WQ0032723_Residual Annual Report 2021_20220228

Initial Review
Reviewer
EADS\ndthornburg
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0032723
ApplicantlPermittee City of Reidsville
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Brent Collins
Email Address*
[e-mail]
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
336-399-3646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Perm it Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number: *
WQ0032723
Has Current Existing permit number
Applicant/Permittee Address*
1100 Vance Street, Reidsville NC 27320
Facility Name*
City of Reidsville Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2021 Reidsville WTP Annual Report - WO0032723.pdf 9.15MB
Upload only 1 PDF document (less than 250 Me). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/28/2022

MA
--Resources, Inc.
February 28, 2022
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2021 Annual Report — Reidsville WTP
Treatment and Land Application of Residuals
Permit No. WQ0032723
Dear Sir or Madam:
Enclosed is one copy of the 2021 Annual Report for the above referenced land
application permit.
During 2021 EMA Resources, Inc. land applied 111.74 dry tons of wastewater residuals
to 57 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Brent Collins
Director of Technical Services
[e-mail]
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

IMA
-.-Resources, Inc.
City of Reidsville WTP
2021 Annual Report
Residuals Land Application
Permit No. WQ0032723
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0032723 FACILITY NAME:
PHONE:
Reidsville WTP
COUNTY: Rockingham
OPERATOR:
City of Reidsville
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
El Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year?
Yes 0 No ❑ -* If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
June
July
August
September
October
November
December
Total from FORM DMSDF (sup)
0
111.74
111.74
111.74
Totals:
Annual (dry tons):
0
111.74
111.74
111.74
Amendment(s) used:
Bulking Agent(s) used:
DMSDF (Supp)
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form
0
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit
(including but not limited to items 1-3 below) issued by the Division of Water Quality:
O Yes
❑ No If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Jam1mrel- hind v (
Summer Woodard (Feb 28, 202210:01 EST)
Signature of Permittee
Feb 28, 2022
C. S0tt7ewe1G
C. Scott Jewell (Feb 24, 2022 15:28 EST)
Date Signature of Preparer**
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Feb 24, 2022
Date
DENR FORM DMSDF (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: WQ0032723 FACILITY NAME:
PHONE:
COUNTY:
City of Reidsville WTP
Rockingham
OPERATOR: City of Reidsville
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
September
City of Reidsville WTP
111.74
111.74
Ronnie Marshall
111.74
Soil Amendment
Totals:
Annual (dry tons):
0
111.74
111.74 111.74
Amendment(s) used:
Bulking Agent(s) used:
DMSDF (Supp)
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form
1
DENR FORM DMSDF (Supp) (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
WQ0032723 Laboratory: 1) Waypoint Analytical
Reidsville WTP
NC0046345
Reidsville WTP
2)
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
(mg/kg),
Sample or Composite Date
9/15/21
Percent Solids (%)
NA
4.25
Arsenic
75
12.4
Cadmium
85
0.476
Copper
4,300
226
Chromium
NA
41
Lead
840
18.5
Mercury
57
0.155
Molybdenum
75
3.21
Nickel
420
18.7
Selenium
100
7.62
Zinc
7,500
67.9
Total Phosphorus
NA
1350
TKN
NA
13500
Ammonia -Nitrogen
NA
793
Nitrate and Nitrite
NA
652
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
C. t �s'z z 7eweGG
C. Scott Jewell (Feb 24, 2022 15:28 EST)
Signature of Preparer *
Feb 24, 2022
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
Facility Name:
Residual Source
NPDES # or WQ#:
WWTP Name:
WQ0032723 Laboratory: 1) Waypoint Analytical
Reidsville WTP
NC0046345
Reidsville WTP
Residual Analysis Data
2)
3)
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
9/15/21
Aluminum
119000
Calcium
1060
Magnesium
1690
pH
6.8
Potassium
1570
Sodium
402
PAN
2319
SAR
0.37
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
C. t �sort 7eweGG
C. Scott Jewell (Feb 24, 2022 15:28 EST)
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Feb 24, 2022
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
City of Reidsville - WTP Total Dry Tons Applied (Annual):
WQ0032723
Cation Exchange Capacity (non 503 only):
23.04
Operator: Auman French Owner: State of North Carolina Predominant Soil Series: RnB
Acres Used:
5.19 Acres Permitted:
5.19 Site #: RC140 Field #:
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 I
2
3
1 4
1 5
1 6
1 7
1 8
1 9
110
111
112
9/15/21
% Solids
4.25
Arsenic
I 2.4
Cadmium
0.476
Copper
226
Chromium
41
Lead
18.5
Mercury
0.155
Molyb-
denum
3.21
Nickel
18.7
Selenium
7.62
Zinc
67.9
Total
Phos-
phorus
1350
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
App.
Event
1
2I
3
4
5
6
7
II
9
10
12
Totals:
4.44
Arsenic
0.110
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.110
Cadmium
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
2.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.006
Chromium
0.364
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.364
Lead
0.164
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.164
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
denum
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Nickel
0.166
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.166
Selenium
0.068
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.068
Zinc
0.603
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.603
Total
Phos-
phorus
11.985
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.985
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/10/2022
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville - WTP WQ Permit #: WQ0032723 Field #: 1
Land Owner: State of North Carolina Annual Dry Tons Applied: 23.04 Site #: RC 140
Operator: Auman French
Crop 1 Name:
Fescue -Hay
Predominant Soil Series:
Acres Utilized:
Acres Permitted:
5.19
5.19
RnB Cation Exchange Capacity (non 503): 0
Crop 1 Max. PAN: 167
Crop 2 Name:
Crop 2 Max. PAN:
Date or
Month
Volume
enter one)Solids/
Liquid
Cu. Yds
applied
Gallons
%
Solids
Volume
Appliedper
pP
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
Application
Method*
Volatilization
Rate**
Mineralizatio
n Rate***
TKN
mg/kg
Ammonia 'Z
rn
Nitrogen
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/14
84500
4.25
2.885
Reidsville WTP
Dry
<.5"
S
0.5
0.1
13500
793
652
13.384
NA
Wheat
9/15
45500
4.25
1.554
Reidsville WTP
Dry
<.5"
S
0.5
0.1
13500
793
652
7.207
NA
Wheat
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
0
130000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
20.591
0.000
Lime Applied
Annual lbs/acre
0.110
0.004
2.006
0.364
0.164
0.001
0.028
0.166
0.068
0.603
11.985
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.110
0.004
2.006
0.364
0.164
0.001
0.028
0.166
0.068
0.603
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1st/2nd Crop
167
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
2/10/2022
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
City of Reidsville - WTP Total Dry Tons Applied (Annual):
WQ0032723
Cation Exchange Capacity (non 503 only):
18.66
Operator: Auman French Owner: State of North Carolina Predominant Soil Series: RnB
Acres Used:
7.33 Acres Permitted:
7.33 Site #: RC 140 Field #:
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 I
2
3
1 4
1 5
1 6
1 7
1 8
1 9
I10
111
1.12
9/15/21
Uniti
4/13/21
% Solids
4.25
2.04
Arsenic
12.4
12
Cadmium
0.476
1
Copper
226
198
Chromium
41
63
Lead
18.5
85.5
Mercury
0.155
0.413
Molyb-
denum
3.21
6.75
Nickel
18.7
13.1
Selenium
7.62
16
Zinc
67.9
760
Total
Phos-
phorus
1350
4870
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
App.
Event
1
2
1.13
3
4
5
6
7
II
9
10
12
Totals:
1.41
Arsenic
0.035
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.062
Cadmium
0.001
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.639
0.448
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.087
Chromium
0.116
0.143
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.259
Lead
0.052
0.194
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.246
Mercury
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
denum
0.009
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Nickel
0.053
0.030
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.083
Selenium
0.022
0.036
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.058
Zinc
0.192
1.721
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.913
Total
Phos-
phorus
3.818
11.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
14.843
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/10/2022
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville - WTP WQ Permit #: WQ0032723 Field #: 2
Land Owner: State of North Carolina Annual Dry Tons Applied: 18.66 Site #: RC 140
Operator: Auman French Predominant Soil Series:
Crop 1 Max. PAN: 95
Crop 1 Name:
Wheat
RnB
Crop 2 Name:
Acres Utilized:
Acres Permitted:
7.33
7.33
Cation Exchange Capacity (non 503): 0
Small Grain Crop 2 Max. PAN:
50
Date or
Month
Volume
enter one)Solids/
Liquid
Cu. Yds
applied
Gallons
%
Solids
Volume
Appliedper
pP
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
Application
Method*
Volatilization
Rate**
Mineralizatio
n Rate***
TKN
mg/kg
Ammonia 'Z
rn
Nitrogen
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/15
58500
4.25
1.414
Reidsville WTP
Dry
<.5"
S
0.5
0.1
13500
793
652
6.561
NA
Wheat
12/2
97500
2.04
1.132
Unifi
Dry
<.5"
S
0.5
0.3
17000
5550
760
Na
15.774
SG
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
0
156000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
6.561
15.774
Lime Applied
Annual lbs/acre
0.062
0.004
1.087
0.259
0.246
0.001
0.024
0.083
0.058
1.913
14.843
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.062
0.004
1.087
0.259
0.246
0.001
0.024
0.083
0.058
1.913
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1st/2nd Crop
95
50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
