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WQ0018352_Residual Annual Report 2021_20220225
Non-Discharge Branch Upload/Submittal Form �. NORTH CAROLINA EnWrvnmenfol Quoity Version 2-Revised June 23,2020 Initial Review Reviewer Thornburg,Nathaniel D Is this submittal an application?(Excluding additional information.)* Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2021 Permit Number(IR)* WQ0018352 Applicant/Permittee Town of Boiling Springs Email Notifications Does this need review by the hydrogeologist?* Yes No Regional Office Mooresville CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence. ............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................ Name* Michael F.Gibert Email Address* Phone Number* mike.gibert@boilingspringsnc.net 704-434-2357 Project Information Application/Document Type* New(Fee Required) Modification-Minor Modification-Major(Fee Required) Renewal Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1, Required) NDAR-2 Annual Report Residual Annual Report Additional Information Change of Ownership Other We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High-Rate Infiltration Other Wastewater Reclaimed Water Closed-Loop Recycle Residuals Single-Family Residence Wastewater Other Irrigation Permit Number:* WQ0018352 Has Current Existing permit number Applicant/Permittee Address* PO Box 1014 Boiling Springs NC 28017 Facility Name* Town of Boiling Springs Class B Residuals Program Please provide comments/notes on your current submittal below. 2021 Annual LA Residuals Report for the Town of Boiling Springs permit#WQ0018352 At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form,Engineering Plans,Specifications,Calculations,Etc.) 2021 Annual LA Residuals Report.pdf 6.77MB Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre-review until the fee(if required)has been received by the Non- Discharge Branch.Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order(as specified by the application). Mail payment to: NCDEQ—Division of Water Resources Attn:Non-Discharge Branch 1617 Mail Service Center Raleigh,NC 27699-1617 Signature Submission Date 2/25/2022 THE TOWN OF BOILING SPRINGS Date: 2/21/2022 To: The Information Processing Unit NCDWR Non-Discharge Branch 1617 Mail Service Center Raleigh,NC 27699-1617 Re: 2021 Annual Land Application of Residuals Town of Boiling Springs I NC Permit#WQ0018352 To Whom it May Concern: Please find enclosed the original report and all applicable forms and test results for the Annual Residuals Land Application Report for the Town of Boiling Springs.An electronic copy of the 2021 Annual Land Application Report has also been submitted.Aerobic digested residuals continue to be land applied to permitted fields for the beneficial reuse as a soil conditioner and fertilizer supplement. Please let me know if additional information is needed at 704-434-2357. Sincerely J ti angina Town Manager Town of Boiling Springs Enclosures: Annual Land Application Report 2021 ANNUAL LAND APPLICATION OF RESIDUALS 2021 ANNUAL REPORT TOWN OF BOILING SPRINGS 'I Permit No. WQ0018352 THE TOWN OF BOILING SPRINGS CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0018352 County: Cleveland Year: 2021 Facility Name(as shown on permit): Town of Boiling Springs Land Application Operator: Todd Humphries Phone: 704-300-8641 Land application of residuals as allowed