WQ0000672_2021 Residual Annual Report_20220301

Initial Review
Reviewer
EADS\ndthornburg
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0000672
ApplicantlPermittee City of Lumberton
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office Fayetteville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Michael C Hunt
Email Address*
[e-mail]
Project Information
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
9107385311
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Perm it Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number: *
WQ0000672
Has Current Existing permit number
Applicant/Permittee Address*
700 Lafayette Street, Lumberton, NC 28358
Facility Name*
City of Lumberton Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Annual Report 2021.pdf 36.01 MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 3/1/2022

ENVIRO.. H ICE
W
PO Box 309
Lumberton, NC 28359
Phone: [phone]
Fax: [phone]
February 28, 2022
NC Environmental Quality-DWQ
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Attention: Compliance Representative
Subject: 2021 Annual Report for City of Lumberton Land Application Program
(City of Lumberton WQ0000672)
Dear Compliance Representative,
Enclosed is (1) copy of the monitoring and reporting information as requited in the referenced
permit for the City of Lumberton, North Carolina. This report was complied from land
application records provided by the City of Lumberton and Enviro-Choice Recycling. The report
includes: 1) a state required annual certification for and facility information page, 2) the 2021
annual application summary table, 3) annual residual sampling summary form and laboratory
analysis reports, 4) field loading reports, 5) pathogen and vector reduction documentation, and 6)
soil analysis reports.
Should you need more information regarding this land application program, please contact me at
910-738-5311 or envirochoicencgggmaiLcom.
A �Lj
Michael C. Hunt
Enviro-Choice Recycling
CC: Henry Harper, Wastewater ORC, City of Lumberton WWTP
Office: 910-671-3859 hharperkci.lumberton.nc.us

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0000672 County:
Facility Name (as shown on permit):
Land Application Operator:
Robeson
Year: 2021
City of Lumberton
Enviro-Choice Recycling, LLC Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
EE Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
43
Total number of fields utilized for land application during the year:
16
Total amount of dry tons applied during the year for all application sites:
1262.959
Total number of acres utilizes for land application during the year:
350.5
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. RI Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Henry Harper VWVfP ORC
Permittee Name and Title (type
�Jj2/8/2022
Sig at e A Permittee Date
Signature of Preparer*u Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 265.00
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Tracy Bullard Owner: Tracy Bullard Predominant Soil Series: Wab-Wagram
Acres Used: 62.5 Acres Permitted: 62.5 Site #: 6 Field #: NC-RO-39-09
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4j
51
6
7
8
91
10
11
12
DT/Ac./
App.
Event
1.86
0.82
1.56
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
2.055
0.000
1.256
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.310
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.067
0.322
0.076
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.466
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
2.937
0.000
2.957
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.894
Total
Phos-
56.574
16.748
62.320
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
135.643
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
J�_J1
Signature of Land Applier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Carnell Locklear Owner: Robert Baskersville Predominant Soil Series:
56.9 Acres Permitted: 56.9 Site #: 2 Field #
68.68
GoA
NC-RO-28-2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4j
51
6
7
8
91
10
11
12
DT/Ac./
App.
Event
1.21
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
24.623
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
24.623
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
W-
Signature of Land Appher
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual):
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Ronald G. Hammonds Owner: Taylco, INC Predominant Soil Series:
Acres Used: 10.6 Acres Permitted: 10.6 Site #: 14 Field #:
50.82
GoA-Goldsboro
NC-RO-20-14
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4
11/12/21
5
6
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
9
10
11
12,
DT/Ac./
App.
Event
4.04
0.76
Arsenic
1 0.000
0.000
0.000
1 0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
4.459
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.459
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.146
0.000
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.147
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
6.374
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6.374
Total
Phos-
122.786
0.000
0.000
0.095
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
122.881
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
�_Jj
Signature of Land Appaer
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald Hammonds Owner: Ronald Hammonds Predominant Soil Series:
73.2 Acres Permitted: 73.2 Site #:
Field #
314.61
GoA-Goldsboro
NC-RO-20-08
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
91
10
11
12
DT/Ac./
App.
Event
0.63
2.56
0.12
0.99
Arsenic
0.000
0.000
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.700
0.000
0.093
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.793
Chromium0.000
0.000
0.000
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Lead
0.023
1.003
0.006
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.033
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
1.000
0.000
0.218
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.219
Total
Phos-
19.274
52.204
4.600
0.125
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
76.202
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/28/2022
Signature of Land Ap ier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 67.65
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Ronald G. Hammonds Owner: Taylco, INC Predominant Soil Series: GOA-Goldsboro
Acres Used: 13 Acres Permitted: 13 Site #: 7 Field #: NC-RO-20-07
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
91
10
11
12
DT/Ac./
App.
Event
0.00
3.73
0.00
1.47
Arsenic
0.000
0.000
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromium0.000
0.000
0.000
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Lead
0.000
1.463
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.465
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
76.153
0.000
0.185
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
76.339
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/28/2022
Signature of Land Appl r Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Lumberton Total Dry Tons Applied (Annual): 53.64
Permit #: WQ0000672 Cation Exchange Capacity (non 503 only):
Operator: Ronald G. Hammonds Owner: Taylco, INC Predominant Soil Series: GOA-Goldsboro
Acres Used: 6.7 Acres Permitted: 6.7 Site #: 7 Field #: NC-RO-20-06
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
51
6
7
8
91
10
11
12
DT/Ac./
App.
Event
3.49
4.51
Arsenic
0.000
0.000
0.000
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromium0.000
0.000
0.000
0.023
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Lead
0.000
1.369
0.000
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.373
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
71.257
0.000
0.569
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
71.826
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
jL_jj I
Signature of Land App er
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald Hammonds Owner: Ronald Hammonds Predominant Soil Series:
24.9 Acres Permitted: 24.9 Site #:
Field #
74.75
WkB-Wakulla
NC-RO-20-03
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4j
51
6
7
8
91
10
11
12
DT/Ac./
App.
Event
3.00
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
1.177
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.177
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
61.241
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
61.241
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land App er
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker
Owner: James Campen Predominant Soil Series:
12.3 Acres Permitted: 12.3 Site #: 18 Field #:
64.17
WaB-Wagram
NC-RO-16-18
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4j
51
6
7
8
91
10
11
12
DT/Ac./
App.
Event
1.17
4.05
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
3.265
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.265
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.457
0.198
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.656
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
7.689
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.689
Total
Phos-
0.000
23.786
162.040
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
185.826
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land App ' r
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker
Owner: James Campen Predominant Soil Series:
Acres Permitted: 6 Site #: 17 Field #:
27.37
WaB-Wagram
NC-RO-16-17
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
91
10
11
12
DT/Ac./
App.
Event
1.76
2.80
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
2.256
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.256
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.000
0.137
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.137
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
5.313
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.313
Total
Phos-
0.000
35.945
111.960
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
147.905
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
' `1�4
2/28/2022
Signature of Land Appl r Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker
Owner: James Campen Predominant Soil Series:
Acres Permitted: 5 Site #: 16 Field #:
25.67
WaB-Wagram
NC-RO-16-16
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4j
51
6
7
8
91
10
11
12
DT/Ac./
App.
Event
5.13
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
104.734
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
104.734
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
jL_jj I
Signature of Land Appli
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
The City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Owner:
17.5 Acres Permitted:
17.5 Site #:
Predominant Soil Series:
Field #
86.92
NoA-Norfolk
NC-RO-16-07
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4j
51
6
7
8
91
10
11
12
DT/Ac./
App.
Event
3.32
1.65
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
1.326
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.326
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
1.302
0.081
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.383
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
3.122
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.122
Total
Phos-
0.000
67.769
65.800
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
133.569
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
' Lj
2/28/2022
Signature of Land ApImer Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker Owner: Ozzell Baker Predominant Soil Series:
14.8 Acres Permitted: 14.8 Site #: NC-RO-16 Field #
50.01
NoA- Norfolk
6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3j
4j
51
6
7
8
91
10
11
12
DT/Ac./
App.
Event
2.24
1.14
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.915
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.915
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.880
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.935
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
2.154
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.154
Total
Phos-
0.000
45.778
45.400
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
91.178
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Appli
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker Owner: Ozzell Baker Predominant Soil Series:
8.7 Acres Permitted: 8.7 Site #: NC-RO-16 Field #
30.12
NoA- Norfolk
5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3j
4j
51
6
7
8
91
10
11
12
DT/Ac./
App.
Event
2.08
1.38
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
1.111
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.111
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.817
0.068
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.884
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
2.617
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.617
Total
Phos-
0.000
42.493
55.160
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
97.653
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
A-Ald
2/28/2022
Signature of Land Ap lier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker Owner: Ozzell Baker Predominant Soil Series:
3.6 Acres Permitted: 3.6 Site #: NC-RO-16 Field #
13.80
Ra-Rains Sandy
4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5
6
7
8
91
10
11
12
DT/Ac./
App.
Event
3.83
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
3.089
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.089
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.000
0.188
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.188
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
7.273
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.273
Total
Phos-
0.000
0.000
153.280
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
153.280
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/28/2022
Signature of Land Ap ier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ000672 Cation Exchange Capacity (non 503 only):
Ozzell Baker Owner: Ozzell Baker Predominant Soil Series:
3.6 Acres Permitted: 3.6 Site #: NC-RO-16 Field #
19.20
GoA-Goldsboro
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4j
51
6
7
8
91
10
11
12
DT/Ac./
App.
Event
5.33
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
4.298
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.298
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.000
0.261
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.261
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
10.120
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
10.120
Total
Phos-
0.000
0.000
213.280
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
213.280
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Ap lier
2/28/2022
Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Lumberton Total Dry Tons Applied (Annual):
WQ0000672 Cation Exchange Capacity (non 503 only):
Ronald Hammonds Owner: Charles Brown Predominant Soil Series:
31.2 Acres Permitted: 31.2 Site #: 4 Field #
58.13
WkB-Wakulla
NC-RO-20-4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
2/24/21
2
4/20/21
3
7/22/21
4j
11/12/21
5
6 j
7
8
9
10
11
12
% Solids
2.76
2.92
2.32
1 1.72
Arsenic
ND
ND
ND
0.35
Cadmium
ND
ND
ND
0.021
Copper
552
ND
403
ND
Chromium
2.6
Lead
18.1
196
24.5
0.45
Mercury
ND
ND
ND
0.007
Molyb-
denum
ND
ND
ND
ND
Nickel
ND
ND
ND
ND
Selenium
ND
ND
ND
0.1
Zinc
789
ND
949
ND
Total
Phos-
horus
15200
10200
20000
63
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4j
51
6
7
8
91
10
11
12
DT/Ac./
App.
Event
1.86
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Chromium0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.730
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.730
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Molyb-
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
denum
Nickel
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
38.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
38.005
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/28/2022
Signature of Land ApPlier Date
DENR FORM MFLSF (12/2006)

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ANALYTICAL REPORT
March 05, 2021
Hunt Environmental Associates
Sample Delivery Group
Samples Received:
Project Number:
Description:
Report To:
L132OOO1
02/25/2021
Enviro-Choice Recycling
Cody Hunt
3330 Saddletree Road
Lumberton, NC 28359
Entire Report Reviewed By: 4��
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
aceAnalytical
National Center for Testing & Innovation
AW
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1320001 03/05/2115:05 1 of38

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
WW-1 L1320001-01
5
Fn
WW-1 L1320001-02
7
Qc: Quality Control Summary
9
Fr
Total Solids by Method 2540 G-2011
9
Total Solids by Method 2540B
10
FC
Wet Chemistry by Method 350.1
11
F
Wet Chemistry by Method 351.2
14
Wet Chemistry by Method 353.2
15
[Al
Wet Chemistry by Method 365.4
16
Wet Chemistry by Method 365.4M
17
RC
Wet Chemistry by Method 4500 CN E-2011
18
Wet Chemistry by Method 4500NOrg C-2011
20
Wet Chemistry by Method 9012 B
21
Wet Chemistry by Method 9034-9030B
22
Wet Chemistry by Method 9040C
24
Wet Chemistry by Method 9045D
25
Wet Chemistry by Method 9056A
26
Wet Chemistry by Method D93/1010A
27
Mercury by Method 7470A
29
Mercury by Method 7471B
30
Metals (ICP) by Method 6010D
31
GI: Glossary of Terms
35
Al: Accreditations & Locations
36
Sc: Sample Chain of Custody
37
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates L1320001
03/05/2115:05 2 of38