2/10/2022
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
City of Reidsville - WTP Total Dry Tons Applied (Annual):
WQ0032723
Cation Exchange Capacity (non 503 only):
19.26
Operator: Auman French Owner: State of North Carolina Predominant Soil Series: RnB
Acres Used:
5.2 Acres Permitted:
5.2 Site #: RC 140 Field #:
3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 I
2
3
1 4
1 5
1 6
1 7
1 8
1 9
110
111
112
9/15/21
Uniti
4/13/21
% Solids
4.25
2.04
Arsenic
12.4
12
Cadmium
0.476
1
Copper
226
198
Chromium
41
63
Lead
18.5
85.5
Mercury
0.155
0.413
Molyb-
denum
3.21
6.75
Nickel
18.7
13.1
Selenium
7.62
16
Zinc
67.9
760
Total
Phos-
phorus
1350
4870
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
App.
Event
1
2
1.49
3
4
5
6
7
II
9
10
12
Totals:
2.22
Arsenic
0.055
0.036
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.091
Cadmium
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
1.001
0.590
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.591
Chromium
0.182
0.188
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.369
Lead
0.082
0.255
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.337
Mercury
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
denum
0.014
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Nickel
0.083
0.039
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.122
Selenium
0.034
0.048
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.081
Zinc
0.301
2.263
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.564
Total
Phos-
phorus
5.981
14.503
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
20.483
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/10/2022
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville - WTP WQ Permit #: WQ0032723 Field #: 3
Land Owner: State of North Carolina Annual Dry Tons Applied: 19.26 Site #: RC 140
Operator: Auman French
Crop 1 Name:
Wheat
Predominant Soil Series:
Crop 1 Max. PAN: 95
RnB
Crop 2 Name:
Acres Utilized:
Acres Permitted:
5.2
5.2
Cation Exchange Capacity (non 503): 0
Small Grain Crop 2 Max. PAN:
50
Date or
Month
Volume
enter one)Solids/
Liquid
Cu. Yds
applied
Gallons
%
Solids
Volume
Appliedper
pP
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
Application
Method*
Volatilization
Rate**
Mineralizatio
n Rate***
TKN
mg/kg
Ammonia 'Z
rn
Nitrogen
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/15
65000
4.25
2.215
Reidsville WTP
Dry
<.5"
S
0.5
0.1
13500
793
652
10.276
NA
Wheat
12/4
71500
2.04
1.170
Unifi
Dry
<.5"
S
0.5
0.3
17000
5550
760
Na
16.305
SG
12/7
19500
2.04
0.319
Unifi
Dry
<.5"
S
0.5
0.3
17000
5550
760
Na
4.447
SG
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
0
156000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
10.276
20.752
Lime Applied
Annual lbs/acre
0.091
0.005
1.591
0.369
0.337
0.002
0.034
0.122
0.081
2.564
20.483
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.091
0.005
1.591
0.369
0.337
0.002
0.034
0.122
0.081
2.564
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1st/2nd Crop
95
50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
2/10/2022
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
City of Reidsville - WTP Total Dry Tons Applied (Annual):
WQ0032723
Cation Exchange Capacity (non 503 only):
26.59
Operator: Auman French Owner: State of North Carolina Predominant Soil Series: RnB
Acres Used:
9.28 Acres Permitted:
9.28 Site #: RC 140 Field #:
4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 I
2
3
1 4
1 5
1 6
1 7
1 8
1 9
110
111
112
9/15/21
Uniti
4/13/21
% Solids
4.25
2.04
Arsenic
12.4
12
Cadmium
0.476
1
Copper
226
198
Chromium
41
63
Lead
18.5
85.5
Mercury
0.155
0.413
Molyb-
denum
3.21
6.75
Nickel
18.7
13.1
Selenium
7.62
16
Zinc
67.9
760
Total
Phos-
phorus
1350
4870
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
App.
Event
1
2
1.25
3
4
5
6
7
II
9
10
12
Totals:
1.61
Arsenic
0.040
0.030
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Cadmium
0.002
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Copper
0.730
0.495
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.225
Chromium
0.132
0.158
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.290
Lead
0.060
0.214
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.274
Mercury
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
denum
0.010
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Nickel
0.060
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.093
Selenium
0.025
0.040
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
Zinc
0.219
1.902
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.121
Total
Phos-
phorus
4.358
12.185
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
16.543
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/10/2022
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Reidsville - WTP WQ Permit #: WQ0032723 Field #: 4
Site #: RC 140
State of North Carolina
Auman French
Crop 1 Name:
Wheat
Annual Dry Tons Applied: 26.59
Predominant Soil Series:
Crop 1 Max. PAN: 95
Acres Utilized:
Acres Permitted:
RnB Cation Exchange Capacity (non 503):
Crop 2 Name: Small Grain Crop 2 Max. PAN:
9.28
9.28
0
50
Date or
Month
Volume
enter one)Solids/
Liquid
Cu. Yds
applied
Gallons
%
Solids
Volume
Appliedper
pP
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
Application
Method*
Volatilization
Rate**
Mineralizatio
n Rate***
TKN
mg/kg
Ammonia 'Z
rn
Nitrogen
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/16
84500
4.25
1.614
Reidsville WTP
Dry
<.5"
S
0.5
0.1
13500
793
652
7.485
NA
Wheat
12/4
65000
2.04
0.596
Unifi
Dry
<.5"
S
0.5
0.3
17000
5550
760
Na
8.306
SG
12/6
71500
2.04
0.655
Unifi
Dry
<.5"
S
0.5
0.3
17000
5550
760
Na
9.137
SG
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
0
221000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
7.485
17.443
Lime Applied
Annual lbs/acre
0.070
0.004
1.225
0.290
0.274
0.002
0.027
0.093
0.065
2.121
16.543
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.070
0.004
1.225
0.290
0.274
0.002
0.027
0.093
0.065
2.121
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1st/2nd Crop
95
50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
2/10/2022
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
City of Reidsville - WTP Total Dry Tons Applied (Annual):
WQ0032723
Cation Exchange Capacity (non 503 only):
65.10
Operator: Auman French Owner: State of North Carolina Predominant Soil Series: CdB2
Acres Used:
30 Acres Permitted:
30 Site #: RC 140 Field #:
5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 I
2
3
1 4
1 5
1 6
1 7
1 8
1 9
I10
111
1.12
9/15/21
Uniti
4/13/21
% Solids
4.25
2.04
Arsenic
12.4
12
Cadmium
0.476
1
Copper
226
198
Chromium
41
63
Lead
18.5
85.5
Mercury
0.155
0.413
Molyb-
denum
3.21
6.75
Nickel
18.7
13.1
Selenium
7.62
16
Zinc
67.9
760
Total
Phos-
phorus
1350
4870
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
App.
Event
1
2
0.44
3
4
5
6
7
II
9
10
12
Totals:
1.73
Arsenic
0.043
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
Cadmium
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
0.781
0.175
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.956
Chromium
0.142
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.197
Lead
0.064
0.076
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.140
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
denum
0.011
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Nickel
0.065
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.076
Selenium
0.026
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.040
Zinc
0.235
0.672
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.907
Total
Phos-
phorus
4.666
4.305
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.971
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
2/10/2022
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Reidsville - WTP WQ Permit #: WQ0032723 Field #: 5
Land Owner: State of North Carolina Annual Dry Tons Applied: 65.10 Site #: RC140
Operator: Auman French
Crop 1 Name:
Fescue -Hay
Predominant Soil Series:
Acres Utilized:
Acres Permitted:
30
30
CdB2 Cation Exchange Capacity (non 503): 0
Crop 1 Max. PAN: 209
Crop 2 Name:
Crop 2 Max. PAN:
Date or
Month
Volume
enter one)Solids/
Liquid
Cu. Yds
applied
Gallons
%
Solids
Volume
Appliedper
pP
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry, Wet,
Moist)
Precip.
Past 24
Hrs.
inches
Application
Method*
Volatilization
Rate**
Mineralizatio
n Rate***
TKN
mg/kg
Ammonia 'Z
rn
Nitrogen
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
9/20
123500
4.25
0.730
Reidsville WTP
Dry
<.5"
S
0.5
0.1
13500
793
652
3.384
NA
Fescue
9/21
39000
4.25
0.230
Reidsville WTP
Dry
<.5"
S
0.5
0.1
13500
793
652
1.069
NA
Fescue
9/22
130000
4.25
0.768
Reidsville WTP
Dry
<.5"
S
0.5
0.1
13500
793
652
3.562
NA
Fescue
12/7
156000
2.04
0.442
Unifi
Dry
<.5"
S
0.5
0.3
17000
5550
760
6.166
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
0
448500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
14.181
0.000
Lime Applied
Annual lbs/acre
0.053
0.003
0.956
0.197
0.140
0.001
0.017
0.076
0.040
0.907
8.971
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.053
0.003
0.956
0.197
0.140
0.001
0.017
0.076
0.040
0.907
Permitted C. P. L. R.****
36
34
1338
267
15
374
89
2498
Permit PAN Limit 1 st/2nd Crop
209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
2/10/2022
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypoint
ANALYTICAL
9/23/2021
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 21-259-0173
Client Project Description: Reidsville, NC
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on
The above referenced project has been analyzed
accordance with the applicable analytical method
stage (refer to the chain of custody) results apply
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° fax [phone]
www.waypointanalytical.com
9/16/2021 for the analyses presented in the following report.
per your instructions. The analyses were performed in
. Where the laboratory was not responsible for the sampling
to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '--' symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Ca,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