by the permit occurred during the past calendar year? Yes El No -If No,skip Part A,and Part B and proceed to Part C. Also,If residuals were generated but not land applied,please attach an explanation on how the residuals were handled. Part A-Residuals Application Summary: Total number of application fields in the permit: 3 Total number of fields utilized for land application during the year: 2 Total amount of dry tons applied during the year for all application sites: 14.9 Total number of acres utilizes for land application during the year:I 26.2 Part B-Annual Compiance Statement: Facility was compliant during calendar year 2021 with all conditions of the land application permit (including but not limited to items 1-13 below)issued by the Division of Water Resources. iJ Yes 1] No If no please,provide a written description why the facility was not compliant,the dates,and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)copies of laboratory results are attached. 4) Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1105(a)or the Pollutant Loading Rates in 15A NCAC 02T.1105(b)(applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in I 5A NCAC 02T.I 111 were complied with(applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals,as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C-Certification: "I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate, and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." 4„ Justin Longino/Town Manager -`s g z3 'l.t gtur t Permittee Name and Title(type or print) -of Permittee Date Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T.1102(26) DENR FORM ACF(12/2006) RESIDUALS SAMPLING FORMS V 4.4 (0 a e V Cl/] 0 *4 l L w C U) S. CC Y i W �r LTO a c 2 • w y C — CV V7 0 0 ct 'a =c o. E 7 • uw toz G 6ais CI •cO y L'O _ _ _ _ _ el O U ' o _, I. cn 'Z n4 • I. *1 p a� m E _� Z E m O = 0 rl +�+ F- U V c .a r A 0 4V * Q � �COD � • i1 I, E — Q c .a cn 2 c� r, _ w° C ;04 o CI A C. 0 CN sz. a Cm— . te C p Q 0 g0 . i!t �+ w▪ = cov .. 2 � v at, n ++ z ry E-, z C o ea v in M 0 '4 c 03 a `-- erg 0° en n n oo N M, `,0 0 0 *° �� pti1. N c N C. y L. 6• p ik 0] � 0. = E 4 a 6to a a c0.i imt— G e4 74 _ 0 Z d' Ca Z O — 04 Z N 0o a Z 000 `^ �— a v Z Z Z Z y ;0" v � I?_", U a E N cn � CL bi0 lei ' w - et a) ort = p" ?' E a o = C O 0. . c. F Q 7 c 1.0 bh csD ti o cv sV E 0 COU _ w ar 0 y w L to +_+ eC • a Q nr a. It ° ea a z el 3 .4 S. . *. CI 114 iw• 3 01. a1 i, V 0 E og L It C 0 V •— tz } 0 U0 C'( 4 c� V .0 1 ca v a., C0 ea IWO Cr C .Q 0 • C �" �" L .a m c A cl 0.0 0 re) � c FIT.] cla w G 73 va E — ° o aa cc c .c v • 41 Z a a - ° a a° a� o, m ,-, A o a• v) .) •c ' f�1 r� _ ee QaA o a. ,E = 7 •� V¢] a �°' yam, s.. GL �" Chi a = GL, - Q U 2 Q- sr,. c evd cva " 'y~.,� v r cC a.d 0. e4 Ce �. 0 C4 C4 �0. y bD METALS FIELD LOADING SUMMARY LAND APPLICATION FIELD SUMMARY CD a 0 N fl•7 N „t tJ r- f--' '6 c 0. :J yr LL a.N o v: W CJ .al,._ < y y o er ,C E 'ai Q o 3 a a a 3 3 a s „a e'. z C G D U a. a. a a a a Cr. R. C. G. 0 = L , '� rY I i. tr., C C �+ z ~ .� C N a Q ._ a• EQQQQQ ¢ QQQO � '� `� v, a z z Z z z z z z z z o 0 0 a s �j o += 8 = x a o v. m a, ^� m` c Q - 'C s. Z e 0 Q. Fy 2 7 - N N n N n -- a `' a o Q, e� C.$ y R n a uy n r.; '0 - eT N a s C �•� C C Q G.i d N a. r: 2 a m ^�`• V'1 �S^. 