WQ0010689_Residual Annual Report 2021_20220225

Initial Review
Reviewer
EADS\ndthornburg
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0010689
ApplicantlPermittee Baxter Healthcare Corporation
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office Asheville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Corey Carpentier
Email Address*
[e-mail]
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
828-756-6636
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Perm it Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number: *
WQ0010689
Has Current Existing permit number
Applicant/Permittee Address*
65 Pitts Station Road, Marion, NC 28752
Facility Name*
Baxter Healthcare Corporation Class A Residuals Program
Please provide comments/notes on your current submittal below.
2021 Annual Report
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
WO0010689, Baxter Healthcare, Annual Report.pdf 6.76MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Cc3✓e� Car`�e��e✓
Submission Date 2/25/2022

Baxter
2/23/2022
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
RE: 2021 Annual Ash Report
Permit No. WQ0010689
Wood Boiler — North Cove, NC
Enclosed is the 2021 Annual Ash Distribution Report using the forms provided by NCDEQ
DWQ. Included in this report is the following information:
- Class A Annual DMSDF and Supplemental Information
- Annual Residual Sampling Summary Form and Form-B
- Ash Distribution Landowner Utilization Agreements
- Lab Sheets
There were no permit deviations during the 2021 Reporting Year.
If you have any questions or require additional information, please contact myself at 828-756-
6636.
Sincerely,
Corey Carpentier
Attachments: Annual Ash Report (3 copies)
Baxter Healthcare Corporation
PO Box 1390, Marion, NC 28752
T 828.756.4151

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DENR FORM RSSF - B (12/2006)

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to *FA Al 40b (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed Iaboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): //''t Date:
00._}
Ash Recipient's Address: F s 73 )41$ vv . --
Intended Use of Ash: •a' J J1J PRD aNl eztj�
Expected Qty/Yr: l'eLc2-13
of L. / 410
Baxter Representative Signature:
Page 2 of 3
Updated: January 2020

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to C/ L .S ( .4"/Ve ,k/
the aforementioned ash is prohibited except in accordance with the instructions on this sheet. (Recipient}. Application of
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify,
harmless from and against any and all liability, damage, loss, cost, expense (including aorneys'afec fnd ees), ld a,[demter andd, suit,eaction,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient):
Date: 2/
Ash Recipient's Mailing Address: es 5e
Intended Use of Ash and Crop Type: ✓ /ii-z &-
Expected Qty/Yr: Z 1
20
Baxter Representative Signature:
.der/0/1/
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to n
the aforementioned ash is prohibited except in accordance with the Instructi sno this on sheet. (Recipient). Application of
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall riot be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify,
harmless from and against any and all liability, damage, loss, cost, expense (including a o eys'and fee ),cllaim, de and,tsu tetaconn,,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient):
Ash Recipient's Mailing Address:
Intended Use of Ash and Crop Type:
Expected Qty/Yr: 0A/
Baxter Representative Signature:
Date: • -2 6 .
573e 7 Ij /; / Sk91 // // )764e✓
and:
<t7 l
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided toQ
the aforementioned ash is prohibited except in accordance with the instructions on this sl et (Recipient). Application of
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to Iand application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed Iaboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify,
Health, Co
harmless from and against any and all liability, damage, loss, cost, expense (including aorneys'and fee ), cla n,hold�ter demand, suiiit,eact onn,,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient):
Ash Recipient's Mailing Address:
Intended Use of Ash and Crop Type:
Expected Qty/Yr:
Baxter Representative Signature:
Date: g'��'/
05 2 / /,.-.4)/4/z 2 07S-2
tof
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to �,�/b
the aforementioned ash is prohibited except in accordance with the i structions on this sheet. (Recipient). Application of
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage.: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
Iiming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689 and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the infonnation sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify,
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys'af e s),claim,�demand, ter suHealtcit eac on,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transporta ionhhandling
or other use of the ash.
Signed (Ash Recipient):
Ash Recipient's Mailing Address:
,/
Intended Use of Ash and Crop Type: /; ,
ii-
Expected Qty/Yr: f ? ./J
and: ,�6.)
Baxter Representative Signature:
Page 2 of 3

Baxter Healthcare, Corp,
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 12/31/21), Ilaxter Copy
Baxter Healthcare, Corp,, is the generator of the ash provided to iiverq /1410 " k.re.S(Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructidns on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Recipients should soil test fields BOTH prior to and within 6 months of land application of ash. If the soil test reflects a high
Sodium Adsorption Rate following land application, please notify us for assistance.
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash. T� 1Ji� ��1
Signed (Ash Recipient):`,/ it 1 I4/L. L`p Date: D 1
7 9'q 5 G/ S j g e Nr I Afv,✓Ja .tr r % " ,7
Ash Recipient's Address:
Intended Use of Ash and Crop Type:
`S©J I En /i £ n c e , :�.
Expected Qty/Yr: & , 5 CAnz-
Baxter Representative Signature'.JI P4
Acres of Land: ] Q , er€
Updated: May 2021
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
�__N---- l// J`-
Baxter Healthcare, Corp., is the generator of the ash provided to �/.��%� S G� ,�" S �
the aforementioned ash is prohibited except in accordance with the instructions on this sheet, (Recipient). Application of
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage.: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
•
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application • Application of ash cake residuals shall not occur within 100 feet of a public or private water supply perennial waterbodies, and wetlands.
Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
• Copies of this Utilization Agreement, Ash Permit No. WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o Hale application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient tlrs de, vo r)evr0 Date: 3_7- 202 f
Ash Recipient's Mailing Address: 6 2 <"'G
Intended Use of Ash and Crop Type:
Expected Qty/Yr: / z)•
•5
Baxter Representative Signature:
Acres of Land:
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Co ��
rp., is the generator of the ash provided to , j?7 ���c) Az (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
•
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application • Application of ash cake residuals shall not occur within 100 feet of a public or private water supply perennial waterbodies, and wetlands.
Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the Land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): 552-fita4 ( � _
Ash Recipient's Mailing Address: _
Intended Use of Ash and Crop Type:
Expected Qty/Yr: ?Oo )L,,,i5
Baxter Representative Signature:
Date:
7z- zeW
ied /1/e2 7J2
Wald: d: Jr
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 12/31/21), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to 1 "(�%' � (c Ii M) (Recipient). Application of
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Recipients should soil test fields BOTH prior to and within 6 months of land application of ash. If the soil test reflects a high
Sodium Adsorption Rate following land application, please notify us for assistance.
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter I-Iealthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
/Signed (Ash Recipient):Y/6,2,; �''�°���� v � ` � �� Date:
Ash Recipient's Address: i. q j l3 6' oos c (07(k. m e r r l a y) \ /v ( 2 K 752
2
Intended Use of Ash and Crop Type: b t 1 1Y1 r LC -AN V Div ' i4 Q I
Expected Qty/Yr: 7s T w s AArrs of -hand: `jam
Baxter Representative Signature:
Updated: May 2021
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
_ I�1
Baxter Healthcare, Corp., is the generator of the ash provided to k E cL' L.--� ,.(,r
the aforementioned ash is prohibited except in accordance with the inistructions on this sheet L { (Recipient). Application of
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof, Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): jati4je 62,./aze..."(1
Ash Recipient's Address: /0 (jree�-
Intended Use of Ash: /%y
Expected Qty/Yr: ) t
Baxter Representative Signature:
Date: '� "/,„2
fi .e 49 e '97
La %q
age 2 of 3
Updated: January 2020

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to A 't y Ltd �c,
the aforementioned ash is prohibited except in accordance with the instructions or/ this sheet. (Recipient). Application of
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No. WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the Iand application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient):
Ash Recipient's Address:
Intended Use of Ash:
Expected Qty/Yr: 3 00
Baxter Representative Signature:
Date: T — f - )
— / i5 u) 7,M/ /fir 6;04 t e e A g 77 7
and.
Page 2 of 3
Updated: January 2020
1f 0

Baxter Healthcare, Corp,
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 3/30/2025), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to . V &46I /s
the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
(Recipient). Application of
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and hazards to public
health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Spill control
provisions must be available during transportation or land application activities. Any spill occurring while ash is in transport or on the
application fields is the responsibility of the transporter.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. The
use of wetting agents, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be
controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to meet the
liming requirements of the crops being grown on the land).