Waypoint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointa nalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
Alabama State Program 40750 02/28/2022
Arkansas State Program 88-0650 02/07/2022
California State Program 2904 06/30/2022
Florida State Program - NELAP E871157 06/30/2022
Georgia State Program C044 02/18/2023
Georgia State Program 04015 06/30/2022
Illinois State Program - NELAP 200078 10/10/2022
Kentucky State Program 80215 06/30/2022
Kentucky State Program KY90047 12/31/2021
Louisiana State Program - NELAP LA037 12/31/2021
Louisiana State Program - NELAP 04015 06/30/2022
Mississippi State Program MS 02/11/2023
North Carolina State Program 415 12/31/2021
Pennsylvania State Program - NELAP 68-03195 05/31/2022
South Carolina State Program 84002 06/30/2022
South Carolina State Program 84002 06/30/2022
Tennessee State Program 02027 02/11/2023
Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021
Texas State Program - NELAP T104704180 09/30/2021
Virginia State Program 00106 06/30/2022
Virginia State Program - NELAP 460181 09/14/2022
Page 1 of 1 00001/21-259-0173
Page 2 of 7

Waypoint
ANALYTICAL
Report Number: 21-259-0173
Client Project Description: Reidsville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointa nalytical. com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received
88586 Reidsville WTP Solids 09/15/2021 07:45 09/16/2021
Page 3 of 7

Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville , NC 27028
Report Number : 21-259-0173
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointa nalytical. cam
Project Reidsville, NC
Information :
REPORT OF ANALYSIS
Report Date : 09/23/2021
Received : 09/16/2021
49-Qc� (»-)9
Danyale Love
Project Manager
Lab No : 88586 Matrix: Solids
Sample ID : Reidsville WTP Sampled: 9/15/2021 7:45
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Moisture 95.8 % 0.010 1 09/21/21 15:58 FMM SW-DRYWT
Ammonia Nitrogen 793 ] mg/Kg - dry 381 2380 1 09/22/21 12:00 JPJ 4500NH3C-2011
Nitrate+Nitrite-N 652 mg/Kg - dry 116 116 1 09/23/21 14:52 ZBD 4500NO3F-2011
Organic N 12660 ] mg/Kg - dry 381.0 2381 1 09/21/21 10:00 DH CALCULATION
pH 6.8 s.u. 1 09/21/21 15:07 DRS 9045D
Total Solids 4.25 % 0.010 0.010 1 09/21/21 15:58 FMM 2540G-2011
Total Volatile Solids 29.7 % 0.010 0.010 1 09/21/21 15:58 FMM 2540G-2011
Total Kjeldahl Nitrogen 13500 mg/Kg - dry 238 5950 1 09/21/21 10:00 JPJ iM-4500-NH3C-TKO
Phosphorus 1350 mg/Kg - dry 65.7 119 1 09/23/21 01:44 JTR 6010D
Aluminum 119000 mg/Kg - dry 110 119 1 09/23/21 01:44 JTR 6010D
Arsenic 12.4 mg/Kg - dry 5.71 11.9 1 09/23/21 01:44 JTR 6010D
Cadmium <0.476 mg/Kg - dry 0.476 2.38 1 09/23/21 01:44 JTR 6010D
Calcium 1060 ] mg/Kg - dry 921 1190 1 09/23/21 01:44 JTR 6010D
Chromium 41.0 mg/Kg - dry 5.62 5.95 1 09/23/21 01:44 JTR 6010D
Copper 226 mg/Kg - dry 7.38 11.9 1 09/23/21 01:44 JTR 6010D
Iron 38600 mg/Kg - dry 203 238 1 09/23/21 01:44 JTR 6010D
Lead 18.5 mg/Kg - dry 4.29 7.14 1 09/23/21 01:44 JTR 6010D
Magnesium 1690 mg/Kg - dry 61.4 119 1 09/23/21 01:44 JTR 6010D
Manganese 8640 mg/Kg - dry 7.74 11.9 1 09/23/21 01:44 JTR 6010D
Mercury <0.155 mg/Kg - dry 0.155 0.355 1 09/20/21 13:46 TJS 7471A
Molybdenum <3.21 mg/Kg - dry 3.21 5.95 1 09/23/21 01:44 JTR 6010D
Nickel 18.7 mg/Kg - dry 2.86 5.95 1 09/23/21 01:44 JTR 6010D
Potassium 1570 mg/Kg - dry 147 238 1 09/23/21 01:44 JTR 6010D
Qualifiers/
Definitions
DF Dilution Factor J Estimated value
L Limit Exceeded MQL Method Quantitation Limit
Page 4 of 7

Waypoint.
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Road
Mocksville , NC 27028
Report Number : 21-259-0173
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointa nalytical. cam
Project Reidsville, NC
Information :
REPORT OF ANALYSIS
Report Date : 09/23/2021
Received : 09/16/2021
49-Qc� (»-)9
Danyale Love
Project Manager
Lab No : 88586 Matrix: Solids
Sample ID : Reidsville WTP Sampled: 9/15/2021 7:45
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Selenium <7.62 mg/Kg - dry 7.62 11.9 1 09/23/21 01:44 JTR 6010D
Sodium 402] mg/Kg - dry 310 595 1 09/23/21 01:44 JTR 6010D
Zinc 67.9 mg/Kg - dry 19.3 29.8 1 09/23/21 01:44 JTR 6010D
Sulfur 3430 mg/Kg - dry 123 238 1 09/23/21 01:44 JTR 6010D
Sodium Absorption Ratio 0.36] Ratio 0.01 0.01 1 09/23/21 01:44 CALCULATION
Qualifiers/
Definitions
DF Dilution Factor
J Estimated value
Page 5 of 7

Waypoi nt
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 21-259-0173
• Fed Ex
O UPS
Shipping Method
O US Postal 0 Lab
O Client 0 Courier
0 Other :
Thermometer ID: FT
—
Shipping container/cooler uncompromised? # Yes
O No
Number of coolers/boxes received [ 1
Custody seals intact on shipping container/cooler? Yes
O No
• Not Present
Custody seals intact on sample bottles? 0 Yes
O No
• Not Present
Chain of Custody (COC) present? # Yes
O No
COC agrees with sample label(s)? # Yes
O No
COC properly completed # Yes
O No
Samples in proper containers? # Yes
O No
Sample containers intact? # Yes
O No
Sufficient sample volume for indicated test(s)? # Yes
O No
All samples received within holding time? # Yes
O No
Cooler temperature in compliance? # Yes
O No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
O No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
0 Yes
0 Yes
O No
O No
O N/A
O N/A
Trip Blanks received with VOAs
0 Yes
O No
O N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
O No
O N/A
r High concentration container (48 hr) r Low concentration EnCore samplers (48 hr)
r High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature:
Summer Harrison
Date & Time:
Page 6 of 7
09/16/2021 15:46:05

Client Name/Address
EMA Resources Inc
755 Yadkinville Rd
Mocksville, NC 27028
Client Project Manager/Contact
Brent Collins
Billing Information
Account #46245
For Laboratory Use Only
Project Description
Project/Site Location (City/State)
(j Jl
ee; ci S`�+ t 1 - /A) C
^
....
—
RUSH -- Additional charges apply
Special Detection Limit(s)
Date Results Needed
Method of Shipment
Fed Ex
❑ Courier
Other
UPS CUSPS
Client Drop Off
Matrix Key
WW - Wastewater GW - Groundwater
DW - Drinking Water 5 -Soil /Solid 0 -Oil
P - Product M - Mist
Project Number
Projects Manager Phone 4
33 6 - 3 9 9 - 36 46
Project Manager Email
[e-mail]
Purchase Order Number
Site/Facility ID #
Waypoint
2790 Whitten
Memphis, TN
[phone]
e
ANALYTICAL
Road
38133
Unless noted, all containers
per Table 11136of 40CFR Part
Number of Containers
Matrix (Refer to key)
(G)rab or (C)omposite j
Metals (6010D)
TKNIAmmonia
Nitrate/Organic N
Total Solids
T(G
C:
w
k.—)
A Cool < 1OC Ne2S2031Micro Only)
B Cool c_ 6C I
tt ®4 0Hc2
❑ None Required
E NafH pH tO
F HNO3 p�lc2
HapHc2
H cool y=6C A2S203
Date
Time
Sample Identification
Required
Analysis / Preservative
Comments/Notes
1i/5
7=9$ai
ee d54; 11 c j„ -rP
1
4,,e
c,
v/
t/
L'
^ ✓
t�
Metals;AI,As,Ca.Cd,Cr,Cu,Fe,Pb
I
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
21 Z59-0173
WWIISINICIIlll09-
MIA
Resourceslr�I�IIIIIIIIIII11lII1�InIlI11
c
6-2021 —
15.45.32
''
Reidsville,
NC
—
1
1
I
I
For Laboratory Use Only
Sampled by
of
(Name - Print)
�j//,�,
'
Client Remarks/Comments
Sludge Samples - Report Dry Weight
Ice
s %` N
Cody
-
Lab Comments
Relinqui d by: (SIGN RE)
Date Time
Received by: (SIGNATURE)
Date Time
Blank/Cooler Temp
Stiq
Relinquished by: (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time
Relinquished by: (SIGNATURE)
Date Time
.A
eceived by: (SIGN URE) 4
LLa lilt/.- Giro J 3i\ Q iei9i
Date Time
tX `oo

