, a newspaper published in 3aston County, Gastonia, N.C., in issue(s): 10/27/2012 kisbuY' 1C-October27,2012. Name of Account: NCDENR/DWQ/NPDES text GS522836 to 56654Order Number: 54522836 Ad Number: 54593059 Sworn to, and subscribed before me this 29 th day of October. 2012. Carla Norris Potter, Notary Public My Commission Expires Sept.14, 2013 DENR-:DATER QUALITY POINT SOURCE BRANCH ATA NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Charles Wakild, P. E. Dee Freeman Governor Director Secretary MEMORANDUM To: From: Subject: 06q c,:.nofect/ October 29, 2012 Setzer, Britt (britt.setzer@ncdenr.gov) NCDENR / DWR / Regional Engineer Mooresville Regional Office Julie Grzyb NPDES Unit Review of Draft NPDES Permit NC0005274 Kings Mountain Venture #1, LLC Gaston County Please indicate below your agency's position or viewpoint on the draft permit and return this form by November 30, 2012. If you have any questions on the draft permit, please contact me at (919) 807-6389 or e- mail Julie.grzyb@ncdenr.gov. RESPONSE: (Check one) Concur with the issuance of this permit provided the facility is operated and maintained properly, the stated effluent limits are met prior to discharge, and the discharge does not contravene the designated water quality standards. Concurs with issuance of the above permit, provided the following conditions are met: Opposes the issuance of the above permit, based on reasons stated below, or attached: Signed 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Location: 512 N. Salisbury St. Raleigh, North Carolina 27604 Phone: 919-807-63001 FAX: 919-807-6492 Internet: www.ncwaterauality.orq An Equal Opportunity t Affirmative Action Employer Date: /0 Z 9 / 2 - NorthCarol.ina ,7Vatura!!j Table 1 - Yorkshire Americas WWTP Summary of Analytical Results H&H Job No. IPP-001 • Tank 4 Tank 3 Tank 2 Tank 1 Upper Middle Low Upper Middle Low Upper Middle Low Upper Middle Low SC-4A 1/5/2010 SC-4B 1/5/2010 SC-4C 1/5/2010 ET-3A 1/5/2010 ET-3B 1/5/2010 ET-3C 1/5/2010 PC-2A 1/5/2010 PC-2B 1/5/2010 PC-2C 1/5/2010 AT 1A 1/5/2010 AT-1B 1/5/2010 AT-1C 1/5/2010 4-Methyl 2-pentanone ug/L 7.1 7 8.2 BRL BRL BRL 7.8 8.5 7.8 !3RL BRL BRL Acetone ug/L BRL BRL BRL BRL BRL BRL 20 22 20 BRL BRL BRL Benzene ug/L 4.3 4.2 4.4 BRL BRL MI 8.9 9.7 8.8 11 10 10 Carbon Disulfide ug/L 5.2 5.3 5.8 BRL BRL BRL 11 13 11 Mil BRL BRL Chlorobenzene ug/L BRL BR1. BRL BRL BRL BRL 1.5 1.5 1.5 BRL BRL BRL Ethylbenzene ug/L BRL BRL URI_ BRL BRL BRL 1.4 1.4 1.3 BRL BRL BRL m,p-xylenes ug/L BR_ BRL BRL BRL BRL BRL 5.3 5.5 5.5 3.1 3 2.9 Toluene ug/L 3.9 3.8 3.9 BRL BRL BRL 2.8 3 2.8 4.2 4 4 3&4 Methylphenol ug/L liiti BRL BRL BRL URL BRL BRL BRL BRL 190 BILL BRL Total PAHs ug/L BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL Chromium JJ JJ EEEEE BRL BRL BRL BRL BRL 0.012 BRL BRL BRL BRL 0.0054 BRL Copper BRL BRL 0.013 0.015 0.017 0.57 BRL BRL BRL 0.085 0.11 0.097 Lead BRL BRL ri;l. BRL BRL BRL BRL BRL BRL BRL BRL BRL Nickel BRi BRL BRL BRL BRL BRL 0.013- 0.012 0.013 0.01 0.01 0.011 Zinc BRL BRL BRL 0.036 0.037 0.058 0.031 BRL BRL BRL BRL BRL BOD-5 mg/L 75 74 78 14 14 15 91 91 95 29 27 28 • Total Cyanide mg/L 0.013 0.017 0.015 0.074 0.040 0.072 0.0053 0.0087 0.0074 0.024 0.025 0.023 Nitrate as N mg/L 0.16 0.17 0.17 <0.10 <0.10 <0.10 0.22 0.23 0.23 0.25 0.23 0.24 Total Phenolics mg/L 0.41 0.26 0.72 0.072 0.072 <0.050 0.1 0.16 0.2 0.2 0.59 0.35 Phosphorous Total mg/L 2.8 3 3 0.44 0.43 0.72 3.8 3.8 3.9 4.3 4.4 4.4 Kjeldahl Nitrogen mg/L 36 39 40 28 28 31 75 81 34 82 34 36 Total Nitrogen mg/L 36 39 41 28 28 31 75 81 34 83 35 36 Total Suspended Solids mg/L <25 <25 38 <25 <25 74 <25 <25 <25 <25 <25 <25 pH 6.94 7.13 7.13 8.81 . 7.94 7.88 7.21 7.27 7.11 7.89 7.45 7.37 Temperature °C 8.27 7.71 8.35 5.85 6.51 6.46 6.02 6.25 6.69 7.21 7.35 7.49 Conductivity uS/cm3 4033 4107 4105 2915 2927 2910 5165 5248 5317 5780 5782 5782 Dissolved Oxygen mg/L 0.48 0.41 0.41 2.33 1.52 1.42 0.86 0.75 0.58 1.09 1.29 0.80 Notes: BRL= Below Reporting Limits ug/L = Micrograms Per Liter mg/L:= Milligrams Per Liter °C = Degrees Celcius uS/cm3 = Microseimens per cubic centimeter Kings Mountain Venture REASONABLE POTENTIAL ANALYSIS NC0005274 Qw (MGD) = 0.20 1Q10S(cfs)= 100.25 7Q10S(cfs)= 123.00 7Q10W(cfs)= 200.00 30Q2 (cfs) = 310.00 Avg. Stream Flow, QA (cfs) = 798.00 Receiving Stream: South Fork Catawba River WWTP/WTP Class: IWC @ 1Q10S = 0.31% IWC @ 7Q10S = 0.25% IWC@7Q1OW= 0.15% IWC@30Q2= 0.10% IWC@QA= 0.04% Stream Class: WS-V Outfall 001 Qw = 0.2 MGD CHRONIC TEST N/A ASSIGN 90% ACUTE TEST PARAMETER APE (1) STANDARDS & CRITERIA (2) PQL UNITS REASONABLE POTENTIAL RESULTS RECOMMENDED ACTION NC WQS / Applied '/ FAV / Chronic Standard Acute n H Det. Max Pred Cw 2,743.2 Allowable Cw Total Phenolic Compounds NC 3O;) A(30Q2) u:J1_ 12 11 Acute: NO WQS _ _- Chronic: 300,000.0 No value > Allowable Cw No RP, Predicted Max < 50% of Allowable Cw - No Monitoring required __________________________ Chromium NC 50 FW(7Q10s) 1022 ug/L 2 2 Note: n < 9 Limited data set 88.7 Default C.V. Acute: 329,677.4 _ _ Chronic: 20,000.0 No value > Allowable Cw No RP. Predicted Max < 50% of Allowable Cw - No Monitoring required Copper (AL) NC 7 FW(7Q10s) 7 ug/1. 7 7 Note: n <_ 9 Limited data set 2,018 Dcfault C.V. Acute: 2,354.8 _ _ _ Chronic: 2,800.0 No value> Allowable Cw No RP , Predicted Max a 50% of Allowable Cw - Action Level standard, WET testing will be performed to determine wastewater toxicity Cyanide NC 5 FW(7Q1Os) 22 10 ut_/I, 12 12 310.8 Acute: 7,096.8 _ _ Chronic: 2,000.0 No value> Allowable Cw No RP, Predicted Max < 50% of Allowable Cw - No Monitoring requlred __________-_ Nickel NC 25 WS(7Q10s) 261 ug/L 6 6 Note: n <_ 9 Limited data set 49.7 Default C.V. Acute: 84,193.5 _ _- Chronic:10,000.0 No value > Allowable Cw No RP, Predicted Max < 50% of Allowable Cw- No Monitoring required Zinc (AL) NC 50 FW(7Q10s) 67 ug/L 4 4 Note: n < 9 Limited data set 274.9 Default C.V. Acute: 21,612.9 _ _- Chronic_20,000.0 No value> Allowable Cw No RP, Predicted Max < 50% of Allowable Cw - No -_-_-_ _ _ _-_ Monitoring required Nitrate as N NC 10 WS(7Q10s) mull 12 9 0.56500 Acute: NO WQS _ _ Chronic: 4000.00000 No value > Allowable Cw No RP, Predicted Max < 50% of Allowable Cw - No Monitoring required Page 1 of 1 2011 RPA-FreshwaterKMV.xlsm, rpa 10/17/2012 REASONABLE POTENTIAL ANALYSIS USE ONLY "PASTE 8 USE ONLY "PASTE 9 USE ONLY "PASTE Total Phenolic Compounds SPECIAL- Chromium SPECIAL- Copper P P ( AL ) SPECIAL - Date Data BDL=1/2DL Results Values" WITH "COpy" Date Data BDL=1/2DL Results Values" WITH "COPY" Date 1 2 3 4 5 6 7 8 9 10 11 12 13 Data Values" WITH BDL=1/2DL Results "COPY" 13 13 Std Dev. 198.6604 15 15 Mean 129.5714 17 17 C.V. (default) 0.6000 570 570 n 7 85 85 110 110 Mult Factor = 3.54 97 97 Max. Value 570.0 ug/L Max. Pred Cw 2017.8 ug/L 1 2 3 4 5 6 7 8 9 10 11 12 13 12 5.4 12 Std Dev. 5.4 Mean C.V. (default) n Mult Factor = Max. Value Max. Pred Cw 4.6669 8.7000 0.6000 2 7.39 12.0 ug/L 88.7 ug/L 1 410 410 Std Dev. 217.3573 2 260 260 Mean 263.2500 3 720 720 C.V. 0.8257 4 72 72 n 12 5 72 72 6 50 25 Mult Factor = 3.81 7 100 100 Max. Value 720.0 ug/L 8 160 160 Max. Pred Cw 2743.2 ug/L 9 200 200 10 200 200 11 590 590 12 350 350 13 2011 RPA-FreshwaterKMV.xlsm, data 2 - 10/15/2012 REASONABLE POTENTIAL ANALYSIS 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Total Phenolic Compounds Date Data 1 410 260 720 72 72 50 100 160 200 200 590 350 BDL=1/2DL Results 410 Std Dev. 260 Mean 720 C.V. 72 n 72 25 Mult Factor = 100 Max. Value 160 Max. Pred Cw 200 200 590 350 USE ONLY "PASTE SPECIAL - Values" WITH "COPY" 217.3573 263.2500 0.8257 12 3.81 720.0 ug/L 2743.2 ug/L Chromium Date Data BDL=1/2DL Results 1 12 12 Std Dev. 2 5.4 5.4 Mean 3 C.V. (default) 4 n 5 6 Mult Factor = 7 Max. Value 8 Max. Pred Cw 9 10 11 12 13 14 USE ONLY "PASTE SPECIAL - Values" WITH "COPY" 4.6669 8.7000 0.6000 2 7.39 12.0 ug/L 88.7 ug/L 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Copper (AL) Date Data 1 13 15 17 570 85 110 97 BDL=1/2DL Results 13 Std Dev. 15 Mean 17 C.V. (default) 570 n 85 110 Mult Factor = 97 Max. Value Max. Pred Cw USE ONLY _ "PASTE SPECIAL - Values" WITH "COPY" 198.6604 129.5714 0.6000 7 3.54 570.0 ug/L 2017.8 ug/L -1- 2011 RPA-FreshwaterKMV.xlsm, data 10/15/2012 19 Nitrate as N Date Data 1 2 3 4 5 6 7 8 9 10 11 12 13 14 0.16 0.17 0.17 0.1 0.1 0.1 0.22 0.23 0.23 0.25 0.23 0.24 BDL=1/2DL 0.16 0.17 0.17 0.05 0.05 0.05 0.22 0.23 0.23 0.25 0.23 0.24 Results Std Dev. 0.0786 Mean 0.1708 C.V. 0.4599 n 12 Mult Factor = Max. Value Max. Pred Cw USE ONLY "PASTE SPECIAL. - Values" WITH "COPY" 2.26 0.250000 mg/L 0.565000 mg/L REASONABLE POTENTIAL ANALYSIS 2011 RPA-FreshwaterKMV.xlsm, data - 2 - 10/15/2012 REASONABLE POTENTIAL ANALYSIS 10 USE ONLY "PASTE 15 USE ONLY "PASTE 18 USE ONLY "PASTE Cyanide SPECIAL- Nickel SPECIAL- Zinc (AL) SPECIAL - 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Date Data 13 17 15 74 40 72 5 9 7 24 25 23 BDL=1/2DL 13 17 15 74 40 72 5 5 5 24 25 23 Results Std Dev. Mean C.V. n Mult Factor = Max. Value Max. Pred Cw Values" WITH "COPY" 23.9716 26.50 0.9046 12 4.20 74.0 ug/L 310.8 ug/L 1 2 3 4 5 6 7 8 9 10 11 12 13 14 BDL=1/2DL 13 12 13 10 10 11 Results Std Dev. Mean C.V. (default) n Mult Factor = Max. Value Max. Pred Cw Values" WITH "COPY" 1.3784 11.5000 0.6000 6 3.82 13.0 ug/L 49.7 ug/L 10 11 12 13 14 BDL=112DL 36 37 58 31 Results Std Dev. Mean C.V. (default) n Mult Factor = Max. Value Max. Pred Cw Values" WITH "COPY" 11.9583 40.5000 0.6000 4 4.74 58.0 ug/L 274.9 ug/L Date Data 13 12 13 10 10 11 Date 1 2 3 4 5 6 7 8 9 Data 36 37 58 31 -1- 2011 RPA-FreshwaterKMV.xlsm, data 10/15/2012 IWC Calculations Facility: Kings Mountain Venture NC0005274 Prepared By: Julie Grzyb Enter Design Flow (MGD): Enter s7Q10 (cfs): Enter w7Q10 (cfs): 0.15 123 200 Total Residual Chlorine (TRC) Daily Maximum Limit (ugll) s7Q10 (CFS) DESIGN FLOW (MGD) DESIGN FLOW (CFS) STREAM STD (UG/L) Upstream Bkgd (ug/I) IWC (%) Allowable Conc. (ug/l) Fecal Coliform Monthly Average Limit: (If DF >331; Monitor) (If DF<331; Limit) Dilution Factor (DF) 123 0.15 0.2325 17.0 0 0.19 9011 Ammonia (Summer) Monthly Average Limit (mg NH3-N/I) s7Q10 (CFS) DESIGN FLOW (MGD) DESIGN FLOW (CFS) STREAM STD (MG/L) Upstream Bkgd (mg/I) IWC (%) Allowable Conc. (mg/I) Ammonia (Winter) Monthly Average Limit (mg NH3-N/I) w7Q10 (CFS) got Required DESIGN FLOW (MGD) DESIGN FLOW (CFS) STREAM STD (MG/L) 530.03 Upstream Bkgd (mg/I) IWC (%) Allowable Conc. (mg/I) Total Residual Chlorine 1. Cap Daily Max limit at 28 ug/I to protect for acute toxicity Ammonia (as NH3-N) 1. If Allowable Conc > 35 mg/I, Monitor Only 2. Monthly Avg limit x 3 = Weekly Avg limit (Municipals); capped at 35 mg/I 3. Monthly Avg limit x 5 = Daily Max limit (Non-Munis); capped at 35 mg/I 4. BAT for Minor Domestics: 2 mg/I (summer) and 4 mg/I (winter) 5. BAT for Major Municipals: 1 mg/I (year-round) 123 0.15 0.2325 1.0 0.22 0.19 413.6 200 0.15 0.2325 1.8 0.22 0.12 1360.9 Fecal Coliform 1. Monthly Avg limit x 2 = 400/100 ml = Weekly Avg limit (Municipals) = Daily Max limit (Non -Muni) NPDES Server/Current Versions/WLA; TB 1/16/2009 NC 2010 Integrated Report Categories 4 and 5 Impaired Waters All 13,123 Waters in NC are in Category 5-303(d) List for Mercury due to statewide fish consumption advice for several fish species AU_Number AU Name AU_Description LengthArea AU_Units Classification Category Parameter Reason for Rating Use Category Collection Year 303(d)year Catawba River Basin Lower South Fork Catawba River Watershed 0305010206 Q 11-129-(15.5) South Fork Catawba From a point 0.4 mile upstream of Long River Creek to Cramerton Dam and Lake Wylie at Upper Armstrong Bridge 5 Low pH 18.1 FW Miles WS-V Standard Violation Aquatic Life 2008 2010 5 Turbidity Standard Violation Aquatic Life 2008 2008 NC 2010 Integrated Report Category 4 and 5 303(d) List EPA Approved Aug 31, 201 9/20/2010 Page 27 of 145 Catawba River Basin > AU Number Name 2012 North Carolina 303(d) List -Category 5 10-digit Watershed 0305010206 Description Lower South Fork of the Catawba River Length or Area Units Classification Category Rating Use Reason for Rating Parameter Year > 11-129-15-5 Mauney Creek From source to Hoyle Creek Category 4.4 FW Miles WS-IV 5 5 Impaired Aquatic Life Poor Bioclassification Ecological/biological Integrity Benthos 2000 12-digit Subwatershed 030501020603 > 11-129-(15.5) South Fork Catawba River From a point 0.4 mile upstream of Long Creek to Cramerton Dam and 18.1 Lake Wylie at Upper Armstrong Bridge Lower Long Creek FW Miles WS-V 5 Impaired Aquatic Life Standard Violation Turbidity 2008 5 > 11-129-16-(4) Long Creek From Mountain Creek to South Fork Catawba River 15.3 FW Miles C 5 5 Impaired Aquatic Life Standard Violation Turbidity 2012 > 11-129-16-7b Dallas Branch From Dallas WWTP to Long Creek 0.8 FW Miles C 5 Impaired Aquatic Life Fair Bioclassification Ecological/biological Integrity Benthos 1998 Catawba River Basin Catawba River Basin 8-digit Subbasin 03050103 10-digit Watershed 0305010301 5 Catawba River Sugar Creek 12-digit Subwatershed 030501030104 Irvins Creek > 11-137-9a McAlpine Creek (Waverly Lake) From source to SR 3356, (Sardis Rd) 8.5 FW Miles C 5 5 Impaired Aquatic Life Fair Bioclassification Ecological/biological Integrity Benthos 1998 12-digit Subwatershed 030501030102 Little Sugar Creek > 11-137-8a Little Sugar Creek From source to Archdale Rd 11.6 FW Miles C 5 Impaired Aquatic Life Standard Violation Copper 5 Impaired Fish Consumption Standard Violation Water column Mercury 2008 2010 5 Thursday, March 29, 2012 For EPA Review Submitted March 30, 2012 Page 34 of 177 Safe-T-raining and Environmental Services PO Box 735 Emmaus PA 18049 Phone: 610-432-1180 Cell: 484-634-0948 May 9, 2012 Julie Grzyb NC DENR 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Revised Kings Mountain Venture NPDES permit renewal application Julie: In follow up to our many conversations, enclosed are three copies of the revised Kings Mountain Venture permit application for NPDES Permit # NC0005274. Some additional steps will need to be taken at the Kings Mountatin Venture site in Lowell, North Carolina related to the discharge of the wastewater from the site. Tentative plans are to transfer the wastewater to a 400,000 gallon storage tank on site where the water will be aerated for approximately eight hours. Once the aeration is completed and a Dissolved Oxygen of greater then 5.0 is reached the water will be discharged at the predetermine rate which is outlined below along with the estimated volume of wastewater in each tamk. The proposed discharge rate and total volume of the tanks is as follows: • AT 1 -Discharge rate of 200,000 gallons/day with a volume of approximately 750,000 gallons • PC 2 - Discahrge rate of 150,000 gallons/day with a volume of approximately 564,000 gallons • ET 3 - Discharge rate of 200,000 gallons/day with a volume of approximately 994,000 gallons • SC 4 - Discharge rate of 150,000 gallons/day with a volume of approximately 205,000 gallons Total discharge amount of wastewater to be discharged is approximately 2,500,000 gallons The discharge will continue for approximately 120 days based on proposed flow rates, water transfer activities from tank to tank and the aeration activities associated with the discharge. Sludge which is present in all of the tanks will be addressed separately after the discharge is complete but the estimated volume of the sludge in the tanks is approximately 1,500 cubic yards. If you have any questions or require additional clarification on any of the information enclosed in this application, please contact me at (484) 634 — 0948. Sin Stephen Timm Safety\Environmental Director Safe-T-raining and Environmental Services titMOVLEL MAY 1 1 2012 DENR-WATER QUALITY POINT SOURCE BRANCH Grzyb, Julie From: safetytraining©rcn.com Sent: Tuesday, August 14, 2012 1:57 PM To: Grzyb, Julie Subject: Question #4 (Sludge Handling) Good Afternoon, Julie. After speaking with the client, some different options related to disposal of the dewatered sludge are currently being evaluated by the client. But before I discuss the disposal options, the first step after the majority of water is discharged, the client would hire an outside contractor to vacuum the remaining free water from the top of the sludge. This water would transported and disposed of off -site. Once the free water is removed, the sludge would be then transported to one of the contained concrete pad areas where it would be spread to dry in the sun. If rain is expected the sludge would be covered to minimize any contact with the storm water. Once the sludge is dried, the sludge material would be either land applied at the site after the necessary permits are obtained or the material would be taken off site for disposal in a approved land fill. Please let me know if you have any questions related to the managment of the sludge as oultined above at the KMV site. You can reach me at 484-634-0948. Thanks ---- Original message ---- >Date: Tue, 7 Aug 2012 20:38:19 +0000 >From: "Grzyb, Julie" <iulie.grzyb(ancdenr.gov> >Subject: KMV permit >To: "safetytraininarcn.com" <safetytrainingOrcn.com> > Stephen, > I have several questions regarding the KMV > application: > 1) Did you run any toxicity tests on the > wastewaters? Can you scan and send me the results. > 2) For the analytical tests run on the > wastewaters (upper, lower, and middle sections of > the vats), can you send me a copy of the lab results > - looking for the pages that identify the > quantitative levels (detection levels) and the EPA > test method or procedure. For example, I need to > know what test method was used for phenols >-420.1,420.4 or 625 and the actual BDL value - > quantitative level. > 3) Do you have any analytical tests results on > color (ADMI units) or turbidity (NTU) from the > upper, lower, and middle sections of the vats? > 4) You state that the sludge will be addressed > separately. First, what steps will be taken to > prevent sludge from being discharged to the storage > tank?Identify the trigger that will stop the pumping > of wastewaters from the vats to the storage tanks > (ie. turbidity = 25 NTUs). Second, KMV must identify > what action will be taken with the sludge (ie. how > will it be tested and disposed of). 