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Home My WebLink AboutWQ0037637_Residual Annual Report 2021_202202252021 ANNUAL REPORT REVISED CRAVEN AG SERVICES, INC. LAND APPLICATION PROGRAM PERMIT #WQ0037637 Prepared For: Craven Ag Services, Inc. 2115 NC Highway 55 New Bern, North Carolina 28562 Prepared By: Branch Residuals & Soils, LLC 1735 Heckle Blvd. Suite 103-291 Rock Hill, SC 29732 BRANCH RESIDUALS & SOILS, LLC 1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732 PHONE (336) 312-9007 February 25, 2022 North Carolina Department of Environmental Quality Division of Water Resources 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Reference: 2021 LAND APPLICATION ANNUAL REPORT Craven Ag Services, Inc. Permit No. WQ0037637 Branch Residuals & Soils Project No. 2019-132 Information Processing Unit: Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced permit on behalf of the Craven Ag Services, Inc. This data includes: 1) Certification Forms, 2) Aruival Residual Sampling Summary Forms, 3) Annual Metals Field Loading Summary Forms, 4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Pathogen & Vector Attraction Forms, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils Lab Data 10) 2021 Application Summary Table, and 11) 2021 Application Condition Summaries. A total of 166,000 gallons (12.05 dry tons) of Class B lime -stabilized biosolids were surface or incorporated to 27.29 acres in 2021. This material was divided as follows: • 86,000 gallons (9.25 dry tons) from Maysville WWTP, ® 80,000 gallons (2.80 dry tons) from Bridgeton WWTP. • 0 gallons (0 dry tons) from Pruitt Health Sea Level WWTP, and • 0 gallons (0 dry tons) from Town of River Bend. If any further information is required regarding this land application program, please do not hesitate to contact me at (336) 312-9007. Sincerely, 01 Robert T. Branch, L.S.S. Land Application/Residuals Operator 15676 [,M cc: Craven Ag Services, Inc. TABLE OF CONTENTS SECTION NO. TITLE I Certification Forms II Annual Residual Sampling Summary Forms III Annual Metals Field Loading Summary Forms IV Annual Land Application Field Summary Forms V Residual Analysis Lab Sheets VI Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report VII Pathogen and Vector Attraction Reduction Forms VIII Pathogen and Vector Attraction Reduction Documentation IX Soil Analysis Reports X 2021 Application Summary Table XI 2021 Application Condition Summaries CERTIFICATION FORMS ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0037637 County: Craven Year: Facility Nam2021e (as shown on permit): '- Services, Inc Land Application Operator: Craven Ag Services, Inc. Phone: —F25-26�33-5334 L and application of residuals as allowed by the permit occurred during the past calendar year? 'I Yes �.,] No - If No, sicip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A. - # - — - — ------ uring e year::' 27.29 Part IR Anntial 9------e_�tatement- Facility was Compliant during calendar year 2021 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water If Quality. J N;- Yes no please, provide a r written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the perrnit and lime was applied (if needed) to achieve a sil•H•f at least . the limit specified opo60 o in the permit. 3) Annual soils analysis were perfon-ned on each site receiving residuals during the past calendar year and three (3) copi of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached, 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Liiiiits in 15A NCAC 02T. 1 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Pa. , 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification, "I certify, under penalty of law, that the above information is, to the best of my knowledge and beliet trnp- Arrairate and coAg— 4 - - - Know1u,-- Mr. John W. Dunham, Owner 7Fe;iiittee Name and Title (type or print) gnature of �Pe:m-�ttee Date See Attached Signature of Preparer* Date gnature of LaAdApp�lier Date (if different from Perrrtittee) different of from P, rn and Prepare,) if different from Permittee and Preparer) Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) f Part B - Annual Compiance Statement: Facility was compliant during calendar year 2020 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. Yes i, J No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. I ) Only residuals approved for tl-ds permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the pern-dt and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached, 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T.1 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Peitwere complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T.1 I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occur -red. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. tart C - Certification. pt I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." K �12 , Statement. Facility was compliant during calendar year 2021 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes D No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective ,2ction taken. 1) Only residuals approved for this pen -nit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the pen -nit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T. I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Pe were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and reiriediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. PLq C - Certif- ication. 4 certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Date at of oof -Pr (if different from Perntittee) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T . 