Sodium
Calcium
Magnesium
Percent Solids
9/15/2021
mg/kg mg/L Equiv Weight Milli Equiv
402 17.085 23 0.742826
1060 45.05 20 2.2525
1690 71.825 12 5.985417
4.25
SAR =
SAR 0.37
Na
�2 (Ca2 i + Mgt )

ace Analytical®
A\ALYTICAL
REPO
September 28, 2021
RT
EMA Resources
Sample Delivery Group: L1403906
Samples Received: 09/15/2021
Project Number:
Description: Sludge
Report To:
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By:
Cassandra Foster
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
4
Cn
5
Sr
LQC]
GI
rAI1
9
SC
ACCOUNT:
EMA Resources
PROJECT:
SDG:
L1403906
DATE/TIME:
09/28/21 09:05
PAGE:
1of20

TABLE OF CONTENTS
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
REIDSVILLE WTP L1403906-01 5
Qc: Quality Control Summary 7
Wet Chemistry by Method 9012 B 7
Wet Chemistry by Method 9034-9030B 8
Wet Chemistry by Method 9045D 9
Wet Chemistry by Method D93/1010A 10
Mercury by Method 7470A 11
Metals (ICP) by Method 6010D 12
Volatile Organic Compounds (GC/MS) by Method 8260D 13
Chlorinated Acid Herbicides (GC) by Method 8151A 14
Pesticides (GC) by Method 8081B 15
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 16
GI: Glossary of Terms 18
Al: Accreditations & Locations 19
Sc: Sample Chain of Custody 20
Cp
2
Tc
3
SS
4
Cn
5
Sr
LQC]
GI
s
AI
9
SC
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
L1403906 09/28/21 09:05 2 of 20

SAMPLE SUMMARY
REIDSVILLE WTP L1403906-01 Waste
Collected by
Brent Collins
Collected date/time Received date/time
09/14/21 09:00 09/15/21 09:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Preparation by Method 1311 WG1742604 1 09/19/21 09:00 09/19/21 09:00 APH Mt. Juliet, TN
Preparation by Method 1311 WG1742759 1 09/19/2117:14 09/19/21 17:14 CJW Mt. Juliet, TN
Wet Chemistry by Method 9012 B WG1743298 1 09/21/2117:44 09/22/2113:17 KEG Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B WG1744140 1 09/21/21 20:00 09/21/21 20:00 CAT Mt. Juliet, TN
Wet Chemistry by Method 9045D WG1743932 1 09/22/2112:00 09/22/2114:00 MRM Mt. Juliet, TN
Wet Chemistry by Method D93/1010A WG1742753 1 09/20/21 02:18 09/20/21 02:18 WOS Mt. Juliet, TN
Mercury by Method 7470A WG1742917 1 09/20/21 08:33 09/21/21 09:59 ABL Mt. Juliet, TN
Metals (ICP) by Method 6010D WG1743041 1 09/20/2114:48 09/21/21 22:34 CCE Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1743446 1 09/21/21 22:29 09/21/21 22:29 ADM Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A WG1743366 1 09/22/21 07:43 09/26/21 03:06 HLJ Mt. Juliet, TN
Pesticides (GC) by Method 8081B WG1743400 1 09/23/21 22:00 09/24/2116:44 JMB Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1743399 1 09/21/21 22:12 09/22/2117:57 TMM Mt. Juliet, TN
i
Cp
Tc
3
Ss
4
Cn
5
Sr
LQC]
GI
8
Al
9
Sc
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
L1403906 09/28/21 09:05 3 of 20

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Cassandra Foster
Project Manager
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-9030B.
Co
Tc
3
Ss
Cn
5
Sr
GI
9
SC
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
L1403906 09/28/21 09:05 4 of 20

REIDSVILLE WTP SAMPLE RESULTS - 01
Collected date/time: 09/14/21 09:00 L1403906
Preparation by Method 1311
Result Qualifier Prep Batch
Analyte date / time
TCLP Extraction - 9/19/20219:00:11 AM WG1742604
TCLP 7HE Extraction - 9/19/2021 5:14:54 PM WG1742759
Fluid 1 9/19/20219:00:11 AM WG1742604
Initial pH 5.77 9/19/20219:00:11 AM WG1742604
Final pH 4.83 9/19/20219:00:11 AM WG1742604
Wet Chemistry by Method 9012 B
Analyte
Result Qualifier RDL Dilution Analysis
mg/kg mg/kg date / time
Batch
Reactive Cyanide ND 0.250 1 09/22/202113:17 WG1743298
Wet Chemistry by Method 9034-9030B
Analyte
Reactive Sulfide
Result Qualifier RDL Dilution Analysis Batch
mg/kg mg/kg date / time
36.5 25.0 1 09/21/2021 20:00 WG1744140
Wet Chemistry by Method 9045D
Result Qualifier Dilution Analysis
Analyte su date / time
Corrosivity by pH
Batch
6.99 T8 1 09/22/202114:00 WG1743932
Sample Narrative:
L1403906-01 W81743932: 6.99 at 20.3C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte Deg. F date /time
—
Ignitability DNI at 170 1 09/20/2021 02:18 WG1742753
Mercury by Method 7470A
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/ date/time
Meicury ND 0.0100 0.20 1 09/21/2021 09:59 WG1742917
Metals (ICP) by Method 6010D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/ date/time
—
Arsenic ND 0.100 5 1 09/21/2021 22:34 WG1743041
Barium 0.239 B 0.100 100 1 09/21/2021 22:34 WG1743041
Cadmium ND 0.100 1 1 09/21/2021 22:34 WG1743041
Chromium ND 0.100 5 1 09/21/2021 22:34 WG1743041
Lead ND 0.100 5 1 09/21/2021 22:34 WG1743041
Selenium ND 0.100 1 1 09/21/2021 22:34 WG1743041
Silver ND 0.100 5 1 09/21/2021 22:34 WG1743041
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/ date/time
Benzene ND 0.0500 0.50 1 09/21/202122:29 WG1743446
Carbon tetrachloride ND 0.0500 0.50 1 09/21/2021 22:29 WG1743446
Chlorobenzene ND 0.0500 100 1 09/21/2021 22:29 WG1743446
Chloroform ND 0.250 6 1 09/21/2021 22:29 WG1743446
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
L1403906 09/28/21 09:05 5 of 20