• Residual ash cake shall not be stockpiled for more than 60 days prior to land application
• Application of ash cake residuals shall not occur within 100 feet of a public or private water supply
• Application of ash cake residuals shall not occur within 25 feet of surface waters such as intermittent and perennial streams,
perennial waterbodies, and wetlands.
• Copies of this Utilization Agreement, Ash Permit No.WQ0010689, and the Operation and Maintenance Plan shall be maintained
at the land application site when bulk residuals are being applied.
• Ash shall not be placed within one foot of the seasonal high water table or bedrock.
• Ash shall not be applied to any site under the following conditions:
o Flooded, frozen, or snow-covered or other condition causing runoff
o During precipitation events or within 24-hrs following a 0.5" rainfall
o If the land application site does not have established vegetative cover crop
o If the application causes any nuisance conditions to adjacent property, natural resources, or wildlife
A summary of the ash chemical analyses is located on page 3 of the information sheet. Detailed laboratory results are available upon
request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp
will have no responsibility and shall not be held liable by Recipient or any third party for any spill, misuse, misapplication or other
mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as
an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,
judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling
or other use of the ash.
Signed (Ash Recipient): 1) 41 9141LCiP. Date: — 1 0 1
Ash Recipient's Address: p v ` 3 C a�r f t C �' U T Sip rc-4 c
Intended Use of Ash:
o 1 E
Expected Qty/Yr: 306 ` / p w'
r A es Land: o
Baxter Representative Signature:
Page 2 of 3
Updated: January 2020
rt

#=CL#
February 24, 2022
LIMS USE: FR - RICKY STYLES
LIMS OBJECT ID: 92516882
92516882
Project:
Pace Project No.:
RE:
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
Baxter Biomass 1/13
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on January 15, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
Revised Report: Report revised to include PAN calculation to final report
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 23
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 23
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92516882001 SP1132021A EPA 6010D 18 PASI-ASH1
EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-ASOO
EPA 7471B 1 PASI-ASOO
SW-846 1 PASI-CKDF
EPA 9045D 1 PASI-ASMK
None 1 PASI-AEWS
EPA 350.1 Rev 2.0 1993 Mod.1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
EPA 365.1 Rev 2.0 1993 1 PASI-AMFO
92516882002 SP1132021B EPA 6010D 18 PASI-ASH1
EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-ASOO
EPA 7471B 1 PASI-ASOO
SW-846 1 PASI-CKDF
EPA 9045D 1 PASI-ASMK
None 1 PASI-AEWS
EPA 350.1 Rev 2.0 1993 Mod.1 PASI-AKDF1
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
EPA 365.1 Rev 2.0 1993 1 PASI-AMFO
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Sample:SP1132021A Lab ID:92516882001 Collected:01/13/21 10:30 Received:01/15/21 11:07 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Aluminum 8860 mg/kg 01/19/21 15:41 7429-90-501/18/21 15:2319.0 1
Arsenic ND mg/kg 01/19/21 15:41 7440-38-201/18/21 15:234.7 1
Barium 1060 mg/kg 01/19/21 15:41 7440-39-301/18/21 15:231.9 1
Cadmium 2.1 mg/kg 01/19/21 15:41 7440-43-901/18/21 15:230.19 1
Calcium 74900 mg/kg 01/20/21 18:06 7440-70-201/18/21 15:2347510
Chromium 16.7 mg/kg 01/19/21 15:41 7440-47-301/18/21 15:230.95 1
Copper 48.8 mg/kg 01/19/21 15:41 7440-50-801/18/21 15:239.5 1
Iron 7110 mg/kg 01/19/21 15:41 7439-89-601/18/21 15:2395.0 1
Lead 15.4 mg/kg 01/19/21 15:41 7439-92-101/18/21 15:231.9 1
Magnesium 8890 mg/kg 01/19/21 15:41 7439-95-401/18/21 15:2319.0 1
Manganese 2480 mg/kg 01/20/21 18:06 7439-96-501/18/21 15:239.5 10
Molybdenum ND mg/kg 01/19/21 15:41 7439-98-701/18/21 15:239.5 1
Nickel 13.8 mg/kg 01/19/21 15:41 7440-02-001/18/21 15:230.95 1
Potassium 11300 mg/kg 01/19/21 15:41 7440-09-701/18/21 15:239501
Selenium ND mg/kg 01/19/21 15:41 7782-49-201/18/21 15:231.9 1
Silver 0.97 mg/kg 01/19/21 15:41 7440-22-401/18/21 15:230.95 1
Sodium 7650 mg/kg 01/19/21 15:41 7440-23-501/18/21 15:239501
Zinc 159 mg/kg 01/19/21 15:41 7440-66-601/18/21 15:231.9 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 01/20/21 14:52 Initial pH: 5.39; Final pH: 2
Pace Analytical Services - Asheville
6010 MET ICP, TCLP
Arsenic ND mg/L 01/22/21 17:24 7440-38-201/22/21 02:010.050 1
Barium 3.5 mg/L 01/22/21 17:24 7440-39-301/22/21 02:010.25 1
Cadmium ND mg/L 01/22/21 17:24 7440-43-901/22/21 02:010.0050 1
Chromium ND mg/L 01/22/21 17:24 7440-47-301/22/21 02:010.050 1
Lead ND mg/L 01/22/21 17:24 7439-92-101/22/21 02:010.025 1
Selenium ND mg/L 01/22/21 17:24 7782-49-201/22/21 02:010.10 1
Silver ND mg/L 01/22/21 17:24 7440-22-401/22/21 02:010.025 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 01/20/21 14:52 Initial pH: 5.39; Final pH: 2
Pace Analytical Services - Asheville
7470 Mercury, TCLP
Mercury ND mg/L 01/22/21 13:04 7439-97-601/22/21 10:130.00020 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury ND mg/kg 01/20/21 15:02 7439-97-601/19/21 16:130.0051 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 56.8 %01/18/21 13:290.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Sample:SP1132021A Lab ID:92516882001 Collected:01/13/21 10:30 Received:01/15/21 11:07 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
9045 pH Soil
pH at 25 Degrees C 9.3 Std. Units 01/25/21 14:24 H30.10 1
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
Plant Available Nitrogen 1000 mg/kg 02/22/22 16:16 N21
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/kg 01/21/21 11:41 7664-41-701/20/21 13:1023.2 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 3350 mg/kg 01/22/21 01:57 7727-37-901/21/21 16:191161
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3 ND mg/kg 01/16/21 02:42 H301/15/21 23:159.1 1
Nitrogen, Nitrate ND mg/kg 01/16/21 02:42 14797-55-801/15/21 23:159.1 1
Nitrogen, Nitrite ND mg/kg 01/16/21 02:42 14797-65-0 H301/15/21 23:159.1 1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
365.1 Phosphorus, Total
Phosphorus 1670 mg/kg 01/22/21 07:38 7723-14-001/21/21 17:3010550
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Sample:SP1132021B Lab ID:92516882002 Collected:01/13/21 10:30 Received:01/15/21 11:07 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Aluminum 8630 mg/kg 01/19/21 15:44 7429-90-501/18/21 15:2316.6 1
Arsenic ND mg/kg 01/19/21 15:44 7440-38-201/18/21 15:234.1 1
Barium 1400 mg/kg 01/19/21 15:44 7440-39-301/18/21 15:231.7 1
Cadmium 3.7 mg/kg 01/19/21 15:44 7440-43-901/18/21 15:230.17 1
Calcium 103000 mg/kg 01/20/21 18:09 7440-70-201/18/21 15:2341410
Chromium 17.8 mg/kg 01/19/21 15:44 7440-47-301/18/21 15:230.83 1
Copper 50.8 mg/kg 01/19/21 15:44 7440-50-801/18/21 15:238.3 1
Iron 7220 mg/kg 01/19/21 15:44 7439-89-601/18/21 15:2382.9 1
Lead 24.2 mg/kg 01/19/21 15:44 7439-92-101/18/21 15:231.7 1
Magnesium 10100 mg/kg 01/19/21 15:44 7439-95-401/18/21 15:2316.6 1
Manganese 2520 mg/kg 01/20/21 18:09 7439-96-501/18/21 15:238.3 10
Molybdenum ND mg/kg 01/19/21 15:44 7439-98-701/18/21 15:238.3 1
Nickel 14.2 mg/kg 01/19/21 15:44 7440-02-001/18/21 15:230.83 1
Potassium 10400 mg/kg 01/19/21 15:44 7440-09-701/18/21 15:238291
Selenium ND mg/kg 01/19/21 15:44 7782-49-201/18/21 15:231.7 1
Silver 0.99 mg/kg 01/19/21 15:44 7440-22-401/18/21 15:230.83 1
Sodium 7490 mg/kg 01/19/21 15:44 7440-23-501/18/21 15:238291
Zinc 236 mg/kg 01/19/21 15:44 7440-66-601/18/21 15:231.7 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 01/20/21 14:52 Initial pH: 5.02; Final pH: 2
Pace Analytical Services - Asheville
6010 MET ICP, TCLP
Arsenic ND mg/L 01/22/21 17:28 7440-38-201/22/21 02:010.050 1
Barium 1.1 mg/L 01/22/21 17:28 7440-39-301/22/21 02:010.25 1
Cadmium ND mg/L 01/22/21 17:28 7440-43-901/22/21 02:010.0050 1
Chromium ND mg/L 01/22/21 17:28 7440-47-301/22/21 02:010.050 1
Lead ND mg/L 01/22/21 17:28 7439-92-101/22/21 02:010.025 1
Selenium ND mg/L 01/22/21 17:28 7782-49-201/22/21 02:010.10 1
