WQ0037135_2021 Residual Annual Report_20220227

Initial Review
Reviewer
EADS\ndthornburg
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0037135
ApplicantlPermittee U.S. Biosolids, Inc.
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Zach Key
Email Address*
[e-mail]
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3367776909
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Perm it Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number: *
WQ0037135
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 146 Ronda, NC 28670
Facility Name*
U.S. Biosolids Class B Residuals Program
Please provide comments/notes on your current submittal below.
2021 Land Application Annual Report for US Biosolids, Inc. Permit WQ0037135
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2021 Annual Report -US Biosolids Class B.pdf 3.91MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature ;L4
Submission Date 2/27/2022

U.S. Biosolids, Inc.
Class B Permit
2021 Annual Report
Land Anslic , �up
&A' , 9* ,
lugiumvkl�v I MIX #M

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0037105
County:
Wilkes
Year: 2021
Facility Name (as shown on permit):
Land Application Operator:
US Biosolids, Inc.
US Biosolids. Inc.
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes C7 No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Annlientinn Summnrv-
Total number ofapplication fields in the ermit: 49
Total number of fields utilized for land application during the year: 16
Total amount of dry tons applied during the year for all application sites:1 181.88
Total number of acres utilizes for land application during the year.1 512.91
Part B - Annual Com iance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 21 Yes LJ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
I ) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 1 1 1 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources,
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Lach Key, President US Biosolids, Inc.
Permittee Name and Title (type or print)
si
re of Pretarer*
Date
Sature of Permittee Date
4
-
Signoire of Land Applier
;)-.I
Date
(if different from Permittee) (if efferent From Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26) DENR FORM ACF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc. Total Dry Tons Applied (Annual):
WQ0037135 Cation Exchange Capacity (non 503 only):
William Poerter Owner: William Porter Predominant Soil Series:
29.35
Acres Permitted: 29.35 Site #: NC-WK-BP Field #:
136.10
FeB2-Fairview
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use make, I%. Solids use Raw Percent #):
Sample or.
C 0111-
posite
Date
1...
4/28!21
2
3..i
a'
S
„6 ,
7 °
8
9
10
11
12 '
% Solids
5.4
Arsenic
9.26
Cadmium
1.85
Copper
369
Chromium
57.4
Lead
35
Mercury
L I I
Molyb-
denum
6.07
Nickel
23.5
Selenium
9.26
Zinc
1040
Total
Phos-
horus
14900
Annual Heavv Metal Field Loadings (Calculated in Ibs/acre):
Total
?._?
2 j
3
4
5
6
L7 i
8
9'
10
11
12
DT/Ac./
o
App.
Event
4.64
14
Arsenic
0.086
1 0.000
0.000
0,000
1 0,000
0,000
1 0.000
0.000
0.000
0.000
1 0.000
0.000
1 0.086
Cadmium
0.017
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.017
Copper
3.422
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.422
Chromium
0,532
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.532
Lead
0.325
0.000
1 0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.325
Mercury
0.010
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.010
Molyb-
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.056
denum
Nickel
0.218
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.218
Selenium
0.086
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0,000
0.086
Zinc
9.645
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0,000
0.000
0.000
9.645
Total
Phos-
138.183
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
138,183
horus
..t cernty, under penalty of taw, tnat this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
-10-a-V -
Signat e of Land Applier
�- ? s-,)•; )-
Date --
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US E3iosolids, Inc.
WQ0037135
W i I liarn Poerter Owner:
13.36 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
William Porter Predominant Soil Series:
13.36 Site #: NC-WK-BP Field #:
73.29
FeB2-Fairview
3
Residual Analysis Data (Heavy Metals and Total Phosnhorus use mt31ke. `Yo Solids use Raw Percent #):
Sample or-,
Com-
posite
Date
4/28/21
2
3
4j
5
6
7
B
9
10!
11
12',
% Solids
5.4
Arsenic
926
Cadmium
1.85
Copper
369
Chromium
57.4
Lead
35
Mercury
1.11
Molyb-
denum
6.07
Nickel
23.5
Selenium
9.26
Zinc
1040
Total
Phos-
horus
14900
Annual Heavy Metal Nleld Loadings (C:alculated in lbs/acre):
Total
1
2
31
41
5
6',
7
8
9
10
11
12',
DTIAc.I
_
T
o
App.
Event
5.49
Arsenic
0.102
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.102
Cadmium
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Copper
4.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.049
Chromium
0.630
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.630
Lead
0.384
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.384
Mercury
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Molyb-
0.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
denum
Nickel
0.258
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.258
Selenium
0.102
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.102
Zinc
11.411
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.411
'total
Phos-
163.483
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
163.483
horus
"i ceruty, under penahty oh taw, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Sign ure of d Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
US Biosolids, Inc.
WQ0037135
Operator: Dennis Key Owner:
Acres Used: 6.36 Acres Permitted:
Total Dry Tons Applied (Annual): 24.67
Cation Exchange Capacity (non 503 only):
Dennis Key Predominant Soil Series:
6.36 Site #; NC-WK-DK Field #:
PbB2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
3/11/21
21
3
4,
5
6''
7
8;
9..
10;
11
12'
%Solids
2.46
Arsenic
20
Cadmium
4
Copper
174
Chromium
14.6
Lead
12
Mercury
0.612
Molyb-
denum
10
Nickel
10
Selenium
20
Zinc
223
Total
Phos-
horus
13500
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
Total
1_
2'
3j
4
5
6
L71
8
9
10
11
121
App.
m
Event
3.88
y
Arsenic
0.155
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.155
Cadmium
0.031
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.031
Copper
1.350
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.350
Chromium
0.113
0.000
0.000
0.000
0.000
0A00
0.000
0.000
0.000
0.000
0.000
0.000
0.113
Lead 1
0.093
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.093
Mercury
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
denum
0.078
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.078
Nickel
0.078
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.078
Selenium 1
0.155
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.155
Zinc
1.730
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.730
Total
Phos-
104.733
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
104.733
horus
"t certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signat e of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
WQ0037135
Lee Walker Owner:
14.05 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Lee Walker Predominant Soil Series:
14.05 Site #: NC-WK-LW Field #:
6.00
FeB2-Fairview
1
Residual Analysis Data (Heavv Metals and Total Phosphorus use mg/kg. % Solids use Raw Pereent M-
Sample or
Com-
posite
Date
_.1
3/ 1 1121
2 I
3
R .
5.
_
6 I
7,
8 _
v 9 I
10
11
12
% Solids
2.46
Arsenic
20
Cadmium
4
Copper
174
Chromium
14.6
Lead
12
Mercury
0.612
Molyb-
denum
10
Nickel
10
Selenium
20
Zinc
223
Total
Phos-
horus
13500
Annual rieavv tvtetal rlela uoaptnLys tl_alcu[ated In thslacrel:
Total
_1.
2
3
4;
5
61
7;
8
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11',
12',
0
App.
m
Event
0.43
y
Arsenic
0.017
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0,000
1 0.000
0.000
0.000
1 0.017
Cadmium
0.003
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
0.149
0.000
0,000
0.000
0.000
0.000
0.000
Q.000
0.000
0.000
0.000
0.000
0.149
Chromium
0.012
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0,012
Lead
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.010
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
denum
0.009
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0,000
0.009
Nickel
0.009 i
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.009
Selenium
0,017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.017
Zinc
0.190
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.190
-total
Phos-
11.529
0.000
0.000
0,000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
11.529
horus
a Utrt1iy, uuterr Penalty of law, inat tnls aocument was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
a• Il-YA33..
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
31.55
FeB2-Fairview
2
Residual Analysis Data (Heavv Metals and Tntnl 1Phncnharnc imp mry/U" 04 c.,ii.1 ., u ,... Q .. _L L._
US Biosolids, Inc. Total Dry Tons Applied (Annual):
WQ0037135 Cation Exchange Capacity (non 503 only):
1,ee Walker Owner: Lee Walker Predominant Soil Series:
8.16 Acres Permitted: 8.16 Site #: NC-WK-1..W Field #:
Sample or.1_;
2F
_..,
3 4
5',
6'
7;
8'
9
10i
91
121 .
Com-
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Gate
3/11/21
4/28/21
Solids
2.46
5.4
Arsenic
20
9.26
Cadmium
4
1.85
Copper
174
369
Chromium
14.6
57.4
Lead
12
35
Mercury
0.612
1.11
Molyb-
10
6.07
denum
Nickel
10
23.5
Selenium
20
9.26
Zinc
223
1040
Total
Phos-
13500
14900
horus
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Total
1
2i
3 4
5i
61
L7j
8,_1
9'
10
11
12
DT/Ac./
c
App.
sa
Event
0.82
3.05
Arsenic
0.033
0.056
0.000 0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.089
Cadmium
0.007
0.011
0.000 0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Copper
0.0
2.
0.000 0...
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0.000
0.000
0.000
0.000
0.000
0.000
2.534
Chromium
4
0.24
0.350 50
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.374
Lead
0.020
0.213
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.233
Mercury
0.001
0.007
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
denumMolyb
denum
0.016
0.037
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
Nickel
0.016
0.143
0.000 0.000
0.000
0.000
0.00o
o.000
0.000
0.000
0.000
0.000
0.160
Selenium
0.033
0.056
0.000 0.000
0.000
0.000
0-000
0.000
0.000
0.000
0.000
0.000
0.089
Zinc
0.364
6.342
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.706
Total
Phos- 22.059 90.860 0.000 0.000
0.000
0.000 0.000
o.0o0 0.000
0.000
0.000
0.000
112,919
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated
the
information submitted.
I am aware that there are significant penalties for submitting false information,
including the possibility of fines
and
imprisonment for knowing violations".
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual): 46.67
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Lee Walker Owner: Lee Walker Predominant Soil Series: FeK-Fairview
Acres Used: 17.7 Acres Permitted: 17.7 Site #: NC-WK-LW Field #: 3
rcesiauaAnalysts uata
(Heavy
Metals and Total Phosphorus use mg/kg, %o Solids use
Raw Percent #):
Sample or 1_ 2 F
._
3
4. 5 6
Com-
posite
Date 3/ 11/2
% Solids
2.46
Arsenic
1 20
Cadmiurnj
4
Copper
174
Chromium
14.6
Lead
12
Mercury
0.612
Molyb-
denum
10
Nickel
10
Selenium
20
"Zinc
223
Total
Phos-
13500
horus
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Heavy
Metal Field Loadings
(Calculated in Ibs/acre):
Total
1
21
3_I
4
5;
61
78
9
10 :
t 1 J
12
.r' DTIAc
_
App.
Event
2.64
Arsenic
0.105
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.105
Cadmium
0,021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Copper
0.918
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0. 000
0.000 1
0.918
Chromium
0.077
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000 1
0.077
Lead
0.063
0.000
0.000 1
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Mercury
0.003
0.000
0.000 10.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
denum
0.053
0,000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
Nickel
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0,000
0.000
0.053
Selenium
0.105
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.105
"Zinc
1,176
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.176
Total
Phos-
71.1991
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
71.199
horus
-- --- ,--.____1 . -_.., ...w.., 1'.c�,a.cu U11 ve my u,reclwn UrSuperVlslon In accoruance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier pate
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to he submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual): 15.82
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Charles Killian Owner: Charles Killian Predominant Soil Series: CeB2
Acres Used: 4.3 Acres Permitted: 4.3 Site #: NC-GA-Mli-2 Field #: 4
Residual Analvsis Data (Heavy Metals and Tatnl Phaenhnr,.c ...o .....n ,. oi_ C I:A _. n_--. n_____ ­,
Sample or
z..
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11
12
Com-
posite
Date
4/13/21
%Solids
4.49
Arsenic
11.1
Cadmium
2.22
Copper
311
Chromium
71.8
Lead
26.9
Mercury
0.867
Molyb-
5.56
denum
Nickel
19.4
Selenium
11.1
Zinc
1580
Total
Phos-
23800
horus
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■7___- _ *r_
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Total
�_
21
3 a
5
6'
7I
18.
9
10
11
12
DTIAc.!
-
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0
Event
3.68
Arsenic
0.082
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0M82
Cadmium
0.016
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Copper
2.288
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.288
Chromium
0.528
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.528
Lead
0.198
1 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.198
Mercury
0.006
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Molybdenurn
enum
0.041
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.041
Nickel
0.143
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.00a
0.000
0.143
Selenium
0.082
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.082
Zinc
11.626
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.626
Total
Phos-
175.120
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
175.120
horus
frl .. ..t:r 1
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--•„-••---• r'. •••..• .•.... 1 a..aq aui� ui1culncllt waN preparell unuer my ulrectlon or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signat e of Land Applier Datc
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
WQ0037135
Charles Killian Owner:
24.6 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Charles Killian Predominant Soil Series:
24.6 Site #: NC-GA-M11-2 Field #:
42.61
CeB2
5
Residual Analysis Data (Heavy Metals and Total Phosnhorus use mp/kg. %, Solids use Raw Pereent #1-
Sample or
Com-
posite
Date
?
4/ 13/21
2 1
31
4'
5
6;
7 1
.......
8 i
9
10
11
__.
12
% Solids
4.49
Arsenic
11.1
Cadmium
2.22
Copper
311
Chromium
71.8
Lead
26.9
Mercury
0.867
Molyb-
denum
5.56
Nickel
19.4
Selenium
11.1
Zinc
1580
Total
Phos-
L_pkqrus
23800
Annual Heavy lvletai rlew LoadtnEs (t_alculated in lbs/acre):
Total
_3_
_?
3_
4
5
6
7
&
9
10
11
12;
DT/Ac./
_...
c
App.
Event
1.73
Arsenic 1
0.038
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.038
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
1.077
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.077
Chromium
0.249
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.249
Lead
0.093
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.093
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
denum
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Nickel
0.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Selenium
0.038
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.038
Zinc
5.473
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 5.473
Total
Phos-
82.443
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
82.443
horus
i certlly, unuer penalty of law, tnat tnis a cument was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signal re of Lard Applier
a-A-a42.1
Date
DENR FORM MFLSF (12/2006)

