WQ0038087_Residual Annual Report 2021_20220301

M
fV
TERRA
renal
PO BOX 399 • DARDANELLE • ARKANSAS • 72834
479.747.8192
terrarenewal.com
2021 ANNUAL REPORT
for NC Land Application Permit Number:
WQ0038087
(Class B Residuals)
Permittee / Submitted By:
Terra Renewal Services
P.O. Box 399
Dardanelle, AR 72834
Attention:
North Carolina Department of Environmental Quality
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
512 N. Salisbury Street; 6t" Floor
Raleigh, NC 27604

11
TERRA
renewal
March 1, 2022
North Carolina Department of Environmental Quality
Division of Water Resources
Water Quality Permit Section
Non -Discharge Permitting Unit
Information Processing Unit
6th Floor
512 N. Salisbury Street
Raleigh, NC 27699
East Region Environmental Office
P.O. Box 1746
Watkinsville, GA 30677
phone [phone]
RE: 2021 Annual Report for Land Application Permit No. WQ0038087
Permittee: Terra Renewal Services, Inc
Dear Sir or Madam,
The enclosed documentation is intended to serve as the annual report for the land application of residuals
sources related to the above referenced permit in Wilkes and Yadkin Counties.
The following information is provided:
PPrmittPP-
Terra Renewal Services, Inc.
P.O. Box 399
Dardanelle, AR 72834
Preparer & Contact:
Terra Renewal Services, Inc
David C. Coyle; Senior Environmental Manager
P.O. Box 1746
Watkinsville, GA 30677
phone: [phone]
email: david.coyle(cDterrarenewal.com
These items are included with the report (in order):
1) The Annual Land Application Certification Form (ACF)
2) The Annual Residuals Sampling Summary Form (RSSF) and Annual Residuals Sampling
Summary Form — B (RSSF-B) for each residuals source
3) The Annual Metals Field Loading Summary Form (MFLSF), Annual Land Application Field
Summary Form (FSF), and Annual Land Application Field Summary Form Supplement (FSF-
SUP)
4) Lab Analyses for Residuals:
— Nutrients, Metals, TCLP, Other
— Fecal Density (Seven Set)
5) Annual Pathogen and Vector Attraction Reduction Form for NCAC 2T Rules (PVRF 2T)
6) Soil Test Reports (for fields applied in 2020)

Page 2
2021 Annual Report
WQ0038087
7) Complimentary Data:
— Executive Summary
— Fecal Analysis Summary
— Poultry Litter Analysis Summary and Poultry Litter Analyses
If additional information is required or there are any questions regarding this annual report, please contact
David Coyle via the information listed above. Thank you for your cooperation and attention to this matter.
Sincerely,
David C. Coyle
Senior Environmental Manager
NC LSS #1315

Denali
%%;A 1 V; W l -'.
3308 Bernice Avenue
Russellville, AR 72802
479.498.5000
March 19, 2019
North Carolina Department of Environmental Quality
Division of Water Resources
Water Quality Permits Section
Non -Discharge Permitting Unit
512 N. Salisbury Street
Raleigh, NC 27604
RE: Letter of Delegation for Signature Authority
Ar IML
TERRA
renewal
P.O. Box 399
Dardanelle, AR 72834
479.498.5000
This "Letter of Delegation" authorizes David C. Coyle, Environmental Manager, as a
representative and employee of Denali Water Solutions and Terra Renewal to produce, review,
or certify via signature any documentation associated with the following:
- Permit application, modification, and renewal
- Site & residuals source certification
- Reporting
- Permit transfer and termination
This authorization is provided under the guidelines of Rule 15A NCAC 02T .0106(b) and any
other applicable rules regarding compliance with the NC DEQ regulations.
For questions or further information regarding this matter, I may be contacted at
[e-mail] or 479-668-4502.
Sincerely,
;,� /-%, c;Ze�
Andy McNeill
Chief Executive Officer
Denali Water Solutions

1
Annual Land Application Certification Form (ACF)

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0038087 County: Wilkes & Yadkin Year:
Facility Name (as shown on permit):
Land Application Operator:
Terra Renewal Services, Inc
2021
Terra Renewal Services, Inc Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
r❑ Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
57
Total number of fields utilized for land application during the year:
23
Total amount of dry tons applied during the year for all application sites:
1,599
Total number of acres utilizes for land application during the year:
697
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources.❑ Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T . I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
David C. Coyle; Environmental Manager
Permittee Name and Title (type or print)
2/28/2022
Signature of Permittee
Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)

2
Annual Residuals Sampling Summary Form (RSSF)
Annual Residuals Sampling Summary Form — B (RSSF-B)

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3
Annual Metals Field Loading Summary Form (MFLSF)
Annual Land Application Field Summary Form (FSF)
Annual Land Application Field Summary Form Supplement (FSF-SUPP)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 39.63
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
21.8 Acres Permitted: 21.8 Site #: WK-CH-01 Field #:
10.4
Danripple
WK-CH-01
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
6/10/21
2
RVAF
6/l/21
31
Tyson-
Wilkes
6/l/21
L4]5
6
7
8
9
10
11
12
% Solids
3.7
3.6
4.8
Arsenic
6.7
6.4
4.9
Cadmium
1 2.2
2.1
1.6
Copper
1 640.0
6.8
28.0
Chromium
Lead
6.2
4.3
3.3
Mercury
2.0
2.2
1 1.6
Molyb-
denum
18.0
17.0
13.0
Nickel
18.0
17.0
13.0
Selenium
8.9
8.6
6.5
Zinc
280.0
30.0
63.0
Total
Phos-
horus
7,400
6,400
2,800
Annual Heavy Metal Field Loadings (Ualculated in lbs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
1.32
0.50
Arsenic
0.000
0.017
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Cadmium
0.000
0.006
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.000
0.018
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.011
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Mercury
0.000
0.006
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Molyb-
0.000
0.045
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
denum
Nickel
0.000
0.045
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Selenium
0.000
0.023
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Zinc
0.000
0.079
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.142
Total
Phos-
0.000
16.922
2.778
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
19.699
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/25/2021
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 88.15
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
41.6 Acres Permitted: 41.6 Site #: WK-CH-03 Field #:
11.6
Banister
WK-CH-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
6/10/21
2
RVAF
6/l/21
31
Tyson-
Wilkes
6/l/21
L4]5
6
7
8
9
10
11
12
% Solids
3.7
3.6
4.8
Arsenic
6.7
6.4
4.9
Cadmium
1 2.2
2.1
1.6
Copper
1 640.0
6.8
28.0
Chromium
Lead
6.2
4.3
3.3
Mercury
2.0
2.2
1 1.6
Molyb-
denum
18.0
17.0
13.0
Nickel
18.0
17.0
13.0
Selenium
8.9
8.6
6.5
Zinc
280.0
30.0
63.0
Total
Phos-
horus
7,400
6,400
2,800
Annual Heavy Metal Field Loadings (Ualculated in Ibs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.07
1.30
0.75
Arsenic
0.001
0.017
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
Cadmium
0.000
0.005
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
0.088
0.018
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.148
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.001
0.011
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Mercury
0.000
0.006
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Molyb-
0.002
0.044
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
denum
Nickel
0.002
0.044
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
Selenium
0.001
0.022
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
Zinc
0.039
0.078
0.095
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.211
Total
Phos-
1.021
16.627
4.206
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.854
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 98.41
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
35.8 Acres Permitted: 35.8 Site #: WK-CH-04 Field #:
10.9
Codorus
WK-CH-04
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
6/10/21
2
RVAF
6/l/21
31
Tyson-
Wilkes
6/l/21
L4]5
6
7
8
9
10
11
12
% Solids
3.7
3.6
4.8
Arsenic
6.7
6.4
4.9
Cadmium
1 2.2
2.1
1.6
Copper
1 640.0
6.8
28.0
Chromium
Lead
6.2
4.3
3.3
Mercury
2.0
2.2
1 1.6
Molyb-
denum
18.0
17.0
13.0
Nickel
18.0
17.0
13.0
Selenium
8.9
8.6
6.5
Zinc
280.0
30.0
63.0
Total
Phos-
horus
7,400
6,400
2,800
Annual Heavy Metal Field Loadings (Ualculated in Ibs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.04
2.24
0.47
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0.001
0.029
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Cadmium
0.000
0.009
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
0.051
0.030
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.108
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0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.019
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
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0.000
0.010
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
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0.001
0.076
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.090
denum
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0.001
0.076
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.090
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0.001
0.039
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.045
Zinc
0.022
0.134
0.059
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.216
Total
Phos-
0.592
28.659
2.632
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
31.883
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 24.26
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
13.2 Acres Permitted: 13.2 Site #: WK-MF-09 Field #:
10.6
Fairview
W K-MF-09
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
6/10/21
2
RVAF
9/2/21
31
Tyson-
Wilkes
8/26/21
L4]5
6
7
8
9
10
11
12
% Solids
3.7
6.4
5.8
Arsenic
6.7
3.7
4.1
Cadmium
1 2.2
1.2
1.4
Copper
1 640.0
4.5
5.3
Chromium
Lead
6.2
2.5
2.8
Mercury
2.0
1.2
1 1.3
Molyb-
denum
18.0
9.9
11.0
Nickel
18.0
9.9
11.0
Selenium
8.9
5.0
5.5
Zinc
280.0
27.0
62.0
Total
Phos-
horus
7,400
9,100
3,600
Annual Heavy Metal Field Loadings (Ualculated in Ibs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.85
0.99
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0.000
0.006
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Cadmium
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
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0.000
0.008
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
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0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Mercury
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
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0.000
0.017
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.039
denum
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0.000
0.017
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.039
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0.000
0.008
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Zinc
0.000
0.046
0.123
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.168
Total
Phos-
0.000
15.452
7.121
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
22.573
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 31.97
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
19.6 Acres Permitted: 19.6 Site #: WK-MF-10 Field #:
10.9
Fairview
WK-MF-10
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
6/10/21
2
RVAF
9/2/21
31
Tyson-
Wilkes
8/26/21
L4]5
6
7
8
9
10
11
12
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3.7
6.4
5.8
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6.7
3.7
4.1
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1 2.2
1.2
1.4
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1 640.0
4.5
5.3
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6.2
2.5
2.8
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2.0
1.2
1 1.3
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denum
18.0
9.9
11.0
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18.0
9.9
11.0
Selenium
8.9
5.0
5.5
Zinc
280.0
27.0
62.0
Total
Phos-
horus
7,400
9,100
3,600
Annual Heavy Metal Field Loadings (Ualculated in lbs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.82
0.81
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0.000
0.006
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
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0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
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0.000
0.007
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
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0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
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0.000
0.004
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
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0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
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0.000
0.016
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
denum
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0.000
0.016
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
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0.000
0.008
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Zinc
0.000
0.044
0.101
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.145
Total
Phos-
0.000
14.869
5.861
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
20.730
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 32.27
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
22.5 Acres Permitted: 22.5 Site #: WK-MF-11 Field #:
9.8
Fairview
WK-MF-11
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
6/10/21
2
RVAF
9/2/21
31
Tyson-
Wilkes
8/26/21
L4]5
6
7
8
9
10
11
12
% Solids
3.7
6.4
5.8
Arsenic
6.7
3.7
4.1
Cadmium
1 2.2
1.2
1.4
Copper
1 640.0
4.5
5.3
Chromium
Lead
6.2
2.5
2.8
Mercury
2.0
1.2
1 1.3
Molyb-
denum
18.0
9.9
11.0
Nickel
18.0
9.9
11.0
Selenium
8.9
5.0
5.5
Zinc
280.0
27.0
62.0
Total
Phos-
horus
7,400
9,100
3,600
Annual Heavy Metal Field Loadings (Ualculated in lbs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.85
0.58
Arsenic
0.000
0.006
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.000
0.008
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Mercury
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.000
0.017
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
denum
Nickel
0.000
0.017
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
Selenium
0.000
0.009
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Zinc
0.000
0.046
0.072
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.118
Total
Phos-
0.000
15.543
4.176
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
19.719
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 96.09
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
33.8 Acres Permitted: 33.8 Site #: WK-MF-13 Field #:
12.0
Fairview
WK-MF-13
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
11/30/21
2
RVAF
11/30/21
31
Tyson-
Wilkes
11/30/21
L4]5
6
7
8
9
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
1 0.3
2.2
1.6
Copper
1 450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings (Ualculated in Ibs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.84
2.00
Arsenic
0.000
0.011
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
Cadmium
0.000
0.004
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Copper
0.000
0.022
0.108
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.130
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.007
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Mercury
0.000
0.004
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Molyb-
0.000
0.029
0.052
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.081
denum
Nickel
0.000
0.029
0.052
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.081
Selenium
0.000
0.015
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.040
Zinc
0.000
0.095
0.152
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.246
Total
Phos-
0.000
32.072
14.793
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
46.865
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 17.27
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
23.4 Acres Permitted: 23.4 Site #: WK-MF-14 Field #:
10.1
Fairview
WK-MF-14
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
11/30/21
2
RVAF
11/30/21
31
Tyson-
Wilkes
11/30/21
L4]5
6
7
8
9
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
1 0.3
2.2
1.6
Copper
1 450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings (Ualculated in lbs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.20
0.54
Arsenic
0.000
0.003
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Cadmium
0.000
0.001
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
0.000
0.005
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Mercury
0.000
0.001
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.000
0.007
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
denum
Nickel
0.000
0.007
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Selenium
0.000
0.004
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Zinc
0.000
0.023
0.041
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Total
Phos-
0.000
7.714
3.959
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.673
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 32.98
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
13.8 Acres Permitted: 13.8 Site #: WK-MF-15 Field #:
10.4
Fairview
WK-MF-15
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
11/30/21
2
RVAF
11/30/21
31
Tyson-
Wilkes
11/30/21
L4]5
6
7
8
9
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
1 0.3
2.2
1.6
Copper
1 450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings (Ualculated in lbs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.76
1.63
Arsenic
0.000
0.010
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Cadmium
0.000
0.003
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
0.000
0.020
0.088
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.108
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.007
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Mercury
0.000
0.003
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Molyb-
0.000
0.026
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.068
denum
Nickel
0.000
0.026
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.068
Selenium
0.000
0.013
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Zinc
0.000
0.085
0.124
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.209
Total
Phos-
0.000
28.804
12.077
0.000
0.000
0.000
0.000
0.000
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with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 108.16
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
59.2 Acres Permitted: 59.2 Site #: WK-MF-23 Field #:
8.7
Fairview
W K-MF-23
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
6/10/21
2
RVAF
9/2/21
31
Tyson-
Wilkes
8/26/21
L4]5
6
7
8
9
10
11
12
% Solids
3.7
6.4
5.8
Arsenic
6.7
3.7
4.1
Cadmium
1 2.2
1.2
1.4
Copper
1 640.0
4.5
5.3
Chromium
Lead
6.2
2.5
2.8
Mercury
2.0
1.2
1 1.3
Molyb-
denum
18.0
9.9
11.0
Nickel
18.0
9.9
11.0
Selenium
8.9
5.0
5.5
Zinc
280.0
27.0
62.0
Total
Phos-
horus
7,400
9,100
3,600
Annual Heavy Metal Field Loadings (Ualculated in Ibs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.92
0.91
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0.000
0.007
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Cadmium
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
0.000
0.008
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
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0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.005
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Mercury
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
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0.000
0.018
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.038
denum
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0.000
0.018
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.038
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0.000
0.009
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Zinc
0.000
0.050
0.112
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.162
Total
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0.000
16.744
6.530
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
23.274
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 52.18
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
15.1
Danripple
18.9 Acres Permitted: 18.9 Site #: WK-NIRF-03 Field #: WK-MRF-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
12/3/20
2
RVAF
11/19/20
3
Tyson-
Wilkes
11/19/20
4
Advance
Pierre
2A/21
5
RVAF
1/28/21
6
Tyson-
Wilkes
1/28/21
7
8
9
10 j
12
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2.7
9.4
6.2
6.5
3.1
6.2
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9.3
2.6
4.0
0.7
8.0
3.9
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3.1
0.9
1.3
0.2
2.7
1.3
Copper
490.0
1.7
31.0
31.0
8.7
34.0
Chromium
Lead
6.2
1.7
2.7
0.5
5.4
2.6
Mercury
2.8
0.9
1 1.2
1.2
2.6
1 1.2
Molyb-
denum
25.0
7.0
11.0
1.8
21.0
10.0
Nickel
25.0
7.0
11.0
2.2
21.0
10.0
Selenium
12.0
3.5
5.4
0.9
11.0
5.2
Zinc
82.0
8.7
69.0
8.0
60.0
82.0
Total
Phos-
horus
14,000
4,500
3,800
5,700
8,100
2,600
Annual Heavy Metal Field Loadings (Ualculated in Ibs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
1.12
0.99
0.00
0.41
0.25
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0.000
0.006
0.008
0.000
0.007
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.022
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0.000
0.002
0.003
0.000
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.000
0.004
0.061
0.000
0.007
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.089
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.005
0.000
0.004
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Mercury
0.000
0.002
0.002
0.000
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.007
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0.000
0.016
0.022
0.000
0.017
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.059
denum
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0.000
0.016
0.022
0.000
0.017
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.059
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0.000
0.008
0.011
0.000
0.009
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.030
Zinc
0.000
0.019
0.136
0.000
0.049
0.040
0.000
0.000
0.000
0.000
0.000
0.000
0.245
Total
Phos-
0.000
10.080
7.486
0.000
6.642
1.279
0.000
0.000
0.000
0.000
0.000
0.000
25.487
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 73.98
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
14.1
Danripple
25.3 Acres Permitted: 25.3 Site #: WK-NIRF-05 Field #: WK-MRF-05
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
12/3/20
2
RVAF
11/19/20
3
Tyson-
Wilkes
11/19/20
4
Advance
Pierre
2A/21
5
RVAF
1/28/21
6
Tyson-
Wilkes
1/28/21
7
8
9
10 j
12
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2.7
9.4
6.2
6.5
3.1
6.2
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9.3
2.6
4.0
0.7
8.0
3.9
Cadmium
3.1
0.9
1.3
0.2
2.7
1.3
Copper
490.0
1.7
31.0
31.0
8.7
34.0
Chromium
Lead
6.2
1.7
2.7
0.5
5.4
2.6
Mercury
2.8
0.9
1 1.2
1.2
2.6
1 1.2
Molyb-
denum
25.0
7.0
11.0
1.8
21.0
10.0
Nickel
25.0
7.0
11.0
2.2
21.0
10.0
Selenium
12.0
3.5
5.4
0.9
11.0
5.2
Zinc
82.0
8.7
69.0
8.0
60.0
82.0
Total
Phos-
horus
14,000
4,500
3,800
5,700
8,100
2,600
Annual Heavy Metal Field Loadings (Ualculated in lbs/acre):
Total
1 1
2j
3 j
4
5J
J
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.84
0.74
0.06
0.67
0.61
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0.000
0.004
0.006
0.000
0.011
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Cadmium
0.000
0.001
0.002
0.000
0.004
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
0.000
0.003
0.046
0.004
0.012
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.106
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
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0.000
0.003
0.004
0.000
0.007
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Mercury
0.000
0.002
0.002
0.000
0.004
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Molyb-
0.000
0.012
0.016
0.000
0.028
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.069
denum
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0.000
0.012
0.016
0.000
0.028
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.069
Selenium
0.000
0.006
0.008
0.000
0.015
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.035
Zinc
0.000
0.015
0.102
0.001
0.081
0.101
0.000
0.000
0.000
0.000
0.000
0.000
0.299
Total
Phos-
0.000
7.533
5.594
0.730
10.919
3.188
0.000
0.000
0.000
0.000
0.000
0.000
27.963
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 52.19
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
14.8
Danripple
24.9 Acres Permitted: 24.9 Site #: WK-NIRF-06 Field #: WK-MRF-06
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
12/3/20
2
RVAF
11/19/20
3
Tyson-
Wilkes
11/19/20
4
Advance
Pierre
2A/21
5
RVAF
1/28/21
6
Tyson-
Wilkes
1/28/21
7
8
9
10 j
12
% Solids
2.7
9.4
6.2
6.5
3.1
6.2
Arsenic
9.3
2.6
4.0
0.7
8.0
3.9
Cadmium
3.1
0.9
1.3
0.2
2.7
1.3
Copper
490.0
1.7
31.0
31.0
8.7
34.0
Chromium
Lead
6.2
1.7
2.7
0.5
5.4
2.6
Mercury
2.8
0.9
1 1.2
1.2
2.6
1 1.2
Molyb-
denum
25.0
7.0
11.0
1.8
21.0
10.0
Nickel
25.0
7.0
11.0
2.2
21.0
10.0
Selenium
12.0
3.5
5.4
0.9
11.0
5.2
Zinc
82.0
8.7
69.0
8.0
60.0
82.0
Total
Phos-
horus
14,000
4,500
3,800
5,700
8,100
2,600
Annual Heavy Metal Field Loadings (Ualculated in Ibs/acre):
Total
1 1
2j
3 j
4
5J
J
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.85
0.25
0.00
0.44
0.56
Arsenic
0.000
0.004
0.002
0.000
0.007
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Cadmium
0.000
0.001
0.001
0.000
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
0.000
0.003
0.015
0.000
0.008
0.038
0.000
0.000
0.000
0.000
0.000
0.000
0.064
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.003
0.001
0.000
0.005
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Mercury
0.000
0.002
0.001
0.000
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.006
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0.000
0.012
0.005
0.000
0.018
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.047
denum
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0.000
0.012
0.005
0.000
0.018
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.047
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0.000
0.006
0.003
0.000
0.010
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Zinc
0.000
0.015
0.034
0.000
0.052
0.092
0.000
0.000
0.000
0.000
0.000
0.000
0.193
Total
Phos-
0.000
7.650
1.892
0.000
7.063
2.917
0.000
0.000
0.000
0.000
0.000
0.000
19.523
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 79.69
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
12.5
Pfafftown
25.1 Acres Permitted: 25.1 Site #: WK-NIRF-12 Field #: WK-MRF-12
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
12/3/20
2
RVAF
11/19/20
3
Tyson-
Wilkes
11/19/20
4
Advance
Pierre
2A/21
5
RVAF
1/28/21
6
Tyson-
Wilkes
1/28/21
7
8
9
10 j
12
% Solids
2.7
9.4
6.2
6.5
3.1
6.2
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9.3
2.6
4.0
0.7
8.0
3.9
Cadmium
3.1
0.9
1.3
0.2
2.7
1.3
Copper
490.0
1.7
31.0
31.0
8.7
34.0
Chromium
Lead
6.2
1.7
2.7
0.5
5.4
2.6
Mercury
2.8
0.9
1 1.2
1.2
2.6
1 1.2
Molyb-
denum
25.0
7.0
11.0
1.8
21.0
10.0
Nickel
25.0
7.0
11.0
2.2
21.0
10.0
Selenium
12.0
3.5
5.4
0.9
11.0
5.2
Zinc
82.0
8.7
69.0
8.0
60.0
82.0
Total
Phos-
horus
14,000
4,500
3,800
5,700
8,100
2,600
Annual Heavy Metal Field Loadings (Ualculated in lbs/acre):
Total
1 1
2j
3 j
4
5 j
6
7
81
91
L1
11
12
DT/Ac./
App.
14
Event
0.05
1.59
0.47
0.07
0.68
0.31
Arsenic
0.001
0.008
0.004
0.000
0.011
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Cadmium
0.000
0.003
0.001
0.000
0.004
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
0.053
0.005
0.029
0.004
0.012
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.125
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.001
0.005
0.003
0.000
0.007
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Mercury
0.000
0.003
0.001
0.000
0.004
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.009
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0.003
0.022
0.010
0.000
0.029
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.070
denum
Nickel
0.003
0.022
0.010
0.000
0.029
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Selenium
0.001
0.011
0.005
0.000
0.015
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Zinc
0.009
0.028
0.065
0.001
0.082
0.051
0.000
0.000
0.000
0.000
0.000
0.000
0.235
Total
Phos-
1.512
14.337
3.602
0.741
11.016
1.607
0.000
0.000
0.000
0.000
0.000
0.000
32.815
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
WQ0038087 Cation Exchange Capacity (non 503 only):
Terra Renewal Services Owner: Mathis Properties, LLC Predominant Soil Series:
52.3 Acres Permitted: 52.3 Site #: WK-MRF-20 Field #:
291.21
10.4
Dan River
WK-MRF-20
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
Advance
Pierre
6/10/21
2
RVAF
9/2/21
3
Tyson-
Wilkes
8/26/21
4
Advance
Pierre
11/30/21
5
RVAF
11/30/21
6
Tyson-
Wilkes
11/30/21
7
8
9
10
11
12
% Solids
3.7
6.4
5.8
7.0
3.8
5.0
Arsenic
1 6.7
3.7
4.1
1 1.0
6.5
4.8
Cadmium
2.2
1.2
1.4
0.3
2.2
1.6
Copper
1 640.0
4.5
5.3
450.0
13.0
27.0
Chromium
Lead
6.2
2.5
2.8
1.9
4.3
3.2
Mercury
2.0
1.2
1.3
0.3
2.1
1.7
Molyb-
denum
18.0
9.9
11.0
2.6
17.0
13.0
Nickel
18.0
9.9
11.0
35.0
17.0
13.0
Selenium
8.9
5.0
5.5
1.3
8.7
6.4
Zinc
280.0
27.0
62.0
140.0
56.0
38.0
Total
Phos-
horus
7,400
9,100
3,600
800
19,000
3,700
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
App.
Event
0.03
2.60
1.44
0.02
0.47
1.01
Arsenic
0.000
0.019
0.012
0.000
0.006
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.047
Cadmium
0.000
0.006
0.004
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Copper
0.035
0.023
0.015
0.016
0.012
0.054
0.000
0.000
0.000
0.000
0.000
0.000
0.156
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.013
0.008
0.000
0.004
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.032
Mercury
0.000
0.006
0.004
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Molyb-
0.001
0.052
0.032
0.000
0.016
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.127
denum
Nickel
0.001
0.052
0.032
0.001
0.016
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.128
Selenium
0.000
0.026
0.016
0.000
0.008
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.064
Zinc
0.015
0.141
0.179
0.005
1 0.053
0.076
0.000
0.000
0.000
0.000
0.000
0.000
0.469
Total
Phos-
0.400
47.356
10.390
0.029
17.974
7.437
0.000
0.000
0.000
0.000
0.000
0.000
83.585
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
WQ0038087 Cation Exchange Capacity (non 503 only):
Terra Renewal Services Owner: Mathis Properties, LLC Predominant Soil Series:
27.8 Acres Permitted: 27.8 Site #: WK-MRF-21 Field #:
104.75
12.3
Dan River
WK-MRF-21
Residual Analvsis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
Advance
Pierre
6/10/21
2
RVAF
6/1/21
3
Tyson-
Wilkes
6/1/21
4
RVAF
9/2/21
5
Tyson-
Wilkes
8/26/21
6
7
8
9
10
11
12
% Solids
3.7
3.6
4.8
6.4
5.8
Arsenic
1 6.7
6.4
4.9
1 3.7
4.1
Cadmium
2.2
2.1
1.6
1.2
1.4
Copper
1 640.0
6.8
28.0
4.5
5.3
Chromium
Lead
6.2
4.3
3.3
2.5
2.8
Mercury
2.0
2.2
1.6
1 1.2
1.3
Molyb-
denum
18.0
17.0
13.0
9.9
11.0
Nickel
18.0
17.0
13.0
9.9
11.0
Selenium
8.9
8.6
6.5
5.0
5.5
Zinc
280.0
30.0
63.0
1 27.0
62.0
Total
Phos-
horus
7,400
6,400
2,800
9,100
3,600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 11
1
1
1 1
1 111
1 11 •
1 11
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 11
1 11
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11:
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1 111
1 11 •
1 1 •
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 11
1 11
1 111
1 11:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
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1 111
1 11
1 11
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11:
1 111
1 1
1 1
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 1
1 1
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
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1 111
1 11:
1 11
1 11
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 1
1 1•
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1 •
1 111
1111
1 111
1 111
1111
1 111
1111
Total
Phos-
1 111
•1
1•
1 •:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11:
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
WQ0038087 Cation Exchange Capacity (non 503 only):
Terra Renewal Services Owner: Barker, Kim Tharpe Predominant Soil Series:
57.8 Acres Permitted: 57.8 Site #: WK-RJ-02 Field #:
19.48
7.9
Dan River
WK-RJ-02
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
Advance
Pierre
2/4/21
2
RVAF
1/28/21
3
Tyson-
Wilkes
1/28/21
4
5
6
7 j
8
9
Lj
11
12
% Solids
6.5
3.1
6.2
Arsenic
1 0.7
8.0
3.9
Cadmium
0.2
2.7
1.3
Copper
1 31.0
8.7
34.0
Chromium
Lead
0.5
5.4
2.6
Mercury
1.2
2.6
1.2
Molyb-
denum
1.8
21.0
10.0
Nickel
2.2
21.0
10.0
Selenium
0.9
11.0
5.2
Zinc
8.0
60.0
82.0
Total
Phos-
horus
5,700
8,100
2,600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
11
1
11:
1 111
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 11
1 11
1 11 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
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1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 111
1 1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11 •
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1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
Total
Phos-
1 •
••
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 187.62
WQ0038087
Terra Renewal Services Owner:
45.1 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Johnson, J L Predominant Soil Series:
45.1 Site #: WK-RJ-05 Field #:
11.5
Dan River
WK-RJ-05
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
Advance
Pierre
2/4/21
2
RVAF
1/28/21
3
Tyson-
Wilkes
1/28/21
4
Advance
Pierre
11/30/21
5
RVAF
11/30/21
6
Tyson-
Wilkes
11/30/21
7
8
9
10
11
12
% Solids
6.5
3.1
6.2
7.0
3.8
5.0
Arsenic
1 0.7
8.0
3.9
1 1.0
6.5
4.8
Cadmium
0.2
2.7
1.3
0.3
2.2
1.6
Copper
1 31.0
8.7
34.0
450.0
13.0
27.0
Chromium
Lead
0.5
5.4
2.6
1.9
4.3
3.2
Mercury
1.2
2.6
1.2
0.3
2.1
1.7
Molyb-
denum
1.8
21.0
10.0
2.6
17.0
13.0
Nickel
2.2
21.0
10.0
35.0
17.0
13.0
Selenium
0.9
11.0
5.2
1.3
8.7
6.4
Zinc
8.0
60.0
82.0
140.0
56.0
38.0
Total
Phos-
horus
5,700
8,100
2,600
800
19,000
3,700
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
App.
Event
0.04
1.00
1.10
0.00
0.61
1.42
Arsenic
0.000
0.016
0.009
0.000
0.008
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Cadmium
0.000
0.005
0.003
0.000
0.003
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Copper
0.002
0.017
0.075
0.000
0.016
0.076
0.000
0.000
0.000
0.000
0.000
0.000
0.187
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.011
0.006
0.000
0.005
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.031
Mercury
0.000
0.005
0.003
0.000
0.003
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Molyb-
0.000
0.042
0.022
0.000
0.021
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.122
denum
Nickel
0.000
0.042
0.022
0.000
0.021
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.122
Selenium
0.000
0.022
0.011
0.000
0.011
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.062
Zinc
0.001
0.120
0.181
0.000
1 0.068
0.108
0.000
0.000
0.000
0.000
0.000
0.000
0.477
Total
Phos-
0.410
16.151
5.725
0.000
23.218
10.471
0.000
0.000
0.000
0.000
0.000
0.000
55.976
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual):
WQ0038087 Cation Exchange Capacity (non 503 only):
Terra Renewal Services Owner: Red Oak Meadows, LLC Predominant Soil Series:
24.6 Acres Permitted: 24.6 Site #: WK-RJ-07 Field #:
43.44
11.2
Fairview
WK-RJ-07
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
Advance
Pierre
2/4/21
2
RVAF
1/28/21
3
Tyson-
Wilkes
1/28/21
4
5
6
7 j
8
9
Lj
11
12
% Solids
6.5
3.1
6.2
Arsenic
1 0.7
8.0
3.9
Cadmium
0.2
2.7
1.3
Copper
1 31.0
8.7
34.0
Chromium
Lead
0.5
5.4
2.6
Mercury
1.2
2.6
1.2
Molyb-
denum
1.8
21.0
10.0
Nickel
2.2
21.0
10.0
Selenium
0.9
11.0
5.2
Zinc
8.0
60.0
82.0
Total
Phos-
horus
5,700
8,100
2,600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
1 11
1 ••
1
1 111
1 1
1 11:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
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1 111
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
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1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 11
1 11 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 111
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11 •
1 111
1 1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 111
1 1 •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
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1 111
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
®
1 111
1 1:
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
Total
Phos-
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 18.91
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
13.5 Acres Permitted: 13.5 Site #: YK-YF-01 Field #:
12.6
Nathalie
YK-YF-01
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
11/30/21
2
RVAF
11/30/21
31
Tyson-
Wilkes
11/30/21
L4]5
6
7
8
9
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
1 0.3
2.2
1.6
Copper
1 450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings (Ualculated in Ibs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.07
0.78
0.56
Arsenic
0.000
0.010
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Cadmium
0.000
0.003
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
0.063
0.020
0.030
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.113
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.007
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Mercury
0.000
0.003
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.000
0.026
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.041
denum
Nickel
0.005
0.026
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Selenium
0.000
0.013
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Zinc
0.020
0.087
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.149
Total
Phos-
0.112
29.450
4.114
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
33.676
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 44.56
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
22.3 Acres Permitted: 22.3 Site #: YK-YF-03 Field #:
13.3
Clifford
YK-YF-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
6/10/21
2
RVAF
9/2/21
3
Tyson-
Wilkes
8/26/21
4
Advance
Pierre
11/30/21
5
RVAF
11/30/21
6
Tyson-
Wilkes
11/30/21
7
8
9
10 j
11
12
% Solids
3.7
6.4
5.8
7.0
3.8
5.0
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6.7
3.7
4.1
1.0
6.5
4.8
Cadmium
1 2.2
1.2
1.4
0.3
2.2
1.6
Copper
1 640.0
4.5
5.3
450.0
13.0
27.0
Chromium
Lead
6.2
2.5
2.8
1.9
4.3
3.2
Mercury
2.0
1.2
1 1.3
0.3
2.1
1 1.7
Molyb-
denum
18.0
9.9
11.0
2.6
17.0
13.0
Nickel
18.0
9.9
11.0
35.0
17.0
13.0
Selenium
8.9
5.0
5.5
1.3
8.7
6.4
Zinc
280.0
27.0
62.0
140.0
56.0
38.0
Total
Phos-
horus
7,400
9,100
3,600
800
19,000
3,700
Annual Heavy Metal Field Loadings (Ualculated in Ibs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.86
0.59
0.00
0.21
0.34
Arsenic
0.000
0.006
0.005
0.000
0.003
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Cadmium
0.000
0.002
0.002
0.000
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
0.000
0.008
0.006
0.000
0.006
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.038
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.003
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Mercury
0.000
0.002
0.002
0.000
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Molyb-
0.000
0.017
0.013
0.000
0.007
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.046
denum
Nickel
0.000
0.017
0.013
0.000
0.007
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.046
Selenium
0.000
0.009
0.006
0.000
0.004
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Zinc
0.000
0.047
0.073
0.000
0.024
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.169
Total
Phos-
0.000
15.688
4.219
0.000
8.094
2.494
0.000
0.000
0.000
0.000
0.000
0.000
30.495
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 11.30
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
23.3 Acres Permitted: 23.3 Site #: YK-YF-04 Field #:
13.2
Clifford
YK-YF-04
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
11/30/21
2
RVAF
11/30/21
31
Tyson-
Wilkes
11/30/21
L4]5
6
7
8
9
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
1 0.3
2.2
1.6
Copper
1 450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings (Ualculated in lbs/acre):
Total
1 1
2
J
4 j
5J
6j
7
81
91
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.16
0.32
Arsenic
0.000
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Cadmium
0.000
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Copper
0.000
0.004
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.001
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Mercury
0.000
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.000
0.006
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
denum
Nickel
0.000
0.006
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Selenium
0.000
0.003
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Zinc
0.000
0.018
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.043
Total
Phos-
0.000
6.194
2.383
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.577
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Terra Renewal Services, Inc Total Dry Tons Applied (Annual): 50.06
WQ0038087
Terra Renewal Services
Cation Exchange Capacity (non 503 only):
Owner: Mathis Properties, LLC Predominant Soil Series:
13.2
Fairview
51.5 Acres Permitted: 51.5 Site #: WK-YK-YF-5 Field #: WK-YK-YF-5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mPA2. % Solids use Raw Percent ft
Sample
or Com-
posite
Date
1 1
Advance
Pierre
11/30/21
2
RVAF
11/30/21
31
Tyson-
Wilkes
11/30/21
L4]5
6
7
8
9
10
11
12
% Solids
7.0
3.8
5.0
Arsenic
1.0
6.5
4.8
Cadmium
1 0.3
2.2
1.6
Copper
1 450.0
13.0
27.0
Chromium
Lead
1.9
4.3
3.2
Mercury
0.3
2.1
1 1.7
Molyb-
denum
2.6
17.0
13.0
Nickel
35.0
17.0
13.0
Selenium
1.3
8.7
6.4
Zinc
140.0
56.0
38.0
Total
Phos-
horus
800
19,000
3,700
Annual Heavy Metal Field Loadings (Ualculated in Ibs/acre):
Total
1 1
2j
3 j
4
5J
6
7
8
9
10
11
12
y
DT/Ac./
App.
14
Event
0.00
0.46
0.51
Arsenic
0.000
0.006
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.000
0.012
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.040
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.004
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Mercury
0.000
0.002
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.000
0.016
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
denum
Nickel
0.000
0.016
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Selenium
0.000
0.008
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Zinc
0.000
0.052
0.039
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.091
Total
Phos-
0.000
17.556
3.774
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
21.330
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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4
Laboratory Analyses:
- Nutrients, Metals, TCLP, Other