WW-1 L1320001-01 Solid
Method
Total Solids by Method 2540 G-2011
Wet Chemistry by Method 350.1
Wet Chemistry by Method 365.4M
Wet Chemistry by Method 4500NOrg C-2011
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method 9056A
Wet Chemistry by Method D93/1010A
Mercury by Method 7471B
Metals (ICP) by Method 6010D
WW-1 L1320001-02 GW
Method
Total Solids by Method 2540B
Wet Chemistry by Method 350.1
Wet Chemistry by Method 351.2
Wet Chemistry by Method 353.2
Wet Chemistry by Method 365.4
Wet Chemistry by Method 4500 CN E-2011
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9040C
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
SAMPLE SUMMARY
Collected by
Carrigan Harris
ONE LAB. NATIONWIDE. *
Collected date/time Received date/time
02/24/2110:45 02/25/2109:50
Cp
Batch
Dilution
Preparation
Analysis
Analyst
date/time
date/time
WG1628004
1
03/03/2122:33
03/03/2122:57
MMF
WG1628181
1
03/03/2112:00
03/04/2123:57
SDL
WG1628800
5
03/03/2114:27
03/04/2102:39
SDL
WG1628796
2
03/03/2114:26
03/04/2109:38
MSP
WG1627906
3
03/02/211123
03/02/2119:04
SDL
WG1628802
1
03/03/2123:00
03/03/2123:00
LDT
WG1627249
1
03/01/2110:53
03/01/2120:04
KPS
WG1627678
1
03/01/2119:00
03/02/2102:11
ELN
WG1629797
1
03/05/2107:58
03/05/2107:58
CAT
WG1627148
1
03/01/2110:43
03/01/2115:08
BMF
WG1627126
1
02/28/2117:25
03/02/2118:51
KMG
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
FC
Mt. Juliet, TN
F-I
Collected by
Collected date/time
Received date/time
Carrigan Harris
02/24/2110:45
02/25/21 09:50
SAI
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
WG1627998
1
03/02/2120:02
03/02/21 20:35
MMF
9
Mt. Juliet, TN Sc
WG1626193
5
02/26/2114:13
02/26/2114:13
SL
Mt. Juliet, TN
WG1629156
200
03/03/2115:47
03/04/21 06:13
SDL
Mt. Juliet, TN
WG1628709
1
03/03/2116:15
03/03/2116:15
LRP
Mt. Juliet, TN
WG1628555
1
03/03/2115:47
03/04/21 04:53
SDL
Mt. Juliet, TN
WG1628371
10
03/03/2112:21
03/03/2115:07
JER
Mt. Juliet, TN
WG1625981
100
02/27/2116:16
02/27/2116:16
LRP
Mt. Juliet, TN
WG1625888
1
02/26/21 09:00
02/26/21 09:00
SAC
Mt. Juliet, TN
WG1628339
1
03/03/2117:18
03/03/2117:18
CO
Mt. Juliet, TN
WG1627375
10
03/01/2114:44
03/01/2117:36
BMF
Mt. Juliet, TN
WG1627280
5
02/28/21 2141
03/01/2112:16
EL
Mt. Juliet, TN
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1320001 03/05/2115:05 3 of38

CASE NARRATIVE
ONE LAB. NATIONWIDE. *
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
FC
4�z
F,
Heather J Wagner
[Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1320001 03/05/2115:05 4 of38

WW-1
Collected date/time: 02/24/21 10:45
Total Solids by Method 2540 G-2011
SAMPLE RESULTS - 01
L1320001
Result
Qualifier Dilution Analysis
Batch
Analyte %
date / time
Total Solids 2.76
1 03/03/2021 22:57
WG1628004
Wet Chemistry by Method 350.1
Result (dry)
Qualifier RDL (dry) Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Ammonia Nitrogen 3790
362 1
03/04/202123:57 WG1628181
Wet Chemistry by Method 365.4M
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Phosphorus, Total 15200 3620 5 03/04/202102:39 WG1628800
Wet Chemistry by Method 4500NOrg C-2011
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Kjeldahl Nitrogen, TKN 48700 1450 2 03/04/2021 09:38 WG1628796
Wet Chemistry by Method 9012 B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Cyanide ND
0.750
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Sulfide ND
25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
3 03/02/202119:04 WG1627906
Dilution Analysis Batch
date / time
1 03/03/202123:00 WG1628802
Result Qualifier
Dilution Analysis
Batch
Analyte su
date / time
pH 7.17 T8
1 03/01/202120:04
WG1627249
Sample Narrative:
L1320001-01 WG1627249: 7.17 at22C
Wet Chemistry by Method 9056A
Result (dry) Qualifier
RDL (dry) Dilution
Analysis
Analyte mg/kg
mg/kg
date / time
Nitrate -Nitrite ND
725 1
03/02/2021 02:11
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at170
Mercury by Method 7471B
Qualifier Dilution Analysis Batch
date / time
1 03/05/202107:58 WG1629797
Batch
WG1627678
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 1.45 1 03/01/202115:08 WG1627148
ONE LAB. NATIONWIDE. *
FP
Fc
FS
Fn
Fc
F,
SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1320001 03/05/2115:05 5 of38

WW-1
Collected date/time: 02/24/21 10:45
Metals (ICP) by Method 6010D
Result (dry) Qualifier
Analyte mg/kg
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
25700
ND
ND
10200
552
18.1
ND
ND
ND
4180
ND
15500
789
SAMPLE RESULTS - 01
L1320001
RDL (dry)
Dilution Analysis
mg/kg
date / time
725
1 03/02/202118:51
72.5
1 03/02/2 02118:51
18.1
1 03/02/2 02118:51
3620
1 03/02/2 02118:51
72.5
1 03/02/2 02118:51
18.1
1 03/02/2 02118:51
3620
1 03/02/2 02118:51
18.1
1 03/02/2 02118:51
72.5
1 03/02/2 02118:51
1810
1 03/02/2 02118:51
72.5
1 03/02/2 02118:51
3620
1 03/02/2 02118:51
181
1 03/02/202118:51
ONE LAB. NATIONWIDE. *
Batch
FP
WG1627126
� F
WG1627126
WG1627126
WG1627126
F
WG1627126
WG1627126
Fn
WG1627126
WG1627126
WG1627126
FA
WG1627126
WG1627126
6
QC
WG1627126
WG1627126
�GI
SAI
RC
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG:
L1320001
DATE/TIME: PAGE:
03/05/2115:05 6 of38

WW-1
Collected date/time: 02/24/21 10:45
Total Solids by Method 2540B
SAMPLE RESULTS - 02
L1320001
Result Qualifier Dilution Analysis Batch
Analyte mg/I date / time
Total Solids 27300 1 03/02/2021 20:35 WG1627998
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Ammonia Nitrogen 38.6 1.25 5 02/26/202114:13 WG1626193
Wet Chemistry by Method 351.2
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Kjeldahl Nitrogen, TKN 1590 50.0 200 03/04/2021 06:13 WG1629156
Wet Chemistry by Method 353.2
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Nitrate -Nitrite 0.505 0.100 1 03/03/202116:15 WG1628709
Wet Chemistry by Method 365.4
Result Qualifier
RDL
Dilution Analysis
Batch
Analyte mg/I
mg/I
date / time
Phosphorus, Total 0.338
0.100
1 03/04/202104:53
WG1628555
Wet Chemistry by Method 4500 CN E-2011
Result Qualifier
RDL
Dilution Analysis
Batch
Analyte mg/I
mg/I
date / time
Reactive Cyanide ND
0.0500
10 03/03/202115:07
WG1628371
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL
Analyte mg/I mg/I
Reactive Sulfide 16.4 5.00
Wet Chemistry by Method 9040C
Dilution Analysis Batch
date / time
100 02/27/202116:16 WG1625981
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 7.07 T8 1 02/26/202109:00 WG1625888
Sample Narrative:
L1320001-02 WG1625888: 7.07 at19.8C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte deg F date/time
Flashpoint DNF at170 1 03/03/202117:18 WG1628339
Mercury by Method 7470A
Analyte
Mercury
Result Qualifier RDL Dilution Analysis Batch
mg/I mg/I date / time
0.00362 0.00200 10 03/01/202117:36 WG1627375
ONE LAB. NATIONWIDE. *
FP
Fc
FS
Fn
Fc
F,
SAI
Rc
ACCOUNT:
Hunt Environmental Associates
PROJECT: SDG: DATE/TIME: PAGE:
L1320001 03/05/21 15:05 7 of 38

WW-1
Collected date/time: 02/24/21 10:45
Metals (ICP) by Method 6010D
SAMPLE
RESULTS - 02
L1320001
ONE LAB. NATIONWIDE.
Result
Qualifier RDL
Dilution Analysis
Batch
FPAnalyte
mg/I
mg/I
date / time
Aluminum
551
1.00
5
03/01/202112:16
WG1627280
F
Arsenic
0.168
0.0500
5
03/01/202112:16
WG1627280
Cadmium
0.0201
0.0100
5
03/01/202112:16
WG1627280
Calcium
258
5.00
5
03/01/202112:16
WG1627280
F
Copper
12.9
0.0500
5
03/01/202112:16
WG1627280
Lead
0.385
0.0300
5
03/01/202112:16
WG1627280
Fn
Magnesium
50.1
5.00
5
03/01/202112:16
WG1627280
Molybdenum
0.118
0.0250
5
03/01/202112:16
WG1627280
Nickel
0.460
0.0500
5
03/01/202112:16
WG1627280
FA
Potassium
97.0
10.0
5
03/01/202112:16
WG1627280
Selenium
ND
0.0500
5
03/01/202112:16
WG1627280
FC
Sodium
364
15.0
5
03/01/202112:16
WG1627280
Zinc
19.0
0.250
5
03/01/202112:16
WG1627280
F,
F
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental
Associates
L1320001
03/05/2115:05 3 of38

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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE. *
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
FS
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
RDL (dry)
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fc
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
F
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Rc
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
E
The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial
calibration (ICAL).
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8
Sample(s) received past/too close to holding time expiration.
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1320001 03/05/2115:05 35 of38

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. *
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN, 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197 _
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915 _
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033 _
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1320001 03/05/2115:05 36 of38

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From 1/1/2021 To
WQ Permit Number:
NPDES Number:
3/31 /2021
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
Alt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens u
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Composting ❑ jAerobic Digestion IZ
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
inSlud e
Pathogen Density
Number ol
Excee-
deuces
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
ni ue
inim
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
35400
62500
106000
CFU/ g
Quarterly
Qu Y
Grab
222D-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC
Preparer Name and Title (type or LIT)
Signature of Preparer*
Michael C Hunt, ORC
Land Applier Name and Title (if applicable)(type or print)
2/22/2022
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Cameron Testing Services, Inc, Laboratory Deport
NCDr: NR#654
NC PHHS to37799
Client:
Enviro-Choice Recycling CTS PrO
210 -189
US EPA ONC01S1 B
DWCert*37799
Project
City of Lumberton RegulatoryYes
Sample Information
"-sa
C- Harris oats 02124/21 Recelvod J.
Cameron Date
02124121
Analyses and results
Lab ]D
Sample ID Analyte Result E
St& Mothads
[a
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2102-189
-01 3'Ijdpr nr Fee Caliform-S 106000 cfiur@
35400
0212021 RL
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-02 <35400 crwQ
35400
-03 35400 GrUew
35400
-04 35500 CM9
35500
-05 106000 cFUry
35400
-06 106000 GFllfp
3$300
-07 70500 CFwa
3530o
Genmean 6 500
2102-189
-01 sUaijt Cg T9 (%) 2.83%
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13
ace Analytical ' ANALYTICAL REPORT
May 11, 2021
Hunt Environmental Associates
Sample Delivery Group: L1343223
Samples Received: 04/23/2021
Project Number:
Description: Enviro-Choice Recycling
Report To: Cody Hunt
3330 Saddletree Road
Lumberton, NC 28359
Entire Report Reviewed By: 4�41
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343223 05/11/2114:16 1 of 15

TABLE OF CONTENTS
Cp: Cover Page
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
GI: Glossary of Terms 5
Al: Accreditations & Locations
Sc: Sample Chain of Custody
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343223 05/11/2114:16 2 of 15

SAMPLE
SUMMARY
Collected by
Collected date/time
Received date/time
WW-2 L1343223-01 Solid
Carrigan Harris
04/20/211120
04/23/2115:00
Method
Batch
Dilution Preparation
Analysis
Analyst Location
date/time
date/time
Subcontracted Analyses
WG1658866
1 05/11/21 00:00
05/11/21 00:00
Subcontract
Collected by
Collected date/time
Received date/time
WW-2 L1343223-02 GW
Carrigan Harris
04/20/211120
04/23/2115:00
Method
Batch
Dilution Preparation
Analysis
Analyst Location
date/time
date/time
Subcontracted Analyses
WG1658866
1 05/11/21 00:00
05/11/21 00:00
Subcontract
FP
FC
F
Fn
5G1
6AI
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343223 05/11/2114:16 3 of 15

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
5G1
6AI
4�z
Sc
Heather J Wagner
Project Manager
Project Narrative
L1343223 -01, -02 contains subout data that is included after the chain of custody.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343223 05/11/2114:16 4 of 15

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
SDG Sample Delivery Group.
Uncertainty
(Radiochemistry) Confidence level of 2 sigma.
Fn
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control This section ofthe report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
F
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
R
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343223 05/11/2114:16 5 of 15

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343223 05/11/2114:16 6 of 15

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13
ace Analytical ' ANALYTICAL REPORT
May 27, 2021
Hunt Environmental Associates
Sample Delivery Group: L1343221
Samples Received: 04/23/2021
Project Number:
Description: Enviro-Choice Recycling
Report To: Cody Hunt
3330 Saddletree Road
Lumberton, NC 28359
Entire Report Reviewed By: 4�41
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343221 05/27/2111:23 1 of37