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ANNUAL, METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc.
WQ0037135
Norman McDaniel Owner:
6.2 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Norman McDaniel Predominant Soil Series:
6.2 Site #: NC-R13-NM Field #:
12.97
PbB2
I
Residual Analysis Data fHeavv Metals and Total Phosnhorus use mg/Itg.'% Snlidc tise Raw Pereont #l-
Sample or
Com-
posite
Date
1'
._.__
2/24,121
2
3
_
4i
_.�
5
6
7
8i V
_.�
v.
9
_
10 i
�...
11
12
% Solids
14
Arsenic
3.57
Cadmium
1.51
Copper
260
Chromium
42.1
Lead
65.4
Mercury
2.77
Molyb-
denum
Nickel
13.5
Selenium
8.64
Zinc
1050
Total
Phos-
horus
17600
ivnnuat tieavv tvietat meta Loaatnes (l.:alculatecl to lbs/acrel:
Total
L3r
4s
5
6
7:
8
9'
10
11
12,
D l /Ac.l
o
App.
w
Event
2.09
Arsenic
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
1.088
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.088
Chromium
0.176
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.176
Lead
0.274
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.274
Mercury
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
denur
denum
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Nickel
0.056
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.056
Selenium
0.036
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Zinc
4.393
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.393
Total
Phos-
73.638
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
73.638
horus
'■1,7, U11 V. t,c,.aay U� yaw, Uiat cub uucutnettt was prepareu unaer my Qirectton or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signatu of Land Appl er
Date
DENR FORM MFLSF (1212006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility blame:
Permit #:
Operator:
Acres Used:
US Biosolids, Inc. Total Dry Tons Applied (Annual):
WQ0037135 Cation Exchange Capacity (non 503 only):
Norman McDaniel Owner: Norman McDaniel Predominant Soil Series:
4.2 Acres Permitted: 4.2 Site #: NC-RIJ-NM Field #:
9.08
PaC2
2
Residual Analvsis Data (Heavv Metals and Total Phosphorus use molke- %, 4nlidv. imo Raw PPrrPnt lil•
Sample or
Com-
posite
Date
I I_
2/24/21
I 2.1
3
4
5
--6`':
-
7;
-
8 v
V9
101
11
12
%Solids
14
Arsenic
3.57
Cadmium
1.51
Copper
260
Chromiurrq
42.1
Lead
65.4
Mercury
2.77
Molyb-
denum
6.31
Nickel
13.5
Selenium
8.64
Zinc
1050
Total
Phos-
horus
17600
A11HUai 11CHVV ivleial rieiQ Loauiniis (L-aicuiateti in ins/acre$:
Total
1j
2#
L3,
4'
5'
6i
7
8
9
10a
11
12':
DT/Ac.i�
-
0
App.
a:
Event
2.16
Arsenic
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
1.124
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.124
Chromium
0.182
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.182
Lead
0.283
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.283
Mercury
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Molyb-
denum
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Nickel
0.058
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Selenium
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Zinc
4.540
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
4.540
Total
Phos-
76.102
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
76.102
horus
■ GCE' , UERICI pril'aEty U" law, luau finis uocument was prepares unuer my uirection or supervision In accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of nd Applier
a-2�S )°a1
Date
DENR FORM MFLSF (1212006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosoiids, Inc. Total Dry Tons Applied (Annual): 16.86
Permit #; WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Forest Calton Owner: Forest Calton Predominant Soil Series: PbB2
Acres Used: 5.5 Acres Permitted: 5.5 Site #: NC-RU-FC Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosnhorus use mo/ko- IV.. Cnlidr nP.P Raw Pvrrnnt ltl•
Sample or
Com-
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Date
i..
2/24/21
2:
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�'
S
.6 i
7,
S.i
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11
12
__....
% Solids
14
Arsenic
3.57
Cadmium
1.51
Copper
260
Chromium
42.1
Lead
65A
Mercury
2.77
Molyb-
denum
6.31
Nickel
13.5
Selenium
8.64
Zinc
1050
Total
Phos-
horus
17600
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Total
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5
6',
7
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10
11
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3.07
Arsenic
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Cadmium
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
1.594
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.594
Chromium
0.258
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.258
Lead
0.401
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
j 0A01
Mercury
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Molyb-
denum
0.039
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.039
Nickel
0.083
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.083
Selenium
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
Zinc
6.439
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
6.439
Total
Phos-
107.923
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
107.923
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with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of lines and
imprisonment for knowing violations".
SignatU. PofLand App 'er
Date
DENR FORM MFLSF (12/2006)

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ANNUAL. METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US 8iosolids, Inc. Total Dry Tons Applied (Annual): 20.75
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Forest Calton Owner: Forest Calton Predominant Soil Series: Pb132
Acres Used: 8.6 Acres Permitted: 8.6 Site #: NC-RU-FC Field #: 3
Residual Analysis Data (Heavv Metals and Total Phosphorus use mg/kg- "/, SnGrlc me,- Raw Pi rrpnf Rl-
Sample or._�_
Com-
posite
Date
2/24/21
2
3i
4
5',
6'
7
8,
9..
10
11
12:
% Solids
14
Arsenic
3.57
Cadmium
1.51
Copper
260
Chromium
42,1
Lead
65A
Mercury
2.77
Molyb-
denum
6.31
Nickel
13.5
Selenium
8.64
Zinc
1050
Total
Phos-
horus
17600
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Total
�j
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3
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7�
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9,
10,
11
12-
DT/Ac.l
_u
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2.41
Arsenic
0,017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.017
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
1.255
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.255
Chromium
0.203
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.203
Lead
0.316
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.316
Mercury
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
enu
denum
0,030
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.030
Nickel
0.065
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
Selenium
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.042
Zinc
5.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.067
Total
Phos- 84.938 0.000 0.000 0.000 0.000 0.000 0.000 0M00 0.000 0.000 0.000 0.000 84.938
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signatur of Land Appiier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual):
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Larry Bailey Owner: Larry Bailey Predominant Soil Series:
Acres Used: 8 Acres Permitted: 8 Site #: NC-RU-LB Field #:
29.83
PbB2
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, `Yo Solids use Raw Percent #):
Sample or
Com-
posite
Date
_�
2/24/21
L2j
3,
4;
5
6'
7
8'
9
_.......
10
11 L
12
_a
% Solids
14
Arsenic
3.57
Cadmium
1.51
Copper
260
Chromium
42.1
Lead
65.4
Mercury
2.77
Molyb-
denum
6.31
Nickel
1 13.5
Selenium
8.64
Zinc
1050
Total
Phos-
horus
17600
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1_
2a
3
4
6
_
6j
7
$-`
9
10.
11N
12
DT/Ac./
0
App.
m
Event
3.73
y
Arsenic
0.027
0.000
070007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.011
Copper
1.939
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1,939
Chromium
0.314
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.314
Lead
0.488
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.488
Mercury
0.021
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Molyb-
denum
0.047
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.047
Nickel
0.101
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.101
Selenium
0.064
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.064
Zinc
7.831
0,000
0-000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
7.831
Total
Phos-
131.261
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
131,261
horus
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted,
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature Land Applier pate
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids, Inc. Total Dry Tons Applied (Annual):
Permit #: WQ0037135 Cation Exchange Capacity (non 503 only):
Operator: Larry Bailey Owner: Larry Bailey Predominant Soil Series:
Acres Used: 11.7 Acres Permitted: 11.7 Site #: NC-RU-LB Field #:
10.38
PbB2
2
Residual Analvsis Data (Heavv Metals and Total Phosphorus use me/ke,'% Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
3
4 3
..,
5
6
7j
ST
9',
1D f
11
_.,
12
% Solids
14
Arsenic
3.57
Cadmium
1.51
Copper
260
Chromium
42.1
Lead
65.4
Mercury
2.77
Molyb-
denum
6.31
Nickel
13.5
Selenium
8.64
"Zinc
1050
Total
Phos-
L_phorus
17600
Annual l-leavv Metal rleld Loadings VUalculated in Ibs/acre[:
Total
1
2;
3
4
5'
6
7:
8
9',
10
11 '
12
DT/Ac.l
_...
__
_
_
_W
_.
App'
Event
0.89
Arsenic
0.006
1 0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.006
Cadmium
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
0.461
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.461
Chromium
0.075
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.075
Lead
0.116
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.116
Mercury
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.011
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
denum
Nickel
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Selenium
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Zinc
1.863
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.863
Total
Phos-
31.222
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
31.222
horus
ceruiy, unuer penalty of law, inai rnis aocument was prepares under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
'4A- 14� ._
Signat of Land Applier
7- s'J�aZ
Date
DENR FORM MFLSF (1212006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Total Dry Tons Applied (Annual): 15.56
WQ0037135 Cation Exchange Capacity (non 503 only):
Larry Bailey Owner: Larry Bailey Predominant Soil Series:
4.4 Acres Permitted: 4.4 Site #: NC-RU-LB
US Biosolids, Inc.
PbB2
Field #: 3
tcestdual Analysts Data
(Heavy
Metals and Total Phosphorus use mg/kg,
% Solids
use
Raw Percent 9):
Sample or_?
2
3
a
5
6E
_m _
7;
_.
8
9
10` I
11
12
Com-
posite
Date
2/24/21
% Solids
14
Arsenic
3.57
Cadmium
1.51
Copper
260
Chromi um
42.1
Lead
65.4
Mercury
2.77
Molyb-
denum
6.31
Nickel
13.5
Selenium
8.64
Zinc
1050
Total
Phos-
17600
horus
Annual
Heavy
Metal Field Loadings
(Calculated in lbs/acre):
Total
�._;
23
33
4
5
6
7
---
S
9'
10
11
12
DT/Ac,/
o
App.
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Event
3.54
Arsenic
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
1.839
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.839
Chromium
0.298
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.299
Lead
0.463
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.463
Mercury
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Molydenu b
denumn
0.045
0.000
0.000
0.000
0. 000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.045
Nickel 1
0.095
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.095
Selenium
0.061
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.061
Zinc
7.428
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.428
Total
Phos-
124,502
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
124,502
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1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
M
Signatu of Lan Applier
P r•l�i}�
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: US Biosolids. Inc. Total Dry Tons Applied (Annual): 20.75
Permit #: WQ0037135
Operator: Larry Bailey Owner:
Acres Used: 5.4 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Larry Bailey Predominant Soil Series:
5.4 Site #: NC-RU-LB Field #:
PbB2
4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kQ. % Solids use Raw Pereent 4)-
Sample or
Com-
posite
Date
2/24/21
2�
3
_ ..
4:
_..
5
6
7 i
8
9!
10
11
12
% Solids
14
Arsenic
3.57
Cadmium
1.51
Copper
260
Chromium
42.1
Lead
65.4
Mercury
2.77
Molyb-
denum
6.31
Nickel
13.5
Selenium
8.64
Line
1050
Total
Phos-
horus
17600
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
1'
21
3
4,I
5
61,
7;
Si
9
10
�1
12'
D'F/Ac./
c
App.
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3.84
Arsenic
0.027
0.000
0.000
0,000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0,000
0.027
Cadmium
0,012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.012
Copper
1.998
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.998
Chromium
0.323
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.323
Lead
0.503
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.503
Mercury
0.021
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Molyb-
denum
0.048
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.048
Nickel
0.104 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.104
Selenium
0.066
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
Zinc
8.068
0.000
0.000 1
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
8.068
Total
Phos-
135.238
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
135.238
horus
"i ceriny, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signattle of Lan Applier
Date
DENR FORM MFLSF (12/2006)

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of North Wilkesboro
WWTP Name: Thurmon Street WW'fP
Monitoring Period: From I/1/2021
_ WQ Permit Number:
_ NPOES Number:
To 12/31/2 021
WQ0037135
NCO020761
o.,tti,,,.o., I?nri—f— r14A X AC t»T 1 MAI - Pience indicate level achieved and alternative performed:
Class A:
Lit B (Alk Treatment) Cl Alt. C (Prior Testing)®
Alt.D (No Prior Test) L1 I
Process to Further Reduce Pathogengs C)
If applicable to alternative pefformed (Class A only) indicate "Process to Fu rther Reduce Pathogens":
Compost ©
Heat Drying 0 IHeat
Treatment DTltcrnu�philic
C
Beta Ray j
Ganutna Ray t'J
Pasteurization J
Class B:
JAIt. (1) Fecal Density 21
Alt. (2) Proccss to Significantly Reduce Pathogens C
If applicable to alternative performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization !LJ
Air Drying ElCom
posting I
Aerobic Digestion J
Anaerobic Digestior.
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um er o
F.xcee-
dgilces
I
Frecqucncy
of Analysis
Sample
Type
Analytical
Tech -
Minimum
Geo, Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
56522
85924
103448
MPN/g
0
7
grab
sm9221 e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
wei =ht
Vector Attraction Reduction 115A NCAC 02I A 11171 - Please indicate alternative pertormea:
Alt.I (VS reduction) Ll
Alt. 2 (40-day bench) Lj
Alt. 3 (30-day bench) 21
Alt. 4 (Spec. O, uptake) i
Alt. 5 (14-Day Aerobic) j
Alt. 6 (Alk. Stabilization Lj
Alt 7 (Drying- Stable) 0
Alt. 8 (Drying- Unstable)
Alt. 9 (injection) L1
Alt. 10 (incorporation) Ll
No vector attraction reduction alternatives were performed Ll
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02'I' .1107 have been met."
LJ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Z o, Itc., PrrPj,,+ uj 6+j2f. Zach Key US Biosolids. Inc.
Preparer me and Title (type or print) Land Applier Name
and Title (if applicable)(type or print)
SijKature of Preparer* Date Signa re of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 21' . 1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Yadkin Valley Sewer Authority
WWTP Name: Yadkin Valley Sewer Authority
Monitoring Period: From 1/1/2021 To
WQ Permit Number: WQ0037135
NPDES Number: NCO020567
12/31 /2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time:itemp)
Alt B (Alk Treatrncnt) ® All. C (Prior 'ftsting)D
Alt.D (No Prior Test) L
P1-0CCSS to further Reduce Pathogengs 0
If applicable to alternative
pez-formed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 0
Heat Drying 0
Heat Treatment J
l-hermnophilic
Beta Ray
Gatnma Ray D
Pasteurization El
Class B:
Alt. (I) Fecal Density
Alt_ (2) Process to Si_rtittcantIN Reduce Pathogens L1
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
.11
Lime Stabilization Ll
Air Drying
Composting A
jAcrobic Digestion Ll
Anaerobic Digestior.
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Fxcee-
n
1=requency
of Analysis
Sample
Type
Analytical
Tech -
litclue
Minimum
Geo. Mean
Maximum
Units
Fecal Colifor m
2 x 10 to the
6th power
per gram of
total solids
MPN
20747
51081
98765
MPN/g
0
7
grab
sm9221 c
CFU
1000 mpn per gram
of total solid (dry
wei ht)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) LJ
Alt. 2 (40-day bench) Lj
Alt. 3 (30-day bench) R1
Alt. 4 (Spec. 0� uptake)
Alt. 5 (14-Day Aerobic) LEI
Alt. 6 (Alk. Stabilization Lj
Alt 7 (Drying - Stable) Ll
Alt. 8 (Drying - Unstable) LJ
Alt. 9 (Injection) Ll
Alt. 10 (Incorporation) Lj
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
RJ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
J "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02'T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
VS O1• +Ill hC
Pre rer Name and Title (type or print)
Dennis Key US Biosolids, Inc.
Land Applier Name and Title (if applicable)(type or print)
Si ature of reparer* Date Signature of ].and Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 21' .I 102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Belmont WQ Permit Number: W00037135
WWTP Name: City of Belmont W WTP NPDES Number: NCO21 181
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (timei'temp) ❑
Alt B (Alk Treattnent) ❑ I
Alt. C (Prior Testing)❑
Alt.D (No Prier Test) ❑ I
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Ilcat Treatment J
"I'herinophilic
Beta Ray ©
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 1
Alt_ (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only)indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization LiAIr
Drying k pp--
COttlpC35til1�' ❑
Ael'Obll Dtgestton LJ
Anaerobic Digestion,
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
dences
Frequency
ol'Analysis
Sample
Type
Analytical
Tech -
i ciue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
576
1820
4339
MPN/g
0
7
grab
sm9221 C
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) L]
Alt. 3 (30-day bench) ]
Alt. 4 (Spec. O, uptake)
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
2,. , k (X VS fg;aso C-661Tnc Zach Key US Biosolids, Inc.
Preparer Name nd Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Sig ure of Pre arer* T Date Sign ire of LA' Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 21' .1102 (26)
DENR FORM PVRF 02T (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Forest City WWTP
WQ Permit Number. WQ0037135
WWTP Name: Forest City WWTP NPDES Number: NCO025984
Monitoring Period: From l /l /2021 To 12/31 /202 l
Pathogen Reduction (15A NCAC 02T. 1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time,%telllp) Ll
Alt B (Alk -I reatnient) D Alt. C (Prior Testing)C)
Alt.D (No Prier Test) C1
Process to Furthcr Reduce Pathogengs i1
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost [l
Heat Drying Cl
Heat Treatment D
Flierinophilic 0
Beta Ray CI
Winma Ray D
Pasteurization 0
Class B:
JAIL (1) Fecal Density 21
Alt. (2) Process to Sigtiific;andy Reducc Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
V
Lime Stabilization D
F Air Drying LJ
Composting Ll
jAcrobic Digestion lJ
Anaerobic Digestion. 0
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um er o
E:xcee-
1=requencv
of Analysis
Sample
Tences ype
na vt,ca
fech-
i que
Minimut
Geo. MeanMaximu]
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
55944
180401
633803
MPN/g
0
7
grab
sm9221 c
CFtJ
1000 lnpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.] (VS reduction) Lj
Alt. 2 (40-day bench) Ll
Alt. 3 (30-day bench) 21
Alt. 4 (Spec. O, uptake) Lj
Alt. 5 (14-Day Aerobic)
Alt. 6 (Alk. Stabilization Lj
Alt 7 (Drying- Stable) D
Alt. 8 (Drying - Unstable) 0
Alt. 9 (Injection) L`I
Alt. 10 (Incorporation) Lj
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02'I' .1107 have been met."
F-1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .l 107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. 1 am aware that there are
significant penalties for false certification including fine and imprisonment."
Z-a ! % VS 4:6J O W.S . :CRc _
Preparer Na e and Title (type or print)
Signifture of Preparer*
lach Kev US Biosolids. Inc.
land Applier Name and Title (iFapplicable)(typc or print)
Date Sig ture of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 21-.1 102 (26)
DENR FORM PVRF 02T (12/2006)