0p
0
PaceAnalyfical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:WA29002
Date Completed:02/11/2021
NIM�I�Mr�
02/12/2021 9:26 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WA29002
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids, the initial sample amount used for the following samples was 3x more than the
standard procedure: WA29002-001, WA29002-002. The LOQ has been adjusted accordingly.
The following samples were not fully oxidized after the addition of 15mL of HNO3: WA29002-001,
WA29002-002. This is indicated by the samples exhibiting persistent brown fumes after complete acid
addition. Due to being biosolids and having low percent solids, the samples will not be weighed to a lower
mass and analysis will proceed as usual.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WA29002
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson/Wilkesboro Solid 01/28/2021 1430 01/29/2021
002 Tyson/Harmony Solid 01/28/2021 1530 01/29/2021
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WA29002
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Tyson/Wilkesboro
Solid
% Volatile Solids
SM 2540G-
98
%
5
001
Tyson/Wilkesboro
Solid
Ammonia - N (gas
350.1
1500
mg/kg
5
001
Tyson/Wilkesboro
Solid
Nitrate -Nitrite - N (soluble)
353.2
21
mg/kg
5
001
Tyson/Wilkesboro
Solid
Phosphorus
365.1
2600
mg/kg
5
001
Tyson/Wilkesboro
Solid
TKN
351.2
62000
mg/kg
5
001
Tyson/Wilkesboro
Solid
Aluminum
6010D
500
mg/kg
6
001
Tyson/Wilkesboro
Solid
Copper
6010D
34
mg/kg
6
001
Tyson/Wilkesboro
Solid
Zinc
601OD
82
mg/kg
6
002
Tyson/Harmony
Solid
% Volatile Solids
SM 2540G-
90
%
7
002
Tyson/Harmony
Solid
Ammonia - N (gas
350.1
24000
mg/kg
7
002
Tyson/Harmony
Solid
Nitrate -Nitrite - N (soluble)
353.2
45
mg/kg
7
002
Tyson/Harmony
Solid
Phosphorus
365.1
8100
mg/kg
7
002
Tyson/Harmony
Solid
TKN
351.2
46000
mg/kg
7
002
Tyson/Harmony
Solid
Aluminum
6010D
14000
mg/kg
8
002
Tyson/Harmony
Solid
Calcium
6010D
23000
mg/kg
8
002
Tyson/Harmony
Solid
Copper
6010D
8.7
mg/kg
8
002
Tyson/Harmony
Solid
Potassium
6010D
5600
mg/kg
8
002
Tyson/Harmony
Solid
Sodium
6010D
6900
mg/kg
8
002
Tyson/Harmony
Solid
Zinc
6010D
60
mg/kg
8
(19 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4of12

Client: Terra Renewal Services, Inc. Laboratory ID: WA29002-001
Description: Tyson/Wilkesboro Matrix: Solid
Date Sampled:01/28/2021 1430 % Solids: 6.18 01/29/2021 2327
Date Received:01/29/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
02/04/2021 0109 MOM
81767
1 350.1
(Ammonia - N ) 350.1
5
02/04/2021 1205 DRD
81813
1
(Nitrate-Nitr) 353.2
1
02/08/2021 2200 SRB
82243
1
(Phosphorus) 365.1
5
02/04/2021 1006 DMA
02/02/2021 1829 81587
1
(Soil pH meas) 9045D
1
02/03/2021 1834 AAB
81768
1 351.4
(TKN) 351.2
5
02/03/2021 1111 DMA
02/02/2021 1829 81582
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
98
%
1
Ammonia - N (gas diffusion)
350.1
1500
810
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
21
3.2
mg/kg
1
Phosphorus
7723-14-0 365.1
2600
400
mg/kg
1
Soil pH measured in water @ 18.1 ° C
9045D
3.9
su
1
TKN
351.2
62000
2000
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 02/04/2021 1218 NCM
02/02/2021 2115 81616
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
280
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
280
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
280
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
280
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
280
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
280
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
280
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
109 41-132
Tetrachloro-m-xylene
103 35-106
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 02/02/2021 0923 JAB2 02/02/2021 0622 81496
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 1.2 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5of12

Client: Terra Renewal Services, Inc. Laboratory ID: WA29002-001
Description: Tyson/Wilkesboro Matrix: Solid
Date Sampled:01/28/2021 1430 % Solids: 6.18 01/29/2021 2327
Date Received:01/29/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 02/04/2021 1334 KSH2 02/02/2021 1115 81355
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
500
100
mg/kg
1
Arsenic
7440-38-2
6010D
ND
3.9
mg/kg
1
Cadmium
7440-43-9
6010D
ND
1.3
mg/kg
1
Calcium
7440-70-2
6010D
ND
1300
mg/kg
1
Copper
7440-50-8
6010D
34
2.6
mg/kg
1
Lead
7439-92-1
601OD
ND
2.6
mg/kg
1
Magnesium
7439-95-4
601OD
ND
1300
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
10
mg/kg
1
Nickel
7440-02-0
6010D
ND
10
mg/kg
1
Potassium
7440-09-7
601OD
ND
1300
mg/kg
1
Selenium
7782-49-2
601OD
ND
5.2
mg/kg
1
Sodium
7440-23-5
6010D
ND
1300
mg/kg
1
Zinc
7440-66-6
6010D
82
13
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6of12

Client: Terra Renewal Services, Inc. Laboratory ID: WA29002-002
Description: Tyson/Harmony Matrix: Solid
Date Sampled:01/28/2021 1530 % Solids: 3.10 01/29/2021 2327
Date Received:01/29/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
02/04/2021 0109 MOM
81767
1 350.1
(Ammonia - N ) 350.1
25
02/04/2021 1213 DRD
81813
1
(Nitrate-Nitr) 353.2
1
02/08/2021 2201 SRB
82243
2
(Phosphorus) 365.1
10
02/04/2021 1850 DMA
02/02/2021 1829 81587
1
(Soil pH meas) 9045D
1
02/03/2021 1759 AAB
81768
1 351.4
(TKN) 351.2
2
02/03/2021 1112 DMA
02/02/2021 1829 81582
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
90
%
1
Ammonia - N (gas diffusion)
350.1
24000
8100
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
45
6.5
mg/kg
1
Phosphorus
7723-14-0 365.1
8100
1600
mg/kg
2
Soil pH measured in water @ 17.3 ° C
9045D
6.1
su
1
TKN
351.2
46000
1600
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 02/04/2021 1231 NCM
02/02/2021 2115 81616
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
550
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
550
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
550
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
550
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
550
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
550
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
550
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
106 41-132
Tetrachloro-m-xylene
106 35-106
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 02/02/2021 0931 JAB2 02/02/2021 0622 81496
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471B ND 2.6 mg/kg 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7of12

Client: Terra Renewal Services, Inc. Laboratory ID: WA29002-002
Description: Tyson/Harmony Matrix: Solid
Date Sampled:01/28/2021 1530 % Solids: 3.10 01/29/2021 2327
Date Received:01/29/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 02/04/2021 1338 KSH2 02/02/2021 1115 81355
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
14000
210
mg/kg
1
Arsenic
7440-38-2
6010D
ND
8.0
mg/kg
1
Cadmium
7440-43-9
6010D
ND
2.7
mg/kg
1
Calcium
7440-70-2
6010D
23000
2700
mg/kg
1
Copper
7440-50-8
6010D
8.7
5.4
mg/kg
1
Lead
7439-92-1
601OD
ND
5.4
mg/kg
1
Magnesium
7439-95-4
601OD
ND
2700
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
21
mg/kg
1
Nickel
7440-02-0
6010D
ND
21
mg/kg
1
Potassium
7440-09-7
6010D
5600
2700
mg/kg
1
Selenium
7782-49-2
6010D
ND
11
mg/kg
1
Sodium
7440-23-5
6010D
6900
2700
mg/kg
1
Zinc
7440-66-6
6010D
60
27
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8of12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9of12

PACE ANALYTICAL SERVICES. LLC
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Pace Analytical Services, LLC (formerly Shealy
Environmental Services, Inc.)
106 Vantage Point Drive
West Columbia,
SC 29172
[phone]
Fax [phone]
www.pacelabs.com
Page 10 of 12
T

PACE ANALYTICAL SERVICES, LLC
North Carolina Permit Parameters
Rusiduals shall be a ly i Irr domonst.ato thy+ line s-surae t 7;15Cr.'$tivn
Sri Ro�t�very Act (RCRA 'l7xe aill Ys
9ht1' qsi [t . spb&fied in
Atmch t A, and the Pcrmittee sla.:ll rnair.ta-m d rcaults for a n1kd1 x = of frV a years. Any
exeopLiLl s flnm dW Nqui: l 11M in this c'OTkditi�'n sltiall i,e SPMifiod in r"Lti�lc'11x1Cdtt A.
nalysis shall:.jKd-d.Le Ike fnUowing parameters {t1 9 x09:11atory level is rnilligruaS lm liter
is ui pmnth=-S}
3. An awlysr shall '�n -zmdudul on rmidMls fma eaCJl uroe tc=atLng rauility �t ale fi'KRepuy
�, ificd Mi Attachmeat A, and ehe Pmmai _ee }hail Maintain file rowlts for a r 1blin 1w. of frve yeam
The analysts sly include tine folluwx na pr.r4meter&
� Alu�ixiwn 1�T�c.ury
�- �llmmemi�-I�Iitro�en N1al�'hderruul
O.
r�
Cadmi=
M
Gnidum
CbPgB
.
W
Lead
�
p��siurod
Nkkcl
jtrzt�-i[nLe Nitrogm
Pert Total Solids
pH
y`hcsplvo us
TERRA RENEWAL SERVICES
479-747-8192
Affarhawt ho COG fvr-.-.-S4urG25:
Potassium
MeTL-•U3ri
LLF.!1
TKN
Volatiio Solids
1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
samples Receiptcrracklist {SR10 (DAEotk18C-15) :,Evise :9J?912020
10,2011rty f I5wing Aithority; Pace ENV - WCOI. Pam I of 1
sample Receipt Checklist (SRO
CaraRere+val � ol�m 1T,s�ecte' b Malta- KS { 4]x3Sk�g21 Lot ii+= WA29002
- -
Won$ of recoipt, Pace CI lent � I[� I'$ Fo�Lx tether;
ye No 1. Were c1lstndy ssr4ls Present ou tho Coo'
Yes Rio MA 2. if eusiod sC9ri5 ware resent, were thou intact and unbrakolt
Ti f+trip IB; xa fvhlrrri_re Strip lD. rrn� _ Tesred b}:�.. —
C9rigitrrJ toeuparags+� trQan raCei}rt 1 L]oriVad (Correa 1 icr[3Per3# I C upon rz€s ipr °Solid Srn p Cup [i1:
1.2 11.2 '� NA INS. cC N& IN& 4C AA _INA oC
zhod: F13'�mperature Blank aiust Bottles lit Guri 1D; 5 _ TR Gum f nrrcetiun Factor: �C
raa+I, r.,rr.1A,+ wrtice �leeYackg ❑ lee 1lu,re
ElYesl Q-lo' UN
Yes U N
Yes N.
©-y-.;~ [IN
Y
ny
3. Jf#rmpemturoOfarty oyster exgwLed 6.VOC, xas 1'T itct [ iarran�7et 1`lvtlfier:`�
Pi41 was Hq:itied by. pbanc I On ail I 6e04u-f3cc (circle one)-
. 1 tha u,mrr_eniEd courie.'� packirlg 9.7P attars= ro this final?
S. Were proper cw-wly eL�rlures (.Ml`.n uishcdiiceelved) fol!owW7
6. WC.v 3iL1T-n la 11)5 listed on the CSC?
7- -3ra s$tnple [Dr listed on all 3empin coneaine-s2
R. was co;lecdm date & &Le 1].3te�d CM the cOCR' —
9_ Was cwllection rate & time listedaa 431 sWmple eontah'-S _
I0_ Did Ell iAAtaincr 1p be l in forrrEaliM (LD, date, tithe) a Ven w ith th t: COC"
11, Wvm tests to be performed lister ar t1re TE
l'�- Dio all s.rnp%!. aTrLve in the praPer con[ainers for each tr*st in A* in P.-Ood condition
J(unbrukun, lids on, etc:)?
lNo 13. w= adegn2lte sar_�ple vulema a4ailalAW
'g3 14, Were all sar,pl x rccci#cd v.ilhin the holdir t,mc {tr 48 Moors, wh:eb.1ver cameo :rrst7
t o 13. Were any yang les i;rsri�inors rrtissingiexcess (oirple anA) �s,rupiesl�fsn listed on COC7
16. For VOA and KSK-175 samples, 4wm bubbl present i~ peasize (W:or 6-In Li d k MV-.ef)
No L- 6r j N A in any- u1`CISa VOA 47815?
No { NA 17_ WMTc iIIDR, O+rne,taiS�nurriantS�Cr1 ]esrx�eitiedata pTT o�<�:
Ju 'NA l$, evEL ide sam 31.m received At a pFl �- 12 anid ou:fide-%xnplt-,S reccil"mJ at a pH > 97
af
- --. _ t -rry rFr, ...i la ,,.,11r373 1,`f08. fIrP11.. 5filrLt]_PS
No M l~I.4 f .
residual chlorine?
client Arks+rexlucs (i_e, rrsyuested dihilians ?Id5i14S31J deli nati4n5, ere.. •}
EDYe-No EVI2dA,enrreCtly Ma3crib-d ;r43En th0 COC intrFtre c�mmeEr secl:Qur iv L1 S?
s No 1, as to Ante number Listed an the: +:uutabWL- label'? if -cs, Qu nto'�
Sample Freservatiaa (,Mtrt` Ire cornple-.xd fcr arryr 3ample(s) incunrCtly p ;ertrr:d or wild ]i sidepace.)
SstltpEe(s� " �tircm rcreiv�ed inmCrectly W3e� v .d and were adjustod rx
in sarnpl- rewiving with _ml. of circle one: HIS{ k#, HNO3, HC:, NaOH using Sit 4 NA
Tirr,n of pmscrV3ti13n MA Lf moru tisau ones prewuwLiva is Ev ded, pl ,rsc t14te in 1he anmm431U itclo4o�
arnplc(s) HA
weru remived with bubbles -16 m m In diamul cv'.
�L�rplesa(3} x` ante recei4rxi 1MLlt TRC::r 0.5 EnglL (11:-k19 is; no) and tuere
d',usted accordirkOY in &maple rceaiving with sodium thiosulftrte (Na�S203) with-isealy ID;---
barcode'abols vpplied by, ►:Cc
{`.ircru r ellt5;
L7aLC; ptj29�2D3]
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 12