TABLE OF CONTENTS
Cp: Cover Page
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
Fss]
WW-2 L1343221-01
5
Fn
WW-2 L1343221-02
7
Qc: Quality Control Summary
9
Fr
Total Solids by Method 2540 G-2011
9
Total Solids by Method 2540B
10
Rc
Wet Chemistry by Method 350.1
11
F
Wet Chemistry by Method 351.2
14
Wet Chemistry by Method 353.2
15
[Al
Wet Chemistry by Method 365.4
16
Wet Chemistry by Method 365.4M
17
RC
Wet Chemistry by Method 4500 CN E-2011
18
Wet Chemistry by Method 4500NOrg C-2011
19
Wet Chemistry by Method 9012 B
20
Wet Chemistry by Method 9034-9030B
21
Wet Chemistry by Method 9040C
23
Wet Chemistry by Method 9045D
24
Wet Chemistry by Method 9056A
25
Wet Chemistry by Method D93/1010A
26
Mercury by Method 7470A
28
Mercury by Method 7471B
29
Metals (ICP) by Method 6010D
30
GI: Glossary of Terms
34
Al: Accreditations & Locations
35
Sc: Sample Chain of Custody
36
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates L1343221
05/27/2111:23
2 of37

WW-2 L1343221-01 Solid
Method
Total Solids by Method 2540 G-2011
Wet Chemistry by Method 350.1
Wet Chemistry by Method 365.4M
Wet Chemistry by Method 4500NOrg C-2011
Wet Chemistry by Method 9012 B
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9045D
Wet Chemistry by Method 9056A
Wet Chemistry by Method D93/1010A
Mercury by Method 7471B
Metals (ICP) by Method 6010D
WW-2 L1343221-02 GW
Method
Total Solids by Method 2540B
Wet Chemistry by Method 350.1
Wet Chemistry by Method 351.2
Wet Chemistry by Method 353.2
Wet Chemistry by Method 365.4
Wet Chemistry by Method 4500 CN E-2011
Wet Chemistry by Method 9034-9030B
Wet Chemistry by Method 9040C
Wet Chemistry by Method D93/1010A
Mercury by Method 7470A
Metals (ICP) by Method 6010D
SAMPLE SUMMARY
Collected by
Carrigan Harris
Batch
Dilution
Preparation
date/time
W G1661921
1
05/02/21 22:03
W G1659238
1
04/27/21 0715
WG1675157
5
05/21/2120:17
WG1661391
5
04/29/2120:16
W G1663337
1
05/05/21 0240
W G1659614
1
04/27/21 23:00
WG1662396
1
05/03/21 09:00
W G1660742
1
04/28/21 23:16
W G1663442
1
05/05/21 22:00
W G1658339
1
04/26/211414
W G16582 86
1
04/26/2118:17
Collected by
Carrigan Harris
Batch
Dilution
Preparation
date/time
W G1658938
1
04/27/2110:19
WG1664139
50
05/05/211114
WG1664073
250
05/04/2114:26
WG1663981
1
05/04/21 22:00
WG1664552
1000
05/04/2114:26
WG1661488
25
04/30/2105:14
WG1659250
20
04/27/211108
W G1662397
1
05/01/21 08:51
WG1662910
1
05/03/21 00:09
WG1661811
10
04/30/2110:40
WG1663698
5
05/05/211411
Collected date/time Received date/time
04/20/211120 04/23/2115:00
Cp
Analysis
date/time
05/03/21 02:07
04/29/2113:51
05/23/21 09:35
04/30/2113:11
05/05/2114:19
04/27/21 23:00
05/03/211100
04/29/21 08:31
05/05/21 22:00
04/28/2110:45
04/29/21 0130
Analyst
MMF
MSP
SDL
MSP
KAB
LDT
SAC
MCG
CO
ABL
CCE
Location
FC
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fn
Mt. Juliet, TN
Mt. Juliet, TN
Mt. Juliet, TN
Fr
Mt. Juliet, TN
Mt. Juliet, TN
Rc
Mt. Juliet, TN
Collected date/time Received date/time
04/20/211120 04/23/2115:00
[Al
Analysis
Analyst
Location
date/time
MMF
Mt. Juliet, TN
RC04/27/211127
05/05/211114
JD
Mt. Juliet, TN
05/05/21 08:03
SDL
Mt. Juliet, TN
05/04/21 22:00
JER
Mt. Juliet, TN
05/05/21 0918
SDL
Mt. Juliet, TN
04/30/21 2132
JER
Mt. Juliet, TN
04/27/211108
AKA
Mt. Juliet, TN
05/01/21 08:51
AMH
Mt. Juliet, TN
05/03/21 00:09
CO
Mt. Juliet, TN
05/01/21 22:20
SD
Mt. Juliet, TN
05/05/21 23:52
CCE
Mt. Juliet, TN
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343221 05/27/2111:23 3 of37

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
Rc
4�z
F,
Heather J Wagner
[Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 901213.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/903013.
Method 365.2: Phosphorus was analyzed out of hold on sample WW-2 (11343221-01) due to the need for re -analysis which could
not be completed within hold time.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343221 05/27/2111:23 4 of37

SAMPLE RESULTS - 01
L1343221
WW-2
Collected date/time: 04/20/21 11:20
Total Solids by Method 2540 G-2011
Result
Qualifier Dilution Analysis
Batch
Analyte %
date / time
Total Solids 2.92
Q 1 05/03/2021 02:07
WG1661921
Wet Chemistry by Method 350.1
Result (dry)
Qualifier RDL (dry) Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Ammonia Nitrogen 3110
342 1
04/29/202113:51 WG1659238
Wet Chemistry by Method 365.4M
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Phosphorus, Total 10200 Q 3420 5 05/23/202109:35 WG1675157
Wet Chemistry by Method 4500NOrg C-2011
Result (dry) Qualifier RDL (dry) Dilution Analysis
Analyte mg/kg mg/kg date / time
Kjeldahl Nitrogen, TKN 55100 3420 5 04/30/202113:11
Wet Chemistry by Method 9012 B
Batch
WG1661391
Result Qualifier
RDL
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250
1 05/05/202114:19
WG1663337
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Dilution Analysis
Batch
Analyte mg/kg
mg/kg
date / time
Reactive Sulfide ND
25.0
1 04/27/2021 23:00
WG1659614
Wet Chemistry by Method 9045D
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 7.22 T8 1 05/03/20211100 WG1662396
Sample Narrative:
L1343221-01 WG1662396: 7.22 at 22.3C
Wet Chemistry by Method 9056A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Nitrate -Nitrite ND 685 1 04/29/202108:31 WG1660742
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte Deg. F date / time
Ignitability DNI at170 1 05/05/2021 22:00 WG1663442
Mercury by Method 7471B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 1.37 1 04/28/202110:45 WG1658339
— FP
— Fc
FS
—
Fn—
—
Rc
�GI
— SAI
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343221 05/27/2111:23 5 of37

SAMPLE RESULTS - 01
L1343221
WW-2
Collected date/time: 04/20/21 11:20
Metals (ICP) by Method 6010D
Result (dry)
Analyte
mg/kg
Aluminum
ND
Arsenic
ND
Cadmium
ND
Calcium
ND
Copper
ND
Lead
196
Magnesium
ND
Molybdenum
ND
Nickel
ND
Potassium
ND
Selenium
ND
Sodium
ND
Zinc
ND
Qualifier RDL (dry)
mg/kg
685
68.5
17.1
3420
68.5
17.1
3420
17.1
68.5
1710
68.5
3420
171
Dilution Analysis
date / time
1 04/29/2021 0130
1 04/29/2021 0130
1 04/29/2021 0130
1 04/29/2021 0130
1 04/29/2021 0130
1 04/29/2021 0130
1 04/29/2021 0130
1 04/29/2021 0130
1 04/29/2021 0130
1 04/29/2021 0130
1 04/29/2021 0130
1 04/29/2021 0130
1 04/29/2021 0130
Batch
WG1658286
WG1658286
WG1658286
WG1658286
WG1658286
WG1658286
WG1658286
WG1658286
WG1658286
WG1658286
WG1658286
WG1658286
WG1658286
ACCOUNT: PROJECT: SDG:
Hunt Environmental Associates L1343221
DATE/TIME:
05/27/21 11:28
PAGE:
6 of 37

SAMPLE RESULTS - 02
L1343221
WW-2
Collected date/time: 04/20/21 11:20
Total Solids by Method 2540B
Result Qualifier Dilution Analysis Batch
Analyte mg/I date / time
Total Solids 27400 1 04/27/20211127 WG1658938
Wet Chemistry by Method 350.1
Result Qualifier RDL
Analyte mg/I mg/I
Ammonia Nitrogen 214 12.5
Wet Chemistry by Method 351.2
Result Qualifier
RDL
Analyte mg/I
mg/I
Kjeldahl Nitrogen, TKN 1600
62.5
Sample Narrative:
L1343221-02 WG1664073: dilution due to nitrate interference
Wet Chemistry by Method 353.2
Result Qualifier
RDL
Analyte mg/I
mg/I
Nitrate -Nitrite ND
0.100
Wet Chemistry by Method 365.4
Result Qualifier RDL
Analyte mg/I mg/I
Phosphorus, Total 511 100
Wet Chemistry by Method 4500 CN E-2011
Result Qualifier RDL
Analyte mg/I mg/I
Reactive Cyanide ND 0.125
Wet Chemistry by Method 9034-9030B
Dilution Analysis Batch
date / time
50 05/05/20211114 WG1664139
Dilution Analysis Batch
date / time
250 05/05/202108:03 WG1664073
Dilution Analysis Batch
date / time
1 05/04/202122:00 WG1663981
Dilution Analysis Batch
date / time
1000 05/05/202109:18 WG1664552
Dilution Analysis Batch
date / time
25 04/30/20212132 WG1661488
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Reactive Sulfide 1.86 1.00 20 04/27/20211108 WG1659250
Wet Chemistry by Method 9040C
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 6.95 T8 1 05/01/202108:51 WG1662397
Sample Narrative:
L1343221-02 WG1662397: 6.95 at20.4C
Wet Chemistry by Method D93/1010A
Result
Qualifier Dilution
Analysis Batch
Analyte deg F
date/time
Flashpoint DNF at170
1
05/03/2021 00:09 WG1662910
Mercury by Method 7470A
Result
Qualifier RDL
Dilution Analysis Batch
Analyte mg/I
mg/I
date / time
Mercury 0.00527
0.00200
10 05/01/202122:20 WG1661811
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1343221 05/27/2111:23 7 of37

WW-2
Collected date/time: 04/20/21 11:20
Metals (ICP) by Method 6010D
SAMPLE
RESULTS - 02
L1343221
Result
Qualifier RDL
Dilution Analysis
Batch
FPAnalyte
mg/I
mg/I
date / time
Aluminum
660
1.00
5 05/05/202123:52
WG1663698
F
Arsenic
0.167
0.0500
5 05/05/202123:52
WG1663698
Cadmium
0.0244
0.0100
5 05/05/202123:52
WG1663698
Calcium
344
5.00
5 05/05/202123:52
WG1663698
Fss]
Copper
16.4
0.0500
5 05/05/202123:52
WG1663698
Lead
0.552
0.0300
5 05/05/202123:52
WG1663698
Fn
Magnesium
56.8
5.00
5 05/05/202123:52
WG1663698
Molybdenum
0.138
0.0250
5 05/05/202123:52
WG1663698
Nickel
0.516
0.0500
5 05/05/202123:52
WG1663698
Potassium
91.5
10.0
5 05/05/202123:52
WG1663698
Selenium
0.149
0.0500
5 05/05/202123:52
WG1663698
F
Sodium
454
15.0
5 05/05/202123:52
WG1663698
Zinc
24.3
0.250
5 05/05/202123:52
WG1663698
F,
F
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343221 05/27/2111:23 3 of37

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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
RDL (dry)
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fc
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
F
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Rc
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
E
The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial
calibration (ICAL).
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix interfered with the ability to make any accurate determination, spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
Q
Sample was prepared and/or analyzed past holding time as defined in the method. Concentrations should be
considered minimum values.
T8
Sample(s) received past/too close to holding time expiration.
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1343221 05/27/2111:23 34 of37

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1343221 05/27/2111:23 35 of37

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From 4/1/2021 To
WQ Permit Number:
NPDES Number:
6/30/2021
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
Alt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens u
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Composting ❑ jAerobic Digestion IZ
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
inSlud e
Pathogen Density
Number ol
Excee-
deuces
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
ni ue
inim
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
46600
51500
92700
CFU/ g
Quarterly
Qu Y
Grab
222D-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC
Preparer Name and Title (type or print)
Signature of Prepare *
Michael C Hunt, ORC
Land Applier Name and Title (if applicable)(type or print)
2/22/2022
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

I
Cameron Testing Services, Inc. Laboratory Report
NC DENR#654
NC PHHS #37799
US EPA #NC01918
Client:
Enviro Choice CTS Proj.
2104-218
D1N Cert # 37799
Project:
City
of LUmberton Regulatory
Yes
Sample Information
Sampled
Date 04/27/21 Received
M. Autry ate
04/27/21
Analyses and Results
" f_ab c
Sample ID
a Analyte Result
M ca c
Std.Methods
+°
1X _J
a
Reference
2104-218
-01
3ludge Gr Fec. Coliform-S <46600
CFUlg
46600
04/28/21 RL
9222D - MF
-02
<46700
CFU1g
46700
-03
<46600
CFUIg
46600
-04
92700
#
46300
-05
<46700
CFUlg
46700
-06
46600
CFurg
46600
-07
<46700
CFUrg
46700
Geomean 51500
2104-218
-01
3iudgE Gr TS (%) 2.15%
001
04/28/21 RL
2540 G JS
-02
2.14%
0.01
-03
2.15%
0.01
-04
2.16%
0.01
-05
2.14%
0.01
-06
2.14%
0.01
-07
214%
0.01
Report -
Review
Lab i ctor
1— � c�-f`
Date
219 S. Steele Str.
Sanford NC 27330
919-208-4240
[e-mail] camerontcsting.com