North Wilkesboro
NCO020761

Waypointo
ANALYTICAL
46381
US &osolids Inc
Dennis Key
958 Hoots Road
Roaring River , NC 28669
Report Number:21-123-0004
Lab No : 76127
Sample ID : North Wilkesboro
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 4 Fax $04-271-6446
www.waypointanalytical.com
Project North Wilkesboro
Information :
REPORT OFANALYSIS
Report Date:05/11/2021
Received : OS/03/2021
TA,'ct
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 4/ 28 / 20Z 1 11:00
Test
Results
Units
MQL
of
Date / Time
Analyzed
By
Analytical
Method
Total Solids
5.40
%
0.010
1
05/04/21 16:30
FMM
SM-2540G
Total Kjeldahl Nitrogen
44600
mg/Kg - dry
4630
1
05/10/21 09:00
JPJ
iM-4500-NH3C-TKF
Phosphorus
14900
mg/Kg - dry
92.6
1
05/07/21 01:00
TJS
6010D
Potassium
3350
mg/Kg - dry
185
1
05/07/21 01:1)0
TJS
6010D
Sulfur
6800
mg/Kg - dry
185
1
05/07/21 01:00
TJS
6010D
Calcium
9540
mg/Kg - dry
926
1
05/07/21 01:00
TJS
6010D
Magnesium
2720
mg/Kg - dry
92.6
1
05/07/21 01:00
TJS
6010D
Sodium
781
mg/Kg - dry
463
1
05/07/21 01:00
TJS
6010D
Iron
22600
mg/Kg - dry
185
1
05/07/21 01:00
TJS
6010D
Manganese
265
mg/Kg - dry
9.26
1
05/07/21 01:00
T]S
6010D
Copper
369
mg/Kg - dry
9.26
1
05/07/21 01:00
TJS
6010D
Zinc
1040
mg/Kg - dry
23.1
1
05/07/21 01:00
TJS
6010D
Organic N
36900
mg/Kg - dry
4630
1
05/10/21 09:00
CALCULATION
Nitrate+Nitrite-N
415
mg/Kg - dry
90.7
1
05/10/21 13:50
ZBD
4500NO3F-2011
Nickel
23.5
mg/Kg - dry
4.63
1
05/07/21 01:00
TJS
6010D
Mercury
1.11
mg/Kg - dry
0.293
1
05/06/21 13:26
DD8
SW-7471B
Selenium
<9.26
mg/Kg - dry
9.26
1
05/07/21 01:00
TJS
6010D
PH
6.6
S.U.
1
05/08/2115:30
CxC
9045D
Qualifiers/ *
Outside QC Limit
B
Analyte detected in blank
Definitions C
GCMS Confirmation Analysis
E
Result above cal range
g
GGA Outside QC Limits
H
Beyond holding time
J
Estimated value
M
Minimum value
NA
Not on Scope of Accreditation
NC
Not confirmed
Q
RPD >40% dual column results
T
Sample exhibits toxicity
U
Unconfirmed
Refer to cover letter,
Page 3 of 6

•
Waypoint,
7ti221Nhitepine
Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46381
US Biosolids Inc
Project
North Wilkesboro
Dennis Key
Report Date : 05/11/2021
958 Hoots Road
Information :
Received : 05/03/2021
Roaring River , NC 28669
rq�}
1R►V'c W irl6Wy�
Pauric Mc Groary Ph.D., CPA
Report Number :21-123-0004
REPOR T OF A NAL YSIS
Agronomist
Lab No : 76127
Matrix:
Solids
Sample ID : North Wilkesboro
Sampled: 4/28/2021 11:00
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Method
Ammonia Nitrogen
7720
mg/Kg - dry
1850
1 05/10/21 09:00
JPJ SM-4500-NH3C
Aluminum
47000
mg/Kg - dry
92.6
1 05/07/21 01:00
TJS 6010D
Arsenic
<4.26
mg/Kg - dry
9.26
1 05/07/21 01:00
TJS 6010D
Cadmium
<1.85
mg/Kg - dry
1.85
1 05/07/21 01:00
T3S 6010D
Chromium
57.4
mg/Kg - dry
4.63
1 05/07/21 01:00
TJS 6010D
Lead
35.0
mg/Kg - dry
5.56
1 05/07/21 01:00
TJS 6010D
Molybdenum
6.07
mg/Kg - dry
4.63
1 05/07/21 01:00
TJS 6010D
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF Date / Time
By Analytical
Analyzed
Batch
Moisture
94.6
%
0.010
1 05/04/2116:30
FMM L551007
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 4 of 6

-
o
cci
0
O
0
cn
oN
0)
Y
0
to
cn
(A
0)
N
-
E
m
E
O
II
II
II
it
N
.o

SAR
Sodium Absorption Ratio
Na : Sodium (MgIL) Equivalent weight: 23
Ca : Calcium (MgIL) Equivalent weight: 20
Mg : Magnesium (MgIL) Equivalent weight: 12
Milli Equivalent = MgIL 1 Equivalent weight
Na M /L Ca M IL M MIL
42.174 1 515.16 1 146.88
NAME Ca (ME) M9AWQ
1.833652 25.758 12.24
SAR= Na Milli Equivalentl[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)10.5 power
SAR = 0.4206$ (From MgIL entered above)
SAR= 0.412948 (From ME entered below)
Na ME Ca (ME) M ME
1.8 1 25.8 1 12.2
The amour
amount of E
Permitting

Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 03/02/2021
Reported: 03/03/2021
For: N WILKESBORO
Comments: GEOMETRIC MEAN: 85,924 MPNIg
STATESVILLE
ANALYTICAL
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
210302-32-01
Fecal Coliforms
NW1
103448
MPNIg
SM92210E-20M
03/02/2021
MD
210302-32-01
Percent Solids
NW1
0.29
%
SM254❑B-2011
03/02/2021
MD
210302-32-02
Fecal Coliforms
NW2
56522
MPN/g
SM92210E-2006
03/02/2021
MD
210302-32-02
Percent Solids
NW2
0.23
%
SM25408-2011
03/02/2021
MD
210302-32-03
Fecal Coliforms
NW3
88462
MPN/g
SM92210E-2006
03/02/2021
MD
210302-32-03
Percent Solids
NW3
0.26
%
SM254OB-2011
03/02/2021
MD
210302-32-04
Fecal Coliforms
NW4
103448
MPNIg
SM92210E-2006
03/02/2021
MD
210302-32-04
Percent Solids
NW4
0.29
%
SM254❑B-2011
03/02/2021
MD
210302-32-05
Fecal Coliforms
NW5
76667
MPNIg
SM92210E-2006
03/02/2021
MD
210302-32-05
Percent Solids
NW5
0.3
%
SM254❑B-2011
03/02/2021
MD
210302-32-06
Fecal Coliforms
NW6
81482
MPNIg
SM92210E-2006
03/02/2021
MD
210302-32-06
Percent Solids
NW6
0.27
%
SM254DB-2011
03/02/2021
MD
210302-32-07
Fecal Coliforms
NW7
103448
MPNIg
SM92210E-2006
03/02/2021
MD
210302-32-07
Percent Solids
NW7
0.29
%
SM254❑B-2011
03/02/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Analytical Results -�-11
ALL
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 05/11/2021
Reported: 06/21 /2021
For: N Wilkesboro
Comments:
Sample Number
Parameter
Sample ID
Result
Unit Method Analyzed
Analyst
210511-28-01
30 Day Benchscale
NWilkesboro
10.0
% EPA625-R-92I0 05/11/2021
MD
210511-28-01
TCLP
NWilkesboro
See Attached
as Noted 05/12/2021
PACE
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 e 704/872/4697
Page 1 of 34

Analytical Results
US BIOSOLIDS For: N WILKESBORO
958 HOOTS RD
ROARING RIVER, NC 28669
Entered: 5/11/21
Reported: 6121/21
Sample ID: 220511-29-01
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge 130day1
Total Solids
Volatile Solids
% Volatile Solids
Week
1
1.82
0.92
0.5055
Week
2
1.83
0.93
0.5082
Week
3
1.77
0.87
0.4915
Week
4
1.78
0.88
0.4944
Week
5
1.68
0.81
0.4821
Week
_6
1.69
0.81
0.4793
Volatile
Solids Reduction:
0.5055 - 0.4793 X 100 =
0.5055 - (0,5055 X 0.4793)
10.0%
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.€t 44ONC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 33 of 34

30 Day Bench Warksheet
Sample I'D # 210511-28
WEEK 1
Samples
I Total Solids
Volatile Solids
% Volatile Fraction
1
1.82
0.92
2
1.83
0.93
3
Avera e:
1.82
1.82
0.92
0.42
0.S0SS
WEEK 2
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.80
0.91
2
1.86
0.95
3
1.82
0.92
Average:
1.83
0.93
0.5082
WEEK 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
E 1.76
0.87
2
1.79
0,88
_ m
3
1.75
0.86
Avera c:
1.77
0.87
4915
WEEK 4
Samples
' Total Solids
Volatile Salida
% Volatile Fraction
1
1.76
0.86
2
1.84
0.90
3._. _.
1.75
0.87
Average:
1 1.78
0.88
0.4944
WEEK 5
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.67
0.80
2
1.70
0.82
3
1.68
0,82
Avera e: ':
1.68
0.81
0.4821
WEEK 6
I Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.69
0.82
2
1.73
0.83
_
3
1.65
0.79
Avera e:
1.69
0.81.
0.4793
Van Kleeck Reduction: 0.5055 -- 0.4793 X 100 = %
0.5055 - ( 0,5055 X 0.4793)
Final Result: 1.0.0%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 34 of 34

IceArrafy#ical
- www.penlat6s-sae
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 210511-28-01
Pace Project No.: 92538409
Sample: 210511-28-01
Lab ID: 92538409001 Collected. 05111/21 09:00
Received: 0502121 13:26 Matrix: Solid
Results reported on a 'dry weight" basis and are adjusted for percent moisture, sample sire and any dilutions.
Parameters
Results Units Report Limit OF
Prepared Analyzed CAS No. Qual
Chlorinated Herb. (GC) 8151A
Analytical Method: EPA 8151A Preparation Method: 8151A
Leachate Method/Date: 1311; 05119I21
14:58 Initial pK
6.8; Finat pH: 4.92
Pace National - Mt. Juliet
2,4,5-TP (Silvex)
NO mg1L
0,00200 1
05121P21 09:22 05/23121 10;51 93.72-1 R1
2,4-D
NO mg1L
0.00200 1
0512V2109:22 0512312110:51 94.75-7 LO.ML.
R1
Surrogates
2,4•DCAA(S)
45.8 %
14.0-158 1
0512112109:22 0512312110.51 19719-28-9
8081 TCLP Pesticides RVE
Analytical Method: EPA 8081 B Preparation Method: EPA 3510C
Leachate MethodlDale: EPA 1311: 05113/21 15:22 Initial pH:; Final pH: 5
Pace Analytical Services - Charlotte
gamma-BHC (Lindene)
NO ug1L
0.50 1
05/17/21 08:15 05117/21 12:46 58-89-9
Chlordane (Technical)
NO uglL
3.0 1
05/17121 08:15 05117121 12:46 57-74-9
Endrin
ND uglL
0.50 1
051171210815 05/17121 12:46 72-20-8
Heptachlor
ND ug1L
0.50 1
0511712108:15 05117121 12:46 76-44-8
Heptachlor epoxide
ND uglL
0.50 1
05/1701 08:15 05)17121 12:46 1024-57.3
Methoxychlor
NO uglL
1000 1
050712108:15 05117121 12:46 72-43-5
Toxaphene
NO uglL
3.0 1
05117121 08:15 0511712112-46 8001-35.2
Surrogates
Decachlorobiphenyt (S)
77 %
10-154 1
05117121 08:15 05/17121 12:46 2051.24-3
Tetrachloro-m-xytene(S)
60 %
10-184 1
05/17121 08:15 05/17121 12,46 877-09-8
8082 GCS PCB
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016)
NO uglkg
977 1
05/21121 15:48 05124121 16:53 12674-11-2
PCB-1221 (Aroclor 1221)
NO uglkg
977 1
05/21121 15:48 W2411 16:53 11104-28-2
PCB-1232 (Aroclor 1232)
NO uglkg
977 1
05/21/21 16:48 05/24/21 16:53 11141-16-6
PCB-1242 (Aroclor 1242)
ND uglkg
977 1
05/21/21 15:48 05124)21 16:53 53469-21-9
PCB-1248 (Aroclor 1248)
NO ugNg
977 1
Q5121121 15:48 05124/21 16:53 12672.29-6
PCB-1254 (Aroclor 1254)
ND uglkg
977 1
05/21/21 15:48 05/24/21 16:53 11097-69-1
PCB-1260 (Aroclor 1260)
NO uglkg
977 1
05/21/21 15:48 05124/21 16:53 11096-82-5
Surrogates
Decachlorobiphenyl (S)
26 %
10-160 1
05/21/21 15:48 05124121 16:53 2051-24-3
8082 TCLP PCBs RVE
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311: 05)13121 15:22 Initial pH: ; Final pH: 5
Pace Analyticai Services - Charlotte
PCB-1016 (Aroclor 1016)
NO uglL
1000 1
05117121 08:15 05119121 03:39 12674-11-2
PCB-1221 (Aroclor 1221)
NO uglL
1000 1
05117121 08:15 05/19121 03:39 11104-28-2
PCB-1232 (Aroclor 1232)
NO uglL
1000 1
05117121 08:15 05/19/21 03:39 11141-16.5
PCB-1242 (Aroclor 1242)
NO uglL
1000 1
05/17121 08:15 05/19/21 0139 53469-21-9
PCB-1248 (Aroclor 1248)
NO ugIL
1000 1
05/17121 08:15 05/19/21 03:39 12672-29-6
PCB-1254 (Aroclor 1254)
ND ug1L
1000 1
05117121 08 15 05/19121 0139 11097-69-1
PCB-1260 (Aroclor 1260)
NO uglt
1000 1
05117/21 08:15 05119/21 03:39 11096-82-5
Surrogates
Decachlorobiphenyl (S)
87 %
10-181 1
05MD21 08:15 05119121 03:39 2051-24-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 05128/2021 03:08 PM without the written consent of Pace Analytical Services. LLC
Page 5 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 9 of 34