1 > > > > Please call if you have any questions. Please > respond within two weeks. > > Julie > > > > > > Julie A. Grzyb, Environmental Engineer > > NC DENR / Division of Water Quality / Surface Water > Protection Section > > NPDES Complex Permitting, Point Source Branch > > 1617 Mail Service Center, Raleigh, NC 27699-1617 > > 919/807-6389 (wk); 919/807-6495 (fax) > > > > **Please note, my email address has changed to > -iulie.grzybPncdenr.Rov > > > > E-mail correspondence to and from this address may > be subject to the North Carolina Public Records law > and may be disclosed to third parties. > > 2 Grzyb, Julie From: Grzyb, Julie Sent: Tuesday, August 07, 2012 4:38 PM To: 'safetytraining@rcn.com' Subject: KMV permit Stephen, I have several questions regarding the KMV application: 1) Did you run any toxicity tests on the wastewaters? Can you scan and send me the results. 2) For the analytical tests run on the wastewaters (upper, lower, and middle sections of the vats), can you send me a copy of the lab results — looking for the pages that identify the quantitative levels (detection levels) and the EPA test method or procedure. For example, I need to know what test method was used for phenols -420.1,420.4 or 625 and the actual BDL value - quantitative level. 3) Do you have any analytical tests results on color (ADMI units) or turbidity (NTU) from the upper, lower, and middle sections of the vats? 4) You state that the sludge will be addressed separately. First, what steps will be taken to prevent sludge from being discharged to the storage tank?Identify the trigger that will stop the pumping of wastewaters from the vats to the storage tanks (ie. turbidity = 25 NTUs). Second, KMV must identify what action will be taken with the sludge (ie. how will it be tested and disposed of). Please call if you have any questions. Please respond within two weeks. Julie Julie A. Grzyb, Environmental Engineer NC DENR / Division of Water Quality / Surface Water Protection Section NPDES Complex Permitting, Point Source Branch 1617 Mail Service Center, Raleigh, NC 27699-1617 919/807-6389 (wk); 919/807-6495 (fax) **Please note, my email address has changed to julie.. rzvlX ncdenr.kov E-mail correspondence to and from this address may be subject to the North Carolina Public Records law and may be disclosed to third parties. i Grzyb, Julie From: Grzyb, Julie Sent: Wednesday, February 15, 2012 7:01 PM To: 'safetytraining@rcn.com' Subject: RE: Kings Mtn. Venture application Attachments: Limits.xlsx Stephen, Since the previous permit was protective of the stream and whatever you propose will be at a significantly lower discharge rate than 0.400 MGD which is what the permit was based on, assume that if you can meet the limits in the current permit you will be okay. For instance, current permit has a BODS Monthly average of 123 lbs/day. If for instance, you plan to discharge at 0.002 MGD (not 0.400 MGD) than 0.002 MGD X 8.34 x 95 mg/L (worst case) = 1.58 lb/day -the limit would be met. For the OCPSF Subpart I parameters (see 40 CFR 414.90) see the attached file. If you can meet all the concentrations listed in red or the pounds/day in columns under Daily Max and Monthly avg. than you will not have a problem since these numbers are either Federal Guidelines or based on Water Quality Standards using the significantly higher discharge flow of 0.400 MGD. I will have to recalculate numbers when you decide on a max discharge rate but if you are under these numbers you should not have a problem. This was the fastest way to answer your question. Your last question - " Next, I was wondering if you could provide me some information on Narrative Standard that is outlined under the Freshwater Aquatic Life Section. How can I obtain limits for this Standard. " What parameter are you referring to? Again, to issue this permit we need the General Forms, updated vat volumes and diagrams submitted along with a proposed discharge rate and a commitment that this project will be completed within a year. This is a major permit and will require EPA approval, however, with a set time commitment we hope EPA will find the permit acceptable given the unusally circumstances and the fact that this is a Brownfield site. Also, a description of how the solids in the bottom of the vats will be handled is needed as well. Please call if you have questions, Julie Original Message From: safetytraining@rcn.com [mailto:safetytraining@rcn.com] Sent: Friday, February 03, 2012 2:37 PM To: Grzyb, Julie Subject: RE: Kings Mtn. Venture application Hello Julie. I hope all is well. Two questions as I create the concentration table for the Kings Mountain Venture Site. One question was how do I handle if there is no concentration limit listed for a chemical that is outlined in the facility's present permit pertaining to its categorical classification example would be Acenaphthylene. Next, I was wondering if you could provide 1 me some information on Narrative Standard that is outlined under the Freshwater Aquatic Life Section. How can I obtain limits for this Standard. Thanks and I will await your response. Have a nice weekend. ---- Original message ---- >Date: Wed, 25 Jan 2012 20:46:39 +0000 >From: "Grzyb, Julie" <julie.grzyb@ncdenr.gov> >Subject: RE: Kings Mtn. Venture application >To: "safetytraining@rcn.com" <safetytraining@rcn.com> >Cc: "Belnick, Tom" <tom.belnick@ncdenr.gov>,"Krebs, Rob" ><rob.krebs@ncdenr.gov> >Stephen, > I am glad you will be meeting with Kings Mtn. Venture. The original application is over three years old and was incomplete (no data was submitted). Please go ahead and revise the Form 1 General portion of this application. This is the portion that was attached in the last email. >Also, Kings Mountain Venture must clearly state in a cover letter what they are asking an NPDES permit for, time period, discharge flow rate, and the exact location of the discharge point. It should be clearly stated that no operations or additional wastewaters are being produced at this facility and that the permit is being requested in order to dispose of remaining wastewaters left from..., etc. We will need three copies of all the information (two more copies of the data submitted on 1-18- 2012 are needed as well). Up to date diagrams, tank volumes, etc. are necessary. >The Mooresville Regional Office will be reviewing the information along with NPDES. >Please call if you have any questions, >Julie > Original Message >From: safetytraining@rcn.com [mailto:safetytraining@rcn.com] >Sent: Tuesday, January 24, 2012 8:39 AM >To: Grzyb, Julie >Subject: Re: Kings Mtn. Venture application >Good Morning, Julie. Hope you had a nice weekend. I am planning to have a meeting with the owners of King's Mountain Venture site this week to discuss your the different questions outlined in your email. >Take Care and I will be in touch next week. >---- Original message »Date: Fri, 20 Jan 2012 17:03:53 +0000 »From: "Grzyb, Julie" <julie.grzyb@ncdenr.gov> 2 »Subject: Kings Mtn. Venture application »To: "safetytraining@rcn.com" <safetytraining@rcn.com> »Cc: "Belnick, Tom" <tom.belnick@ncdenr.gov> » Stephen, » I just wanted to let you know that we received the » data for Kings Mtn. Venture. » The original application included Form 1 General » information with tank volumes and a diagram. » Please review the originally submitted information, » which is an attached file, and verify whether it is » still correct. If'it is not, you must revise and » resubmit the information. Also, what is the » timeframe needed for Kings Mtn. Venture to discharge » these wastewaters and at what flow rate? This » application can not be processed without this » information. » Sincerely, » Julie » DWQ logo » Julie A. Grzyb, Environmental Engineer » NC DENR / Division of Water Quality / Surface Water » Protection Section » NPDES Complex Permitting, Point Source Branch » 1617 Mail Service Center, Raleigh, NC 27699-1617 » 919/807-6389 (wk); 919/807-6495 (fax) 3 » » **Please note, my email address has changed to » .julie.grzyb@ncdenr.gov » » » » E-mail correspondence to and from this address may » be subject to the North Carolina Public Records law » and may be disclosed to third parties. » »Form 1 Generall.pdf (11516k bytes) 4 Grzyb, Julie From: Grzyb, Julie Sent: Wednesday, October 26, 2011 9:46 AM To: Gore, Deborah Subject: RE: Kings Mountain Ventures discharge Thanks for looking into it. From: Gore, Deborah Sent: Wednesday, October 26, 2011 7:43 AM To: Grzyb, Julie Subject: FW: Kings Mountain Ventures discharge FYI — wish it was better news for you O From: Lesley, John Sent: Tuesday, October 25, 2011 3:09 PM To: Gore, Deborah Cc: Krebs, Rob; Bell, Wes Subject: Kings Mountain Ventures discharge The City of Lowell has denied Kings Mountain Ventures request to discharge wastewater to the Lowell WWTP according to Ben Blackburn, City Manager. The City decided that their first responsibility was to protect the WWTP from potential damage and noncompliance and that their cost recovery was not sufficient. Kings Mountain Ventures has offered to do more studies etc. but so far there is no agreement. JL John Lesley -Johnlesley@ncdenr.gov North Carolina Dept. of Environment & Natural Resources Div. of Water Quality 610 E. Center Ave., suite 301 Mooresville, NC 28115 Switchboard: (704) 663-1699 Direct line: (704) 235-2198 Fax: (704) 663-6040 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties unless this content is exempt by statute or other regulation. i /0— I —c f Leh S p f /t- op L, G . -11 ov ,r A v l� v%'l e . ?'" ,Grzyb, Julie From: Grzyb, Julie Sent: Wednesday, October 21, 2009 6:10 PM To: 'safetytraining@rcn.com' Cc: Bell, Wes Subject: Kings Mountain Venture NPDES permit renewal Stephen, Thank you for calling yesterday. I will look forward to hearing from you on when additional information will be submitted regarding Kings Mountain Venture's permit renewal. Specifically, items needed include: a request for a stormwater discharge outfall, timeline, drainage area map, stormwater GC/MS sampling data a wastewater characterization of each of the process wastewaters to be discharged, treatment to be provided, and the estimated discharge rate(s). I was glad to hear that you have collected much of this data already, please call if you have any questions. Also, Tony Chiarella has called and left a message that the legal Department is sending a letter authorizing you to represent the company for the permit renewal. Hopefully, that will be received shortly. Julie Julie A. Grzyb, Environmental Engineer NC DENR / Division of Water Quality / Surface Water Protection Section NPDES West, Point Source Branch 1617 Mail Service Center, Raleigh, NC 27699-1617 919/807-6389 (wk); 919/807-6495 (fax) **Please note, my email address has changed to julie.JrzVlancdenr.Rov E-mail correspondence to and from this address may be subject to the North Carolina Public Records law and may be disclosed to third parties. i .Grzyb, Julie From: Grzyb, Julie Sent: Monday, October 19, 2009 3:32 PM To: 'safetytraining@rcn.com' Subject: Kings Mountain Venture permit renewal Stephen Timm, The current application for Kings Mountain Venture is incomplete and can not be processed without additional information. The best time to reach me is tomorrow, Tues. 10-20, from 9 am to 10:30 am on my cell at 336-210-8454, I would appreciate hearing from you. If you can not call at that time please let me know a time you can call either tomorrow or Wed. and I will make myself available. The only appointment I have is on Tues. from 11:30 am to 1:30 PM and again it would be best to call my cell if you call before or after the appointment times. I will be back in the DWQ office on Wed. at 9:30 am and can be reached either on my cell or my office number (919-807-6389). Thanks and I'II look forward to hearing from you, Julie Grzyb Julie A. Grzyb, Environmental Engineer NC DENR / Division of Water Quality / Surface Water Protection Section NPDES West, Point Source Branch 1617 Mail Service Center, Raleigh, NC 27699-1617 919/807-6389 (wk); 919/807-6495 (fax) **Please note, my email address has changed to julie.grzVbnncdenr.gov E-mail correspondence to and from this address may be subject to the North Carolina Public Records law and may be disclosed to third parties. 1J- icf'°5 Tb� / 61 I; 4 t S' J ` 4‘0 { (ek ,1offfc j 4-1,4x± ley 1 r SOC PRIORITY PROJECT: No To: Western NPDES Unit Surface Water Protection Section Attention: Gil Vinzani Date: February 2, 2009 NPDES STAFF REPORT AND RECOMMENDATIONS County: Gaston NPDES Permit No.: NC0005274 PART I - GENERAL INFORMATION Physical Address 1. Facility and address: Kings Mountain Venture #1 LLC 1602 Main Street 17 A Marlen Drive Lowell, NC 28098 Hamilton, NJ 08691 2. Date of investigation: January 22, 2009 3. Report prepared by: Michael L. Parker, Environmental Engineer II 4. Person contacted and telephone number: Stephen Timm, WWTP consultant (484) 634- 0948 5. Directions to site: The site is located at 1602 North Main Street in the Town of Lowell. 6. Discharge point(s): Latitude: 35 ° 17' 13" Longitude: 81° 06' 13" USGS Quad No.: F14SE 7. Receiving stream or affected surface waters: South Fork Catawba River a. Classification: WS-V b. River Basin and Subbasin No.: Catawba 030836 c. Describe receiving stream features and pertinent downstream uses: Downstream uses are primarily agriculture and secondary recreation (the receiving stream is large enough to support swimming, however, swimming is not considered a frequent use of these waters at the point of discharge). PART II - DESCRIPTION OF DISCHARGE AND TREATMENT WORKS 1. a. Volume of wastewater: The applicant proposes to discharge s• 0.200 MG of wastewater/storm water until the existing tankage is empty. This flow will not be on a daily basis, but as needed. b. What is the current permitted capacity: 0.400 MGD Page Two d. Description of existing or substantially constructed WWT facilities: The existing WWT facility was at one time used as treatment for a dye manufacturing operation. After the plant closed, many of the existing tankage and appurtenances were vandalized, so they are incapable of operating as they were originally intended. In this renewal, the applicant plans to modify an existing equalization tank to effect a batch type treatment for the remaining wastewater held in the WWTP's existing tankage (see Part IV below). Available treatment will include: pH adjustment, flocculation, coagulation, mixing, chemical precipitation, and settling. e. Description of proposed WWT facilities: There are no proposed WWT facilities. f. Possible toxic impacts to surface waters: Toxicity testing is required by the current permit. 2. Residual handling and utilization/disposal scheme: Residuals will be removed as necessary and taken to a private landfill for disposal. 3. Treatment plant classification: Class IV (based on components that presently exist at the site). 