0p
0
PaceAnalyfical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:WB05005
Date Completed:02/22/2021
NIM�I�Mr�
02/22/2021 3:14 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
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'ye I
ANSI NdmlAccre00- Board
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Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WBO5005
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
% Volatile Solids
The following samples were analyzed outside of analytical holding time due to analyst oversight:
WB05005-001, WB05005-002.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WB05005
Sample Number Sample ID Matrix Date Sampled Date Received
001 Adv. Foods/Claremont Solid 02/04/2021 1430 02/05/2021
002 Perdue/Concord Solid 02/04/2021 1500 02/05/2021
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WB05005
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Adv. Foods/Claremont
Solid
% Volatile Solids
SM 2540G-
90 H
%
5
001
Adv. Foods/Claremont
Solid
Ammonia - N (gas
350.1
340
mg/kg
5
001
Adv. Foods/Claremont
Solid
Nitrate -Nitrite - N (soluble)
353.2
16
mg/kg
5
001
Adv. Foods/Claremont
Solid
Phosphorus
365.1
5700
mg/kg
5
001
Adv. Foods/Claremont
Solid
TKN
351.2
25000
mg/kg
5
001
Adv. Foods/Claremont
Solid
Aluminum
601OD
870
mg/kg
6
001
Adv. Foods/Claremont
Solid
Copper
601OD
31
mg/kg
6
001
Adv. Foods/Claremont
Solid
Nickel
601OD
2.2
mg/kg
6
001
Adv. Foods/Claremont
Solid
Sodium
601OD
260
mg/kg
6
001
Adv. Foods/Claremont
Solid
Zinc
601OD
8.0
mg/kg
6
002
Perdue/Concord
Solid
% Volatile Solids
SM 2540G-
84 H
%
7
002
Perdue/Concord
Solid
Ammonia - N (gas
350.1
860
mg/kg
7
002
Perdue/Concord
Solid
Nitrate -Nitrite - N (soluble)
353.2
40
mg/kg
7
002
Perdue/Concord
Solid
Phosphorus
365.1
26000
mg/kg
7
002
Perdue/Concord
Solid
TKN
351.2
33000
mg/kg
7
002
Perdue/Concord
Solid
Aluminum
601OD
34000
mg/kg
8
002
Perdue/Concord
Solid
Potassium
601OD
7000
mg/kg
8
002
Perdue/Concord
Solid
Sodium
601OD
11000
mg/kg
8
(18 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4of12

Client:Terra Renewal Services, Inc. Laboratory ID:WB05005-001
Description: Adv. Foods/Claremont Matrix: Solid
Date Sampled:02/04/2021 1430 % Solids: 6.54 02/10/2021 2345
Date Received:02/05/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
02/15/2021 0025 MOM
82943
1 350.1
(Ammonia - N) 350.1
1
02/08/2021 1647 KFE
82140
1
(Nitrate-Nitr) 353.2
1
02/16/2021 2135 SRB
82951
3
(Phosphorus) 365.1
10
02/21/2021 1048 DMA
02/19/2021 1753 83053
1
(Soil pH meas) 9045D
1
02/09/2021 2014 AAB
82081
3 351.4
(TKN) 351.2
2
02/17/2021 1206 DMA
02/16/2021 1828 83036
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
90 H
%
1
Ammonia - N (gas diffusion)
350.1
340
150
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
16
3.1
mg/kg
1
Phosphorus
7723-14-0 365.1
5700
760
mg/kg
3
Soil pH measured in water C> 18.9 ° C
9045D
4.5
su
1
TKN
351.2
25000
760
mg/kg
3
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 02/15/2021 1103 NCM
02/14/2021 1119 82827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
260
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
260
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
260
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
260
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
260
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
260
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
260
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
93 41-132
Tetrachloro-m-xylene
90 35-106
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 02/09/2021 1353 JAB2 02/09/2021 0707 82263
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471 B N D 1.2 mg/kg 1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WB05005-001
Description: Adv. Foods/Claremont Matrix: Solid
Date Sampled:02/04/2021 1430 % Solids: 6.54 02/10/2021 2345
Date Received:02/05/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 02/11/2021 2353 KSH2 02/10/2021 0956 82277
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
870
18
mg/kg
1
Arsenic
7440-38-2
6010D
ND
0.68
mg/kg
1
Cadmium
7440-43-9
6010D
ND
0.23
mg/kg
1
Calcium
7440-70-2
6010D
ND
230
mg/kg
1
Copper
7440-50-8
6010D
31
0.45
mg/kg
1
Lead
7439-92-1
6010D
ND
0.45
mg/kg
1
Magnesium
7439-95-4
6010D
ND
230
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
1.8
mg/kg
1
Nickel
7440-02-0
6010D
2.2
1.8
mg/kg
1
Potassium
7440-09-7
6010D
ND
230
mg/kg
1
Selenium
7782-49-2
6010D
ND
0.90
mg/kg
1
Sodium
7440-23-5
6010D
260
230
mg/kg
1
Zinc
7440-66-6
6010D
8.0
2.3
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WB05005-002
Description: Perdue/Concord Matrix: Solid
Date Sampled:02/04/2021 1500 % Solids: 4.73 02/05/2021 2331
Date Received:02/05/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
02/15/2021 0025 MOM
82943
1 350.1
(Ammonia - N) 350.1
1
02/08/2021 1649 KFE
82140
1
(Nitrate-Nitr) 353.2
1
02/16/2021 2136 SRB
82951
3
(Phosphorus) 365.1
25
02/21/2021 1130 DMA
02/19/2021 1753 83053
1
(Soil pH meas) 9045D
1
02/09/2021 2016 AAB
82081
3 351.4
(TKN) 351.2
2
02/17/2021 1206 DMA
02/16/2021 1828 83036
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
84 H
%
1
Ammonia - N (gas diffusion)
350.1
860
210
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
40
4.2
mg/kg
1
Phosphorus
7723-14-0 365.1
26000
2600
mg/kg
3
Soil pH measured in water C> 19 ° C
9045D
5.3
su
1
TKN
351.2
33000
1100
mg/kg
3
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 02/15/2021 1117 NCM
02/14/2021 1119 82827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
350
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
350
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
350
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
350
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
350
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
350
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
350
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
80 41-132
Tetrachloro-m-xylene
81 35-106
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471 B 7471 B 1 02/09/2021 1355 JAB2 02/09/2021 0707 82263
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 7471 B N D 1.6 mg/kg 1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WB05005-002
Description: Perdue/Concord Matrix: Solid
Date Sampled:02/04/2021 1500 % Solids: 4.73 02/05/2021 2331
Date Received:02/05/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 02/11/2021 2356 KSH2 02/10/2021 0956 82277
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
34000
400
mg/kg
1
Arsenic
7440-38-2
6010D
ND
15
mg/kg
1
Cadmium
7440-43-9
6010D
ND
5.0
mg/kg
1
Calcium
7440-70-2
6010D
ND
5000
mg/kg
1
Copper
7440-50-8
6010D
ND
10
mg/kg
1
Lead
7439-92-1
6010D
ND
10
mg/kg
1
Magnesium
7439-95-4
6010D
ND
5000
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
40
mg/kg
1
Nickel
7440-02-0
6010D
ND
40
mg/kg
1
Potassium
7440-09-7
6010D
7000
5000
mg/kg
1
Selenium
7782-49-2
6010D
ND
20
mg/kg
1
Sodium
7440-23-5
6010D
11000
5000
mg/kg
1
Zinc
7440-66-6
6010D
ND
50
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9of12

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 10 of 12
0
now

PACE ANALYTICAL SERVICES, LLC
North Carolina Permit Pararnators
2. Rcsiduab shalt be mua=}led to camoatrate thcy src ourca Cons�►raCion
Lad Recowry A,-,t (RC:RA). Tlie art=1 fie8
specified in
A14abinenl A, and tht Fsrmirzee shall iuuutaxn them results fer a minirnw-o of fiva yea-rs Any
exceptions € aL the >w.uL-=Pnts in this OcurfiUou Sliall be specified in A.ttwJurne It A.
the nalysis shall irrjur'n the i.'ou',',`Ag P==tus (tile Mgulatlwy lGwt:l in miliigams prat lit :r
is in Parentheses
3, An anmlysia sUL. be w,,AuUuJ un-DsidualR from eac11 source gMienati fael3ty at -11u hequency
sp=fmd in AtW1wij-,nt A, and dw Piurmittee 41HU Maimain the rMULE -or a Minimum of five years.
Ae 81L81ysis ibdd ,irwlude Lhu fulkm-inn parameters:
r....
_ -
_ Air um
Bvi=Ury
Potdssiu,a
O
A.loPnunrir-NiArDgen
e
�eleuieim
Molybdonum
Arsw c
Nickel
SDdiara
w�'i1f]mi�zm
I�1tYRt��1t11t1� �11T(]�+.[l
CBicium
ft-cul fatal Sohda
Tl
_ Tint;
VolaWe Sol Us
Cowu
PH
Jxad Phosphorus
TERRA RENEWAL SERVICES
47C-747-8192
Attachmmt to COC tor..,..8-aw=s: data,
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
Sarnpl-Es Receipt Checklist (SRC) (MEDO 15) e4�1 t d 9,'29f2076
'0AFn41AP71 Issui7EAuthor'ly Pace ENV -Vd 7L Page y rr L
Sample Receipt Checklists RQ
GII#�itir_ 74-rmRrnc.v:d Coolcrinspeclad e'dE.W: JS11 _a 02.+U5i2Q2L Lot4; W095005
Means of rL�cc;ipt: I j Pace l bent L1P5 Ferlf x Otllcr; �
Yc w ,p, No 11L Wrrc w0ffdw seals 1)M5_l on the coolrsrll
Yea No V WA 2. Ii- custod qls were nroso:tt, were they inimt uW u nbrolDu'r'
pil Swig II)- NA Chlorine Strip ID- HA Tuslvd by, �
prigrinal temjlar s-tire uproe re%�,ai-it i 'ived (Colrectcdl L-mprwatotr upwt rtctipt �uSalid Simp Cup 1r): 2u-05
1A j1. 0C rdA fY oC NA I NA o,C NA INN oC
Ma:thcd: �Tempemum J�lar,k ❑ granat BuUl 5 1R Gua ID; 5 IR Gun Curr+ctian �Factar � °C
M4ctltvd {oftrsoiant: 0 WO Zcu D lce Packs ❑ Dry 1= ❑ Nora
FMvrN 3- Iftvrnperrlurc OF2uiy cDDlermftded 6-D C,was Net -Brea 4 anagerNoti(Ted?
[� " !aJaM was Nnti find ity_ pmrc l err_all 1 ftzelto-face (eiTtil0 ase).
,4 4. la the torrmerctf.l mirit;r' pack=ng slip attakbe3 io t`"his faun?
d Yes Noi. Vb'er'e r Mrtody procedures (reiinqulshedlreceived) fi�;luwti'eal?
Yes No6, WLrc sample IDs listed an t110 C00
,f Yes No 7. V4=sample IUs h3tQd un ail sainple con#aindM?
Yes LJNu S, %Vm. collection date & time listed on the WC?
PM
Yes No 9' INIMSC011eclian dale, & tune listed analllimulp1t: uirrtainers?
Yes ❑ No I O, D3 d al I contait}cr lubal information (fl), daft, 6") a ee with the C C?
Yesl FINQ 11. Were Lasts La be ptirroTmed illsted an the t-7007
' I ❑Nc� 12. Did all samples ayfive in Pha pTi r coiw*a:ners forcau,lt tcsL widlar in goon. condition
(unbroken, lids cn, etc,)?
❑Ye51 El No
13. Wtu 0Uquam sam le volume available'?
14, Were al_ samples received within % the 1icrlr:irgthnc or 49 h0'.Irs, %vhi0hcrcr Lamas fiW-
15, �b=r: any sainplcs can-LinCrS Not listed oil CUIC?
❑ 16. Fv_• YC}A and R -L?S samples, v.= bubbles pLese�rt ('�{"ur term in diumreer)
NA In krny oCthe V40A vials?
?tiA I7- Were all DR irnetalslnutrient samples received at g p:
NA I S" Were all cywpni xarnpies received at a pN > 12 aild sal
^(/ �^� I Y' WOM ALI appl LC
iN No I.TJI I,�i —i ;.,-1 n.kI yr`l
< �n
a
Mffriplcs iveeived ar a pH > 99
{()_5ffjE_!7L) SnmVle% Fret rr
Y:es D�20- Mere client rouse rWrequcsta (i.c.: ul ut3ted dilutions, MiSINISID cesignadam, ctc, , ,
[b)
❑ �' s ❑ ° correctly tl'ansaed fmm the C OC into lnc d
counrienl seain n L M,3?
vie N" 11 [lie uuatc nuynbt .' :fisted on tlta I;o:lrainc; larul? Ifyes, Quote V --
Preservation (MiAit bt-, uOulpteted for Onp ra*tple(e} ineomcctly gra.*erved or writ headspoct,)
r�ple(s} ;n _ vvt rcxxiVetl incarreatly urzservccI and wei%, adjuawd acmdiagly
sarnp:e. rerceiyul,g with irL of circle one: H2SO4, HNO3, HCI, NaOR usirig SR 0 '"
rnn ref timmrvadcu NA L'taore thm we preoxyattvc is nocdad. please ngte in tba arrr„ments belaw.
rnp e(s) N vet-e rcQci-%`ed with hubbtes>6 mm ;a diwneter-
Rrples(s)" _ _14m receiver vuith TRC i 0.5 mgrL Cif ttl9 is Ito) and ti"rn
jumd accordindy in samrle mceiving with ;tudiwn twostilfats (' a2.9201) tuhh Shealy 1 D; N-�
barrr.,pde labels applied by' _ _ Daw. 02MI.102L
CammMls_
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 12 of 12

0p
0
PaceAnalyfical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:WF02004
Date Completed:06/14/2021
NIM�I�Mr�
06/15/2021 8:45 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WF02004
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low percent solids, the following samles were weighed at 3x the standard procedure: WF02004-
001 and WF02004-002. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WF02004
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson - Wilksboro Solid 06/01/2021 1330 06/02/2021
002 Tyson - Harmony Solid 06/01/2021 1430 06/02/2021
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WF02004
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Tyson
- Wilksboro
Solid
% Volatile Solids
SM 2540G-
99
%
5
001
Tyson
- Wilksboro
Solid
Ammonia - N (gas
350.1
12000
mg/kg
5
001
Tyson
- Wilksboro
Solid
Nitrate -Nitrite - N (soluble)
353.2
38
mg/kg
5
001
Tyson
- Wilksboro
Solid
Phosphorus
365.1
2800
mg/kg
5
001
Tyson
- Wilksboro
Solid
TKN
351.2
79000
mg/kg
5
001
Tyson
- Wilksboro
Solid
Aluminum
601OD
310
mg/kg
6
001
Tyson
- Wilksboro
Solid
Copper
601OD
28
mg/kg
6
001
Tyson
- Wilksboro
Solid
Zinc
601OD
63
mg/kg
6
002
Tyson
- Harmony
Solid
% Volatile Solids
SM 2540G-
89
%
7
002
Tyson
- Harmony
Solid
Ammonia - N (gas
350.1
27000
mg/kg
7
002
Tyson
- Harmony
Solid
Nitrate -Nitrite - N (soluble)
353.2
51 S
mg/kg
7
002
Tyson
- Harmony
Solid
Phosphorus
365.1
6400
mg/kg
7
002
Tyson
- Harmony
Solid
TKN
351.2
43000
mg/kg
7
002
Tyson
- Harmony
Solid
Aluminum
601OD
4600
mg/kg
8
002
Tyson
- Harmony
Solid
Calcium
601OD
15000
mg/kg
8
002
Tyson
- Harmony
Solid
Copper
601OD
6.8
mg/kg
8
002
Tyson
- Harmony
Solid
Potassium
601OD
3900
mg/kg
8
002
Tyson
- Harmony
Solid
Sodium
601OD
5200
mg/kg
8
002
Tyson
- Harmony
Solid
Zinc
601OD
30
mg/kg
8
(19 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 4of12

Client:Terra Renewal Services, Inc. Laboratory ID:WF02004-001
Description: Tyson - Wilksboro Matrix: Solid
Date Sampled:06/01/2021 1330 % Solids: 4.83 06/03/2021 0023
Date Received:06/02/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
06/08/2021 2358 MOM
94835
1 350.1
(Ammonia - N) 350.1
25
06/08/2021 1456 KFE
94701
1
(Nitrate-Nitr) 353.2
1
06/03/2021 2034 AAB
94397
1
(Phosphorus) 365.1
5
06/03/2021 1616 DMA
06/03/2021 1133 94171
1
(Soil pH meas) 9045D
1
06/11/2021 1924 DAK
95346
1 351.4
(TKN) 351.2
5
06/10/2021 1339 DMA
06/09/2021 1758 94960
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
99
%
1
Ammonia - N (gas diffusion)
350.1
12000
5200
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
38
4.1
mg/kg
1
Phosphorus
7723-14-0 365.1
2800
520
mg/kg
1
Soil pH measured in water C> 21.6 ° C
9045D
5.8
su
1
TKN
351.2
79000
5200
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 06/11/2021 1550 JPB
06/09/2021 2133 94992
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
350
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
350
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
350
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
350
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
350
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
350
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
350
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
90 41-132
Tetrachloro-m-xylene
78 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 06/10/2021 1702 CMS2 06/09/2021 1510 94942
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B N D 1.6
mg/kg 1
LOQ - Limit of Quantitation
B - Detected in the method blank
E - Quantitation of compound exceeded the calibration range
Q - Surrogate failure
ND - Not detected at or above the LOQ
N - Recovery is out of criteria
P - The RPD between two GC columns exceeds 40%
L - LCS/LCSD failure
H - Out of holding time
W - Reported on wet weight basis
S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WF02004-001
Description: Tyson - Wilksboro Matrix: Solid
Date Sampled:06/01/2021 1330 % Solids: 4.83 06/03/2021 0023
Date Received:06/02/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 06/10/2021 1228 JMH 06/10/2021 0417 94929
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
310
130
mg/kg
1
Arsenic
7440-38-2
6010D
ND
4.9
mg/kg
1
Cadmium
7440-43-9
6010D
ND
1.6
mg/kg
1
Calcium
7440-70-2
6010D
ND
1600
mg/kg
1
Copper
7440-50-8
6010D
28
3.3
mg/kg
1
Lead
7439-92-1
6010D
ND
3.3
mg/kg
1
Magnesium
7439-95-4
6010D
ND
1600
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
13
mg/kg
1
Nickel
7440-02-0
6010D
ND
13
mg/kg
1
Potassium
7440-09-7
6010D
ND
1600
mg/kg
1
Selenium
7782-49-2
6010D
ND
6.5
mg/kg
1
Sodium
7440-23-5
6010D
ND
1600
mg/kg
1
Zinc
7440-66-6
6010D
63
16
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q - Surrogate failure
L - LCS/LCSD failure
S - MS/MSD failure
Page 6 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WF02004-002
Description: Tyson - Harmony Matrix: Solid
Date Sampled:06/01/2021 1430 % Solids: 3.64 06/03/2021 0023
Date Received:06/02/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
06/08/2021 2358 MOM
94835
1 350.1
(Ammonia - N) 350.1
25
06/08/2021 1416 KFE
94701
1
(Nitrate-Nitr) 353.2
1
06/03/2021 2035 AAB
94397
1
(Phosphorus) 365.1
5
06/03/2021 1617 DMA
06/03/2021 1133 94171
1
(Soil pH meas) 9045D
1
06/11/2021 1926 DAK
95346
1 351.4
(TKN) 351.2
2
06/10/2021 1339 DMA
06/09/2021 1758 94960
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
89
%
1
Ammonia - N (gas diffusion)
350.1
27000
6900
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
51 S
5.5
mg/kg
1
Phosphorus
7723-14-0 365.1
6400
690
mg/kg
1
Soil pH measured in water @ 21.6 ° C
9045D
5.9
su
1
TKN
351.2
43000
2700
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 06/11/2021 1604 JPB
06/09/2021 2133 94992
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
470
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
470
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
470
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
470
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
470
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
470
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
470
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
103 41-132
Tetrachloro-m-xylene
95 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 06/10/2021 1705 CMS2 06/09/2021 1510 94942
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B N D 2.2
mg/kg 1
LOQ - Limit of Quantitation
B - Detected in the method blank
E - Quantitation of compound exceeded the calibration range
Q - Surrogate failure
ND - Not detected at or above the LOQ
N - Recovery is out of criteria
P - The RPD between two GC columns exceeds 40%
L - LCS/LCSD failure
H - Out of holding time
W - Reported on wet weight basis
S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WF02004-002
Description: Tyson - Harmony Matrix: Solid
Date Sampled:06/01/2021 1430 % Solids: 3.64 06/03/2021 0023
Date Received:06/02/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 06/10/2021 1418 JMH 06/10/2021 0417 94929
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
4600
170
mg/kg
1
Arsenic
7440-38-2
6010D
ND
6.4
mg/kg
1
Cadmium
7440-43-9
6010D
ND
2.1
mg/kg
1
Calcium
7440-70-2
6010D
15000
2100
mg/kg
1
Copper
7440-50-8
6010D
6.8
4.3
mg/kg
1
Lead
7439-92-1
6010D
ND
4.3
mg/kg
1
Magnesium
7439-95-4
6010D
ND
2100
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
17
mg/kg
1
Nickel
7440-02-0
6010D
ND
17
mg/kg
1
Potassium
7440-09-7
6010D
3900
2100
mg/kg
1
Selenium
7782-49-2
6010D
ND
8.6
mg/kg
1
Sodium
7440-23-5
6010D
5200
2100
mg/kg
1
Zinc
7440-66-6
6010D
30
21
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q - Surrogate failure
L - LCS/LCSD failure
S - MS/MSD failure
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9of12

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,
LLC (formerly Shealy Environmental
Services, Inc.)
106 Vantage Point Drive
West Columbia,
SC 29172
[phone]
Fax [phone] www.pacelabs.corn
Page 10 of 12
C a
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PACE ANALYTICAL SERVICES, LLC
North Carolina Permit Parameters
2_ RasiduAls shall be anal}^red W demoistmic diet lue - srauecc Gin �cra'n[:on
end Xj3pavcry Aut (RCRA} The an
S -cqusaicy 6peodi in
Am.chm.cnt k and the Per,. luee snarl mamtairi. thmt: rewll s fcr a nx n` ujn of five year& Any
execptiars from trfe regWreuw.& in ik s.00radit on shall be specifni in AIW-2 uueat A
'xbj?.�naiysis shall inrdak Eha, foUDwing paramcters (die reguhtwy b ve1 1A miftream per liter
iH iu pf-IM11ILesen�
3.
An analysis shall Ic conducted on resjduals frara e h r49 racrating faeay at the ftcq=Tpcy
spciJf1cd in Attacbinent A, and the ehaU oja.intaLj to jaQU for a miriim m of five year:.
The analysis u.irwhidetlse fuD wing "zmttcrx
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Aluminum Meraary
P sitIru
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A�tLcxania-itt,��eo �f�;lyburuc�t7t
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Mag ncsiutu
-
$
TERRA RENEWAL SERVICES
Attachmmnttn COC far__.._S.*ur-ces- sue, rk, ,l e► _ Date
e-5
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
Samples rierelpt Ulnerldla {SRC) (INIEN23C-15) FteVI512d:5129J'2020
t9r' yQ I#W .ing Autflority Pacc ENV .. WOOL ?ape i of 1
Sample Receipt Checklist ( RQ
Client- Lora rn-ewal Cooter bsperled E�edaw: 1RG2 , Ogn-2217111 LuL 8; 1VFM04
ars of mcrypt: Pace
CI iont ! UP5 1'extrxYULI
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PNI was Noti:iCslby; phon, JemaiI i-fi.:co-to-face (circle one).
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10. DiLl LdI OIIlliriir label irLL% nfation (JD, date, tirrra) agrm with the COC?
7'
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lam, Did ail sarnp,es arrive ;u Lit$ proper eontain=rs for CM11 test andhtt in gooc condition
[unbroken, lids on, Ctcj! ._
, ❑Yes
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Is_ Was adequate sample vohime availably?
✓ Y.QSj
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17. Were al l DR-0/metn18h-lutricatt sarri pies received at a pli of ¢ w
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18. Were al cyanide Sair11 k:s xwivcd at & el I ;� 12 and srslfrrin smrkp les received a . pH > T.
Wcros applicabJeNI1113'KNJcymnidclpie:lo. S.IJ¢G$,3(cG.3[rg/L)samplesTreeof,
residual chlorine?
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correctly transcribed from the COC JaiW tluu cumircnt sacti6n in [J S?
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sairr e(sj \h _ were -received item-rceffy pl'eserved and wcrc xdj!mled acevixijaZly
to sarr_pde raceivingwith NA mLofcire12 one; MS04,IIN03, 11CI, -NaOH icing Si-4 hA
Lima ofpreservatk-on KA Ifrnora than anc,, preservative -s needed, pkast no-e in ihu corr]ment8 below,
�aimrlf(s) NA were m"ivcd with bubbics >� rtkru in diammi'.
aii "'A were i iVC{l with '11{I_: > 0, 7 rn tl , (if Ot 9 is rjo) and were
lus'xd uworaingly in sample IleoMvE1g wi-I sodituil thiesulfnte (Njj282o,) wide Shealy 1-D- I`11A k
SIC barcode Itbr.ls apFLed by 1[tC2 1]atle; t 97J2321
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 12 of 12