13
ace Analytical ' ANALYTICAL REPORT
August 26, 2021
Revised Report
Hunt Environmental Associates
Sample Delivery Group: L1381975
Samples Received: 07/23/2021
Project Number:
Description: Enviro-Choice Recycling
Report To: Cody Hunt
3330 Saddletree Road
Lumberton, NC 28359
Entire Report Reviewed By: 4�41
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy ofthe information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1331975 03/26/21 13:47 1 of 52

TABLE OF CONTENTS
Cp: Cover Page
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
5
Sr: Sample Results
6
Fss]
WW-3 L1381975-01
6
Fn
WW-3 L1381975-02
8
WW-3 L1381975-03
10
Fr
WW-3 L1381975-04
12
Qc: Quality Control Summary
14
Rc
Total Solids by Method 2540 G-2011
14
F
Total Solids by Method 2540B
15
Wet Chemistry by Method 350.1
16
[Al
Wet Chemistry by Method 351.2
18
Wet Chemistry by Method 353.2
19
RC
Wet Chemistry by Method 365.4
20
Wet Chemistry by Method 365.4M
21
Wet Chemistry by Method 4500 CN E-2011
22
Wet Chemistry by Method 4500 S2 D-2011
24
Wet Chemistry by Method 4500NOrg C-2011
25
Wet Chemistry by Method 9012 B
26
Wet Chemistry by Method 9034-9030B
27
Wet Chemistry by Method 9040C
28
Wet Chemistry by Method 9045D
29
Wet Chemistry by Method 9056A
30
Wet Chemistry by Method D93/1010A
31
Mercury by Method 7470A
33
Mercury by Method 7471B
35
Metals (ICP) by Method 6010B
36
Metals (ICP) by Method 6010D
37
Volatile Organic Compounds (GC/MS) by Method 8260B
41
Chlorinated Acid Herbicides (GC) by Method 8151A
43
Pesticides (GC) by Method 8081B
44
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
45
GI: Glossary of Terms
47
Al: Accreditations & Locations
49
Sc: Sample Chain of Custody
50
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates L1331975
03/26/21 13:47
2 of 52

SAMPLE SUMMARY
Collected by
Collected date/time
Received date/time
WW-3 L1381975-01 Solid
Carrigan Harris
07/22/2108:30
07/23/2108:30
FP
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
TC
Total Solids by Method 2540 G-2011
WG1727999
1
08/23/2116:04
08/23/2116:29
MMF
Mt. Juliet, TN
Wet Chemistry by Method 350.1
WG1711470
1
07/26/211134
07/28/21 02:48
SDL
Mt. Juliet, TN
Wet Chemistry by Method 365.4M
WG1720789
5
08/11/2115:42
08/12/2110:33
KEG
Mt. Juliet, TN
Wet Chemistry by Method 4500NOrg C-2011
WG1713310
5
07/28/21 2153
07/30/21 02:34
SDL
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1715694
1
08/02/2110:55
08/03/2112:12
KEG
Mt. Juliet, TN
Fn
Wet Chemistry by Method 9034-9030B
WG1714014
1
07/29/21 22:00
07/29/21 22:00
LDT
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1711572
1
07/26/21 09:00
07/26/211100
BMD
Mt. Juliet, TN
Wet Chemistry by Method 9056A
WG1713769
1
07/29/2122:51
07/30/2108:36
GB
Mt. Juliet, TN
Fr
Wet Chemistry by Method D93/1010A
WG1712853
1
07/28/21 20:41
07/28/21 20:41
CAT
Mt. Juliet, TN
Mercury by Method 7471B
WG1711402
1
07/27/21 09:31
07/27/2116:07
BMF
Mt. Juliet, TN
Rc
Metals (ICP) by Method 6010D
WG1711294
1
08/01/2122:28
08/05/21 05:46
CCE
Mt. Juliet, TN
�GI
Collected by
Collected date/time
Received date/time
WW-3 L1381975-02 GW
Carrigan Harris
07/22/21 08:30
07/23/21 08:30
SAI
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Solids by Method 2540B
WG1712724
1
07/27/2118:32
07/27/2118:36
MMF
Mt. Juliet, TN
RCTotal
Wet Chemistry by Method 350.1
WG1718757
20
08/10/2113:12
08/10/2113:12
SL
Mt. Juliet, TN
Wet Chemistry by Method 351.2
WG1715100
200
08/02/2113:11
08/03/2115:53
KEG
Mt. Juliet, TN
Wet Chemistry by Method 353.2
WG1714605
1
08/03/2113:13
08/03/2113:13
JER
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1716554
100
08/02/2113:11
08/06/21 23:41
SDL
Mt. Juliet, TN
Wet Chemistry by Method 4500 CN E-2011
WG1714403
1
07/30/2116:18
07/31/21 00:00
SDL
Mt. Juliet, TN
Wet Chemistry by Method 4500 S2 D-2011
WG1710908
50
07/27/2117:27
07/27/2117:27
ARM
Mt. Juliet, TN
Wet Chemistry by Method 9040C
WG1711426
1
07/25/2113:00
07/25/2113:00
BMD
Mt. Juliet, TN
Wet Chemistry by Method D93/1010A
WG1711514
1
07/26/211100
07/26/211100
KAB
Mt. Juliet, TN
Mercury by Method 7470A
WG1711149
1
07/25/2110:25
07/26/211103
SD
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1714808
1
08/03/21 02:40
08/05/211122
CCE
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1714808
5
08/03/21 02:40
08/05/2114:01
CCE
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
WW-3 L1381975-03 Waste
Carrigan Harris
07/22/21 08:30
07/23/21 08:30
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Preparation by Method 1311
WG1712201
1
07/27/2116:02
07/27/2116:02
IDW
Mt. Juliet, TN
Preparation by Method 1311
WG1712721
1
07/28/2111:28
07/28/211128
APH
Mt. Juliet, TN
Mercury by Method 7470A
WG1713699
1
07/29/21 09:20
07/29/2114:11
ABL
Mt. Juliet, TN
Metals (ICP) by Method 6010B
WG1713941
1
07/29/2112:03
07/30/21 03:01
CCE
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B
WG1713357
1
07/29/21 03:54
07/29/21 03:54
JHH
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1713691
1
07/29/2110:32
07/29/2119:21
AO
Mt. Juliet, TN
Pesticides (GC) by Method 8081B
WG1714408
1
07/31/2114:16
08/02/2115:34
HMH
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270C
WG1714064
1
07/30/21 06:27
07/30/2118:49
AMG
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
WW-3 L1381975-04 Waste
Carrigan Harris
07/22/21 08:30
07/23/21 08:30
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
Preparation by Method 1311
WG1712201
1
07/27/2116:02
07/27/2116:02
IDW
Mt. Juliet, TN
Preparation by Method 1311
WG1712721
1
07/28/211128
07/28/211128
APH
Mt. Juliet, TN
Mercury by Method 7470A
WG1713699
1
07/29/21 09:20
07/29/2114:13
ABL
Mt. Juliet, TN
Metals (ICP) by Method 6010B
WG1713941
1
07/29/2112:03
07/30/21 03:03
CCE
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260B
WG1713357
1
07/29/21 0415
07/29/21 04:15
JHH
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1713691
1
07/29/2110:32
07/29/2119:36
AO
Mt. Juliet, TN
Pesticides (GC) by Method 8081B
WG1714408
1
07/31/2114:16
08/02/2115:46
HMH
Mt. Juliet, TN
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates
L1331975
03/26/2113:47
3 of 52

SAMPLE SUMMARY
Collected by Collected date/time Received date/time
WW-3 L1381975-04 Waste Carrigan Harris 07/22/21 08:30 07/23/21 08:30 , C
P
Method Batch
Semi Volatile Organic Compounds (GC/MS) by Method 8270C WG1714064
Dilution Preparation Analysis
date/time date/time
1 07/30/2106:27 07/30/2119:11
Analyst
AMG
Location
FC
Mt. Juliet, TN
F
Fn
Fr
Rc
F,
F
RC
ACCOUNT: PROJECT: SDG:
Hunt Environmental Associates L1331975
DATE/TIME: PAGE:
03/26/21 13:47 4 of 52

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
Rc
4�z
F,
Heather J Wagner
F
Project Manager
RC
Report Revision History
Level II Report -Version 1: 03/12/21 1414
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Cyanide results reported in the attached report were determined as totals using method 4500 CN E-2011.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013.
All Reactive Sulfide results reported in the attached report were determined as totals using method 4500 S2 D-2011.
Revised Report: Revised to include total solids on sample WW-3 (11381975-01). This report replaces the report issued 3/12/2021.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1331975 03/26/21 13:47 5 of 52

SAMPLE RESULTS - 01
L1381975
WW-3
Collected date/time: 07/22/21 08:30
Total Solids by Method 2540 G-2011
Result
Qualifier Dilution Analysis
Batch
Analyte %
date / time
Total Solids 2.32
T8 1 08/23/202116:29
WG1727999
Wet Chemistry by Method 350.1
Result (dry)
Qualifier RDL (dry) Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Ammonia Nitrogen 4400
431 1
07/28/2021 02:48 WG1711470
Wet Chemistry by Method 365.4M
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Phosphorus, Total 20000 4310 5 08/12/202110:33 WG1720789
Wet Chemistry by Method 4500NOrg C-2011
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Kjeldahl Nitrogen, TKN 42000 4310 5 07/30/2021 02:34 WG1713310
Wet Chemistry by Method 9012 B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Cyanide ND J6
0.250
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Sulfide ND
25.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 08/03/202112:12 WG1715694
Dilution Analysis Batch
date / time
1 07/29/202122:00 WG1714014
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 7.51 T8 1 07/26/20211100 WG1711572
Sample Narrative:
L1381975-01 WG1711572: 7.51 at 24.1C
Wet Chemistry by Method 9056A
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Nitrate -Nitrite ND 862 1 07/30/202108:36 WG1713769
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte Deg. F date / time
Ignitability DNI at170 1 07/28/2021 20:41 WG1712853
Mercury by Method 7471B
Result (dry) Qualifier RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Mercury ND 1.72 1 07/27/202116:07 WG1711402
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1331975 03/26/21 13:47 6 of 52

WW-3
Collected date/time: 07/22/21 08:30
Metals (ICP) by Method 6010D
SAMPLE
RESULTS - 01
L1381975
Result (dry)
Qualifier RDL (dry)
Dilution Analysis
Batch
FPAnalyte
mg/kg
mg/kg
date / time
Aluminum 33000
862
1 08/05/202105:46
WG1711294
FC
Arsenic ND
86.2
1 08/05/20210546
WG1711294
Cadmium ND
21.6
1 08/05/202105:46
WG1711294
Calcium 16300
4310
1 08/05/202105:46
WG1711294
Fss]
Copper 403
86.2
1 08/05/20210546
WG1711294
Lead 24.5
21.6
1 08/05/202105:46
WG1711294
Fn
Magnesium ND
4310
1 08/05/20210546
WG1711294
Molybdenum ND
21.6
1 08/05/20210546
WG1711294
Nickel ND
86.2
1 08/05/202105:46
WG1711294
Potassium 4620
2160
1 08/05/20210546
WG1711294
Selenium ND
86.2
1 08/05/202105:46
WG1711294
F
Sodium 33900
4310
1 08/05/202105:46
WG1711294
Zinc 949
216
1 08/05/202105:46
WG1711294
F,
F
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates
L1331975
03/26/21 13:47
7 of 52

SAMPLE RESULTS - 02
L1381975
WW-3
Collected date/time: 07/22/21 08:30
Total Solids by Method 2540B
Result Qualifier Dilution Analysis Batch
Analyte mg/I date / time
Total Solids 22400 1 07/27/202118:36 WG1712724
Wet Chemistry by Method 350.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Ammonia Nitrogen 118 5.00 20 08/10/202113:12 WG1718757
Wet Chemistry by Method 351.2
Result Qualifier
RDL
Analyte mg/I
mg/1
Kjeldahl Nitrogen, TKN 960
50.0
Sample Narrative:
L1381975-02 WG1715100: dilution due to nitrate interference
Wet Chemistry by Method 353.2
Result Qualifier
RDL
Analyte mg/I
mg/I
Nitrate -Nitrite 0.770
0.100
Wet Chemistry by Method 365.4
Result Qualifier RDL
Analyte mg/I mg/I
Phosphorus, Total 186 10.0
Wet Chemistry by Method 4500 CN E-2011
Dilution Analysis Batch
date / time
200 08/03/202115:53 WG1715100
Dilution Analysis Batch
date / time
1 08/03/202113:13 WG1714605
Dilution Analysis Batch
date / time
100 08/06/202123:41 WG1716554
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Reactive Cyanide 0.00756 0.00500 1 07/31/2021 00:00 WG1714403
Wet Chemistry by Method 4500 S2 D-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Reactive Sulfide 7.65 2.50 50 07/27/202117:27 WG1710908
Wet Chemistry by Method 9040C
Result Qualifier Dilution Analysis Batch
Analyte su date / time
pH 7.30 T8 1 07/25/202113:00 WG1711426
Sample Narrative:
L1381975-02 WG1711426: 7.3 at21.9C
Wet Chemistry by Method D93/1010A
Result
Qualifier Dilution
Analysis
Batch
Analyte deg F
date/time
Flashpoint DNF at170
1
07/26/20211100
WG1711514
Mercury by Method 7470A
Result
Qualifier RDL
Dilution
Analysis Batch
Analyte mg/I
mg/I
date / time
Mercury 0.000820
0.000200
1
07/26/202111:03 WG1711149
ACCOUNT:
PROJECT:
SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1331975 03/26/21 13:47 3 of 52