'A a+ -• a C [V y 4 p _ .. ce ❑ Q v rs a. rr7 eri C* oc v, ni t- t- - k i � a a N nx rn , v 0 al = Gz] v U a, 12 o, n n n n n N- n n n n x ee y y _ a0o 0 0 0 0 0 0 0 0 0 0DO N N N N N N N N N N � ��- r.i a1 y +., 14 ais O iv �+ ed g re Ammonia a, '0 '0 '0 m '0 'C 'C 'C '0 � ° a te ,, o rn OO 6" o Nitrogen E r' v v r, v, v, v, v, �, n N p rat 0. C U0. a i U i M. 07 C u L 1 _ W U U z z` ea 0 w 0' v o a 0 o , ea u7 cn rel a n.l . rn f'S cn n•-k M M M M M e'S L7 w - L" ie'i 13 +6•� tYr 4 7J+ 44 /-w Cl Q _ ti. ‘D N •� i▪ 2 0 g U.. F .° Mineralization rn en rn M M M M r^ rn Lz oa n a es _ 'v to p cn E z Rate*** o 0 0 o c o 0 0 0 0 = Z o 0 0 v_ L ,a.,t� ❑ 4 Neu . _ Q. 7�y 4) .� Q+A Q W L 0v J 4 V • aC C.)W ° Volatilization v, v, in in vi p ; tr, 77 a G _ U Rate** o 0 0 0 o a o a o o c2 o = o �,o o a p * *W W 3 a Q * 0 Ind I, ,z+ f=7 X d L. .... a.. sZ G o Application c �' '° aq ^ e Qa GCev u r en rn en Ui C./1 CI, Cll. Cep , _ c co $'7 Method* c o ND 00 N 1 G ' 'H' U Yo rMr y ° N cz u a E v U4z7 Z e �oo L L y r o 0 0 o C C C C o o c 40 o Nn 0 a. a Ln ,c. 6 a p c�C a dIl 3 a v O a 0 4 ❑ aQ p +• ▪ `O o c0-1 c▪ dv C ' ' i; ^ C -U o 'a '- fIJ NfQ n � mZs c b b v a o o s 0 o a = = =c Ci Y Q a' a E 1. a s � i 0'c3 r- m en rr7 M m M M M M a 0 0Z. 00 .t m_ x =.� 0 aQ � � a. o3 .- y a a a a a a a aaa yV0 - M - •r_ 0.4 ▪ CCI W z 7rsrf� Q °� o o nop v o 0 0 0 0 0 c - ▪ U ee U a [t] o 0 0 0 o a o 0' o 0 • �0 _ ❑ U U U U U U U U V U on 'Cf o G03 c a 3 z z 2 z z z z z z z °j V o — rn v 2 C Zo. Q � Z o00 0 lee 0 o y ei 'O V C F0. .,., co -a '0 0 n '-a 00 - o v a o o M n ^ r t"" Cl.. rt s 6 = N C' N n r'y - - N *C Ir a o rfi 0.. Cr 'e u. = e4 0 oD., G•1 , Q - - 4 r. - r0 o N a o �r1 Sri M i. U = Q o 0 0 c . o Q Y - -= .�. �, a.) Q 8. es Q q s 4) - a. 0 a . . +� 3 Z W op N a Q Le! tr, h kn kn w" s -n ▪ oa a 7,63 a c o. 0 o 2 o y d _ .a i] o a- z e' c o a o o ^ o o c. 4 - eve U Q. a mr ;'a 0 0' O p b d 9 q C� O .7 iF 'G Q y eC u] a o 0 0 0 o a a S . o .- r�li i3 c ▪ s. bA O [� Y N o N S - - O i[• N 01. 0.▪ H � 0.w _ 42 Cl.) Y - G' a ee ~ C C E i '- — Q .\.,::‘ 5' p c. � 4 v 4 w •Oz ° c. o -a cei {,) -0 Q 7, quo NNQLLQ = Q c • 1.-e„ `° � N 'to u ea e aa d0 2�t?U r� = i 8 8 8 Q .-. cr , i n n QA. U C C r ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Town of Boiling Springs Total Dry Tons Applied(Annual): 10.36 Permit#: WQ0018352 Cation Exchange Capacity(non 503 only): Operator: Todd Humphries Owner: James Petty Predominant Soil Series:Pacolet-Bethieher Acres Used: 9.84 Acres Permitted: 22.41 Site#: 1 Field#: dP1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mglkg, % Solids use Raw Percent#): Sample or_1_ 2 3 4 5 6 _. 8 9 10 11 12 Com- posite _ Date 9/30/21 9/30/21 9/30/21 9/30/21 9/30/21 9/30/21 9/30/21 9/30/21 9/30/21 9/30/21 %Solids 1.5 1.5 1.5 1.5 1.5 1.5 1.5 1.5 1.5 1.5 Arsenic 1.48 1.48 1.48 1.48 1.48 1.48 1.48 1.48 1.48 1.48 Cadmium 0.253 0.253 0.253 0.253 0.253 0.253 0.253 0.253 0.253 0.253 Copper , 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 40.7 Chromium Lead 2.6 2.6 2.6 2.6 2.6 2.6 2.6 2.6 2.6 2.6 Mercury 0.473 0.473 0.473 0.473 0.473 0.473 0.473 0.473 0.473 0.473 Molyb- 1.64 1.64 1.64 1.64 1.64 1.64 1.64 1.64 1.64 1.64 denum Nickel 3.08 3.08 3.08 3.08 3.08 3.08 3.08 3.08 3.08 3.08 Selenium 1.07 1.07 1.07 1.07 1.07 1.07 1.07 1.07 1.07 1.07 Zinc 87.3 87.3 87.3 87.3 87.3 87.3 87.3 87.3 87.3 87.3 Total Phos- 22867 22867 22867 22867 22867 22867 22867 22867 22867 22867 phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total _1 2 3 