Silver ND mg/L 01/22/21 17:28 7440-22-401/22/21 02:010.025 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 01/20/21 14:52 Initial pH: 5.02; Final pH: 2
Pace Analytical Services - Asheville
7470 Mercury, TCLP
Mercury ND mg/L 01/22/21 13:07 7439-97-601/22/21 10:130.00020 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.046 mg/kg 01/20/21 15:04 7439-97-601/19/21 16:130.013 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 56.3 %01/18/21 13:290.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 23
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Sample:SP1132021B Lab ID:92516882002 Collected:01/13/21 10:30 Received:01/15/21 11:07 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
9045 pH Soil
pH at 25 Degrees C 9.4 Std. Units 01/25/21 14:25 H30.10 1
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
Plant Available Nitrogen 1140 mg/kg 02/22/22 16:16 N21
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/kg 01/21/21 11:43 7664-41-701/20/21 13:1022.4 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 3800 mg/kg 01/22/21 01:59 7727-37-901/21/21 16:191141
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3 ND mg/kg 01/16/21 02:43 H301/15/21 23:159.0 1
Nitrogen, Nitrate ND mg/kg 01/16/21 02:43 14797-55-801/15/21 23:159.0 1
Nitrogen, Nitrite ND mg/kg 01/16/21 02:43 14797-65-0 H301/15/21 23:159.0 1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
365.1 Phosphorus, Total
Phosphorus 1750 mg/kg 01/22/21 07:39 7723-14-001/21/21 17:3010450
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
594565
EPA 7470A
EPA 7470A
7470 Mercury TCLP
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92516882001, 92516882002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3134496
Associated Lab Samples:92516882001, 92516882002
Matrix:Water
Analyzed
Mercury mg/L ND 0.00020 01/22/21 12:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3137049LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/L 0.00230.0025 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3137050MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92516316002
3137051
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/L 0.0025 96 75-12593 40.0025ND 0.0024 0.0024
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
593504
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92516882001, 92516882002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3132113
Associated Lab Samples:92516882001, 92516882002
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0060 01/20/21 14:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3132114LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0880.083 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3132115MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92516801002
3132116
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg R10.035 79 75-125117 260.0350.017 0.044 0.058
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
593458
EPA 3050B
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92516882001, 92516882002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3131897
Associated Lab Samples:92516882001, 92516882002
Matrix:Solid
Analyzed
Aluminum mg/kg ND 10.0 01/19/21 14:50
Arsenic mg/kg ND 2.5 01/19/21 14:50
Barium mg/kg ND 1.0 01/19/21 14:50
Cadmium mg/kg ND 0.10 01/19/21 14:50
Calcium mg/kg ND 25.0 01/19/21 14:50
Chromium mg/kg ND 0.50 01/19/21 14:50
Copper mg/kg ND 5.0 01/19/21 14:50
Iron mg/kg ND 50.0 01/19/21 14:50
Lead mg/kg ND 1.0 01/19/21 14:50
Magnesium mg/kg ND 10.0 01/19/21 14:50
Manganese mg/kg ND 0.50 01/19/21 14:50
Molybdenum mg/kg ND 5.0 01/19/21 14:50
Nickel mg/kg ND 0.50 01/19/21 14:50
Potassium mg/kg ND 500 01/19/21 14:50
Selenium mg/kg ND 1.0 01/19/21 14:50
Silver mg/kg ND 0.50 01/19/21 14:50
Sodium mg/kg ND 500 01/19/21 14:50
Zinc mg/kg ND 1.0 01/19/21 14:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3131898LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum mg/kg 484500 97 80-120
Arsenic mg/kg 45.650 91 80-120
Barium mg/kg 48.850 98 80-120
Cadmium mg/kg 46.350 93 80-120
Calcium mg/kg 481500 96 80-120
Chromium mg/kg 47.750 95 80-120
Copper mg/kg 49.050 98 80-120
Iron mg/kg 483500 97 80-120
Lead mg/kg 47.450 95 80-120
Magnesium mg/kg 470500 94 80-120
Manganese mg/kg 47.250 94 80-120
Molybdenum mg/kg 50.750 101 80-120
Nickel mg/kg 48.350 97 80-120
Potassium mg/kg ND500 98 80-120
Selenium mg/kg 43.450 87 80-120
Silver mg/kg 23.525 94 80-120
Sodium mg/kg 489J500 98 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3131898LABORATORY CONTROL SAMPLE:
LCSSpike
Zinc mg/kg 46.150 92 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3131899MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92516889001
3131900
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Aluminum mg/kg M146036175-125234 16439257042303590
Arsenic mg/kg 46 89 75-12588 543.92.1J 43.0 40.8
Barium mg/kg 46 110 75-12594 1443.917.9 68.2 59.2
Cadmium mg/kg 46 91 75-12589 643.90.36 42.1 39.6
Calcium mg/kg M1,R1460-927 75-125-1420 364391070064304470
Chromium mg/kg 46 104 75-12595 1243.95.8 53.7 47.5
Copper mg/kg 46 101 75-12597 743.99.5 56.0 52.0
Iron mg/kg M146016375-125180 1439333040804120
Lead mg/kg 46 104 75-12584 1243.950.2 98.3 87.3
Magnesium mg/kg 460 120 75-125105 10439418971879
Manganese mg/kg 46 106 75-12594 943.939.4 88.2 80.9
Molybdenum mg/kg 46 97 75-12596 643.9ND 44.9 42.5
Nickel mg/kg 46 94 75-12592 643.92.8 45.9 43.1
Potassium mg/kg 460 117 75-125103 13439ND699613
Selenium mg/kg 46 84 75-12582 643.90.64J 39.2 36.9
Silver mg/kg 22.9 92 75-12591 522ND21.2 20.1
Sodium mg/kg 460 89 75-12581 11439ND518464
Zinc mg/kg 46 115 75-12593 943.990.5 143 131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
594564
EPA 3010A
EPA 6010D
6010 MET TCLP
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92516882001, 92516882002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3134496
Associated Lab Samples:92516882001, 92516882002
Matrix:Water
Analyzed
Arsenic mg/L ND 0.050 01/22/21 16:39
Barium mg/L ND 0.25 01/22/21 16:39
Cadmium mg/L ND 0.0050 01/22/21 16:39
Chromium mg/L ND 0.050 01/22/21 16:39
Lead mg/L ND 0.025 01/22/21 16:39
Selenium mg/L ND 0.10 01/22/21 16:39
Silver mg/L ND 0.025 01/22/21 16:39
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3137046LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 2.52.5 99 80-120
Barium mg/L 2.42.5 97 80-120
Cadmium mg/L 2.52.5 98 80-120
Chromium mg/L 2.42.5 98 80-120
Lead mg/L 2.42.5 95 80-120
Selenium mg/L 2.52.5 100 80-120
Silver mg/L 1.11.2 89 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3137047MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92516316001
3137048
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/L 2.5 98 75-12596 22.5ND 2.4 2.4
Barium mg/L 2.5 97 75-12598 12.5ND 2.5 2.6
Cadmium mg/L 2.5 96 75-12597 12.5ND 2.4 2.4
Chromium mg/L 2.5 97 75-12597 02.5ND 2.4 2.4
Lead mg/L 2.5 95 75-12597 12.50.38 2.8 2.8
Selenium mg/L 2.5 99 75-12599 12.5ND 2.5 2.5
Silver mg/L 1.2 88 75-12588 11.2ND 1.1 1.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
593444
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92516882001, 92516882002
Parameter Units
Dup
Result QualifiersRPDResult
92516825001
3131812SAMPLE DUPLICATE:
Percent Moisture %17.2 416.6
Parameter Units
Dup
Result QualifiersRPDResult
92516882002
3131813SAMPLE DUPLICATE:
Percent Moisture %56.6 056.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
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Page 13 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
594893
EPA 9045D
EPA 9045D
9045 pH
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92516882001, 92516882002
Parameter Units
Dup
Result QualifiersRPDResult
92516715001
3138528SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 7.2 H317.1
Parameter Units
Dup
Result QualifiersRPDResult
92517810001
3138529SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 6.8 H316.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
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[phone]
Page 14 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
594057
EPA 350.1 Rev 2.0 1993 Mod.