0p
0
PaceAnalyfical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:WF11024
Date Completed:06/25/2021
NIM�I�Mr�
06/25/2021 2:51 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
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ANSI NdmlAccre00- Board
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Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WF11024
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to percent solids, the following samples were weighed out at 3x the standard procedure: WF11024-
001, WF11024-002. The LOQ has been adjusted.
PCBs by GC
The following sample was diluted due to the nature of the sample matrix: WF11024-002. The LOQ has
been elevated to reflect the dilution.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WF11024
Sample Number Sample ID Matrix Date Sampled Date Received
001 Perdue/Concord Solid 06/10/2021 1430 06/11 /2021
002 Advanced Foods/Claremont Solid 06/10/2021 1530 06/11 /2021
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WF11024
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
Perdue/Concord
Solid
% Volatile Solids
SM 2540G-
89
%
5
001
Perdue/Concord
Solid
Ammonia - N (gas
350.1
3000
S
mg/kg
5
001
Perdue/Concord
Solid
Nitrate -Nitrite - N (soluble)
353.2
27
S
mg/kg
5
001
Perdue/Concord
Solid
Phosphorus
365.1
22000
S
mg/kg
5
001
Perdue/Concord
Solid
TKN
351.2
47000
mg/kg
5
001
Perdue/Concord
Solid
Aluminum
601OD
19000
mg/kg
6
001
Perdue/Concord
Solid
Calcium
601OD
2200
mg/kg
6
001
Perdue/Concord
Solid
Copper
601OD
7.3
mg/kg
6
001
Perdue/Concord
Solid
Potassium
601OD
6300
mg/kg
6
001
Perdue/Concord
Solid
Sodium
601OD
7800
mg/kg
6
001
Perdue/Concord
Solid
Zinc
601OD
83
mg/kg
6
002
Advanced Foods/Claremont
Solid
% Volatile Solids
SM 2540G-
89
%
7
002
Advanced Foods/Claremont
Solid
Ammonia - N (gas
350.1
1500
mg/kg
7
002
Advanced Foods/Claremont
Solid
Nitrate -Nitrite - N (soluble)
353.2
36
mg/kg
7
002
Advanced Foods/Claremont
Solid
Phosphorus
365.1
7400
S
mg/kg
7
002
Advanced Foods/Claremont
Solid
TKN
351.2
7700
mg/kg
7
002
Advanced Foods/Claremont
Solid
Aluminum
601OD
14000
mg/kg
8
002
Advanced Foods/Claremont
Solid
Calcium
601OD
4400
mg/kg
8
002
Advanced Foods/Claremont
Solid
Copper
601OD
640
mg/kg
8
002
Advanced Foods/Claremont
Solid
Lead
601OD
6.2
mg/kg
8
002
Advanced Foods/Claremont
Solid
Nickel
601OD
34
mg/kg
8
002
Advanced Foods/Claremont
Solid
Potassium
601OD
2200
mg/kg
8
002
Advanced Foods/Claremont
Solid
Sodium
601OD
13000
mg/kg
8
002
Advanced Foods/Claremont
Solid
Zinc
601OD
280
mg/kg
8
(24 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4of12

Client:Terra Renewal Services, Inc. Laboratory ID: WF11024-001
Description: Perdue/Concord Matrix: Solid
Date Sampled:06/10/2021 1430 % Solids: 5.70 06/12/2021 2001
Date Received: 06/11/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
06/17/2021 2357 MOM
95937
1 350.1
(Ammonia - N) 350.1
5
06/16/2021 1452 KFE
95636
1
(Nitrate-Nitr) 353.2
1
06/16/2021 2108 AAB
95887
1
(Phosphorus) 365.1
25
06/14/2021 1345 DMA
06/11/2021 1709 95282
1
(Soil pH meas) 9045D
1
06/13/2021 1952 NBW
95369
1 351.4
(TKN) 351.2
5
06/14/2021 1326 DMA
06/11/2021 1800 95288
CAS Analytical
Parameter
Number Method
Result
Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
89
%
1
Ammonia - N (gas diffusion)
350.1
3000
S
880
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
27
S
3.5
mg/kg
1
Phosphorus
7723-14-0 365.1
22000
S
2200
mg/kg
1
Soil pH measured in water Ca) 21.3 ° C
9045D
4.5
su
1
TKN
351.2
47000
4400
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 06/24/20211403 JPB
06/18/20211511 96014
CAS Analytical
Parameter
Number Method
Result
Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
300
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
300
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
300
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
300
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
300
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
300
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
300
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
95 41-132
Tetrachloro-m-xylene
94 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 06/16/2021 1738 CMS2 06/15/2021 1638 95526
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B N D 1.4
mg/kg 1
LOQ - Limit of Quantitation
B - Detected in the method blank
E - Quantitation of compound exceeded the calibration range
Q - Surrogate failure
ND - Not detected at or above the LOQ
N - Recovery is out of criteria
P - The RPD between two GC columns exceeds 40%
L - LCS/LCSD failure
H - Out of holding time
W - Reported on wet weight basis
S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID: WF11024-001
Description: Perdue/Concord Matrix: Solid
Date Sampled:06/10/2021 1430 % Solids: 5.70 06/12/2021 2001
Date Received:06/11/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 06/17/2021 0655 JMH 06/16/2021 1038 95491
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
19000
110
mg/kg
1
Arsenic
7440-38-2
6010D
ND
4.0
mg/kg
1
Cadmium
7440-43-9
6010D
ND
1.3
mg/kg
1
Calcium
7440-70-2
6010D
2200
1300
mg/kg
1
Copper
7440-50-8
6010D
7.3
2.7
mg/kg
1
Lead
7439-92-1
6010D
ND
2.7
mg/kg
1
Magnesium
7439-95-4
6010D
ND
1300
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
11
mg/kg
1
Nickel
7440-02-0
6010D
ND
11
mg/kg
1
Potassium
7440-09-7
6010D
6300
1300
mg/kg
1
Selenium
7782-49-2
6010D
ND
5.3
mg/kg
1
Sodium
7440-23-5
6010D
7800
1300
mg/kg
1
Zinc
7440-66-6
6010D
83
13
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q - Surrogate failure
L - LCS/LCSD failure
S - MS/MSD failure
Page 6 of 12

Client:Terra Renewal Services, Inc. Laboratory ID: WF11024-002
Description: Advanced Foods/Claremont Matrix: Solid
Date Sampled:06/10/2021 1530 % Solids: 3.71 06/12/2021 2001
Date Received: 06/11/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
06/17/2021 2357 MOM
95937
1 350.1
(Ammonia - N) 350.1
2
06/16/2021 1458 KFE
95636
1
(Nitrate-Nitr) 353.2
1
06/16/2021 2112 AAB
95887
2
(Phosphorus) 365.1
10
06/17/2021 1816 DMA
06/11/2021 1709 95282
1
(Soil pH meas) 9045D
1
06/13/2021 1953 NBW
95369
1 351.4
(TKN) 351.2
1
06/14/2021 1233 DMA
06/11/2021 1800 95288
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
89
%
1
Ammonia - N (gas diffusion)
350.1
1500
540
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
36
5.4
mg/kg
1
Phosphorus
7723-14-0 365.1
7400 S
1300
mg/kg
2
Soil pH measured in water C> 21.4 ° C
9045D
5.5
su
1
TKN
351.2
7700
1300
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
5 06/24/20211535 JPB
06/18/20211511 96014
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
2300
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
2300
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
2300
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
2300
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
2300
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
2300
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
2300
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
47 41-132
Tetrachloro-m-xylene
54 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 06/16/2021 1741 CMS2 06/15/2021 1638 95526
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B N D 2.0
mg/kg 1
LOQ - Limit of Quantitation
B - Detected in the method blank
E - Quantitation of compound exceeded the calibration range
Q - Surrogate failure
ND - Not detected at or above the LOQ
N - Recovery is out of criteria
P - The RPD between two GC columns exceeds 40%
L - LCS/LCSD failure
H - Out of holding time
W - Reported on wet weight basis
S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 12

Client:Terra Renewal Services, Inc. Laboratory ID: WF11024-002
Description: Advanced Foods/Claremont Matrix: Solid
Date Sampled:06/10/2021 1530 % Solids: 3.71 06/12/2021 2001
Date Received:06/11/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 06/17/2021 0659 JMH 06/16/2021 1038 95491
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
14000
180
mg/kg
1
Arsenic
7440-38-2
6010D
ND
6.7
mg/kg
1
Cadmium
7440-43-9
6010D
ND
2.2
mg/kg
1
Calcium
7440-70-2
6010D
4400
2200
mg/kg
1
Copper
7440-50-8
6010D
640
4.5
mg/kg
1
Lead
7439-92-1
6010D
6.2
4.5
mg/kg
1
Magnesium
7439-95-4
6010D
ND
2200
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
18
mg/kg
1
Nickel
7440-02-0
6010D
34
18
mg/kg
1
Potassium
7440-09-7
6010D
2200
2200
mg/kg
1
Selenium
7782-49-2
6010D
ND
8.9
mg/kg
1
Sodium
7440-23-5
6010D
13000
2200
mg/kg
1
Zinc
7440-66-6
6010D
280
22
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q - Surrogate failure
L - LCS/LCSD failure
S - MS/MSD failure
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9of12

PACE ANALYTICAL SERVICES, LLC
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 10 of 12
M

PACE ANALYTICAL SERVICES, LLC
North Carolina Permit Purariteterz,
2_ -m-.siduivls sLoll be arLalyzcdto demCvlsi-cHly LILT'^} arcri � 5, .,,"'" , _,,�' I;y ,]irrwv Coy crr3�C-11
and Reeovory Ac.' �R(.. A, Tf- 'nal D u
sd rl requ c�T' .spenifcd in
Ati cb nellt uAL tY-r- F)erndteu :ia_I L_-]�Mj(? in ',11.:ac fes'01ts far F_ Ulinimum of f�W- yrars. Au}•
e�c' 't onk trflL*S t C Lu. __ze�� ,r, fl is nnditian &A1 be Gr fcorl 1n AMr. u, E3 L A-
i ��e '�uLal sits kylf;l include folimin,g para_ie,aers (tile rt�ilaIDl'jry ae1 isl n1Jltgra3rLs pGE :roe:
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and tho PCmattc,: „. __pie in tle xz:TEilty far n Uu,_?,ru'aM- of s.vc: yea. -.I
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PICR`.:
Date:
Page g Cat 12
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
Samples Receipt Checklist (SRC] (MEpu19r,X5)
hCe1 �7�y4iC8' Issulrg Authorlty- Para ENV-+ArCOL
Sample Rcecipt Checklist (5RQ
Clicut: 'J'emReneK'al 5rulc� Jrx}ra�[cxl b;�{l�tc: JR02 f Ofwl112021 1 t . '.4F1]112+1
RcvJ5Cd:7,��9r+Z02ta
P�ga � rif S
\"Jeans of receipt Faces I lcfleiv UPS FedEx EJ Otbet-
1--IYCSI WIN01L
Were alstody WIS rese-ni on the cooler?
Yea Na
!( NA
2- if eustod y wnl1 i wi:rc -irescnt, were they intact and unbroken'
pH Strip if); MA chlorine t trip 11); Tested lky;
ri inMI tom scum u PUO TZ"ipt i Uorivcd Giarrecteti tomperalure upcmi,eU; t %13[Aid Sn Cu 1J7: 21 23s
4.8 14A .0 NA j h A r,C hR e NA 9- VA I NA �C — -
Metltod: ❑Temperatmne Bla33k Lr tkgairiyl B(Hl.Ll q IR Gun ID. 5 rR Clun COri+ec inn Factor tJ 'C;
Method o coolant. 0 Wept Ice LJ IMpftc"�s ❑ Dry foe ❑ gene:
❑ `,fct
❑ No
❑NA
3. 1f0�n1�C�8tuiC aC�sy' uu.�Ice�.cuea�Jex1 6_{I'f'., v.aR T�-njed Manager Natiflec?
PM wets IoOwd by; phone 1 email i face-to-face (Circle onn'..
_ d Ye.,
Nd
[ A
4, is the minrr:ercfal wuriWs ppckinr,slip attached to dais fcrnt2
V yeq
NO
5. Were prrparcv-stody (}rMdureS (reli0quishedfreceived) fallowod2
d
Yevi
Wa
6, W6-m sample IDs Iistud on r#iit COC"?
YCs
©-NU
7- Were sa,nple D5 Ii:iud or. all sample containers? f -
Vr
No
R- Was colrec 1011 da'o &. tilne listed an the. GOrl?
EY"I
LJ
No
R. Wus e31lx:c:irrr161u& fimn listed on all sample coniaipel,5?
M- yesl
Elmo
Did s:l oexn ilcr label information (ID, date. thne) agrmc With t'ao C OU!
Yeit
NO
i 1. W,-rc tc5#5 to Le performed listed pu Eha OOCI
21 Y e5
❑ 1
]?. Did all samples au ive in the pTopor wr3ta;nci,3 for 4=11L test andlar in nnad cond id on
Y115-
(uikuruken, lids un., cw.r �Y
❑, �-29
No
13, Was adequate carol; le vol'ime availab=e?
Yes
.11ca
p NO
14- VVrar ull smcip-G� mcxiivedl wittrin V. holding time or 48 hours, whichever termer first.`?
❑ Yes
Wffm&V sale les (circle one) satriplen Not lis:'xd on Coc?
C] Ycs
❑ Ne
EINAk
J 6, For VOA wid BJSK-175 samples. were hubbits presmt>"Rea--9i2e" (.6"ur 61nm in diameter)
in any ofthc VOA vials?
IT 'Were 21l DRD;metz fnvCrient samn-Aes reaeiued W a ph off 2"
- Yes
Na
,l' N.4
Yes
No
, l+�A
18. %x1ae s fi cvanidc sampF�a rcr:ei�red a7 a pT-r > I2 and Snttidet same pies mc.,ivW lit a pH > 97
❑ Yes
El No
F�/I}t4
19. Were all applieable WJ-13f I KNMYaluda+phen.olf62 , 3 ¢ U.Smg+Lj samples free o
resicual elilorinc?
❑ Y,,
E'Ne
❑, NA
20- Wure elk m[ runtAx"auests (i.e- reque.,Ee;i (1170ions, d'.' SAISD der i;naiu)rN, ctc,,,j
w"Pt utly I-r-'surib-1 rrnm the. C()C inra the co=ncr,t section in LIMSF
ZlYesl
+UNor
21, Was the r ore number Jis-od oil the coutaireer label? If yes Qunte #
Sample Preservation (MLot b6 cofaVlclid Cx- emy smnplo{ ] incorrect-y proserved or wid] haedspaue,)
Sample;"y— tvuc received incDTrectly pre served and were ad;ustccl accordingly.
'.r snrnrle. neoeivirtg with _NA mL of GU-cle enc; H2544, hNO3, HO: NaQH i41nn SR i; 11A
+one of presery for NA Jf more than oac preservative is ncedcd, please note in Elie unrnmsn(s bel-ow-
NAwere reeeived vritii bubbles'-b mrn in JLgrn,ete r.
tunplcs(s) iA wane rmvived with'1-ICC > 0-3 trtVL (If 919 is pro) and wcrc
adjusted accardinhly in 5arnp=e raceivbigwi[it sodium thiasulfa:c will, Shealy ID: NA
Sp 1vw rcodn I nberls applied by, date: P lJ .,M I
Comments;
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 12 of 12

0p
0
PaceAnalyfical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Tyson Wilkesboro
Lot Number:WH27011
Date Completed:09/10/2021
NIM�I�Mr�
09/10/2021 2:52 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI Ndm[ACere00- -Board
ANSI
eORft
Al
C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WH27011
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, the following sample had an initial weight that is 3x greater than standard
procedure: WH27011-001. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WH27011
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson Wilkesboro Solid 08/26/2021 1400 08/27/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of10

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WH27011
Sample Sample ID
Matrix
Parameter Method
Result Q
Units
Page
001
Tyson Wilkesboro
Solid
% Volatile Solids SM 2540G-
98
%
5
001
Tyson Wilkesboro
Solid
Ammonia - N (gas 350.1
940 S
mg/kg
5
001
Tyson Wilkesboro
Solid
Nitrate -Nitrite - N (soluble) 353.2
36
mg/kg
5
001
Tyson Wilkesboro
Solid
Phosphorus 365.1
3600
mg/kg
5
001
Tyson Wilkesboro
Solid
TKN 351.2
57000
mg/kg
5
001
Tyson Wilkesboro
Solid
Copper 601OD
5.3
mg/kg
6
001
Tyson Wilkesboro
Solid
Zinc 601OD
62
mg/kg
6
(7 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 10

Client:Terra Renewal Services, Inc. Laboratory ID:WH27011-001
Description: Tyson Wilkesboro Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 5.78 09/01/2021 0138
Date Received:08/27/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
08/31/2021 2357 MOM
14024
1 350.1
(Ammonia - N) 350.1
2
08/31/2021 2212 DRD
13796
1
(Nitrate-Nitr) 353.2
1
09/01/2021 2039 AAB
14288
1
(Phosphorus) 365.1
5
08/31/2021 1536 DMA
08/27/2021 2030 13643
1
(Soil pH meas) 9045D
1
08/29/2021 1934 NBW
13723
1 351.4
(TKN) 351.2
5
09/07/2021 1756 DMA
09/02/2021 1634 14260
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
98
%
1
Ammonia - N (gas diffusion)
350.1
940 S
350
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
36
3.5
mg/kg
1
Phosphorus
7723-14-0 365.1
3600
430
mg/kg
1
Soil pH measured in water C) 20.9 ° C
9045D
4.1
su
1
TKN
351.2
57000
4300
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 09/02/2021 2027 DAL1
08/30/2021 1706 13817
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
290
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
290
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
290
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
290
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
290
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
290
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
290
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
83 41-132
Tetrachloro-m-xylene
86 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 09/02/2021 1658 CMS2 09/01/2021 1527 14067
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B N D 1.3
mg/kg 1
LOQ - Limit of Quantitation
B - Detected in the method blank
E - Quantitation of compound exceeded the calibration range
Q - Surrogate failure
ND - Not detected at or above the LOQ
N - Recovery is out of criteria
P - The RPD between two GC columns exceeds 40%
L - LCS/LCSD failure
H - Out of holding time
W - Reported on wet weight basis
S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 10

Client:Terra Renewal Services, Inc. Laboratory ID:WH27011-001
Description: Tyson Wilkesboro Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 5.78 09/01/2021 0138
Date Received:08/27/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 09/02/20211609 JMH 09/01/20210137 13906
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
ND
110
mg/kg
1
Arsenic
7440-38-2
6010D
ND
4.1
mg/kg
1
Cadmium
7440-43-9
6010D
ND
1.4
mg/kg
1
Calcium
7440-70-2
6010D
ND
1400
mg/kg
1
Copper
7440-50-8
6010D
5.3
2.8
mg/kg
1
Lead
7439-92-1
6010D
ND
2.8
mg/kg
1
Magnesium
7439-95-4
6010D
ND
1400
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
11
mg/kg
1
Nickel
7440-02-0
6010D
ND
11
mg/kg
1
Potassium
7440-09-7
6010D
ND
1400
mg/kg
1
Selenium
7782-49-2
6010D
ND
5.5
mg/kg
1
Sodium
7440-23-5
6010D
ND
1400
mg/kg
1
Zinc
7440-66-6
6010D
62
14
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q - Surrogate failure
L - LCS/LCSD failure
S - MS/MSD failure
Page 6 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 10

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 8 of 10

PACE ANALYTICAL SERVICES, LLC
North Carolina Permit Parameters
2. Cuiawrvvitan
4nd Re :ovary APA �RCRAj Uo w
sEa gt wn y s
Pcdftb in
A(Ur, neatt 4 aaa tho P=ittMe BLd mfuntain thew P=ults f-ur a m-uuuum of fivc years Auy
excet, ors from the requirements in this.aonditior shall he spenif ed i) Agar[ A
TIIO�LYLys;s SJO uIclwde lip,:. �OGWixLg pnjAM4f 4; (lJe regUlau ltr4 in MZg.-Hmn Per )ii,-r
is in pm-entheses),
._ „ ..., ._ .....,.J.-
9_ but analysis sal: be ooaduaed cr. residuals Prom each seume Ming fm-1 }. at the lkegw cy
specified it At�&z ument A, and tha T'eimince shaU maintain di-- results for a minimum Df five yeEm
Tie anialys% s1A unlade ake fo1kw!(Lg pmweE--m
Ahiminiim
M-brM.Ery
PoLaHrlMn --
AbiIImouia-Nitrogen
Mkiybdenum
Soleuium
A %CfdC
Mick: l
Sodium
Cadmium
N tow -Nitride Nitrugcn
cak;iuzn
Moent Tate: Sa]i&
%KN
Copper
pH
Mir,
P?hasplwrw
Volatile SaGds
_A+(�gnosiva}
PAC f3'S
TERRA RENEWAL SERVICES
479.747-8192
Attachlneattr. COI; for...,.5ouroes;
wQ003C Vcrjjou 1.0 Slra.l Ve g9 nn E40210 Pope S of 12
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
Sempfes lieeeipt Checklist [SRC) [MC0019C-15j Revised,9/2012020
.erlstl�a�l.vi �i
ISSuing f,uthnrity: :Is c-a FNtif - l+dCOL Po ge 1 of 1
Sample Receipt Checklist (SRC}
Client' 'I'4rru Iteacwal [ r�lcr Tn9ncclir: hLrdo-iic JSH 1 4Sr2712Q21 i _nI fi W]1274311
Alum Of'rCCelpt: PaceI lClient ,f 1JPredEx ; OLhat:
Yea
/ N01
11. WeM custody seats Msent on the cooler?
Yol
ENA
12. ff cuswo sk,,ub v"v prvN�_nl., wtrU Illy , inLML and ar_trroken?
-ON-ul
pH Strip ID: Nw CliharintSLrip IU; N^ - 'J'Csrcd by: NA
Ori€inal tniiperature u.jois recant; DLcrivrd (-C4rR`4-.wd) Iclrpuajivc upon receip[ '6solid SnLP-Cm If]: 'ZI 147-,5
2.4 /2_4 oC NA iNA oC NA +,NA <C NA INA °C
MUhud: ❑ t'olnperaturo Blank f7kgairst Bottle!; IRGun ID, 5 11t Gun Correction Facton ;C
MUllod u F rw:dmt 0 Wa Ice ❑ Ice Pa,:ks ❑ Dry lra Nanm
❑ Yes
❑_.N
I
d❑NA
_
3' 1°tr.Tpmature o#suy 000leY a caeded 6,0°C, tirAs Prrajat k ]anagcr [4otifiwd't
i PM was NOvificd by: phone r'email i face-ro-farc (circle orrLj.
Yes
Nol
f7NA14.
is the rornrncrcial cnurier'.s nackrr.g slip attached to Llus roan?
,! Yas
�Jo
S. Were per custody }la�Q,21dwR_fi (at liiayuis[k4dlrcxwiy(A) rb[loweO
J Yes
-No
16.
Wcrc sample IOs listed on the CO 4
J; Yes
ONo
7, Were sample IDs li�l sleun all NLunplc caclaincr97
Yes
N,3
6. €stool-wdondaae & tilne iilswd ua thrCOC?
'Jo
9. Was cal.cctior, date & time Ikted 9-1 a[, samolc� CorL afiicrs?
Ycg
No
10_ T}Pd all container label hifi•Ltlai on flf], dote, Lime)ugrw W&I -Le Ct
Yeti
No
I 1 _ )A'Lmc WSIs to be performed listed en the: COC?
Yffl
❑ No
12. Di all salttp]es arrive in the ptvT," covainc;-. for cacll test andlor ill EOL41 UUuditiou
(onbrukci. lids on, ec.)'f �w _
Yes
__ No
13. teat adequate �,irn�lc wu li mut mw ilabl e7?
I i Yes
-❑No
14. Worou[i aalnpl-csrkccivcdwithin Yr the holding time w48 hours, wbrthiml- Courts first"'
Yes
No
i5, Wcrc o sam Les coniainerx mKAngicx; css (eirxLe aue) samples Not [isLed oil COO- —
16, For VOA and RSK-175 sarn-oles, wera Ir-I":3k3IM p msaat>"pca-size (Vor 6min in diame-ler)
in Lilly ofdL VOA wla'LV
U Sees
❑No
Q N.r4
Ycs
Lj No
LJj NA
_
17. %Vcrc all 13RO nietals,+nutrient mra 3e5 se"ivcdof a -jHof < 2°
Yes
77No
J NA
IS. Were all cyannle Zinnlrs rraxiVCd at a pH > 12 and sulfide saii:y[CS lrL'CiVC13 Lil:Y pH '-• Cy?
❑ Yes
No
❑NA
[ . Were aA applicable NH+TKNirymirJLfphcncrllb'2�,3 ,]rGU8(. OZbJr@`L)samp:esfree{tr
residual chlorine?
❑ Ycs: ❑ No
[Z]NA
20, Were elimil. Tom wrlc Acquom (i.c, meucsted dllutims KiiMS[] desivations, CxC'
corAwdy tmnsarbcd Tarn the L:O :rim 4he camment section. in LIMS?
Yes
No
?. I% Was the , uote nuFnWr Esced ea the cOl'Wn-er label? J," was, Quote $
Sample Frcwr vulion (Must OC CDIMPleted for any saLnp le(S) iHebrMC'jy prcecrvad or with heaspace_)
aSnp1e{3j '� 1VC1' I'CCtiVCd:nCC1M011k'PreSaVeL1anr. weir.adjustudar,Gprdl_IS-ly
in sample recalriag whir NA ml.e17O-x C ow: H2SO4, HNO3, HC1. NaelI acing SR 9
Tine of preservation MA IFIRIJP�U11.onz pry wrva6w is needed, pJzmm rote irLrhe, thnnenI& hnlow.
Sample(s) NA -Core "wiwd with bubblcs>6irm in diameter.
amples(s) � _ - werr' reocivcd with] 1kt =} 11,5 1rtg1L (!f lT] 4 is pro) and were
a4iustcd amardingly Ill Sarrlp.e rou�iving Mth 5odiLim thlasulfitEr (JagS�05) wah 4Lh a[y If]; K'd ---
SR ba:reodee Labalsapp_ied bp" K.7Jt','1 L�FJ27l IS�t_
Col: ments:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 10 of 10

0p
0
PaceAnalyfical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Mathis Storage
Lot Number:WH27009
Date Completed:09/20/2021
NIM�I�Mr�
09/21/2021 7:21 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WH27009
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, the following sample had an initial weight that is 3x greater than standard
procedure: WH27009-001. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WH27009
Sample Number Sample ID Matrix Date Sampled Date Received
001 Mathis Storage Solid 08/26/2021 1400 08/27/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WH27009
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Mathis Storage
Solid
% Volatile Solids
SM 2540G-
44
%
5
001
Mathis Storage
Solid
Ammonia - N (gas
350.1
170000
mg/kg
5
001
Mathis Storage
Solid
Flashpoint (Pensky-
1010B
>140
° F
5
001
Mathis Storage
Solid
Nitrate -Nitrite - N (soluble)
353.2
430 S
mg/kg
5
001
Mathis Storage
Solid
Paint Filter Test
9095B
Fail
pass/fail
5
001
Mathis Storage
Solid
Phosphorus
365.1
28000
mg/kg
5
001
Mathis Storage
Solid
TKN
351.2
220000
mg/kg
5
001
Mathis Storage
Solid
3+4-Methylphenol
8270E
1.9
mg/L
6
001
Mathis Storage
Solid
Calcium
601 OD
72000
mg/kg
8
001
Mathis Storage
Solid
Potassium
601 OD
43000
mg/kg
8
001
Mathis Storage
Solid
Sodium
601 OD
27000
mg/kg
8
(11 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4of12