1102 (26) ANNUAL RESIDUAL SAMPLING SUMMARY FORMS tico-mfi� ob m 522MAM -2 we 1� I u milli 11 �iIIY III it II I loll19 • to CD CD N CN CD 0 LL w z LU 0 ANNUAL METALS FIELD LOADING SUMMARY FORMS ANNUAL IT .1 Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: - Craven Ag Services Total Dry Tons Applied (Annual): 0.74 Permit #: WQ0037637 Cation Exchange -Capacity (non 503 only): n/a ---------- Operator: Allen Roach Owner: Allen & Gloria Roach ----------- Predominant Soil Series Se Acres Used: 3.65 Acres Permitted: 3.65�Site #: 3 Field #: [W) - Kesidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent# BEI- ME EMU= RMEM UMMI a= Ron mmm INMI MM: of IBM • I W. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" -�igna�tureof Land Applier ZIA --Z 2— Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) V "T Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Craven A - Services -Total Dry Tons Applied (Annual): 6.17 Permit WQ0037637 Cation Exchange Capacity (non 503 only): a Operator: Allen Roach Owner: Allen & Gloria Roach Predominant Soil Series To Acres Used: 12.01 Acres Permitted: 12.01 Site #: 3 Field #: -2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent H): BEI-440A M21-03724 RPI-44nA 3/9/21 - - U+-WAUNCISIGUE Tiff NIIIII-mmm, 0.06 0.39 0.06 --o.00 o.02- -7.-00 - 0.02 TO-0- --o0 -1 o.ao --O-o -7 -00- 0.02 0.00 F 0.02 0.04 0.21 0.05 0.30 0.00 0.02 0.00 '---- 0.02 O.Oo iToo a.00 0.00 0.00 0.01 0.00 0.02 0.00 0.01 0.00 0.02 0.00 0.01 0.00 0.02 0.23 0.52 0.24 0.99 1.85 16.40 1.94 20.18 "I certi y, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" jg'nature of Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) gm- ro Prmr, • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submittinu false information, including the possibility of fines and imprisonment for knowing violationsto --z- 2- ignat�ureof L�andAppher � Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) I � I �'I 1 11, WIN11411170311117i Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Permit #: Operator: Acres Used: Craven Ag Services Total Dry Tons Applied [A.—Ila WQ0037637 Allen Roach 4.38 Cation Exchange Capacity (non 503 only): Owner. Roach Trust Predominant Soil Series Acres Permitted: 4.38 Site #: 6 Field #: 0.63 a Ln Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent 4): BE[-44—Q§6 rig 1, 1, FTF-MM, IMMM 0.14 Arsenic 0.00 0.00 Cadmium 0.00 ----------0'00 �hromiu,-56 F 0.01 Copper 0.11 0.11 Lead 0.01 0.01 Mercury 0.00 Molyb- ---------- 0.00 denum 0.00 0.00 Nickel 0.00 0.00 Selenium 0.00 0.00 Zinc 0.56 0.56 Total Phos- 4.55 phorus_ 4.55 'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibty of flnes and imprisonment for knowing violations" .7- �gnatue okf Land Applier Author Daryl D. Merritt Date DENR FORM MFLSF (7/2002) ANNUAL LAND APPLICATION FIELD SUMMARY FORMS ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND All nutrients and metals concentrations listed on the following annual land application field summary forms are on a pound per acre basis. The following is a list of symbols and abbreviations used on the field loading rate report: %TS — Percent Solids DT/ACRE — Dry Tons Applied per Acre lb/ac — Pounds per Acre Metals (lbs/ac) As — Arsenic Cd — Cadmium Cr — Chromium Cu — Copper Pb — Lead Hg — Mercury Mo — Molybdenum Ni — Nickel Se — Selenium Zn — Zinc Nutrients (lbs/ac) PAN — Plant Available Nitrogen P — Phosphorus K — Potassium Annual Totals — lbs/ac applied during the calendar year. Cumulative Totals — lbs/ac applied during the lifetime of field use. ad C-: a - Ammonia Y Nitrogen 11�9 !I �N �e 1 �81 Appli-cation IY Method* 111 1 1 1 i� or e L Lal .4onth �� 11 e11111n IN. o c Q ri cv Z � v LW a o CA u i u 0 Q � o i r �oil Y � I I M IM I �s Ammonia L� Nitrogen E' 1 �9 ■ 1 �I Date or on 0 I- wk 0 1 i Ammonia Nitrogen R- n doil Date or NOUNn Month I 0 i RESIDUAL ANALYSIS LAB SHEETS Facility: Source: Location: Contractor: Type of Analysis: Report No: Date Sampled: Date Reported: Reporting Period: Town of Maysville Maysville WWTP Maysville, North Carolina Carven Ag Services Wastewater Treatment Plant M21-03724 1/28/2021 Type of Stabilization: 2/10/2021 Annual 2021 Parameter % PPM Dry Weight EPA Monthly Limits Solids* 2.580 Nitrogen (TKN)* 6.790 67,900.00 Phosphorus 2.080 20,800.00 Potassium 0.265 2,650.00 Sulfur Calcium 2.870 28,700.00 Magnesium 0.224 2,240.00 Sodium 0.213 2,130.00 Iron --- Aluminum --- 8260.00 Manganese --- Copper --- 264.00 1,500 Zinc --- 663.00 2,800 Ammonia Nitrogen* 0.405 4,050.00 Nitrate N / Nitrite N* --- 9.65 Cadmium --- 18.60 39 Chromium --- 1,200 Nickel --- 18.60 420 Lead --- 24.50 300 Arsenic --- 26.60 41 Mercury --- 0.67 17 Selenium --- 18.60 100 pH 6.740 Calcium Carbonate Eq. (est) 0.00 Organic Nitrogen 6.385 Molybdenum --- 18.60 75 Chloride --- Boron Available P2O5 Specific Gravity 8.340 Wastewater Treatment Plant Maysville WWTP Maysville, North Carolina Carven Ag Services Annual 2021 Date Reported: 2/10/2021 Report No: M21-03724 Note All Units in Pounds Per Dry Ton Macro Nutrients Physical Characteristics PAN Surf. 42.379 PAN Inj. 46.429 P 41.600 K 5.300 Lime (estimated) 0.000 Secondary Nutrients Calcium 57.400 Magnesium 4.480 Sodium 4.260 SAR 0.522 Chloride 0.000 Iron 0.000 Alumium 16.520 Manganese 0.000 Boron 0.000 Sulfur 0.000 % Solids 2.58 pH 6.740 Min Rate 0.300 Residual Nitrogen Calculation Year Min Rate PAN #/Acre Metals Arsenic 0.053 Cadmium 0.037 Chromium 0.000 Copper 0.528 Lead 0.049 Mercury 0.001 Molybdenum 0.037 Nickel 0.037 Seleniun 0.037 Zinc 1.326 2018 2019 2020 2021 0.30 38.31 2022 0.15 13.41 2023 0.08 5.70 2024 0.04 2.64 2025 2026 2027 2028 Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 29405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Town