REIDSVILLE WTP SAMPLE RESULTS - 01
Collected date/time: 09/14/21 09:00 L1403906
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/1 date/time
1,2-Dichloroethane ND 0.0500 0.50 1 09/21/2021 22:29 WG1743446
1,1-Dichloroethene ND 0.0500 0.70 1 09/21/2021 22:29 WG1743446
2-Butanone (MEK) ND 0.500 200 1 09/21/2021 22:29 WG1743446
Tetrachloroethene ND 0.0500 0.70 1 09/21/2021 22:29 WG1743446
Trichloroethene ND 0.0500 0.50 1 09/21/2021 22:29 WG1743446
Vinyl chloride ND 0.0500 0.20 1 09/21/2021 22:29 WG1743446
(S) Toluene-d8 105 80.0-120 09/21/202122:29 WG1743446
(S)4-Bromofluorobenzene 89.7 77.0-126 09/21/202122:29 WG1743446
(S)1,2-Dichloroethane-d4 118 70.0-130 09/21/202122:29 WG1743446
Chlorinated Acid Herbicides (GC) by Method 8151A
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/1 date/time
2,4,5-TP (Silvex) ND 0.00200 1 1 09/26/2021 03:06 WG1743366
2,4-D ND 0.00200 10 1 09/26/2021 03:06 WG1743366
(S) 2,4-Dichlorophenyl Acetic Acid 143 14.0-158 09/26/202103:06 WG1743366
Pesticides (GC) by Method 8081B
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/ date/time
Chlordane ND 0.00500 0.03 1 09/24/202116:44 WG1743400
Endrin ND 0.00500 0.02 1 09/24/202116:44 WG1743400
Heptachlor ND 0.00500 0.0080 1 09/24/202116:44 WG1743400
Heptachlor epoxide ND 0.00500 0.0080 1 09/24/202116:44 WG1743400
Lindane ND 0.00500 0.40 1 09/24/202116:44 WG1743400
Methoxychlor ND 0.00500 10 1 09/24/202116:44 WG1743400
Toxaphene ND 0.0100 0.50 1 09/24/202116:44 WG1743400
(S) Decachlorobiphenyl 63.5 10.0-128 09/24/202116:44 WG1743400
(S) Tetrochloro-m-xylene 104 10.0-127 09/24/202116:44 WG1743400
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/ date/time
1,4-Dichlorobenzene ND 0.100 7.50 1 09/22/202117:57 WG1743399
2,4-Dinitrotoluene ND 0.100 0.13 1 09/22/202117:57 WG1743399
Hexachlarobenzene ND 0.100 0.13 1 09/22/202117:57 WG1743399
Hexachlaro-1,3-butadiene ND 0.100 0.50 1 09/22/202117:57 WG1743399
Hexachlaroethane ND 0.100 3 1 09/22/202117:57 WG1743399
Nitrobenzene ND 0.100 2 1 09/22/202117:57 WG1743399
Pyridine ND 0.100 5 1 09/22/202117:57 WG1743399
3&4-Methyl Phenol ND 0.100 400 1 09/22/202117:57 WG1743399
2-Methylphenol ND 0.100 200 1 09/22/202117:57 WG1743399
Pentachlorophenol ND 0.100 100 1 09/22/202117:57 WG1743399
2,4,5-Trichlorophenol ND 0.100 400 1 09/22/202117:57 WG1743399
2,4,6-Trichlorophenol ND 0.100 2 1 09/22/202117:57 WG1743399
(S) 2-Fluorophenol 54.0 10.0-120 09/22/20211757 WG1743399
(S) Phenol-d5 35.3 10.0-120 09/22/202117'57 WG1743399
(S) Nitrobenzene-d5 82.0 10.0-127 09/22/202117'57 WG1743399
(S) 2-Fluorobiphenyl 73.5 10.0-130 09/22/202117'57 WG1743399
(S)2,4,6-Tribromophenol 71.0 10.0-155 09/22/202117'57 WG1743399
(S) p-Terphenyl-d14 70.3 10.0-128 09/22/202117'57 WG1743399
Cp
Tc
3
SS
4
Cn
5
Sr
6
Qc
GI
9
Sc
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
L1403906 09/28/21 09:05 6 of 20

WG1743298
Wet Chemistry by Method 9012 B
Method Blank (MB)
(MB) R3707339-1 09/22/2113:04
J
O
CO LP
CO 0) N
E O
hCO
4)
co
Q
m
03
Reactive Cyanide
L1404491-01 Original Sample (OS) • Duplicate (DUP)
(OS) 0404491-01 09/22/2113:23 • (DUP) R3707339-6 09/22/2113:24
0
ce
E
03 J o ON
DUP Qualifier
d
03
03
0 o
O
0
CC O O]
d
E
N
03
p al O CO.
O E
Reactive Cyanide
Laboratory Control Sample (LCS)
(LCS) R3707339-2 09/22/2113:05
d)
Oc
N
U
01
E
O
LO
Reactive Cyanide
DATE/TIME:
ACCOUNT:
09/28/21 09:05
EMA Resources

WG1744140
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3707074-1 09/21/21 20:00
� • J
• E
Lri
Reactive Sulfide
Laboratory Control Sample (LCS)
(LCS) R3707074-2 09/21/21 20:00
0
U
E
a)
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0
O
E
a,
71.
0
O
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a1
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0
L1403889-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
N
N
ce
c O1
O E
(9I
0
Reactive Sulfide
DATE/TIME:
ACCOUNT:
09/28/21 09:05
EMA Resources

Q
U
v
H
cn
c
U
cn
Lrl
0
('D
WG1743932
Wet Chemistry by Method 9045D
L1404534-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1404534-04 09/22/2114:00 • (DUP) R3707419-3 09/22/2114:00
DUP Qualifier
O
0
Corrosivity by pH
Sample Narrative:
OS: 9.82 at 20.6C
DUP: 9.82 at 20.4C
Laboratory Control Sample (LCS)
Sample Narrative:
LCS: 10.05 at 20.4C
DATE/TIME:
ACCOUNT:
09/28/21 09:05
EMA Resources

Q
U
v
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WG1742753
Wet Chemistry by Method D93/1010A
L1403039-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1403039-01 09/20/21 02:18 • (DUP) R3706103-3 09/20/21 02:18
DUP Qualifier
O
L1404768-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1404768-01 09/20/21 02:18 • (DUP) R3706103-4 09/20/21 02:18
DUP Qualifier
0
d
0
0
C
O
0
N
0
0
N
cc
to
C
0
0
Ll
w
0
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0
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Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
E
0
0
0
0
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O
U
E
O
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0
0
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0
0
c9
0
0
Ll
▪ Ln
o N
Ll
w
0
Ll
a)
0
M
DATE/TIME:
ACCOUNT:
09/28/21 09:05
EMA Resources