Client:Terra Renewal Services, Inc. Laboratory ID:WH27009-001
Description: Mathis Storage Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 0.416 09/01/2021 2332
Date Received: 08/27/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
08/31/2021 2357 MOM
14024
3 350.1
(Ammonia - N) 350.1
20
09/17/2021 1444 MSG
15693
1
(Flashpoint () 1010B
1
08/30/2021 1016 KMC
13812
1
(Nitrate-Nitr) 353.2
1
09/01/2021 2035 AAB
14288
1
(Paint Filter) 9095B
1
08/30/2021 1217 KMC
1
(Phosphorus) 365.1
5
08/31/2021 1536 DMA
08/27/2021 2030 13643
1
(Reactive Cya) 7.3.3
1
08/31/2021 2053 AAB
08/31/2021 1649
1
(Reactive Sul) 7.3.4
1
09/01/2021 0012 DMA
08/31/2021 1649
1
(Soil pH meas) 9045D
1
08/29/2021 1933 NBW
13723
1 351.4
(TKN) 351.2
1
08/30/2021 1325 DMA
08/27/2021 1854 13592
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
44
%
1
Ammonia - N (gas diffusion)
350.1
170000
48000
mg/kg
3
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
° F
1
Nitrate -Nitrite - N (soluble)
353.2
430 S
48
mg/kg
1
Paint Filter Test
9095B
Fail
pass/fail
1
Phosphorus
7723-14-0 365.1
28000
6000
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water C> 20.7 ° C
9045D
5.0
su
1
TKN
351.2
220000
12000
mg/kg
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 09/10/20210308 JDF
14928 09/07/20211804
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WH27009-001
Description: Mathis Storage Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 0.416 09/01/2021 2332
Date Received:08/27/2021
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
Bromofluorobenzene
95
70-130
1,2-Dichloroethane-d4
98
70-130
Toluene-d8
98
70-130
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 09/10/20211910 SCD 09/08/2021 1830 14793 09/02/20210041
2 1311/3520C 8270E 5 09/11/20210015 SCD 09/08/2021 1830 14793 09/02/20210041
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.040
mg/L
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.080
mg/L
Hexachlorobenzene
118-74-1
8270E
ND
0.040
mg/L
Hexachlorobutadiene
87-68-3
8270E
ND
0.040
mg/L
Hexachloroethane
67-72-1
8270E
ND
0.040
mg/L
2-Methylphenol
95-48-7
8270E
ND
0.040
mg/L
3+4-Methylphenol
106-44-5
8270E
1.9
0.20
mg/L
Nitrobenzene
98-95-3
8270E
ND
0.040
mg/L
Pentachlorophenol
87-86-5
8270E
ND
0.20
mg/L
Pyridine
110-86-1
8270E
ND
0.040
mg/L
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.040
mg/L
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.040
mg/L
Run 1
Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery
Limits Q
% Recovery
Limits
2-Fluorobiphenyl
71
37-129
73
37-129
2-Fluorophenol
52
24-127
50
24-127
Nitrobenzene-d5
78
38-127
83
38-127
Phenol-d5
78
28-128
92
28-128
Terphenyl-d14
95
10-148
74
10-148
2,4,6-Tribromophenol
85
41-144
66
41-144
TCLP Herbicides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/8151A 8151A 1 09/14/20211045 CMF 09/08/2021 1819 14790 09/02/20210041
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
2,4-D 94-75-7 8151A ND 0.020 mg/L 1
2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 mg/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
DCAA 81 50-112
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WH27009-001
Description: Mathis Storage Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 0.416 09/01/2021 2332
Date Received:08/27/2021
PCBs by GC
Run Prep Method Cleanup
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A
1 09/02/2021 2014 DAL1
08/30/2021 1706 13817
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
4000
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
4000
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
4000
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
4000
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
4000
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
4000
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
4000
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
82 41-132
Tetrachloro-m-xylene
82 35-106
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 09/13/20211732 DAL1
09/08/2021 1630 14770 09/02/20210041
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
N D
0.00040
mg/L
1
Methoxychlor
72-43-5 8081 B
N D
0.0016
mg/L
1
Toxaphene
8001-35-2 8081 B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
79 20-131
Tetrachloro-m-xylene
85 26-132
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 09/02/2021 1655 CMS2
09/01/2021 1527 14067
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471B
ND
18
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:WH27009-001
Description: Mathis Storage Matrix: Solid
Date Sampled:08/26/2021 1400 % Solids: 0.416 09/01/2021 2332
Date Received:08/27/2021
TCLP Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3010A 6010D 1 09/03/20211131 JMH 09/03/20210121 14330 09/02/20210041
1 1311/7470A 7470A 1 09/03/2021 1835 CMS2 09/03/2021 1427 14392 09/02/2021 0041
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2
6010D
ND
0.15
mg/L
1
Barium
7440-39-3
6010D
ND
0.25
mg/L
1
Cadmium
7440-43-9
6010D
ND
0.050
mg/L
1
Chromium
7440-47-3
6010D
ND
0.10
mg/L
1
Lead
7439-92-1
6010D
ND
0.10
mg/L
1
Mercury
7439-97-6
7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2
6010D
ND
0.20
mg/L
1
Silver
7440-22-4
6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 09/02/20211601 JMH 09/01/20210137 13906
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
ND
1600
mg/kg
1
Arsenic
7440-38-2
6010D
ND
58
mg/kg
1
Cadmium
7440-43-9
6010D
ND
19
mg/kg
1
Calcium
7440-70-2
6010D
72000
19000
mg/kg
1
Copper
7440-50-8
6010D
ND
39
mg/kg
1
Lead
7439-92-1
6010D
ND
39
mg/kg
1
Magnesium
7439-95-4
6010D
ND
19000
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
160
mg/kg
1
Nickel
7440-02-0
6010D
ND
160
mg/kg
1
Potassium
7440-09-7
6010D
43000
19000
mg/kg
1
Selenium
7782-49-2
6010D
ND
78
mg/kg
1
Sodium
7440-23-5
6010D
27000
19000
mg/kg
1
Zinc
7440-66-6
6010D
ND
190
mg/kg
1
Footnote(s): *Paint Filter: 100ml- collected;
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9of12

PACE ANALYTICAL SERVICES, LLC
V
E
M
z
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 10 of 12

PACE ANALYTICAL SERVICES, LLC
North Carolina Permit ParamOem
I Residuals dM11 be snalyaed to demonstrate thi i are Ur" Canw Valion
pud kmovevy r1Ct {RXR.'1J, The [ e€ varrosivity, ignita lity, renHivi and tnilelty
charncteri!Stk I�ur n; procedure 7`CIr 0 L , ixlucucy 1i j;ee �1*x1 !it
Al-taebiueat Al Md the Fffi-M M Stall mainiain t'hesr results faa a Mininnaum 0p liV6 yeas Any
earceptims from tha req-1LT2 entS in thiq.1.13nf1jIA Dn shKl l be q-r :i F01 in ALI.aul7TrH%d A.
TL•e l'CLP a a1ys:s shalt jielude tiie fbho>a p iametcrs (thc rcguluory t ve; lin milligrams per liter
is in parrmthcsos):
A.rst:uir- (5 k)
Barium (100,10)
Cadmium (1.0)
C.xboattetrachloride (0,5)
CI lordana (0 )03)
CkJOIrbeuZeue (100.0)
C11 uruiorm
011+d11± Mt { 0)
m-Crew! (20U-0)
0-cresol (200.0)
p-Cmsol (2.00,0)
Cresol
1,4-Dich1orubLmz== (7.5)
1,2.Mchiorocttiuo (0,5)
1,1-Dic1io-octhylone(0.7)
2,4-Diuitrot;,kmva (0-13)
En,dxin (0. Cr')
llexaab].ar�bea��ene (p_13)
Heptachlor (and its hydmAdz)
13exat:Irioac-1,3-butad�r,e {�_D)
#1inxacbloraeLharxc (3.0)
L.ac (5_0)
Lindanc (04)
1149—Ty (0.2) '
)i�i�#hnvcyohlvr (1 D,0)
Nitrobe ne (2.0)
Fcntaehlomphcaol (1010)
pyridine
�elerrialm {1 ,ft)
Silver-
1'etrachlnr�elr}i�ne (0.7)
Toxapheno (0-5)
Tricwaur'thyl=n (O.q
A5-TrieLkwophenD1(4120.0)
2,4,6-`1h4chloroph=ol (2,0)
234,5-i'F (5itvex) (I.0)
ViT V1l:lLloa',da (01)
3, An aaalysii shall bu 4unr3ucA oil a�Maals Loin each source generatizg #aclity of 'lit. frecluex:y
6o,,j,5er1 in AttacFrmerrt A. and ,hs Penyft:ee s:isil mautain the results :Ig tl miri:amm {r, Gwe years.
Tho malyms Ah iiwluda Um -Muwfiig pravw eteLs:
fx
.krj7Tn(Mi F1-hTi [Blgcn
I�
Ar.�eEdc
Imo-
Cydmi-am
UoW
Z
CDpp
Lead
ti
ZI l�+iitgn��iurrt
,
wQOkOM036 Version I
--bi(crcury P010931t7 U
Molybd&wlli 9aInriurn
i :ekel sediurn
?dtr��te-�1_tiit6 N'itrogcn
Perrem Total Sdids
pH
` KN
Zinc
'Phnsj6arus
Volatib Solids
PG13's
TERRA RENEWAL SERVICES
47 9-747 - e l 92
Sliall4'�rs�t�u 1-02.=a
Ptq�w 8 of I 1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
5ampks Rc mlpt Cheekllst (SRCI (MEDOiSC-15] I; a15!�d:912912.ozu
ace�4fu> 4� ! IssulnRAuthor[ty: Pace ENV -WOOL Peige l of
Sample Receipt Checklist { R `j
Cliarst oTaRcw-val CualerinsecctedhvMate- 3,s,r r 08+27;2M] l.nr ir. WH27049
Wang of MICiPt, Paw Client ZU P~x Fedl xLj
Di hkr:
❑ Ym
,f N-o
1- %%Ierr ri I study seals pmsent on the cool er"
Yes
No
NA
12. 1C euAkr v- c= wry re€clu were 11i.,;y intact and ir_broknn?
pH Strip ID: ",'- ChlorineSorip ID- r", Tasrwd b r.rvn
Ofional rt�,tLperatarG c73un N6"i-jt i Drdval (Corrected) temperatul%e upor. mceipi -'/@Solid 5Tmp-CLLtp ID- 2L-I.d2.1.'
Z4 e2A oC KA I"A VC N.JL /NA CC NA fNA aC
McthQd: ❑-t-ompertttn-e Blank ' sl Boules IR Gun 1D; � 1R Gun Crwmcl inm r n.Lm- � °C
7��ethd)d Of aoolsrt: Wet lee H Tee Fucks --U.Pry 1ra ❑ None
❑J Yes ❑-No �TIA 3, 1t tr:mm-arim of auy ewle^ e;tiCYeded G.0° ' tiva5 13rojcat Manager Notitled7
PM was Novi ied by_ plrar_e f eiraii i furc-u i,--F= (eireJG olie).
Yes
No
NAti
. Js the carnwrcial courier's sacking sl i ; atiar}:ed to Nis fbt-M7 --
,.r Yes
L1 N,)
S. Were proper GujL;,eiy pro4W=2 (Fdinquishedfraceived) 5DIlowcV "
Yes
ONO
6- Were saMplY 71D5 ]istcd rtn t[10 OC C.
Yes
DNI 3
7" NVcre LimuploMs'igwl �an a[l sarnDJe C-D.-trainers?
Yes
No
9. Wes 0011ectior. dace & time listed on th-3 COC?
❑ Yes
No
19. Was collection date & tintC.1istfid on ad sample ooittaint:r;$
IF,71 Yas
No
10- Did-�dl cortairker lalrGl inQumatiun (JID, date, time) = wirh Lhe C-OC',?
Yes
hfo
11. lsk'emten to be nerf^.rm.-d listed on t1le COC?
Yeas
❑ Nu
12. Di all xamp€cs WrivG in the proper ccurtaiswrs for rar_-3 iVSt aruJ OT- in ;;ovd canditioat
(unbrDkcn, licb on, etc)? -
Yes
No
13. A%& .adequate simple iro hfine avdi[dble?
Mca
7,No
H. Wurc all swplQ �-eceived withinor 4S hours, ,v1,ic1:ever cwnus fi- I!?
Yes
d N.
15-'«'4'e rc any samp[cs containers A]r}solgiex=.,Ls (uirolc ama) sarnpJes Not listed an COC?
Id. For -VOA mid RSK-[71 sampim, were bubbles preaent s'Na-siel (f"a- 6mnt in d€acieer)
Ja any afthe VC A vials?
❑ Yesl
❑-Na
nNA
Yes
No
I J INA
17- Were a] I DROfirn-om Wnutrient sans 21es rem[%,,L J ul IL pH c Jf < '617
LJ Ye5f
LiFlo
d Nil
IS. Were a]I cyaride Sduila_es rerxived Ht H pF; � 1'� and sulfide samples hived al; a pH > 9?
I9- Wore: ail applirob�c-FJ111'1.1{NrcyauidelnlseaoU $,Ir < 0.5m &rl- 2iarnfylcs [Fuc vF
resid�.al olslarilte'�
❑ Yes
L� to
[7NA
_ _ _
QA
Ys
NO
'0. Wcm client remarkslreauesis (i.C. rcquzstod d=iutions, MSOMSD ksigmitiors, CU...)
on .cetly transcribed from the COC into the Mlime lit sectiusi i i i ]..TMS?
211. '~seas ifre qjcic number listed on roe conto bier Label? lfycs, Oklota 4
Yet
+ Zrp
Stemple 17sscrTatiun (Must be ronk €eted `br tn_v sziulp_c(s) ilsccri-mtly pfese'we+d orwilh her'a3ap"e.)
ISarapJa(s)NA - _ ware reci'iYet] inrorrcatlypreserved widwereadjuwtcdLcLor]ingly
i-s sa€npie = eaeiv hYg With A >ttL of o Qc:e astc: [ ]? 5C?4, i i1ti 11 S, FIC'1, 1+la+JH using S 1fi
]"ilne trfpl c, vatien N4 __-. lfmara thats nhe rqe;crvsllir, is n�-ded, �3lasse utite in ttpmmGuls wo[rnu,
Sarnpla(s] NA were received with bubM �6 rnm is diarnv--w-
Sam 3es;s) " — were received with Mc n 0.5 lingfL (Mwlq is no) xud were
Iadiusted aeuvding[y in samp]o mcziving wish sodiutn 111[cLswIblu iKFt,303±'� with 511caly ID= ^
:SR bal+oode labels applied by; KDFVN Didle- aar.!W20 YI —
C::mmcnts.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 12 of 12

0
aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:W103004
Date Completed:09/27/2021
I
09/27/2021 1:27 PM
Approved and released by:
Project Manager II: Lucas Odom
se W- -
zw
A116
�
ArrSl xaaonerkcremrrrrcn 8wrp
A C C R E O I T E❑
9BaRATO
TESTING L OFATOFY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 12

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: W103004
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following reported analyses are currently not listed on
our TNI scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 601 OD, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, the initial weight of the following samples is 3x greater than standard
procedure: W103004-001, W103004-002. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 12

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: W103004
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
Tyson/Harmony
Solid
09/02/2021 1330
09/03/2021
002
Solid
09/02/2021 1430
09/03/2021
(2 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of12

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: W103004
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Tyson/Harmony
Solid
% Volatile Solids
SM 2540G-
91
%
5
001
Tyson/Harmony
Solid
Ammonia - N (gas
350.1
9600
mg/kg
5
001
Tyson/Harmony
Solid
Nitrate -Nitrite - N (soluble)
353.2
25
mg/kg
5
001
Tyson/Harmony
Solid
Phosphorus
365.1
9100
mg/kg
5
001
Tyson/Harmony
Solid
TKN
351.2
60000
mg/kg
5
001
Tyson/Harmony
Solid
Aluminum
601OD
4800
mg/kg
6
001
Tyson/Harmony
Solid
Calcium
601OD
11000
mg/kg
6
001
Tyson/Harmony
Solid
Copper
601OD
4.5
mg/kg
6
001
Tyson/Harmony
Solid
Potassium
601OD
1900
mg/kg
6
001
Tyson/Harmony
Solid
Sodium
601OD
2000
mg/kg
6
001
Tyson/Harmony
Solid
Zinc
601OD
27
mg/kg
6
002
1
1
1
1
1
1
1
1
1
(21 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4of12

Client:Terra Renewal Services, Inc. Laboratory ID:W103004-001
Description: Tyson/Harmony Matrix: Solid
Date Sampled:09/02/2021 1330 % Solids: 6.36 09/09/2021 0031
Date Received:09/03/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
09/09/2021 2341 MOM
14922
3 350.1
(Ammonia - N) 350.1
15
09/25/2021 1603 DRD
16480
1
(Nitrate-Nitr) 353.2
1
09/11/2021 0913 AAB
15082
1
(Phosphorus) 365.1
25
09/07/2021 1601 DMA
09/03/2021 1806 14449
1
(Soil pH meas) 9045D
1
09/05/2021 1409 NBW
14531
1 351.4
(TKN) 351.2
5
09/17/2021 1150 DMA
09/16/2021 1346 15511
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
91
%
1
Ammonia - N (gas diffusion)
350.1
9600
2400
mg/kg
3
Nitrate -Nitrite - N (soluble)
353.2
25
3.1
mg/kg
1
Phosphorus
7723-14-0 365.1
9100
2000
mg/kg
1
Soil pH measured in water C> 18.7 ° C
9045D
5.7
su
1
TKN
351.2
60000
3900
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 09/10/20211344 NCM
09/05/20211745 14536
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
260
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
260
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
260
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
260
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
260
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
260
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
260
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
94 41-132
Tetrachloro-m-xylene
90 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 09/10/2021 1430 CMS2 09/09/2021 1342 14850
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B N D 1.2
mg/kg 1
LOQ - Limit of Quantitation
B - Detected in the method blank
E - Quantitation of compound exceeded the calibration range
Q - Surrogate failure
ND - Not detected at or above the LOQ
N - Recovery is out of criteria
P - The RPD between two GC columns exceeds 40%
L - LCS/LCSD failure
H - Out of holding time
W - Reported on wet weight basis
S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 12

Client:Terra Renewal Services, Inc. Laboratory ID:W103004-001
Description: Tyson/Harmony Matrix: Solid
Date Sampled:09/02/2021 1330 % Solids: 6.36 09/09/2021 0031
Date Received:09/03/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 09/08/20210821 JMH 09/08/20210041 14562
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
4800
99
mg/kg
1
Arsenic
7440-38-2
6010D
ND
3.7
mg/kg
1
Cadmium
7440-43-9
6010D
ND
1.2
mg/kg
1
Calcium
7440-70-2
6010D
11000
1200
mg/kg
1
Copper
7440-50-8
6010D
4.5
2.5
mg/kg
1
Lead
7439-92-1
6010D
ND
2.5
mg/kg
1
Magnesium
7439-95-4
6010D
ND
1200
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
9.9
mg/kg
1
Nickel
7440-02-0
6010D
ND
9.9
mg/kg
1
Potassium
7440-09-7
6010D
1900
1200
mg/kg
1
Selenium
7782-49-2
6010D
ND
5.0
mg/kg
1
Sodium
7440-23-5
6010D
2000
1200
mg/kg
1
Zinc
7440-66-6
6010D
27
12
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q - Surrogate failure
L - LCS/LCSD failure
S - MS/MSD failure
Page 6 of 12

Description:
h' .It r x _
Date Received:-
NINE
IIII
,
III
NINE
-
NINE
IN
0
LOO = Umit of Ouantitation B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the L00 N = Recovery 5 out of criteria P = The RPD between two GC columns exceeds 40% L = LCSILCSD failure
H = Out of holding time W = Reported on wet weight basis S = MSIMSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 12

-
mglkg
1
LOQ = Limit of Ouairlitation B = DetecWd in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCSILCSD failure
H = Out of holding time W = Reported on wet weight basis S = MSIMSD failure
Pace Analytical Services, LLC (formerly Shealy ERvlronmental Services, fnc.)
106 Vantage Pant Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 12

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9of12

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy EnvironmenWServrces, Inc-)
106 Vantage Paint Grrve West Columbia, SC 29172 (BG3)791-9700 Fax [phone] www.paceiabs.com
Page 10 of 12

PACE ANALYTICAL SERVICES, LLC
North Carolina Permit Parameters
2. . rFr�rw C:umaLvaUarl
and Recavery Act (RCM). The gnal.+ses
a d>er aq`uoucy Specz and in
Ai°Achm=t A, and tw Pr-mitloa shell meintaia these :exalts for a w.mmum of &c }roars. AiLu
exceptions fr>:rm the rNu:remerts in diis•cand inn s:tiali he spcuurerl iu 1VWJu=A A.
T%e�nalysts shall incli.iir the fii:iuwil-g 1,miatuctas (the regulatory IeWc! in milligrams per liter
iN n: PaeW1'1=3).
An analyts shall ?tic cnnduc*ed an residt.a13 f1um ouch 9owce genefating hwility al the fregumey
sparaficd in A-aiwhuteut A, anti the Permitter stall maintain =.hc results Lr u miniu-iju of fire yearn.
The cnalysis shall Wd-;ldc the fktilinwin.- paramcters:
�
�`
AJ+�iAum
Q
�aaclatua•Nivo�n
Vi
111setlic
Fa-
C'admntlu
to
Calcium
�
vi
W
I2&d
H-
Iyft►gnea�ihrn
�
I
h.crcu77
NUyhdenw n
-Nickel
ViL-uu,-;litriw Nitrogen
Pcr=nt T(A91 BoUds
PT
TERRA RENEWAL SERVICES
479-7¢7-d192
Attachment to COC far.-AcurCS9: �"� � )'
- Zt-
WQM6936 Yersim 1.D
SbA v -:ion iaJC-.'_n
P�+tsssi.un '---
s6willm
&ilium
TK N
zinc
Volatile Solids
PCB's -
Date: 9 n _ ) -
Pap 6 of 13
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc-)
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] www.paceiabs.com
Page 11 of 12

PACE ANALYTICAL SERVICES, LLC
Samples Recelpt Checkilst [SRC) (MEOOISC-I5) Revised: 9/29j2 020
Pdc A hrtica� lssuing Autl,orlty: Pwe FNAV - WCt]L Page 1 of 1
Sarrlple Receipt Checklist (SRC}
linnY Tara Rcneti••ol Coalcr Ins •Ctcxl byddate. KSC + Of-MO)21 Lot #. WloWicl.
A4e; ns &.`recoipr Lj Puce LjCliear L,UPS Lj 17edlix I I Uhcr. _
yV5 ,/ No] 1. W rc custody ycaIs present on the cooler?
�'cs
N,z
N.4
1 ! �uitcrd y seals were pirmint, were they intact and unbruki:O
pH Strip ID: ;^Strip ID:.I" . -- Tasted by: NA -
--•---C'hlorino
Original Wn:perature upon rrccipt; 1}trivod (Cm-oci4 temperature uprm mccipt %Solid Snap -Cup ID: 21-:425
2.7 i 23 nC KA `NA q• VA r VA aC NA i MA a�
Method, 7j7'cmp(.nxlurL Blw;k 046ailrst Bottles 1RUan 11): IR Gun Corr.clion l=a::lor. 0 cc
MQ111100 u! CQ011111. 0 Wet lcc ❑ lee Packs ❑ Dry Ioc ❑ M1unc
❑Yes
©No
❑�lA
i I F L-rr pcxulure of :cly cooler exceeder. C,.[l`C_, was Project Man: rer Noti Pied?
?M WKS Nrltj111Gd by: phone i entail? face -tin -fare (cire.e one).
4- is the rnmrneTzidl courier's packing slip ar"acicd to th:s form?
15. were prop" euslody procedures (reii-iquishcdrtaccivori) follovried? - -
Yes
V 0
yA
d Yes
ND:
VPb
Ll Nal
6. Were sa:rtpin IT).-, lis ed on the COO
f Yes
❑ No
?. W'crc sample IDH listed on all sample containers?
�
-tin
S. Was collecliun dau, & [hive listed on ttte UK?
9. Was collctcrinn rate & time lig:ed ott ell saniplc conlaincrs? -
0 Yes
rTNo
❑ NO
lU, Di all com�tinm luhcl infarmadan (ID, date. time.) agree with the t'�f]C?
No
11. Weia tests to be performed HiEec on the COO
ij_Didullsurn�lesrurivair_ tirorrojl ercontaincrs lire.each Leit a.` &or !it goad coadl:fUnUi
F,(Yes
❑ 1tin
(Liabroken, tins on, ctc.)" -�
13. Was a&�^quaL sutnple volume available?y ._
0 Yesr LTNo
V-1 v'as I
L No
No
_
14. Were a] l sem pks received within 5! tF a hn King 1 imc r iftR lwu�s, wi ric hevelcanes rust?
l5_ Were arty samples centaincrs rnisa4rg14wxcess lcirrie one) samples Not h4vri rm On ?
❑ v `
❑Np
0 N ti
16. For ►1UA turd 1{S!{-1 15 samples, were bubbles prescnt >"Fw-sirx"(A"or 6:tun in diameter)
in any of the VOA via! s?
17. Wcrr all U_ROittretalsrtlut:•ient samples recAvrd at u:II1 of <27
1$. Wcrc a.1 cyanide rdtnples received at a pH T 12 and sulfide samples received a- a PH > 9?
19, Wcre a' applicable I.608_3 (j, 0.5:n j L) Samples tire: or=
Yes
LjNa
.7 NA
Y cs
LJNc
d NA
❑ Yes
❑ No
0NA
residuel chlal-inc:' ._
20. Were cliex rrmF.rkskcgttrslx (i.e. requeiced dilutions, h1Sih1SD r osignrt'.ium, cic... I
yes
❑ No
[DNA
comedy .twiscribed frorn the COC into i,e cr+mment section in L1hiS?
21. %Vas [tin q uutc o;tmber listed on'ha comailler label? If yes, Quote r
YTs
d Nu
_
sample Preservation (Must be completed for any sarnplta(s) incorrectly preserved or Keith hcwtspnm.)
SLrnpkei(s) NA -_ vtwt received inrnc oactly pT�wil dnd ware adjusted accordingly
h NA in sample receiving wNAmL a circle [me: 112SO4, I I.NtYj, HC:, N1bOH :rsiag SR u Nn
Time ofpcesei-vation NA _. If rlore than one prese"iive is rccdQ& plcusc now is the calrnteuts belD -
Sample(s) 4A wm roc:eived with bubbles >6 r1-rt in diameter.
Sar jpj.M(R) NA - _ %ymc received With IA[: > V nlel. (if �'t19 is rru) and w•cm
a 11.5ttd accordingly in sample receiving wilb sodium Ihivsu:flt;x (NL15203) wilt Shealy ID: NA
--
SR bode laoels applied by: JPG2 Datc: O*}.+011202t
Cgnurlencs_
Pace Analytical Services, LLC (formerly Shealy EnvironmenW Sermes, Inc-)
106 Vantage Point Drlve West Columbia, SC 29172 [phone] Fax [phone] www.paceiabs.com
Page 12 of 12