4. Compliance Background: None for the current facilities. PART III - OTHER PERTINENT INFORMATION 1. Special monitoring or limitations (including toxicity) requests: None at this time. 2. Important SOC/JOC or Compliance Schedule dates: This facility is neither under an SOC nor is one being considered at this time. 3. Alternative analysis evaluation: There is no known alternative to a discharge at this time. The nearest municipality (Town of Lowell) has insufficient hydraulic capacity. PART IV - EVALUATION AND RECOMMENDATIONS The applicant, Kings Mountain Venture #1, LLC (KMV) is requesting renewal of the subject permit. KMV purchased the property and assets of what was formally Yorkshire Americas, who closed operations several years ago. When the plant was closed, the WWTP was shut down without the removal of any of the wastewater or residuals. Subsequent to the plant's closure, the buildings and WWTP were vandalized, which rendered the WWTP incapable of functioning without a significant expenditure. In addition, rainwater co -mingled with the wastewater in the various tanks adding to the quantity of contaminated water on -site. KMV purchased the site in 2008 and has plans to remove the existing tankage so the site can be put up for sale. Page Three Given the fact that the WWTP is incapable of operating as was designed, the new owners and their WWTP consultant are proposing to utilize a portion of the existing tankage to set up a batch type treatment process that will allow KMV to remove the wastewater/storm water from the remaining tanks and discharge this water to the receiving stream under the effluent limitations contained in the current permit. Each of the tanks described in the application will be dewatered and pumped to the final "treatment tank", which will be equipped to provide the necessary levels of treatment to achieve compliance with the current permit limitations. Plans are to discharge up to 0.002 MGD, however, actual flow will be determined based on settleability rates and effluent quality. In conversations with KMV staff, it was pointed out to them the difficulty of promulgating effluent limitations based on current site conditions, and an inconsistent waste stream. Furthermore, since this is a one-time dewatering event and there are no plans by KMV to utilize these WWT facilities in the future, there is really no need for this permit to be renewed provided KMV can effectively treat and discharge the remaining wastewater/storm water under the effluent limitations contained in the current permit (due to expire 6/30/2009). KMV staff have been advised of this matter and have indicated a desire to get the "treatment tank" ready to accept and treat the water stored in the remaining tanks prior to the subject permit's expiration. Although it is possible that the state of the current economy may put constraints on how quickly the site dewatering can be accomplished, KMV staff have expressed a willingness to do whatever is necessary to get the existing tankage dewatered prior to permit expiration. If this can be accomplished, there will be no need for permit renewal and it can be allowed to expire and removed from the Division's records. Signature of Report Preparer Water Quality Regional Supervisor h:ldsr\dsr091kingsmtn.doc Date Safe-T-raining and Environmental Services December 26, 2008 Mrs. Dina Sprinkle NC DENR/DWQ Point Source Branch 1617 Mail Service Center Raleigh, NC 27699 Re: Renewal of NPDES Permit NC0005274 PO Box 735 Emmaus PA 18049 Phone: 610-432-1180 Cell: 484-634-0948 JAN 2 2009 Mrs. Sprinkle: Enclosed is the renewal application for NPDES Pernut NC0005274 for the facility located in Lowell, NC. The facility is currently a shutdown dye manufacturing operation. The existing wastewater treatment plant that was used under normal operations has been vandalized and is no longer operational in its present condition. Tentative plans are being developed to use the empty southern equalization tank which has an approximate volume of 400,000 gallons to treat the remaining waste water onsite. Each remaining tank that contains wastewater will be treated individually or handled as a batch type treatment process in the southern equalization tank. Prior to treatment, samples will be gathered at different water levels with in the tank to be treated through bench scale analysis. Once a recipe is determined, the wastewater to be treated will be pumped to the southern equalization tank for full scale treatment. The estimated volume of the remaining waster water on -site is as follows: • AT 1- approximately 633,000 gallons • PC 2 — approximately 275,000 gallons • ET 3 — approximately 993,509 gallons • SC 4 - approximately 93,949 gallons • Totaling approximately 2,000,000 gallons (Details provided in application). All treated wastewater will be discharged through Outfall 001 and will not exceed approximately 200,000 gallons a day which is a reduction in flow from the present permit flow limit of 400,000 gallon per day. In addition to treating the remaining wastewater on -site, the southern most equalization tank will be used to capture any storm water that may come in contact with the site during demolition activities and cleaning operations of the buildings during future demolition of the buildings onsite. Lastly, Outfall 002 will be terminated since it has been historically associated with non contact cooling water at the site. If you have any questions concerning this application please contact me at 484-634-0948. Stephen Timm Safety Training and Environmental Services Please print or type in the unshaded areas only (lit! -in areas are spaced for elite type. i.e.. 12 charactersliinch1. For Approved OMB No. 2040-0086 Approval expires 5-31-92 ' . FORM U.S. ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. NUMBER INFORMATION F T,A 1GENERAL Consolidated Permits Program NCD04444475 D GENERAL 1 (Read the "General instructions" before starting.) j 2 13 14 15 LABEL ITEMS GENERAL INSTRUCTIONS I. EPA I.D. NUMBER If a preprinted label has been provided. affix it in the designated space. Review the Information carefully; if any of it is III. FACILITY NAME incorrect, cross through i1 and enter the correct data in the appropriate fill-in area --- below. Also, if any of the preprinted data is V. FACILITY MAILING LIST absent (the area to the left of the label PLEASE PLACE LABEL IN THIS SPACE space lists the information that should appear), please provide it in the proper fill - i ��9 in area(s) below. If the label is complete r'. Cand correct, you need not complete Items 1 I. III, V, VI(except VI-B VI. FACILITY LOCATION . . t . • and which must be Completed regardless). Complete all items if no label has been proved. Refer to the instructions for detailed item descriptions and for the legal authorization under which this data is collected. II. POLLUTANT CHARACTERISTICS ' UCT O.( : omplete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer "yes" to any questions, you must submit this form and the supplemental from listed in the parenthesis following the question. Mark "X" in the box In the third column if the supplemental form is attached. If you answer "no" to each question. you need not submit any of these forms. You may answer "no" if your activity is excluded from permit requirements: see Section C of the instructions. See a so, Section D of the instructions for definitions of bold-faced terms. MARK "X" MARK'X" SPECIFIC QUESTIONS YES NO FORM ATTACHED SPECIFIC QUESTIONS YES NO FORM ATTACHED A. Is this facility a publicly owned treatment works which results in a discharge to waters of the U.S.? (FORM 2A) ❑ gq ga ❑ 8 Does or will this facility (either existing or proposed) include a concentrated animal feeding operation or aquatic animal production facility which results in a discharge ❑ ❑ 18 17 18 to waters of the U.S.? (FORM 2B) 19 20 21 C. Is this facility which currently results in discharges to waters of the U.S. other than rf�i �d ❑ ❑ D. Is this proposal facility (other than those described in A or B above) which will result in a discharge ❑ 7 'ES 0 those described in A or B above? (FORM 2C) 22 23 24 to waters of the U.S.? (FORM 2D) 25 26 27 E. Does or will this facility treat, store, or dispose of hazardous wastes? (FORM 3) ❑ E ❑ F. Do you or will you inject at this facility industrial or municipal effluent below the lowermost stratum containing. within one quarter mile of the well bore, underground sources of drinking water? ❑ 1133 is 28 29 30 (FORM 4) 31 32 33 G. Do you or win you inject at this facility any produced water other fluids which are brought to the surface in connection with conventional oil or natural gas production. infect fluids used for enhanced recovery of oil or natural gas, or inject fluids for storage of liquid hydrocarbons? ❑ a� ❑ H. Do you or will you inject at this facility fluids for • special processes such as mining of sulfer by the Frasch process. solution mining of minerals, in situ combustion of fossil fuel. or recovery of geothermal energy? (FORM 4) • 1 ❑ (FORM 4) 34 35 36 37 38 39 I. Is this facility a proposed stationary source which is one of the 28 industrial categories listed in the instructions and which will potentially emit 100 tons per year of any air pollutant regulated under the Clean Air Act and may affect or be ❑ [�]� tii ❑ J. Is this facility a proposed stationary source which Is NOT one of the 28 industrial categories listed in the instructions and which will potentially emit 250 tons per year of any air pollutant regulated under the Clean Air Act and may affect ❑ ❑ located in an attainment area? FORM 5 40 41 42 or be located in an attainment are? (FORM 5) 43 44 45 111. NAME OF FACILITY c S SKIP Kings Mountain Venture #1, LLC 15 16-29 30 69 IV. FACILITY CONTACT A. NAME & TITLE (last, first. & title) B. PHONE (area code 8 no.) 1586 2 Tony Chiarella, Director of Operations 609 i 8004 15 16 45 46 48 49 51 52 55 V. FACILITY MAILING ADDRESS A. STREET OR P.O. BOX C 3 17 A Marten Drive 15 16 45 B. CITY OR TOWN I C. STATE D. ZIP CODE I ~ Hamilton— 1 NJ 08691 15 16 40 41 42 47 51 I VI. FACILITY LOCATION A STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER c 5 1602 Main Street i5 16 45 B. COUNTY NAME Gas_tnn_ 4b 70 C. CITY OR TOWN D. STATE E. ZIP CODE F. COUNTY CODE I c 6 Lowell NC 1 1 28098 15 18 40 41 42 1 47 51 52 54 I EPA FORM 3S10-1 1tl-'Ittt CUNT IN('El) ON REVERSE CONTINUED FROM TI•IE FRONT •VII. SIC CODES (4-digit, in order of priorry) Efrain • A. FIRST c 1 (specify) 9999 1 5. 1 128651r—i Cyclic Organic Byes and Pigs >;t.+� 15 C. THIRD c I (specify) 15 ,s 17 1 NA VIII. OPERATOR INFORMATION c1 s" Stephen Tlmm/Safety Training and Environmental Services 1a iv C. STATUS OF OPERATOR (Enter the apatopriafe letter into the answer box: if "Other." specify.) D. PHONE (area code. & no.) F = FEDERAL M = PUBLIC (other than leuerar or stare) (specify) C ' ' If a?r: a .. 13. SECOND (specify) Nonclassiible Establishments D. FOURTH (specify) NA 55 1 P T P PRIVATE : B. Is ihe name listed in lien VI II -A also the owner? ❑ YES NO S = STATE o = OTHER (,pec,ry) Consultant A f 484 ; ` 634 ! 0948 15 _ r s t S ` 19 . 21 22094285 1 2 � E. STREET OR PO BOX PO Box 735 F. CITY OR TOWN Emmaus 5 15. X. EXISTING ENVIRONMENTAL PERMITS A. NPDES (Discharges to Surface Water) 9 I N 1-1 NC0005274 15 1 IC 1.17 113 - - B. UIC (Underground injection of Fluids c 7 1 16 ! 17 171 C. RCRA (Hazardous wastes) C T 1 s R 15 16 17 1 16 55-1_ G. STATE H. ZIP CODE I IX. INDIAN LAND PA 7 18049 Is We facility located on Indian lands? _ TH ❑ YES NO D. `.,d PSD (Air Emissions burn Proposers Sources) • 9 1 P 30 I 15 ( 16. i 17 NA 31; NA Xl. MAP 9 15 [11i_, 1;i:a E. OTHER Ls/NY/AL_ rTrir:j NA 9 i . NA E. OTHER (specify) 15 1 16 17 NA 30 (Specify) (Specify) Attach to this application a topographic map of the area extending to at least one mile beyond propertyboundaries. The map must show the outline of the facility, me iocation of each of its existing and proposed intake and discharge structures, each of its hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. include all springs, rivers and other surface water bodies in the ma area See instructions for •recise re•uirements. XII, NATURE OF BUSINESS (provide a brief..descri•iion) The facility is a shutdown dye manufacturing operation in Lowell, NC. The existing wastewater treatment plant that was used under norrhal operations has been vandalized and is no longer operational in its present condition. Tentative plans are to use the empty southern equalization tank which has an approximate volume of 400,000 gallons to treat the remaining waste water onsite. Each remaining tank that contains wastewater will treated individually. Prior to treatment, samples will be gathered at differentwateraevels with in the tank to be treated through bench scale analysis. Once a recipe is determined, probably a combination of flocculent and coagulant chemicals, the wastewater to be treated will be pumped to the southern equalization tank For fitll.scate tregtnjent. The' estimated volume of the remaining waster water on -site is as follows: • AT 1- approximately 633,000 gallons • PC 2 — approximately 275,000 gallons • ET 3 — approximately 993,509 gallons • SC 4 - approximately 93,949 gallons • Totaling approximately 2,000,000 gallons. (See Attached Sheet) JAN 2 2009 In addition to treating the remaining wastewater on -site, the southern most equalization tank will be used to capture any storm water that may come in contact with the site during future demolition of the buildings onsite. XIi . CERTIFICATION (see instructions) I certify under penalty of lair that 1 have. personally examined and am familiar with the information submitted in this application and all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in the application. t believe that the information is true, accurate and complete. 1. am aware that there are significant penalties for submitting false information including the_possibility of fine and imprisonment. A. NAME & OFFICIAL TITLE (type or print) f B. Si RE C. DATE SIG>�IED Tony Chiarella COMMENTS FOR OFFICIAL USE ONLY -C-. PORrI 35t0-1 " 39� i SIN 17'30" Latitude: 3517'13" Longitude: 81"06' 13"- Quad# F14SE Stream Class: WS-V Subbasin: 30S36 Receiving Stream: South Fork Catawba River ( ,. •r' t • NC0005274 Yorkshire Americas, Inc. • • �\ t J Wastewater Treatment Area o% e- I - Jti4;‘) weo tfr-4-5 '3 —3 "•ee`j (pc. - Z. ) I. a 1 ' 1 ~ eVk 1 1 1 rp2c-cis J ie:nA LCS. MUMAER(.uG>iuci /los 1 .-,l: o: nl t); rc nts Appreved. f_1MO tuu 2O4O- X1E# . Approval expires 3-31 ev•l Clause print or vrni :r, cn13 r U11.433Cy ulcr 1r-� — TM L. •_ - MtsN!UFACT11ATN(3, .� � -....�.. ,."�••�= ,.„.,�-. ,.at --••••.at-.-...� PROTECTION AGENCY PERM T TO DISCHARGE WASCEWATER MINING AND SlLVIC{.fi, r•i.iRAl_ iOPERATiONS :''''. - _ 3 rIW r.i1ii 71.. :" LLn I . _ _ .+«:==av�suaar.+ra,;amrl +'.iP`W _ ..... .. pe S rOFIrt sup I i Lk ,,o1 L 44/Ez,,os.,l:ff_4 tui'A`L. :,,., LOCATION fi ^ � - U.S. ENVIRONMENTAL APPLICATION FUA COMMERCiAi., n^' ^(i• ?, I. OiJi'F'ALL . For each autfall, Iist the latitudeandlongitude of it; location to t u nearest 15 seconds and the name of the receiving water. A. O'UTFALL NUMUER fXI./ U. LATITUDE C. LONGITUDE 3-4, RECEIVING WAiCN (name) South Fork Catawba. Rive.r.___..-.._.________ ._..._._. 1. Oa.. t..IN. ). 113C. 1.1310 J. MIN. 3. fl[f_. 001 35 17 13 81 06 r 13 a II. ROWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES intake water, operations contributing wastewater to the affluent, item S. Construct a water balance on the line drawing by showing average cannot be determined fag., for certain mining activities), provide a or treatment measures. , e„ ch$d 1 A. Attach a line drawing showing the water flow through the facility. Indicate sources.of and treatment units labeled to correspond to the more detailed descriptions in Sows between Intakes, operations, ttreettnefst units, end airfoils. If 6 water balance pictorial description of the nature and amount of any sources of water and any collectian B. For each outfall, provide a description of: It) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, and storm water runoff; R2l The average flaw tomrihuted by each operation; and (3) The treatment received by the wastewater. Continuo on additional sheets if nocemary. t.0U7- r'ALLN ((Ell X. O RATtON(SI CONTRIBUTING rLow 3. TREATMENT a. orever.•ricsu Wit) b. AVERAGE FLOW (inducts uni40 a. DESCRIPTION . LIST cones FROM TA aLE 2C-1 001 All tanks contain a comb. Weather Treatment will be __-,-___1-G determined through bench _ 1-0 2-D 2-C of treated,untreated, Dependant storm water from past ing_but will 1-U o erations include possible pH i adjustment, -].osculation agud.1t L , , heroical precipitation and settling. . — -f -- - -t-- . _ _ a . - {PFIr5C2PL ig.: titsa ONLY (Thus e; ,rut liin ......-..-..".. . .......,,.,,..e.....� a &..1b-eFtagOraca) . _ _ .. -. - ...-o...zw........-, o„isevmowr.�w�oa..