4 5 5 7 8 9 10 11 12 DTIAc.I 1-3 App. Event 0.08 0.14 0.13 0.08 0.04 0.11 0.11 0.03 0.09 0.25 Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.003 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.00I Copper 0.006 0.011 0.010 0.006 0.003 0.009 0.009 0.002 0.007 0.021 0.000 0.000 0.086 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Lead 0.000 0.00I 0.00 i 0.000 0.000 0.001 0.001 0.000 0.000 0.001 0.000 0.000 0.005 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _0.000 0.000 0.001 Molyb- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.003 denum Nickel 0.000 0.001 0.001 0.000 0.000 0.001 0.001 0.000 0.001 0.002 0.000 0.000 0.006 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.002 Zinc 0.013 0.024 0.022 0.013 0.007 0.020 0.020 0.004 0.016 0.044 0.000 0.000 0.184 Total Phos- 3.476 6.403 5.808 3.476 1.738 5.214 5.214 1.143 4.070 11.616 0.000 0.000 48.158 phorus "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations". Z -ZI z Z Signature of Land Applier Date DENR FORM MFLSF(12/2006) to 0 n E. rA b = O 0— v y IL Q N p to Cc O c& rz CJ - - L U ha•2 Q a. d = . Z 6 G cg •p Q 7 7 7 = = 0 .-� ¢. a. a. a p a , z 034 Ih a - co pdo0ooaaoa na R =E k aat w °' U 0. �, 0. A a7 s., ^� Z 0 41 O. �^. ^ rl [� a 4 C �' c. V W L °� rY'r Q `--' . CC �^. QC ,C — ^yJ G Vl p a p CC Q V Q� tV a v ... yr O .O C O .^7• O `1. lV CJ a� ❑ Q V a {] v; ri v-i r ._. o o a .. o nl U7 = «, p d +st W as U U a n � ccyL , ea y „ _ O iC 4 0, O 0 Ne — cc Q = co U ai C �y W Ammonia x .gsi `-7,1: x.,5,.,.: ea �'_ _ _ G ° .1 c Nitrogen N d °; c ^a U c°'i o 3 0 Gr Cq _ _ C �' cn t U E O. 7y ❑ Q = 000001111111 °' n v CA v1 el i .= Q a p. ri U w �' 6 o Q °O ete o co 04 y a Mineralization1111:111111111 G a rr ea t, p 2 . E z Rates s .6 ' t o a ❑ � am g a'.3 L N Z. 7 3 V V v Z y A Q W Volatilization ❑ o 41 c W W = a U Rate" - o 0 0 0 E v' a 4 o i—c 3 7 y r. o 0 Q * * 0 * F 41 x ti Z a m p Application = V 6 .• o Q Method* "60 '� Il O ry DO cl d� U Y a ono •°y' ° N m 0 -- r l E C m V C7 Q d ��tr) y o x oMo v w . p ao -a 3 G0- ti oao ,0r!l ❑ Q cC ? E = 2. c°nUCa3 ° o U y V' o = L 4 [-1 Ao - 40 d C k d o v Q - Zit- . , d ns r,7 rn r^, r, cn a C r- cc o r°.-, G. •L'" 0 Q y 0 Cr7 , = N = o a ^ �, 17 CC W C s. 3wd :? o 0 0 0 0 Ts y e a � v� U 3 a p C? C} V V U R Z 2 0�. = u- 3 44447 C U o o a rr C a C el a 'C ^C Ak 0. E 'a nn .rvc 00 a v-, o c o Cv v-, r ex ,. ► th L ° d a a Q a a a Q '. 'C = ^0 ,- U L 7 a o o a 4 a o o 6 a o a) -I acc; Q 0 = 0 CI] DI a, _ ++ _ .0 Ca. Y e .N N Q o tn tn v? tn 113 Q _ Q o 0 0 M O y G] U 03 G. ',..,,�' C. c� C4 o p y ,- Gz7 w d 3 ei y _0 U U G. r 0 G v! p O O O 4 r- c�G *# "6 0 s W 3 E v Z •a0 0. 0 o , _ 7 -0 *e (-4 = C. C •, a 8 ,. U e ›- m C6 3 ° Q U ,_1 = s. cc gluoW NQry 3 ? w Le 8 u. C N M ,0 ¢ t_ = ff 0 d0 OWG M N N C� C�+ o _ •O = OJ w E- Qa, Uac a5 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Town of Boiling Springs Total Dry Tons Applied(Annual): 4.52 Permit#: WQ0018352 Cation Exchange Capacity(non 503 only): Operator: Todd Humphries Owner: James Petty Predominant Soil Series:Pacolet-Bethieher Acres Used: 16.36 Acres Permitted: Site#: 2 Field #: JP2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#): Sample or 1 2 3 4 5 6 7 8 9 10 11 12 Com- posite Date 9/30/21 9/30/21 9/30/21 9/30/21 9/30/21 %Solids 1.5 1.5 1.5 s 1.5 1.5 Arsenic 1.48 1.48 1.48 1.48 1.48 Cadmium 0.253 0.253 0.253 0.253 0.253 Copper 