EPA 350.1 Rev 2.0 1993 Mod.
350.1 Ammonia
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92516882001, 92516882002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3134328
Associated Lab Samples:92516882001, 92516882002
Matrix:Solid
Analyzed
Nitrogen, Ammonia mg/kg ND 10.0 01/21/21 11:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3134329LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/kg 491490 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3134330MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92516975006
3134331
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/kg 1130 100 90-11098 1113065917901770
REPORT OF LABORATORY ANALYSIS
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Page 15 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
594418
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92516882001, 92516882002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3136267
Associated Lab Samples:92516882001, 92516882002
Matrix:Solid
Analyzed
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 01/22/21 01:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3136268LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/kg 9.310 93 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3136269MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92516975006
3136270
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/kg M122008690-11086 0220060325002500
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3136271MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92516975008
3136272
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/kg M1,R117107990-11028 59179052018701020
REPORT OF LABORATORY ANALYSIS
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Page 16 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
593209
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92516882001, 92516882002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3131032
Associated Lab Samples:92516882001, 92516882002
Matrix:Solid
Analyzed
Nitrogen, Nitrate mg/kg ND 4.0 01/16/21 02:40
Nitrogen, Nitrite mg/kg ND 4.0 01/16/21 02:40
Nitrogen, NO2 plus NO3 mg/kg ND 4.0 01/16/21 02:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3131033LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/kg 15.715 105 90-110
Nitrogen, Nitrite mg/kg 10.210 102 90-110
Nitrogen, NO2 plus NO3 mg/kg 25.925 103 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3131034MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92516781001
3131035
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/kg 1010 108 90-110106 21020ND10901070
Nitrogen, Nitrite mg/kg 676 101 90-110100 0676ND677680
Nitrogen, NO2 plus NO3 mg/kg 1690 101 90-11099 11690ND17701750
REPORT OF LABORATORY ANALYSIS
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Page 17 of 23
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
594340
EPA 365.1 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
365.1 Phosphorus, Total
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92516882001, 92516882002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3135734
Associated Lab Samples:92516882001, 92516882002
Matrix:Solid
Analyzed
Phosphorus mg/kg ND 0.96 01/22/21 05:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3135735LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus mg/kg 53.250 106 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3135736MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92517207001
3135737
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phosphorus mg/kg M1,R194.6 271 90-110101 6162160416222
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3135738MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92517207002
3135739
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phosphorus mg/kg M177.3 125 90-110133 787.2173 270 289
REPORT OF LABORATORY ANALYSIS
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Page 18 of 23
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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Page 19 of 23
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92516882
Baxter Biomass 1/13
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92516882001 593458 593541SP1132021AEPA 3050B EPA 6010D
92516882002 593458 593541SP1132021BEPA 3050B EPA 6010D
92516882001 594564 594609SP1132021AEPA 3010A EPA 6010D
92516882002 594564 594609SP1132021BEPA 3010A EPA 6010D
92516882001 594565 594694SP1132021AEPA 7470A EPA 7470A
92516882002 594565 594694SP1132021BEPA 7470A EPA 7470A
92516882001 593504 593813SP1132021AEPA 7471B EPA 7471B
92516882002 593504 593813SP1132021BEPA 7471B EPA 7471B
92516882001 593444SP1132021ASW-846
92516882002 593444SP1132021BSW-846
92516882001 594893SP1132021AEPA 9045D
92516882002 594893SP1132021BEPA 9045D
92516882001 680116SP1132021ANone
92516882002 680116SP1132021BNone
92516882001 594057 594085SP1132021AEPA 350.1 Rev 2.0 1993
Mod.
EPA 350.1 Rev 2.0 1993
Mod.
92516882002 594057 594085SP1132021BEPA 350.1 Rev 2.0 1993
Mod.
EPA 350.1 Rev 2.0 1993
Mod.
92516882001 594418 594582SP1132021AEPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92516882002 594418 594582SP1132021BEPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92516882001 593209 593222SP1132021AEPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993
92516882002 593209 593222SP1132021BEPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993
92516882001 594340 594592SP1132021AEPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993
92516882002 594340 594592SP1132021BEPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/24/2022 09:16 AM
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Page 20 of 23
Page 21 of 23
Page 22 of 23
Page 23 of 23
#=CL#
March 31, 2021
LIMS USE: FR - RICKY STYLES
LIMS OBJECT ID: 92527130
92527130
Project:
Pace Project No.:
RE:
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
North Pond 3/9
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on March 10, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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Page 1 of 33
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92527130
North Pond 3/9
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Page 2 of 33
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92527130
North Pond 3/9
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92527130001 NP3092021A EPA 6010D 13 PASI-ASH1
EPA 7471B 1 PASI-ASOO
SM 2540G-2011 1 PASI-CKDF
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
Calculated 1 PANCCE
EPA 9045D 1 PASI-ASMK
None 1 PASI-ADMN
EPA 350.1 Rev 2.0 1993 Mod.1 PASI-ANAL
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ACJL
EPA 365.1 Rev 2.0 1993 1 PASI-AMDW
92527130002 NP3092021B EPA 6010D 13 PASI-ASH1
EPA 7471B 1 PASI-ASOO
SM 2540G-2011 1 PASI-CKDF
SW-846 1 PASI-CKDF
SM 2540G 1 PANKDW
Calculated 1 PANCCE
EPA 9045D 1 PASI-ASMK
None 1 PASI-ADMN
EPA 350.1 Rev 2.0 1993 Mod.1 PASI-ANAL
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-ACJL
EPA 365.1 Rev 2.0 1993 1 PASI-AMDW
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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Page 3 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92527130
North Pond 3/9
Sample:NP3092021A Lab ID:92527130001 Collected:03/09/21 14:00 Received:03/10/21 15:36 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Aluminum 6740 mg/kg 03/17/21 03:35 7429-90-5 M1,R103/15/21 14:2119.4 1
Arsenic ND mg/kg 03/17/21 03:35 7440-38-203/15/21 14:214.8 1
Cadmium 2.0 mg/kg 03/17/21 03:35 7440-43-903/15/21 14:210.19 1
Calcium 60500 mg/kg 03/18/21 05:26 7440-70-2 M1,R103/15/21 14:212425
Copper 47.5 mg/kg 03/17/21 03:35 7440-50-803/15/21 14:219.7 1
Lead 13.8 mg/kg 03/17/21 03:35 7439-92-103/15/21 14:211.9 1
Magnesium 8220 mg/kg 03/18/21 06:40 7439-95-4 M1,R103/15/21 14:2119.4 1
Molybdenum ND mg/kg 03/17/21 03:35 7439-98-703/15/21 14:219.7 1
Nickel 12.0 mg/kg 03/17/21 03:35 7440-02-003/15/21 14:210.97 1
Potassium 16400 mg/kg 03/18/21 06:40 7440-09-7 M103/15/21 14:219691
Selenium ND mg/kg 03/17/21 03:35 7782-49-203/15/21 14:211.9 1
Sodium 14400 mg/kg 03/18/21 06:40 7440-23-5 M103/15/21 14:219691
Zinc 150 mg/kg 03/17/21 03:35 7440-66-6 M103/15/21 14:211.9 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury ND mg/kg 03/18/21 11:40 7439-97-603/17/21 18:360.0097 1
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
2540G Total Percent Solids
Total Solids 42.3 %03/12/21 14:120.10 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 57.7 %03/12/21 14:05 N20.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 44.2 %03/17/21 14:0203/17/21 13:501
Analytical Method: Calculated Preparation Method: Calc
Pace National - Mt. Juliet
Calculated Results
Sodium Adsorption Ratio 73.2 03/18/21 10:00 SAR03/18/21 10:001