WW-3
Collected date/time: 07/22/21 08:30
Metals (ICP) by Method 6010D
SAMPLE
RESULTS - 02
L1381975
Result
Qualifier RDL Dilution Analysis
Batch
FPAnalyte
mg/I
mg/I
date / time
Aluminum
620
1.00 5
08/05/202114:01
WG1714808
F
Arsenic
0.189
0.0100 1
08/05/20211122
WG1714808
Cadmium
0.0172
0.00200 1
08/05/20211122
WG1714808
Calcium
314
1.00 1
08/05/20211122
WG1714808
Fss]
Copper
8.71
0.0100 1
08/05/20211122
WG1714808
Lead
0.418
0.00600 1
08/05/20211122
WG1714808
Fn
Magnesium
42.2
1.00 1
08/05/20211122
WG1714808
Molybdenum
0.0823
0.00500 1
08/05/20211122
WG1714808
Nickel
0.545
0.0100 1
08/05/20211122
WG1714808
Potassium
80.1
2.00 1
08/05/20211122
WG1714808
Selenium
0.0434
0.0100 1
08/05/20211122
WG1714808
Rc
Sodium
692
3.00 1
08/05/20211122
WG1714808
Zinc
17.8
0.0500 1
08/05/20211122
WG1714808
F,
F
RC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1331975 03/26/21 13:47 9 of 52

SAMPLE RESULTS - 03
L1381975
WW-3
Collected date/time: 07/22/21 08:30
Preparation by Method 1311
Result
Qualifier Prep
Batch
Analyte
date / time
TCLP Extraction
7/28/20211128:48 AM
WG1712721
TCLP ZHE Extraction -
7/27/20214:02:32 PM
WG1712201
Fluid 1
7/28/20211128:48 AM
WG1712721
Initial pH 6.64
7/28/20211128:48 AM
WG1712721
Final pH 4.90
7/28/20211128:48 AM
WG1712721
Mercury by Method 7470A
Result
Qualifier RDL Limit
Dilution Analysis Batch
Analyte mg/I
mg/I mg/I
date/time
Mercury ND
0.0100 0.20
1 07/29/202114:11 WG1713699
Metals (ICP) by Method 6010B
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Arsenic
ND
0.100
5
1 07/30/20210301
WG1713941
Barium
ND
0.100
100
1 07/30/20210301
WG1713941
Cadmium
ND
0.100
1
1 07/30/202103:01
WG1713941
Chromium
ND
0.100
5
1 07/30/202103:01
WG1713941
Lead
ND
0.100
5
1 07/30/20210301
WG1713941
Selenium
ND
0.100
1
1 07/30/202103:01
WG1713941
Silver
ND
0.100
5
1 07/30/20210301
WG1713941
Volatile Organic Compounds (GC/MS) by Method 8260B
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Benzene
ND
J3
0.0500
0.50
1 07/29/202103:54
WG1713357
Carbon tetrachloride
ND
J3
0.0500
0.50
1 07/29/2021 03:54
WG1713357
Chlorobenzene
ND
0.0500
100
1 07/29/202103:54
WG1713357
Chloroform
ND
0.250
6
1 07/29/202103:54
WG1713357
1,2-Dichloroethane
ND
0.0500
0.50
1 07/29/202103:54
WG1713357
1,1-Dichloroethene
ND
0.0500
0.70
1 07/29/202103:54
WG1713357
2-Butanone (MEK)
ND
0.500
200
1 07/29/2021 03:54
WG1713357
Tetrachloroethene
ND
J3
0.0500
0.70
1 07/29/202103:54
WG1713357
Trichloroethene
ND
J3
0.0500
0.50
1 07/29/202103:54
WG1713357
Vinyl chloride
ND
J3
0.0500
0.20
1 07/29/2021 03:54
WG1713357
(S) Toluene-dH
101
80.0-120
071291202103.54
WG1713357
(S) 4-Bromofluorobenzene
88.6
77.0-126
071291202103.54
WG1713357
(S) 1,2-Dichloroethane-d4
ill
70.0-130
071291202103.54
WG1713357
Chlorinated Acid Herbicides (GC)
by Method
8151A
Result Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
2,4,5-TP (Silvex)
ND
0.00200
1
1 07/29/202119:21
WG1713691
2,4-D
ND
0.00200
10
1 07/29/202119:21
WG1713691
(S) Z4-Dichlorophenyl Acetic Acid
63.6
14.0-158
071291202119.21
WG1713691
Pesticides (GC) by Method
8081B
Result Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 08/02/202115:34
WG1714408
Endrin
ND
0.00500
0.02
1 08/02/202115:34
WG1714408
Heptachlor
ND
0.00500
0.0080
1 08/02/202115:34
WG1714408
Lindane
ND
0.00500
0.40
1 08/02/202115:34
WG1714408
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1331975 03/26/21 13:47 10 of 52

WW-3
Collected date/time: 07/22/21 08:30
Pesticides (GC) by Method 8081B
Result
Analyte mg/I
Methoxychlor ND
Toxaphene ND
(S) Decochlorobiphenyl 46.5
(S) Tetrochloro-m-xylene 72.0
Semi Volatile Organic Compounds
SAMPLE RESULTS
L1381975
Qualifier RDL Limit Dilution
mg/I mg/I
0.00500 10 1
0.0100 0.50 1
10.0-128
10.0-127
(GC/MS) by Method 8270C
- 03
Analysis
date/time
08/02/202115:34
08/02/202115:34
081021202115.34
081021202115.34
Batch
WG1714408
WG1714408
WG1714408
WG1714408
F
Fc
SS
F
Fn
Result
Qualifier RDL
Limit Dilution
Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene ND
0.100
7.50 1
07/30/202118:49
WG1714064
2,4-Dinitrotoluene ND
0.100
0.13 1
07/30/202118:49
WG1714064
6
Hexachlorobenzene ND
0.100
0.13 1
07/30/202118:49
WG1714064
QC
Hexachloro-1,3-butadiene ND
0.100
0.50 1
07/30/202118:49
WG1714064
Hexachloroethane ND
0.100
3 1
07/30/202118:49
WG1714064
F
Nitrobenzene ND
0.100
2 1
07/30/202118:49
WG1714064
Pyridine ND
0.100
5 1
07/30/202118:49
WG1714064
e
3&4-Methyl Phenol ND
0.100
400 1
07/30/202118:49
WG1714064
AI
2-Methylphenol ND
0.100
200 1
07/30/202118:49
WG1714064
Pentachlorophenol ND
0.100
100 1
07/30/202118:49
WG1714064
F
2,4,5-Trichlorophenol ND
0.100
400 1
07/30/202118:49
WG1714064
2,4,6-Trichlorophenol ND
0.100
2 1
07/30/202118:49
WG1714064
(S) 2-Fluorophenol 27.0
10.0-120
071301202118.49
WG1714064
(S) Phenol-d5 16.0
10.0-120
071301202118.49
WG1714064
(S) Nitrobenzene-d5 55.6
10.0-127
071301202118.49
WG1714064
(S) 2-Fluorobiphenyl 58.5
10.0-130
071301202118.49
WG1714064
(S)2,4,6-Tribromophenol 60.0
10.0-155
071301202118.49
WG1714064
(S) p-Terphenyl-d14 56.8
10.0-128
071301202118.49
WG1714064
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates
L1331975
03/26/2113:47
11 of 52

SAMPLE RESULTS - 04
L1381975
WW-3
Collected date/time: 07/22/21 08:30
Preparation by Method 1311
Result
Qualifier Prep
Batch
Analyte
date / time
TCLP Extraction
7/28/20211128:48 AM
WG1712721
TCLP ZHE Extraction -
7/27/20214:02:32 PM
WG1712201
Fluid 1
7/28/20211128:48 AM
WG1712721
Initial pH 6.68
7/28/20211128:48 AM
WG1712721
Final pH 4.90
7/28/20211128:48 AM
WG1712721
Mercury by Method 7470A
Result
Qualifier RDL Limit
Dilution Analysis Batch
Analyte mg/I
mg/I mg/I
date/time
Mercury ND
0.0100 0.20
1 07/29/202114:13 WG1713699
Metals (ICP) by Method 6010B
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Arsenic
ND
0.100
5
1 07/30/20210303
WG1713941
Barium
ND
0.100
100
1 07/30/20210303
WG1713941
Cadmium
ND
0.100
1
1 07/30/202103:03
WG1713941
Chromium
ND
0.100
5
1 07/30/202103:03
WG1713941
Lead
ND
0.100
5
1 07/30/20210303
WG1713941
Selenium
0.116
B 0.100
1
1 07/30/20210303
WG1713941
Silver
ND
0.100
5
1 07/30/20210303
WG1713941
Volatile Organic Compounds (GC/MS) by Method 8260B
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Benzene
ND
J3
0.0500
0.50
1 07/29/20210415
WG1713357
Carbon tetrachloride
ND
J3
0.0500
0.50
1 07/29/2021 0415
WG1713357
Chlorobenzene
ND
0.0500
100
1 07/29/20210415
WG1713357
Chloroform
ND
0.250
6
1 07/29/20210415
WG1713357
1,2-Dichloroethane
ND
0.0500
0.50
1 07/29/20210415
WG1713357
1,1-Dichloroethene
ND
0.0500
0.70
1 07/29/20210415
WG1713357
2-Butanone (MEK)
ND
0.500
200
1 07/29/2021 0415
WG1713357
Tetrachloroethene
ND
J3
0.0500
0.70
1 07/29/20210415
WG1713357
Trichloroethene
ND
J3
0.0500
0.50
1 07/29/20210415
WG1713357
Vinyl chloride
ND
J3
0.0500
0.20
1 07/29/2021 0415
WG1713357
(S) Toluene-dH
101
80.0-120
071291202104.15
WG1713357
(S) 4-Bromofluorobenzene
88.7
77.0-126
071291202104.15
WG1713357
(S) 1,2-Dichloroethane-d4
ill
70.0-130
071291202104.15
WG1713357
Chlorinated Acid Herbicides (GC)
by Method
8151A
Result Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
2,4,5-TP (Silvex)
ND
0.00200
1
1 07/29/202119:36
WG1713691
2,4-D
ND
0.00200
10
1 07/29/202119:36
WG1713691
(S) Z4-Dichlorophenyl Acetic Acid
65.2
14.0-158
071291202119.36
WG1713691
Pesticides (GC) by Method
8081B
Result Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
Chlordane
ND
0.00500
0.03
1 08/02/202115:46
WG1714408
Endrin
ND
0.00500
0.02
1 08/02/202115:46
WG1714408
Heptachlor
ND
0.00500
0.0080
1 08/02/202115:46
WG1714408
Lindane
ND
0.00500
0.40
1 08/02/202115:46
WG1714408
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1331975 03/26/2113:47 12 of 52

WW-3
Collected date/time: 07/22/21 08:30
Pesticides (GC) by Method 8081B
Result
Analyte mg/I
Methoxychlor ND
Toxaphene ND
(S) Decochlorobiphenyl 81.2
(S) Tetrochloro-m-xylene 86.6
Semi Volatile Organic Compounds
SAMPLE RESULTS
L1381975
Qualifier RDL Limit Dilution
mg/I mg/I
0.00500 10 1
0.0100 0.50 1
10.0-128
10.0-127
(GC/MS) by Method 8270C
- 04
Analysis
date/time
08/02/202115:46
08/02/202115:46
081021202115.46
081021202115.46
Batch
WG1714408
WG1714408
WG1714408
WG1714408
F
Fc
SS
F
Fn
Result
Qualifier RDL
Limit Dilution
Analysis
Batch
Analyte mg/I
mg/I
mg/I
date/time
1,4-Dichlorobenzene ND
0.100
7.50 1
07/30/202119:11
WG1714064
2,4-Dinitrotoluene ND
0.100
0.13 1
07/30/202119:11
WG1714064
6
Hexachlorobenzene ND
0.100
0.13 1
07/30/202119:11
WG1714064
QC
Hexachloro-1,3-butadiene ND
0.100
0.50 1
07/30/202119:11
WG1714064
Hexachloroethane ND
0.100
3 1
07/30/202119:11
WG1714064
F
Nitrobenzene ND
0.100
2 1
07/30/202119:11
WG1714064
Pyridine ND
0.100
5 1
07/30/202119:11
WG1714064
e
3&4-Methyl Phenol ND
0.100
400 1
07/30/202119:11
WG1714064
AI
2-Methylphenol ND
0.100
200 1
07/30/202119:11
WG1714064
Pentachlorophenol ND
0.100
100 1
07/30/202119:11
WG1714064
F
2,4,5-Trichlorophenol ND
0.100
400 1
07/30/202119:11
WG1714064
2,4,6-Trichlorophenol ND
0.100
2 1
07/30/202119:11
WG1714064
(S) 2-Fluorophenol 34.0
10.0-120
071301202119.11
WG1714064
(S) Phenol-d5 22.1
10.0-120
071301202119.11
WG1714064
(S) Nitrobenzene-d5 62.3
10.0-127
071301202119.11
WG1714064
(S) 2-Fluorobiphenyl 65.7
10.0-130
071301202119.11
WG1714064
(S)2,4,6-Tribromophenol 67.5
10.0-155
071301202119.11
WG1714064
(S) p-Terphenyl-d14 67.3
10.0-128
071301202119.11
WG1714064
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates
L1331975
03/26/21 13:47
13 of 52