- A Farm 3510-20 WW1 CONTINUED FROM THE FRONT C. Except for storm runoff, leaks, or spills, are any of the discharpes described in items II -A or ©intorminent or seasonei7 f7 YES (complete the following rob'.) ONO (go ro Section Ill) �S 1. OUTFALL NUMBER (Jilt) 2. OPERATION(I) CONTRIBUTING FLOW (Iflt) 3. FREQUENCY 4. FLOW e. DAYS PER WEEK (specify average) b. MONTHS PER YEAR (specify average) a. FLOW RATE (in reed) b. TOTAL VOLUME (specify with unit.) c. DUR- N ATt yi (in days) I• I. ONO TIT RN Avennos -. nA,%IM UM ��. I.'o"D "INN v a. NxziN N vA LYu 001 TBD— 111. PRODUCTION A. Does an effluent [J Yes Outlined in Section IIA The facility can not determine since it is unable to determine treated wastewater. But, not discharge more then 2C0,000 activities. guideline limitation promulgated by EPA under (complete Item I1l•B) TBD the the It can gallons Section 304 TBD prese settability be assumed of the Clean TBD t rate the per day Water Act apply r]No (to to 0.2MGD of the rate of the facility ased ori to your Facility? Section IV) TBD discharge the past TBD will TBD B. P-e the limitations in the applicable effluent guideline expressed in terms of production (or ocher measure of operation)? (—Ives (complete Item Ill•C) R] NO (go to Section IV) C. If you answered yes- to Item III-B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the applicable effluent guideline, and indicate the affected outfalls. 1. AVERAGE DAILY PRODUCTION 2, AFFECTED OUTFALLS (list outfall numbers) a, QUANTITY Faw MAY b. uNIre or NaAsuw[ C. ION, .w ooucr, MArawu�, arc. (specify) NA IV. IMPROVEMENTS A. Are you now required water treatment equipment but is not limited to, or loan conditions. by any Federal, State or or practices or any other permit conditions, administrative yes ocal authority to meet any implementation schedule for the construction, upgrading environmental programs which may affect the discharges described in this application? or enforcement orders, enforcement compliance schedule letters, stipulations, (complete the following table) [4No (go to Item IV, B) or operation of waste• This includes, court orders, and grant 1, IDENTIFICATION OF CONDITION, AGNI[MENT, ETC. 2. AFFECTED OUTFALLS 2. BRIEF DESCRIPTION OF PROJECT 4. PIMA aVe. IReR[-O M Pi GYFRROO- [, NO, t1, SOW eC■ OF DIe CNA RI. It 8. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your dixharyes) you now have underway or which you, plan. Indicate whether each program is now underway or planned, and indicate your actual or Planned schedules for construction. OMANK "X" IF Dttscei TION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED a,• etre 361 O-2C (Rev. 2-85) PAGE 2 OF 4 CONTINUE ON PAGE 3 CONTINUED FROM PAGE 2 EPA I.D. NUMBER (copy from Item 1 of Form li NCD04444475 V. INTAKE AND EFFLUENT CHARACTERISTICS A, B, & C; See instructions before proceeding — Complete one set of tables for each outfall — Annotate the outfall number in the space provided. NOTE: Tables V-A. V-B, and V-C are included on separate sheets numbered V-7 through V-9. D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions, which you know or have reason to believe is discharged or may be discharged from any outfall. For evary pollutant you list, briefly describe the reasons you believe it to be present end report any analytical data in your • Possession. 1. POLLUTANT 2. SOURCE I. POLLUTANT 2. SOURCE No pollutnats outlined in Table 2C-3 are know to be present. VI. POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture es an intermediate or final product or byproduct? [_I Y ES ills( all sur)I pollutnnts below) [XNO (go to Item VI•B) PAGE' 3 OF .t CONTINUE ON REVERS' EPA Form 3510-2C (9-90) PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information on separate sheets (use the same format) instead of completing these pages. SEE INSTRUCTIONS. EPA 1.0. NUMOER (copy from Ikon 1 of Form 1) NCD04444475 V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2•C) table. Complete one table for each outfall. See instructions for additional OUT FALL NO 001 PART A • You must provide the results of at least one analysis for every pollutant in this details. 1. POLLUTANT 2 EFFLUENT 3. UNITS (sP. Ci(r if blank) 4. INTAKE (upr(unal) a. MAXIMUM DAILY VALUE MAXI ty��M 70 pAY VALUE �I/ ova la ble) a.LONG TERM AVRG VALUE 1 (it oua/fable) I d. n O. O F ANALYSES a. LONG AVERAGF TERM VALUE l�l .+was b. NO. OF ANALYSES a*THATICONCN- TF+ATION b. MASS til C4NCC NITRATION (e)Mwss (l) CaNCCNITN wT,OH III uAss Ill CONIC [NTa ATION (�I Mas+ jl .rr cONccNTnA r.ON a. Biochemical Oxyge(0D) Demand (eoD) Analys Y s will beperformed duringNextplanned 1 discharge g event at the facili- -Y b. Chemical Oxygen Demand (COD) c. Total Organic Carbon (TOG') d. TOtel Sufponded SOlids (TSS) a. Ammonia (as NI f- Flow VALUE VALUE VALUE VALVE Q. Temperature (winter) VALUE VALUE VALUE 'C VALUE h.T/mpRatura (mummer) VALUE VALUE VALUC oc VALVE i. nH MINIMUM MAXIMUM MINIMUM MAXIMUM STANDARD UNITS PART B - Mark "X•' in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe 10 be absent. If you mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that po lutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements- 1. POLLUT- ANT AND CAS NO. Of (refillable) 2. MARK'X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a• Ve, Rc� `seNT b. ae- ��.❑ sr.:". e. MAXIMUM DAILY VALUE b. MAXIMUM 10 OAY VALUE (1 ova a e) c.LONG TAR a a `G VALUE (,f ���J ENO. OF ANAL- YSES a. CONCEN• TRATION b,MASS a. LUNG TERM AVERAGE VALUE a NO OF ANAL. Il) cONIce Tw Ar,oN (') MAss ill cn,aca• cATIow I I MASS I') CONIC. NTTTT MN (rl �'' Ass CONS ArloN tr)MA[s R. Bromide (24959-67-9) b. Chlorine. Total Rasiduel c. Color d. Focal Collforrn a, Fluoride (181184-48-8 ) f. Nttrets-- Nllrttw (es N) EPA Form 3510 2C (8-90) PAGE V-1 CONTINUE ON REVERSE ITEM V-13.CONTINUED FROM tiv, P�ILLUT•3. NTAND NO._ (1/svapabl!) • Ea..MARK'X' EFFLUENT 4. UNITS 5. INTAKE (optional) a. as- Itvtotl�v�o ►wt- sew"' b, at -a. wa- ANT MAXIMUM DAILY VALUC b. MAXI '!Y VALUE ,nuc Q V�) C.t.or4-0, ot, f VALULr 1 d. No.oF ANAL- YSES e CONC6N• TRATION b. MASS a �,p�{. E T IXtCAB A1/EFTAGE 1�ALUC b. NO.OF ANAL- YSES Ili CONCtNT1�ATION IZ) w1Aft (1) CONCTTTTTTION (t) ma.' CONCTTTTTTION lol MASS (�) CONCtNTRATioN (1) MA9.s li; Nitrogen, T0tli;organic roiN analysis will be performed during next planned discharge event at the facility. h. 011 and Gramm 1. Phosphorus (ai P). Total (7723.14.0) I. Radioactivity (1) Alpha, Total (2) Beta, Total (3) Radium, Total (4) Radium 226. Total k. Sulfate (as SO4) (14806.79-8) I. Sulfide (as S) m. Sulfite ON SO3) 414265-45-3) .� n. Surfactants o. Aluminum, Total (7429-90.5) p. arum, Total (7440.39.3) q. Boron, Total (7440-42-8) r. Cobalt, Total (7440-48-4) a. Iron, Total (7439-89-6) 1 L Magnaslum, Total (7 439-95.4) '" u. Molybdenum, Total (7439.88.7) v. TMianrfanesa, Total (7439.96.6) t ti- w. Tin. Total (7440.31-5 ) x. Titanium. Total (7440-32-5) EPA Form 3510.2C (8-90) PAGE V-Z CONTINUE ON PAGE V -3 CONTINUED FROM PAGE 3 OF FORM 2-C - EPA I.D. NUMBER (copy from Item 1 of Form I) NCD4444475 OUTFALL NUMBER 001 PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outtalk, and nonrequired GC/MS fractions'. mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant -If you mark column 2b for any pollutant, you must provide the results of at (east one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b. you must either submit at (east one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for additional details and requirements. 1. POLLUTANT AND CAS NUMBER (If available) 2. MARK •x• 3. EFFLUENT 4. UNITS 5. INTAKE (optional/ 'LT."' ma Rc- ou1R- EO b-••' LICVQOLIQV6C ♦Rc- ilNT a ••' Ae- satyr o. MAXIMUM DAILY VALUE b. MAXI M 3 D^ Y VALUE b! J ovaia Q C.LONG T M aVarn �(� VALUE ���7- V @ (=l MAff d, NO.OF ANAL ANAL- YSES a GONCeN- TRATION b. MASS \ e. LONG AVERAGE TERM VALVE (,I MASS b. HO.OF ANAL - YSES A (i) CONE CNTRATION (a) Ilwss CO coNcawrn AT1oN (,) MA1f 1 CONCENTRATION (I) CUNCBN• !RATION METALS, CYANIDE, AND TOTAL PHENOLS 1M. Antimony. Total (7440-36-0) Analylis will be performed during the next planned discharge event at the facility. 2M. Arsenic, Total (7440-38.2 ) 3M. beryllium, Total, 7440.41.7) 4M, Cadmium. Total (7440.43.9) SM. Chromium, Total (7440-47-3) 6M. Copper. Total (1440.50-8) 7M. Lead. Total (7439-92-1) OM. Mercury, Total (7439-97-6) 9M. Nickel, Total (7440-02-0) 10M. Selenium, Total (7782-49-2) 11M.Sliver, Total (7440.22.4) • 12M. Thallium, Total (7440.28.0) 13M. Zinc, Total (7440-66-6) 14M. Cyanide, Total (57-12-5) 16M. Phenols, Total DIOXIN 2,3,7,$-Tetra- chloredthem o-P- Dloittn (1764,01.6) DESCRIBE RESULTS EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (I QYO(IQ�Ia) a. MURK x• 3. EFFLUENT 4. UNITS 5. INTAKE (optional) aTUST�b► lea Itr• pea . at- Itvlto�levte ►wc- fRNT a et- ANT fRNT' a• MAXIMUM DAILY VALUE b. MAX IVIr 3A fAY VALUE auQ a1 c.LONG T M AA��[[�� VALUE �(�QV01lQblE�• BANAL-F VSES a CONCEN• TRATFON MASS a. LONG AVERAG (I) CONCUN- T //A71ae TERM VALUE (Z) MAfi b. NO.OF ANAL - YSs:S CONCt(TIIATIpN 1=I MArf caecaa...stae (_) MAff CONcaN4.1 TNAl10N (2) MA%I CMS FRACTION - VOLATILE COMPOUNDS le 07-022--8)ln Analysis will be performed during .he next planned discharge event at the facility. 2V. Acrylonitrlle (107-13-1) 3V. Bonzono (71.43-2) 4V. Ble (Chloro- rrrathyl) Ether (542.88.1 ) ~ 5V. Bromoiorm (75-26-2) ` 6V. Carbon Tetrachloride (56-23-5) 7V. Chlorobenzene 1108.90.7 ) 8V. ChlorodI. bromomothano (124.48.1) 9V. Chtoroethano (75-00-3) 10V.2-Chloro- othylvInyl Ether (110-75-8) 11 V. Chloroform (67-68-3) 12V. Dlehloro- bromomothano (75-27-4) 13V. Dlchloro- difluorometheno (75-71-8) 14V. 1,1-Dichioro- ethane (76-34-3) 16V. 1,2-13Ichloro- ethane (107-06-2) 18V. 1,1-Dlchtoro• ethylene (75-35-4) -,-- 17V. 1,2-Dichloro- propane 178-87.6) 18V.1,3-Dichloro- aomlene (&4Z•76-8) 19V. Ethylbenzene (100.41-4► 20V. Methyl Bromide (74-83-9) 21V. Methyl Chloride (74.87.3) EPA Form 3510.2c (6- PAGE V-4 CONTINUE ON PAGE V-t CONTINUED FROM PAGE V-4 1. POLLUTANT AND CAS NUMBER (ijauallable) 2. MARK •x• 3. EFFLUENT 4. UNITS - 5. INTAKE (optional) aTtaT• �Nq gvle- CO et- r:::; isnT Get- �A". siNT a, MAXIMUM DAILY VALUE b. MAXI M 3 aua p Y VALUE O @) b� c.LONG T M VALUE J�jt �j�(� (tfaWatloblQ�• Q NO.OF ANAL- YSES a. CONCEN• TRATION b. MASS a. LONG TERM AVERAGg VALUE b. ND.OF ANAL - Y$E$ I�1- CONCtNTNATION (31 Mwfs 'CONCRNTRA TION la) .rwst CONC[NT Ar10N (a) MAss (s) toNC[N- TRAT1pN {a) MMs GC/MS FRACTION — VOLATILE COMPOUNDS (continued) 22V. Methylene Chloride (75-09-2) Analysis lill be performed during the next planned discharge event at the facility. 23V. 1,1.2,2-Tetra- ch)oroethane (79-34-5 ) 24V. Tetrechloro- ethylene (127-18-4) 25V. Toluene (108.88-3) 26V. 1,2-Tram Olehtoroethylene (156-60.6) 27V. 1,1,1-TrI- chloroethane (71-55.0) 28V, 1,1,2-Tri- chIoro.thano (79.00.6 ) 29V. Trlchloro- ethylene (79-01-6) 30V. Trichloro- f luoromethane (75.69.4) —' 31V. Vinyl Chloride (75-01-4) GC/M9 FRACTION — ACID COMPOUNDS 1 A. 2-ChlorophenoI (95-57-8 ) • 2A. 2,4-D tch Toro. phenol (120-83-21 1' 3A. 2.4-D imethyl- phenol (100-67-91 4A. 4,6-Dinitro-O- Cresol (534-52-1) 5A. 2.4-0lnitro- phenol (51-28.5) OA. 2-Nltrophonol (88.75-5) 7A. 4-N Itrophenol (100-02-7) 8A. P-Chloro-M- Cr000l (59-50-7) 9A Pentechloro- phenor (87-86-5) 10A:.Phenol '.: Tri- nii of e I . .. . EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE • CONTINUED FROM THE FRONT I. POLLUTANT AND CAS NUMBER (if available) 2. MARK 'x' 3. EFFLUENT 4. UNITS 5. INTAKE (uptin,lal) dTc.T e on:. h ■c- eaeo�rwsr<c •t .; G •c• "ft* A. MAXIMUM DAILY VALUE R. MAX11M�M 3 DAY VALUE t apal a CJ (i (( bl C.LONG Y M VALUE }� AA{{[(�� JoDatlRble� tt NO.OP ANAL- YSES a. CONCEN TRATION b. M ASS a. LONG AVERAGE TERM VAt,UE It) .6.6. b. NO.OF ANAL YSES 1.1 {s) rlwaf CONCt NTw ATION 111 cOOCtoT..w T,o•• (:1 ..A�! 1�1 CDoc[NTMATION 14 .AA.• 1.I coot•••• TawiroN GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS 18.Acenaptlthene (83-32-9) Analysis will be performed during the next planned discharge event at the facility. 28. Acenaphtylene (208-96-8) 3B. Anthracono (120-12-7) r 4B. Benzidine (92-87-5) 1 5B. Benzo (a) Anthrecene (56-55-3) J .• 813. Benzo (a) Pyrene (50-32-8) 78. 3,4-Bonzo- lluoranthene (205-99-2) 88. Benzo (Phi) Perylene j 191.24-2) 98. Benzo (k) F luo►anthene (207.08-9) 108. Ells (2-Chloro- etthory) Methane) (111.91-1) '"'—""' 11 B. Biz (2-Chtoro- ethyl) Ether (111-44-4) 7 7 128. BIS 2-Chloroiso• p Etter (102-50-I) 138. Biz (2-Ethyl- heryl) Phthalate (11741-7) _ 149, 4-8rarno- phprwl Phenyl .Eth. (101.65-3) 15B. Butyl Benzyt Phthillata (80.68-7) 116Sv3-Chioro- taiens 1.785541-7CChlofo- PbiatiitPhenyl • Blite t.1005.72.3) 'i88 Chrysane 121841-9) 19B..D1benzo (a,h) ;Anthrecane (53-70-3) 200. 1,2-Dlchloro- benzene (95-50-1) I218. 1,3-Dichloro- benzene (541-73-11 EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7 CONTINUED FROM PAGE V-8 i. POLLUTANT AND CAS NUM6ER (ltaValialNe) 2. MARK .x• • 3. EFFLUENT 4. UNITS 5. INTAKE (lepriunol) arra' /Mf. w.- :A.-, AO b..r- �t►ay.okl.va ewe.• 17 4i ere•b. q w�- ..MT a. MAXIMUM DAILY VALVE MAXIMUM 3. Dte7 VALUE (iiaua►+able C.LONG T jtM atta AVRG. VALUE a e ct. NO.OF ANAL, TSES a. CONCEN- TRATIgN b. MASS n. LONG AVERAGE TERM VALUE (,) .Ast b. NO.OF ANAL- V SES Ili Is) ma CONC. ref w ATION 111 0) .wwsa CONC k WIN arsond (/) CVNC.NTNATIOM lel s.Ass ( 1 cal«et«• TNA TION GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued, R �0I I �a Ar.alylis will be performed during the next planned discharge event at the facility. -238. 3,3'-D ich loro- t lgtl[[dlns (9.144L1) P lste (0466.2) '22 41:!PRgthyl -~— -- •' b)-N-ButylAi"741at-21 .27,8. 2.4-DInItro- talu.rto_(121-14-2) . • 288. 3.8-DInitro- toluen. (606-20-2) '298. D1-N-Cctyl Phthelst. (117.84-0) 308.1.2.Otphenyi- hydrssin. (as Aso- &Asy tt) (122.66-71 l 318. Fluorsnthene (206.440) 328. Ptuoren. (86-73-7 ) 338, li chbtobentene (1i8•74-I) 348. H sxs- chlorobutadlsne (87-68-3) 358. Hexechloro- cyclopentadtene (77-47-4) 368. Hexechloro- sthan. (67-72-1) 378.Indeno (1.2.3•cd) Pyrana (193-39-5) 388. lsophorone (78-59-1) 398. Naphthalene (91-20-3) 4013. Nitrobenzene (98-95-3) 418. N-Nitro- sodlmethylamina (62-75-9) 428. N-N(trosodi- N-Propylamine (621-64-7) ► _ EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER ((javafJoblc) Z. MARK •x• 3. EFFLUENT 4. UNITS 5. INTAKE (optional) arctr «c wt• on;- ra b es' a►Rvtoa►evsr, ►wt• •a«r _ C •c' a. MAXIMUM DAILY VALUE b. NIAXIIy�.IM 30 pqY VALUE (1lCuWfablsJ c.LONC TFRM tai VALUe (Y/auaiiab[e?' d NO.OF ANAL VSES A. CONCEN• TRATION MASS MASS r LONG TERM VALVE fo1 ..wit b.No.Or gNAL• ySES w�• tt«r (►) (sl Mass co«c►«rwwr►o« (►I O'.CYN►NAr►OM (r) watt I'I CO..fcNviaAIION l•l mast Isi CO"CC.. ATION GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) 438. N-Nitro- wdlphenylemtne (8&30-8) Analysis will be perf ormec during the next rlanned discharge event at the facility. 449.Phenanthrono (85-01.8 ) 468. Pyrene (1 29-00-0) 488. 1,2,4 - Tr I- chlorobenzeno (13043-1) , GCIM$FRACTlON — PESTICIDES fP.`,d ein (30910-2) 2P. Q4BHC (319.84.8) 3P. NC (31 -7) 4P. -t3HC (68-89-9) 5P. a-BHC (319-86-8) - 6P. Chlordane (57-74-9) 7P. 4,4'-DOT (60.29.3) 8P. 4,4'-DOE (72-68-9 ) 9P.4,4'-OD0 (72-64.8 ) 10P. Dieldrin (60.87-1) • 11P. a-Endosulfen (115-29.7) 12P. j3-Endosulfen (115.29-7) 13P. Endosulfen Sulfate (1031-07-8) 14P. Endrin (72-20-8) 15P. Endrin Aldehyde (7421-93-4) 16P. Heptachlor (76-44-8) ♦ EPA Form 3510-2C (8.90) PAGE V-8 CONTINUE ON PAGE V-9 CONTINUED FROM PAGE V-B EPA I.O. NUM2to r o4m741em 1 o/Form 1JJOUTF161 NUMBER 1. POLLUTANT AND CAS NUMBER (!/auo!!abl�J 2. MARK 'x• 3. EFFLUENT 4. UNITS 5. INTAKE Optional) n*"�T Ma wll• oulw- b' •w' LIQVeacsaveD •wk. ITN _ Cow- ww- 0. MAXIMUM DAILY VALUE b. MAXi M s b Y VALUE ,)1 p p ova a —�--} ER AYFt�. C.LONG T(_f M )lab VALUE t aua cIb. NO.OF ANAL-b- YSES i. CONCEN- TRATION MASS a_ LONG AVERAGE TERM VALUE (fI MA•• NO.OF ANAL. YSES •!NT ('I CONCLNTRATION (//i MASI III tONCtNTNAfION (t) ..wtl! _ (f) CONCwNTwATION 1,1 NA~r' 1 cVNt.N• ( ) c."CN GC/MS FRACTION — PESTICIDES (continued) 17P. Heptachlor Epoxide (1024-57.3) Analysis will be preformed during the next planned discharge event at the facility. 