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
9045 pH Soil
pH at 25 Degrees C 8.8 Std. Units 03/22/21 15:42 H30.10 1
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
Plant Available Nitrogen 1760 mg/kg 03/22/21 14:01 N21
REPORT OF LABORATORY ANALYSIS
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Page 4 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92527130
North Pond 3/9
Sample:NP3092021A Lab ID:92527130001 Collected:03/09/21 14:00 Received:03/10/21 15:36 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/kg 03/22/21 11:53 7664-41-703/22/21 07:3322.7 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 5860 mg/kg 03/16/21 05:15 7727-37-903/15/21 18:415915
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3 ND mg/kg 03/12/21 20:46 H1,H203/12/21 19:169.3 1
Nitrogen, Nitrate ND mg/kg 03/12/21 20:46 14797-55-803/12/21 19:169.3 1
Nitrogen, Nitrite ND mg/kg 03/12/21 20:46 14797-65-0 H1,H203/12/21 19:169.3 1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
365.1 Phosphorus, Total
Phosphorus 2340 mg/kg 03/16/21 20:15 7723-14-003/15/21 19:4043.0 20
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 5 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92527130
North Pond 3/9
Sample:NP3092021B Lab ID:92527130002 Collected:03/09/21 14:00 Received:03/10/21 15:36 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Aluminum 6370 mg/kg 03/17/21 03:55 7429-90-503/15/21 14:2118.0 1
Arsenic ND mg/kg 03/17/21 03:55 7440-38-203/15/21 14:214.5 1
Cadmium 1.8 mg/kg 03/17/21 03:55 7440-43-903/15/21 14:210.18 1
Calcium 56400 mg/kg 03/18/21 21:38 7440-70-203/15/21 14:212255
Copper 44.9 mg/kg 03/17/21 03:55 7440-50-803/15/21 14:219.0 1
Lead 12.9 mg/kg 03/17/21 03:55 7439-92-103/15/21 14:211.8 1
Magnesium 8110 mg/kg 03/18/21 21:38 7439-95-403/15/21 14:2190.1 5
Molybdenum ND mg/kg 03/17/21 03:55 7439-98-703/15/21 14:219.0 1
Nickel 11.1 mg/kg 03/17/21 03:55 7440-02-003/15/21 14:210.90 1
Potassium 14700 mg/kg 03/18/21 21:38 7440-09-703/15/21 14:2145005
Selenium ND mg/kg 03/17/21 03:55 7782-49-203/15/21 14:211.8 1
Sodium 12600 mg/kg 03/18/21 21:38 7440-23-503/15/21 14:2145005
Zinc 135 mg/kg 03/17/21 03:55 7440-66-603/15/21 14:211.8 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury ND mg/kg 03/18/21 11:42 7439-97-603/17/21 18:360.0088 1
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
2540G Total Percent Solids
Total Solids 42.7 %03/12/21 14:120.10 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 57.3 %03/12/21 14:05 N20.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 44.8 %03/17/21 14:0203/17/21 13:501
Analytical Method: Calculated Preparation Method: Calc
Pace National - Mt. Juliet
Calculated Results
Sodium Adsorption Ratio 76.0 03/18/21 09:28 SAR03/18/21 09:281
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
9045 pH Soil
pH at 25 Degrees C 8.8 Std. Units 03/22/21 15:44 H30.10 1
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
Plant Available Nitrogen 1620 mg/kg 03/22/21 14:01 N21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92527130
North Pond 3/9
Sample:NP3092021B Lab ID:92527130002 Collected:03/09/21 14:00 Received:03/10/21 15:36 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/kg 03/22/21 11:55 7664-41-703/22/21 07:3318.6 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 5400 mg/kg 03/16/21 05:16 7727-37-903/15/21 18:415325
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3 ND mg/kg 03/12/21 20:47 H1,H203/12/21 19:169.2 1
Nitrogen, Nitrate ND mg/kg 03/12/21 20:47 14797-55-803/12/21 19:169.2 1
Nitrogen, Nitrite ND mg/kg 03/12/21 20:47 14797-65-0 H1,H203/12/21 19:169.2 1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
365.1 Phosphorus, Total
Phosphorus 2550 mg/kg 03/16/21 20:16 7723-14-003/15/21 19:4040.4 20
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92527130
North Pond 3/9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
607355
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92527130001, 92527130002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3199760
Associated Lab Samples:92527130001, 92527130002
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0060 03/18/21 11:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3199761LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0870.083 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3199762MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92527486007
3199763
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg 0.12 95 75-12596 20.12ND 0.12 0.12
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92527130
North Pond 3/9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
606614
EPA 3050B
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92527130001, 92527130002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3196029
Associated Lab Samples:92527130001, 92527130002
Matrix:Solid
Analyzed
Aluminum mg/kg ND 10.0 03/17/21 03:28
Arsenic mg/kg ND 2.5 03/17/21 03:28
Cadmium mg/kg ND 0.10 03/17/21 03:28
Calcium mg/kg ND 25.0 03/17/21 03:28
Copper mg/kg ND 5.0 03/17/21 03:28
Lead mg/kg ND 1.0 03/17/21 03:28
Magnesium mg/kg ND 10.0 03/18/21 06:37
Molybdenum mg/kg ND 5.0 03/17/21 03:28
Nickel mg/kg ND 0.50 03/17/21 03:28
Potassium mg/kg ND 500 03/18/21 06:37
Selenium mg/kg ND 1.0 03/18/21 06:37
Sodium mg/kg ND 500 03/18/21 06:37
Zinc mg/kg ND 1.0 03/17/21 03:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3196030LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum mg/kg 484500 97 80-120
Arsenic mg/kg 42.350 85 80-120
Cadmium mg/kg 47.350 95 80-120
Calcium mg/kg 484500 97 80-120
Copper mg/kg 53.550 107 80-120
Lead mg/kg 46.450 93 80-120
Magnesium mg/kg 474500 95 80-120
Molybdenum mg/kg 50.850 102 80-120
Nickel mg/kg 50.050 100 80-120
Potassium mg/kg ND500 99 80-120
Selenium mg/kg 40.750 81 80-120
Sodium mg/kg 483J500 97 80-120
Zinc mg/kg 44.250 88 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3196031MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92527130001
3196032
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Aluminum mg/kg M1,R196920675-1252 26969674087406760
Arsenic mg/kg 96.9 82 75-12581 196.9ND 82.4 81.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92527130
North Pond 3/9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3196031MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92527130001
3196032
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cadmium mg/kg 96.9 91 75-12592 196.92.0 90.7 91.6
Calcium mg/kg M1,R196982575-125-979 29969605006850051000
Copper mg/kg 96.9 107 75-12592 1096.947.5 151 136
Lead mg/kg 96.9 84 75-12582 296.913.8 95.0 93.3
Magnesium mg/kg M1,R196923475-125-43 299698220105007800
Molybdenum mg/kg 96.9 92 75-12595 396.9ND 90.5 93.3
Nickel mg/kg 96.9 89 75-12588 296.912.0 98.6 96.8
Potassium mg/kg M196914175-125-60 12969164001780015800
Selenium mg/kg 96.9 80 75-12583 496.9ND 77.6 80.5
Sodium mg/kg M196913375-125-38 11969144001570014100
Zinc mg/kg M196.9 101 75-12556 1996.9150 248 205
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92527130
North Pond 3/9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
606319
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92527130001, 92527130002
Parameter Units
Dup
Result QualifiersRPDResult
92526726002
3194273SAMPLE DUPLICATE:
Percent Moisture %88.1 N2088.1
Parameter Units
Dup
Result QualifiersRPDResult
92527130002
3194274SAMPLE DUPLICATE:
Percent Moisture %57.7 N2157.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92527130
North Pond 3/9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1635342
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92527130001, 92527130002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3632071-1
Associated Lab Samples:92527130001, 92527130002
Matrix:Solid
Analyzed
Total Solids %0.00100 03/17/21 14:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3632071-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 99.9 85.0-115
Parameter Units
Dup
Result QualifiersRPDResult
L1326757-01
R3632071-3SAMPLE DUPLICATE:
Total Solids %90.5 1.5391.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92527130
North Pond 3/9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
608096
EPA 9045D
EPA 9045D
9045 pH
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92527130001, 92527130002
Parameter Units
Dup
Result QualifiersRPDResult
92524937003
3203537SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 12.9 E,H3012.9
Parameter Units
Dup
Result QualifiersRPDResult
92528638004
3203538SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 9.9 H309.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92527130
North Pond 3/9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
608125
EPA 350.1 Rev 2.0 1993 Mod.