0p
0
PaceAnalyfical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Mathis Storage Tank
Lot Number:W125016
Date Completed:10/27/2021
NIM�� Mr�
10/27/2021 10:30 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI Ndm[ACere00- -Board
ANSI
eORft
Al
C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: W125016
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 601 OD, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids, the initial sample amount used for the following sample deviated 3X greater than the
standard procedure: W125016-001. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: W125016
Sample Number Sample ID Matrix Date Sampled Date Received
001 Mathis Storage Tank Solid 09/23/2021 1330 09/24/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of10

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: W125016
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Mathis Storage Tank
Solid
% Volatile Solids
SM 2540G-
92
%
5
001
Mathis Storage Tank
Solid
Ammonia - N (gas
350.1
28000
mg/kg
5
001
Mathis Storage Tank
Solid
Nitrate -Nitrite - N (soluble)
353.2
55 S
mg/kg
5
001
Mathis Storage Tank
Solid
Phosphorus
365.1
8900 S
mg/kg
5
001
Mathis Storage Tank
Solid
TKN
351.2
73000
mg/kg
5
001
Mathis Storage Tank
Solid
Aluminum
601 OD
2500
mg/kg
6
001
Mathis Storage Tank
Solid
Calcium
601 OD
15000
mg/kg
6
001
Mathis Storage Tank
Solid
Copper
601 OD
19
mg/kg
6
001
Mathis Storage Tank
Solid
Potassium
601 OD
8600
mg/kg
6
001
Mathis Storage Tank
Solid
Sodium
601 OD
4600
mg/kg
6
001
Mathis Storage Tank
Solid
Zinc
601 OD
43
mg/kg
6
(11 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 10

Client:Terra Renewal Services, Inc. Laboratory ID:W125016-001
Description: Mathis Storage Tank Matrix: Solid
Date Sampled: 09/23/2021 1330 % Solids: 4.02 09/28/2021 2314
Date Received:09/24/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
09/30/2021 2351 MOM
17282
1 350.1
(Ammonia - N) 350.1
25
10/07/2021 1835 DAK
18067
1
(Nitrate-Nitr) 353.2
1
09/30/2021 1530 AAB
17351
1
(Phosphorus) 365.1
10
10/06/2021 1209 DMA
09/30/2021 1140 17151
1
(Soil pH meas) 9045D
1
09/27/2021 2239 NBW
16750
2 351.4
(TKN) 351.2
5
10/05/2021 1824 DMA
10/05/2021 1216 17657
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
92
%
1
Ammonia - N (gas diffusion)
350.1
28000
6200
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
55 S
5.0
mg/kg
1
Phosphorus
7723-14-0 365.1
8900 S
1200
mg/kg
1
Soil pH measured in water C> 17.5 ° C
9045D
5.0
su
1
TKN
351.2
73000
6200
mg/kg
2
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 10/26/20211017 CMF
10/19/2021 2053 19390
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
420
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
420
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
420
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
420
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
420
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
420
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
420
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
76 41-132
Tetrachloro-m-xylene
68 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 09/30/2021 1354 CMS2 09/29/2021 1239 16640
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B N D 1.9
mg/kg 1
LOQ - Limit of Quantitation
B - Detected in the method blank
E - Quantitation of compound exceeded the calibration range
Q - Surrogate failure
ND - Not detected at or above the LOQ
N - Recovery is out of criteria
P - The RPD between two GC columns exceeds 40%
L - LCS/LCSD failure
H - Out of holding time
W - Reported on wet weight basis
S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 10

Client:Terra Renewal Services, Inc. Laboratory ID:W125016-001
Description: Mathis Storage Tank Matrix: Solid
Date Sampled: 09/23/2021 1330 % Solids: 4.02 09/28/2021 2314
Date Received:09/24/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 09/29/20211537 JMH 09/28/2021 1049 16783
2 3050B 6010D 1 09/30/20210629 JMH 09/28/2021 1049 16783
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5
6010D
2500
160
mg/kg
1
Arsenic
7440-38-2
6010D
ND
5.9
mg/kg
1
Cadmium
7440-43-9
6010D
ND
2.0
mg/kg
1
Calcium
7440-70-2
6010D
15000
2000
mg/kg
1
Copper
7440-50-8
6010D
19
3.9
mg/kg
1
Lead
7439-92-1
6010D
ND
3.9
mg/kg
1
Magnesium
7439-95-4
6010D
ND
2000
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
16
mg/kg
1
Nickel
7440-02-0
6010D
ND
16
mg/kg
1
Potassium
7440-09-7
6010D
8600
2000
mg/kg
2
Selenium
7782-49-2
6010D
ND
7.9
mg/kg
1
Sodium
7440-23-5
6010D
4600
2000
mg/kg
1
Zinc
7440-66-6
6010D
43
20
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 10

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 8 of 10

PACE ANALYTICAL SERVICES, LLC
North Carol ina Permit Pa ram eta rs
2. kesidu4g &wl be aaalrw to dernous(:att, trey 8L-0 -source ComBn-dtian
Awl 'Re-w cry Act (RCi2N. 'date aaa`
sh - queney specified -n
AttRobm- ent A, and tle- Pen ittee s:lnli mmntahi these rauktm fix r mii urmn d �ut� yews, Any
axr� li��aH fRnrl the rrc)ni-rnuntg;n ERt3.crndition shall be specified im AttachmmT A-
i xu n lysis shaf imlud-z the following paia uelbrs (dbe, regulatory lavvi in in illiyMMs pur Iilcr
is in Parea[h- eses�
3. Au analysis shall be LDDUducted an rr--NWt !i from um-h s%)urcc l,murating N::ility at the fT--giLn y
si rxaficd in Attaelureeat A, and the P,=ittw shall Mairttaitx the FMtlltr iOf a imfnimllm ffVt' Yt.�LM.
The analysis sheO iuclude the iull,awa� p,rr,mctum
Aluminum T'.'Ierewy
elwas 'um
O
Ammonia- )from ___-- hlaiybdteTmtrl
SS'1C'rALIM
Arv—,ric NickrA
Sodium
�.I
wr
a�rniuir
i 2$iEtaO�PVi�te LVi[rcr�e¢L
i il+}iu L
ii+cent Toni SQ"
i"
Copper-- - -
— pH
71ac
—
Volatile sulidli
TparT
)NI usgl,r,nlx
�j
magnesium
TERRA RENEWAL SERACE
AttacimmittaCOCior---sources: Date;
WQN36936 Version L.0
Shall Version 1402 0
E'aj�a g �-I6 :22
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
Samples Receipt Checklist {SRC) (MEOOISC-151
RCti'€Ser$'SJ29{ DZ4
acu twOne, Issulr.R AuthoTlty; Pace ENV - WCOL Pam "- VF
Sample Rc cipt Chooldist (SRC)
Client rear,, Reflowill Cc olwlr lnspudod by[date; tc; 49 25+_I13I Lot 1: W 25 D 15
bieart of ruc;aipt; J PucQ Client € PS FcdGx Ortar-.
Yes
J I Ala
E_ Were CxisLoejy Beals prnnnt on the cook r?
'Ycsl
F!NDI
d NA
2, 1l'custud}' scals wore •rosent, wemit-ey intact and umbml:ffn',
pH Strip ID: C k lorine- Sutir m: KA Tasted by- J A _
Original it-npetaaQa upon receipt ! Derived (Carrect:.d) tomp-cranmro upon Teceipt °1nSolid Snap -Cup ID- 21.1928
3,6 j K6 c�C NA j NA cC+ NA � HA 8Cr NA I NA e.-C
mellrod; ❑R;nperaturc clank 04 ainst r3oulen TR Gaya, ID: list Ciun C m-reckon Faclor. 'C
Method efcoolaur ❑*� lk+et Ice � Ice Pranks ❑ Dry:ce ❑ None
[7Yesj
$
❑N(3
❑✓ NA
3. EfterthpErature of any coin 16rtxct2�jod C.FC'., was I rojactManagerplat=tied?
L'rM ■gas ;Notified by., phone.' email I face-to-face (cimlc onc),
4_ N rho commercial oxvtw's packing slip attached to ibis Earn'?
5, Were prapar custody pr0CCd.;rrs(reliEiquishadlrecelved) foil ckwead?
f Yes
T4(3
NA
,7 -yesl
Lj NO
_
77
Yes
[-. No
6. Weave =YPPlP IDS Iiskxl on ft: CDC.:':
+{
Yes
No
17. Were sample IDs listed qm all sample Contaor O.
❑
Ycs
No
& Was col lectinn Late & rime lis'od on the C OU?
d
Ye5
I _. Nu
LiNo
9. Vdas col1t eC iva 6u[e & time listed on all sample € Dnta iners?
r Yeq
113, Did all uentainer ]abal bfarmation (ID, clear, time) ugrcc with the
d Ye.;
El Ncr
J J , 1Wum ta5-1s to be perfiormed listed on th a COC?
2, L)id all .sairnples arrive in 11,e grope- CrmtaineT.9 fnr Poch rlsst andiar 'n goad oorsditiars —
(un N*jkCrL hcl.� r)rt, cl-',') wry..._.._
-3. Was adequate samplcvolurrla availab]e?
❑ Ycs
❑Pao
© Ycs
No.'
Ycs I
L I Noj
14. Ware all carnpla;s receivedl wi hin V. the holding time or49hotim, wdelievereom6s CrsC
JZ Ye,;
Ld -lr1
❑NO
I .S. W'Lrg any SM P1es MIt3i11ers to issitt `exr es (eirclrr ono) snmplcs Not listed ai C QC7
❑Yes
❑, NA
l6_ For VOA antl RSK-175 sainplcs,'Ncm bubbles present>'°pea-.size" ;'/+" nr 6mm it. dime=.)
ut arty of the VOA vials''
YcsLl
Nn
I/NA
17. Vr = all D1104-3rktAl5rnafrient samples r+eceivecl fJ a pH of•,- 2° — -
13. Wmall cyaa7id samples received at a pH > 12 erd buffida sfunp,lca r ircd at a pH> y,,
Y
L F-\.-e>
rNA
❑ Yzti
El N4
ONA
19. wtvr ;ail upphi R'b:e NHy er cyanr er 0623, (< 0,5mg-IL) sanmp cs o
residual Chlorine?
I ❑ Yes
❑ Nn
ONA
�bo. Were client rcmzrka?requesik (i_e_ reslue-q'r l dHution% MS,MSD desiguationns, etc...j
t;urruk;tly i-amuribedform die COC into toe cnmrriert t linn in 1.1MS?
W'95 tcwc uo�c number listed on the ewtain r IWi6i? if ycs. Qiiotc #
Ycs
J No
121.
'anrpk PreScr vati41r ( Unt be c o nplctod for any samplc(s) incorrectly preservfA err wiIh h midspar:m,)
Sannplc(s).wurc rwci%7A incorrect v preserved and were adihrsted newrdingly
in sam pie receiving with NA n aL pf ai rub, orm: M SO4.. HNW, HCI, NaOH using SR -i� "A
Time of pmervoilon NA _._.. If :noro than one pr:servstivc is :heeded, please note in the comments helmv-
Sarnpl.5(s) xa wcm rccchrod with bubbles mm in Run =r.
Sarrhnl&;(;) NA were received %virb TRC > 0.5 inglL (W419 is j,) ) aiul were
8(1jus-rd auurd'uigly in sample receivill2 vrith 3odiwn Ilt =lf (N4�S203) with Shealy ID; NA
SR k aCcode labols app[jW 4'; dSH Dim: c s.-2021
Corr MCnts;
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 10 of 10

0p
0
PaceAnalyfical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: NC Samples
Lot Number:WL01015
Date Completed:01/26/2022
Revision Date: 01/19/2022
NIM�I�Mr�
01/27/2022 9:38 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 20

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WL01015
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
This report supersedes all other versions of the same report.
Inorganic Metals
Due to the matrix and low percent solids, these samples had an initial weight that is 3x greater than
standard procedure: WL01015-001, WL01015-002, WL01015-003. The LOQ has been adjusted
accordingly.
Report Revision 01/27/22
Due to client request the % solids result was reanalyzed for sample -003. The sample yielded a lower
result and has been reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 20

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WL01015
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
Tyson/Willisboro
Solid
11/30/2021 1130
12/01/2021
002
Tyson/Harmond
Solid
11 /30/2021 1230
12/01/2021
003
Advanced Foods/Claramont
Solid
11 /30/2021 1430
12/01/2021
(3 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 20

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WL01015
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
Tyson/Willisboro
Solid
% Volatile Solids
SM 2540G-
98
%
8
001
Tyson/Willisboro
Solid
Ammonia - N (gas
350.1
1500
mg/kg
8
001
Tyson/Willisboro
Solid
Flashpoint (Pensky-
1010B
>140
° F
8
001
Tyson/Willisboro
Solid
Nitrate -Nitrite - N (soluble)
353.2
44
S
mg/kg
8
001
Tyson/Willisboro
Solid
Paint Filter Test
9095B
Fail
pass/fail
8
001
Tyson/Willisboro
Solid
Phosphorus
365.1
3700
S
mg/kg
8
001
Tyson/Willisboro
Solid
TKN
351.2
52000
S
mg/kg
8
001
Tyson/Willisboro
Solid
Aluminum
6010D
150
mg/kg
11
001
Tyson/Willisboro
Solid
Copper
6010D
27
mg/kg
11
001
Tyson/Willisboro
Solid
Zinc
6010D
38
mg/kg
11
002
Tyson/Harmond
Solid
% Volatile Solids
SM 2540G-
87
%
12
002
Tyson/Harmond
Solid
Ammonia - N (gas
350.1
12000
mg/kg
12
002
Tyson/Harmond
Solid
Flashpoint (Pensky-
1010B
>140
° F
12
002
Tyson/Harmond
Solid
Nitrate -Nitrite - N (soluble)
353.2
58
mg/kg
12
002
Tyson/Harmond
Solid
Paint Filter Test
9095B
Fail
pass/fail
12
002
Tyson/Harmond
Solid
Phosphorus
365.1
19000
S
mg/kg
12
002
Tyson/Harmond
Solid
TKN
351.2
59000
mg/kg
12
002
Tyson/Harmond
Solid
3+4-Methyl phenol
8270E
0.83
mg/L
13
002
Tyson/Harmond
Solid
Aluminum
6010D
8100
mg/kg
15
002
Tyson/Harmond
Solid
Calcium
6010D
39000
mg/kg
15
002
Tyson/Harmond
Solid
Copper
6010D
13
mg/kg
15
002
Tyson/Harmond
Solid
Potassium
6010D
3600
mg/kg
15
002
Tyson/Harmond
Solid
Sodium
6010D
3700
mg/kg
15
002
Tyson/Harmond
Solid
Zinc
6010D
56
mg/kg
15
003
Advanced Foods/Claramont
Solid
% Volatile Solids
SM 2540G-
95
%
16
003
Advanced Foods/Claramont
Solid
Ammonia - N (gas
350.1
170
mg/kg
16
003
Advanced Foods/Claramont
Solid
Flashpoint (Pensky-
1010B
>140
° F
16
003
Advanced Foods/Claramont
Solid
Nitrate -Nitrite - N (soluble)
353.2
3.8
mg/kg
16
003
Advanced Foods/Claramont
Solid
Paint Filter Test
9095B
Fail
pass/fail
16
003
Advanced Foods/Claramont
Solid
Phosphorus
365.1
800
mg/kg
16
003
Advanced Foods/Claramont
Solid
TKN
351.2
11000
mg/kg
16
003
Advanced Foods/Claramont
Solid
Aluminum
6010D
3400
mg/kg
19
003
Advanced Foods/Claramont
Solid
Calcium
6010D
570
mg/kg
19
003
Advanced Foods/Claramont
Solid
Copper
6010D
450
mg/kg
19
003
Advanced Foods/Claramont
Solid
Lead
6010D
1.9
mg/kg
19
003
Advanced Foods/Claramont
Solid
Nickel
6010D
35
mg/kg
19
003
Advanced Foods/Claramont
Solid
Potassium
6010D
540
mg/kg
19
003
Advanced Foods/Claramont
Solid
Sodium
6010D
1700
mg/kg
19
003
Advanced Foods/Claramont
Solid
Zinc
6010D
140
mg/kg
19
(39 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 4 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-001
Description: Tyson/Willisboro Matrix: Solid
Date Sampled:11/30/2021 1130 % Solids: 4.96 12/03/2021 0215
Date Received:12/01/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
12/07/2021 2024 MSG
24853
1 350.1
(Ammonia - N) 350.1
2
12/06/2021 1541 DMA
24642
1
(Flashpoint () 1010B
1
12/08/2021 0850 KMC
24958
1
(Nitrate-Nitr) 353.2
1
12/04/2021 1640 AAB
24599
1
(Paint Filter) 9095B
1
12/10/2021 1118 KMC
1
(Phosphorus) 365.1
5
12/02/2021 1311 DMA
12/01/2021 1453 24173
1
(Reactive Cya) 7.3.3
1
12/03/2021 1030 AAB
12/02/2021 1117
1
(Reactive Sul) 7.3.4
1
12/08/2021 1626 SJL
12/02/2021 1117
1
(Soil pH meas) 9045D
1
12/12/2021 1927 NBW
25322
1 351.4
(TKN) 351.2
2
12/08/2021 1554 DMA
12/08/2021 1036 24899
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
98
%
1
Ammonia - N (gas diffusion)
350.1
1500
400
mg/kg
1
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
° F
1
Nitrate -Nitrite - N (soluble)
353.2
44
S
4.0
mg/kg
1
Paint Filter Test
9095B
Fail
*
pass/fail
1
Phosphorus
7723-14-0
365.1
3700
S
500
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water Ca) 20.2 ° C
9045D
4.5
su
1
TKN
351.2
52000
S
2000
mg/kg
1
TCLP
Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 12/20/20211308 BWS
26259 12/07/20210012
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
Units
Run
Benzene
71-43-2
8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7
8260D
ND
0.050
mg/L
1
Chloroform
67-66-3
8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6
8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4
8260D
ND
0.010
mg/L
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-001
Description: Tyson/Willisboro Matrix: Solid
Date Sampled:11/30/2021 1130 % Solids: 4.96 12/03/2021 0215
Date Received:12/01/2021
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
Bromofluorobenzene
78
70-130
1,2-Dichloroethane-d4
116
70-130
Toluene-d8
94
70-130
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 01/10/2022 1828 CMF 12/10/2021 1730 25236 12/08/2021 1827
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1
8270E
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.040
mg/L
1
Hexachloroethane
67-72-1
8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7
8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5
8270E
ND
0.040
mg/L
1
Nitrobenzene
98-95-3
8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5
8270E
ND
0.20
mg/L
1
Pyridine
110-86-1
8270E
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.040
mg/L
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
87
37-129
2-Fluorophenol
54
24-127
Nitrobenzene-d5
72
38-127
Phenol-d5
73
28-128
Terphenyl-d14
100
10-148
2,4,6-Tribromophenol
108
41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/8151A
8151A 1 12/16/2021 1602 DAL1
12/13/2021 0915 25336 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L 1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
55 50-112
LOQ - Limit of Quantitation
B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
Q - Surrogate failure
ND - Not detected at or above the LOQ
N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
L - LCS/LCSD failure
H - Out of holding time
W - Reported on wet weight basis
S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-001
Description: Tyson/Willisboro Matrix: Solid
Date Sampled:11/30/2021 1130 % Solids: 4.96 12/03/2021 0215
Date Received:12/01/2021
PCBs by GC
Run Prep Method Cleanup
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A
1 12/15/2021 2243 DAL1
12/03/2021 2140 24550
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
340
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
340
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
340
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
340
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
340
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
340
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
340
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
65 41-132
Tetrachloro-m-xylene
60 35-106
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 12/16/2021 1913 DAL1
12/10/2021 1700 25232 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
N D
0.00040
mg/L
1
Methoxychlor
72-43-5 8081 B
N D
0.0016
mg/L
1
Toxaphene
8001-35-2 8081 B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
49 20-131
Tetrachloro-m-xylene
81 26-132
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 12/08/2021 0807 JAB2
12/08/2021 0331 24447
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471B
ND
1.7
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-001
Description: Tyson/Willisboro Matrix: Solid
Date Sampled:11/30/2021 1130 % Solids: 4.96 12/03/2021 0215
Date Received:12/01/2021
TCLP Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3010A 6010D 1 12/10/2021 1230 KSH2 12/10/2021 0230 25139 12/08/2021 1827
1 1311/7470A 7470A 1 12/14/2021 1038 JAB2 12/14/2021 0642 25465 12/08/2021 1827
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2
6010D
ND
0.15
mg/L
1
Barium
7440-39-3
6010D
ND
0.25
mg/L
1
Cadmium
7440-43-9
6010D
ND
0.050
mg/L
1
Chromium
7440-47-3
6010D
ND
0.10
mg/L
1
Lead
7439-92-1
6010D
ND
0.10
mg/L
1
Mercury
7439-97-6
7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2
6010D
ND
0.20
mg/L
1
Silver
7440-22-4
6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 12/03/2021 1115 KSH2 12/03/2021 0250 24274
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
150
130
mg/kg
1
Arsenic
7440-38-2
6010D
ND
4.8
mg/kg
1
Cadmium
7440-43-9
6010D
ND
1.6
mg/kg
1
Calcium
7440-70-2
6010D
ND
1600
mg/kg
1
Copper
7440-50-8
6010D
27
3.2
mg/kg
1
Lead
7439-92-1
6010D
ND
3.2
mg/kg
1
Magnesium
7439-95-4
6010D
ND
1600
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
13
mg/kg
1
Nickel
7440-02-0
6010D
ND
13
mg/kg
1
Potassium
7440-09-7
6010D
ND
1600
mg/kg
1
Selenium
7782-49-2
6010D
ND
6.4
mg/kg
1
Sodium
7440-23-5
6010D
ND
1600
mg/kg
1
Zinc
7440-66-6
6010D
38
16
mg/kg
1
Footnote(s): *Paint Filter: 59mL collected;
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date Sampled:11/30/2021 1230 % Solids: 3.81 12/03/2021 0215
Date Received:12/01/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
12/07/2021 2024 MSG
24853
1 350.1
(Ammonia - N) 350.1
10
12/06/2021 1417 DMA
24642
1
(Flashpoint () 1010B
1
12/08/2021 1006 KMC
24958
1
(Nitrate-Nitr) 353.2
1
12/04/2021 1645 AAB
24599
1
(Paint Filter) 9095B
1
12/10/2021 1118 KMC
1
(Phosphorus) 365.1
25
12/02/2021 1311 DMA
12/01/2021 1453 24173
1
(Reactive Cya) 7.3.3
1
12/03/2021 1043 AAB
12/02/2021 1117
1
(Reactive Sul) 7.3.4
1
12/08/2021 1626 SJL
12/02/2021 1117
1
(Soil pH meas) 9045D
1
12/12/2021 1928 NBW
25322
1 351.4
(TKN) 351.2
2
12/08/2021 1554 DMA
12/08/2021 1036 24899
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
87
%
1
Ammonia - N (gas diffusion)
350.1
12000
2600
mg/kg
1
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
° F
1
Nitrate -Nitrite - N (soluble)
353.2
58
5.3
mg/kg
1
Paint Filter Test
9095B
Fail
pass/fail
1
Phosphorus
7723-14-0 365.1
19000 S
3300
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water Ca) 20.3 ° C
9045D
5.8
su
1
TKN
351.2
59000
2600
mg/kg
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 12/20/20211333 BWS
26259 12/07/20210012
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date Sampled:11/30/2021 1230 % Solids: 3.81 12/03/2021 0215
Date Received:12/01/2021
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
Bromofluorobenzene
80
70-130
1,2-Dichloroethane-d4
121
70-130
Toluene-d8
100
70-130
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 01/12/2022 2303 CMF 12/10/2021 1730 25236 12/08/2021 1827
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1
8270E
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.040
mg/L
1
Hexachloroethane
67-72-1
8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7
8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5
8270E
0.83
0.040
mg/L
1
Nitrobenzene
98-95-3
8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5
8270E
ND
0.20
mg/L
1
Pyridine
110-86-1
8270E
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.040
mg/L
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
86
37-129
2-Fluorophenol
79
24-127
Nitrobenzene-d5
101
38-127
Phenol-d5
107
28-128
Terphenyl-d14
101
10-148
2,4,6-Tribromophenol
71
41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/8151A
8151A 1 12/16/2021 1649 DAL1
12/13/2021 0915 25336 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L 1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
68 50-112
LOQ - Limit of Quantitation
B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
Q - Surrogate failure
ND - Not detected at or above the LOQ
N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
L - LCS/LCSD failure
H - Out of holding time
W - Reported on wet weight basis
S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date Sampled:11/30/2021 1230 % Solids: 3.81 12/03/2021 0215
Date Received:12/01/2021
PCBs by GC
Run Prep Method Cleanup
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A
1 12/15/2021 2256 DAL1
12/03/2021 2140 24550
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
440
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
440
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
440
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
440
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
440
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
440
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
440
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
73 41-132
Tetrachloro-m-xylene
71 35-106
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 12/16/2021 1928 DAL1
12/10/2021 1700 25232 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
N D
0.00040
mg/L
1
Methoxychlor
72-43-5 8081 B
N D
0.0016
mg/L
1
Toxaphene
8001-35-2 8081 B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
81 20-131
Tetrachloro-m-xylene
80 26-132
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 12/08/2021 0815 JAB2
12/08/2021 0331 24447
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471B
ND
2.1
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-002
Description: Tyson/Harmond Matrix: Solid
Date Sampled:11/30/2021 1230 % Solids: 3.81 12/03/2021 0215
Date Received:12/01/2021
TCLP Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3010A 6010D 1 12/10/2021 1249 KSH2 12/10/2021 0230 25139 12/08/2021 1827
1 1311/7470A 7470A 1 12/14/2021 1051 JAB2 12/14/2021 0642 25465 12/08/2021 1827
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2
6010D
ND
0.15
mg/L
1
Barium
7440-39-3
6010D
ND
0.25
mg/L
1
Cadmium
7440-43-9
6010D
ND
0.050
mg/L
1
Chromium
7440-47-3
6010D
ND
0.10
mg/L
1
Lead
7439-92-1
6010D
ND
0.10
mg/L
1
Mercury
7439-97-6
7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2
6010D
ND
0.20
mg/L
1
Silver
7440-22-4
6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 12/03/2021 1141 KSH2 12/03/2021 0250 24274
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
8100
170
mg/kg
1
Arsenic
7440-38-2
6010D
ND
6.5
mg/kg
1
Cadmium
7440-43-9
6010D
ND
2.2
mg/kg
1
Calcium
7440-70-2
6010D
39000
2200
mg/kg
1
Copper
7440-50-8
6010D
13
4.3
mg/kg
1
Lead
7439-92-1
6010D
ND
4.3
mg/kg
1
Magnesium
7439-95-4
6010D
ND
2200
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
17
mg/kg
1
Nickel
7440-02-0
6010D
ND
17
mg/kg
1
Potassium
7440-09-7
6010D
3600
2200
mg/kg
1
Selenium
7782-49-2
6010D
ND
8.7
mg/kg
1
Sodium
7440-23-5
6010D
3700
2200
mg/kg
1
Zinc
7440-66-6
6010D
56
22
mg/kg
1
Footnote(s): *Paint Filter: 50mL collected;
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date Sampled:11/30/2021 1430 % Solids: 6.95 01/24/2022 2259
Date Received:12/01/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
12/07/2021 2024 MSG
24853
1 350.1
(Ammonia - N) 350.1
1
12/06/2021 1419 DMA
24642
1
(Flashpoint () 1010B
1
12/08/2021 1040 KMC
24958
1
(Nitrate-Nitr) 353.2
1
12/04/2021 1647 AAB
24599
1
(Paint Filter) 9095B
1
12/10/2021 1118 KMC
1
(Phosphorus) 365.1
5
12/02/2021 1156 DMA
12/01/2021 1453 24173
1
(Reactive Cya) 7.3.3
1
12/03/2021 1032 AAB
12/02/2021 1117
1
(Reactive Sul) 7.3.4
1
12/08/2021 1626 SJL
12/02/2021 1117
1
(Soil pH meas) 9045D
1
12/12/2021 1932 NBW
25322
2 351.4
(TKN) 351.2
5
12/14/2021 1712 DMA
12/08/2021 1036 24899
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
95
%
1
Ammonia - N (gas diffusion)
350.1
170
41
mg/kg
1
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
° F
1
Nitrate -Nitrite - N (soluble)
353.2
3.8
0.82
mg/kg
1
Paint Filter Test
9095B
Fail
pass/fail
1
Phosphorus
7723-14-0 365.1
800
100
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water Ca) 20.3 ° C
9045D
4.3
su
1
TKN
351.2
11000
1000
mg/kg
2
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 12/20/20211358 BWS
26259 12/07/20210012
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date Sampled:11/30/2021 1430 % Solids: 6.95 01/24/2022 2259
Date Received:12/01/2021
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
Bromofluorobenzene
84
70-130
1,2-Dichloroethane-d4
122
70-130
Toluene-d8
101
70-130
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 01/10/2022 1915 CMF 12/10/2021 1730 25236 12/08/2021 1827
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7
8270E
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1
8270E
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
0.040
mg/L
1
Hexachloroethane
67-72-1
8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7
8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5
8270E
ND
0.040
mg/L
1
Nitrobenzene
98-95-3
8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5
8270E
ND
0.20
mg/L
1
Pyridine
110-86-1
8270E
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
0.040
mg/L
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
90
37-129
2-Fluorophenol
66
24-127
Nitrobenzene-d5
78
38-127
Phenol-d5
87
28-128
Terphenyl-d14
99
10-148
2,4,6-Tribromophenol
131
41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/8151A
8151A 1 12/16/2021 1712 DAL1
12/13/2021 0915 25336 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L 1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
65 50-112
LOQ - Limit of Quantitation
B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
Q - Surrogate failure
ND - Not detected at or above the LOQ
N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
L - LCS/LCSD failure
H - Out of holding time
W - Reported on wet weight basis
S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date Sampled:11/30/2021 1430 % Solids: 6.95 01/24/2022 2259
Date Received:12/01/2021
PCBs by GC
Run Prep Method Cleanup
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A
1 12/15/2021 2309 DAL1
12/03/2021 2140 24550
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
69
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
69
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
69
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
69
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
69
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
69
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
69
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
72 41-132
Tetrachloro-m-xylene
69 35-106
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 12/16/2021 1944 DAL1
12/10/2021 1700 25232 12/08/2021 1827
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
N D
0.00040
mg/L
1
Methoxychlor
72-43-5 8081 B
N D
0.0016
mg/L
1
Toxaphene
8001-35-2 8081 B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
79 20-131
Tetrachloro-m-xylene
66 26-132
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 12/08/2021 0817 JAB2
12/08/2021 0331 24447
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471B
ND
0.31
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 15 of 20