18P. PCB-1242 (53469-21-9 ) 19P. PCB-1254 (11097.69.1) 20P. PCB-1221 (11104-28.2) y • 21P. PCB-1232 (11141.16.5) I 22P. PCR-1248 (12672.29.6) 23P. PC9-1260 (11098-82.5) 24P. PC8-1016 (12674.11-2 ) 25P. Toxepliene (8001-36-2) V -9 :PA Form 3510-2C (8.90) CON(trlUED F41O1,4 T}3E FRONT itii. BlotaFr At TXECTY T oIESTING DATA A Co you hove any knowledge or reason to bl.te.e that any biological test for rt._to o chronic toxicity has been made on any of your discharges or on a 3 reoeivin{j water in relation to your discharge w:7hi the Last 3 yrafs? * A Chronic Toxicity Definitive with Ceriodphnia was performed on September 15, 2008 to determine the quality of water in the equalization tank prior to discharge. Thel water passed the iFst 1 * A Chronic TElxicity Pass/Fail with Ceriodaphnia dubia was performed for compliance 1 against the facility's current permit when the ' water in the 400,000 gallon tank was discharged in the months of November and December. The water passed the testa III.CONTRACT ANALYSIS INFORMATION Vero any of the analyses reported in Item V performed by a contract laboratory or eon;:Jting firm? Yes Mgt the name, nddr. &, and telephone number of and put(utanhe unal>. ec/ b+-, each euCI: kfhonrtory or Jinn below) A. NAME Analysis to be performed at a later time once wastewater is treated and ready for discharge. E. AOORE55 i jNO (go to Section IX) EL6TH UUNE i-5t-CirrAfR Ts ANALY'TI?p (area:oded no. IX,CCEFlTIFICATION • Ark 1 certify under penalty of law that this document end all attachments were prepared under my direction or supervision ire accordance with a system designedto a assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person Of persons who manage the system or those persons directly responsible forgathering the information, the information submitted is, to the best of my knowledge and belief, (rue, accurate, and complete. ! am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knnw,nq violations A. I./Am!: a Of, ICIAf Trrt.l' U t'tIONI: 1,1:1 ., .. Tony Chiarella, Director of Operations EPA Korn, 3510-2C {8-90) PAGE SOFA 609- 586-8004 i Z - l -- 08 1 4 Form Approved. OMB No. 2040-0086. Please print or type In the unshaded areas only. , FORM U.S. ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. NUMBER GENERAL INFORMATION s VA c 1 &EPA Cansoifdated Permits Program "General/nstrucnons" F NCD04444475 ❑ GENERAL (Read the before starting.) 1 2 12 N 13 LABEL ITEMS GENERAL INSTRUCTIONS If a preprinted label has bean provided. affix it in the designated space Review the information carefully: If any of it I. EPA I.D. NUMBER is incorrect, cross through It and enter the correct data in the appropriate fill-in area below. Also, if any of the preprinted data III. FACILITY NAME PLEASE PLACE LABEL IN THIS SPACE is absent (the area to the let of the label space lists the information that should appear), please provide it in the proper fill -In area(s) below. If the label Is complete and correct, you V. FACILITY MAILING ADDRESS need not complete Items I, III, V, and VI (except Vl•B which must be completed regardless). Complete all Items if no label has been provided Refer to the Instructions far detailed item VI. FACILITY LOCATION II. POLLUTANT CHARACTERISTICS INSTRUCTIONS: Complete A through submit this form and the supplemental you answer "no" to each question, instructions. See also, Section D J to determine whether you need to submit any permit application forms to the form listed in the parenthesis following the question. Mark 'X" in the box in the you need not submit any o these forms. You may answer "no" if your activity is excluded of the instructions for definitions of boldfaced terms. descriptions and for the legal authorizations under which lids data is collected. EPA. If you answer "yes' to any questions, you must third column if the supplemental form is attached. If from permit requirements; see Section C of the Mark 'X' Mark 'X' SPECIFIC QUESTIONS YES NO FORM mcH ED ATTACH SPECIFIC QUESTIONS vas NO FORM H ATTACHED A. Is this facility a publicly owned treatment works which results in a discharge to waters of the U.S.? (FORM 2A) X 8. Does or will this facility (either existing or proposed) include a concentrated animal feeding operation or aquatic animal production facility which results in a 15 Ir le discharge to waters of the U.S.? (FORM 28) la 20 21 C. Is this a facility which currently results in discharges to waters of the U.S. other than those described in A or 8 2C) X D. Is this a proposed facility (other than those described in A or B above) which will result in a discharge to waters of the U.S.? 2D) X above? (FORM 22 z2 2, (FORM 25 23 2? E. Does or will this facility treat, store, or dispose of hazardous wastes? (FORM 3) X F. Do you or will you inject at this facility industrial or municipal effluent below the lowermost stratum containing, within one quarter mile of the well bore, X 23 23 20 underground sources of drinking water'? (FORM 4) 21 22 23 G. Do you or will you inject at this facility any produced water or other fluids which are brought to the surface in connection with conventional ell or natural gas production, inject fluids used for enhanced recovery of oil or natural gas, or inject fluids for storage of liquid hydrocarbons? X H. Do you or will you inject at this facility fluids for special processes such as mining of sulfur by the Frasch process, solution mining of minerals, in situ combustion of fossil fuel, or recovery of geothermal energy? (FORM 4) X (FORM 4) s, 35 za 22 2a 2a I. Is this facility a proposed stationary source which is one of the 28 industrial categories listed in the Instructions and which will potentially emit 100 tons per year of any air pollutant regulated under the Clean Air Act and may affect X J. Is this facility a proposed stationary source which Is NOT one of the 28 industrial categories listed in the instructions and which will potentially emit 250 tons per year of any air pollutant regulated under the Clean Air Act �/ X or be located in an attainment area? (FORM 5) .2 it Q and may affect or be located in an attainment area? (FORM 5) 0 ii 6 III c 1 NAME SKIP OF FACILITY Kings Mountain Venture .1, LLC M ra - 1a 2a 62 IV FACILITY CONTACT A. NAME & TITLE (fast, first, & title) B. PHONE (area code & no.) 111111111111111.1111.11111111111 ,,y Ton Chiarella, Director oerations( III III 0 ) 5 6-B 04 fi i5 H 1a I H 21 i St- 22 V.FACILTY MAILING ADDRESS A. STREET OR P.O. BOX 3 1a 1 1 1 I 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 17 A Marten Drive 5 I ,i 45 B. CITY OR TOWN C. STATE D. ZIP CODE a Hamilton I I I l l l l l l l l l l l l l l l l l NJ 0861 1 1 IS la ii it Q IT 51 VI. FACILITY LOCATION A. STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER 5 ( iti0I 1 ainl Strelet 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 12 la .2 B. COUNTY NAME Gaston 1 I I I I I I I t 1 1 I I I ( i I I I I I ri 70 C. CITY OR TOWN D. STATE E. ZIP CODE F. COUNTY CODE ([known) s Lb i 1i 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Z�C 2�097 1 1 I I 15 li ,G Al 22 AT al i2 l •_.. .31..0 .•_ f'� EPA Form 3510-1 (8 90) ChNT)NUE 'ON'R {J�L7gJ ��7} W is i MAY 1 1 2012 1 L- fr V DENR-WATER QUALITY 1 POINT SOURCE BRANCH CONTINUED FROM THE FRONT VII. SIC CODES 4-di.it, in order of .,ion A. FIRST B. SECOND 7 2 1 1 I (specify) cyclic organic dyes and Pigments 1 ? 9999 (spec fNonclassialsle Entabl ishment 15 1e • 19 ,! ,e• 19 C. THIRD D. FOURTH c 11 I (spec')NA 7 I I I (speciP}rA 15 16 • 19 15 16 19 VIII. OPERATOR INFORMATION A. NAME B. Is the name listed In Item c III 1 1 1 1 1 1 1 1 1 1 II 1 I 1 1 I I 1 1 1 I 1 1 I 1 I I 1 I 1 1 I 1 1 1 alStephen Timm/Safe-T-raining and Environmental Services VIII-A also the owner? ❑ YES ®NO 5 (10 55 6e C. STATUS OF OPERATOR (Enter the appropriate letter into the answer box: tf "Other," specify) D. PHONE (area code & no.) F = FEDERAL M=PUBLIC (other tfianfederal orstate) S=STATE O= OTHER (specify) P = PRIVATE P (specify) consultant = 1 1 1 1 1 1 1 1 1 A (484) 634-0948 5e 15 a • mils • 01 173 - >D E. STREET OR P.O. BOX P( boX 17315 l i l l i l l i l l l( I I l l l l l l l l l l 16 es F. CITY OR TOWN G STATE H. ZIP CODE IX. INDIAN LAND c B 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Emmaus I PA 1- I 1 1 18049 Is the facility located on Indian lands? ❑ YES El NO S2 15 19 .0 41 420 - s1 X. EXISTING ENVIRONMENTAL PERMITS A. NPDES Discharges to Su ace Water D. PSD (Air Ernlssions rom Pm ated Sources) C r 1 1 I l i t I I I I c * 1 I I 1 1 I Ip 1 1 1 1 1 g N NC0005274 g , NA 16 ,e 11 19 30 15 1e P 1e 33 B. UIC ((Under roundlnlection of/ Fluids)) E. OTHER spec, ) crit 1 t I I I I l l l l l l 9 U Nili1111111111 e NA (s ec+p fy) 15 1e IT1e 30 15 16 11 1e 50 C. RCRA (Hazardous Wastes) E. OTHER (sped) c- 1 1 I 1( 1 1 1 1 1 1 1 1 c*, 1 1 1 I I I I i I I I (SeClp i) 9 R NA g • NA 5 Xl. Attach location injects XII. The that Tentative aerated 5.0 and The • AT • PC • ET • SC • Totaling The from the the XIII. 1 cerfify inquiry am 04 MAP NATURE facility is the total discharge tanks tanks CERTIFICATION aware 17 to of fluids was 1- 2 3 4 tank under of those ie A this application a topographic map of the area extending each of its existing and proposed intake and discharge underground. Include all springs, rivers, and other OF BUSINESS (provide a brief description) is a shutdown dye manufacturing used under normal operations has plans are to transfer the waste for approximately eight hours. reached the water will be discharged 2C Form of this application. volume that will be discharged approximately 750,000 gallons - approximately 564,000 gallons - approximately 994,000 gallons - approximately 205,000 gallons approximately 2,500,000 gallons will continue for approximately to tank and the aeration activities will be addressed separately after is approximately 1,500 cubic yards. (see instructions) penally of law that 1 have personally examined persons immediately responsible for obtaining that (here are significant penalties for submitting false 15 surface Once is and the information, 16 16 70 to at least one mile beyond property boundaries. The structures, each of its hazardous waste treatment, storage, water bodies in the map area. See instructions for precise operation in Lowell, NC. The existing been vandalized and is no longer operational water to a 400,000 gallon storage tank the aeration is completed and a Dissolved at the predetermine rate which has been as follows: 120 days based on proposed flow rates, associated with the discharge. Sludge the discharge is complete but the estimated am familiar with the information submitted in this application information contained in the application, I believe that the including the possibility of fine and imprisonment. map must show the outline of the facility, the or disposal facilities, and each well where It requirements. wastewater treatment plant in its present condition. on site where the water will be Oxygen of greater then outlined in the cover letter water transfer activities which is present in all of volume of the sludge in and all attachments and that, based on my information Is true, accurate, and complete. 1 A. NAME 8 OFFICIAL TITLE (type or print) Tony Chiarella, Dir.of OperationsCT:\ B. SIGNATURE a4-e-12a-- iDIA.00s epS C. DATE SIGNED h I�Z COMMENTS c C FOR OFFICIAL USE ONLY 15 16 SS EPA Form 3510-1 (8-90) '15 Yitta 30 toz 17'30" Latitude: 35°1713" Langihnle: 81°05' 13" • Quad # Al4SE Stream Class: WS-V Sulibatin: 30336 Receiving Stream: South Fork Catawba River 4 \ l• • , \‘• \*J. • 111,1' r-- )\-- t \ NC0005274 Yorkshire Americas, Inc. .1 "1,2 7'4 ' • •-• *pi --- • • • .• • ..• . f 0 " SCALE 112.410tr • r Wastewater Treatffteflt Area 1 riot or type In the unshaded areas only. EPA I.D. NUMBER (copy from item I of Form I) NCD04444475 Form Approved. OMB No. 2040-0086. Approval expires 3-31-98. FORM 2C NPDES I. OUTFALL LOCATION „EPA U.S. ENVIRONMENTAL PROTECTION AGENCY APPLICATIOFOR PERMIT TO DISCHARGE WASTEWATER EXISTING MANUFACTURING,JCOMMERCIAL, MINING AND SILVICULTURE OPERATIONS Consolidated Permits Program For each outfali, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water. A OUTFALL NUMBER B. LATITUDE C. LONGITUDE (bsr) 1. DEG 2. MIN 3. SEC 1. DEG 2. MIN 3. SEC D. RECEIVING WATER (name) 001 35 17 13 81 06 13 South Fork Catawba River II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units labeled to correspond 10 the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations, treatment units, and outfalls. If a water balance cannot be determined (e.g., for certain mining activities), provide a pictorial description of the nature and amount of any sources of water and any collection or treatment measures. B. For each outfall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue an additional sheets if necessary. 1. OUT- 2. OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT FALL NO. (list) a. OPERATION (list) b. AVERAGE FLOW (include units) a. DESCRIPTION b. LIST CODES FROM TABLE 2C-1 001 A11 tanks contain a combination of Between 150, 000 and 200, 000 Water contained in the the tanks wi11 be 3-E treated, untreated and storm water Gallons per Daybased on the Cranefer:ed to a 400.000 gallon storage tank en -site from pant operations Tank beingdischarged 9 where the water will be aerated for approimately eight hours. Once the aeration is completed and a dissolved oxygen of greater then 5.0 is reached the water will be discharged at a predetermined flow rate. OFFICIAL USE ONLY(effluent grudelrnessub-catagorres) EPA Form 3510-2C (8.90) PAGE 1 of 4 CONTINUE ON REVERSE C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items II -A or B intermittent or seasonal? I% YES (complete the following table) ❑ NO (go to Seaton 11I) 1 OUTFALL NUMBER(flsr) 2 OPERATION(s) CONTRIBUTING FLOW (list) 3. FREQUENCY 4. FLOW a DAYS PER WEEK (specib avcmgc) b. MONTHS PER YEAR (spec5average) a FLOW RATE (rn mgd) B TOTAL VOLUME (sped with units) C DURATION (In days) 1. LONG TERM AVERAGE 2 MAXIMUM DAILY i LONG TERM AVERAGE 2. MAXIMUM DAILY 001 III PRODUCTION A. Does an effluent ❑ Outlined in Section IIB of this application guideline limitation promulgated by EPA under Section YES (complete Item III-B) Weekly dischage upon issuance of permit 304 of the TBD Clean Water NA Act apply to your IV) NA facility? NA 200,000 Gallons per Day 120 Days P4 NO (go to Section B. Are the limitations in the applicable effluent guideline expressed in terms of production ❑ YES (complete Item 111-C) (or other measure of operation)? IV) MI NO (go to Section C. If you answered "yes" to Item III-B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used In the applicable effluent guideline, and indicate the affected outfalls. 1. AVERAGE DAILY PRODUCTION 2. AFFECTED OUTFALLS (hstoulfall numbers) a. QUANTITY PER DAY b. UNITS OF MEASURE C. OPERATION. PRODUCT, MATERIAL, ETC. (sped) NA IV. IMPROVEMENTS required or administrative YES (complete by any Federal, State or local practices or any other environmental or enforcement orders, the following table) authority to meet any implementation schedule for the construction, programs which may affect the discharges described in this appl enforcement compliance schedule letters, stipulations, court orders, and FA NO (go to Item IV-B) upgrading or operations of wastewater cation? This Includes, but is not limited to, grant or loan conditions. A. Are you now treatment equipment permit conditions, ❑ 1. IDENTIFICATION OF CONDITION, AGREEMENT, ETC. 2. AFFECTED OUTFALLS 3. BRIEF DESCRIPTION OF PROJECT 4. FINAL COMPLIANCE DATE a NO b SOURCE OF DISCHARGE a REQUIRED b. PROJECTED B. OPTIONAL: You may attach addi Tonal sheets describing any additional water pollution control programs (or other environmental projects which may affect your discharges) you now have underway or which you plan Indicate whether each program is now underway or planned, and indicate your actual or planned schedules far construction. ❑ MARK "X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED EPA Form 3510-2C (8-90) PAGE 2 of 4 CONTINUE ON PAGE 3 CONTINUED FROM PAGE 2 V. INTAKE AND EFFLUENT CHARACTERISTICS A, 8, & C: See instructions before proceeding — Complete one set of tables for each outfall —Annotate the outfall number In the space provided. NOTE: Tables V-A, V-B, and V-C are included on separate sheets numbered V-1 through V-9. EPA I.D. NUMBER (copy from Item I of Form 1) NCD04444475 D. Use the space below to list any of the pollutants listed in Table 2c-3 of the Instructions, which you know or have reason to believe is discharged or may be discharged from any outfall. For every pollutant you Rat, briefly describe the reasons you believe it to be present and report any analytical data in your possession. 