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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
(dry)
Results are reported based on the dry weight ofthe sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
Fn
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
RDL (dry)
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fc
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
F
reported.
Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
R
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
B
The same analyte is found in the associated blank.
E
The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial
calibration (ICAL).
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J2
Surrogate recovery limits have been exceeded, values are outside lower control limits.
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix interfered with the ability to make any accurate determination, spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination, spike value is low.
P RPD between the primary and confirmatory analysis exceeded 40%.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
ACCOUNT: PROJECT: SDG: DATE/TIME:
PAGE:
47 of 52
Hunt Environmental Associates
L1331975 03/26/21 13:47

GLOSSARY OF TERMS
Qualifier Description
T8
V
Sample(s) received past/too close to holding time expiration.
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1331975 03/26/21 13:47 43 of 52

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1331975 03/26/21 13:47 49 of 52

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From 7/1/2021 To
WQ Permit Number:
NPDES Number:
9/30/2021
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
Alt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens u
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Composting ❑ jAerobic Digestion IZ
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
inSlud e
Pathogen Density
Number ol
Excee-
deuces
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
ni ue
inim
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
40000
40500
40800
CFU/ g
Quarterly
Qu Y
Grab
222D-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC
Preparer Name and Title (type o�rint)
W-) ')
Signature of Preparer*
2/28/2022
Date
Michael C Hunt, ORC
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Cameron Testing Services, Inc. Laboratory Report
NC ❑ENR #654
NC PHHS #37799
US EPA #NC01918
Client:
Enviro-Choice Recycling CTS Proj.
2107_02e9
OW Cert# 37799
Project:
City of Lumberton Regulatory
Yes
Sample Information
Sampled
C. Harris 07/22/21 Received
R. Lloyd QaW
07/22/21
Analyses and Results
Lab I❑
Sample 1Q E o 2 Analyte Result
' y_
Std. Methods
v
D
a r
Reference
d
2107-0209
-01 3ludge Gr Fec. Coliform-S <40800
cFulg
40800 07/22/21 RL
9222D - €NF
-02 <40700
crurg
40700
-03 <40500
Uuwg
40500
-04 <40600
CFug
40600
-05 <40700
CFulg
40700
-06 <40300
CFulo
40300
-07 <40000
Uuig
40000
Geomean <40500
2107-0209
-01 aIudgt Gr 7S (%) 2.45%
0•01 07/22/21 RL
2540 G JS
-02 2,46%
0.01
-03 2.47%
0.01
-04 2.47%
0.01
-05 2.46%
0.01
-06 2.48%
0.01
-07 2.50%
0.01
Report
Review
Project Manager
--Vg1"q 4�
Date
219 S. Steele Str.
Sanford NC 27330
919-2084240
[e-mail] camcrontesting.com

IGS VOA
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13
ace Analytical ' ANALYTICAL REPORT
December 20, 2021
Hunt Environmental Associates
Sample Delivery Group:-1431317
Samples Received: 11/13/2021
Project Number:
Description: City of Lumberton
Report To: Cody Hunt
3330 Saddletree Road
Lumberton, NC 28359
Entire Report Reviewed By: 4�41
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1431317 12/20/2110:16 1 of 20

TABLE OF CONTENTS
Cp: Cover Page
FP
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
,i
Fss]
4 L1431317-01
5
Fn
4 L1431317-02
i
Qc: Quality Control Summary
7
Fr
Wet Chemistry by Method 350.1
7
Wet Chemistry by Method 351.2
8
Rc
Wet Chemistry by Method 353.2
9
F
Wet Chemistry by Method 365.4
10
Wet Chemistry by Method 4500 CN E-2016
11
[Al
Wet Chemistry by Method 4500 S2 D-2011
12
Wet Chemistry by Method 9045D
13
RC
Wet Chemistry by Method D93/1010A
14
Mercury by Method 245.1
15
Metals (ICP) by Method 200.7
16
GI: Glossary of Terms
18
Al: Accreditations & Locations
19
Sc: Sample Chain of Custody
20
ACCOUNT: PROJECT:
SDG: DATE/TIME:
PAGE:
Hunt Environmental Associates
L1431317 12/20/2110:16
2 of 20

SAMPLE SUMMARY
4 L1431317-01 WW
Collected by
Carrigan Harris
Collected date/time
11/12/21 09:55
Received date/time
11/13/21 09:00
FP
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
F
Wet Chemistry by Method 350.1
WG1778749
50
11/24/211124
11/24/211124
SL
Mt. Juliet, TN
Wet Chemistry by Method 351.2
WG1779261
200
11/28/2110:06
12/17/2110:29
KEG
Mt. Juliet, TN
Wet Chemistry by Method 353.2
WG1785719
1
12/09/21 20:52
12/09/2120:52
LDT
Mt. Juliet, TN
Wet Chemistry by Method 365.4
WG1790778
20
11/28/2110:06
12/16/2118:00
KEG
Mt. Juliet, TN
Wet Chemistry by Method 4500 CN E-2016
WG1776396
10
11/18/2117:08
11/18/21 22:29
SDL
Mt. Juliet, TN
Fn
Wet Chemistry by Method 4500 S2 D-2011
WG1777670
50
11/20/21 00:07
11/20/21 00:07
UNP
Mt. Juliet, TN
Wet Chemistry by Method D93/1010A
WG1775415
1
11/17/21 03:53
11/17/21 03:53
WOS
Mt. Juliet, TN
Mercury by Method 245.1
WG1777130
10
11/21/211113
11/22/2116:31
ABL
Mt. Juliet, TN
Fr
Metals (ICP) by Method 200.7
WG1782896
5
12/03/2119:37
12/05/2113:59
CCE
Mt. Juliet, TN
Rc
Collected by
Collected date/time
Received date/time
4 L1431317-02 Solid
Carrigan Harris
11/12/2109:55
11/13/2109:00
7G1
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
F
Wet Chemistry by Method 9045D
WG1791616
1
12/17/2114:00
12/17/2118:00
SCM
Mt. Juliet, TN
RC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Hunt Environmental Associates
L1431317
12/20/2110:16
3 of 20

CASE NARRATIVE
FP
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
FS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
0
Fr
Rc
4�z
F,
Heather J Wagner
[Al
Project Manager
RC
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 4500 CN E-2016.
All Reactive Sulfide results reported in the attached report were determined as totals using method 4500 S2 D-2011.
Sample Delivery Group (SDG) Narrative
The following analysis were performed from an unpreserved, insufficiently or inadequately preserved sample.
Lab Sample ID Project Sample ID Method
L1431317-01 4 4500 CN E-2016
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1431317 12/20/2110:16 4 of 20

SAMPLE RESULTS - 01
L1431317
4
Collected date/time: 11/12/21 09:55
Wet Chemistry by Method 350.1
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Ammonia Nitrogen 174
12.5
50
11/24/20211124
WG1778749
Wet Chemistry by Method 351.2
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Kjeldahl Nitrogen, TKN 1470
50.0
200
12/17/202110:29
WG1779261
Wet Chemistry by Method 353.2
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date / time
Nitrate -Nitrite ND
Wet Chemistry by Method 365.4
0.100 1 12/09/202120:52 WG1785719
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I _ mg/I date/time
Phosphorus, Total 45.4 2.00 20 12/16/202118:00 WG1790778
Wet Chemistry by Method 4500 CN E-2016
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Reactive Cyanide 0.0748
0.0500
10
11/18/2021 22:29
WG1776396
Wet Chemistry by Method 4500 S2 D-2011
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Reactive Sulfide 21.4 T8
2.50
50
11/20/2021 00:07
WG1777670
Wet Chemistry by Method D93/1010A
— FP
— Fc
FS
-
Fn-
-
Rc
F,
[Al
Rc
Result
Analyte deg F
Flashpoint DNF at170
Mercury by Method 245.1
Qualifier Dilution
1
Analysis
date/time
11/17/2021 03:53
Batch
WG1775415
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Mercury 0.00509
0.00200
10
11/22/202116:31
WG1777130
Metals (ICP) by Method 200.7
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte mg/I
mg/I
date / time
Arsenic 0.250
0.0500
5
12/05/202113:59
WG1782896
Barium 4.61
0.0250
5
12/05/202113:59
WG1782896
Cadmium 0.0151
0.0100
5
12/05/202113:59
WG1782896
Chromium 1.91
0.0500
5
12/05/202113:59
WG1782896
Lead 0.323
0.0250
5
12/05/202113:59
WG1782896
Selenium 0.0754
0.0500
5
12/05/202113:59
WG1782896
Silver ND
0.0250
5
12/05/202113:59
WG1782896
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Hunt Environmental Associates
L1431317
12/20/2110:16 5 of 20

SAMPLE RESULTS - 02
L1431317
4
Collected date/time: 11/12/21 09:55
Wet Chemistry by Method 9045D
Result
Analyte su
pH 7.12
Sample Narrative:
L1431317-02 WG1791616:7.12 at19.7C
Qualifier Dilution Analysis Batch
date / time
T8 1 12/17/202118:00 WG1791616
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1431317 12/20/2110:16 6 of 20

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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
u
Fc
Fss]
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
Fn
RDL
Reported Detection Limit.
Rec.
Recovery.
Fr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Fc
Analyte
The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
F
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
LEI
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe
samples from the time of collection until delivery to the laboratory for analysis.
This section ofyour report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
E
The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial
calibration (ICAL).
J
The identification ofthe analyte is acceptable, the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J5
The sample matrix interfered with the ability to make any accurate determination, spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination, spike value is low.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8
Sample(s) received past/too close to holding time expiration.
v
The sample concentration is too high to evaluate accurate spike recoveries.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates
L1431317 12/20/2110:16 13 of 20

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
N E-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704 _
Georgia
NELAP
North Carolina 3
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky' 6
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee'"
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas5
LABO152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2 LA
A2LA— ISO17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A2 LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
Rc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Hunt Environmental Associates L1431317 12/20/2110:16 19 of 20

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lumberton
WWTP Name: City of Lumberton
Monitoring Period: From 10/1/2021 To
WQ Permit Number:
NPDES Number:
12/31 /2021
WQ0000672
NCL-024571
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)[]
Alt. C (Prior Testing)❑
Alt.D (No Prior Test)
I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray
Gamma Ray ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens u
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Composting ❑ jAerobic Digestion IZ
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
inSlud e
Pathogen Density
Number ol
Excee-
deuces
Frequency
of Analysis
Y
Sample
Type
Analytical
Tech -
ni ue
inim
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
57900
89100
291000
CFU/ g
Quarterly
Qu Y
Grab
222D-MF
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
colifonn)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAIL 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Michael C Hunt, ORC
Preparer Name and Title�or print)
/�j
Signature of Preparer
Michael C Hunt, ORC
Land Applier Name and Title (if applicable)(type or print)
2/28/2022
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Cameron Testing Services, Inc. Laboratory Report
NC DENR #654
NC PHHS #37799
US EPA #NC01918
Client:
Enviro-Choice
CTS Proj.
2111-0214 Dwcert#37799
Project:
City
of Lumberton
Regulatory
Yes
Sample Information
Sampled
C. Harris
Date 11/23/21
Received
J. Cameron
Date 11/23/21
Analyses and Results
Lab !D
Sample ID
x E
o Analyte
Result
E
ra `=
m E
N
}, :'
Y Std, Methods
r, �?
D
-J
C
= Reference
2111-0214
-01
Sludge Gr Fec.Coliform-S
<58200
cFurg
58200
11/23/21
RL 9222D-MF
-02
116000
GFUIg
57900
-03
57940
GFUIg
67900
-04
116000
eFUIg
57200
-05
<58300
cFUIg
58300
-06
291000
cFurg
58100
-07
<58100
cFUIg
58100
Geomean
89100
-01
3ludge Gr TS (%)
1.72%
0.01
11/23/21
RL 2540 G -TS
-02
1.73%
0,01
-03
1.73%
0.01
-04
1.72%
a.o1
-05
1.72%
0.01
-06
1.72%
0.01
-07
1.72%
0.01
Report
Review
Project Manager
Date
219 S. Steele Str.
Sanford NC 27330
919-208-4240
chris@camerontesting, com