11ceAnalytical
www"Colabstm
ANALYTICAL RESULTS
Pace Anatytieal Services, LLC
9800 Kincey Ave. Suite 1W
Huntersville. NC 20078
[phone]
Project : 210 511-28-01
Pace Project No.: 92538409
Sample: 210511.28.01
Lab lV: 92538409001 Collected: 05111/21 09:00 Received: 05112121 13:26 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit OF Prepared Analyzed CAS No.
Qual
6010 MET 1CtP, TCLP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Leachate Method/Date, EPA 1311, 05120121 15:04 Initial pH:: Final pH: 2
Pace Analytical Services - Asheville
Arsenic
NO mg/L 0.050 1 05/22121 09:18 05122/21 20:29 7440-38.2
Barium
NO mglL 0.25 1 05122/2109:18 05122121 20:29 7440-39-3
Cadmium
ND mglL 0.0050 1 05/2212109:18 05/22/21 20:29 7440-43-9
Chromium
NO mg1L 0,050 1 0512212109:18 05J2212120:29 7440-47-3
Lead
ND mg1L 0-025 1 0512212109-18 05/22/21 20;29 7439-92-1
Selenium
ND mglL 0.10 1 05/2212109:18 05/22/21 20:29 7782-49-2
Silver
ND mglL 0,025 1 0512212109:18 0512212120:29 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 05120/21 15:04 Initial pH: ; Final pH: 2
Pace Analytical Services - Asheville
Mercury
ND mglL 0,00020 1 0512412109:35 05/24121 12:45 7439-97-6
0270E TCLP RVE
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Leachate MethodlDate: EPA 1311: 05113121 15:22 Initial pH:: Final pH: 5
Pace Analytical Services - Charlotte
1,4-Dichlorobenzene
ND ug1L 50.0 1 051171210818 05J17121 1510 106-46.7
2,4-Dinitrotoluene
NO ug/L 50.0 1 051171210&16 05M7/2115:20 121-14-2
L1
Hexachloro-1,3-butadiene
ND ug1L 50.0 1 05117/21 08:18 05A7121 15 20 87-66-3
Hexachlorobenzene
ND ug1L 50.0 1 05117121 08 18 05A712115.20 118-74-1
L1
Hexachloroethane
ND u91L 50.0 1 051171210818 0511712115:20 67-72-1
2-Methylphenol(o-Creso€)
NO ug1L 50.0 1 05117/2108:18 050712115:20 95-48-7
3&4-Methylphenol(m&p Cresol)
ND uglL 50.0 1 05117/21 08:18 05J17121 15:20 15831-10-4
Nitrobenzene
ND ug1L 50.0 1 05117)210818 05/17121 15:20 98-95.3
Pentachiorophenol
ND ug1L 100 1 05117/21 D8:18 05117/21 1520 87-66-5
Pyridine
ND ug1L 50.0 1 0511712108:18 05/17/21 15:20 110-86-1
2,4,5-Trichlorophenol
NO ugJL 50.0 1 0511712108:18 0511712115:20 95-95-4
L1
2,4.6-Trichlorophenol
ND ug1L 50.0 1 05117/21 08:18 05J1712115:20 88-06-2
L1
Surrogates
Nitrobenzene-d5 (S)
86 % 10-144 1 05/17/21 08:18 05/17/21 15:20 4165-60-0
2-Fluorobiphenyl (S)
77 % 10-130 1 OF417121 08:18 05/17/21 15:20 321-60-8
Terpher l-d14 (S)
97 % 34-163 1 05117121 08:18 05/17121 15:20 1718-51.0
Phenol-d6 (S)
48 % 10-130 1 05/17121 08:18 05117/21 15:20 13127-88-3
2-Fluorophenol (5)
60 % 10-130 1 05117/21 08:18 05/17/21 15:20 367-12-4
2,4,6-Tribromophenol (S)
95 % 10-144 1 05/17121 08:18 05117/21 15:20 118-79-6
8260D MSV TCLP
Analytical Method: EPA 8260D Leachate MethodlDate: EPA 1311; 05/24/21 14:23
Pace Analytical Services - Charlotte
Benzene
ND ug1L 100 20 05/2512l14:13 7143-2
2-Butanone (MEK)
NO ug1L 200 20 05125J21 1413 78-93-3
Carbon tetrachloride
ND ug1L 100 20 05125r'21 14:13 56-23-5
Chiorobenzene
ND uglL 100 20 0512512114:13 108-90-7
Chloroform
NO ug1L 100 20 05125i2l 14:13 67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
Date: 0512812021 03,08 PM
without the written consent of Pace Analytical Services, LLC.
Page 6 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 10 of 34

�ceA aiytica1-
WWW.{ecrdN&CM
ANALYTICAL RESULTS
Project 210511-28-01
Pace Project No 92538409
Pace Analytical Services, LLC
98001(0ceyAve- Suite 100
Hunlerwilie, NC 28078
[phone]
Sample: 210511-28-01 Labia: 92538409001 Collected: 05/11121 09:00 Received 05/12121 13:26 Matrix: Solsd
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
8260D M5V TCLP
Analytical Method: EPA 8260D Leachate Melhoc lDate:
EPA 1311, 05124/21 14:23
Pace Analytical Services - Charlotte
1,4-Dichlorobenzene
NO uglL 100 20
05/25/21 14:13 106-46-7
1,?-Dichloroelhane
NO u91L 10o 20
051251211413 107-06-2
1,1-DicNomethene
NO uglL 100 20
0512512114:13 75.354
Tetrachloroethene
ND ug/L 100 20
0512512114:13 127-184
Trichloroethene
NO ug/L 100 20
05/25121 14:13 79-01-6
Vinyl chloride
NO ug1L 100 20
05/25121 14:13 75-01-4
Surrogates
1,2-1)ichloroethans-0 (S)
106 % 70-130 20
05/25121 14:13 17060-07-0
Toluene-d8 (9)
101 % 67-135 20
05/25121 14:13 2037-26-5
4-Bromofluorobenzene (S)
100 % 70-130 20
05125/21 14:13 460-00-4
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
94.4 % 0.10 1
06/12121 17:57 N2
1010 Flashpoint,Ctosed Cup
Analytical Method. EPA 10106
Pace Analytical Services - Asheville
Flashpoint
5200 deg F 1
06124121 15:53
9045 pH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.8 Sid. Units 0.10 1
05124121 16:04 H3
9095 Paint Filter Liquid Test
Analytical Method: EPA 90958
Pace Analytical Services - Asheville
Free Liquids
Fail 1-0 1
05f2412115:18 T3
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Pace Analytical Services - Greensburg
Cyanide, Reactive
NO mgfk9 18.0 1
05/17/21 16:21 05/19121 18:22
734S Reactive Sulfide
Analytical Method: SM 4500S2F-2011 Preparation Method:
SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Suffide, Reactive
NO mglkg 180 1
05/17121 16:21 05117/21 16:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except it full,
Date: 0512MO21 03,08 PM without the written consent of Pace Analylcal Services. lLC Page 7 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page i 1 of 34

Yadkin Valley Sewer Authority
N CO020567

Waypoint(l)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 " rax 804-271-6446
www.waypointanalytical.com
46381
US Biosolids Inc Project Yusa
Dennis Key Report Date ; 03/25/2021
958 Hoots Road Information ; Received : 03/15/2021
Roaring River , NC 28669
�piy,G �1� (yloa K/
Report Number: 21-074-0007 REPORT OF ANALYSIS Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 75439 Matrix: Solids
Sample ID : Yusa Sampled: 3/11/2021 12:30
Test Results Units MQL DF Date r Time By Analytical
Analyzed Method
Moisture 97.5 % 0,010 1 03/18/2116:48 FMM SM-254OG
Test Results units MQL DF Date I Time By Analytical
Analyzed Method
Ammonia Nitrogen
4840
mg/Kg - dry
4000
L
03/22/21 14:30
JP3
SM-4500-NH3C
Nitrate+Nitrite-N
<195
mg/Kg _ dry
t95
1
03/19/21 14:4B
LBD
4500NO3F-2011
Organic N
SS600
mg/Kg - dry
10000
1
03/22/21 10:00
CALCULATION
PH
6.3
s.u,
1
03/19/2117:06
ADM
90450
Total Solids
2.46
%
0.010
1
03/1B/21 16:48
FMM
SM-254OG
Total Kjeldahl Nitrogen
60400
m9/Kg - dry
WOW
1
03/22/21 10:00
JP1 ;M-4500-NH3C-TKf
Phosphorus
13500
mg/Kg - dry
200
1
03/20/21 03:59
JTR
60100
Aluminum
21900
mg/Kg - dry
200
1
03/20/21 03:59
JTR
6010D
Arsenic
<20.0
mg/Kg - dry
20.0
1
03/23/21 22:40
]ADS
6010D
Calcium
3920
mg/Kg - dry
2000
1
03/20/21 03:59
JTR
60101)
Cadmium
<4.00
mg/Kg - dry
4,00
1
03/20/21 03:59
JTR
6010D
Chromium
14.6
mg/Kg - dry
10.0
1
03/23/21 22:40
DADS
6010D
Copper
174
mg/Kg - dry
20.0
1
03/20/21 03:59
JTR
6010D
Iron
9720
mg/Kg - dry
400
1
03/20/2I 03:59
JTR
6010D
Lead
<12.0
mg/Kg - dry
12.0
1
03/20/21 03:59
JTR
6010D
Magnesium
1720
mg/Kg - dry
200
1
03/20/21 03:59
JTR
6010D
Manganese
237
mg/Kg - dry
20.0
1
03/20/21 03:59
JTR
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 3 of 7

Waypoint.
(2)
7627. Whitepine Road, Richmond, VA 23Z37
Main 804.743.9401 " Fax [phone]
ANALYTICAL
www.waypointanalyticaLcom
46381
US 9losolids Inc
Project
Yusa
Dennis Key
Report Date : 03/25/2021
958 Hoots Road
Information :
Received ; 03/15/2021
Roaring River , NC 28669
Trutl"C PIf (rlaar
Pauric Mc Groary Ph,D., CPA
Report Number: 21-074-0007
REPORT
Agronomist
Lab No: 75439
Matrix:
Solids
Sample ID: Yusa
Sampled:
3/11/2021 12:30
Test
Results
Units
MQL
OF Date 1 Time
By Analytical
Analyzed
Method
Mercury
<0.612
mg/Kg - dry
0.612
1 03/18/21 11:11
DDB SW-7471B
Molybdenum
< 10.0
mg/Kg - dry
10.0
1 03/20/21 03:59
JTR 6010D
Nickel
< 10.0
mg/Kg - dry
10.0
1 03/20/21 03:59
JTR 6010D
Potassium
3890
mg/Kg - dry
400
1 03/20/21 03:59
JTR 6010D
Selenium
<20.0
mg/Kg - dry
20.0
1 03/20/21 03:59
JTR 6010D
Sodium
2110
mg/Kg - dry
1000
1 03/20/21 03:59
JTR 6010D
Zinc
223
mg/Kg - dry
50.0
1 03/20/21 03:59
?TR 6010D
Sulfur
3O5O
mg/Kg - dry
400
1 03/20/21 03:59
JTR 6010D
Qualifier:/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Fxceeded
Page 4 of 7

Analytical Results
U.S. Biosolids Inc
958 Moots Road
Roaring River, NC 28669
Receive Date: 03/02/2021
Reported: 03/03/2021
For: YVSA
Comments: GEOMETRIC MEAN: 51,081 MPN/g
STATESVILLE
ANALYTICAL
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
210302-33-01
Fecal Coliforms
YVSA 1
85238
MPN/g
SMMlCE-20M
03/02/2021
MD
210302-33-01
Percent Solids
YVSA 1
2.52
%
SM25400-2011
03/02/2021
MD
210302-33-02
Fecal Coliforms
YVSA 2
53719
MPN/g
SM92210E-2oo6
03/02/2021
MD
210302-33-02
Percent Solids
YVSA 2
2.42
%
SM25QB-2011
03/02/2021
MD
210302-33-03
Fecal Coliforms
YVSA 3
50980
MPN/g
SM92210E-20os
03/02/2021
MD
210302-33-03
Percent Solids
YVSA 3
2.55
%
SM2540&2011
03/02/2021
MD
210302-33-04
Fecal Coliforms
YVSA 4
53061
MPNIg
SAA92210E-2006
03/02/2021
MD
210302-33-04
Percent Solids
YVSA 4
2.45
%
SM25408-2011
03/02/2021
MD
210302-33-05
Fecal Coliforms
YVSA 5
98765
MPN/g
SM92210E-2006
03/02/2021
MD
210302-33-05
Percent Solids
YVSA 5
2.43
%
SM25409-2011
03/02/2021
MD
210302-33-06
Fecal Coldorms
YVSA 6
32000
MPNIg
SM92210E-20%
03/02/2021
MD
210302.33-08
Percent Solids
YVSA6
2.5
%
sM254M62011
03/02/2021
MD
210302-33-07
Fecal Coliforms
YVSA 7
20747
MPNIg
SM92210E-20M
03/02/2021
MD
210302-33-07
Percent Solids
YVSA 7
2.41
%
SM29408-2011
0310212021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert 937755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 v 704/872/4697
Pagel of 4

Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 05/11/2021
Reported: 06/21 /2021
For: YVSA
Comments:
Sample Number parameter Sample 1D Result Unit Method Analyzed Analyst
210511-31-01 30 Day Benchscale YVSA
Respectfully submitted
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
55
0/0 -Maers.?_9�,r 05111/2021 MD
PO Box 228 « Statesville, NC 28687 • 704/872/4697
Page t of 5

STATFSV11. i-r
ANALYTICAL
Analytical Results
US 810SOUDS for: YVSA
958 HOOTS RD
ROARING RIVER, NC 28669
Entered: S/11/21
Reported: 6/21/21
Sample 11): 210511-31-01
PARAMI TES: _V_e_ctor Attraction Redd on/Aerobicaily OinesttRo Blades 119dav)
Total Solids Volatile Solids % Volatile Solids
1.44 0.73 0.5069
Week 2 1.48 0.75 0;5M
Week 3. „ 1.46 0.73 0.5000
W"k 4 1.41 -- 0,69 _ ....,.. 0.4894
Week 5 1.40 0.69 , „ _. 0.4929
Week 6 1 .67 0,4927
Volatile Solids Reduction: 0.5069_ - 0.4927 X 10.0 = 5.5 %
0.5069 - (0.5069 X 0.4927)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.# 440NC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 5

30 Day Bench Worksheet
Sample ID N 210511-31-01
WEEK I
Samples
I Total Solids
Volatile Solids 1
% Volatile Fraction
1
1.43
0.72
2
1.43
0.72
3
1.46
0.74
Avers e:
1.44
0.73
0.5069
WEEK 2
Samples
I Total Solids
Volatile Solids
% Volatile Fraction
1
1,46
0.74
2
1.49
0.76
3
1.49
0.75
Average:
1.48
0.75
0.5063
WEEK 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.47
0.73
2
1.46
0.73
3
1.46
0.73
Average:
1.46
0.73
0.5000
WEEK 4
Samples
I Total Solids
Volatile Solids
% Volatile Fraction
1
lAl
0.69
2
1.41
0.70
3
1.41
0.69
Average:
1.41
0,69
0.4894
WEEK 5
Samples
I Total Solids
Volatile Solids
% Volatile Fraction
1
1.39
0.68
2
1.40
0.69
3
1.40
0.69
Average:
1.40
0.69
0.4929
WEEK 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.35
0.66
2
1.37
0,67
3
1,36
0.67
Average:
1.36
0.67
0.4927
Van Kleeck Redaction; Q.5Q69 - 0.4927 X 100 = %
0.5069 - ( 0.5069 X 0.4927)
Final Result: 5.5%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 5

11C6Aa*kj1 e
r
ANALYTICAL RESULTS
Pace AnatolCal Sorvices, LLC
98M Kincey Ave. Side 100
Hummvilb, NC 2SD70
(7041875-W92
Protect YVSA
Pace Protect No.: 92WS61
SampW 201010.20.01 LmbIP: 92S43661001 Collected: OW10121 13A7 Received: 0&11121 08:35 Matrix: Solid
Rasutts rep~ on a 'dry waiaht' basis and an adjusted far psment moWwv, samph she and any dilutlons.
Parameters Resutts Units Report Limit OF Prepared Analyzed CAS No. dual
Chlorinated Herb, (GC) 8151A Analytical Method: EPA8151A Preparation Method: 8151A
Leaohale MedwxlfDate: 1311; 06119121 11:35 Initial pH: 6.53: Final pH: 4.89
Pace National - Mt. Juliet
2,4,5-TP (Silvex) NO mgfL 0.00200 1 06/21121 09:39 06/23/21 15:15 93-72.1
2.4-0 HD mglL 0.00200 1 0612112109:39 06123121 15:15 94-75-7
Surrogaaes
24DCAA(S)
121 %
14.0-158
1 OW21f21 09:39 W2312t 15:15 19719.25-9
8081 TCLP Pesticides RYE
Analytical Msuwd EPA806IB Preparation Method: EPA35IDC
Leachate MethodlDate: EPA 1311. OW021 15:39 Initial pH: 5.08, Final pH 5
Pace Analytical Services - Charlotte
gamma-SHC(Lindane)
NO ugfL
0.60
1 06/16/2109:33 0611712t t5:15 58.89.9
Chlordane (Technical)
NO uglL
3.0
1 06/16121 09:33 06117121 15:15 57-74-9
Endrin
NO uglL
0.50
1 0&161210933 06117f211515 12-20-8
Heptathtor
NO ugA
0.50
1 OWt&2109:33 0611712115-15 76-41-8
Hoptactilor epoxide
NO uglL
0.50
1 WI&2109-33 0&1712115:15 1024.57.3
Methonychior
NO ug1L
1000
1 0611M109:33 O&1712115:15 7243-5
To)faphene
NO uglL
3-0
1 0611W2109:33 OW1712115:15 8001-35-2
surrupates
DecacMorobiphenyl(5)
107 %
10-154
1 06116/2109:33 06/17121151$ 2051.24.3
Tetracmero-m-xylene (S)
83 %
10-154
1 06116/21 09:33 06/17121 1& 15 877-09-8
8082 TCLP PCBs RVE
Analytical Method: EPA 8082A Preparation Method: EPA 351 OC
Leachate MemodlDale: EPA 1311: 0&14l21 15:39
Initial pH. 5.08: Final pH: 5
Pace Analytical Servioes - Chanotle
PCB-1016 (Aroclor 1016)
NO ug/L
1000
1 0&16121 09:33 06117121 21:43 12674-11.2
PCB-1221 (Amdor 1221)
NO ug/L
1000
t 06116121 09:33 D6117121 21:43 11104-28-2
PCB-1232 (Arocbr 1232)
NO uSIL
1000
1 06116f21 09:33 D6117121 21:43 11141-16-5
PCB-1242 (Arodor 1242)
ND u91L
1000
1 0611612l 09:33 08117/21 2I A3 53469-21-9
PCB-1248 (Arodor 1248)
NO ug1L
1000
1 0&1&21 09:33 06117121 21:43 12672-2I3-6
PCB-1254 (Arbclor 1254)
NO u91L
1000
1 06r1921 09:33 06117121 21:43 11097-69-1
PCB-1260 (Arodor 1260)
NO ugA
1000
1 0&16121 09:33 06117121 21 43 11096-82-5
Surrogates
Dacachlorobiphenyt(S)
104 %
10-181
1 06/16121 09:33 D&17121 21.43 2051.24-3
6018 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06114/21 16:20
Initial pH: 5.09; Final pH: 2
Pace Analytical Services - Ashavdts
Arsenic
NO mg/L
ODOM
1 060612109:45 DW1712105:21 7440-30-2
Barium
NO mg/L
OVO
1 06116i210945 061171210521 7440-39-3
Cadmium
NO mgfL
0.00020
1 06/16/21 WAS 0&17121 05:21 7440-43-9
Chromium
ND mg1L
0 OD20
1 0&1 W21 09AS 06/17121 05:21 7440 47-3
Lead
NO mglL
0.0010
1 0611612109:45 06117/2105:21 7439-92.1
Selenium
NO mgA-
0.0040
1 OW16f2109:45 0611712105-21 7782-49.2
Silver
NO mglL
O.DO10
1 06116/2109:4$ 06/17121 O5,21 7440.22A
REPORT OF LABORATORY
ANALYSIS
This report shW1 not be reproduced, eu*pl m Full.
Date: 0&2512021 04:41 PM
without the written consent Of
Par* Araty4C41 S600"S. LLC,
Page 5 of 28
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 7 of 30

An^ •
�I7i a�
r
l
ANALYTICAL RESULTS
Pave Anal"" S•rvlfM, LLC
9800 Kincey Ave- Suke 100
Huntersrifle, NC 28078
{704)875-9092
Project: YVSA
Pace Project No.: 92543661
Sample: 201610.26.01 Lab lo: 92543361001 Collected: OW10121 13:47 Received: 06111121 08:35 Mama: Solid
Rasu is roporMd on a 'dry weight' basis and are adjusted for percent molstcns, sample sire and any dilutions.
Parameters Results Units Report Limit OF Prepared Ansiyzed CAS No. Dual
7470 Mercury, TCLP Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311. 06/14121 16:23 IntOat pH: 5.09; Final pH: 2
Pace Analytical Services - Asheville
Mercury No mg/L 0.00020 1 06116/21 10 33 06/16r21 14:14 7439.97.6
8270E TCLP RVE
Analytical Method: EPA 8270E Preparation Method: EPA 351 DC
Leachate Method/Date: EPA 1311, 0&14/21 15:39 Initial
pH: 5.08; Final pH: 5
Pace Analytical Services - Charlotte
1,4-Dichlorobenzene
NO
ugiL
5D.0
t
06116/2109:35 06116/2117:19 106-46-7
2,4-DiNtrotoluene
NO
ug1L
50.0
1
06/16/2109:35 06/16/21 IT19 121-14-2
Heaachloro-1,3-butadiene
NO
ug/L
50.0
1
06/1612109:35 06/161211719 87-68-3
Hexaddombenzens
NO
411-
50.0
1
06116/2109:35 06/16/2117:19 118.74.1
HexacNoroethene
NO
uglL
50.0
1
06116f2109:35 06ft6r2117:19 67-72-1
2-Methy1phano1(o-Creso1)
NO
ug/L
50.0
1
O6f16/2109:36 W16/2117:19 95-48-7
364-MOlhylphenokrn&p Cresol►
NO
ug/L
50.0
1
0&16f21 09:35 06116/21 17:19 15831-10-4
Nitrobenzene
NO
u9/1-
50.0
1
0&1612109:35 OWIW21 17:19 W95-3
PentactiWophencil
NO
ug/L
100
1
06/1&2109:35 06116f2117:19 67.86-5
Pyridine
NO
ug/L
50.0
1
0&1&2109,35 0611612117:19 110-86-1
2,4,5-Trichlorophergl
NO
ug/L
50-0
1
06/1612109:35 D611612117:19 95-954
2,4.6-TnchtorupherKil
NO
ug1L
50.0
1
0611W109:36 0611&21 17 19 88-06-2
Surrogates
Nitrobenzen"S(S)
72
%
10-144
1
Ml&2109:35 06176/2117:19 4165.60.0
2-Fluorobiphenyt(S)
68
%
10-13D
1
06/i&2109:35 1)6/1612117:19 321-6"
Terphenyl-d14 (S)
100
%
34-163
1
0&16121 09:35 06116121 17:19 1718-51-0
Phenol-dii(S)
40
%
10-130
1
M16r2109:35 061161211719 13127-8&3
2-Ftuorophenol (S)
54
%
10.130
1
06/16/21 09:35 06116f21 17:19 367.12.4
2,4.6-Tribrornophenol(S)
97
%
10-144
1
06116/2109:35 06/1612117,19 118-79-6
82UO tMW TCLP
Analytical Method EPA 8260D Leaehate Method/Oate: EPA 1311: 06/22121 14:40
Pace Analytical Services - Charlotte
t3enzene
NO
ug/L
100
20
0&23/21 118:40 71-43-2
2-Butanone (MEK)
NO
ug/L
200
20
0&23/21 18:40 78-93-3
Carhop tetrac to ide
NO
ug/L
100
20
06123M 18:40 56-23-5
Chlorobenzene
NO
uq/L
100
20
06/23/2118:40 108-90-7
Chloroform
NO
ug/L
100
20
0612312118:40 67-66-3
1.4-Diddorobenzene
NO
ugfL
1DO
20
0612W118:40 106-46-7
12-Oictilunxrhane
NO
ug/L
100
20
06/23)2118:40 107.06-2
1.1-Didgoroethene
NO
ug/L
1D0
20
06/2M118:40 75-35-4
Tetrachtoroethene
NO
ug1L
100
20
06123r21 f8:40 127.18-4
TricNoroethene
NO
ug/L
100
20
06123/2118:40 79.01.6
Vinyl chloride
ND
u91L
100
20
W23/2118:40 75-01-4
Sumpgetp
1,2.Dichlomethaine-64(5)
95
%
70.130
20
06/23/21 18A0 11060-07-0
Toluene-dB(S)
103
%
67-135
20
D6/23f21 18:40 2037-26-5
4-BromoAuorobertzene (S)
98
%
70-130
20
06/23/21 18.40 460.00-4
REPORT OF LABORATORY
ANALYSIS
This report !hall not be reproducer%, except n lull.
Date: 06/25/2021 04:41 PM
h thaut the mitten ccinawl of Paw Analytical Services. LLC.
Page 6 of 28
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 8 of 30

ire At a •
1r1rn11sea1Ws�
ANALYTICAL RESULTS
Pace Analytical Servieee, LLC
96M Kinoey Ave. Suite 100
Huntersvifle. NC 24074
17041475-9092
Project YVSA
Pace Project NO.' 92543MI
Sample: 201610.28,01
L.ab 10: 92543861001 Collected- 06110/21 13 47 Received: 06111121 08:35 Matrix: Solid
Resu#s repWW on a 'dry weight'
basis and are adjusted Ow percent moisture, sample size and aptly dilutions.
Parameters
Results Units Report Limit DF Prepared Anaiyxed CAS No. Ouai
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services • Charlotte
PercentMoisUra
98.4 % 0.10 1 0611V2117,48 N2
1010 Flashpoint Closed Cup
Analytical Method: EPA 10108
Pace Analytical Services - Asheville
Flashpoini
>200 deg F 1 06122/21 08:41
9045 PH Soil
Analytical Method: EPA 90450
Pace Anatylical Services - Asheville
pH at 25 Degrees C
7.0 Sid, Units 0.10 1 0W21121 14:35 H3
OHS Paint Fltbr Liquid Teat
Analytical Method'. EPA 90M
Pace Analytical Services - Asheville
Free Liquids
Fail 1.0 1 06/21/21 14-24
733C S Reactive Cyanide
Analytical Meilhod: EPA 9014 Preparation Method: SW-846 7.3.3.2
Pace Analytical Services • Greensburg
Cyanide, Reactive
NO rllgfhg 61,5 1 06/16/21 17:17 06116/21 17:56
734E Reactive Sulfide
Analytical Method: SM 45DD-S2-F-2011 Preparation Method: SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive
NO mg/kg 615 1 06116/21 17.17 06116121 11:35
Sample: 2018'10.28.01 PCB
Lab 40: 92543861002 Collected:
06/10121 13:47
Received', 06111/21 08:35 Matrix: Water
Parameters
Results
Units Report Limit
DF
Prepared Analyzed CA$ No 0"
8062 GCS PCB RVE
Anafyliical Mathad: EPA8082A Preparation Method EPA 35tOC
Pace Analytical
Services - Charlotte
PCB-1016 (Arodor 10161
ND
ug1L
0.50
1
06124121 10:0a 0W24171 15:07 12674-11-2
PCB-1221 (Amcor 1221)
NO
u91L
0.50
1
D6124121 10:08 OW24121 15:07 11104-29-2
PCB-1232 (Aroclor 1232)
NO
ugll
0,50
1
06124121 10:08 06124121 15:07 11141-165
PCB•1242 (Arcclor 1242)
ND
uglL
0-50
1
06/24121 10:08 06/24121 15:07 53469-21-9
PCB-1248 (Arodor 1248)
ND
u9lL
0-50
1
06/24/21 10:08 06124/21 15:07 12672.29.E
PCB-1254 (AWjw 1254)
ND
ugll
0-60
1
06124121 10:06 OW4M 16:07 11097.69-1
PCB-1260 (Arockw 1260)
NO
uyL
0,50
1
06/24121 10:W 06✓24r21 15 07 11096-W-5
Surroples
Decachiorobiphenyl(S)
39
%
10-181
1
06/24/21 10:08 06124f21 15:07 2051-24-3
REPORT OF LABORATORY ANALYSIS
This report snag rwt be roproduced, except le full.
Date. 0&2512021 04:41 PM wi1hou101e wmen as iienl of Pace Anaiytirel Services. L LC Page 7 0f 28
PO Box 228 9 Statesville, NC 28687. 704/872/4697
Page 9 of 30