40.7 40.7 40.7 40.7 40.7 Chromium Lead 2.6 2.6 2.6 2.6 2.6 Mercury 0.473 0.473 0.473 0.473 0.473 Molyb- 1.64 1.64 1.64 1.64 1.64 denum Nickel 3.08 3.08 3.08 3.08 3.08 Selenium 1.07 1.07 1.07 1.07 1.07 Zinc 87.3 87.3 87.3 87.3 87.3 Total Phos- 22867 22867 22867 22867 22867 phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ App. Event 0.08 0.05 0.08 0.06 0.02 Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 0.006 0.004 0.006 0.004 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Lead 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0 000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 denum Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 -Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Zinc 0.013 0.009 0.013 0.010 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.048 Total Phos- 3.476 2.470 3.476 2.515 0.686 0.000 0.000 0.000 0.000 0.000 0.000 0.000 12.623 phorus "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) RESIDUALS ANALYSIS LAB SHEETS Illi Pace Analytical Services,LLC Pace Analytical 9800 Kinney Ave. Suite 100 Huntersville,NC 28078 wompacelabs.com (704}875-9092 ANALYTICAL RESULTS Project: DIGESTER SLUDGE TEST ANNUAL Pace Project No.: 92564384 Sample: DIGESTER SLUDGE#8 Lab ID: 92564384001 Collected: 09/30/21 08:00 Received: 09/30/21 08:20 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method:EPA 6010D Preparation Method:EPA3010A Pace Analytical Services-Asheville Aluminum 21800 uglL 100 1 10/04/21 11:58 10/07/21 17:43 7429-90-5 Arsenic 22.2 ug/L 10.0 1 10/04/21 11:58 10/07/21 17:43 7440-38-2 Cadmium 3.8 uglL 1.0 1 10/04/21 11:58 10/07/21 17:43 7440-43-9 Calcium 487000 ug/L 1000 10 10/04/21 11:58 10107/21 17:33 7440-70-2 Copper 611 ug/L 5.0 1 10/04/21 11:58 10/07/21 17:43 7440-50-8 Lead 0.039 mg/L 0.0050 1 10/04/21 11:58 10/07/21 17:43 7439-92-1 Magnesium 42000 ug/L 100 1 10/04/21 11:58 10/07/21 17:43 7439-95-4 Molybdenum 24.6 ug/L 5.0 1 10/04/21 11:58 10/07/21 17:43 7439-98-7 Nickel 46.2 ug/L 5.0 1 10/04/21 11:58 10/07/21 17:43 7440-02-0 Potassium 83700 ug/L 5000 1 10/04/21 11:58 10/07/2117:43 7440-09-7 Selenium 16.1 ug/L 10.0 1 10/04/21 11:58 10/07/21 17:43 7782-49-2 Sodium 52100 ug/L 5000 1 10/04/21 11:58 10/07/21 17:43 7440-23-5 Zinc 1310 uglL 10.0 1 10/04121 11:58 10/07/21 17:43 7440-66-6 245.1 Mercury Analytical Method:EPA 245.1 Rev 3.0 1994 Preparation Method:EPA 245.1 Rev 3.0 1994 Pace Analytical Services-Asheville , Mercury 7.1 ug/L 2.0 1 10/06/21 11:30 10/07/21 13:37 7439-97-6 Sample: DIGESTER SLUDGE#9 Lab ID: 92564384002 Collected: 09/30/21 08:00 Received: 09/30/21 08:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Plant Available Nitrogen Analytical Method:None Pace Analytical Services-Asheville Plant Available Nitrogen 499 mg/L 1 10/18/21 10:27 N2 350.1 Ammonia Analytical Method:EPA 350.1 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Ammonia 8.4 mg/L 1.0 10 10/15/21 10:48 7664-41-7 Y 351.2 Total Kjeldahl Nitrogen Analytical Method:EPA 351.2 Rev 2.0 1993 Preparation Method:EPA 351.