of Maysville Date of Report: Feb 10, 2021 Post Office Box 265 Customer PO : Maysville NC 28555 Customer ID: 17020023 Attention: Schumata Brown Report M 2021-01506 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 21-03724 Site: Sludge 1/28/2021 8:20 AM Solid/Sludge Connie Branch Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 8260 mg/kg 01/29/2021 Arsenic EPA 200.7 26.6mg/kg 01/29/2021 Cadmium EPA 200.7 <18.6mg/kg 01/29/2021 Calcium EPA 200 7 28700 mg/kg 01/29/2021 Chromium EPA 200.7 18.6mg/kg 01/29/2021 Copper EPA 200.7 264 mg/kg 01/29/2021 Lead EPA 200.7 24.5 mg/kg 01/29/2021 Magnesium EPA 2007 2240mg/kg 01/29/2021 Molybdenum EPA 200 7 <18.6 mg/kg 01/29/2021 Nickel EPA 200 7 <18.6 mg/kg 01/29/2021 Potassium EPA 200 7 2650 mg/kg 01/29/2021 Selenium EPA 200 7 <18.6 mg/kg 01/29/2021 Sodium EPA 200 7 2130 mg/kg 01/29/2021 Zinc EPA 200.7 663 mg/kg 01/29/2021 Nitrate+Nitrite-Nitrogen EPA 353 2 9.65 mg/kg 02/08/2021 Total Solids (%) SM 2540 B 2.58 % 02/01 /2021 pH SM 4500 H B 6.74 units 02/04/2021 Ammonia Nitrogen SM 4500 NH3 C 4050 mg/kg 01/29/2021 Total Kjeldahl Nitrogen (TKN) SM 4500 org B 67900 mg/kg 01/29/2021 Total Phosphorus SM 4500 P F 20800 mg/kg 02/04/2021 Mercury SW8467471B <0.67mg/kg 01/29/2021 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: _ - Report2021-01506 Page 1 of 1 Receipt of sample: ECHEMPkkup'Lf______ Client Delivery 13 UPSO—Re—dExll Ot er 1. Were custody seals present on the cooler? 'How temperature taken: 0 Temperature Blank IR Gun ID: Thomas Traceable S/N 192511657 IR Gun CorreEtion Factor 'C: 0.0 11111111M*�� 3. if temperature of cooler exceeded 6*C, was Project Mgr./QA notified? 4. were proper custody procedures (relinquished/received) followed? - -- - ----- --- 5were sample ID's listed on the COC? 6. Were samples ID's listed on sample containers? 7. were collection date and time listed on the COC? 8. Were tests to be performed listed on the COC? 3. Nd sampfes arrive in proper containers for each Did samples arrive in good condition for each test? 12. Were samples received within proper holding time for requested tests? �13. Were acid preserved samples received at a AM of <27 *- EL - — - ------- ------- ----- --- - — -- 14. Were cyanide samples received at a pH >12? 15. Were sulfide samples received at a pH >V 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? 18. Were orthophosphate samples filtered in the field within 15 minutes? TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) 'Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH -Time of preservation: If more than one preservative is needed, notate in comments below 'Note: Notify custome, service immediately for incorrectly preserved samples. Obtain a new sample or iinotify the state lab if directed to analyzed by the customer. Who was notified, date and time: olatiles Sample(s) were received with headspace 1•• • I �$ = Ln ®N cm Zc o c® v �° Mn E LL cu r � v 34m E _® c e CD .0 � W y N LL a CD L C w O LU U U) 0 N An E d G/ C U w Q CL ❑ 0 2 Q m E t w 0 c —' WQ m M p o j a`) n U Z CLLn y) a ro T Z Q a L: -.. w co cn N Q m W H3H10 90 m Z olml O h Q HOVN 6�1 tONH W u YOSZH LL lOH ®- 3NON X maewnN Or err M m E_ -116W auuo140 m (V 10 d) a. (D n. (J 0- (D n. (,7 0- (D d (J CL Joureruoo gejJ Jo U (7 U U U U U (7 U U' U (D U (7 U (D alrsodwo0 adAl ardweg m � ❑. 7 C tr o +J c w d y N d E t ® h t.J v cc ® 1 r` m V w � � w C ti b d � Q E tT N d 7 d v m NJ Facility: Source: Location: Contractor: Type of Analysis: Report No: Date Sampled: Date Reported: Reporting Period: Ina Plant e of Stabilization: Lime Parameter % PPM Dry Weight EPA Monthly Limits Solids* 0:840 Nitrogen (TKN)* 4.651 46,510.00 Phosphorus 1.582 15,820.00 Potassium 0.563 5,625.00 Sulfur Calcium 2.881 28,814.00 Magnesium 0.351 3,509.00 Sodium 1.016 10,156.00 Iron --- Aluminum --- 5887.00 Manganese --- Copper --- 368.00 1,500 Zinc --- 1938.00 2,800 Ammonia Nitrogen* 0.060 595.00 Nitrate N / Nitrite N* --- 30.89 Cadmium --- 2.70 39 Chromium --- 18.0,0 1,200 Nickel --- 14.00 420 Lead --- 21.00 300 Arsenic --- '2`.50 41 Mercury --- 0.23 17 Selenium --- 5.00 100 pH 7.000 Calcium Carbonate Eq. (est) 0.00 Organic Nitrogen 4.592 45,915.00 Molybdenum --- 6.00 75 Chloride --- Boron Available P2O5 Specific Gravity 8.340 Wastewater Treatment Plant Bridgeton WWTP Havelock, North Carolina Carven Ag Services Annual 2021 Date Reported: 4/6/2021 Report No: BEI-440A Note All Units in Pounds Per Dry Ton Macro Nutrients Physical Characteristics PAN Surf. 28.206 PAN Inj. 28.801 P 31.640 K 11.250 Lime (estimated) 0.000 Secondary Nutrients Calcium 57.628 Magnesium 7.018 Sodium 20.312 SAR 1.375 Chloride 0.000 Iron 0.000 Alumium 11.774 Manganese 0.000 Boron 0.000 Sulfur 0.000 Residual Nitrogen Calculation Year Min Rate PAN #/Acre % Solids 0.84 pH 7.000 Min Rate 0.300 Metals Arsenic 0.005 Cadmium 0.005 Chromium 0.036 Copper 0.736 Lead 0.042 Mercury 0.000 Molybdenum 0.012 Nickel 0.028 Seleniun 0.010 Zinc 3.876 2018 2019 2020 2021 0.30 27.55 2022 0.15 9.64 2023 0.08 4.10 2024 0.04 1.90 2025 2026 2027 2028 Environment 1, Inco rated TOWN OF BRIDGETON HYDRO SERVICES & CONSULTING MR. KEVIN MULLINEAUX P.O. BOX 317 HAVELOCK ,NC 28532 PARAMETERS PH (not to be used for reporting) Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. basis),mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Sodium Adsorption Ratio (calc) Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 7.0 03/09/21 DU 4500HB-11 5887 03/16/21 LFJ EPA200.7 < 2.5 03/18/21 MTM 311311-04 28814 03/16/21 LFJ EPA200.7 2.7 03/16/21 MTM 3113B-04 368 03/16/21 LFJ EPA200.7 18 03/16/21 LFJ EPA200.7 21 03/17/21 MTM 3113B-04 3509 03/16/21 LFJ EPA200.7 0.23 