Client:Terra Renewal Services, Inc. Laboratory ID:WL01015-003
Description: Advanced Foods/Claramont Matrix: Solid
Date Sampled:11/30/2021 1430 % Solids: 6.95 01/24/2022 2259
Date Received:12/01/2021
TCLP Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3010A 6010D 1 12/10/2021 1300 KSH2 12/10/2021 0230 25139 12/08/2021 1827
1 1311/7470A 7470A 1 12/14/2021 1054 JAB2 12/14/2021 0642 25465 12/08/2021 1827
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2
6010D
ND
0.15
mg/L
1
Barium
7440-39-3
6010D
ND
0.25
mg/L
1
Cadmium
7440-43-9
6010D
ND
0.050
mg/L
1
Chromium
7440-47-3
6010D
ND
0.10
mg/L
1
Lead
7439-92-1
6010D
ND
0.10
mg/L
1
Mercury
7439-97-6
7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2
6010D
ND
0.20
mg/L
1
Silver
7440-22-4
6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 12/03/2021 1144 KSH2 12/03/2021 0250 24274
2 3050B 6010D 3 12/03/2021 1356 KSH2 12/03/2021 0250 24274
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
3400
26
mg/kg
1
Arsenic
7440-38-2
6010D
ND
0.96
mg/kg
1
Cadmium
7440-43-9
6010D
ND
0.32
mg/kg
1
Calcium
7440-70-2
6010D
570
320
mg/kg
1
Copper
7440-50-8
6010D
450
1.9
mg/kg
2
Lead
7439-92-1
6010D
1.9
0.64
mg/kg
1
Magnesium
7439-95-4
6010D
ND
320
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
2.6
mg/kg
1
Nickel
7440-02-0
6010D
35
2.6
mg/kg
1
Potassium
7440-09-7
6010D
540
320
mg/kg
1
Selenium
7782-49-2
6010D
ND
1.3
mg/kg
1
Sodium
7440-23-5
6010D
1700
320
mg/kg
1
Zinc
7440-66-6
6010D
140
3.2
mg/kg
1
Footnote(s): *Paint Filter: 72mL collected;
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range Q - Surrogate failure
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 20

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 17 of 20

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 18 of 20

PACE ANALYTICAL SERVICES, LLC
North Carolina Perrtnit Parameters
2, Rcsiduals a:iall be aoalyztxd to they are - oura� Cpr�yefyatlou
ar_d RTtmvfjy Acr. (RCRA)_ 'Poe amijUp rrwivw V, [pliabibty, r�acii and toxicity
characiriatic lexclxi��g procedure TC sl�a 4y apacitied ku
4.tCer,hTnenl. A, aisd the Pcrmijae shall mtlin�xi I.Lww zelaks :-3x a rtiini M of five years, Any
rxcePtia sT�s fir�»n tlae retluii aittieuts lu diLs vm litkm shall ire specTicd ii A#tar.Lu=( A.
The TCLP awdygis shall include the Miming piErnmr-tcrs [th(,, in niftpms Per liter
is it parenthpara};
LU
4
4
C}
�'sea.ic (5.0}
] ,�T}iti3�lorr�attiaene {7.5}
l�ikr4bene {2.0)
Pezimi lm-opbrM]. (100-0)
H nnum (] ODA)
1,2-Dichloroc brw (03)
T# nzgte {i}.5)
1.1-filchlarouthyLue (0.71
PyHdLuc (5,0)
Selzer-Jm (1,0)
CaEVlriv (1-il)
2,4-Dhdtrota1ivac (0.13)
2,rb [e#sQcfikorida (CS)
Eridriu (0.02)
Sr1v (5-0)
ChlbrdsmC (0,01}
11exach1erobcnacnc (0,;3)
Tetrae:7loroethyla (0. r)
-clik robanzeita (100.0}
aAorcrfoiin (u_ 0)
1Sro iu�i(5.0'
egtaclli (aaud +ts hyd7 rid e) ; ToxaplYelae (U 5)
, i-bnrtadi (0,5) Tricaloroelhylene (0-5)
Hcxrohl{art l3�a� {3.b1 2,%U-Tri&lvr4?4ct,l(400A)
meal MCI,)
($.0) 7,4,6-Tric}t'nnp4tcnai (2,0)
v-Cr=Ql MOM)
Lindamo (0,4)
2,4,5 ` P (Sslvox) (1-0)
p-Cresol (200-0)
-- Mcrc:uy (0.2)
Vinyl aliln6dde (0.2)
ao1(200.0)
Mr:CaQXWl,14X- (10.0)
.2.s4-U. f10,01
h e#h l ttltyl kc,ttmo RO-0,0} --
._..
3_ An mab-sls shill be uvnduotel ar- rmidua15 fbin eacJh fourae gmicrating fkdhly at the tiapxmcy
Epeaifed in Alrachment A, and the I'FrmiGtLIZ s13a11 j,a13Lr8i❑ Ole insults fir a-titrmt,m of live ycar&
The analysis shall inAudt the following pzxarnek ;
Ablrninum -.
i
Am rionla-Nifmorn
Arsenic
Cadrium
calcium
( pGr
T rlcl
Magmsflm
WQ2036936 Yer6tin 1-D
1tiUmury
patasslum
MiAybdwum
Selr—uum
Nickel
Sodimu
1*x113�taNitrito �ltr�ger
T3
Port: Total Solids
Ph
c
Fhosplxan,s
Volatile Solids
PCs!$
TERRA RENEWAL SERVICES
479 747-fI92
S1>,U V eraian 140210
pea 8 of l
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 19 of 20

PACE ANALYTICAL SERVICES, LLC
Samples Receipt Cfiecldist(5R3CI (MEj3aj9C-isj Kevis�,9/29f2020
. ace rr�r+yl,Caf t55u h' FF AL 1hoi i ty_ Pace ENV • WCOL Page 1 of!
aMPIC receipt C hecldiSt (S'R
Client: araKerxnral Onaler Intlx:vrM [;yi&,Lte- JI CiY 12rC11f 1Y21 I,cSti : WUJIO15
PpHS
rrftCOdpt: Pane GEjmt UPS Fecif;x Otfl-•-
s _ V, No 1, Were cust�d . seab PTeW 4311 fte coal�r7
s NU +� N A 2, if ;uEtotiw� scars were rep.ent, were they intact and unbrokcn7
Ir1D-- `A C'1torirtr. St-ip ID= -` _ Teml by; r4rt
Wgi:na[ te.ntperdurz upon receipt? f)rrived (Corrected) t.emperaxtrc upon receipt %solid Suap-Cup [1): 3t-2bGl-2�G1
3.7 ++3.7 oe vli- Yiti c�C rKA IKA oC NA fNA v�
Method: E[lamperatum Blank �--VJAgairim I.IotticA IN Gan ID: III Our. Correc`on Far, -or; C `r~
Meal od 4�i 4x*hLut' U1 Wet 1 t;r. ❑ 14'e Pa4❑ D r Ica ❑ Norre -
r IIf 1 t f of 4
❑ Yes
❑ Nu
I.Y 1 1ri
- Cmpau urI I� awy CO et .,T,;, od G.v C, AwW; rnijCct fv1anRVr3Nlottlieol(
Pb1 was Mytifipd b}r� p}lorle f emlil I face-W-fact(cirr lz: nnp),
Yex
No
NA
d. 15 1[1e CCNruncruibl CJllriel,'.s packing.0ip a7aobed Lu rhi5 fora,'
zYes
71 Yes
Nu
�. Were proper custody procelimts (rellnquishaYrcceived) fo€IOP cM
16. Were =ip[-u IDs AstLd on C-in C'f C?
_Yes
Yes
❑M
Na
7. % eJ%e sarn;,le 11)5:israd w ill 8amp[c conminera?
&Was cu11Vticn date & time 144ud on the COO R_
yes
No
9. Wa-s cullm4iun date & time I -Pled or, all sa.lupleconklinvrs7
J Ye~;
T''o 1
10. Did all container Jabal j-0formation (I[}, fie, lirae) ftgrcc wit1 Lila COC?
Q Yea
LANOI
I J J , WEM tuts 0 be perfaimed lisred on th C)OC4 -
❑ v,-;LJNO
Yes No
Ycs No
El Yed '7No
i2- Did a.] samples arrive in Ihe. proper Mitainers fur cwh tesr artdlar in goad conditias
(unroroken, lidw on. cri.`.);.
13. Was adequ* sa-1 [a vDlulneavailubl.0
14- Wtwe JAI samples received wKin Vz the [holding time or 48 hours, whEchcvcr caires J M- 0
15, Were zny 9pmplcE containers miFOngkxcess (circle Cnv) salrplc-e lent Iiajt�cl on f_,OC?
❑d NA 16. For VOA and RSK-L75 wapies, wert�bubblw present "peg-tiiz#r" 4'ra"ar6inm in diam't
is any of the VOA Vlais?
V NA 17. Were al DROlmetali+nuLrient sam pies received at a pi of< 2?
[71NA 18- Wm all cywilde sa mp'tM reooivcd at a Id > 12 turd su117c[r harm ley nxCi'v.d at a pH > 9`
A ..- . War all upp it a NI-kVTK Cyan +pliena i25. l: i j08.3 (-=z 0.5mg i) sarr.'p tFs rce of
20. VYCrC tilicllt rcmarkOracu�ts (i.e- reqursccxl dilutions, 1vtS!MSD designmtinus, etc...)
�❑ Yes ❑ ri;o �hi turrutly traimcri had Freff he COC into tie gammon[ seWon in LIMS?
Yes N :-i, Was the uoleltumbcr Iister! tt7t INN: container label? I Fyvb,PaoLriv - —
5ample I'reservatiun (I41ust he cl3mplet i ally s ,ply s} irt+rsarrcxtly preserved or will headspace-)
Sarripia(h) m,' _. were t�eceivcd inmT-crtly presenTedand wcre adjusted a000rJ:rr',
in sample re+caiv[rtgW[1FI K mL afc'_rcle nr_o; fi I� O4, HNQ3, I✓]CI, hiu0li u�iur It! 1 t _
T' me of preseryanon If more OM oPreserve V-e is n"&d, p Icasv 11111M in Fit- ccxiimants below.
NA - - -
were reeeimil with bubbles >6 rnm ifS diarrML
tnples(s) NA wcre received with TKC m&+L (I f 4 J 9 is fJ{P ; and tyere
lusCet kAUcord1ngly ir, arnft[t m0eiving wl[it sodium thiouiitsre (Na�S20x1 vt itil 811eaJy 1D: A
bwtrnit lxbrls Hllplied by_ JR43Z UBP
Conlint:'aI.5;
0041: 129)Z12Q21
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 20 of 20

0p
0
PaceAnalyfical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Mathis-1
Lot Number:WL10011
Date Completed:12/31/2021
NIM�I�Mr�
01/04/2022 8:49 AM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: WL10011
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 601 OD, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix and low percent solids, the following samples have an initial weight that is 3x greater
than standard procedure: WL10011-001. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The following sample was analyzed outside of analytical holding time: WL10011-001. Sample has been
qualified with an "H" accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: WL10011
Sample Number Sample ID Matrix Date Sampled Date Received
001 Mathis-1 Solid 12/08/2021 1630 12/10/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of10

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: WL10011
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
Mathis-1
Solid
% Volatile Solids
SM 2540G-
95 BH
%
5
001
Mathis-1
Solid
Ammonia - N (gas
350.1
17000
mg/kg
5
001
Mathis-1
Solid
Nitrate -Nitrite - N (soluble)
353.2
34 S
mg/kg
5
001
Mathis-1
Solid
Phosphorus
365.1
7000
mg/kg
5
001
Mathis-1
Solid
TKN
351.2
48000
mg/kg
5
001
Mathis-1
Solid
Aluminum
601OD
3100
mg/kg
6
001
Mathis-1
Solid
Calcium
601OD
11000
mg/kg
6
001
Mathis-1
Solid
Copper
601OD
56
mg/kg
6
001
Mathis-1
Solid
Potassium
601OD
3000
mg/kg
6
001
Mathis-1
Solid
Sodium
601OD
1600
mg/kg
6
001
Mathis-1
Solid
Zinc
601OD
110
mg/kg
6
(11 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 10

Client:Terra Renewal Services, Inc. Laboratory ID: WL10011-001
Description: Mathis-1 Matrix: Solid
Date Sampled:12/08/2021 1630 % Solids: 8.54 12/13/2021 2328
Date Received:12/10/2021
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
12/16/2021 1929 GAH
25969
2 350.1
(Ammonia - N) 350.1
50
12/30/2021 2230 DAK
27046
1
(Nitrate-Nitr) 353.2
1
12/17/2021 1118 AAB
26061
1
(Phosphorus) 365.1
25
12/14/2021 1219 DMA
12/11/2021 1559 25306
1
(Soil pH meas) 9045D
1
12/12/2021 2001 NBW
25322
1 351.4
(TKN) 351.2
5
12/15/2021 1757 DMA
12/15/2021 1231 25672
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 2540G-1997
95 BH
%
1
Ammonia - N (gas diffusion)
350.1
17000
5900
mg/kg
2
Nitrate -Nitrite - N (soluble)
353.2
34 S
2.3
mg/kg
1
Phosphorus
7723-14-0 365.1
7000
1500
mg/kg
1
Soil pH measured in water Ca) 20.6 ° C
9045D
5.4
su
1
TKN
351.2
48000
2900
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 12/16/2021 2245 DAL1
12/12/2021 1825 25318
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
200
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
200
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
200
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
200
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
200
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
200
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
200
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
70 41-132
Tetrachloro-m-xylene
70 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 12/20/2021 0551 JAB2 12/20/2021 0225 25655
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B N D 0.90
mg/kg 1
LOQ - Limit of Quantitation
B - Detected in the method blank
E - Quantitation of compound exceeded the calibration range
Q - Surrogate failure
ND - Not detected at or above the LOQ
N - Recovery is out of criteria
P - The RPD between two GC columns exceeds 40%
L - LCS/LCSD failure
H - Out of holding time
W - Reported on wet weight basis
S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 10

Client:Terra Renewal Services, Inc. Laboratory ID: WL10011-001
Description: Mathis-1 Matrix: Solid
Date Sampled:12/08/2021 1630 % Solids: 8.54 12/13/2021 2328
Date Received:12/10/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 12/21/2021 0800 JMH 12/20/2021 0042 26150
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
3100
73
mg/kg
1
Arsenic
7440-38-2
6010D
ND
2.7
mg/kg
1
Cadmium
7440-43-9
6010D
ND
0.91
mg/kg
1
Calcium
7440-70-2
6010D
11000
910
mg/kg
1
Copper
7440-50-8
6010D
56
1.8
mg/kg
1
Lead
7439-92-1
6010D
ND
1.8
mg/kg
1
Magnesium
7439-95-4
6010D
ND
910
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
7.3
mg/kg
1
Nickel
7440-02-0
6010D
ND
7.3
mg/kg
1
Potassium
7440-09-7
6010D
3000
910
mg/kg
1
Selenium
7782-49-2
6010D
ND
3.7
mg/kg
1
Sodium
7440-23-5
6010D
1600
910
mg/kg
1
Zinc
7440-66-6
6010D
110
9.1
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range
ND - Not detected at or above the LOQ N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40%
H - Out of holding time W - Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q - Surrogate failure
L - LCS/LCSD failure
S - MS/MSD failure
Page 6 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 10

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 8 of 10

PACE ANALYTICAL SERVICES, LLC
North Carolina Permil Parameters
2 Xis duab stall be znalyzed w demmatraou dvti y are Conservation
at•.! RecorCTY Act {11-CF ti TM atgogj
requerrc�r specified in
A't;dUCKt A, t[1r1 tln Parmitt431e shill rnfi.lALu -.h, €w msulfs for a miuilmar- of five years. Any
cxceptiow f':om the rcLjmT% melt8 is this. coi4r Loa bliAll by specified in Attacla:amtA
,Ijle nmlysis sh211 b'cluiimU folly ILS rrarrmefM Me. ftvktory level mmilEigramr per liter
A in =enamu a},
3_ AP aataiysis half WU&Qted Ct -cddt�als froul Moh 5ourac mratjng S cility at Jl e fctgjrwV
gpeciii&i iu A=lamerr, A, armi the Jtrmittm shall M1911tain dir, resttlts fcr Z MinUMI t Df five yeas
the a-7atlyas sltaU iiuclude tLL: t'I)llowng panjbetuer&
W�
Atulvieum
pA��nuniH-I�tseq
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9cl�tiium
Nirlcol
Sodium
Nitrate_Mitrite itrog=
1P=Mf TOW Solids
TKN
F
i.ro
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volatile Solids
P B's
TERRA RENEWAL SERVICES
479-747-8192
++aliiC '11112111.tk {�. t'4i.•,OiiC 9` � f3 11 4 - �ry _ _ Dom• i'�- 14
WQ003035 Va7sion I'() L
Shall Veision 1407 iO 17-- R of t)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
Samples Receiprt Cherldist (5RCI 1ME00-18t-i5) Revised;9/29/2020
acGrlrwh lice I55uing,5.uthority: Pace ENV -buCOL Pagelof 1
aMPIC Receipt Checklist1� (SRC)
-client; Tcrr, ,:neY+f.l ConierInspected bv{dutu 2 '= ]MQ'202; Lts[.r. w..ICpEl
[+4ceu7s u-rec4:pt: LJ P-,3 M j lChcrilt A UPS U 1edEai
Yes ,-" 'No' :, WCF4; c-jsmd ' @fills pre�cnt iin Ole cooleO
Yes' Nu J NA 'Z If wst0dY sells wcrc prs�ert, wol rlijy intact and unrirokert?
I I [ Strip 10: KA Chlorine Strip JD: NA 1'Cstod by NA _
Oi:433a'. kmperature Itpow rers:ipt! Derived (i'o:rected) Innipvratare nrpm receipt lyn; p[ ad Snap -Cap ID; 21-2"J
}.3 j4,3 wC NA eNA DC 1+A ,HA eC, *tit {:tA o-C
Method: fempCCalure [3;r,nk J k iRsr aoctles Jtt Ulm 1D IR Otert Caribuliun factor_ u °C
Method a s:oulari� Wei too L1 Ice JjUks ❑ DTv fccEj -IN4M]e
El yes ONO RINA 3. A1.eml,ex,9nae{ofmnycooler e:sceeded6,0°C.Was PrtsjeCtMara rNotified?
1'M why Nod ied ay: phorin I email f face-to-face (6T.r]e 0]10)-
w Yes Nc, QNA14. ]s nc� s rnmet5cial vaunts: `s paeki slip rrtt;i[ ht d ro this form'
Yes
No
15, iueVc Prtrper cu€.Inrly rocaduruy (relinquisYi lrec ivcr�) follavired`I
7W
Ll No
6. WOro sample Jds 1lstac On the CO M �—
YL-3
!No
7, 11 ere sm. p [a I Ds '-Jstcd ar al] aum>r le ooiswhers?
YGS
No
hdo
S, W;4 cvliact]on d2dc time listed on dse COG.
9. Was celloction EO,; & tame listed On all sum pie onnta:ase,4?
Yew
ties
No.
o
10. Did all 4=tainar :al,rl iilfofrralion (ID. date, time) agrL:: with the CC]C7
l I , WMe E lasbi to be performed listed 4n the COC?
YES
=Y05N-a
12 Drd all ramp:w arrive in tnp prop,- ::onlainerm Fair mHc7 xsf unWar is goad eandillan
(unbraken, lids Orl,
13, Was arfsxluaoa ;m"PI volunse available?Li —
Yes 0 14ri 14. Were all satrtples rmoived tvitltiirl Y2 tht: bolding time tw 48 'ioufb, uh.icaever:0ms s fir.
Yes No 15. Were an snmplCs containers tni sine}ckceas(circle ogle) s,-rmples Nlti Iucd oil Mr.?
LJ Yes ❑No7iXt 16. For VDA U.d RSK-175 �aruples, were bubbles present >"pea-siu'° ('l,"nr 6rnr11 in dlan
inarry oftl;e VDA vials?
yes No VIN A I ?. Were all :3KWm�ta Isrnutrienr sash lea ved at a pH of = 27
yes No �'NA t R. Wer a a:l Cyanide 58c, Ics rece ivej Ara I3 > 12 and s u tf-A, yarn Les Mcc[vuc at a pJi >
Q Ye5 J Na ❑7 fA I`, 1"fere all app]rca a NHx,'f h[,'C an tde p-e�tall 5, IJ6G8,3 G.3rngfl,) samples fC�s o:
�] Ces No �hlq 20` Wr rc -Hent remar{cs,'rcqueRt (i,e, rtquesl.d di]u+irmM, MSI)IST) �csi a2icns, sate.
correctly rranS"IbUd frarn the COC ittur ll:ir c:arnmetrr..kecton in LJhr1S?
Yes LJ , J O I
12l. W;15 the quKirr n„Tnb5r iis4od on the Ifyt;2, < 1130,-
mple Preservatsun (Mint ht� completed for any samplz(.$) incorrcctl}' pnes�ved or w uli hcadspace.)
rnple(s) OJA WM Jr-wived uwturect=y rmi,rved and were ad�ssred accordingly
stunpia Fecnivinp with EA _ mL of cirolsa Ana, MSO4: 21N01, HCI, T+Tu01'i using SR P, 14A tie of preser"Hon 1`A TfMMOMt[tais wtv prmeruatiue is needt�,l, please note in the =nmu_nm below,
NA
weir r'eoc;ivedwith b-bbles:•6 min h diametcr.
41 Vl` k] ) - -- - wen rcccived with '1'RC > 0.5 mglL (lf *W14 is rro) and were
Ins;" accardingiy its sa mP1Pm rec-irinE, tyir]i srldium #JiitlfuIfaLL: with S11=1v 11)r err
harerr,-le labels HppJied by, JRG2
commerrs.
Dblr: 171iV+f9Ql
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.corn
Page 10 of 10