EPA 350.1 Rev 2.0 1993 Mod.
350.1 Ammonia
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92527130001, 92527130002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3203618
Associated Lab Samples:92527130001, 92527130002
Matrix:Solid
Analyzed
Nitrogen, Ammonia mg/kg ND 10.0 03/22/21 11:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3203619LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/kg 503500 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3203620MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92527278001
3203621
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/kg M1,R117808190-110162 562140114025904600
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92527130
North Pond 3/9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
606620
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92527130001, 92527130002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3196071
Associated Lab Samples:92527130001, 92527130002
Matrix:Solid
Analyzed
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 03/16/21 04:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3196072LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/kg 9581000 96 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3196073MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92526324002
3196074
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/kg M1144012790-110130 41300124030602950
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92527130
North Pond 3/9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
606401
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92527130001, 92527130002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3194994
Associated Lab Samples:92527130001, 92527130002
Matrix:Solid
Analyzed
Nitrogen, Nitrate mg/kg ND 4.0 03/12/21 20:38
Nitrogen, Nitrite mg/kg ND 4.0 03/12/21 20:38
Nitrogen, NO2 plus NO3 mg/kg ND 4.0 03/12/21 20:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3194995LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/kg 15.115 101 90-110
Nitrogen, Nitrite mg/kg 9.810 98 90-110
Nitrogen, NO2 plus NO3 mg/kg 25.025 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3194996MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92527278001
3194997
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/kg 82.5 118 90-110119 082.5ND 97.9 98.3
Nitrogen, Nitrite mg/kg H3,M155.4 85 90-11086 155.4ND 49.1 49.4
Nitrogen, NO2 plus NO3 mg/kg H31389790-11098 1138ND147148
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92527130
North Pond 3/9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
606668
EPA 365.1 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
365.1 Phosphorus, Total
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92527130001, 92527130002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3196395
Associated Lab Samples:92527130001, 92527130002
Matrix:Solid
Analyzed
Phosphorus mg/kg ND 1.0 03/16/21 19:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3196396LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus mg/kg 48.749 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3196397MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92526324003
3196398
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phosphorus mg/kg M6,R177.6 395 90-110-187 3060.21310 1610 1200
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 33
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92527130
North Pond 3/9
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Analysis conducted outside the EPA method holding time.H1
Extraction or preparation conducted outside EPA method holding time.H2
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
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Huntersville, NC 28078
[phone]
Page 18 of 33
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92527130
North Pond 3/9
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92527130001 606614 606754NP3092021AEPA 3050B EPA 6010D
92527130002 606614 606754NP3092021BEPA 3050B EPA 6010D
92527130001 607355 607434NP3092021AEPA 7471B EPA 7471B
92527130002 607355 607434NP3092021BEPA 7471B EPA 7471B
92527130001 606589NP3092021ASM 2540G-2011
92527130002 606589NP3092021BSM 2540G-2011
92527130001 606319NP3092021ASW-846
92527130002 606319NP3092021BSW-846
92527130001 1635342 1635342NP3092021ASM 2540 G SM 2540G
92527130002 1635342 1635342NP3092021BSM 2540 G SM 2540G
92527130001 1634598 1634598NP3092021ACalcCalculated
92527130002 1634598 1634598NP3092021BCalcCalculated
92527130001 608096NP3092021AEPA 9045D
92527130002 608096NP3092021BEPA 9045D
92527130001 608265NP3092021ANone
92527130002 608265NP3092021BNone
92527130001 608125 608134NP3092021AEPA 350.1 Rev 2.0 1993
Mod.
EPA 350.1 Rev 2.0 1993
Mod.
92527130002 608125 608134NP3092021BEPA 350.1 Rev 2.0 1993
Mod.
EPA 350.1 Rev 2.0 1993
Mod.
92527130001 606620 606785NP3092021AEPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92527130002 606620 606785NP3092021BEPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92527130001 606401 606404NP3092021AEPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993
92527130002 606401 606404NP3092021BEPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993
92527130001 606668 606997NP3092021AEPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993
92527130002 606668 606997NP3092021BEPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/31/2021 11:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 33
Page 20 of 33
Page 21 of 33
ANALYTICAL REPORT
March 18, 2021
Pace Analytical - Asheville, NC
Sample Delivery Group:L1326756
Samples Received:03/13/2021
Project Number:92527130
Description:North Pond 3/9
Site:001
Report To:Christopher Derouen
2225 Riverside Drive
Asheville, NC 28804
Entire Report Reviewed By:
March 18, 2021
[Preliminary Report]
Christl M Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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March 18, 2021
Christl M Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
NP3092021A L1326756-01 5
NP3092021B L1326756-02 6
Qc: Quality Control Summary 7
Total Solids by Method 2540 G-2011 7
Gl: Glossary of Terms 8
Al: Accreditations & Locations 9
Sc: Sample Chain of Custody 10
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE SUMMARY
Collected by Collected date/time Received date/time
NP3092021A L1326756-01 Solid 03/09/21 14:00 03/13/21 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Calculated Results WG1634598 1 03/18/21 10:00 03/18/21 10:00 CCE Mt. Juliet, TN
Total Solids by Method 2540 G-2011 WG1635342 1 03/17/21 13:50 03/17/21 14:02 KDW Mt. Juliet, TN
Collected by Collected date/time Received date/time
NP3092021B L1326756-02 Solid 03/09/21 14:00 03/13/21 09:00
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Calculated Results WG1634598 1 03/18/21 09:28 03/18/21 09:28 CCE Mt. Juliet, TN
Total Solids by Method 2540 G-2011 WG1635342 1 03/17/21 13:50 03/17/21 14:02 KDW Mt. Juliet, TN
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Page 24 of 33
CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
Christl M Wagner
Project Manager
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Christl M Wagner
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 25 of 33
SAMPLE RESULTS - 01
L1326756
NP3092021A
Collected date/time: 03/09/21 14:00
Calculated Results
Result Qualifier Dilution Analysis Batch
Analyte date / time
Sodium Adsorption Ratio 73.2 1 03/18/2021 10:00 WG1634598
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 44.2 1 03/17/2021 14:02 WG1635342
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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SAMPLE RESULTS - 02
L1326756
NP3092021B
Collected date/time: 03/09/21 14:00
Calculated Results
Result Qualifier Dilution Analysis Batch
Analyte date / time
Sodium Adsorption Ratio 76.0 1 03/18/2021 09:28 WG1634598
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 44.8 1 03/17/2021 14:02 WG1635342
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Page 27 of 33
QUALITY CONTROL SUMMARYWG1635342
Total Solids by Method 2540 G-2011 L1326756-01,02
Method Blank (MB)
(MB) R3632071-1 03/17/21 14:02
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1326757-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1326757-01 03/17/21 14:02 • (DUP) R3632071-3 03/17/21 14:02