04/05/21 MTM EPA7471B 14 03/16/21 LFJ EPA200.7 5625 03/16/21 LFJ EPA200.7 < 5.0 03/22/21 MTM 3113B-04 10156 03/16/21 LFJ EPA200.7 1938 03/16/21 LFJ EPA200.7 15.0 0.84 03/11/21 JMS 254OG-11 c 46510 03/16/21 KES 351.2 R2-93 c 595.0 03/17/21 DTL 350.1 R2-93 c 15820 03/16/21 DTL 365.4-74 c 30.89 03/16/21 DTL 353.2 R2-93 6 03/16/21 LFJ EPA200.7 ' ' `"� PHONE�(262) 751i-8208 FAX (252) 756.0633. ID#: 440 A DATE COLLECTED: 03/09/21 DATE REPORTED : 04/06/21 1J REVIEWEDk,7 V c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORTS A TCLP ANALYSIS IS REQUIRED FOR THE FOLLOWING FACILITIES: TOWN OF BRIDGETON AND TOWN OF MAYSVILLE envirochem �� EnvironmentalEnvironmental�� Chemists, Inc. 0602Windmill Way, Wilmington, ° 910.3920223Lab ^ 910.392.4424Fax 7}OBovserto=oRoad, Manteo,yJC27954 ° 252.473.5702Lub/Pax 255-8Wilmington Highway, Jacksonville, N[2854O ^ 910.347.5843Lab/Fax info@uminmment,-tichemisu.com Town mfMaysville Date mfReport: Feb 1Q.2O21 Post Office Box 2G5 Customer PO#: Maysville NC 28555 Customer ID: 17020023 Attention: 8chumataBnzwn Report #: 2021-01509 Project ID: Sludge LablD Sample ID: CnUeotDate7Timne Matrix Sampled by 21-03728 Site: Sludge 1/203021 8:10AYN Solid/Sludge Connie Branch Test Method Results Date Analyzed Total Solids ow»a*«o 2.6696 02/01/2021 Chlondene(TCLp) mwcweMethod oommom» <0.02mg/L 02/15/2021 Endrin(TCLP) aw8waMethod »«mums,« <0.0005mg/L 02/15/2021 Heptanh|or(TCLp) owo^sMethod «oo1omm« <0.0005mg/L 02/15/2021 Heptachlor epoxide (TCLP) mwe»«Method »»o1oma1» <0.0005mg/L 02/15/2021 Lindane(TCLP) owoeMethod no»1omn10 «0.0005mg/L 02/15/ O2f K8athoxych|or(TCLP) a««moMethod m»n1ams1« <0.0005mg/L 02/15/2021 Toxophena(TCLp) mm»^nMethod o»oIomm« <0.05mQ/L 03/15/2021 1.4-Dinh|orobenzene(TCLP) ow8wsmethod nu/omm» <0.050mg/L 02/10/2021 2.4.5-Tiioh|oropheno| (TCLP) »we^smethod 82/0m510 <0.050mg/L 02U10/2021 3.4.8-Troh|unmpheno| (TCLP) »«»o*amethod »o/mm1« <O.OSOmQ/L 02/10/2021 2'4-Dinitnzbu|uene(TCLP) om/w«emethod 82/0/3510 <0.050mg/L 02/10/ O31 Cresol (TCLP) aw»*smethod a»/«ma1» <0.050mg/L 02/10/2021 Hexaoh|oro-1.3-bubadienw(TCLP) mwn^»method uxn» *10 <0.050mg/L 02/10/2021 Hexeoh|onobenzenm(TOLP) o««e**method o»/m»»10 <0.050mg/L 02/10/2021 Hexooh|oroethane(TCLP) am/m«method «o/»mm» <0.050mg/L 02/10X2021 m+p'Creoo|(TCLp) mwawamethod «o/m»sm <0.050mg/L 02/100021 Nitnobanzene(TCLP) mwo^omethod »zn»»m» <0.050mg/L 02/10/2021 o-Cresol(TCLp) mw8wsmethod e:nmom» <0850mg/L 02/10/2021 Penbach|uropheno|(7CLP) mmo^»method au/»ms1» <0.250mg/L 02/10/2021 pyhdina(TCLp) o««m»method u»/m»m» <0.050mg/L 02/10/2021 2.4.5-Tp(TCLp) oWmsMethod ma1A <0.003mQ/L 02/16/2021 2.4'D(TCLP) »WmoMethod n1m« <0.003mg/L 02/16/2021 1.1-Diuh|omoethy!ene(TCLP) aw84sMethod onem»«»» <0.01mg/L 02/03/2021 1.2'Oich|onoethone(TCLP) «wB4»Method »oems»a« <D.Oimg/L 02/03/2021 Benzane(TCLp) ew84sMethod oo60o»o» <0.01mQ/L 02/03/2021 :en iro'chem ANALYTICAL & CONSULTING CHEMISTS Chemists,Environmental Inc. 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab 1, 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax info@environmentalchemists.com Town of Maysville Date of Report: Feb 19, 2021 Post Office Box 265 Customer PO : Maysville NC 28555 Customer ID: 17020023 Attention: Schumata Brown Report : 2021-01509 Project ID: Sludge Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 02/03/2021 Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 02/03/2021 Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 02/03/2021 Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 02/03/2021 Tetrachloroethylene (TCLP) SW846 Method 6260/5030 <0.01 mg/L 02/03/2021 Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 02/03/2021 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 02/03/2021 RCI Cyanide SM 4500 CN D 1.45 mg/kg 02/02/2021 Sulfide SM 4500 S D 43.4 mg/kg 02/01/2021 Ignitability SW 846 method 1010 >200'F 02/19/2021 pH SW 846 Method 9045D 6.99 units 02/16/2021 TCLP Metals Arsenic EPA 200.7 <1.0 mg/L 02/11/2021 Barium EPA 200.7 <1.0 mg/L 02/11/2021 Cadmium EPA 200.7 <1.0mg/L 02/11/2021 Chromium EPA 200.7 <1.0 mg/L 02/11/2021 Lead EPA 200.7 <1.0 mg/L 02/11/2021 Selenium EPA 200.7 <1.0 mg/L 02/11/2021 Silver EPA 200.7 <1.0 mg/L 02/11/2021 Mercury EPA 245.1 <0.0002 mg/L 02/12/2021 Comment: Reviewed by: Report #:: 2021-01509 Page 2 of 2 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Sample Receipt Checklist Client: A`; S l( I LCC,, -TD tWKI Date: 16168 Report Number: oZ t Receipt of sample: ECHEM Pickup ❑ Client Delivery ❑ 1UPS ❑ FedEx ❑ Other ❑ ❑ YES ❑ NO N/A 1. Were custody seals present on the cooler? ❑ YES ❑ NO N/A 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt °C Corrected temperature upon receipt °C How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 ❑ YES 10 NO 13. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? YES 10 NO 4. Were proper custody procedures (relinquished/received) followed? YES 10 NO 5. Were sample ID's listed on the COC? YES 113 NO 6. Were samples ID's listed on sample containers? Iq YES 10 NO 1 7. Were collection date and time listed on the COC? lik YES I ❑ NO 18. Were tests to be performed listed on the COC? YES 10 NO 19. Did samples arrive in proper containers for each test? YES 10 NO 110. Did samples arrive in good condition for each test? IV YES 10 NO 111. Was adequate sample volume available?' IW YES 10 NO 112. Were samples received within proper holding time for requested tests? ❑ YES I0 NO 113. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 114. Were cyanide samples received at a pH >12? ❑ YES 10 NO 115. Were sulfide samples received at a pH >9? ❑ YES 10 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: Sample(s) by adding (circle one): Time of preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) were received incorrectly preserved and were adjusted accordingly H2SO4 HNO3 HCl NaOH If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 a a SGS Orlando, FL The results set forth herein are provided by SGS North America lnC, e-H( rdcopy 2. P(ntnn►tite d Report Technical Report for Environment 1, Inc Town of Bridgeton Hydro Services & Consulting; Havelock, NC ,. IN SGS Job Number: FA83894 Sampling Date: 03/09/21 Report to: nvironment 1, Inc 0 Box 7085 4reenvllle. NC 27835 N: Ann Brown Total number of pages in report: 13 pe•k O Test results contained within this data package meet die requirements Norm Farmer of ilia National Environmental Laboratory Accreditation Program Technical Director and/or stale specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200003), NC(573), NJ(FL002), NY(12022), SC(08038001) DoD ELAP(ANAB L2220), AZ(AZ0800), CA(2037), TX(T104704404), PA(58.03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except In Its entirely, tailhaut die written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 . tel: 407-425.6700 • fax: 407-425.0707 SGS is the sole authority for authorising edits ur modifications to this document. Please shore your idons about I i of 13 Umuuharir I nm,dilicumun of this report is sit -icily prohhilcd, how we can serve ,you better at: Rcvi.wslondardtcmts;u: htlpa.awwsgs.amt'cnhc nts-nod-condiliona1c1iS.IJS.CttslomerCnnud.es.eon� FA03e94 Sections: Table ®f Contents -1- Section 1: Sample Summary................................................................................................... 3 Section2: Summary of Hits.................................................................................................... 4 Section3: Sample Results........................................................................................................ 5 3.1: FA83894-1: SLUDGE SAMPLE.................................................................................. 6 Section4: Misc. Forms............................................................................................................ 11 4.1: Chain of Custody........................................................................................................... 12 SwS__ 2 of 13 1 FA03004 SGS North America Inc. Sample Summary Environment 1, Inc Job No: FA83894 Town of Bridgeton Hydro Services & Consulting; Havelock, NC Project No: 440C Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID This report contalns'reWis reported as ND = Not detected. The following applies: Organics ND = Not detected above die MDL FA83894-1 03/09/21 09:37 KM 03/13/21 SO Sludge SLUDGE SAMPLE Soil samples reported on a diy weight basis unless otherwise indicated on result page. 1� 3of13 r FAB999d Summary of Hits Job Number: FA83894 Account: Environment 1, Inc Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC Collected: 03/09/21 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA83894-1 SLUDGE SAMPLE Tetrachloroethylene 0.0128 0.010 0.0022 mg/1 SW846 8260B Page 1 of 1 4of13 PAtlJOB=1 + Orlando, FL" . Section Sample Results Report of Analysis .._.SG . 5 of 43 t PA83894 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA83894-1 Date Sampled: 03/09/21 Matrix: SO - Sludge Date Received: 03/13/21 Method: SW846 8260B SW8461311 Percent Solids: n/a Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 P78578.1) 10 03/23/21 15:28 SO 03/16/21 14:00 OP84514 VP3174 Run #2 Purge Volume #1 5.0 ml #2 VOA TCLP List CAS No. Compound Result HW# MCL RL 71-43-2 Benzene ND D018 0.50 0.010 78-93-3 2-Butanone (MEK) a ND D035 200 0.050 56-23-5 Carbon Tetrachloride ND D019 0.50 0.010 108-90-7 Chlorobenzene ND D021 100 0.010 67-66-3 Chloroform ND D022 6.0 0.010 106-46-7 1,4-Diclnlorobenzene ND D027 7.5 0,010 107-06-2 1,2-Dichloroethane ND D028 0.50 0.010 75-35-4 1,1-Dichloroethylene ND D029 0.70 0.010 127-18-4 Tetracldoroethylenne 0.0128 D039 0.70 0.010 79-01-6 Trlcldoroethylene ND D040 0.50 0.010 75-01-4 Vinyl Chloride ND D043 0.20 0.010 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 1868-53-7 Dlbromotluoromelhane 101% 83-118% 17060-07-0 1,2-Dichloroetliane-D4 89% 79-125% 2037-26-5 Toluene-D8 91% 85-112% 460-00-4 4-Bromollumobenzene 95% 83-118% (a) Associated CCV outside of control limits low. TCLP Lenchate method SW8461311 MDL Units Q 0.0031 mg/1 0.020 mg/1 0.0036 mg/l 0.0020 mg/I 0.0030 mg/l 0.0026 mg/I 0,0031 mg/1 0.0032 mg/I 0.0022 mg/I 0.0035 mg/l 0.0041 mg/I ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 2617/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6of13 FAM94 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FAS3894-1 Date Sampled: 03/09/21 Matrix: SO - Sludge Date Received: 03/13/21 Method: SW846 8270D SW840 3510C Percent Solids: n/a Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 X074990.1) 1 03AV2120:08 WH 03/17/2109:45 OP84528 SX3056 Run #2 Initial Volume Final Volume un #1 10.0 ml 1.0 ml un #2 ABN TCLP List CAS No. Compound Result HW# MCL RL 95-48-7 2-Melltylplienol ND D023 200 0.50 3&4-Metitylpltenol a ND D024 200 0.50 87-86-5 Pentacldorophenol ND D037 100 2.5 95-95-4 2,4,5-Trichloroplienol ND D041 400 0.50 88-06-2 2,4,6-Tricliloroplienol ND D042 2.0 0.50 100-46-7 1,4-Dichlorobenzene ND D027 7.5 0.50 121-14-2 2,4-Dinit rotoluene ND D030 0.13 0.50 118-74-1 Hexachlorobenzene ND D032 0.13 0.50 87-68-3 Hexachlorobuladiene ND D033 0.50 0.50 67-72-1 Hexachloroethane ND D034 3.0 0.50 98-95-3 Nitrobenzene ND D036 2.0 0.50 I10-86-1 Pyridine ND D038 5.0 1.0 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 45% 14-67% 4165-02-2 Phenol-d5 35% 10-50% 118-79-6 2,4,6-Tribromophenol 86% 33-118% 