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City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
� . : ' �s i ���%C'I I ti ���� o fo i •. I l � f � - r? r��� � ` �� jf j:
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
it 4�.j 3ii.
0.1247
24.94
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
19.00
8.24
1
19.00
8.13
2
18.00
7.85
3
18.00
7.43
4
18.00
6.99
5
18.00
6.57
6
18.00
6.18
7
18.00
5.74
8
18.00
5.28
9
18.00
4.81
10
18.00
4.33
11
18.00
3.84
12
18.00
3.35
13
18.00
2.84
14
18.00
2.31
15
18.00
1.65
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
mL
9
9
9
g/L
0.45 mg/L/minute
1.08 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
18.125
If sewage sludge is > 20'C, SOUR = 1.18 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.22 (mg/g)/hr
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date &Analyst: 1l5i202'1 07'12 am TLS Dig# 2 Days
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 1Zg
Weight of dish + dried solids: 1268802 g
Weight of dried solids: 0.1277 g
Total Solids: 25.54 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
17.00
7.30
1
17.00
6.83
2
17.00
6.43
3
17.00
6_07
4
17.00
5.75
5
17.00
5.42
6
17.00
5.01
7
17.00
4.65
8
17.00
4.24
9
17.00
3.84
10
17.00
3.47
11
17.00
3.00
12
17.00
2.67
13
17.00
2.23
14
17.00
1.82
15
17.00
1.40
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.39 mg/L/minute
0.91 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
17
If sewage sludge is > 20°C, SOUR = 1.05 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.11 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 1/612021 0121 am TlS Dig# 2 Day 3
Total Solids
Sample volume used for total solids test: 111111111M 5 mL
Weight of dish: 92.9598 g
Weight of dish + dried solids: 93.0859 g
Weight of dried solids: 0.1261 g
Total Solids: 25.22 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
16.00
7.02
1
16.00
6.32
2
16.00
6.15
3
16.00
6.08
4
16.00
5.81
5
16.00
5.60
6
16.00
5.32
7
16.00
5.04
8
16.00
4.76
9
16.00
4.46
10
16.00
4.16
11
16.00
3.89
12
16.00
3.73
13
16.00
3.57
14
16.00
3.23
15
16.00
3.01
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
16
0.25 mg/L/minute
0.61 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.74 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.79 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton .
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: I/7/2021 .6720 .airin .T#..S
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
3
121.3690
0.1237
24.74
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
16.00
8.63
1
16.00
8.52
2
15.00
8.32
3
15.00
8.26
4
15.00
8.09
5
15.,00
7.85
6
15.00
7.78
7
15.00
7.70
8
15.00
7.53
9
15.00
7.27
10
15.00
7.10
11
15.00
7.00
12
15.00
6.73
13
15.00
5.47
14
15.00
6.08
15
15.00
6.01
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
15.125
0.19 mg/L/minute
0.46 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.58 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.64 (mg/g)/hr
SOUR passes if result is _< 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 1/8/2021 0725 am TL5 Dig#
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.4588 g
Weight of dish + dried solids: 125.5719 g
Weight of dried solids: 0.1131 g
Total Solids: 22.62 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
19.00
7.54
1
19.00
7.24
2
19.00
6.90
3
19.00
6.58
4
19.00
6.24
5
19.00
5.91
6
19.00
5.51
7
19.00
5.16
8
19.00
4.80
9
19.00
4.42
10
19.00
4.05
11
19.00
3.65
12
19.00
3.33
13
19.00
3.00
14
19.00
2.60
15
19.00
2.18
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19
0.36 mg/L/minute
0.95 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 1.00 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 1.02 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 111112021 0642 am TLS Dig# 2 Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 120.9180 g
Weight of dish + dried solids: 121.0318 g
Weight of dried solids: 0.1138 g
Total Solids: 22.76 g/L
�Y1�17
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
15.00
8.89
1
15.00
8.84
2
15.00
8.62
3
15.00
8.43
4
15.00
8.25
5
15.00
8.09
6
15.00
7.87
7
15.00
7.73
8
15.00
7.54
9
15.00
7.35
10
15.00
7.13
11
15.00
6.93
12
15.00
6.73
13
15.00
6.48
14
15.00
6.23
15
15.00
5.98
Oxygen Consumption Rate 0.19 mg/L/minute
SOUR 0.51 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
15
If sewage sludge is > 20°C, SOUR = 0.65 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.72 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date &Analyst: 14212621 0632 am TLS De�#2' Dap
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.7498 g
Weight of dish + dried solids: 125.8722 g
Weight of dried solids: 0.1224 g
Total Solids: 24.48 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
16.00
7.49
1
16.00
7.17
2
16.00
6.86
3
16.00
6.64
4
16.00
6.33
5
16.00
6.06
6
16.00
5.77
7
17.00
5.44
8
17.00
5.10
9
17.00
4.92
10
17.00
4.6249
11
17.00
4.34
12
17.00
4.04
13
17.00
3.76
14
17.00
3.44 M
15
17.00
3.13
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
16.5625
0.29 mg/L/minute
0.70 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = (mg/g)/hr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is15 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City ®f Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
3-4-21 0727 am kcl Dig# 1 Day 1
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0329 g
Weight of dish + dried solids: 89.1435 g
Weight of dried solids: 0.1106 g
Total Solids: 22.12 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
15.00
2.91
1
15.00
2.80
2
13.00
2.05
3
13.00
1.94
4
13.00
1.70
5
13.00
1.36
6
13.00
1.05
7
13.00
0.77 I
8
13.00
0.70 I
9
13.00
0.67
10
13.00
0.65
11
13.00
0.57
12
13,00
0.55
13
13.00
0.54
14
13.00
0.52
15
14.00
0.51
Oxygen Consumption Rate 0.16 mg/L/minute
SOUR 0.43 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
13.3125
If sewage sludge is > 20°C, SOUR = 0.59 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.67 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
3-5-21 0704 am kcl Dig# 1 Day 2
Sample volume used for total solids test: 5 mL
Weight of dish: 125,7468 g
Weight of dish + dried solids: 125.8552 g
Weight of dried solids: 0.1084 g
Total Solids: 21.68 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
14.00
2.78
1
14.00
2.63
2
14.00
2.46
3
14.00
2.16
4
14.00
2.00
5
14.00
1,82
6
_
14.00
1.54
7
14.00
1.29
8
14.00
1.03
9
14.00
0.73
10
14.00
0.59
11
14.00
0.56
12
14.00
0.54
13
14.00
0.52
14
14.00
0.50
15
14.00
0.49
Oxygen Consumption Rate 0.17 mg/L/minute
SOUR 0.48 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
14
If sewage sludge is > 20°C, SOUR (mg/g)/hr
If sewage sludge is < 20°C, SOUR (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
3-8-21 0712 am Us Dig# 1 Day 3
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0350 g
Weight of dish + dried solids: 89.1355 g
Weight of dried solids: 0.1005 g
Total Solids: 20.1 g/L
;.�illqNk
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
14.00
8.40
1
14.00
8.09
2
14.00
7.98
3
14.00
7.90
4
14.00
7.87
5
14.00
7.66
6
14.00
7.40
7
14.00
7.09
8
14.00
6.85
9
14.00
6.78
10
15.00
6.57
11
15.00
6.34
12
15.00
6.19
13
15.00
5.93
14
15.00
5.73
15
15.00
5.59
Oxygen Consumption Rate 0.19 mg/L/minute
SOUR 0.57 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
14.375
If sewage sludge is > 20°C, SOUR = 0.75 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = s3 1(mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 3-9-21 0723 am Us Dig# 1 Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 111.4068 g
Weight of dish + dried solids: 111.5140 g
Weight of dried solids: 0.1072 g
Total Solids: 21.44 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
14.00
8.80
1
14.00
8.71
2
14.00
8.61
3
14.00
8.44
4
14.00
8.22
5
14.00
8.04
6
15.00
7.84
7
15.00
7.69
8
15.00
7.47
9
15.00
7.30
10
15.00
7.02
11
15.00
6.87
12
15.00
6.57
13
15.00
6.25
14
15.00
5.98
15
15.00
5.73
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
14.625
0.21 mg/L/minute
0.58 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.75 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.83 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
3-10-21 0655 am Us Dig# 1 Day 5
Sample volume used for total solids test: 5 mL
Weight of dish: 130.0794 g
Weight of dish + dried solids: 130.1919 g
Weight of dried solids: 0.1125 g
Total Solids: 22.5 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
14.00
8.57
1
14.00
8.44
2
14.00
8.34
3
14.00
8.17
4
14.00
7.95
5
14.00
7.88
6
14.00
7.71
7
14.00
7.56
8
14.00
7.37
9
14.00
7.20
10
14.00
7.01
11
15.00
6.84
12
15.00
6.65
13
15.00
6.48
14
15.00
6.26
15
15.00
6.04
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.17 mg/L/minute
0.45 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
14.3125
If sewage sludge is > 20°C, SOUR = 0.59 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.66 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 3-11-21 0713 am tis Dig# 1 Day
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 130.0794 g
Weight of dish + dried solids: 130.1860 g
Weight of dried solids: 0.1066 g
Total Solids: 21.32 g/L
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
15.00
8.09
1
15.00
8.05
2
15.00
8.00
3
15.00
7.87
4
15.00
7.73
5
15.00
7.66
6
16.00
7.52
7
16.00
7.37
8
16.00
7.18
9
16.00
6.97
10
16.00
6.80
11
16.00
6.61
12
16.00
6.42
13
16.00
6.21
14
17.00
6.01
15
17.00
5.78
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.16 mg/L/minute
0.45 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
15.75
If sewage sludge is > 20°C, SOUR = 0.55 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.60 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 3-12-21 0754 am . Us Dig# 1 Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0327 g
Weight of dish + dried solids: 89.1401 g
Weight of dried solids: 0.1074 g
Total Solids: 21.48 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
5.21
1
20.00
5.11
2
20.00
5.01
3
20.00
4.87
4
20.00
4.71
5
20.00
4.23
6
20.00
4.01
7
20.00
3.93
8
20.00
3.81
9
20.00
3.69
10
20.00
3.47
11
20.00
3.23
12
20.00
3.00
13
20.00
2.74
14
20.00
2.68
15
20.00
2.57
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.19 mg/L/minute
0.53 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
20
If sewage sludge is > 20°C, SOUR = 0.53 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.53 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 4-27-21 0724 am kcl Dig#2 Day 1
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 111.4072 g
Weight of dish + dried solids: 111.5112 g
Weight of dried solids: 0.1040 g
Total Solids: 20.8 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
18.00
2.35
1
17.00
1.66
2
17.00
1.41
3
17.00
1.36
4
17.00
1.05
5
17.00
0.85
6
17.00
0.21
7
17.00
0.20
8
17.00
0.19
9
17.00
0.18
10
17.00
0.18
11
17.00
0.18
12
17.00
0.18
13
17.00
0.18
14
17.00
0.18
15
17.00
0.18
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.13 mg/L/minute
0.36 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
17.0625
If sewage sludge is > 20°C, SOUR = 0.42 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.44 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxyaen Uptake Rate (SOUR) Worksheet
Date & Analyst: 4-28-21 0627 am kcl Dig#2 Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.6337 g
Weight of dish + dried solids: 125.7369 g
Weight of dried solids: 0.1032 g
Total Solids: 20.64 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
19.00
1.99
1
19.00
1.69
2
19.00
1.37
3
19.00
1.02
4
19.00
0.69
5
19.00
0.37
6
19.00
0.32
7
19.00
0.32
8
19.00
0.32
9
19.00
0.31
10
19.00
0.31
11
19.00
0.31
12
19.00
0.30
13
19.00
0.30
14
19.00
0.28
15
19.00
6.26
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19
0.10 mg/L/minute
0.28 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.29 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.30 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 4-29-21 06:08am kcl Dig#2 Day 3
Total Solids
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
5
130.0789
130.1840
0.1051
21.02
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
2.20
1
20.00
1.82
2
20.00
1.68
3
20.00
1.48
4
20.00
1.43
5
20.00
1.34
6
20.00
1.33
7
20.00
1.32
8
20.00
1.21
9
20.00
1.07
10
20.00
0.87
11
20.00
0.86
12
20.00
0.65
13
20.00
0.62
14
20.00
0.38
15
20.00
0.36
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
mL
9
9
9
g/L
0.11 mg/L/minute
0.31 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
20
If sewage sludge is > 20°C, SOUR = 0.31 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.31 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
4-30-21 06:24 am kcl Dig#2 Day 4
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0330 g
Weight of dish + dried solids: 89.1355 g
Weight of dried solids: 0.1025 g
Total Solids: 20.5 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
21.00
2.50
1
21.00
2.49
2
21.00
1.50
3
21.00
1.01
4
21.00
0.62
5
21.00
0.52
6
21.00
0.42
7
21.00
0.32
8
21.00
0.28
9
21.00
0.21
10
21.00
0.21
11
21.00
0.20
12
21.00
0.20
13
21.00
0.19
14
21.00
0.19
15
21.00
0.18
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.13 mg/L/minute
0.39 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
21
If sewage sludge is > 20°C, SOUR = 0.38 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = A,37 (mg/g)/hr
SOUR passes if result is 5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst
Total Solids
City ofLumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
5-3-21 5:50 am kci Dig#2 Day 5
Sample volume used for total solids test: 5 mL
Weight of dish: 125.6341 g
Weight of dish + dried solids: 125.7418 g
Weight of dried solids: 0.1077 g
Total Solids: 21.54 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
5.25
1
20.00
5.23
2
20.00
5.04
3
20.00
4.80
4
20.00
4.40
5
20.00
4.13
6
20.00
3.78
7
20.00
3.44
8
20.00
3.10
9
20.00
2.81
10
20.00
2.31
11
20.00
1.96
12
20.00
1.57
13
20.00
1.30
14
20.00
0.82
15
20.00
0.57
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
20
0.33 mg/L/minute
0.93 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.93 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.93 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
5-4-21 6:33 am kcl Dig#2 Day 6
Sample volume used for total solids test:
Weight of dish:
Weight of dish + dried solids:
Weight of dried solids:
Total Solids:
SOUR
5
111.4067'
111.5136
0.1069
21.38
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
21.00
4.91
1
21.00
4.41
2
21.00
4.00
3
21.00
3.52
4
21.00
3.03
5
21.00
2.95
6
21.00
2.47
7
20.00
1.31
8
20.00
1.00
9
20.00
0.69
10
20.00
0.48
11
21.00
0.43
12
21.00
0.40
13
21.00
0.34
14
21.00
0.33
15
21.00
0.20
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
mL
9
9
9
g/L
0.34 mg/L/minute
0.94 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
20.75
If sewage sludge is > 20°C, SOUR = 0.91 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.90 (mg/g)/hr
SOUR passes if result is < 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 5-5-21 7:34 am kci Dig#2 Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 123.1038 g
Weight of dish + dried solids: 123.2091 g
Weight of dried solids: 0.1053 g
Total Solids: 21.06 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
22.00
3.72
1
22.00
3.00
2
22.00
2.62
3
22.00
2.17
4
22.00
2.03
5
22.00
1.79
6
22.00
1.04
7
22.00
0.39
8
22.00
0.18
9
22.00
0.13
10
22.00
0.13
11
22.00
0.13
12
22.00
0.13
13
22.00
0.13
14
22.00
0.13
15
22.00
0.12
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
22
0.24 mg/L/minute
0.68 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.61 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.59 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 7-13-21 0527 am kcl Dig#2 Day 1
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 126.9138 g
Weight of dish + dried solids: 126.9927 g
Weight of dried solids: 0.0789 g
Total Solids: 15.78 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
25.00
1.09
1
25.00
0.69
2
25.00
0.50
3
25.00
0.42
4
25.00
0.36
5
25.00
0.35
6
25.00
0.34
7
25.00
0.32
8
25.00
0.32
9
25.00
0.31
10
25.00
0.31
11
25.00
0.31
12
25.00
0.31
13
25.00
0.31
14
25.00
0.31
15
25.00
0.30
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.03 mg/L/minute
0.11 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
oC
25
If sewage sludge is > 20°C, SOUR = 0.09 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.08 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
7-14-21 0533 am kcl Dig#2 Day 2
Sample volume used for total solids test: 5 mL
Weight of dish: 89.0347 g
Weight of dish + dried solids: 89.1147 g
Weight of dried solids: 0.0800 g
Total Solids: 16 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
aC
0
23.00
3.25
1
23.00
2.58
2
23.00
1.16
3
23.00
0.64
4
23.00
0.61
5
24.00
0.56
6
24.00
0.41
7
24.00
0.35
8
24.00
0.33
9
24.00
0.27
10
24.00
0.25
11
24.00
0.22
12
24.00
0.22
13
24.00
0.21
14
24.00
0.21
15
24.00
0.20
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
23.6875
0.14 mg/L/minute
0.53 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.44 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.41 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City ®f Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
7-15-21 0606 am kcl Dig#2 Day 3
Sample volume used for total solids test: 5 mL
Weight of dish: 120.5328 g
Weight of dish + dried solids: 120.6135 g
Weight of dried solids: 0.0807 g
Total Solids: 16.14 9/1-
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
3.17
1
24.00
2.70
2
24.00
2.06
3
24.00
1.89
4
24.00
1.77
5
24.00
1.52
6
24.00
1 1.06
7
25.00
0.51
8
25.00
0.30
9
25.00
0.30
10
25.00
0.26
11
25.00
0.21
12
25.00
0.17
13
25.00
0.15
14
25.00
0.10
15
25.00
0.05
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.20 mg/L/minute
0.75 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
24.5625
If sewage sludge is > 20°C, SOUR = 0.60 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.55 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 7-16-21 0538 am kcl Dig#2 Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 126.9157 g
Weight of dish + dried solids: 126.9938 g
Weight of dried solids: 0.0781 g
Total Solids: 15.62 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
4.44
1
24.00
3.38
2
24.00
2.11
3
24.00
0.50
4
24.00
0.42
5
24.00
0.38
6
24.00
0.37
7
25.00
0.37
8
25.00
0.35
9
25.00
0.35
10
25.00
0.33
11
25.00
0.31
12
25.00
0.29
13
25.00
0,28
14
25.00
0.25
15
25.00
0.25 .
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
24.5625
0.19 mg/L/minute
0.72 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = 0.57 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.53 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
7-19-21 0539 am kcl Dig#2 Day 5
Sample volume used for total solids test: 5 mL
Weight of dish: 120.9153 g
Weight of dish + dried solids: 120.9936 g
Weight of dried solids: 0.0783 g
Total Solids: 15.66 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
3.26
1
24.00
3.06
2
24.00
2.74
3
24.00
2.63
4
24.00
2.34
5
24.00
2.03
6
24.00
1.95
7
24.00
1.73
8
24.00
1.40
9
24.00
1.28
10
24.00
1.07
11
24.00
0.85
12
24.00
0.63
13
24.00
0.38
14
24.00
0.22
15
24.00
0.21
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.21 mg/L/minute
0.81 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
24
If sewage sludge is > 20°C, SOUR = 0.67 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.62 (mg/g)/hr
SOUR passes if result is15 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 7-20-21 0538 am kci Dig#2 Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 125.4580 g
Weight of dish + dried solids: 125.5365 g
Weight of dried solids: 0.0785 g
Total Solids: 15.7 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
3.29
1
24.00
2.22
2
24.00
1.64
3
24.00
1.61
4
24.00
1.56
5
24.00
1.48
6
24.00,
1.36
7
24.00
1.19
8
24.00
1.01
9
24.00
0.84
10
24.00
0.69
11
24.00
0.38
12
24.00
0.27
13
24.00
0.25
14
24.00
0.25
15
24.00
0.24
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.17 mg/L/minute
0.63 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
24
If sewage sludge is > 20°C, SOUR = 0.52 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.48 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City
of Lumberton
Via: /I
• . • J
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 7-21-21 0638 am kcl Dig#2 Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 121.9551 g
Weight of dish + dried solids: 122.0338 g
Weight of dried solids: 0.0787 g
Total Solids: 15.74 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
24.00
5.46
1
24.00
5.33
2
24.00
5.17
3
24.00
4.92
4
24.00
4.70
5
24.00
4.51
6
24.00
4.40
7
24.00
4.19
8
24.00
4.01
9
24.00
3.86
10
24.00
3.61
11
24.00
3.46
12
24.00
3.23
13
24.00
3.17
14
24.00
2.98
15
24.00
2.82
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.18 mg/L/minute
0.69 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
24
If sewage sludge is > 20°C, SOUR = 0.56 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0 5 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 11-1-21 1117 am kcl Dig#2 Day 1
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 123.1042 g
Weight of dish + dried solids: 123.2016 g
Weight of dried solids: 0.0974 g
Total Solids: 19.48 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
5.25
1
20.00
4.73
2
20.00
3.26
3
20.00
1.69
4
21.00
0.61
5
21.00
0.25
6
21.00
0.24
7
21.00
0.24
8
21.00
0.23
9
21.00
0.22
10
21.00
0.22
11
21.00
0.21
12
21.00
0.20
13
21.00
0.20
14
21.00
0.19
15
21.00
0.19
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.27 mg/L/minute
0.84 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
20.75
If sewage sludge is > 20°C, SOUR = 0.81 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.80 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 11-2-21 0626 am kcl Dig#2 Day 2
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 111.4076 g
Weight of dish + dried solids: 111.5059 g
Weight of dried solids: 0.0983 g
Total Solids: 19.66 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
21.00
6.27
1
21.00
4.38
2
21.00
2.26
3
21.00
0.32
4
20.00
0.16
5
20.00
0.16
6
20.00
0.14
7
20.00
0.14
8
19.00
0.13
9
19.00
0.13
10
19.00
0.13
11
19.00
0.13
12
19.00
0.13
13
20.00
0.13
14
20.00
0.14
15
20.00
0.14
Oxygen Consumption Rate 0.25 mg/L/minute
SOUR 0.77 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
19.9375
If sewage sludge is > 20°C, SOUR = (mg/g)/hr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is <_ 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
11-3-21 am 0820 kcl Dig#2 Day 3
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2446 g
Weight of dish + dried solids: 121.3398 g
Weight of dried solids: 0.0952 g
Total Solids: 19.04 g/L
��1611P
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
20.00
7.48
1
20.00
4.49
2
20.00
3.53
3
19.00
2.92
4
18.00
1.08
5
18.00
0.23
6
18.00
0.18
7
18.00
0.18
8
18.00
0.18
9
18.00
0.17
10
18.00
0.13
11
18.00
0.13
12
17.00
0.13
13
18.00
0.13
14
18.00
0.13
15
18.00
0.13
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
18.375
0.35 mg/L/minute
1.10 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = �Z v,.�;: (mg/g)/hr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 11-4-21 0704am kcl Dig#2 Day 4
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 120.5327 g
Weight of dish + dried solids: 120.6301 g
Weight of dried solids: 0.0974 g
Total Solids: 19.48 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
19.00
6.89
1
17.00
6.88
2
17.00
6.80
3
17.00
6.80
4
17.00
6.80
5
16.00
6.69
6
16.00
6.48
7
16.00
6.26
8
17.00
6.03
9
17.00
5.78
10
17.00
5.50
11
17.00
5.24
12
17.00
4.98
13
17.00
4.69
14
17.00
4.41
15
17.00
4.12
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
16.9375
0.19 mg/L/minute
0.60 (mg/g)/hr
If sewage sludge is > 20°C, SOUR = tiAA (mg/g)/hr
If sewage sludge is < 20°C, SOUR = �M(mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