1. POLLUTANT 2. SOURCE 1. POLLUTANT 2. SOURCE Acetone Chlorobenzene Xylene Historical Operations Historical Operations Historical Operations Carbon Disulfide Ethylbenzene Toluene VI. POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intern El YES (list all such pollutants below ) Vi NO (go to Item V/•B) Historical Operations Historical Operations Historical Operations ediate or final product or byproduct? EPA Form 3510.2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE CONaINUED FROM THE FRONT VII. BIOLOGICAL TOXICITY TESTING DATA Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in relation to your discharge within the last 3 years? © YES (rdennfy the test(s) and describe rhea purposes below) ❑ NO (go to Seaton MI) A Phase II Chronic toxicity test was performed with a portion of water contained in the different tanks at the Kings Mountain Venture Site on the Ceriodaphnia dubia in January of 2010. This test was performed by Environmental Testing Solutions located in Asheville, North Carolina. VIII. CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm? ® YES (list the name, address, and telephone number of and pollutants analyzed by, each such laboratory or firm below) NO (go to Section LX) A. NAME B. ADDRESS C.TELEPHONE (area code & no.) D. POLLUTANTS ANALYZED (lls ) Prism Laboratories IX. CERTIFICATION 449 Springbrook PO Box 240543 Charlotte, NC 28224-0543 828-350-9364 All analytic results that are included in this application were analyzed by Prism ! certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible forgathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information, including the possibilily of fine and imprisonment for knowing violations. A. NAME & OFFICIAL TITLE (type or prtnr) Tony Chiarella, Director of operations B. PHONE NO. (area code & no.) 1609) 586-8004 D. DATE SIGNED of mPS EPA Form 3510-2C (8-90PAGE 4 of 4 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information EPA I.D. NUMBER (copy from Item I of Form I) on separate sheets (use the same format) instead of completing these pages. NCD04444475 SEE INSTRUCTIONS. OUTFALL NO. V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) Aeration Tank-001 PART A —You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details. 2. EFFLUENT 3. UNITS (specrjyrjblank) 4. INTAKE (optional) a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (iifavailable) a. LONG TERM AVERAGE VALUE 1. POLLUTANT CONCENTRATION (2) MASS CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS d. NO. OF ANALYSES a. CONCEN-(1) TRATION b. MASS CONCENTRATION (2) MASS b. NO. OF ANALYSES a. Biochemical Oxygen Demand (SOD) 29 48 NA 1 mg/1 lbs NA b. Chemical Oxygen Demand (COD) No Data No Data c. Total Organic Carbon (TO(') No Data No Data d. Total Suspended Solids(ISS) < 25 42 1 mg/1 lbs e. Ammonia (as N) No Data f. Flow VALUE 200,000 VALUE VALUE GPD VALUE g. Temperature (winter) VALUE 7 .49 VALUE VALUE °C VALUE h. Temperature (summer) VALUE 7 . 49 VALUE VALUE "C VALUE i. pH MINIMUM 7 . 37 MAXIMUM 7 . 89 MINIMUM NA MAXIMUM STANDARD UNITS PART B — Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark'X" in column 2-b for each pollutant you believe to be absent. If you mark co umn 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 1. POLLUTANT AND CAS NO. (ijavailable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a BELIEVED PRESENT b. BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (rjavailable) c. LONG TERM AVRG. VALUE (rjavailable) a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS d. NO. OF ANALYSES (1) CONCENTRATION (2) MASS b. NO. OF ANALYSES Bromide ( 2495959-67-9) X /� NA NA NA NA b. Chlorine, Total Residual >/ /� c. Color X No Data d. Fecal Coliform \ / x /�\ e. Fluoride (16984-48-6) Nitrate-Nitritef. (as (asM X /\ 0.25 0.42 1 mg/1 lbs EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE ITEM V-B CONTINUED FROM FRONT 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CAS NO. (if available) a BELIEVED PRESENT b. BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (ifavailable) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE 'f. b. NO. OF ANALYSES (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS g. Nitrogen. Organic (as M XTotal 8 3 13 8 NA NA 1 mg/1 lbs NA h. Oil and Grease i. Phosphorus (7723-14-0) >c((asP),Total4.4 0.98 1 mg/1 lbs j. Radioactivity (1) Alpha. Total X (2) Beta, Total X (3) Radium, Total v (4) Radium 226, Total v k. Sulfate (as SO4) (14808-79-8) I. Sulfide (as .5)X �/ m. Sulfite (as S03) (14265-45-3) X n. Surfactants X o. Aluminum. Total (7429-90-5) X p. Barium. Total (7440-39-3) ` n q. Boron, Total (7440-42-8) r. Cobalt. Total X s. Iron, Total (7439-89-6) �/ /� t. Magnesium. Total (7439-95-4) X u. Molybdenum, Total (7439-98-7) v. Manganese, Total (7439-96-5) w. Tin, Total (7440-31-5) v x. Titanium, Total (7440-32-6) X EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3 CONTINUED FROM PAGE 3 OF FORM 2-C EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER NCD04444475 Aeration Tank- 001 PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark 'X' In column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS fractions), mark 'X' in column 2-b for each pollutant you know or have reason to believe is present. Mark -X' in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitriie, 2,4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Compiete one table (al 7 pages) for each outfall. See instructions for additional details and requirements. 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK "X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BELIEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (iiavalable) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS METALS, CYANIDE, AND TOTAL PHENOLS 1 M. Antimony, Total (7440-36-0) X V NA NA NA 2M. Arsenic, Total (7440-38-2) v 3M. Beryllium, Total (7440-41-7) 4M. Cadmium. Total (7440-43-9) v Total (744 -47 Total (7440.47-3} , ` X 0.0054 0.009 1 mg/1 lbs ( 440,�8) Total 6M7M. X 0.11 0.18 1 mg/1 lbs Lead, Total (7439-92-1) X BRL BRL 1 mg/1 lbs 8M. Mercury, Total (7439-97-6) v 9M. Nickel, Total (7440.02-0) X 0.011 0. 018 1 mg/1 lbs 10M. Selenium, Total (7782-49-2) 11 M. Silver, Total (7440-22-4) X _ 12M. Thallium, Total (7440-28-0) X - 13M. 7440- nc, 6-6) Total X BRL BRL 1 mg/1 lbs 14M. Cyanide, Total (57-12-5) X 0.025 0.041 1 mg/1 lbs 15M. Phenols, Total X 0.59 0 .98 1 mg/1 lbs DIOXIN 2,3,7,8-Tetra- chlorodibenzo-P- Dioxin (1764-01-6) DESCRIBE RESULTS BRL means Below Reporting Limit EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (rfavailable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a TESTING REQUIRED b. BELIEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (ifavatlable) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE ` '0 b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS _ (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — VOLATILE COMPOUNDS 1V. Accrolein (107-02-8) X BRL BRL NA NA 1 ug/1 lbs NA 2V. Acrylonitrile (107-13-1) X BRL BRL 1 ug/1 lbs (7 1-4�2)ene X 11 0.018 1 ug/1 lbs 4Vme Bis t hl r nierhyl) Ether (542-88-1) X (75 25omoform -2) 5V.6V. X BRL BRL 1 ug/1 lbs Carbon Tetrachloride (56-23-5) X BRL BRL 1 ug/1 lbs " ( 05-90.7)benzene X BRL BRL 1 ug/1 lbs 8V. Chlorodi- bromomethane (124-48-1) X BRL BRL 1 ug/1 lbs 9V. Chloroethane (75-00-3) �/ X BRL BRL 1 ug/1 lbs 10V.2-Chloro- ethylvinyt Ether (110-75-8) X 11V. Chloroform (67-6) X BRL BRL 1 ug/1 lbs 12V. Dichloro- bromomethane (75-27-4) X 13V. Dichloro- difluoromethane (75-71-8) X 14V.1,1-Dichloro- ethane (75-34-3) �/ /� 15V.1.2-Dichloro- ethane (107-06-2) X BRL BRL 1 ug/1 lbs 16V.1,1-Dichloro- ethylene (75.35-4) �/ /� - 17V.1.2-Dichloro- propane (78-87-5) Xg/1 BRL BRL 1 u lbs 18V. 1,3-Dichloro- propylene (542-75-6) 19V. Ethylbenzene (100-41-4) X BRL BRL 1 ug/1 lbs 20V. Methyl Bromide (74-83-9) X 21V. Methyl Chloride (74-87-3) X — EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V 5 CONTINUED FROM PAGE V-4 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BELIEVED PRESENT c a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — VOLATILE COMPOUNDS (continued) 22V. MethyleneX Chloride (75-09-2) BRL BRL NA NA 1 u 1 g/ lbs NA Tetrachloroethane (79-34-5) X BRL BRL — 1 ug/1 lbs 24V. Tetrachloro- ethylene (127-18-4) �/ /� 25V.Tofuene (108-88-3) X 4.2 0.007 1 ug/1 lbs 26V. 1,2-Trans- Dichloroethylene (156-60-5) X BRL BRL 1 ug/1 lbs " 27V. 1.1 ,1-Trichloro- ethane (71-55.6) X BRL BRL 1 ug/ 1 lbs 28V.1,1,2-Trichloro- ethane (79-00-5) X _ _ BRL BRL _ 1 ug/1 lbs 29V Trichloro- ethylene (79-01-6) v 30V. Trichloro- iluoromethane (75-69-4) X - BRL BRL 1 ug/1 lbs 31V. Vinyl Chloride (75-01-4) X BRL BRL 1 ug/ 1 lbs GC/MS FRACTION — ACID COMPOUNDS IA.2-Chlorophenol (95-57-8) X BRL BRL 1 ug/1 lbs 2A.2,4-Dichloro- phenol (120-83-2) X BRL BRL 1 ug . 1 lbs 3A. 2,4-Dimethyl- phenol (105-67-9) X - BRL BRL , 1 ug/1 lbs 4A. 4,6-Dinitro-0- Cresol (534-52-1) X 5A.2,4Oinitro- phenol (51-28-5) X BRL BRL 1 ug/1 lbs 6A. 2-Nitrophenol (88-75-5) X BRL BRL 1 ug/ 1 lbs 7A. 4-Nitrophenoi (100-02-7) X BRL BRL 1 ug/ 1 lbs 8A. P-Chloro-M- Cresol (59-50-7) v 9A. Pentachforo- phenol(87-86-5) X BRL BRL 1 ug/1 lbs 10A. Phenol (108-95-2) X BRL BRL 1 ug/1 lbs 11A 2,4,6-Tnchloro- phenol (88-05-2) X BRL BRL 1 ug/1 lbs EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (ifavailable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BELIEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION_ (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS ce (3-32 )aphthene X BRL BRL NA NA 1 ug/1 lbs NA 2B. Acenaphtylene (208.96-8) XBRL BRL 1 ug/ 1 lbs 3B. Anthracene (120-12-7) X BRL BRL 1 ug/1 lbs 4B. Benzidine (92-87-5) X 58. Benzo (a) Anthracene (56-55-3) X BRL BRL 1 ug/1 lbs 6B. Benzo (a) Pyrene (50-32-8) X BRL BRL 1 ug/1 lbs 7B. 3.4-Benzo- fluoranthene (205-99-2) X BRL BRL 1 ug/1 lbs 8B. Benzo (ghi) Perylene (191-24-2) X BRL BRL 1 ug/1 lbs 98. Benzo (k) Fluoranthene (207-08-9) X BRL BRL 1 ug/1 lbs 108. Bis (2-Chlom- erhoxy) Methane (111-91-1) X BRL _ BRL 1 ug/ 1 lbs 11 B. Bis (2-Chloro- ethyl) Ether (111-44-4) X BRL BRL 1 ug/1 lbs 12B. Bis (2- Cl+loroisopmpyl) Ether (102-80-1) X BRL BRL 1 ug/1 lbs 13B. Bis (2-Ethvl- hexyl)Phthalate (117-81-7) X BRL BRL 1 ug/1 lbs 14B. 4-Bromophenyl Phenyl Ether (101-55-3) X BRL BRL 1 ug/1 lbs 15B. Butyl Benzyl Phthalate (85-68-7) X BRL BRL 1 ug/1 lbs 16B. 2-Chloro- naphthalene (91-58-7) X BRL BRL 1 ug/1 lbs 178. 4-Chloro- phenyl Phenyl Ether (7005-72-3) X BRL BRL _ 1 ug/1 lbs 18B. Chrysene (218-01-9) X BRL BRL 1 ug/1 lbs 19B. Dibenzo (a.h) Anthracene (53-70-3) X BRL BRL _ 1 ug/ 1 lbs 20B. 1,2-Dichloro- benzene (95-50-1) X BRL BRL 1 ug/1 lbs 21 B.1,3-Di-chloro- benzene (541-73-1) X BRL BRL 1 ug/1 lbs EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7 CONTINUED FROM PAGE V-6 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) b. NO. OF ANALYSES a. TESTING REQUIRED b. BEUEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN-(1) TRATION b. MASS a. LONG TERM AVERAGE VALUE BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) 228.1,4-Dichloro- benzene (108-46-7)X BRL BRL ug/1 lbs 23B. 3,3-Dichioro- benzidine (91-94-1) 24B. Diethyl Phthalate (84-66-2) X BRL BRL ug/ 1 lbs Phthalate (131 -11-3) BRL BRL ug/1 lbs 26B. Di-N-Butyl Phthalate (84-74-2) X BRL BRL ug/1 lbs 27B. 2.4-Dinitro- toluene (121-14-2) X ug/1 lbs 288.2,6-Dinitro- (606-20-2) Xtoluene 29B. Di-N-Octyl Phthalate (117-84-0) ` X 30B. 1,2-Diphenyl- hydrazine (as Azo- benzene) (122-66-7) X (20�0) nthene 31328. X BRL BRL ug/1 lbs Fluorene (86-73-7) XBRL BRL ug/1 lbs 338. Hexachloro- benzene (118-74-1) X BRL BRL u g/1 lbs 34B. Hexachloro- butadiene (87-68-3) X BRL BRL ug/1 lbs 35B. Hexachloro- cydopentadiene (77-47-4) X BRL BRL ug/ 1 lbs 36B Hexachloro- ethane (67-72-1) X BRL BRL ug/1 lbs 37B. Indeno (1,2,3-cd) Pyrene (193-39-5) XBRL BRL ug/1 lbs 388. Isophorone (78-59-1) X BRL BRL ug/ 1 lbs 39B. Naphthalene (91-20-3) X BRL BRL ug/1 lbs 408. Nitrobenzene (98-95-3) BRL BRL ug/1 lbs 41B. N-Nitro- sodimethyiamine (62-75-9) X 42B. N-Nitrosodi- N-Propylamine (621-64-7) X BRL BRL ug/1 lbs EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE CONTINUED FROM PAGE V-6 1. POLLUTANT AND CAS NUMBER (f available) 2. MARK 'X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) , b. NO. OF ANALYSES a. TESTING REQUIRED b. BELIEVED PRESENT a a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) ' 226.1,4-Dichioro- benzene (106-46-7) X BRL BRL 1 ug/ 1 lbs 23B. 3,3-DIchloro- benzidine (91-94-1) X 246. Diethyl Phthalate (84-66-2) X BRL BRL 1 ug/1 lbs 258. Dimethyl Phthalate (131 -11-3) X BRL BRL 1 ug/1 lbs 26B. Di-N-Butyl Phthalate (84-74-2) X BRL BRL 1 u g/ 1 lbs 27B. 2,4-Dinitro- toluene (121-14-2) X BRL BRL 1 ug/1 lbs 288.2,6-Dinitro- toluene (608-20-2) X 29B. DI-N-Octyl Phthalate (117-84-0) X 308.1razine (as Az - hydrazine (as Azo- benzene) (122-66-7) X 31B(20 X BRL BRL 1 ug/ 1 lbs -44--0)anthene 3`82&673 u7) rene X BRL BRL 1 ug/1 lbs 33B. Hexachioro- benzene (118-74-1) X BRL BRL 1 u g/ 1 lbs 34B. Hexachloro- butadiene (87-68-3) butadiene X BRL BRL 1 u g/1 lbs 358. Hexachioro- cyclopentadiene (77-47-4) X BRL BRL 1 ug/ 1 lbs 3613 Hexachloro- ethane (67-72-1) X BRL BRL 1 ug/1 lbs 37B. Indeno (1,2,3-cd) Pyrene (193-39-5) X BRL BRL 1 ug/1 lbs 38B. Isophorone (78-59-1) X BRL BRL 1 ug/ 1 lbs 39B. Naphthalene (91-20-3) X BRL BRL 1 ug/1 lbs (8 95 3) benzene X BRL BRL 1 ug/1 lbs 41 B. N-Nitro- sodimethylamine (62-75-9) X - 42B. N-Nitrosodi- N-Propylamine (621-64-7) X BRL BRL 1 ug/1 lbs EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (favailable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BELIEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS _ (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) 43B. N-Niiro- sodiphenylamine (86-30-6) X BRL BRL 1 ug/1 lbs 44B. Phenanthrene (85-01-8) X BRL BRL 1 ug/1 lbs (129-Pyrene X BRL BRL 1 ug/1 lbs 46B.1,2,4-Tri- chlorobenzene (120-82-1) X BRL BRL 1 ug/1 lbs GC/MS FRACTION — PESTICIDES 1 P. Aldrin (309-00-2) �/ /X 2P. a-BHC (319-84-6) �/ /� 3P. p-BHC (319-85-7) �/ X 4P. y-BHC (58-89-9) �/ X 5P. S-BHC (319-86-8) �/ X - 6P. Chlordane X(57-74-9) 7P. 4,4'-DDT (50-29-3) X _ 8P. 4,4'-DDE (72-55-9) \/ /X 9P. 4,4'-DOD (72-54-8) �/ X 10P. Malden (60-57-1) X 11 P. a-Enosulfan X(115.29-7) 12P. (3-Endosutfan (115-29-7) X 13P. Endosutfan Sulfate (1031-07-8) X 14P. Endrin X(72-20-8) 15P.Endrin Aldehyde (7421-93-4) X 16P. Heptachlor X(76.44-8) EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9 EPA I.D. NUMBER (copy from Item 1 of Form 1) I OUTFALL NUMBER NCD04444475 CONTINUED FROM PAGE V-8 Aeration Tank- 001 0 1. POLLUTANT AND CAS NUMBER (ifavailable) 2. MARK'X" j • 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a, TESTING REQUIRED b. BEUEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BEUEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION - PESTICIDES (continued) 17P. Heptachlor Epoxide (1024-57-3) 18P. PCB-1242 (53469-21-9) v 19P. PCB-1254 (11097-69-1) �/ �\ 20P. PCB-1221 (11104-28-2) v 21P. PCB-1232 (11141-16-5) �/ /\ 22P. PCB-1248 (12672-29-6) 23P. PCB-1260 (11096-82-5) 24P. PCB-1016 (12674-11-2) 25P.Toxaphene (8001-35-2) EPA Form 3510-2C (8-90) PAGE V-9 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information on separate sheets (use the same format) instead of completing these pages. SEE INSTRUCTIONS. EPA I.D. NUMBER (copy from Item I of Form )) NCD04444475 OUTFALL NO. V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) Equalization Tank-001 PART A —You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details. 1. POLLUTANT 2. EFFLUENT 3. UN TS (.specify if blank) 4. INTAKE (optional) a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS d. NO. OF ANALYSES (1) CONCENTRATION (2) MASS b. NO. OF ANALYSES a. Biochemical Oxygen Demand(BOU) 15 25 NA 1 mg/1 lbs NA b. Chemical Oxygen Demand (COD) No Data No Data c. Total Organic Carbon (TOC) No Data No Data d. Total Suspended Solids(7SS) 74 123 1 mg/1 lbs e. Ammonia (as N) No Dat a f. Flow VALUE 200,000 VALUE VALUE GPD VALUE g. Temperature (whiter) VALUE 5 . 85 VALUE VALUE °C VALUE h. Temperature (summer) VALUE 6 . 51 VALUE VALUE °C VALUE i. pH MINIMUM 7 _ 88 MAXIMUM 8. 81 MINIMUM NA MAXIMUM STANDARD UNITS PART B — Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark co umn 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 1. POLLUTANT AND CAS NO. (Yawn/able) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a BELIEVED PRESENT b. BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE Of available) a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS d. NO. OF ANALYSES (1) CONCENTRATION (2) MASS b. NO. OF ANALYSES a. Bromide (24959-67-9) X NA NA NA NA b. Chlorine, Total Residual �/ /� c. Color X No Data d. Fecal Cotiform \' X /�\ e. Fluoride (16964-48-8) f.Nitr l�Nitrite v c0.010 0.17 1 mg/1 lbs EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE ITEM V-B CONTINUED FROM FRONT 2. MARK "X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CAS NO. (if available) a. BELIEVED PRESENT b. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION _ (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS g. Nitrogen. Total Organic (as M X 31 51 NA NA 1 mg/1 lbs NA h. Oil and Grease v i. Phosphorus (as P), Total (7723-14-0) X 0.72 1.20 1 mg/1 lbs j. Radioactivity (1) Alpha, Total ` , X ,X` (2) Beta, Total (3) Radium, Total v (4) Radium 226, Total v k. Sulfate (as SO4) (14808-79-8) I. Sulfide (as S) �/ X m. Sulfite (as S0,) (14265-45-3) X n. Surfactants X - o. Aluminum, Total (7429-90-5) p. Barium, Total (7440-39-3) q. Boron, Total (7440-42-8) r. Cobalt, Total (7440-48-4) �/ /� s. Iron, Total (7439-89-6) �/ /� t. Magnesium, Total (7439-95-4) X u. Molybdenum, Total (7439-98-7) v. Manganese. Total (7439-96-5) w. Tin. Total (7440-31-5) v x. Titanium, Total (7440-32-6) EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3 CONTINUED FROM PAGE 3 OF FORM 2-C EPA I.D. NUMBER (copy frontItem 1 of Form 1) OUTFALL NUMBER NCD04444475 Equal. Tank- 001 1 PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2o-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfal's, and nonrequired GC/MS fractions), mark "X' in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2.4 dinitrophenol. or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for additional details and requirements. 1. POLLUTANT AND CAS NUMBER (ijovailable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BEUEVED PRESENT c a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BEUEVED ABSENT (1) CONCENTRATION _ (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS METALS, CYANIDE, AND TOTAL PHENOLS 1 M. Antimony, Total (7440-36-0} X v NA NA NA 2M. Arsenic, Total (7440-38-2) /� 3M. Beryllium, Total (7440-41-7) v 4M. Cadmium, Total (7440-43-9) v , 5M. Chromium, Total (7440-47-3) ..02 0012 0 1 m mg/1 lbs 6 C-o50-88) Total �( ,X 0.57 0.95 1 mg/1 lbs 7M. 439-92 ,Total (7439-92-1) BRL BRL 1 mg/1 lbs 8M. Mercury, Total (7439-97-6) v 9M. Nickel, Total (7440-02-0) X BRL BRL 1 mg/1 lbs 10M. Selenium, Total (7782-49-2) 11 M. Silver, Total (7440-22-4) v 12M. Thallium, Total (7440-28-0) X 13M. Zinc, Total (7440-66-6) �/ /� 0. 058 0. 097 1 mg/ 1 lbs 14M. Cyanide, Total (57-12-5) X 0. 074 0.123 1 m 1 g/ lbs 15M. Phenols, Total v ^ 0.072 0.120 1 mg/1 lbs DIOXIN 2,3,7,8-Tetra- chlorodibenzo-P- Dioxin (1764-01-6) / ,X\ DESCRIBE RESULTS elm means Below Reporting Limit EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BEUEVED PRESENT c. BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE • b. NO. OF ANALYSES (1) CONCENTRATION (2) MASS _ (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — VOLATILE COMPOUNDS (2-8)ein (107-0-oz-s) XBRL BRL NA NA 1 u 1 g/ lbs NA 2V.Acryloniirile (107-13-1) X BRL BRL 1 ug/1 lbs (71-43-2)3VBenzene X BRL BRL 1 ug/1 lbs 4V. Bis (Chloro- aiethv!) Ether (542-88-1) )*( 5V. omofom► (75-25-2) X BRL BRL 1 ug/1 lbs 6V. Tetrachloride Carbon Tetrachloride (56-23-5) , X BRL BRL 1 ug/1 lbs 7V. enzene (108-90-7) X BRL BRL , 1 ug/1 lbs 8V. Chlorodi- bromomethaneX bromomethaneBRL (124-48-1) BRL 1 ug/1 lbs 9V. Chloroethane (75-00-3) X BRL BRL 1 ug/1 lbs 10V. 2-Chooro- ethylvinyl Ether (110-75-8) 11V. Chloroform (67-66-3) (67 X BRL BRL 1 ug/1 lbs 12V. Dichloro- bromomethene (75-27-4) X , difiuoromethane (75-71-8) X 14V. 1,1-Dichloro- ethane (75-34-3) �/ /� ethane15V. (107-0&ro- ethane (107-06.2) X BRL BRL 1 ug/ 1 lbs 16V. 1,1-Dichloro- ethylene (75-35-4) X 17V.1.2propane (78- loco- propane (78-87-5) X BRL BRL 1 ug/1 lbs 18V.1,3-Oichloro- propylene (542-75-6) X 19V.amens 41-4) (100-41-4) X BRL BRL 1 ug/1 lbs 20V. Methyl Bromide (74-83-9) _ 21V. Methyl Chloride (74-87-3) X EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V 5 CONTINUED FROM PAGE V-4 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BEUEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (ifavailable) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE 0 b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION - VOLATILE COMPOUNDS (continued) 22V. MethyleneX Chloride (75-09-2) BRL BRL NA NA 1 u g/ 1 lbs NA 23V. 1,1,2,2- Tetrachloroethane (79-34-5) X BRL BRL 1 ug/1 lbs 24V. Tetrachloro- (127-18-4) Xethylene 25V.Toluene (108-88-3) X BRL BRL 1 ug/1 lbs 26V.1,2-Trans- Dichloroethylene (156-60-5) X BRL BRL 1 ug/1 lbs 27V.1,1,1-Trichloro- ethane(71-55-6) X BRL BRL 1 ug/1 lbs 28V.1,1,2-Trichloro- ethane (79-00-5) X BRL BRL 1 ug/1 lbs 29V Trichloro- ethylene (79-01-6) X 30V. Trichloro- tluaromethane (75-69-4) X BRL BRL 1 ug/1 lbs ' 31V. Vinyl Chloride (75-01-4) X BRL BRL 1 ug/1 lbs GC/MS FRACTION - ACID COMPOUNDS 1A. 2-Chlorophenol (95-57-8) X BRL BRL 1 ug/1 lbs 2A.2,4Dichloro- phenol (120-83-2) X BRL BRL _ 1 ug . 1 lbs 3A. 2,4-Dimethyl- phenol(105-67-9) X BRL BRL 1 ug/1 lbs 4A. 4,6-Dinitro-O- Cresol (534-52-1) �/ /� 5A. 2.4-Dinitro- phenol (51-28-5) X BRL BRL 1 ug/ 1 lbs , 6A. 2-Nitrophenal (88-75.5) X BRL BRL 1 ug/ 1 lbs 7A 4-Nitropheno! (100-02-7) X BRL BRL 1 ug/1 lbs 8A. P-Chloro-M- Cresol (59-50-7) X 9A.Pentachlaro- phenol (87-86-5) X BRL BRL 1 ug/1 lbs 10A. Phenol (108-95-2) X BRL BRL + 1 ug/1 lbs 11A. 2,4,6-Trichloro- phenol (88-05-2) X BRL BRL 1 ug/1 lbs EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (f available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) I a.b. TESTING REQUIRED BELIEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS ` Ace;aphihene X BRL BRL NA NA 1 ug/1 lbs NA 2B. Acenaphtylene (208-96.8) BRL BRL 1 ug/1 lbs 3B.Anthracene ) X BRL BRL 1 ug/1 lbs 4B. Benzidine (92-87-5) �/ X 5B. Benzo (a) Anthracene (56.55.3) X BRL BRL 1 ug/1 lbs 66. Benzo (a) Pyrene (50-32-8) X BRL BRL 1 ug/1 lbs 7B. 3,4-Benzo- iluoranthene (205.99.2) X BRL BRL 1 ug/1 lbs 8B. Benzo (ghi) Perylene (191-24-2) X BRL BRL 1 ug/1 lbs 9B. Benzo (k) Fluoranthene (207-08-9)- BRL BRL 1 ug/1 lbs 108. Bis (2-Ch1oro- ethoxy) Methane (111-91-1) X BRL BRL 1 ug/1 lbs 11 B. Bis (2-Chloro- erhyQ Ether (111-44-4) X BRL BRL • 1 ug/1 lbs 12B. Bis (2- Clrloroisoprop l)X Ether (102-80-1) BRL BRL 1 ug/1 lbs 13B. Bis (2-Ethvl- hexyl)Phthafate (117-81-7) X BRL BRL 1 ug/1 lbs 14B. 4-Bromophenyl Phenyl Ether (101-55-3) X BRL BRL 1 u g/ 1 lbs 15B. Butyl Benzyl Phthalate (85-68-7) X BRL BRL 1 ug/ 1 lbs 16B. 2-Chloro- naphthalene (91-58-7) X BRL BRL _ 1 ug/1 lbs 17B. 4-Chloro- phenyl Phenyl Ether (7005-72-3) X BRL BRL 1 ug/1 lbs 18B. Chrysene (218-01-9) BRL BRL 1 ug/1 lbs 19B. Dibenzo (a.h) Anthracene (53-70-3) X BRL BRL 1 ug/1 lbs 208.1,2-Dichloro- benzene (95-50-1) X BRL BRL 1 ug/1 lbs 218. 1.3-Di-chloro- benzene(541-73-1) X BRL BRL 1 ug/1 lbs EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7 CONTINUED FROM PAGE V-6 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) b. NO. OF ANALYSES a. TESTING REQUIRED b. BEUEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE BELIEVED ABSENT (1) CONCENTRATION _ (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) 22B.1,4-Dichloro- benzene (106.46-7)X BRL BRL 1 ug/ 1 lbs 23B. 3.3-Dichloro- benzidine (91-94-1) 24B. Diethyl Phthalate (84-66-2) X BRL BRL 1 ug/1 lbs Phthalate (131 -11-3) BRL BRL 1 ug/1 lbs 26B. Di-N-Butyl Phthalate(84-74-2) X BRL BRL 1 ug/1 lbs 276.2,4-Dinitro- toluene (121-14-2) BRL BRL 1 u g/ 1 lbs 288.2,6-Dinitro- toluene (606-20-2) X 29B. Di-N-Octyl Phthalate (117-84-0) X 30B. 1,2-Diphenyl- hydrazine (as Azo- benzene) (122-66-7) X _ _ (21�00)anthene ) X BRL BRL 1 ug/1 lbs1 - `8�731�rene X BRL BRL 1 ug/1 lbs 33B. Hexachloro- benzene (118-74-1)X BRL BRL 1 ug/1 lbs 34B. Hexachloro- butadiene (87-68-3)X BRL BRL 1 ug/1 lbs 35B. Hexachloro- cyclopentadiene (77-47-4) X BRL BRL 1 ug/1 lbs ethane (677272-1) ro- -67 36B He X BRL BRL 1 ug/ 1 lbs _ 378. Indeno (1,2,3-W) Pyrene (193-39-5) X BRL BRL 1 ug/1 lbs 38B. Isophorone (78-59-1) X BRL BRL 1 ug/1 lbs 39B. Naphthalene (91-20-3) X BRL BRL 1 ug/1 lbs ' (98-95-3) benzene X BRL BRL 1 ug/1 lbs 41B. N-Nitro- sodimethylamine (62-75-9) X 42B. N-Nitrosodi- N-Propylamine (621-64-7) _ X BRL BRL 1 ug/1 lbs EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK "X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BELIEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if -available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE ' b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS CO CONCENTRATION _ (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) 43B. N-Nitro- sodiphenylamine (86-30-6) BRL BRL 1 ug/1 lbs 44B. Phenanthrene (85-01-8) X BRL BRL 1 ug/1 lbs 45B. Pyrene (129-00-0) X BRL BRL - 1 ug/1 lbs 46B. 1,2,4-Tri- chlorobenzene (120-82-1) BRL BRL 1 ug/1 lbs GC/MS FRACTION — PESTICIDES 1P. Aldrin (309-00-2) X 2P. a-BHC (319-846) X 3P. p-BHC (319-85-7) X - 4P. y-BHC (58-89-9) X 5P. 8-BHC (319-88-8) \/ X 6P. Chlordane (57-74-9) X 7P. 4,4'-DDT (50-29-3) X 8P.4,4'-DDE (72-55-9) X 9P. 4,4'-DDD (72-54-8) \/ X 10P. Dieldrin (60-57-1) X 11 P. a-Enosulfan (115-29-7) X 12P. p-Endosulfan (115-29-7) X 13P. Endosulfan Sulfate (1031-07-8) X 14P. Endrin (72-20-8) X 15P. Endrin Aldehyde (7421-93-4) X 16P. Heptachlor X (76-44-8) EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9 CONTINUED FROM PAGE V-8 EPA I.D. NUMBER (copy from Item 1 of Form 1) I OUTFALL NUMBER NCD04444475 1 Equal. Tank- 001 1. POLLUTANT AND CAS NUMBER (f available) 2. MARK "X" • • 1 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BEUEVED PRESENT c, a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS 1 CONCENTRATION (2) MASS GC/MS FRACTION — PESTICIDES (continued) E o. Heptachlor paxide (1024-57-3) 18P. PCB-1242 (53469-21-9) v 19P. PCB-1254 (11097-69-1) v 20P. PCB-1221 (11104-28-2) �/ /\ 21P. PCB-1232 (11141-16-5) v 22P. PCB-1248 (12672-29-6) 23P. PCB-1260 (11096-82-5) n 24P. PCB-1016 (12674-11-2) 25P.Toxaphene (8001-35-2) . EPA Form 3510-2C (8-90) PAGE V-9 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information on separate sheets (use the same format) instead of completing these pages. SEE INSTRUCTIONS. V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) EPA I.D. NUMBER (copy from Item I of Form 1) NCD04444475 OUTFALL NO. " Primary Clarifier-001 PART A —You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details. 1. POLLUTANT 2. EFFLUENT 3. UN TS (speck rjblank) 4. INTAKE (option!) a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (ijavarlahle) c. LONG TERM AVRG. VALUE W.available) a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS d. NO. OF ANALYSES (1) CONCENTRATION (2) MASS b. NO. OF ANALYSES a. Biochemical Oxygen Demand (BOD) 95 119 NA 1 m 1 g/ lbs NA b. Chemical Oxygen Demand (COD) No Data No Data c. Total Organic Carbon (TOC) No Data No Data d. Total Suspended Solids(TSS) < 25 31 1 mg/1 lbs e. Ammonia (usN) No Data f. Flow VALUE 150,000 VALUE VALUE GPD VALUE g. Temperature (miner)6.02 VALUE VALUE VALUE °C VALUE h. Temperature (summer) VALUE 6.69 VALUE VALUE °C VALUE i. pH MINIMUM 7 . 11 MAXIMUM 7.21 MINIMUM NA MAXIMUM STANDARD UNITS PART B — Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark co umn 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an exp anation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 1. POLLUTANT AND CAS NO. (rfavailahle) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a BELIEVED PRESENT b. BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (rjavailoble) c. LONG TERM AVRG. VALUE (if available) a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS d. NO. OF ANALYSES (1) CONCENTRATION (2) MASS b. NO. OF ANALYSES a. Bromide (24959-67-9) X NA NA NA NA b. Chlorine, Total XResidual c. Color X No Data d. Fecal Colitorm \ / �( /�\ e. Fluoride (16984-48-8) (astv)f. teNitrite X 0.23 0.29 1 mg/1 lbs EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE ITEM V B CONTINUED FROM FRONT 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CAS NO. Of available) a. BEUEVED PRESENT b. BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE • b. NO. OF ANALYSES (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS g. Nitrogen. Total Organic (as N) X 81 101 NA NA 1 mg/1 lbs NA h. Oil and Grease v i. Phosphorus (as P), Total (7723-14-0) X 3.9 4. 88 1 mg/1 lbs j. Radioactivity (1) Alpha, Total X (2) Beta, Total X 'v` _ (3) Radium. Total (4) Radium 226. Total v k. Sulfate (as SO,) (14808-79-8) X I. Sulfide (as S) �/ X m. Sulfite (as SOj) (14265-45-3) ` , y /\ n. Surfactants X o. Aluminum. Total (7429-90-5) �/ X p. Barium, Total (7440-39-3) ` n q. Boron, Total (7440-42-8) r. Cobalt, Total (7440-48-4) �/ X s. Iron, Total (7439-89-6) �/ X t. Magnesium, Total (7439-95-4) u. Molybdenum, Total (7439-98-7) X v. Manganese, Total (7439-98-5) �( /` w. Tin, Total (7440-31-5) X _ x. Titanium, Total (7440-32-6) EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3 CONTINUED FROM PAGE 3 OF FORM 2-C EPA I.D. NUMBER (copyfrom Item 1 of Form 1) OUTFALL NUMBER NCD04444475 Primary Clar.- 001 PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X' in column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. if you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS fractions), mark 'X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for additional details and requirements. 1. POLLUTANT AND CAS NUMBER ('rfavailable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BELIEVED PRESENT a a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION _ (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS 1) CONCENTRATION (2) MASS METALS, CYANIDE, AND TOTAL PHENOLS 1 M. Antimony, Total (7440-36-0) X NA NA NA 2M. Arsenic, Total (7440-38-2) v - 3M. Beryllium, Total (7440-41-7) 4M. Cadmium, Total (7440-43-9) v 5M. Chromium, Total (7440-47-3) X BRL BRL 1 mg/ 1 lbs 6M. Copper, Total (7440-50-8) X BRL BRL 1 mg/1 lbs 7M. Lead, Total (7439-92-1) X BRL BRL 1 mg/1 lbs 8M. Mercury, Total (7439-97-6) v 8M. Nickel, Total (7440-02-0) X 0 .013 0.016 1 mg/1 lbs 10M. Selenium, Total (7782-49-2) X 11M. Silver, Total (7440-22-4) X 12M. Thallium, Total (7440-28-0) v (7440-66-6)13inc, Total X 0. 031 0. 0 3 8 1 mg/1 lbs 14M. Cyanide, Total (57-12-5) X 0.009 0. 010 1 mg/1 1 lbs Total Phenals, X 0 .2 0 0 .2 5 1 mg/1 lbs DIOXIN 2,3.7,8-Tetra- chlorodibenzo-P- Dioxin (1764-01-6) s. / DESCRIBE RESULTS en means Below Reporting Limit EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (javailable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BELIEVED PRESENT a BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (ifavailable) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE . b. NO. OF ANALYSES (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — VOLATILE COMPOUNDS 1 V. Accrolein (107-02-8) X BRL BRL NA NA 1 ug/1 lbs NA 2V. Acrylonitrile (107-13-1) X BRL BRL 1 ug/1 1bs 31-43-2)ene X 9.7 0.012 1 ug/1 lbs 4V. B!hl met) mall?v� Elherr (542-88-1) 5V. Bromoform (75-25-2) X BRL BRL 1 ug/1 lbs 6V. Carbon Tetrachloride (56-23-5) X BRL BRL 1 ug/1 lbs (108--9ai)benzene X 1.5 0.0019 1 ug/1 lbs 8V. Chlorodi- bromomethane (124-48-1) X BRL BRL 1 ug/1 lbs (7 00-3)Chloroethane 9V10V. X BRL BRL 1 ug/1 lbs 2-Chloro- ethylvinyl Ether (110-75-8) X 11V. Chloroform (67-66-3) X BRL BRL 1 ug/1 lbs 12V. Dichloro- bromomethane (75-27-4) X 13V. Dichloro- difluoromethane (75-71-8) X ro 14V. 1.1-Dichlo- ethane (75-34-3) �/ /� 15V.1,2-Dichloro- ethane(107-06-2) X BRL BRL 1 ug/1 lbs 16V.1.1-Dichloro- ethylene (75-35.4) �/ X 17V.1,2-Dichloro- propane (78-87-5) X BRL BRL 1 ug/1 g/ lbs chloro- propylenelone prop (542-75-6) ( o0-41-4) 19V. hyylbenzene X 1.4 0.0018 1 ug/1 lbs 20V. Methyl Bromide (74-83-9) 21V. Methyl Chloride (74-87-3) EPA Form 3510-2C (8-90) PAGEV-4 CONTINUE ON PAGE V-5 CONTINUED FROM PAGE V-4 1. POLLUTANT AND CAS NUMBER (ijavailable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) ', a. TESTING REQUIRED b. BELIEVED PRESENT c, a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — VOLATILE COMPOUNDS (cominned) 22V. MethyleneX Chloride (75-09-2) gam, BRL NA NA 1 ug/1 lbs NA 23V. 1.12.2- Tetrachloroethane (79-34-5) X BRL BRL 1 ug/1 lbs 24V. Tetrachloro- ethylene�/ (127-18-4) /� 25V.Toluene (108-88-3) X 3.0 0.0038 1 ug/1 lbs 26V.1,2-Trans- Dlchloroethylene (156-60-5) X BRL BRL 1 ug/1 lbs 27V.1,1.1-Trichloro- ethane (71-55-6) X BRL BRL 1 ug/ 1 lbs 28V.1,1.2-Trichf°ro- ethane (79-00-5) X BRL BRL 1 ug/1 lbs 29V Trichloro- ethylene (79-01-6) X — 30V. Trichloro- tl>Joromethane (75-69-4) X BRL BRL 1 ug/1 lbs 31V. Vinyl Chloride (75-01-4) X BRL BRL 1 ug/ 1 lbs GC/MS FRACTION — ACID COMPOUNDS 1A. 2-Chlorophenol (95-57-8) BRL BRL 1 ug/1 lbs 2A. 2,4-Dlchloro- phenol (120-83-2) X BRL BRL 1 u 1 g ' lbs 3A. 2,4-Dimethyl- phenol (105-67-9) X BRL BRL 1 ug/1 lbs 4A. 4,6-Dinitro-0- Cresol (534-52-1) �/ /\ 5A 2,4-Dinitro- phenol (51-28-5) X BRL BRL 1 ug/ 1 lbs 6A.2-Nitropheno! (88-75-5) X BRL BRL 1 ug/1 lbs 7A 4-Nitr°phen°f (100-02-7) u , BRL BRL 1 ug/1 lbs 8A P-Chloro-M- Cresol(59-50-7) X 9A. Pentachforo- phenol (87-86-5) X BRL BRL 1 ug/1 lbs 10A Phenol (108-95-2) X BRL BRL 1 ug/1 lbs ' 11A. 2,4,6-Trichloro- phenol (88-05-2) X BRL BRL 1 ug/1 lbs EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (f available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (opllona!) I a. TESTING REQUIRED b. BELIEVED PRESENT c. BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (ifavallable) c. LONG TERM AVRG. VALUE (if available) ' d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE - b. NO. OF ANALYSES (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (B�3A 9,aphthene 8 X BRL BRL NA NA 1 ug/ 1 lbs NA 2B. Acenaphtylene (208-96-8) X BRL BRL 1 ug/1 lbs 3B. Anthracene (120-12-7) XBRL BRL 1 ug/1 lbs 4B. Benzidine (92-87-5) �/ X 56. Benzo (a) Anthracene (56-55-3) X BRL BRL V 1 ug/1 lbs - 