4165-60-0 Nitrobenzene-d5 79% 42-108% 321-60-8 2-Fluorobipltenyl 75% 40-106% 1718-51-0 Terphenyl-dl4 89% 39-121% (a) Associated BS outside control limits high, sample was ND. TCLP Leachate method SW846 1311 MDL Units Q 0.056 mg/1 0.098 mg/1 0.50 mg/1 0.074 mg/I 0.075 mg/1 0.050 mg/I 0.081 mg/1 0.069 mg/1 0.050 mg/1 0.16 mg/1 0.093 mg/l 0.20 mg/I ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 2617/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7of13 f— FAa36®4 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID; FA83894-1 Date Sampled; 03/09/21 Matrix: SO - Sludge Date Received: 03/13/21 Method: SW846 8151A SW846 3510C Percent Solids: n/a Project: Town of Bridgeton Hydra Services & Consulting; Havelock, NC File 1D DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC073215.1) 1 03/18/21 17:42 SH 03/17/21 13:00 OP84530 GCC1809 Run #2 Initial Volume Mont Volume un #1 10.0 ml 5.0 ml un #2 Herbicide TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCI, RI, MDL Units Q 94-75-7 2.4-1) ND D016 10 0.050 0.017 mg/1 93-72-1 2,4,5-TP (Silvex) a ND D017 1.0 0.0050 0.0013 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 19719-28-9 2,4-DCAA 59% 39-135% (a) Associated CCV outside control limits. Confirmed by reanalysis. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 2617/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8of13 .. Fn83994 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA83894-1 Date Sampled: 03/09/21 Matrix: SO - Sludge Date Received: 03/13/21 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: Town of Bridgeton Hydro Services & Consulting; Havelock, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 KK100391.D 1 03/17/21 19:57 WH 03/17/21 13:00 OP84529 GKK3214 Run #2 Initial Volume Final Volume mn #1 10.0 ml 5.0 ml .un #2 Pesticide TCLP List CAS No. Compound Result HW# MCL RL 58-89-9 gamma-BHC (Lindane) ND D013 0.40 0.0010 12789-03-6 Chlordane ND D020 0.030 0.010 72-20-8 Endrin ND D012 0.020 0.0020 76-44-8 Heptachlor ND D031 0.0080 0.0010 1024-57-3 Heptachlor epoxide ND D031 0.0080 0.0010 72-43-5 Methoxychlor ND D014 10 0.0020 8001-35-2 Toxaphene ND D015 0.50 0.050 CAS No. Surrogate Recoveries Run# I Run# 2 Limits 877-09-8 Tehachloro-m-xylene 84% 42-127% 2051-24-3 Decachloroblphenyl 89% 27-127% TCLP Leachate method SW846 1311 MDL Units Q 0.00022 mg/1 0.0038 mg/1 0.00021 mg/l 0.00026 mg/I 0.00020 mg/I 0.00050 mg/1 0.021 mg/l ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 2617/1/11) B = Indicates analyte found in associated method blank E = hndicates value exceeds calibration range N = Indicates presumptive evidence of a compound °�� 9oft3 _ off?_ FA93994 SGS North America Inc. Report of Analysis Page 1 of i a Zent Sample ID: SLUDGE SAMPLE ,ah Sample ID: FAS3894-1 Date Sampled: 03/09/21 latrix: SO - Sludge Date Received: 03/13/21 Pei -cent Solids: n/a roject: Town of Bridgeton Hydro Services & Consulting; Havelock, NC Metals Analysis, TCLP Leachate SW8461311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic < 0.10 D004 5.0 0.10 mg/l 1 03/17/21 03/18/21 LM SW840 6010D 2 SW846 3010A 3 Barium < 2.0 D005 100 2.0 mg/1 1 03/17/21 03/18/21 LM SW846 6010D 2 SW846 3010A 3 Cadmium < 0.050 D006 1.0 0.050 mg/l 1 03/17/21 03/18/21 LM SW846 6010D 2 SW840 3010A 3 Chromium < 0.10 D007 5.0 0.10 mg/1 1 03/17/21 03/18/21 LM SW846 8010D 2 SW846 3010A 3 Lead < 0.050 D008 5.0 0.050 mg/1 1 03/17/21 03/18/21 LM SW840 8010D 2 SW846 3010A 3 Mercury < 0.0050 D009 0.20 0.0050 mg/l 1 03/18/21 03/18/21 is SW840 7470A I SW846 7470A 4 Selenium < 0.10 D010 1.0 0.10 mg/1 1 03/17/21 03/18/21 LM SW846 6010D 2 SW846 3010A 3 Silver < 0.10 D011 5.0 0.10 mg/1 1 03/17/21 03/18/21 LM SW846 6010D 2 SW848 3010A 3 (1) Instrument QC Batch: MA17546 (2) Instrument QC Batch: MA17547 (3) Prep QC Batch: MP38681 (4) Prep QC Batch: MP38685 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) A 10 of 13 _® V- FA0380.4 r tG, SGIS--. 4 v� a itn 4 �m Orlando, FLkw..� Section 4 Is Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody v 11 of 13 FAB3894 Environment I. Inc. P.O. Bor. 7085. 114 Oakmont Dr. Greenville, NC 27858 enviraomentlfae.com 1'I1ane (252) 75ir-6208 • Fax (252) 756.0633 440 C Weeks 1 CLIENT. TOWN OF BRIDGETON HYDRO SERVICES Its CONSULTING M[R. KEVIN ARILLINEAUX P.O. BOX 317 11AVELOCK NC 20S32 (252) 71UIOI COLLE'CDON SMIPtELOCATIDN O�TE T0' ` --OU CHLORINE WuY NONE CHAIN Or CUSTQDY RR CORD f PLEASE READ Irii1delions forcomplelin0 this form on the reverse side. FORM e5 wt C(MINENTS fl8389y Page. I or I CHLORINE NEUTRALRED AT COLLECTION pHCHECK ILq COUPUNERTYFE.PAi CHELWALPRESERVATION A -NONE 0-NACH B-HN'Or F-HCL C-H,SO, F-ZINCACETATEINAC G-NATHIOSULFATE IC CLASSIFICATION WASTEWATERINPDES) ORINIMWATER WAIGW SOUDWASTESEC110N CHAIN OF CUSTODY (SEAL) MAINTAINED m SNAPIESOOILECTEppBY (FisataPMt) SAMPLES R ECf_ NF.D IN LAB Ai%> '11 4`Aampter must place a'C' for composite samplo or a'G' for 9 35* Grab sample in the blocks above for each parameter requested. NO 391101 TA83894: Chain of Custody rage 1 of 2 0 12 of 13 S.