Laboratory Analyses:
- Seven Set Fecal Coliform Data

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 02/04/2021
Reported: 02/05/2021
For: Advance Claremont
Comments: GEOMETRIC MEAN: <241 MPN/g
4 6TATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210204-16-01
Fecal Coliforms
Al
<208
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-01
Percent Solids
Al
9.6
%
SM2540B-2011
02/04/2021
MD
210204-16-02
Fecal Coliforms
A2
<258
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-02
Percent Solids
A2
7.76
%
SM2540B-2011
02/04/2021
MD
210204-16-03
Fecal Coliforms
A3
<263
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-03
Percent Solids
A3
7.6
%
SM2540B-2011
02/04/2021
MD
210204-16-04
Fecal Coliforms
A4
<203
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-04
Percent Solids
A4
9.87
%
SM2540B-2011
02/04/2021
MD
210204-16-05
Fecal Coliforms
A5
<258
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-05
Percent Solids
A5
7.74
%
SM2540B-2011
02/04/2021
MD
210204-16-06
Fecal Coliforms
A6
<257
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-06
Percent Solids
A6
7.79
%
SM2540B-2011
02/04/2021
MD
210204-16-07
Fecal Coliforms
A7
<248
MPN/g
SM92210E-2006
02/04/2021
MD
210204-16-07
Percent Solids
A7
8.07
%
SM2540B-2011
02/04/2021
MD
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210204-16-01 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-02 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-03 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-04 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-05 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-06 Temp on Arrival: 2.5
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210204-16-07 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 06/10/2021
Reported: 06/11/2021
For: Advance Claremont
Comments: GEOMETERIC MEAN = 1399 MPN/g dry weight basis
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210610-17-01
Fecal Coliforms
AC1
<1732
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-01
Percent Solids
AC1
1.16
%
SM2540B-2011
06/10/2021
WC
210610-17-02
Fecal Coliforms
AC2
<1639
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-02
Percent Solids
AC2
1.22
%
SM2540B-2011
06/10/2021
WC
210610-17-03
Fecal Coliforms
AC3
719
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-03
Percent Solids
AC3
2.78
%
SM2540B-2011
06/10/2021
WC
210610-17-04
Fecal Coliforms
AC4
<1183
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-04
Percent Solids
AC4
1.69
%
SM2540B-2011
06/10/2021
WC
210610-17-05
Fecal Coliforms
AC5
<2041
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-05
Percent Solids
AC5
0.98
%
SM2540B-2011
06/10/2021
WC
210610-17-06
Fecal Coliforms
AC6
<2703
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-06
Percent Solids
AC6
0.74
%
SM2540B-2011
06/10/2021
WC
210610-17-07
Fecal Coliforms
AC7
<787
MPN/g
SM92210E-2006
06/10/2021
WC
210610-17-07
Percent Solids
AC7
2.54
%
SM2540B-2011
06/10/2021
WC
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210610-17-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-06 Temp on Arrival: 2.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210610-17-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 03/30/2021
Reported: 03/31 /2021
For: TYSON HARMONY
Comments: GEOMETRIC MEAN: 46,939 MPN/g
4 6TATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210330-17-01
Fecal Coliforms
TH1
36145
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-01
Percent Solids
TH1
0.83
%
SM2540B-2011
03/30/2021
MD
210330-17-02
Fecal Coliforms
TH2
61915
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-02
Percent Solids
TH2
O.81
%
SM2540B-2011
03/30/2021
MD
210330-17-03
Fecal Coliforms
TH3
50000
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-03
Percent Solids
TH3
1.0
%
SM2540B-2011
03/30/2021
MD
210330-17-04
Fecal Coliforms
TH4
31915
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-04
Percent Solids
TH4
0.94
%
SM2540B-2011
03/30/2021
MD
210330-17-05
Fecal Coliforms
TH5
83333
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-05
Percent Solids
TH5
0.96
%
SM2540B-2011
03/30/2021
MD
210330-17-06
Fecal Coliforms
TH6
74468
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-06
Percent Solids
TH6
0.94
%
SM2540B-2011
03/30/2021
MD
210330-17-07
Fecal Coliforms
TH7
22722
MPN/g
SM92210E-2006
03/30/2021
MD
210330-17-07
Percent Solids
TH7
1.01
%
SM2540B-2011
03/30/2021
MD
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210330-17-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-06 Temp on Arrival: 2.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210330-17-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 06/01/2021
Reported: 06/03/2021
For: Tyson Harmony
Comments: GEOMETRIC MEAN: 22,303 MPN/g
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210601-16-01
Fecal Coliforms
TH1
12407
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-01
Percent Solids
TH1
4.03
%
SM2540B-2011
06/01/2021
MD
210601-16-02
Fecal Coliforms
TH2
23936
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-02
Percent Solids
TH2
3.76
%
SM2540B-2011
06/01/2021
MD
210601-16-03
Fecal Coliforms
TH3
34575
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-03
Percent Solids
TH3
3.76
%
SM2540B-2011
06/01/2021
MD
210601-16-04
Fecal Coliforms
TH4
45946
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-04
Percent Solids
TH4
3.7
%
SM2540B-2011
06/01/2021
MD
210601-16-05
Fecal Coliforms
TH5
21108
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-05
Percent Solids
TH5
3.79
%
SM2540B-2011
06/01/2021
MD
210601-16-06
Fecal Coliforms
TH6
21390
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-06
Percent Solids
TH6
3.74
%
SM2540B-2011
06/01/2021
MD
210601-16-07
Fecal Coliforms
TH7
12887
MPN/g
SM92210E-2006
06/01/2021
MD
210601-16-07
Percent Solids
TH7
3.88
%
SM2540B-2011
06/01/2021
MD
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210601-16-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-06 Temp on Arrival: 2.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-16-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 09/02/2021
Reported: 09/07/2021
For: Tyson Harmony
Comments: GEOMETRIC MEAN: 31,173 MPN/g
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210902-15-01
Fecal Coliforms
1-11
40498
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-01
Percent Solids
1-11
3.21
%
SM2540B-2011
09/02/2021
MD
210902-15-02
Fecal Coliforms
H2
74866
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-02
Percent Solids
H2
3.74
%
SM2540B-2011
09/02/2021
MD
210902-15-03
Fecal Coliforms
H3
52147
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-03
Percent Solids
H3
3.26
%
SM2540B-2011
09/02/2021
MD
210902-15-04
Fecal Coliforms
H4
37333
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-04
Percent Solids
H4
3.75
%
SM2540B-2011
09/02/2021
MD
210902-15-05
Fecal Coliforms
H5
9346
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-05
Percent Solids
H5
3.21
%
SM2540B-2011
09/02/2021
MD
210902-15-06
Fecal Coliforms
H6
21164
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-06
Percent Solids
H6
3.78
%
SM2540B-2011
09/02/2021
MD
210902-15-07
Fecal Coliforms
H7
24499
MPN/g
SM92210E-2006
09/02/2021
MD
210902-15-07
Percent Solids
H7
4.49
%
SM2540B-2011
09/02/2021
MD
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210902-15-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-06 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210902-15-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 12/20/2021
Reported: 12/21 /2021
For: Tyson Harmony
Comments: Geometric Mean: 3601 MPN/g
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
211220-19-01
Fecal Coliforms
T-1
<3617
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-01
Percent Solids
T-1
5.53
%
SM2540B-2011
12/20/2021
CL
211220-19-02
Fecal Coliforms
T-2
<3534
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-02
Percent Solids
T-2
5.66
%
SM2540B-2011
12/20/2021
CL
211220-19-03
Fecal Coliforms
T-3
3610
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-03
Percent Solids
T-3
5.54
%
SM2540B-2011
12/20/2021
CL
211220-19-04
Fecal Coliforms
T-4
<3527
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-04
Percent Solids
T-4
5.67
%
SM2540B-2011
12/20/2021
CL
211220-19-05
Fecal Coliforms
T-5
<3745
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-05
Percent Solids
T-5
5.34
%
SM2540B-2011
12/20/2021
CL
211220-19-06
Fecal Coliforms
T-6
<3509
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-06
Percent Solids
T-6
5.70
%
SM2540B-2011
12/20/2021
CL
211220-19-07
Fecal Coliforms
T-7
<3670
MPN/g
SM92210E-2006
12/20/2021
CL
211220-19-07
Percent Solids
T-7
5.45
%
SM2540B-2011
12/20/2021
CL
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 211220-19-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-06 Temp on Arrival: 3.0
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211220-19-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4e4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 08/26/2021
Reported: 08/28/2021
For: Mathis
Comments:
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210826-16-01
Fecal Coliforms
M1
<4444
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-01
Percent Solids
M1
0.46
%
SM2540B-2011
08/26/2021
MD
210826-16-02
Fecal Coliforms
M2
<4444
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-02
Percent Solids
M2
0.45
%
SM2540B-2011
08/26/2021
MD
210826-16-03
Fecal Coliforms
M3
<4348
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-03
Percent Solids
M3
0.46
%
SM2540B-2011
08/26/2021
MD
210826-16-04
Fecal Coliforms
M4
<4348
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-04
Percent Solids
M4
0.46
%
SM2540B-2011
08/26/2021
MD
210826-16-05
Fecal Coliforms
M5
4255
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-05
Percent Solids
M5
0.47
%
SM2540B-2011
08/26/2021
MD
210826-16-06
Fecal Coliforms
M6
4348
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-06
Percent Solids
M6
0.46
%
SM2540B-2011
08/26/2021
MD
210826-16-07
Fecal Coliforms
M7
4255
MPN/g
SM92210E-2006
08/26/2021
MD
210826-16-07
Percent Solids
M7
0.47
%
SM2540B-2011
08/26/2021
MD
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 2

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Page 2 of 2

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 10/12/2021
Reported: 10/14/2021
For: Mathis
Comments:
4 6TATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
211012-32-01
Fecal Coliforms
M1
<7968
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-01
Percent Solids
M1
2.51
%
SM2540B-2011
10/12/2021
MD
211012-32-02
Fecal Coliforms
M2
<7353
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-02
Percent Solids
M2
2.72
%
SM2540B-2011
10/12/2021
MD
211012-32-03
Fecal Coliforms
M3
<8065
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-03
Percent Solids
M3
2.48
%
SM2540B-2011
10/12/2021
MD
211012-32-04
Fecal Coliforms
M4
<7874
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-04
Percent Solids
M4
2.54
%
SM2540B-2011
10/12/2021
MD
211012-32-05
Fecal Coliforms
M5
<8000
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-05
Percent Solids
M5
2.50
%
SM2540B-2011
10/12/2021
MD
211012-32-06
Fecal Coliforms
M6
<8065
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-06
Percent Solids
M6
2.48
%
SM2540B-2011
10/12/2021
MD
211012-32-07
Fecal Coliforms
M7
<8000
MPN/g
SM92210E-2006
10/12/2021
MD
211012-32-07
Percent Solids
M7
2.50
%
SM2540B-2011
10/12/2021
MD
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 211012-32-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-06 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 211012-32-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 01/28/2021
Reported: 01 /29/2021
For: Tyson Wilkesboro
Comments: GEOMETRIC MEAN: <246 MPN/g
4 6TATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210128-12-01
Fecal Coliforms
TW1
233
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-01
Percent Solids
TW1
8.6
%
SM2540B-2011
01/28/2021
MD
210128-12-02
Fecal Coliforms
TW2
<248
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-02
Percent Solids
TW2
8.05
%
SM2540B-2011
01/28/2021
MD
210128-12-03
Fecal Coliforms
TW3
<253
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-03
Percent Solids
TW3
7.92
%
SM2540B-2011
01/28/2021
MD
210128-12-04
Fecal Coliforms
TW4
<249
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-04
Percent Solids
TW4
8.03
%
SM2540B-2011
01/28/2021
MD
210128-12-05
Fecal Coliforms
TW5
<245
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-05
Percent Solids
TW5
8.16
%
SM2540B-2011
01/28/2021
MD
210128-12-06
Fecal Coliforms
TW6
<253
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-06
Percent Solids
TW6
7.92
%
SM2540B-2011
01/28/2021
MD
210128-12-07
Fecal Coliforms
TW7
<242
MPN/g
SM92210E-2006
01/28/2021
MD
210128-12-07
Percent Solids
TW7
8.25
%
SM2540B-2011
01/28/2021
MD
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210128-12-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-06 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 210128-12-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 06/01/2021
Reported: 06/03/2021
For: Tyson Wilkesboro
Comments: GEOMETRIC MEAN: <230 MPN/g
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210601-15-01
Fecal Coliforms
TW1
<240
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-01
Percent Solids
TW1
8.32
%
SM2540B-2011
06/01/2021
MD
210601-15-02
Fecal Coliforms
TW2
<224
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-02
Percent Solids
TW2
8.92
%
SM2540B-2011
06/01/2021
MD
210601-15-03
Fecal Coliforms
TW3
<243
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-03
Percent Solids
TW3
8.24
%
SM2540B-2011
06/01/2021
MD
210601-15-04
Fecal Coliforms
TW4
<213
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-04
Percent Solids
TW4
9.39
%
SM2540B-2011
06/01/2021
MD
210601-15-05
Fecal Coliforms
TW5
<216
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-05
Percent Solids
TW5
9.27
%
SM2540B-2011
06/01/2021
MD
210601-15-06
Fecal Coliforms
TW6
<235
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-06
Percent Solids
TW6
8.51
%
SM2540B-2011
06/01/2021
MD
210601-15-07
Fecal Coliforms
TW7
<239
MPN/g
SM92210E-2006
06/01/2021
MD
210601-15-07
Percent Solids
TW7
8.36
%
SM2540B-2011
06/01/2021
MD
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210601-15-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-06 Temp on Arrival: 3.0
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210601-15-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 08/26/2021
Reported: 08/28/2021
For: TYSON WILKESBORO
Comments:
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210826-17-01
Fecal Coliforms
W1
<426
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-01
Percent Solids
W1
4.7
%
SM2540B-2011
08/26/2021
MD
210826-17-02
Fecal Coliforms
W2
<342
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-02
Percent Solids
W2
5.84
%
SM2540B-2011
08/26/2021
MD
210826-17-03
Fecal Coliforms
W3
<347
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-03
Percent Solids
W3
5.76
%
SM2540B-2011
08/26/2021
MD
210826-17-04
Fecal Coliforms
W4
<407
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-04
Percent Solids
W4
4.91
%
SM2540B-2011
08/26/2021
MD
210826-17-05
Fecal Coliforms
W5
<394
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-05
Percent Solids
W5
5.08
%
SM2540B-2011
08/26/2021
MD
210826-17-06
Fecal Coliforms
W6
<352
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-06
Percent Solids
W6
5.68
%
SM2540B-2011
08/26/2021
MD
210826-17-07
Fecal Coliforms
W7
<344
MPN/g
SM92210E-2006
08/26/2021
MD
210826-17-07
Percent Solids
W7
5.82
%
SM2540B-2011
08/26/2021
MD
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 210826-17-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-06 Temp on Arrival: 2.3
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 210826-17-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 4

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 11/30/2021
Reported: 12/01 /2021
For: Tyson Wilkesboro
Comments:
4 6TATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
211130-19-01
Fecal Coliforms
TW1
<364
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-01
Percent Solids
TW1
5.49
%
SM2540B-2011
11/30/2021
MD
211130-19-02
Fecal Coliforms
TW2
<359
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-02
Percent Solids
TW2
5.57
%
SM2540B-2011
11/30/2021
MD
211130-19-03
Fecal Coliforms
TW3
<368
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-03
Percent Solids
TW3
5.44
%
SM2540B-2011
11/30/2021
MD
211130-19-04
Fecal Coliforms
TW4
<363
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-04
Percent Solids
TW4
5.51
%
SM2540B-2011
11/30/2021
MD
211130-19-05
Fecal Coliforms
TW5
<366
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-05
Percent Solids
TW5
5.47
%
SM2540B-2011
11/30/2021
MD
211130-19-06
Fecal Coliforms
TW6
<370
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-06
Percent Solids
TW6
5.41
%
SM2540B-2011
11/30/2021
MD
211130-19-07
Fecal Coliforms
TW7
<362
MPN/g
SM92210E-2006
11/30/2021
MD
211130-19-07
Percent Solids
TW7
5.52
%
SM2540B-2011
11/30/2021
MD
Respectfully submitted,
X�- � �'?- J, ;'�
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 211130-19-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-06 Temp on Arrival: 3.0
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 211130-19-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

5
Annual Pathogen & Vector Attraction Reduction Form for NCAC 2T Rules
(FORM PVRF 2T)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: AdvancePierre Foods - Claremont, NC
NPDES Number: N/A
Monitoring Period: From l/l/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
1 Alt B (Alk Treatment)[]
Alt. C (Prior Testing)[]
AIt.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
1 Thermophilic ❑
Beta Ray 111
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
203
241
263
MPN/g
0
1/YR
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) r❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: AdvancePierre Foods - Claremont, NC
NPDES Number: N/A
Monitoring Period: From l/l/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
1 Alt B (Alk Treatment)[]
Alt. C (Prior Testing)[]
AIt.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
1 Thermophilic ❑
Beta Ray 111
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
719
1399
2703
MPN/g
0
1/YR
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) r❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: Mathis-1 (Storage Facility)
Monitoring Period: From l/l/2021 To
NPDES Number: N/A
12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
AIt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
4255
4348
4444
MPN/g
0
1/YR
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) r❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: Mathis-1 (Storage Facility)
Monitoring Period: From l/l/2021 To
NPDES Number: N/A
12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
AIt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
7353
7900
8065
MPN/g
0
1/YR
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) r❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: RVAF (Tyson) - Harmony, NC
Monitoring Period: From l/l/2021 To
NPDES Number: N/A
3/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
AIt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
22722
46959
83333
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle: Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: RVAF (Tyson) - Harmony, NC
Monitoring Period: From 4/1/2021 To
NPDES Number: N/A
6/30/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
AIt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
12407
22503
45946
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) r❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: RVAF (Tyson) - Harmony, NC
Monitoring Period: From 7/1/2021 To
NPDES Number: N/A
9/30/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
AIt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
9346
31173
74866
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) r❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc WQ Permit Number: WQ0038087
WWTP Name: RVAF (Tyson) - Harmony, NC
Monitoring Period: From 10/1/2021 To
NPDES Number: N/A
12/31 /2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
AIt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
3509
3601
3745
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) r❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc. WQ Permit Number: WQ0038087
WWTP Name: Tyson - Wilkesboro, NC
Monitoring Period: From l/l/2021 To
NPDES Number: N/A
3/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
AIt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
233
246
253
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc. WQ Permit Number: WQ0038087
WWTP Name: Tyson - Wilkesboro, NC
Monitoring Period: From 4/1/2021 To
NPDES Number: N/A
6/30/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
AIt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
213
230
243
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) r❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc. WQ Permit Number: WQ0038087
WWTP Name: Tyson - Wilkesboro, NC
Monitoring Period: From 7/1/2021 To
NPDES Number: N/A
9/30/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
AIt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
342
372
426
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) r❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Terra Renewal Services, Inc. WQ Permit Number: WQ0038087
WWTP Name: Tyson - Wilkesboro, NC
Monitoring Period: From 10/1/2021 To
NPDES Number: N/A
12/31 /2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
AIt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 01
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Q
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
.... ..... .... .... .... .... ..... ....
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g
Number o
Excee-
dences
Frequency
of Analysis
Sample
Type
na ytica
Tech -
ni ue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
359
365
370
MPN/g
0
1/Qtr
Grab
92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1AIt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) r❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
r❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
David C. Coyle; Enviro. Manager
Preparer Name and Title (type or print)
2/28/2022
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

6
Soil Test Reports
(for fields applied in 2021)

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7
COMPLIMENTARY DATA:
Executive Summary
Fecal Analysis Summary
Poultry Litter Analysis Summary
Poultry Litter Analyses

Executive Summary
Annual Report -2021
Permit No. WQ0038087
Permittee: Terra Renewal Services, Inc
Dry Tons ADDlied Der Source
TERRA
renewal
Field ID
Permitted
Acres
Utilized
Acres
Application
Period
(Months)
Crop
RYE
PAN
(lb/ac)
Adjusted
2021PAN
(lb/ac)
PAN Applied
Residuals
(lb/ac)
PAN Applied
Supplement*
(lb/ac)
Total PAN
Applied
(lb/ac)
AdvPierre
Claremont
(DT/Field)
RVAF
Harmony
(DT/Field)
Tyson
Wilkesboro
(DT/Field)
Annual Dry
Tons Applied
(DT/Field)
NC-WK-CH-01
21.8
21.8
Apr -Jun
Corn Silage
179
145
127
127
28.8
10.8
39.6
NC-WK-CH-03
41.6
41.6
Apr -Jun
Corn Silage
285
220
149
31.2
180
2.9
54.0
31.2
88.1
NC-WK-CH-04
35.8
35.8
Apr -Jun
Corn Silage
270
220
189
31.2
220
1.4
80.2
16.8
98.4
NC-WK-MF-09
13.2
13.2
Aug -Sep
Sm Grains
98
98
97
97
11.2
13.1
24.3
NC-WK-MF-10
19.6
19.6
Sep
Sm Grains
98
98
87
87
16.0
16.0
32.0
NC-WK-MF-11
22.5
22.5
Sep
Sm Grains
80
80
78
78
19.2
13.1
32.3
NC-WK-MF-13
33.8
33.8
Dec
Corn Silage
214
201
139
139
28.5
67.6
96.1
NC-WK-MF-14
23.4
23.4
Dec
Corn Silage
174
164
36
36
4.8
12.5
17.3
NC-WK-MF-15
13.8
13.8
Dec
Corn Silage
174
167
118
118
10.5
22.5
33.0
NC-WK-MF-23
59.2
59.2
Aug -Sep
Sm Grains
98
98
97
97
54.5
53.7
108.2
NC-WK-MRF-03
18.9
18.9
Dec -Jan
Corn Silage
179
143
142
142
28.9
23.3
52.2
NC-WK-MRF-05
25.3
25.3
Dec -Jan
Corn Silage
212
199
154
31.2
185
1.6
38.2
34.1
73.9
NC-WK-MRF-06
24.9
24.9
Dec -Jan
Corn Silage
212
173
98
31.2
129
32.0
20.2
52.2
NC-WK-MRF-12
25.1
25.1
Dec -Jan
Corn Silage
219
187
139
31.2
170
3.0
57.1
19.7
79.8
NC-WK-MRF-20
52.3
52.3
Jul -Aug
Nov -Dec
Corn Silage
Corn Silage
237
224
178
224
73
224
73
2.4
160.8
128.0
291.2
NC-WK-MRF-21
27.8
27.8
Jun -Aug
Corn Silage
237
220
220
220
1.4
52.7
50.7
104.8
NC-WK-RJ-02
57.8
57.8
Mar
Corn Silage
237
230
20
20
1.6
13.2
4.7
19.5
NC-WK-RJ-05
45.1
45.1
Feb -Mar
Oct -Nov
Corn Silage
Corn Silage
237
221
207
123
68
31.2
31.2
155
99
1.6
72.5
113.5
187.6
NC-WK-RJ-07
24.6
24.6
Mar
Corn Silage
214
214
101
31.2
132
17.1
26.4
43.5
NC-YK-YF-01
13.5
13.5
Oct
Sm Grains
98
98
73
73
0.9
10.5
7.5
18.9
NC-YK-YF-03
22.3
22.3
Sep -Oct
Sm Grains
120
120
107
107
24.0
20.6
44.6
NC-YK-YF-04
23.3
23.2
Oct
Sm Grains
120
120
24
24
3.8
7.5
11.3
NC-WK-YK-YF-05
51.5
51.5
Oct
Sm Grains
120
120
51
51
23.8
26.3
50.1
TOTALS: 697 17 842 740 111599

Fecal Analysis Summary - 2021
Permit No: WQ0038087
Permittee: Terra Renewal Services, Inc
TERRA
renewal
Facility: AdvancePierre Foods -Claremont
Result (MPN/gram)
Sample Date 1 2 3 4 5 6 7 Geo Mean
2/4/2021 208 258 263 203 258 257 248 241
6/10/2021 1,732 1,639 719 1,183 2,041 2,703 787 1,399
Facility: RVAF
(Tyson) - Harmony
Result
(MPN/gram)
Sample Date
1
2
3
4
5
6
7
Geo Mean
3/30/2021
36,145
61,915
50,000
31,915
83,333
74,468
22,722
46,959
6/1/2021
12,407
23,936
34,575
45,946
21,108
21,390
12,887
22,303
9/2/2021
40,498
74,866
52,147
37,333
9,346
21,164
24,499
31,173
12/20/2021
3,617
3,534
3,610
3,527
3,745
3,509
3,670
3,601
Facility: Tyson - Wilkesboro
Result (MPN/gram)
Sample Date
1
2
3 4
5
6
7
Geo Mean
1/28/2021
233
248
253 249
245
253
242
246
6/1/2021
240
224
243 213
216
235
239
230
8/26/2021
426
342
347 407
394
352
344
372
11/30/2021
364
359
368 363
366
370
362
365
Result (MPN/gram)
Sample Date 1 2 3 4 5 6 7 Geo Mean
8/26/2021 4,444 4,444 4,348 4,348 4,255 4,348 4,255 4,348
10/12/2021 7,968 7,353 8,065 7,874 8,000 8,065 8,000 7,900

Poultry Litter Analysis Summary - 2021
Source: ASJ Mathis Farms
Sample ID
Total N
(ppm)
Dry Matter
N
PAN
(lb/ton)
MF-1
38,000
62.8
23.9
MF-2
22,600
33.9
7.7
MF-3
26,800
47.1
12.6
MF-4
32,300
28.7
9.3
MF-5
37,600
78.8
29.6
MF-6
23,400
35.5
8.3
MF-7
31,600
19.4
6.1
MF-8
22,800
63.3
14.4
MF-9
24,800
40.7
10.1
MF-10
35,600
84.3
30.0
MF-11
20,400
26.4
5.4
MF-12
29,500
68.1
20.1
MF-13
83,900
25.8
21.6
MF-14
22,600
73.5
16.6
MF-15
35,400
31.3
11.1
Average: 32,487 48.0 15.6
lb/ton = ((%DM/100)*2000 lb/ton) * (Total N ppm/1,000,000) * (MR)
MR = Mineralization Rate = 50% (expressed as decimal: 0.5)

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