6B. Benzo (a) Pyrene (50-32-8) X BRL BRL 1 u 1 g/ lbs 7B. 3,4-Benzo- fluoranthene (205-99-2) X BRL BRL 1 ug/1 lbs 88. Benzo (ghi) Perylene (191-24-2) X BRL BRL 1 ug/1 lbs 9B. Benzo (k) Fluoranthene (207-08-9) X BRL BRL 1 ug/1 lbs 10B. Bis (2-Chloro- erhoxy) Methane (111-91-1) X BRL BRL 1 ug/1 lbs 11B. Bis (2-Chloro- erlryl) Ether (111-44-4) X BRL BRL 1 ug/1 lbs 12B. Bis (2- Clrloroisopropyl) Ether (102-80-1) X BRL BRL 1 ug/1 lbs 13B. Bis (2-Erhvl- hexyl) Phthalate (117-81-7) X BRL BRL 1 ug/ 1 lbs 14B. 4-Bromophenyl Phenyl Ether (101-55-3) X BRL BRL 1 ug/1 lbs 15B. Butyl Benzyl Phthalate (85-68-7) X BRL BRL 1 ug/1 lbs 16B. 2-Chloro- naphthafene (91-58-7) X BRL BRL 1 ug/1 lbs 17B. 4-Chloro- phenyl Phenyl Ether (7005-72-3) X BRL BRL 1 ug/1 lbs 186. Chrysene (218-01-9) X BRL BRL 1 - ug/1 lbs 19B. Dibenzo (a,h) Anthracene (53-70-3) X BRL BRL 1 ug/1 lbs 208.1,2-Dichloro- benzene (95-50-1) X BRL BRL 1 ug/1 lbs 218.1,3.Di-chloro-X benzene (541-73-1) BRL BRL 1 ug/1 lbs EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V 7 CONTINUED FROM PAGE V-6 1. POLLUTANT AND CAS NUMBER Of available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) " a TESTING REQUIRED b. BEUEVED PRESENT a a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE _ * b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION - (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) 22B.1,4-Dichloro- benzene (106-46-7) BRL BRL NA NA 1 u g/ 1 lbs NA 23B. 3,3-Dichloro- benzidine (91-94-1) X — - 248. Diethyl Phthafate(84-66-2) X BRL BRL 1 ug/1 lbs 258. Dimethyl Phthalate (131 -11-3) X BRL BRL 1 ug/1 lbs 268. DI-N-Butyl Phthalate(s4-74-z) X BRL BRL 1 ug/1 lbs 27B. 2,4-Dinitro- toluene (121-14-2)X BRL BRL 1 ug/1 lbs 28B. 2,6-Dinitro- toluene (606-20-2) X 298. Di-N-Octyl Phthalate (117-84-0) X 30B. 1,2-Diphenyl- hydrazine (as Azo- benzene) (122-66-7) X (2 6-0Fluoranthene X BRL BRL 1 ug/1 lbs (t368-73 u7'rene X BRL BRL 1 ug/1 lbs 33B. Hexachloro- benzene (118-74-1) X BRL BRL 1 ug/1 lbs 34B. Hexachloro- butadiene (87-68-3)X BRL BRL 1 ug/1 lbs 358. Hexachloro- cydopentadiene (77-47-4) X BRL BRL 1 ug/1 lbs 368 Hexachloro- ethane (67-72-1) X BRL BRL 1 ug/1 lbs 378. Indeno (1,2,3-cd) Pyrene (193-39-5) X BRL BRL 1 ug/1 lbs 38B. Isophorone (78-59-1) X BRL BRL - 1 ug/1 lbs 398. Naphthalene (91-20-3) X BRL BRL 1 ug/1 lbs 408. Nitrobenzene (98-95-3) X BRL BRL v 1 ug/1 lbs 41B. N-Nitro- sodimethylamine (62-75-9) X — 42B. N-Nitrosodi- N-Propylamine (621-64-7) X BRL BRL 1 ug/ 1 lbs EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (If available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) " a. TESTING REQUIRED b. BELIEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE ' b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS _ (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) 43B. N-Nitro- (sodiphe6n)yiamine X BRL BRL NA NA 1 ug/ 1 lbs NA 4�0P-8)nanthrene X BRL BRL 1 ug/1 lbs (12Pyrene X BRL BRL 1 ug/1 lbs 48B.1,2,4-Tri- chlorobenzene (120-82-1) X BRL BRL 1 ug/1 lbs GC/MS FRACTION — PESTICIDES 1P. Aldrin (309-00-2) X 2P. a-BHC (319-84-6) �/ /\ 3P. P-BHC (319-85-7) X 4P. y-BHC (58-89-9) X 5P. 5-BHC (319-88-8) �/ X 6P. Chlordane (57-74-9) �/ X 7P. 4,4'-DDT (50-29-3) �/ X 8P. 4,4'-DDE (72-55-9) X 9P. 4,4'-DDD (72-54-8) �/ X — 10P. Dieidrin (60-57-1) X - 11 P. a-Enosulfan (115-29-7) X 12P. If-Endosulfan (115-29-7) X V 13P. Endosulfan Sulfate (1031-07-8) X 14P. Endrin (72-20-8) X 15P. Endrin Aldehyde (7421-93-4) X 16P. Heptachlor X (76-44-8) EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9 'w EPA I.D. NUMBER (copy from Item 1 ofFonn 1) I OUTFALL NUMBER NCD04444475 CONTINUED FROM PAGE V-8 Primary Clar.- 001 1. POLLUTANT AND CAS NUMBER Ofavailable) 2. MARK "X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) b. NO. OF ANALYSES a. TESTING REQUIRED b. BELIEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN-(1) TRATION b. MASS a. LONG TERM AVERAGE VALUE BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS CONCENTRATION (2) MASS GC/MS FRACTION — PESTICIDES (contin red) 17P. Heptachlor Epoxide (1024-57-3) X NA NA NA NA NA 18P. PCB-1242 (53469-21-9) �/ �\ 19P. PCB-1254 (11097-69-1) v 20P. PCB-1221 (11104-28-2) v 21P. PCB-1232 (11141-16-5) \/ /� 22P. PCB-1248 (12672-29-6) 23P. PCB-1260 (11096-82-5) 24P. PCB-1016 (12674-11-2) 25P. Toxaphene (8001-35-2) EPA Form 3510-2C (8-90) PAGE V-9 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information EPA I.D. NUMBER (copy/inn( hem 1 of Form 1) on separate sheets (use the same format) instead of completing these pages. NCD04444475 SEE INSTRUCTIONS. OUTFALL NO. V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) Secondary Clarifier-001 PART A —You must prow de the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details. 1. POLLUTANT 2. EFFLUENT 3. UN TS (spceifyifblank) 4. INTAKE (optional) a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS NO. OF d.b. ANALYSES (1) CONCENTRATION (2) MASS NO. OF ANALYSES a. Biochemical Oxygen Demand (BOD) 78 98 NA 1 mg/1 lbs NA b. Chemical Oxygen Demand (COD) No Data No Data c. Total Organic Carbon (TOC) No Data No Data d. Total Suspended Solids(TSS) 38 48 1 mg/1 lbs e. Ammonia (asN) No Data f. Flow VALUE 150, 000 VALUE VALUE GPD VALUE g. Temperature (wooer) VALUE 7 . 71 VALUE VALUE °C VALUE h. Temperature (summer) VALUE 8 . 2 7 VALUE VALUE °C VALUE i. pH MINIMUM 6 . 94 MAXIMUM 7 . 13 MINIMUM NA MAXIMUM STANDARD UNITS PART B — Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark co umn 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 1. POLLUTANT AND CAS NO. (rfavarlable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. BELIEVED PRESENT b, BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (ifavailable) c. LONG TERM AVRG. VALUE (rfavailable) a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS d. NO. OF ANALYSES (1) CONCENTRATION (2) MASS b. NO. OF ANALYSES a. de (249559-67-67- 9) (2 X NA NA NA NA b. Chlorine, Total— Residual �/ /� c. Color X No Data d. Fecal Coliform X e. Fluoride (16984-4B-8) X (.Nitrate -Nitrite (as M \/ /\ 0.17 0.21 1 mg/1 lbs EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE ITEM V-B CONTINUED FROM FRONT 0 2. MARK 'X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CAS NO. (if available) a. BELIEVED PRESENT b. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (ijavatlable) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN-CO TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS CONCENTRATION (2) MASS g. Nitrogen, Total Organic (as M X 41 51 NA NA 1 mg/1 lbs NA h. Oil and Grease X I. Phosphorus P), Total (7723-14-0) X(as 3.0 3.8 _ ,r 1 mg/1 lbs j. Radioactivity (1) Alpha, Total X (2) Beta, Total X (3) Radium, Total v ' (4) Radium 226, Total v k. Sulfate (as SO4) (14808-79-8) X I. Sulfide (ass) \/ X m. Sulfite (as SO,) (14265-45-3) X n. Surfactants X o. Aluminum, Total (7429-90-5) X p. Barium, Total (7440-39-3) `/ n q. Boron, Total (7440-42-8) r. Cobalt, Total (7440-48-4) �/ X s. Iron, Total (7439-89-6) �/ /� 1 t. Magnesium, Total (7439-95-4) X u. Molybdenum, Total (7439-98-7) X _ v. Manganese, Total (7439.98.5) X w. Tin, Total (7440-31-5) 1 x. Titanium, Total (7440-32-6) X EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3 CONTINUED FROM PAGE 3 OF FORM 2-C EPA I.D. NUMBER (copy from Item 1 of Font, 1) OUTFALL NUMBER NCD04444475 Second Clar.- 001 PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2o-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2-methy1-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for additional details and requirements. 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) b. NO. OF ANALYSES a. TESTING REQUIRED b. BELIEVED PRESENT C. BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS 1 ) CONCENTRATION (2) MASS METALS. CYANIDE. AND TOTAL PHENOLS 1 M. Antimony, Total (7440-36.0) X NA NA NA 2M. Arsenic, Total (7440-38-2) v 3M. Beryllium, Total (7440-41-7) v 4M. Cadmium, Total (7440-43-9) v 5M. Chromium, Total (7440-47-3)X BRL BRL 1 mg/1 lbs (7440-50 8)� Total X 0. 013 0.016 1 mg/1 lbs 7M. Lead. Total (7439-92-1) XBRL BRL 1 mg/1 lbs 8M. Mercury. Total (7439-97-6) X 9M. Nickel, Total (7440-02-0) BRL BRL 1 mg/1 lbs 10M. Selenium, Total (7782-49-2) v 11M. Silver, Total (7440-22-4) v 12M. Thallium, Total (7440-28-0) v 13M, Zinc, Total (7440-86-6) X BRL BRL 1 mg/1 lbs 14M. Cyanide, Total (57-12-5) X 0.013 0.021 1 mg/1 lbs Total Phenols, X 0.072 0.90 1 mg/1 lbs DIOXIN 2,3,7,8-Tetra- chlorodibenzo-P- Dioxin (1764-01-6) DESCRIBE RESULTS BRL means Below Reporting Limit EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER ((1 available) 2. MARK "X" 3. EFFLUENT - 4. UNITS 5. INTAKE (optional) I a. TESTING REQUIRED b. BEUEVED PRESENT c, a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (If available) c. LONG TERM AVRG. VALUE (IJavailable) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BEUEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS 1 CONCENTRATION (2) MASS GC/MS FRACTION — VOLATILE COMPOUNDS 2-8ein (107-02-8) X BRL BRL NA NA 1 ug/1 lbs NA 2V. Acrylonitrile (107-13-1) X BRL BRL 1 ug/1 lbs (7 1-43-2)ene X 4.4 0.0055 1 ug/1 lbs 4V. Bis (Chloro- methyl) Ether (542-88-1) X (7 5-25-2)oform X BRL BRL 1 ug/1 lbs 6V. Carbon Tetrachloride (56-23-5) X BRL BRL - 1 ug/1 lbs _ 7V. Chlorobenzene (10s-90-7-9o-7) (10 X BRL BRL 1 ug/1 lbs 8V. Chlorodi- bromomethane (124-48-1) V BRL BRL 1 ug/1 lbs n�3) ethane X BRL BRL 1 ug/1 lbs 10V. 2-Chloro- ethylvinyl Ether (110-75-8) X 11V. Chloroform (67-66-3) X BRL BRL 1 ug/1 lbs 12V. Dichloro- bromomethane (75-27-4) X — 13V. Dichloro- ditluaromethane (75-71-8) X 14V.1.1-Dichloro- ethane (75-34-3)1 �/ /� ethane 5V. e(107-06-2) 21Dichloro- e X BRL BRL 1 ug/1 lbs 16V.1,1-Dichloro- ethylene (75-35-4) 17V. propane (78- taro- propane (78-87-5) X BRL BRL 1 ug/1 lbs 18V.1,3-Dichloro- propylene (542-75-6) X 19V. Ethylbenzene (100-41-4) X BRL BRL 1 ug/ 1 lbs 20V. Methyl Bromide (74-83-9) 21V. Methyl Chloride (74-87-3) EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V 5 CONTINUED FROM PAGE V-4 1. POLLUTANT AND CAS NUMBER Of available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a TESTING REQUIRED b. BELIEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATiON b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS CO CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS GC/MS FRACTION — VOLATILE COMPOUNDS (continued) 22V. Methylene Chloride (75-09-2)X BRL BRL NA NA 1 ug/1 lbs NA 23V. 1,2,2- Tetra. Tetrachloroethane (79-34-5) ` ' X BRL BRL 1 ug/1 lbs 24V. Tetrachloro- (127-18-4) Xethylene 25V. Toluene (108-88-3) X 3.9 0.005 1 ug/1 lbs 28V. 1,2-Trans- Oichloroethylene (156-60-5) X BRL BRL 1 ug/1 lbs ' 27V.1,1,1-Trichloro- ethane (71-55-6) BRL BRL 1 ug/ 1 lbs 28V.1,12-Trichforo- ethane (79-00-5) X BRL BRL 1 ug/1 lbs 29V Trichloro- ethylene (79-01-6) X 30V. Trichforo- fluoromethane (75-69-4) X • BRL BRL 1 ug/1 lbs 31V. Vinyl Chloride (75-01-4) X BRL BRL 1 ug/1 lbs GC/MS FRACTION — ACID COMPOUNDS 1A. 2-Chlorophenol (95-57-8) BRL BRL 1 ug/1 lbs 2A. of (12 Moro- phenol(120-83-2) X BRL BRL _ 1 ug .1 lbs 3A. 2,4-Dimethyl- phenol (105-67-9) X BRL BRL 1 ug/1 lbs 4A. 4,6-Dinitro-0- Cresol (534-52-1) X 5A. 2,4-Dinitro- phenol(51-28-5) X BRL BRL 1 ug/1 lbs 6A. 2-Nitrophenol (88-75-5) X BRL BRL 1 ug/1 lbs 7A.4Nitrophenol (100-02-7) X BRL BRL 1 ug/1 lbs 8A. P-Chloro-M- Cresol (59-50-7) X 9A. Pentachloro- phenol (87-86-5) X BRL BRL 1 ug/ 1 lbs 10A.Pheno! (108-95-2) X BRL BRL 1 ug/1 lbs 11A.2,4,6-Trichloro- phenol (88-05-2) X BRL BRL 1 u 1 g/ lbs EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (javallable) 2. MARK 'X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) , a. TESTING REQUIRED b. BEUEVED PRESENT C. BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (1favailable) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE A b. NO. OF ANALYSES (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS 1 CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (83-32 )aphthene X BRL BRL NA NA 1 ug/1 lbs NA 2B. Acenaphtylene (208-96-8) X BRL BRL 1 ug/1 lbs 3B. Anthracene (120-12-7) X BRL BRL 1 ug/1 lbs 4B. Benzidine (92-87-5) �/ X 5B. Benzo (a) Anthracene (56-55-3) X BRL BRL 1 ug/1 lbs — 6B. Benzo (a) Pyrene (50-32-8) X BRL BRL 1 ug/1 lbs 7B. 3,4-Benzo- tivaranthene (205-99-2) X BRL BRL 1 ug/1 lbs 8B. Benzo (ghi) Perytene (191-24-2) X BRL BRL 1 ug/1 lbs 9B. Benzo (k) Fluoranthene (207-08-9) X BRL BRL 1 ug/ 1 lbs 10B. Bis (2-Chloro- ethoxy) Methane (111-91-1) X BRL BRL 1 ug/1 lbs 11 B. Bis (2-Chloro- ethyl) Ether (111-44-4) X BRL BRL 1 ug/1 lbs 12B. Bis (2- ClrloroisopropvQ Ether (102-80-1) X BRL BRL 1 ug/1 lbs 13B. Bis (2-Ethvl- hezy!) Phthalate (117-81-7) X BRL BRL 1 ug/1 lbs 14B. 4-Bromophenyl Phenyl Ether (101-55-3) X BRL BRL 1 ug/1 lbs 15B. Butyl Benzyl Phthalate (85-68-7) X BRL BRL 1 ug/1 lbs 16B. 2-Chloro- naphthalene (91-58-7) X BRL BRL 1 ug/1 lbs 17B. 4-Chloro- phenyl Phenyl Ether (7005-72-3) X BRL BRL 1 ug/1 lbs 18B. Chrysene (218-01-9) X BRL BRL 1 ug/1 lbs 19B. Dibenzo (a.h) Anthracene (53-70-3) X BRL BRL 1 ug/1 lbs 208.1,2-Dtchloro- benzene (95-50-1) X BRL BRL 1 ug/1 g/ lbs 21 B.1,3-Di-chlaro- benzene (541-73-1) X BRL BRL 1 ug/1 lbs EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7 CONTINUED FROM PAGE V-6 1. POLLUTANT AND CAS NUMBER (favailable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) - a TESTING REQUIRED b. BELIEVED PRESENT c. BELIEVED ABSENT a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (If available) c. LONG TERM AVRG. VALUE (if available) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE ii —_ - b. NO. OF ANALYSES (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS 1) CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) benzene (106-46-7)oro- benzene X BRL BRL NA NA 1 u 1 g/ lbs NA 238.3,3-Dichloro- benzidine (91-94-1) 24B. Diethyl Phthalate (84-66-2) X BRL BRL 1 ug/1 lbs Phthalate (131 -11-3) BRL BRL 1 ug/1 lbs 26B. DI-N-Butyl Phthalate (84-74-2) X BRL BRL 1 ug/ 1 lbs 278.2,4-Dinitro- toluene (121-14-2)X BRL BRL 1 ug/1 lbs 28B. 2.6-Dinitro- toluene (608-20-2) X 298. Di-N-Octyl Phthalate (117-84-0) X 30B. 1,2-Diphenyl- hydrazine (as Azo- benzene) (122-66-7) X 313( (20600)anihene ) X BRL BRL 1 ug/1 lbs 2 8 73-77)Orene X BRL BRL 1 ug/1 lbs 33B. Hexachloro- benzene (118-74-1)X BRL BRLug/1 1 lbs 34B. Hexachloro- butadiene(87-68-3)X BRL BRL 1 ug/1 lbs 35B. Hexachloro- cyclapentadiene (77-47-4) X BRL BRL 1 ug/1 lbs etthh ane (67-72- eHe2-1)) 67-7 X BRL BRL 1 ug/1 lbs 37B. o (1.2, 13-cd)nPyrene (193-39-5) X BRL BRL 1 ug/1 lbs 38B. Isophorone (78-59-1) X BRL BRL 1 ug/1 lbs - 398. Naphthalene (91-20-3) X BRL BRL 1 ug/ 1 lbs 408. Nitrobenzene (98-95-3) X BRL BRL 1 ug/1 lbs 41B. N-Nitro- sodimethyiamine (62-75-9) X 42B. N-Nitrosodi- N-Propyiamine (621-64-7) X BRL BRL 1 ug/1 lbs EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE CONTINUED FROM THE FRONT 1. POLLUTANT AND CAS NUMBER (favailable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) • a. TESTING REQUIRED b. BELIEVED PRESENT c. a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (ifavailable) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BEUEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS 1 CONCENTRATION (2) MASS GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued) 43B. N-Nitro- sodiphenytamine (86-30-6) X BRL BRL NA NA 1 ug/ 1 lbs NA 44B.Phenanthrene (85-01-8) X BRL BRL 1 ug/1 lbs - 45B. Pyrene (129-00-0) X BRL BRL 1 ug/1 lbs 468.1,2,4-Tr1- chlorobenzene (120-82-1) BRL BRL 1 u 1 g lbs GC/MS FRACTION — PESTICIDES 1P. Aldrin (309-00-2) X 2P. a-BHC (319-84-6) \/ X 3P. (i-BHC (319-85-7) v 4P. y-BHC (58-89-9) X 5P. 8-BHC (319.88-8) �/ X 6P. Chlordane (57-74-9) X + 7P. 4.4'-DDT (50-29-3) �/ /� 8P. 4,4'-DDE (72-55-9) X 9P. 4,4'-DDD (72-54-8) X 10P. Dieldrin (60-57-1) X 11P. a-Enosulfan (115-29-7) X 12P. (1-Endosutfan (115-29-7) X 13P. Endosutfan Sulfate (1031-07-8) X 14P. Endrin (72-20-8) X 15P. Endrin Aldehyde (7421-93-4) X 16P. Heptachlor (76-44-8) X EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9 CONTINUED FROM PAGE V-8 EPA I.D. NUMBER (copy from Item I of Form I) I OUTFALL NUMBER NCD04444475 Second Clar.- 001 1. POLLUTANT AND CAS NUMBER (if available) 2. MARK "X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. TESTING REQUIRED b. BELIEVED PRESENT c a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. - VALUE (ifavailable) d. NO. OF ANALYSES a. CONCEN- TRATION b. MASS a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION _ (2) MASS (1) CONCENTRATION (2) MASS CONCENTRATION (2) MASS) GC/MS FRACTION — PESTICIDES (continued) 17P. Heptachlor Epoxide (1024-57-3) X NA NA NA NA NA 18P. PCB-1242 (53469-21-9) v 19P. PCB-1254 (11097-69-1) 20P. PCB-1221 (11104-28-2) �/ �\ 21P. PCB-1232 (11141-16-5) \/ /\ 22P. PCB-1248 (12672-29-6) 23P. PCB-1260 (11098-82-5) - 24P. PCB-1016 (12674-11-2) V • 25P.Toxaphene (8001-35-2) EPA Form 3510-2C (8-90) PAGE V-9