$. FA83ao4 SGS Sample Receipt Summary Job Number: FAB3894 Client: ENVA Project: 440 C Date I Time Received: 3/13120219:35:00 AM Delivery Method, FX AlrbIlift 9546 2845 6913 Therm ID. IR 1; Therm CF: -1.8; of Coolers: I Cooler Temps (Raw Measured) 'C: Cooler 1: (4.8); _VIA 1. Custody Seals Present 1. Sample [abets present on battles 2. Custody Seats Intact 2. Samples preserved property 3V Ii 3. Temp criteria achieved J 3. Sufficient volumekonialnovs recvd for analysts: 4. Cooler lemis verifficallon 4. Condition of sample Intact 5, Cooler media 5. Sample reavd vriffiln HT aLr 6. DatasITImesilDs on CDC match Sample Label N _I A 7. VOCs have headspace 1. Trip Blank present I cooler 8. Sallies received for unspecified tests 2. Trip Blank listed on COC 1 9. Compasiling Instructions dent U 21 10 Von Sol] KlislJors received post 48hrs? ' r I 'A --- QL-S 11. % Solids Jar received? El R 3. Type Of TS Received C1 El W� U. Residual Chlorine Present? I Mlt%jn lorm I Number of Encores: 25-Gram 5-Gram Number of 6035 Field Kits: Number of Lob Filtered Metals: Test Strip Lot Os: pH 0-3 230315 pH 10-12 219813A Othen (Specify) Residual Chlorine Test Strip Lot M Comments Rev. W. OSQ4117 Technician: PETERI-I Cate: 3113120219:35:00 AM Reviewer. DoW FA83894: Chain of Custody Page 2 of 2 1 13 of 13 SGS.; I- FAD3804 PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION The Towns of Bridgeton and Maysville meet pathogen reduction and vector attraction reduction requirements through lime stabilization. Craven Ag Services, Inc. performed the lime stabilizations for Bridgeton and The Town of Maysville performed their own. Some land application events were surface applied, and some were incorporated. The Town of Maysville performed two application events in 2021: 1. March 2021— Lime Stabilized and Surface Applied and 2. October 2021 — lime Stabilized and Incorporated The Town of Bridgeton performed f our application events in 2021: 1. January 2021 — lime Stabilized and Surface Applied, 2. May 2021— Lime Stabilized and Surface Applied, 3. August 2021 — Lime Stabilized and Incorporated, and 4. November 2021 — Lime Stabilized and Incorporated. The forms for these facilities are marked appropriately. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Craven Ag Services, Inc. WQ Permit Number: WQ0037637 WWTP Name: Town of Bridgeton WWTP NPDES Number: NC0074837 Monitoring Period: From 1/1/2021 To 12/31/2021 Pathogen Reduction (15A NCAC 02T .1106) -Please indicate level achieved and alternative erformed• Class A: P Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing) .................... Alt.D (No Prior Test) ❑ Process to Further Reduce Patho ett s f::::➢ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Dl in ❑ Heat Treatment ❑ Thermo hilic (. l Beta Ray ❑ Ganima Ra ❑ Pasteurtzatlon ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens El If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization El Air Drying ❑ Composting ❑ JAerobic Digestion Anaerobic Digest -ion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Pathogen Density g y Number of Frequency Sample Analytical in Sludge Excce- dences ofAnalysis Type Tech-nique Minima Geo. Mean Maxima Units 2 x 10 to the MPN 6th power per gram of Fecal Colifonn total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform J.weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) AJ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O, uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization) Alt 7 (Drying - Stable) ❑ Alt. 8(Drying -Unstable) Alt. 9 (Injection) Alt. 10 (incorporation) ''.! No vector attraction reduction alternatives were performed . 1 CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T 1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the ❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. John W. Dunham Mr. John W. Dunham Preparer Name and Title (type or print) w VIA-1 - d gnature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) d,;,2 S' n tore of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) • on Facility Name: Craven Ag Services. Inc. ww,rP Name: Town of Maysville WW-I'p Monitoring Period: From — 1/] /202 '[To Pathogen Reduction (15A NCAC 02T.1106) - Please indicate le, Class A: Alt. A r-1 I Alt - I �Treatmei AILD (No Prior Ti-.-zt� 0 7!!!7M F—Proct;hb If applicable to alternative performed Compost post 0 Heat ryi� g Beta Ra E❑ 2am�a%Ra3 Class B: JAIL (1) Fecal DCDSi If applicable to alternative performed Lime Stabilization E ic iVe.,. 'ti� Lime D nri 0 Rules) WQ0037637 NCO021482 MT (Class A only) indicate "Proc ess to Further Reduce Pathogens': ❑ Heat Treatment 0 Therniophilic 0 El J—Pasteurization F-1 - tv 0 Alt. (2) Process to Sitynificant1v Reduce Pathogens 0 (Class B only) indicate "Process to Significantly Reduce Pathogens": Air Drying 0 1 Composting 0 --FAerobic Digestion If applicable to alternative performed (Class A or Class B) U Parameter Allowable Level — Pathogen Density in Sludge Kiinimurr Geo. Mean axiML X 10 to the MPN 6t]i power per pain of Fecal Coliforni total solids Cl:U 10-00 _M511 per —_grani of total solid (dry weis-dut) ,alirionella bacteria 3 M PIN per 4 grans (in lieu of fecal total solid (dry -- Excee- Unitsl monitoring data: Frequency Sample Analytical rAn.13,i, Type I Tech-nique Vector Attraction Reduction (I 5A NCAC 027: 1 107) t- Please indicate indi rnative performed: Alt. 1 (VS reduction) ED Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) 0 Alt. 4 (Spec. 0, uptake) 0 7-0 El All. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization Alt7 (Drying - Stable) El 8 (Drying Unstable) E3 It j cti ) -1 ffAlt. 9 (injection) CD EItlo (Incorporation) B No vector attraction reduction alternatives were performed El CERTIFICATION STATEMENT (please check the appropriate statement) - ------- E "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the ------- vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 021'. 1106 —and the 0 vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This nis determination has been made tinder my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are %significant penalties for false certification including fine and imprisonment." el Zj 114t - tv: k.-5 Mr. John W. Dunham L Prepares Erncand Titlq (type or print) Land Applier Name and Title (if applicZli—c)(type or print) -ig�of Pren�,,�� -e A . ...... Signa -e of Preparer* Date <!