O
N
O
N
N
00
Method Blank (MB)
(MB) R3706687-1 09/21/21 09:14
O O
c _ O
o] O]
E O
a
Laboratory Control Sample (LCS)
(LCS) R3706687-2 09/21/21 09:20
E
a)
O
o op
d
N
o
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0
O
E
a,
0
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a
Lo
O
O
O
O
0
L1403330-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1403330-02 09/21/21 09:22 • (MS) R3706687-3 09/21/21 09:24 • (MSD) R3706687-4 09/21/21 09:26
MSD Qualifier
O
0
m
ce
� o
0
ce
Ln
O
O
O
0
L1403651-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
cn
E
0
� - o
d
O
0
a,
Ln
0
0
Original Result
0
0(
L
0
▪ O
E O
a
DATE/TIME:
ACCOUNT:
09/28/21 09:05
EMA Resources

Q
U
v
H
cn
c
U
cn
v
0
('D
v
cn
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icL
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Method Blank (MB)
0
CO O] O O O O O O O
E O O O O O O O
J
CI CO CO M CO M CO ,-0M M M M M M M
M M M M M M M
m Ot O O O O O O O
E O O O O O O O
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Laboratory Control Sample (LCS)
(LCS) R3707265-2 09/21/21 21:26
0
0
U
O O O o
O O O O O O
a,O O O O O O
D' o Op Op Op Op Op Op Op
O O O
d
CC
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N
U
0
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0 0 0 0 0 0 0
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co (3 U vim') [f1
DATE/TIME:
ACCOUNT:
09/28/21 09:05
EMA Resources

0
U
0
H
cn
c
U
cn
0
0
co
('D
0
cn
WG1743446
Volatile Organic Compounds (GC/MS) by Method 8260D
Method Blank (MB)
J O O O
0 0 0 0 0 0 0 0 0 N cV M
O O O o 0 0 0 0 0 0
CC Ln LLO LC) LO LO LO LO LO O Q O
oO OLC,CD] O O O N O O Lo O O O O ^ O
E O O O O O O O O O O co n n
J
C. n n n Cr) n n n n n
CO Lfl Lfl W Lfl Lfl r` Lfl Lfl Lfl
CO Ot O O O O O O O O O
E 0 0 0 O 0 0 O 0 0 0
N
0
DO
CD
CD
O
oO O] V
E
N
0
0
N c = Y =
L tI aW CO
LL
E c
m° 0 0 0 0 0 0`
a
a, O O O U co O
m La C S O O p m E >.
C W 0 N .0U c
¢ CO U U U N H H
(S) 4-Bromofuorobenzene
(S)1,2-Dichloroethane-d4
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3706982-1 09/21/2114:16 • (LCSD) R3706982-2 09/21/2116:00
E
a 0 0 0 0 0 0 0 0 0 0
O N co
•CO M 71-
O
0
U
LCS Qualifier
N
0
o
CC
CC
O
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N
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0
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CO LO 0 ry N c9 N N N
O O O O O O O O O O p O
c9 coI� r` co OM N N
< 0
a
DATE/TIME:
(7
0
N
7 O O CD N N W cD M
t0 71- t0 O M 03 N O p O 0')
m 0-, m rn rn m m 0-, 0-, 0-,rn w
0
0
a
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o0Thoo o o o o 0 0 0
cp I� LCD W N c9 Ol
N 0 M N N
N N N N N N O N N N
O O O O O O O O O
U. LO W O Ln LO
N N N N N N N N N N
0 0 0 0 0 0 0 0 0
0 0 0 0 0 0
Ln Ln Ln Ln Ln Ln
p N N N N N N
E O O O O O O
Carbon tetrachloride
Chlorobenzene
E
0
0
O
U
1,2-Dichloroethane
1,1-Dichloroethene
LO
O O O
0 0 0
Ln Ln Ln
N N N
Trichloroethene
Vinyl chloride
ACCOUNT:
09/28/21 09:05
0
O
CD
w
O
O
a
w

Q
U
v
H
cn
c
U
cnCrl
v
0
('D
WG1743366
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3709272-1 09/26/21 01:18
O
0 • O)
E
0
07 • ))
E
N
Q
Ln
a
0
E
N N
00
Laboratory Control Sample (LCS)
(LCS) R3709272-2 09/26/21 01:33
0
U
• o Ln
CV CV
• O O
N O O
O o to to
0
d
0=
O Lc) W
o0 CV Co
•
N l0 C)
• d N
N 00 LSD
U U 0 0
E o 0
c
=
0
E
0 0
0 0 0
• — Ln Ln
aa) o 0
v) E o 0
DATE/TIME:
ACCOUNT:
09/28/21 09:05

Q
U
Method Blank (MB)
(MB) R3708759-1 09/24/2113:54
v
H
cn
c
U
cn
v
0
co
▪ 0 0 0 0 0 0
O 0 0 0 0 0 0 0
Ln Ln Ln Ln Ln LC)
0 0 0 0 CD CDCD O O
m • O] O O O O O O co; co;
O O O O O O O
00 00 00 00 00 00 CO
0 CO t0 l0 l0 l0 l0 CO
0 =, =, =,0 O O
00 • Ot O O O O O O O
E O co; co; co; co; co; co;
a)
Q
m
L
Z Z Z Z Z Z Z C 00
O
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= X = ( d
E = (c O o F o_
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C7 L) = = (0)I—
(S) Decachlorobiphenyl
(S) Tetrachloro-m-xylene
('D
Laboratory Control Sample (LCS)
(LCS) R3703759-2 09/24/2114:07
N O LO 00 I",
• N M M M LCJ NI NI
O OOO O O O O O O
Lri ^ ^ ^ O O
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(0 0 0 0 0 0
▪ E o 0 0 0 0
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E
0 0 0 0 0
a▪ ) 0 0 0 0 0
VI • E O O O O O
Heptachlor epoxide
(S) Decachlorobiphenyl
(S) Tetrachloro-m-xylene
L1399212-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
E
0
ce
0, 0 LO
CO CO CO
m 0 o
0
(0 ti M M Ln
m
Q
0
N
0
Q
N
co coo co co co
0 co co N N
Oo 0 0 0 o O O
o• o c O c0 O O O
0
0
d
ce
O 0, O c0
N O O
• O7 O7 O7 O7
M. CO N M 0-)m ri 0 ri (0 `� v
W 6 CO (0 (0 00 00
ai O O O
m O (0
00
K (O
01 (0 (0 01
0 — 0 0 0 0
n Ot 0 0 0 0
E O O O O
O
O
7 M m N M M
m M 00 M cO
CC 00 O CO O O
OV) 7, =) =) =) =)O
E O O O O O
m
ce
C
O]
(0 ▪ 0 0 0 0 0
O E Z Z Z Z Z
CO, CO, CO, CO, CO,
0 0 0 0 0
E
O O O O O
CO, CO, CO, CO, CO,
(0
O
0
U N
=
m O O
g L L
E m m
E Q Q
c O 0
C7 Lu = _
O
a
O
(S Decachlorobiphenyl
(S Tetrachloro-m-xylene
DATE/TIME:
ACCOUNT:
09/28/21 09:05
EMA Resources