Date & Analyst:
Total Solids
City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
11-5-21 0628 am kcl Dig#2 Day 5
Sample volume used for total solids test: 5 mL
Weight of dish: 121.2444 g
Weight of dish + dried solids: 121.3424 g
Weight of dried solids: 0.0980 g
Total Solids: 19.6 g/L
6/101117
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
14.00
8.61
1
14.00
8.26
2
14.00
8.14
3
14.00
7.95
4
14.00
7.81
5
14.00
7.64
6
15.00
7.49
7
15.00
7.29
8
15.00
7.07
9
15.00
6.92
10
15.00
6.75
11
15.00
6.50
12
15.00
6.30
13
16.00
6.08
14
16.00
5.94
15
16.00
5.73
Oxygen Consumption Rate 0.19 mg/L/minute
SOUR 0.57 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
14.8125
If sewage sludge is > 20°C, SOUR = 0.73 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.81 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1111

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 11-8-21 0808 am kcl Dig#2 Day 6
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: 111.4079 g
Weight of dish + dried solids: 111.5079 g
Weight of dried solids: 0.1000 g
Total Solids: 20 g/L
SOUR
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
14.00
8.84
1
15.00
8.44
2
15.00
8.29
3
16.00
7.71
4
17.00
7.33
5
17.00
7.31
6
18.00
7.21
7
17.00
7.16
8
16.00
7.16
9
17.00
7.16
10
17.00
7.06
11
17.00
6.82
12
17.00
6.57
13
17.00
6.43
14
17.00
6.20
15
17.00
6.01
Oxygen Consumption Rate
SOUR
SOUR Temperature Correction
0.16 mg/L/minute
0.47 (mg/g)/hr
Average Sewage Sludge
Temperature During Test
°C
16.5
If sewage sludge is > 20°C, SOUR = 0.56 (mg/g)/hr
If sewage sludge is < 20°C, SOUR = 0.60 (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11

City of Lumberton
Environmental Laboratory
Specific Oxygen Uptake Rate (SOUR) Worksheet
Date & Analyst: 11-9-21 0752 am kcl Dig#2 Day 7
Total Solids
Sample volume used for total solids test: 5 mL
Weight of dish: -121.2460 g
Weight of dish + dried solids: 121.3439 g
Weight of dried solids: 0.0979 g
Total Solids: 19.58 g/L
�14111 C1
Time
(Minutes)
Temperature
Dissolved
Oxygen (mg/L)
oC
0
16.00
7.34
1
16.00
7.14
2
16.00
7.03
3
16.00
6.84
4
16.00
6.84
5
16.00
6.74
6
16.00
6.64
7
16.00
6.47
8
16.00
6.28
9
16.00
6.13
10
16.00
5.98
11
16.00
5.80
12
16.00
5.54
13
16.00
5.43
14
16.00
5.25
15
16.00
5.08
Oxygen Consumption Rate 0.15 mg/L/minute
SOUR 0.45 (mg/g)/hr
SOUR Temperature Correction
Average Sewage Sludge
Temperature During Test
°C
16
If sewage sludge is > 20°C, SOUR = yE"T''" (mg/g)/hr
If sewage sludge is < 20°C, SOUR = (mg/g)/hr
SOUR passes if result is:5 1.5 (mg/g)hr
Version 11/1/11