�jnature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) PATHOGEN AND VECTOR ATTRACTION REDUCTION DOCUMENTATION PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION DOCUMENTATION The Towns of Bridgeton and Maysville meet pathogen reduction and vector attraction reduction requirements through lime stabilization. Craven Ag Services, Inc. performed the lime stabilizations for Bridgeton and the Town of Maysville performed their own. Some land application events were surface applied, and some were incorporated. The Town of Maysville performed two application events in 2021: 1. March 2021 — Lime Stabilized and Surface Applied and 2. October 2021 — lime Stabilized and Incorporated The Town of Bridgeton performed f our application events in 2021: 1. January 2021 — lime Stabilized and Surface Applied, 2. May 2021 — Lime Stabilized and Surface Applied, 3. August 2021 — Lime Stabilized and Incorporated, and 4. November 2021 — Lime Stabilized and Incorporated. Documentation of these activities are found in the following section. N"ou 11 w EM Zyo anid. 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WO"d. ee 1"aw. ov 0000 L� I mswm % otlo I t'O —TA OC &new Lz Him"gj MOM 0 Colo aw OTO "d LZ woonw Qc'o sad oc OVO OdGE In ow W trod IrO INd 0910"d — —__ [8Pd ONW 18I '0 "Id Ewo sow88 n�ozd —• OTI iom SOIL ANALYSIS REPORTS CO C-11 z z co -6 Z, 0 z z z C: -61 A 0 z 0 4) �o 0) 0 w z rl cn 0 2 E 0 'o co ED - 61 b X- E 6 -6 a 6 0 C0 s z z CL (L IL co 6 LU w LU z t to c) to o co o 0 0) L: M z -7 m CD z w z am 0 0 > U o 0 CD V to 00 u CO (a N 0 N CD Cl) N 0 m N Nc — N N d) C: = CL Z> = N 0) N r (a :E 2: mM — X = 0) 0 a cli a (D to d) LO in w w aui u 0 u (D U) 0 CN cr) a) 0 Q) LO > CL Ln 0 'IT Z CD 0 r to =3 M 0 15 -W Z 0 <, C r- 0 E Z 2 10 D r 0 o 14 CD cn CO 0 N O o c co Oo ci U') .w 00 ch CO N 0 r® N 00 ch cj 4.4 m N CL 0 CL % E 0 Im E z co Z 0 S co 0 E LL co M S M M MM 7F Ln LO C\l ® M 4) w "U cn C, E -9 C) 6 0 z oE co 0 6 0 z m w u C) 0 E 0 nE CY) N i15:3 tA cs -T 66 :3 0 N C 0 Q 0 a 0 u 0 0 CL — cr CD 0 a) E r 'o z CL (6 0 M z CL 0 z CL r- cj a m a mm ra (D cy) Q E- w < 6 E w a (Dro - 0. E 0 w u 0 > 3: 0 m 4 0 E 'j 0 a u 0 0 h u oE E 0 OL C.) E -T o CL -E C; 0 U) CO ®0 0: ® cl) 0 C-4 u o Z r 2 L CL CI c) w w Q co q C', to 0 75 w 75 cli X ce 3: a) w 'Saw 9%, HvIt. E m 3: 0) Cl E w Z; C. E E w --T co U) m .9 m -0 (D o C� >� 0) b r EE ar o c w E C 2 LL .5 -Z5 C: 8 2 a) a j-- 72 (Lb tf 0 0 uO CD n_W CO ca co co c en a co co E U Lci QQ) ca -r- 0 c: z 0) mM m Zi E E CJ) E u) a) M a) fm - .0 cu cm rm u :3 0 :G 0 , 0 75 c E 2 CD ,2 ca rT 0 0 10 m :3 cc 0 CD ca ca 16 C c E E m cm 2 0- w w 0 0 0 z ce) C14 e .0 0 w CI)l ch X E IL U) z ME WR C N CD m cs o c) a N ro MU) o 0 E 0 co C: cm co 00 = LO cc ca us V U) 0 No CD tm E Lo r, Ln 0 U 00 E 0 co Z Lo to en ® L cD z C 0 IL . m 'a c V 1 r_ (U a) CL E wo E 68 0 CL 0 ci 0 W C-4 co cn Im LIJ b— CCD cv < U) Z!, V) cl 0 z 2021 APPLICATION SUMMARY TABLE I I m 2021 APPLICATION CONDITION SUMMARIES Town of Maysville Maysville, North Carolina Carven Ag Services WQ0037637 Annual 2021 Maysville WWTP Stabilization Method Lime Farmer: Allen Roach Acres: 7.25 Site/Tract: 6 Application Method: Surface Field: 1 Percent Solids: 2.58 Residual Report No.: M21-03724 Crop: Coastal Bermudagrass ........................................................................................................................ Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 3/24/21 1 42,000.0 Dry Warm Sunny 0.00 Tota Gallons 42,000:0 Town of Maysville Maysville, .North Carolina Carven Ag Services WQ0037637 Annual 2021 Maysville WWTP Stabilization Method Lime Farmer: Allen Roach Acres: 12.01 Site/Tract: 3 Application Method: Incorporated Field: 2 Percent Solids: 2.58 Residual Report No.: M21-03724 Crop: Rye (Grain) Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 10/26/21 2 44,000.0 Dry Warm sunny 0.00 . Qta GalloQ$ :..... 44,000,0 Town of Bridgeton Havelock, North Carolina Carven Ag Services WQ0002431 Annual 2021 Bridgeton WWTP Stabilization Method None Farmer: Allen Roach Acres: 3.65 Site/Tract: 3 Application Method: Surface Field: 1 Percent Solids: 0.84 Residual Report No.: BEI-440A Crop: Rye (Grain) Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 1/29/21 1 21,000.0 Dry Cool sunny 0.00 'fatal Ga��ons 21,000,0 Town of Bridgeton Havelock, North Carolina Carven Ag Services WQ01002431 Annual 2021 Bridgeton WWTP Stabilization Method None Farmer: Allen Roach Acres: 4.38 Site/Tract: 6 Application Method: Surface Field: 3 Percent Solids: 0.84 Residual Report No.: BEI-440A Crop: Coastal Bermuclagrass ...... ...... . . Date Field No. Subfield Gallons Son Conditions Weather Conditions Prev. 24 Hour Rainfall 5/12/21 3 18,000.0 Moist WarmOvereast 0.00 Gallons 0000 Town of Bridgeton Havelock, North Carolina Carven Ag Services WQ0002431 Annual 2021 Bridgeton WWTP Stabilization Method None Farmer: Allen Roach Acres: 12.01 Site/Tract: 3 Application Method: Incorporated Field: 2 Percent Solids: 0.84 Residual Report No.: BEI-440A Crop: Rye (Grain) Date Field No. Subfield Gallons Son Conditions Weather Conditions Prev. 24 Hour Rainfall 8/7/21 2 20,000.0 Dry Hot Sunny 0.00 Town of Bridgeton Havelock, North Carolina Carven Ag Services WQ0002431 Annual 2021 Bridgeton WWTP Stabilization Method None Farmer: Allen Roach Acres: 12.01 Site/Tract: 3 Application Method: Incorporated Field: 2 Percent Solids: 0.84 Residual Report No.: BEI-440A Crop: Rye (Grain) ................ Date Field No. Subfield Gallons Soil Weather Prev. 24 Hour Conditions Conditions Rainfall 11/3/21 2 21,000.0 Dry ('001 Sunny 0.00