Q
U
v
H
cn
c
U
cn
v
0
ua
('D
oa
v
cn
WG1743399
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Method Blank (MB)
(MB) R3707394-2 09/22/2111:38
J n O OD O O Ltd
0, 00 0, C U)
O O O O O O O O O O O O
CO O O O O O O O O O O O O O O O O O O
E o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
J
CI CO CO CO CO CO CO Cr) Cr) M CO CO CO
CO CO CO CO CO CO CO CO M CO CO CO
M M M M M M M M M M ("0 M
COO) O O O O O O O O O O O O
E O O O O O O O O O O O O
4)
Q
CD
0
CO a) N co O M v 06
E > > > > > > > > > > > > v M L) N M v
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
0
a
0
N
3&4-Methyl Phenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) Nitrobenzene-d5
(S) 2-Fluorob1phenyl
0
ti
0
(S) 2,4, 6-Tribromophenol
Laboratory Control Sample (LCS)
O O O O O O O o 0 0 0 r, 0 co
N N N
N N C ( N N
O O p p O O O O O O O O O O
co
N ON M N O O O
a,
ce
co co O t0 N O O O c0 CO LO 07 N
J o L.) co N. Ll) CO N cO cO cO N c0 CO CO CO
V)
C
0
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d
0
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I� O N CO LCJ Ol Ln M
c0 LCJ CO O M M N d- O
N M M M M M
OOOOOOOOOOOO
O O O O O O O O O O O O
CD CD CD CD CD CD CD CD CD CD CD CDO Ln Ln Ln Ln Ln Ln Ln Ln Ln Ln Ln Ln
E o 0 0 0 0 0 0 0 0 0 0 0
w
a)
co
0
0
m
Q �
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
0
0
Z
0
0
O N
3&4-Methyl Phenol
Pentachlorophenol
0 0
CD CD
t t
0_ 0_
0 0
0 0
I— 17
Ln
�F �F
N N
(S) Nitrobenzene-d5
(S) 2-Fluorobrphenyl
(S) p-Terphenyl-d14
DATE/TIME:
ACCOUNT:
09/28/21 09:05
EMA Resources

WG1743399
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Laboratory Control Sample (LCS)
d
N N_ �_
O O O
O O O
E
(S) 2,4, 6-Tribromophertol
DATE/TIME:
0
0
N
0
U
0
0
a
ACCOUNT:
09/28/21 09:05
0
0

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec. Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Case Narrative (Cn)
Quality Control
Summary (Qc)
Sample Chain of
Custody (Sc)
Sample Results (Sr)
Sample Summary (Ss)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
T8 Sample(s) received past/too close to holding time expiration.
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
L1403906 09/28/21 09:05 18 of 20

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Alaska
17-026
Arizona A20612
Arkansas 88-0469
California 2932
Colorado _ TN00003
Connecticut PH-0197
Florida E87487
Georgia NELAP
Georgia 923
Idaho TN00003
Illinois 200008
Indiana C-TN-01
Iowa 364
Kansas E-10277
Kentucky1° KY90010
Kentucky2 16
Louisiana A130792
Louisiana LA018
Maine TN00003
Maryland 324
Massachusetts M-TN003
Michigan 9958
Minnesota 047-999-395
Mississippi TN00003
Missouri 340
Montana CERT0086
Nebraska NE-0S-15-05
Nevada TN000032021-1
New Hampshire 2975
New Jersey—NELAP TN002
New Mexico' TN00003
New York 11742
North Carolina Env375
North Carolina DW21704
North Carolina' 41
North Dakota R-140
Ohio—VAP CL0069
Oklahoma 9915
Oregon TN200002
Pennsylvania 68-02979
Rhode Island LA000356
South Carolina 84004002
South Dakota n/a
Tennessee14 2006
Texas T104704245-20-18
Texas LAB0152
Utah TN000032021-11
Vermont VT2006
Virginia 110033
Washington C847
West Virginia 233
Wisconsin 998093910
Wyoming A2LA
A2LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA— ISO 17025 5 1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA—Crypto TN00003
'Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity ° Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Co
Tc
3
SS
4
Cn
5
Sr
LQC]
GI
9
SC
ACCOUNT: PROJECT: S DG: DATE/TIME: PAGE:
EMA Resources L1403906 09/28/21 09:05 19 of 20

Analysis / Container / Preservative
Acctnum. EMARES
Template:T11413
Sample N (lab only)
i
n
E -
N
53adoN-JI]-li d131 x
sa
aN a4]-1I
ns23] x
Billing informati
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
0
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0
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E
00
C'
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Company Name/Address:
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
u
0J
0
a
Cliert Project #
0
a
Site/Facility ID #t
a
Rush? (Lab MUST Be Notified)
0_
z v
Date Resuits Needed
6
E
n
0
'o
1.7
a
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Phone:[phone]
Collected by (signature):
ry
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2021 Reidsville WTP Annual Report -
WQ0032723
Final Audit Report
2022-02-24
Created: 2022-02-22
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAyoHvXhYKb925T-BggN27K9gfogz2LMZx
"2021 Reidsville WTP Annual Report - WQ0032723" History
ti Document created by Brent Collins ([e-mail])
2022-02-22 - 4:51:05 PM GMT- IP address: 206.85.202.26
El Document emailed to C. Scott Jewell ([e-mail]) for signature
2022-02-22 - 4:52:00 PM GMT
674 Email viewed by C. Scott Jewell ([e-mail])
2022-02-24 - 8:27:35 PM GMT- IP address: 12.234.212.82
Document e-signed by C. Scott Jewell ([e-mail])
Signature Date: 2022-02-24 - 8:28:50 PM GMT - Time Source: server- IP address: 12.234.212.82
Agreement completed.
2022-02-24 - 8:28:50 PM GMT
Ea Adobe Sign

2021 Reidsville WTP Annual Report -
WQ0032723
Final Audit Report
2022-02-28
Created: 2022-02-24
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAWfGoWAF4V3ddh2D1PzcfphOX7Z-RuGQ
"2021 Reidsville WTP Annual Report - WQ0032723" History
Document created by Brent Collins ([e-mail])
2022-02-24 - 9:30:23 PM GMT- IP address: 206.85.202.26
Document emailed to Summer Woodard ([e-mail]) for signature
2022-02-24 - 9:31:31 PM GMT
Email viewed by Summer Woodard ([e-mail])
2022-02-28 - 3:00:52 PM GMT- IP address: 12.234.212.82
Document e-signed by Summer Woodard ([e-mail])
Signature Date: 2022-02-28 - 3:01:23 PM GMT - Time Source: server- IP address: 12.234.212.82
Agreement completed.
2022-02-28 - 3:01:23 PM GMT
Ea Adobe Sign