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 91.9 90.5 1 1.53 10
Laboratory Control Sample (LCS)
(LCS) R3632071-2 03/17/21 14:02
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 99.9 85.0-115
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Page 28 of 33
GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Page 29 of 33

Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹TN00003
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶KY90010 South Carolina 84004002
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana LA018 Texas T104704245-20-18
Maine TN00003 Texas ⁵LAB0152
Maryland 324 Utah TN000032021-11
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
1 Cp
2 Tc
3 Ss
4 Cn
5 Sr
6 Qc
7 Gl
8 Al
9 Sc
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Page 30 of 33
Page 31 of 33
Page 32 of 33
Page 33 of 33
#=CL#
July 02, 2021
LIMS USE: FR - RICKY STYLES
LIMS OBJECT ID: 92545080
92545080
Project:
Pace Project No.:
RE:
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
South Pond 6/15
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on June 17, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 20
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92545080
South Pond 6/15
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 20
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92545080
South Pond 6/15
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92545080001 SP6152021A EPA 6010D 13 PASI-ARDT, SH1
EPA 7471B 1 PASI-ASOO
SM 2540G-2011 1 PASI-CKDF
SW-846 1 PASI-CKDF
EPA 9045D 1 PASI-ASMK
None 1 PASI-AEWS
EPA 350.1 Rev 2.0 1993 Mod.1 PASI-ANGP
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
EPA 365.1 Rev 2.0 1993 1 PASI-AKDF1
92545080002 SP6152021B EPA 6010D 13 PASI-ARDT, SH1
EPA 7471B 1 PASI-ASOO
SM 2540G-2011 1 PASI-CKDF
SW-846 1 PASI-CKDF
EPA 9045D 1 PASI-ASMK
None 1 PASI-ADMN
EPA 350.1 Rev 2.0 1993 Mod.1 PASI-ANGP
EPA 351.2 Rev 2.0 1993 1 PASI-AMFO
EPA 353.2 Rev 2.0 1993 3 PASI-AMFO
EPA 365.1 Rev 2.0 1993 1 PASI-AKDF1
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545080
South Pond 6/15
Sample:SP6152021A Lab ID:92545080001 Collected:06/15/21 09:00 Received:06/17/21 12:11 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Aluminum 5870 mg/kg 06/30/21 22:57 7429-90-5 M106/29/21 15:3017.4 1
Arsenic ND mg/kg 06/30/21 22:57 7440-38-206/29/21 15:304.3 1
Cadmium 1.6 mg/kg 06/30/21 22:57 7440-43-906/29/21 15:300.17 1
Calcium 66400 mg/kg 07/01/21 19:35 7440-70-2 M106/29/21 15:3043510
Copper 35.5 mg/kg 06/30/21 22:57 7440-50-806/29/21 15:308.7 1
Lead 11.5 mg/kg 06/30/21 22:57 7439-92-106/29/21 15:301.7 1
Magnesium 7650 mg/kg 06/30/21 22:57 7439-95-4 M106/29/21 15:3017.4 1
Molybdenum ND mg/kg 06/30/21 22:57 7439-98-706/29/21 15:308.7 1
Nickel 9.6 mg/kg 06/30/21 22:57 7440-02-006/29/21 15:300.87 1
Potassium 14100 mg/kg 06/30/21 22:57 7440-09-7 M106/29/21 15:308691
Selenium ND mg/kg 06/30/21 22:57 7782-49-206/29/21 15:301.7 1
Sodium 11900 mg/kg 06/30/21 22:57 7440-23-5 M106/29/21 15:308691
Zinc 136 mg/kg 06/30/21 22:57 7440-66-606/29/21 15:301.7 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury ND mg/kg 06/23/21 18:23 7439-97-606/23/21 16:040.0044 1
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
2540G Total Percent Solids
Total Solids 47.9 %06/18/21 16:050.10 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 52.1 %06/18/21 15:58 N20.10 1
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
9045 pH Soil
pH at 25 Degrees C 9.0 Std. Units 06/28/21 16:34 H30.10 1
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
Plant Available Nitrogen 684 mg/kg 06/23/21 15:22 N21
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/kg 06/23/21 12:02 7664-41-706/23/21 08:2421.3 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 2280 mg/kg 06/23/21 06:06 7727-37-906/22/21 21:4599.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545080
South Pond 6/15
Sample:SP6152021A Lab ID:92545080001 Collected:06/15/21 09:00 Received:06/17/21 12:11 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3 ND mg/kg 06/18/21 03:00 H306/17/21 22:578.2 1
Nitrogen, Nitrate ND mg/kg 06/18/21 03:00 14797-55-806/17/21 22:578.2 1
Nitrogen, Nitrite ND mg/kg 06/18/21 03:00 14797-65-0 H306/17/21 22:578.2 1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
365.1 Phosphorus, Total
Phosphorus 2350 mg/kg 06/24/21 14:04 7723-14-006/24/21 11:2248.3 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545080
South Pond 6/15
Sample:SP6152021B Lab ID:92545080002 Collected:06/15/21 09:00 Received:06/17/21 12:11 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Aluminum 6270 mg/kg 06/30/21 23:10 7429-90-506/29/21 15:3017.3 1
Arsenic ND mg/kg 06/30/21 23:10 7440-38-206/29/21 15:304.3 1
Cadmium 1.7 mg/kg 06/30/21 23:10 7440-43-906/29/21 15:300.17 1
Calcium 67800 mg/kg 07/01/21 19:48 7440-70-206/29/21 15:3043310
Copper 38.7 mg/kg 06/30/21 23:10 7440-50-806/29/21 15:308.7 1
Lead 12.3 mg/kg 06/30/21 23:10 7439-92-106/29/21 15:301.7 1
Magnesium 7960 mg/kg 06/30/21 23:10 7439-95-406/29/21 15:3017.3 1
Molybdenum ND mg/kg 06/30/21 23:10 7439-98-706/29/21 15:308.7 1
Nickel 10.3 mg/kg 06/30/21 23:10 7440-02-006/29/21 15:300.87 1
Potassium 14400 mg/kg 06/30/21 23:10 7440-09-706/29/21 15:308661
Selenium ND mg/kg 06/30/21 23:10 7782-49-206/29/21 15:301.7 1
Sodium 12200 mg/kg 06/30/21 23:10 7440-23-506/29/21 15:308661
Zinc 144 mg/kg 06/30/21 23:10 7440-66-606/29/21 15:301.7 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury ND mg/kg 06/23/21 18:25 7439-97-606/23/21 16:040.0047 1
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
2540G Total Percent Solids
Total Solids 48.1 %06/18/21 16:050.10 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 51.9 %06/18/21 15:58 N20.10 1
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
9045 pH Soil
pH at 25 Degrees C 8.9 Std. Units 06/28/21 16:36 H30.10 1
Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen
Plant Available Nitrogen 717 mg/kg 06/30/21 11:10 N21
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
350.1 Ammonia
Nitrogen, Ammonia ND mg/kg 06/23/21 12:04 7664-41-706/23/21 08:2420.0 1
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 2390 mg/kg 06/23/21 06:07 7727-37-906/22/21 21:4599.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
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9800 Kincey Ave. Suite 100
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Page 6 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92545080
South Pond 6/15
Sample:SP6152021B Lab ID:92545080002 Collected:06/15/21 09:00 Received:06/17/21 12:11 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3 ND mg/kg 06/18/21 03:01 H306/17/21 22:578.1 1
Nitrogen, Nitrate ND mg/kg 06/18/21 03:01 14797-55-806/17/21 22:578.1 1
Nitrogen, Nitrite ND mg/kg 06/18/21 03:01 14797-65-0 H306/17/21 22:578.1 1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
365.1 Phosphorus, Total
Phosphorus 2410 mg/kg 06/24/21 14:05 7723-14-006/24/21 11:2251.0 25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 7 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545080
South Pond 6/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
629028
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92545080001, 92545080002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3305986
Associated Lab Samples:92545080001, 92545080002
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0060 06/23/21 17:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3305987LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0900.083 108 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3305988MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92545301012
3305989
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg M10.068 105 75-125138 110.0640.081 0.15 0.17
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545080
South Pond 6/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
630339
EPA 3050B
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92545080001, 92545080002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3311940
Associated Lab Samples:92545080001, 92545080002
Matrix:Solid
Analyzed
Aluminum mg/kg ND 10.0 07/01/21 19:15
Arsenic mg/kg ND 2.5 07/01/21 19:15
Cadmium mg/kg ND 0.10 07/01/21 19:15
Calcium mg/kg ND 25.0 06/30/21 22:37
Copper mg/kg ND 5.0 07/01/21 19:15
Lead mg/kg ND 1.0 07/01/21 19:15
Magnesium mg/kg ND 10.0 07/01/21 19:15