Belmont
N CO021181

(D
WayPAo nt.
NALYTICAL.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
www.waypointanalytical.com
46381
US Biosatids Inc Project Belmont
Dennis Key Report Date: 04/22/2021
958 Hoots Road Information : Received : 04/14/2021
Roaring River , NC 28669
Tawr< !fi(
REPORTOFANALYSIS Pauric Mc Groary Ph.D., CPA
Report Number : 21-104-OOD2 Agronomist
L,ab No : 75823 Matrix: Solids
Sample ID : Belmont Sampled: 4/13/2021 10.00
Test
Results
knits
MOL
OF
Date i Time
Analyzed
By
Analytical
Method
Total Solids
4.49
%
0.010
1
04/16/21 16:53
FMM
SM-254OG
Total Kjeldahl Nitrogen
43300
mg/Kg - dry
5560
1
04/19/21 10:00
)P)
1'M-4500-NH3C-W
Phosphorus
23800
mg/Kg - dry
ill
I
04/20/21 06:01
T)S
6010D
Potassium
2760
mg/Kg - dry
222
1
04/20/21 06:01
T)S
6010D
Sulfur
9620
mg/Kg - dry
222
1
04/20/21 O&W
T)S
6013D
Calcium
13600
mg/Kg - dry
1110
1
04/20/21 06:01
T)S
6010D
Magnesium
3180
mg/Kg - dry
111
1
04/20/21 06:01
T)S
6010D
Sodium
5130
mg/Kg - dry
556
1
04/20/21 06:Ot
T)S
6010D
Iron
27300
mg/Kg - dry
222
1
04/20/21 06:01
TIS
6010D
Manganese
1.090
mg/Kg - dry
11.1
1
04/20/21 06:01
T)S
60101)
Copper
311
mg/Kg - dry
11.1
1
04/20/21 06:01
T)S
6010D
Zinc
1560
mg/Kg - dry
27.8
1
04/20/21 06:01
T)S
6010D
Organic N
41100
mg/Kg - dry
5560
1
04/19/21 10;00
CALCULATION
Nitrate+Nitrite-N
167
mg/Kg - dry
102
1
04/2t/2114:46
7BD
450ONO3F-2011
Nickel
19.4
mg/Kg • dry
5.56
1
04/20/21 06:01
T)S
60100
Mercury
0.867
mg/Kg - dry
0.336
1
04/19/21 1L:16
DDO
SW-7471B
Selenium
<I1.1
mg/Kg • dry
11,1
1
04/20/21 06:01
T)S
6010D
PH
6.4
S.U.
1
04/21/21 16A7
CxC
90451)
Qualifiers/
Outside QC Limit
R
Analyte detected in blank
Definitions C
GCMS Confirmation Analysis
E
Result above cal range
g
GGA Outside QC Limits
H
Beyond holding time
I
Estimated value
M
Minimum value
NA
Not on Scope of Accreditation
NC
Not confirmed
Q
RPD >40% dual column results
T
Sample exhibits toxicity
U
Unconfirmed
Refer to cover letter.
Page 3 of 6

Waypoint
ANALYTICAL
46381
US Biosoiids Inc Project Belmont
Dennis Key
958 Hoots Road Information
Roaring River , NC 28669
7621 Whitepine Road, Richmond, VA 23237
Mains 804-743.9401 1 Fax [phone]
ww w.waypoin Ofialytical. corn
Report Date : 04/22/2021
qq Received : 04/14/2021
7awc �i G�oa+a/
Pauric Mc Groary Ph D CPA
Report Number : 21-104-0002 REPORT Of ANAL YSIS
Agronomist
Lab No : 75823 Matrix: Solids
Sample ID : Belmont Sampled: 4/13/2021 10:00
Test Results Units MQL DF pate 1 Time By Analytical
Analyzed Method
Ammonia Nitrogen
Aluminum
Arsenic
Cadmium
Chromium
Lead
Molybdenum
Analytical Method: SM-2540G
Test
Moisture
2220
mg/K9 - dry
2220
1
04/21/21 13:00
JP)
SM-4500-NH3C
50900
mg/Kg - dry
111
1
04/20/21 06:01
T}S
6010D
<11.1
mg/Kg - dry
11.1
1
04/20/21 06:01
TJS
6010D
<2.22
mg/Kg - dry
2.22
1
04/20/21 06:01
T]S
6010D
71.8
mg/Kg - dry
5.56
1
04/20/21 06:01
T]S
6010D
26.9
mg/Kg - dry
6.67
1
04/20/21 06:01
T]S
6010D
<5.56
mg/Kg - dry
5.56
1
04/20/21 06:01
T]S
6010D
Results Units MQL
95.5 % 0.010
DF Date 1 Time By Analytical
Analyzed Batch
1 04/26/21 16:53 FMM L547728
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 4 of 6

Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River. NC 28669
Receive Date: 04/0112021
Reported: 04/05/2021
For: Belmont
Comments: GEOMETRIC MEAN 1820 MPNig
Er 3�
AV
A I � L.
i_
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
210401-19-01
fecal Coliforms
81
1805
MPNIg
0410112021
MO
210401-19-01
Percent Solids
B1
1 34
°/,
sv:=ro
04101t2021
MD
210401-19-02
Fecal Coliforms
B2
576
MPNIg
04/01/2021
MO
210401-19-02
Percent Solids
B2
1 78
%
sM xa:}.b "
0410112021
MD
210401-19-03
Fecal Conforms
B3
1848
MPNIg
04101!2021
MO
210401.19-03
Percent Solids
63
2.42
%
04101;2021
MO
210401-19-04
Fecal Coliforms
B4
2698
MPNIg
04/0112021
MD
210401-19-04
Percent Solids
64
1 72
%
`Y77 11:w "
0410112021
MD
210401.19-05
Fecal Coliforms
65
4339
MPNIg
^
0410112021
MD
210401-19-05
Percent Solids
B5
1 71
%
04,0112021
MD
210401-19-06
Fecal Coliforms
B6
1839
MPNIg
5' `°'°''
04101!2021
MD
210401-19-06
Percent Solids
B6
1 74
°Io
04Vi 2021
MD
210401-19-07
Fecal Coliforms
B7
1600
MPNIg
'""'S"` "';,y;
04/01f2021
MD
210401-19-07
Percent Solids
B7
183
0410112021
MO
Respectfully submitted.
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 03/25/2021
Reported: 05/07/2021
For: BELMONT
Comments:
Sample Number parameter Sample ID Result Unit Method Analyzed Analyst
210325-22.01 30 Day Benchscale BELMONT
210325-22-01 TCLP BELMONT
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC90909
2.53 % EPA625-R-9210 03/25/2021 and
See Attached as NNw 0312612021 PACE
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Pagel of 32

Analytical Results
US BIOSOIIDS For: BEI-MOW
958 HOOTS RD
ROARING RIVER, NC 28669
Entered: 3/25/21
Reported: 5/7/21
Sample ID: 210325-22
PARAM E : Vector Attraction► Reduction/AerobicallyReduction/Aerobically Digested Sludge 130dayl
Total Solids
Volatile Solids
% Volatile Solids
Week
1
1.57
0.795
0.5064
Week
2
1.54
0.78
0.5065
Week
3
1.59
0.82
0.5157
Week
4
1.4
0 74 _..—..._._
0.5069
Wep,k
S
1.46
0.75
0.5137
Week
6
1.42
0.71
0.5000
Volatile Solids
Reduction:
0.5064 - 0,5000 X 100 =
0.5064 . (0.5064 X 0.5000)
2.53 %
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.# 440NC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 31 of 32

30 Day Bench Worksheet
Sample 1D # 210325-22-01
WEEK I
Samples
FTotal Solids
Volatile Solids
%-Volatile Fraction
1
_2.__.__
- 1.55
0,785
- -
1.59
0.8
3
1.58
0.8
Avera e:
1.57
_ 0.795
0.5064
WEEK 2
Samples Total Solids
l 1.55
Volatile Solids
0.78
-Fraction
2 �
0.78
3
0.78
-
0.5065
_ _I.54
Avera e: 1.54
-- 0.78
W--•,-EEK 3
Samples Total Solids Volatile Solids %Volatile Fraction
1 - --
�� 1 1.59 0.82
2 1.58 0.$1
3 1.60 0.83
_Average: 1.59 0.82 0.5157
WEEK 4
7Sam les Total Solids Volatile Solids % Volatile Fraction
-_
i 1.46 0.74
2 1.48
-- 3 1.43 0.74 1
Avera e: 1.46 _ 0.74 fl.SOb9
WEEK 5
Sam Total Solids Volatile Solids % Volatile Fraction
1_45 0.74L _
_ 2 _1.47._.-__- 0.76 -
3._ 1.46 0.75
Average: I 1.46 0.75 0.5137
WEEK 6
Sam les Total Solids
Volatilc Solids
% Volatile Fraction
l
0.71 -
2 g.41
0.71
3
0.72
----
Avera e•
0 -
0.5000 -
Van Kleeck Reduction: 0.5064 - 0.5000 X 100 = 0/0
0.5064 - ( 0.5064 X 0.5000)
Final Result: 2.53%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 32 of 32

/ ,!P 6Ana1y�/}ica(
J'
rr1r./eWllairee
ANALYTICAL RESULTS
Pace Aealyticel Services, LLC
9800 Hincey Ave Suite 100
Hu terwile. NC 28078
(704*75.9092
Project: US BEO BELMONT
Pace Project No.: 92529941
Sample: SE1,MONT"210325.22.01
Lab ID: 92529941001 Collected. 03125/21 12 15 Received, 03126/21 08.00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions,
Parameters
Results Unns Report Limit OF Prepared Analyzed
CAS No Quaff
Chlorinated Herb. (GC) 8151A
Analytical MethodEPA8151A Preparaton Method: 815iA
Leachate MelhodlOate 1311: 03130/21 t1:11 Initial pH, 5.57. Final pH: 4.87
Pace National - MI. Juliet
2A,5-TP{Silvex)
ND mglL 0-00200 1 0410112107:45 0410112120'04
93-72.1
2.4-D
NO mg/L 0.002DO 1 0410112107-46 04101!21 20:04
94-75-7
Surrogales
2A-OCAA(9)
101 % 14.0158 1 04,10112107.46 0410u212004
15719-28-9
8081 TCLP Pesticides RYE
Analytical Method, @PA 8081 B Preparation Method: EPA 3510C
Leachate MilthodlDate EPA 13il. 03129121 15�12 Initial pH.. Final pH 5
Pare Anatytical Services - Charloite
gamma-BHC (Lmdane)
NO ugfL 0.50 1 D410V21 10.24 N101121 17 11
58.89.9
Chlordane(Technical)
NO ug1L 3.3 1 0410f121 10:24 04101,121 17 it
57-74-9
Encinn
NO ng1L 0.5D 1 0410112110,24 04101/21 17'.11
72-20-8
Heptachlor
NO ugfL 0.50 1 0410112110:24 04101/21 17.11
76-44-8
Heptachlor epoxide
NO ugfL 0.50 1 04101I21 10'24 04101/21 17:11
1024.57.3
Methoxychw
NO ug1L 1000 1 0410112110:24 0410112117.)1
72-43.5
Toxaphene
NO ugfL 3.0 1 04101121 10:24 04/01!2t 17,11
8001-35-2
Surrogates
Decachlorobigbenyl(S)
67 % 10-154 1 04101121 10.24 0411 17.11
2051-24.3
Tetrachloro-m-xylene (S)
47 % 10-184 1 0410V21 10:24 04/01121 17.11
B77-09-8
B082 TCLP PCBs RVE
Analytical Method. EPA 8082A Preparation Method- EPA 3510C
Leachate MethudtOate. EPA 1311: 0312901 15,12 lniitas pW : Finai pH: 5
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 10161
NO ugA 1000 1 0410V21 10:24 04101121 2117
12674.11.2
Pi221 (Aroclor 1221)
NO ugil- 1000 1 04101,21 10:24 04101121 23:17
11104.28-2
PC8.1232 (Amcjw 1232)
NO uglL 1000 1 04101/21 10.24 D41DII21 23:17
11141-16-5
PCB-1242 (Aroclor 12421
NO ugfL 1000 1 04101121 10.24 0410V21 23-17
53469-21.9
PCB-1248 (ArOC4Or 1248)
NO ugfL 1000 1 04101,121 10.24 0410V21 2.3:17
12572-29-6
PCB-1254 (Aroc♦or 1254)
NO ugfL 1000 1 04/01121 1014 04101!21 23,17
11097-69.1
PCB-1260 (Arodor 1260)
NO ugll. 1000 1 0410101 10:24 DOOV21 73'17
11096-82-5
surrogates
Decaehlptobiphenyl(S)
72 % 10-161 1 04101Rt 10.24 04101/21 23:17
2051-24-3
6010 MET ICP. TCLP
Analytical Method EPA 60100 Preparation Melhod EPA 3010A
Leachate MethodlOate: EPA 1311; 03129121 15.03 lniliai pH: ; Final pH. 2
Pace Analytical Services - Asheville
Arserec
NO mgll- 0.050 1 03131f2t0t-32 03131121 1621
7440-38.2
Barium
NO mg1L 025 1 03131121 (W32 03131i21 1621
7440-39-3
Cadmium
NO mg1L 0.0050 1 OY31/2101 32 03)31121 16.21
7440-43-9
Chromium
NO 111g1L 0.050 1 03131121 01 32 03131/21 16.21
7440-47-3
Lead
ND ni 0,026 1 0313IJ2101:32 0313112116:21
7439-92-1
Selenium
NO rri 0.10 1 03131;21 0132 031311211621
7702-49-2
Silver
Np mg1L 0025 1 03131/21 DI 32 03131121 1621
7440-22-4
REPORT OF LABORATORY ANALYSIS
Tiffs remoi shall not he repraWced. except Vn full,
Date, 04120:2021 04,39 PM
wiUqut the written consem of Pace Analytical Services LLC
Page 5 fll 27
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 8 of 32

/ 2ceAnafAy iol
'J '
�ww.NCMMtuM1
ANALYTICAL RESULTS
Parse Analytical Sarvttos, I,LC
91100 Kinsey Ave. Suite 100
Huntersvllle. NC 28078
1704)875-9092
Proiad. US 810 BELMONT
Para Projecr No : 92529941
Sample: BELMONT•210325.22.01 LabtO: 92529941001 Gollectad: 0375121 12:15 Received_ 03/26/21 08-00 Matrix: ScIld
ResuNs reported on a "dry, weight' bests and are ad/usted !or percent moisture, sample size and arty dilutions.
Parameters Results Units Report Limit OF Prepared AnalyZed CAS No. Qua]
7470 Mercury, TCLP Analytical Method" EPA 7470A Preparaton Method: EPA 7410A
Leachate MethodiOate: EPA 1311. 03129/21 15:03 initial pH:: Final pm: 2
Pace Analytical Services - Asheville
Mercury ND mg1L 0,00020 1 03131121 09:57 0313W21 14 09 7439.97.6
9270E TCLP RYE
Analytical MethodEPA8270F Preparation Method EPA351DC
Leachate MelhodiOale: EPA 1311: 03129/21 15:12
Initial pH:. Final pH 5
Pace Analytical Services - Charlotte
1.4-Dlchlorohenzene
NO
ug/L
50.0
1
04105/21 10:06 04/06/21 11 30 106-46-7
2.4-Oinitrololuene
NO
ug1L
50.0
1
04105/21 10:06 04106/21 1i.30 121-14-2
Hexechloro-1,3-butadiene
NO
ug/L
50.0
1
0410501. 10:06 04106/21 1130 87-68-3
Hexachlorobenzene
NO
ug1L
so
1
04105721 10:06 04/06i21 11:30 118-74.1
HexacWoroethane
NO
ug/L
50.0
1
0410512110:06 04IM21 11.30 67.72-1
2-Methyiphenol(o-Cresot)
NO
ugh
50.0
1
04105t2110:06 G4106/21 11:30 95-48-7
3&4•Methy1phenol(m&p GresalI
NO
ug/L
50.0
1
04105/21 10.06 04/06121 11:30 15831.10-4
Nitrobenzene
NO
ug/L
50.0
1
04r05121 10:06 04106171 11:30 98-95.3
Penlachlorophenol
ND
ug1L
100
1
04105121 1006 04/06/21 41:30 87-86-5
Pyridine
NO
ugll
50.0
1
04105/21 10:06 04MI21 ti.30 110-86-1
2.4,5•Trichlorophenoi
ND
ugiL
50.0
1
04105/21 10-06 0410612111'30 95-95-4
2.4.6-Trichlorophenoi
ND
ug1L
50 0
1
04105/21 10,06 0410N21 11 30 88-06-2
Surrogates
Nitrobenzene-d5 (5)
59
%
10.144
1
04r05121 10:06 04106121 11.30 4165.60.0
2-Fluorobiphenyl (S)
48
%
10-130
1
04105/21 10:06 04106121 11 30 321-60-8
Terphenyl-d14 (S)
92
%
34-163
1
04105(21 10,06 04i06121 11 30 1718-51.0
Phenol-d6(S)
22
%
10.130
1
04105/2110:06 0"6121 t1:30 13127.88-3
2-FhrorophenolIS)
35
%
10-130
1
04i05121 10.06 04106121 t1.30 367-12.4
2.4,6-Tlituomophenol (S)
70
%
10.144
1
04105/21 10:06 04106121 11:30 118-79.6
82600 M8V TCLP
Analyticat Method: EPA 8260D Leachate MethodlDaw EPA 1311: 04/05/21 10:33
Pace Analytical Services - Charlotte
Benzene
NO
ug1L
100
20
04/06121 12A4 71-43-2
2-Bulanone (MEK)
NO
ugiL
200
20
04106121 12.44 76.93-3 IK
Carbon telrathloricia
N❑
ug/L
100
2C
04106121 12 44 56-2�5
Chlarobenzene
NO
u91L
100
20
Oa106121 t2A4 108-90.7
Ghtorotorm
NO
u91L
100
20
04106121 12.44 67-66-3
i 4-Dichlorobenzene
NO
ug/L
100
20
04/06121 12.44 106-46-7
1,2•Dichloroethane
NO
ugiL
100
20
04IM2112:44 107-06-2
1.1-Dichloroethene
NO
ugiL
1D0
20
0410612112.44 75,35.4
Tetrachloroethene
NO
ugiL
1D0
20
04/06121 12.44 127.184
Trichlaroethene
NO
ugiL
1DC
2D
0410612112:44 79.01.6
Vinyl chloride
NO
ug/L
1 D0
20
04t06121 12 44 75-01.4
Surrogates
1.2.Oichlorcetharte-d4 (8)
94
ob
70.130
20
04106121 12.44 17060-07-0
Tattlene-d6 (S)
115
%
67.135
20
04106121 12A4 2037,26.5
4-Sromotluoro0anZene (S)
102
56
70.130
20
04106121 12 44 460-00-4
REPORT
OF LABORATORY ANALYSIS
This report shall mil be reproduced, except n lot.
Date: 0412012021 04:39 PM
without the written consent of Pace Analytical
Services. UC Page 6 of 27
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 9 o132

e
1 ceAnalytical
� eFeRaeuts►uee
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersvrtle. NC 28018
17D4)67S9t192
P(Wd: US BIQ BELMONT
Pace Project No 92529941
Sample, REi.MUNT-210325,22.01
Lab ID: 92520941001 Collected_ 03/25121 12:15
Received 0306121 06:00 Matrix Solid
Results reported on a 'dry weight' basis and are adjusted for percent moisture. sample sirs and any dilutions.
Parameters
Results Units Report Limit OF
Prepared Analyzed
CAS No. Qual
Percent Mpleture
Analytical Method: SW-646
Pace Analytical Services - Chadade
Percent Moisture
95.7 '% 0.10 1
03129121 14.24
N2
9045 pH Solt
Analytical Method: EPA90451)
Pace Analytical Services - Asheville,
PH of 25 Degrees C
5.9 Sid. Units 0,10 1
04M2121 1323
H3
9095 paint Fitter Liquid Test
Analytical Malhod: EPA 9095E
Pace Analytical Services - Ashewite
Free Liquids
Fail 1.0 1
04/12/21 10:51
733C S Raaclive Cyanide
Analytical Method: EPA9014 Preparation Method: SW-646 7,3 3.2
Pace Analytical Services - Greensburg
Cyanide. Reactive
NO mglkg 23 3 1
03129.21 20:47 03130121 16 13
7348 Reactive Sulfide
Analytical Method SM 450062F-201 i Preparation Method SW-846 7-3 4 2
Pace AnslyliW Services - Greensturg
Sulfide, Reactive
NO nlglkg 233 1
03/29/21 20.47 03/29121 20,50
Sample: 13ELMONT-210325.22.01
LabID: 925299410D2 Collected 03125r21 1215
Received 03126121 06,00 Malrix:
Solid
Results reported an a 'dry weight" basis and are adjusted for percent moisture, sample size and any dilutiona-
Paramelers
Results Units Report Limit OF
Prepared Analyzed
CAS No. Quaff
9082 GCS PCs
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
PCB-1016(Atocior1016)
NO ug1Ag 46300 1
D411512109-32 041181211551
12674-11.2 11
PCB-1221 fArocior 1221)
NO vg11c9 46300 1
04115121 09:32 04/18/21 15.51
11104.28.2
PCB-1232 (Arodor 1232)
NO ug1Ag 46300 1
04/15/21 09:32 04/18121 1551
11141.16-5
PCB-1242 (Arodor 1242)
NO ugfkg 46300 1
04115t21 09:32 0411812$ 15,51
53469,21-9
PCB-1248 (Aioclor 1248)
ND u9/K9 46300 1
04115121 09.32 04/18/21 t5'51
12672-29-6
PCB-1254 (Arodlot 1254)
NO ug&g 46300 1
04115121 09:32 04/18/21 t5-51
11097•69.1
PC8-1260 (Aroclor 1260)
NO uglkg 46300 1
0405121 09.32 04118121 15 5t
11096-82-5 0
Surrogates
Derachlorobiphanyl(S)
t25 % 10-160 1
04115121 09.32 04118121 15:51
2051-24-3
Percent Moisture
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percenl Moisture
95.7 % 0.10 1
03129121 W 33
N2
REPORT OF LABORATORY ANALYSIS
Thro report Shall not be reprod�wed. except m Full.
Date04/20/2021 04:39 PM withoul the written senses of Pace Analytical Services. LLC. Page 7 of 27
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 10 of 32

Forest City
NCO025984

Waypoint, 7621 iVhitepinc Road, Richmond, VA 23237
fllfain 804-743-9401 � Fax [phone]
ANALYTICAL www.waypointana€yt;ceil.eam
46381
Southern Soil Builders Project Forest City
Dennis Key Report Date : 03/08/2021
958 Hoots Road Information : Received : 02/25/2021
Roaring River , NC 28669
Report Number : 21-056-0008
Lab No: 75080
Sample ID : Forest City
REPORT OF ANAL YSIS
�p1yIC r t Vto, Glrs/
Pauric Mc Groary Ph.D,, CPA
Agronomist
Matrix: Solids
Sampled: 2/24/2021 9:00
Test Results Units MQL DF Date / Time
Analyzed
By
Analytical
Method
Moisture 86.0 0.010 1 02/26/2115:54
FMM
SM-2540G
Test Results Units MQL DF Date 1 Time
By
Analytical
Analyzed
Method
Ammonia Nitrogen
<114
mg/Kg - dry
714
1
03/04/21 14:30
JPJ
SM-4500-NH3C
Nitrate+ Nitrite-N
B8.6
mg/Kg - dry
35.7
1
03/03/21 14:16
ZBD
450ONO3F-2011
Organic N
69200
mg/Kg - dry
1790
1
03/04/21 10:00
CALCULATION
pH
5.9
510.
1
03/03/2116:30
ADM
9045D
Total Solids
14.0
%
0.010
1
02/26/21 15:54
FMM
SM-254OG
Total Kjeldahl Nitrogen
69200
mg/Kg - dry
1790
1
03/04/21 10:00
JPJ -)M-4500-NH3C-TKh
Phosphorus
17600
mg/Kg - dry
35.7
1
03/04/21 08:07
]ADS
6010D
Aluminum
20000
mg/Kg - dry
35.7
1
03/05/21 01:09
JADS
60101)
Arsenic
<3.57
mg/Kg - dry
3.57
1
03/05/21 01:09
DADS
6010D
Calcium
11100
mg/Kg - dry
357
1
03/04/21 08:07
]ADS
6010D
Cadmium
1.51
mg/Kg - dry
0.714
1
03/04/21 08:07
]ADS
6010D
Chromium
42.1
mg/Kg - dry
1.79
1
03/04/21 08:07
JADS
6010D
Copper
260
mg/Kg - dry
3,52
1
03/05/21 19:21
JTR
6010D
Iron
19900
mg/Kg -dry
71.4
1
03/04/21 08:07
]ADS
6010D
Lead
65.4
mg/Kg - dry
2.14
1
03/04/21 08:07
JADS
6010D
Magnesium
2590
mg/Kg - dry
35.7
1
03/04/21 08:07
JADS
6010D
Manganese
425
mg/Kg - dry
3.57
1
03/04/21 08V
JADS
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quantitation Limit
Page 3 of 7

t:
W
���� ��,
7621. V+}hitePine Road, Richmond, VA23237
Main 804-743-9401
"Fax [phone]
ANALYTICAL
wr "Vwwaypointana[ytical-tom
46381
Southern Soil Builders
Project
Forest City
Dennis Key
Report Date ; 03/08/2021
958 Hoots Road
Information :
Received : 02/25/2021
Roaring River , NC 28669
Report Number : 21-056-0008
REPARTOFANALYSIS
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 75080
Matrix: Solids
Sample ID : Forest City
Sampled: 2/24/2021 9:00
Test
Results
Units
MQL
DF
Date / Time By Analytical
Analyzed Method
Mercury
2.77
mg/Kg - dry
0.101
1
03/02/21 16:37 DDB SW-74716
Molybdenum
6.31
mg/Kg - dry
1.79
1
03/04/21 08:07 ]ADS 60101)
Nickel
13.5
mg/K9 - dry
1.79
1
03/04/21 08:07 ]ADS 6010D
Potassium
3210
mg/Kg - dry
71.4
1
03/05/21 01:09 JADS 6010D
Selenium
8.64
mg/Kg - dry
3.57
1
03/05/21 19:21 JTR 6010D
Sodium
836
mg/Kg - dry
179
1
03/OS/21 01:09 ]ADS 6010D
Zinc
1050
mg/Kg - dry
8.93
1
03/04/21 08:07 ]ADS 6010D
Sulfur
7060
mg/Kg - dry
71.4
1
03/04/21 08:07 ]ADS 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 4 of 7

SAR
Sodium Absorption Ratio
Na M /L
Ca M /L
Mc
jjMg/L)
Na : Sodium (Mg/L) Equivalent weight: 23
117.04
1554
1 362.6
Ca: Calcium (MgIL) Equivalent weight: 20
Mg : Magnesium (MgIL) Equivalent weight: 12
Na (ME),
Ca (MEN
5.088696
77.7
30.21667
Milli Equivalent = Mg/L / Equivalent weight The amour
amount of i
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
Permitting
SAR = 0.692751 (From MgIL entered above)
SAR= 0(From ME entered below)
Na (ME)
1
Ca (ME)
Mg (ME]
5.1
77.7
30.2

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C
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t
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N
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Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 02/18/2021
Reported: 02/22/2021
For: FOREST CITY
Comments: GEOMETRIC MEAN: 180,401 MPNIg
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210218-16-01
Fecal Coliforms
F1
98940
MPNIg
SM92210E-2006
02/19/2021
MD
210218-16-01
Percent Solids
F1
14.2
%
SM254CB-2011
02/19/2021
MD
210218-16-02
Fecal Coliforms
F2
169014
MPNIg
SM92210E-2006
02/19/2021
MD
210218-16-02
Percent Solids
F2
14.2
%
SM25400-2011
02/19/2021
MD
210218-16-03
Fecal Coliforms
F3
633803
MPNIg
Sm92210E-2006
02/19/2021
MD
210218-16-03
Percent Solids
F3
14.2
%
SM2549B-2011
02/19/2021
MD
210218-16-04
Fecal Coliforms
F4
98592
MPNIg
sM92210E-2006
02/19/2021
MD
210218-16-04
Percent Solids
F4
14.2
%
SM2540e-2011
02/19/2021
MD
210218-16-05
Fecal Coliforms
F5
633803
MPNIg
SM92210E-2006
02/19/2021
MD
210218-16-05
Percent Solids
F5
14.2
%
SM25406-2011
02/19/2021
MD
210218-16-06
Fecal Coliforms
F6
167832
MPNIg
SM92210E-2006
02/19/2021
MD
210218-16-06
Percent Solids
F6
14.3
%
SM254OB-2011
02/19/2021
MD
210218-16-07
Fecal Coliforms
F7
55944
MPNIg
SM92210E-2006
02/19/2021
MD
210218-16-07
Percent Solids
F7
14.3
%
SM254CH-2011
02/19/2021
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Analytical Results
ANALYTICAL
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 05/11/2021
Reported: 06/21/2021
For: Forest City
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210511-29-01 30 Day Benchscale Forest City 3.3 % EPA625-R-9210 05/11/2021 MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 5