Molybdenum mg/kg ND 5.0 07/01/21 19:15
Nickel mg/kg ND 0.50 07/01/21 19:15
Potassium mg/kg ND 500 07/01/21 19:15
Selenium mg/kg ND 1.0 07/01/21 19:15
Sodium mg/kg ND 500 07/01/21 19:15
Zinc mg/kg ND 1.0 07/01/21 19:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3311941LABORATORY CONTROL SAMPLE:
LCSSpike
Aluminum mg/kg 505500 101 80-120
Arsenic mg/kg 48.250 96 80-120
Cadmium mg/kg 49.050 98 80-120
Calcium mg/kg 499500 100 80-120
Copper mg/kg 52.550 105 80-120
Lead mg/kg 49.050 98 80-120
Magnesium mg/kg 504500 101 80-120
Molybdenum mg/kg 54.350 109 80-120
Nickel mg/kg 50.450 101 80-120
Potassium mg/kg 513500 103 80-120
Selenium mg/kg 45.250 90 80-120
Sodium mg/kg 520500 104 80-120
Zinc mg/kg 47.350 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3311942MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92545080001
3311943
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Aluminum mg/kg M185619975-125131 8870587075707010
Arsenic mg/kg 85.6 89 75-12592 587ND79.1 82.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545080
South Pond 6/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3311942MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92545080001
3311943
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Cadmium mg/kg 85.6 87 75-12588 3871.6 76.3 78.4
Calcium mg/kg M185666775-125448 3870664007210070300
Copper mg/kg 85.6 97 75-12597 18735.5 118 119
Lead mg/kg 85.6 80 75-12581 38711.5 79.9 82.2
Magnesium mg/kg M185618075-125145 3870765091908910
Molybdenum mg/kg 85.6 88 75-12591 587ND76.7 80.3
Nickel mg/kg 85.6 83 75-12584 3879.6 80.5 82.6
Potassium mg/kg M185610975-125189 5870141001510015800
Selenium mg/kg 85.6 82 75-12583 287ND70.3 72.1
Sodium mg/kg M18568275-125174 6870119001260013400
Zinc mg/kg 85.6 89 75-12585 187136212210
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545080
South Pond 6/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628226
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92545080001, 92545080002
Parameter Units
Dup
Result QualifiersRPDResult
92541778004
3302492SAMPLE DUPLICATE:
Percent Moisture %15.5 N21618.2
Parameter Units
Dup
Result QualifiersRPDResult
92545080002
3302493SAMPLE DUPLICATE:
Percent Moisture %51.1 N2251.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545080
South Pond 6/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
629868
EPA 9045D
EPA 9045D
9045 pH
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92545080001, 92545080002
Parameter Units
Dup
Result QualifiersRPDResult
92545080001
3310021SAMPLE DUPLICATE:
pH at 25 Degrees C Std. Units 9.1 H319.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545080
South Pond 6/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628864
EPA 350.1 Rev 2.0 1993 Mod.
EPA 350.1 Rev 2.0 1993 Mod.
350.1 Ammonia
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92545080001, 92545080002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3305307
Associated Lab Samples:92545080001, 92545080002
Matrix:Solid
Analyzed
Nitrogen, Ammonia mg/kg ND 10.2 06/23/21 11:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3305308LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Ammonia mg/kg 511510 100 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3305309MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92544586001
3305310
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Ammonia mg/kg 25400 99 90-110100 426500ND2570026800
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545080
South Pond 6/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628680
EPA 351.2 Rev 2.0 1993
EPA 351.2 Rev 2.0 1993
351.2 TKN
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92545080001, 92545080002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3304440
Associated Lab Samples:92545080001, 92545080002
Matrix:Solid
Analyzed
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 06/23/21 05:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3304441LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Kjeldahl, Total mg/kg 9451000 95 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3304442MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92544422003
3304443
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Kjeldahl, Total mg/kg M1677010790-11083 27110651007240071000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545080
South Pond 6/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
628046
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92545080001, 92545080002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3301706
Associated Lab Samples:92545080001, 92545080002
Matrix:Solid
Analyzed
Nitrogen, Nitrate mg/kg ND 4.0 06/18/21 02:57
Nitrogen, Nitrite mg/kg ND 4.0 06/18/21 02:57
Nitrogen, NO2 plus NO3 mg/kg ND 4.0 06/18/21 02:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3301707LABORATORY CONTROL SAMPLE:
LCSSpike
Nitrogen, Nitrate mg/kg 15.315 102 90-110
Nitrogen, Nitrite mg/kg 10.010 100 90-110
Nitrogen, NO2 plus NO3 mg/kg 25.325 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3301708MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92544586001
3301709
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/kg 758 101 90-110100 0773114019001910
Nitrogen, Nitrite mg/kg M15038990-11089 1514ND450457
Nitrogen, NO2 plus NO3 mg/kg 1260 96 90-11095 01290114023502360
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3301710MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92545005007
3301711
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrogen, Nitrate mg/kg 19.4 103 90-110102 319ND20.0 19.5
Nitrogen, Nitrite mg/kg 12.8 104 90-110102 412.7ND 13.5 13.0
Nitrogen, NO2 plus NO3 mg/kg 32.2 103 90-110101 331.7ND 33.5 32.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92545080
South Pond 6/15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
629217
EPA 365.1 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
365.1 Phosphorus, Total
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92545080001, 92545080002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3306956
Associated Lab Samples:92545080001, 92545080002
Matrix:Solid
Analyzed
Phosphorus mg/kg ND 0.94 06/24/21 13:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3306957LABORATORY CONTROL SAMPLE:
LCSSpike
Phosphorus mg/kg 47.845.5 105 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3306958MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92545005009
3306959
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Phosphorus mg/kg M157.1 101 90-110120 454105163170
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
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Huntersville, NC 28078
[phone]
Page 16 of 20
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92545080
South Pond 6/15
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 17 of 20
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92545080
South Pond 6/15
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92545080001 630339 630483SP6152021AEPA 3050B EPA 6010D
92545080002 630339 630483SP6152021BEPA 3050B EPA 6010D
92545080001 629028 629121SP6152021AEPA 7471B EPA 7471B
92545080002 629028 629121SP6152021BEPA 7471B EPA 7471B
92545080001 628638SP6152021ASM 2540G-2011
92545080002 628638SP6152021BSM 2540G-2011
92545080001 628226SP6152021ASW-846
92545080002 628226SP6152021BSW-846
92545080001 629868SP6152021AEPA 9045D
92545080002 629868SP6152021BEPA 9045D
92545080001 629092SP6152021ANone
92545080002 630590SP6152021BNone
92545080001 628864 628917SP6152021AEPA 350.1 Rev 2.0 1993
Mod.
EPA 350.1 Rev 2.0 1993
Mod.
92545080002 628864 628917SP6152021BEPA 350.1 Rev 2.0 1993
Mod.
EPA 350.1 Rev 2.0 1993
Mod.
92545080001 628680 628860SP6152021AEPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92545080002 628680 628860SP6152021BEPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993
92545080001 628046 628049SP6152021AEPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993
92545080002 628046 628049SP6152021BEPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993
92545080001 629217 629334SP6152021AEPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993
92545080002 629217 629334SP6152021BEPA 365.1 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/02/2021 06:50 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 20
Page 19 of 20
Page 20 of 20