Analytical Results
US BIOSOLIDS For: Dallas
958 HOOTS RD
ROARING RIVER, NC 28669
Entered, 5/11/21
Reported: 6/21/21
Sample 11): 210511-29-02
PARAMETER: Vector Attraction Reduction LAgrobically Digested Sludge (30day)
Total Solids
Volatile Solids
% Volatile Solids
Week
1
1.87
0.94
0.5027
Week
2
1.94
0.98
0.5052
Week
3
1&5
0.91
0.4920
We
4
1.86
0.94
0.5054
Week
5
138
0.88
0,4944
Week
6
1.74
0.86
0.4943
Volatile Solids Reduction: 0.5027 - 0.4943 X10Q = 3.3%
0.5027 - (0.5027 X 0.4943)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.# 440NC
PO Box 228 - Statesville, NC 28687 - 704/872/4697
Page 4 of 5

30 Day Bench Worksheet
Sample ID # 10511- 9
WEEK 1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
I
1.89
0.95
2
1.87
0.93
_ 1.85
0.93
Avera e:
1.87
0.94
0.5027
WEEK 2
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.97
0.99
2
1.92
0.97
- -
3
1.92
0.98
Average :
1.94
0.98
0.5052
WEEK 3
Samples
Total Solids
Volatile Solids
, % Volatile Fraction
1
1.86
-:0 92
....._-- 2
_
1.84
0.91
3
1.84
_.
0.91
Avera e:
1.85
0.91
0.4920
WEEK 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.86
0.94
1.87
0.94 �I
3
E2
1.86
0.94
Avera e:
1.86
0.94
0.5054
WEEK 5
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.78 �
0.88
2
1.77
0.87
3
1.79
090-
1 Average:
1.78
0.88
0.4944
WEEK 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.74
0.86
2
1.74
0.86
---
3
1.75
0.86
Avera e:
1.74
0.86
0.4943
Van Kleeck Reduction: 0.5027 - 0.4943 X 100 = %
0.5027-(0.5027 X 0,4943)
Final Result: 3.3%
PO Sox 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 5

P I
Analytical Results "',,"A T E S V 1, L L E
1111,4, AL Y T f� C A L
U.S. Road
Inc
9158 Hoots 41
Bios,
Roaring River, NC 28669
Receive Date: 02/18/2021
Reported: 03/04/2021
For: FOREST CITY
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
210218-17-01 TCLP FC See Attached as Noted 02/19/2021 PACE
gzm=I• M!
Melissa Myers
NC Cert #440,
l I Mi I
m4goilmog
PO Box 228 * Statesville, NC 28687 * 704/872/4697
Paget of 31

Pace Analytical Services, LLC
Swo Kincey Ave. Suite 10o
Huntersville, NC 28078
virwapecdolls— (704)875-N92
ANALYTICAL RESULTS
Project: US. Biosolids Inc TCLP
Pace Project No.: 92523083
Sample: FC (210218-17.01) Lab la: 92523083001 Collected: 02118121 13:00 Received: 02119121 08:29 Matrix: Solid
Results reported an a "dry weight" basis and are adfusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual
Chlorinated Herb. (GC) 81S1A
Analytical Method: EPA 8151A Preparation Method: 8151A
Leachate Method/Date: 1311; 02/25121 16:44 Initial pH: 6.31; Final pH:4.87
Pace National - Mt. Juliet
2,4,5-TP (Silvex)
ND mg1L
0.00200 1
031=21 08:08 03104/21 00:05 93-72-1
2,4-D
ND mg/L
0.00200 1
03/02/21 08:08 03f04l2100:05 94-75-7
Surrogates
2,4-DCAA (S)
83.6 %
14.0-158 1
03/02/21 08:08 03IM21 00:05 19719-28-9
8081 TCLP Pesticides RVE
Analytical Method: EPA 80810 Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 02/22/21 15:48 Initial
pH: 5.74; Final pH: 5
Pace Analytical Services - Charlotte
gamma-BHC (Lindane)
ND ug/L
0.50 1
02/24121 10:08 02/25/21 07:24 58-89-9
Chlordane (Technical)
ND ug/L
3.0 1
02/24/21 10:08 02125/21 07:24 57-74-9
Endrin
NO ug/L
0.50 1
0212412110:08 02/2&210724 72-20-8
Heptachlor
ND ug/L
0.50 1
0212412110:08 02/25/21 07:24 76-44-0
Heptachlor epoxide
NO ug/L
0.50 1
02/24/21 10:08 02125/21 07:24 1024-57-3
Methoxychior
ND ug/L
1D00 1
02124/2110:08 02/25/2107:24 72-43-5
Toxapheno
NO ug/L
3.0 1
OD2412110:08 02125/2107:24 8001-35-2
Surrogates
Decachlorobiphenyl(S)
120 %
10-154 1
02124121 10:08 02/25/21 07:24 2051-24-3
Tetrachloro-m-xylene (S)
100 %
10-184 1
02/24121 10:08 02/25/21 07:24 8774)9-8
8082 GCS PCB
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016)
ND ugfkg
257 1
03102/21 11:21 03/02/21 15:14 12674-11-2
PGB-1221 (Aroclor1221)
ND uglkg
257 1
03/02/21 11:21 03102121 15:14 11104-28-2
PCB-1232 (Aroclor 1232)
ND uglkg
257 1
03f02/21 11:21 03102(21 15:14 11141-16-5
PCB-1242 (Aroclor 1242)
NO uglkg
257 1
03/02121 11:21 03102/21 15:14 53469-21-9
PCB-1248 (Aroclor 1248)
NO uglkg
257 1
03/02121 11:21 03102121 15:14 12672-29-6
PC$-1254 (Aroclor 1254)
ND uglkg
257 1
03102/21 11:21 03102121 15:14 11097-69-1
PCB-1260 (Aroclor 1260)
ND uglkg
257 1
03102121 11:21 03102/21 15:14 11096-82-5
Surrogates
Decachlorobiphenyl{$}
95 %
10-160 1
03102121 11:21 03/02/21 15:14 2051-24-3
8082 TCLP PCBs RVE
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Leachate MethodlDate: EPA 1311; 02/22/21 15:48 Initial pH: 5.74; Final pH: 5
Pace Analytical Services - Charlotte
PCB-1016 (Arodor 1016)
ND ug/L
1000 1
02/25121 06714 02125/21 17:45 12674-11-2
PCB-1221 (Aroclor 1221)
NO ug/L
1000 1
0212512106:14 02/25/21 17:45 11104-28.2
PCB-1232 (Arodor 1232)
NO ug/L
1000 1
02125/21 0614 02/25/21 17:45 11141-16-5
PCB-1242 (Arodor 1242)
N❑ ug/L
1000 1
02125/21 06:14 02/25/21 17:45 53469-21-9
PCB-1248 (Arodor 1248)
NO ug/L
1000 1
02125121 06:14 02/25/21 17:45 12672-29-6
PC13-1254 (Aroclor 1254)
ND ug/L
1000 1
02/25121 06:14 02125/21 17:45 11097.69-1
PCB-1260 (Arodor 1260)
ND ug/L
1000 1
02125121 06:14 02125/21 17:45 11096-82-5
Surrogates
Decachlorobiphenyl (S)
79 %
10-181 1
02/25/21 06:14 02125/21 17A5 2051-24-3
REPORT OF LABORATORY
ANALYSIS
This report sharl not be reprofloced, except
in full,
Date: 03104/2021 02:53 PM
without the written consent of
Pace Analytical Services. LLC.
Page 5 of 28
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 8 of 31

Pace Analytical Services, LLC
Ctlu,y_{� a 9800 Kincey Ave. Sude 100
�A
G" ""Hunterswlle, NC 28078
(704W7 -M2
i
ANALYTICAL RESULTS
Project. US. Biosotids Inc TCLP
Pace Project No.: 92523083
Sample: FC (210218-17-01) Lab ID: 92523083001 Collected: 02tlat21 13:00 Received: 02/19/21 08:29 Matrix: Solid
Results reported on a 'dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6010 MET ICR TCLP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 02/22121 15:37
Initial pH; 5-71: Final pH: 2
Pace Analytical Services -Asheville
Arsenic
NO mg1L
0.050
1
02/24/21 02:14 02124/2112705 7440-38-2
Barium
NO M91L
0.25
1
02/2412102:14 02/24/2112:05 7440-39-3
Cadmium
NO mg1L
0.0050
1
0212412102:14 0212412112:05 7440-43-9
Chromium
NO m91L
0.050
1
02/24/21 02:14 0212412112:05 7440-47-3
Lead
NO mg1L
0.025
1
02124/2102:14 0212412112:05 7439.92-1
Selenium
ND mg1L
0.10
1
02/24/2102714 02/24/21 12:05 7782-49-2
Silver
NO mg1L
0-025
1
0212412102:14 02/24/21 12:05 7440-22.4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
Leachate Method/Date: EPA 1311; 02/22121 15:37
Initial pH: 5.71; Final pH: 2
Pace Analytical Services -Asheville
Mercury
NO mg/L
0.00020
1
02/2412109:57 02/2512111:51 7439-97-6
8270E TCLP RVE
Analytical Method: EPA 8270E Preparation Method. EPA 3510C
Leachate Method/Date: EPA 1311; 02122/21 15:48
Initial pH: 5.74; Final pH: 5
Pace Analytical Services - Charlotte
1,4-Dichlorobenzene
NO ug/L
50.0
1
0212412108:17 0212412120:62 10646-7
2,4-Dinitrotoluene
ND ug/L
50.0
1
0212412108:17 02124/2120:52 121-14-2
Hexachloro-1,3-butadiene
ND uglL
50.0
1
0212412108:17 02/24/2120:52 87-68-3
Hexachlorobenzene
NO uglL
50.0
1
0212412108A7 02/24/2120:52 118-74-1
Hexachloroethane
NO ug1L
50.0
1
02/24M 08:17 02124121 20:52 67-72-1
2-Methylphenol(o-Cresol)
NO ug/L
50.0
1
02/24/21 08A7 02/2412120:52 9548-7
3&4-Methylphenot(m&p Cresol)
NO ug/L
50.0
1
0212412l 08:17 02/24121 20:52 15831-10-4
Nitrobenzene
NO ug/L
50.0
1
02/24/21 08:17 02/2412120:52 98-95-3
Pentachlorophenol
NO ug/L
100
1
02/24/21 08:17 02/24/2120:52 87-86-5
Pyridine
NO ug/L
50.0
1
02/24/2108:17 02124/2120:52 110-Wl
2,4,5•Trichlorophenol
ND ug/L
50.0
1
0212412108:17 02Q412120:52 95-95-4
2,4,6-Trichlorophenol
NO ug/L
50.0
1
OZ24/2108:17 0212412120:52 88.06-2
Surrogates
Nitrobenzene-d5 (5)
71 %
10-144
1
02/24/21 08:17 02/24/21 20:52 4165-60-0
2-Fluorobiphenyt (S)
65 %
10.130
1
02124121 08:17 02/24/21 20:52 321-60-8
Terphenyl-d14 (S)
110 %
34-163
1
02/24121 08:17 02/24/21 20:52 1718-51.0
PhenoW6 (S)
36 %
10-130
1
02124/21 08:17 02)24/21 20:52 13127-88-3
2-Fluorophenol (S)
48 %
10-130
1
02124/21 08:17 02/24/21 20:52 367-12-4
2,4,6-Tribromophenol (S)
70 %
10-144
1
02/24121 08:17 02/24/21 20:52 118-79-6
8260D MSV TCLP
Anslytirat Method: EPA 8260D Leachate MethodlDete: EPA 1311; 02124/21 12:55
Pace Analytical Services - Charlotte
Benzene
NO ug/L
100
20
02125121 20:38 71-43-2
2-Butanone (MEK)
NO uglL
200
20
02125121 20:38 78-93-3
Carbon tetrachloride
NO uglL
100
20
02125121 20-38 56-23-5
Chlorobanzene
NO ug/L
100
20
02/25/2120:38 108-90-7
Chloroform
NO ug/L
100
20
02/26/2120:38 67-66-3
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 03104/2021 02:53 PM
without the written consent of PacoAnalylical Serwaes. LLC.
Page 6 of 28
PO Box 228 • Statesville, NC 28687 a 704/872/4697
Page 9 of 31

(�'G)eAa
WW4*Kdd*MN
ANALYTICAL RESULTS
Project: US. Siosolids Inc TCLP
Pace Project No.: 92523083
Pap Anallrecal Services, LLC
9800 IOncey Ave. Suite 100
Huniersville, NC 28078
[phone]
Sample: FC (210218.17-01) Lab ID: 92523083001 Collected: 02/18/21 13:00 Received: 02119121 0829 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Resutts Units Report Limit OF Prepared Analyzed CAS No. Qual
8260D MSY TCL.P
Analytical Method: EPA 8260D Leachate Method/Date: EPA 1311; 02124/21 12:55
Pace Analytical Services - Charlotte
1.4-Dich4orobenzene
NO ug/L 100
20
02125/2120:38 106-46-7
1,2-Dtchloroethane
ND ug1L 100
20
02/25/2120:38 107-06-2
1,1-Dichloroethene
NO ug1L 100
20
0212512120:38 75.35-4
Tetrachloroethene
ND ug/L 100
20
02125/2120:38 127-18-4
Trichloroethene
ND ug/L 100
20
02/25/2120:38 79-01.6
Vinyl chloride
NO ug/L 100
20
02/25/21 20:38 75-014
Surrogates
1,2-Dichloroethane-d4 (S)
101 % 70-130
20
02/25/21 20:38 17060-07-0
Toluene-d8 (S)
99 % 67-135
20
02125/21 20:38 2037-26-5
4-Bromofluorobenzene (S)
96 % 70.130
20
02/25/21 20:38 460-00-4
Percent Moisture
Analytical Method: SW446
Pace Analytical Services - Charlotte
Percent Moisture
87.4 % 0.10
1
02/19/21 16:40 N2
1010 Flashpoint Ctosed Cup
Analytical Method: EPA 1010A
Pace Analytical Services - Asheville
Flashpoint
>200 deg F 70-0
1
03/02/21 09:59
9045 ph Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.4 Std. Units 0.10
1
03/01121 16:07 H3
9095 Paint Filter Liquid Test
Analytical Method: EPA 90956
Pace Analytical Services -Asheville
Free Liquids
Pass 1.0
1
02/22/21 10:45
733C S Reactive Cyanide
Analyticat Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Pace Analytical Services - Greensburg
Cyanide, Reactive
NO mg/kg 7.9
1
02124121 19:56 02/25/21 20:16
734S Reactive Sulfide
Analytical Method: SM 4500S2F-2011 Preparation Method: SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive
ND mg/kg 78.6
1
02/24/21 19:56 02124121 19:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full,
Date: 03/0412021 02:53 PM without the written consent of Pace Analytical Services. LLC. Page 7 of 28
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 10 of 31

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