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Kjeidahl,Total 654 mg/L 50.0 5 10/11/21 20:29 10/12/21 05:08 7727-37-9 353.2 Nitrogen,NO2IN03 unpres Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,NO2 plus NO3 301 mg/L 4.0 100 10/02/21 01:00 Nitrogen,Nitrate 299 rng/L 4.0 100 10/02/21 01:00 14797-55-8 Nitrogen,Nitrite 1.6 mg/L 0.040 1 10/02/21 00:08 14797-65-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/25/2021 05:04 PM without the written consent of Pace Analytical Services,LLC, Page 5 of 25 /62 Pace Analytical Services,LLC • 9800 KinceyAve. Suite 100 au iiii�iJ`r u( Huntersville.NC 28078 www.pacelabs.cont (704)875-9092 ANALYTICAL RESULTS • Project: DIGESTER SLUDGE TEST ANNUAL Pace Project No.: 92564384 Sample: DIGESTER SLUDGE#10 Lab ID: 92564384003 Collected: 09/30/21 08:00 Received: 09/30/21 08:20 Matrix: Solid Results reported on a"dry weight"basis and are adjusted for percent moisture,sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua! 2540G Total Percent Solids Analytical Method:SM 2540G-2011 Pace Analytical Services-Charlotte Total Solids 1.5 °I° 0,10 1 10/07/21 17:45 Percent Moisture Analytical Method:SW-846 Pace Analytical Services-Charlotte Percent Moisture 98.5 °I° 0.10 1 10/07/21 17:41 N2 Sample: DIGESTER SLUDGE#11 Lab ID: 92564384004 Collected: 09/30/21 08:00 Received: 09/30/21 08:20 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Metals(ICP)6010D Analytical Method:EPA 6010D Preparation Method:3015 Pace National-Mt.Juliet Calcium 1190000 ug/L 9000 9 10/22121 12:49 10/22/21 22:11 7440-70-2 Magnesium 85800 ug/L 9000 9 10/22/21 12:49 10/22/21 22:11 7439-95-4 Sodium 58300 ug/L 27000 9 10/22/21 12:49 10/22/21 22:11 7440-23-5 Calculated Results Analytical Method:Calculated Preparation Method:Cale Pace National-Mt.Juliet Sodium Adsorption Ratio 0.439 1 10/22/21 22:11 10/22/21 22:11 SAR Sample: DIGESTER SLUDGE#12 Lab ID: 92564384005 Collected: 09/30/21 08:00 Received: 09/30/21 08:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 9040 pH Analytical Method:EPA 9040C Pace Analytical Services-Asheville pH at 25 Degrees C 7.7 Std.Units 0.10 1 10/12/21 16:41 Q 350.1 Ammonia Analytical Method:EPA 350.1 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen,Ammonia 8.4 mg/L 2.5 25 10/15/21 10:50 7664-41-7 Y 353.2 Nitrogen,N021NO3 unpres Analytical Method:EPA 353.2 Rev 2.0 1993 Pace Analytical Services-Asheville Nitrogen.NO2 plus NO3 389 mg/L 4.0 100 10/02/21 01:01 Nitrogen,Nitrate 385 mg/L 4.0 100 10/02/21 01:01 14797-55-8 Nitrogen,Nitrite 3.9 mglL 0,40 10 10/02/21 01:15 14797-65-0 365.1 Phosphorus,Total Analytical Method:EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365.1 Rev 2.0 1993 Pace Analytical Services-Asheville Phosphorus 343 mg/L 5.0 1 10107/21 21:13 10/08/21 21:14 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in Tull, Date:10/25/2021 05:04 PM Without the writlen consent of Pace Analytical Services,LLC. Page 6 of 25 Pace Analytical Services,LLC 9800 noeyAve. Suite 100 / eAnalytica Huntersvilfe,NC 28078 wew.pacelabs.eom (704)875-9092 ANALYTICAL RESULTS Project: DIGESTER SLUDGE TEST ANNUAL Pace Project No.: 92564384 Sample: DIGESTER SLUDGE#13 Lab ID: 92564384006 Collected: 09/30/21 08:00 Received: 09/30/21 08:20 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 1010 Flashpoint,Closed Cup Analytical Method:EPA 1010B Pace Analytical Services-Asheville Flashpoint >200 deg F 1 10/12/21 17:31 Sample: DIGESTER SLUDGE#14 Lab ID: 92564384007 Collected: 09/30/21 08:00 Received: 09/30/21 08:20 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 733C S Reactive Cyanide Analytical Method:EPA 9014 Preparation Method:SW-846 7.3.3.2 Pace Analytical Services-Greensburg Cyanide,Reactive ND mg/kg 1,0 1 10/08/21 15:52 10/12/21 13:28 7345 Reactive Sulfide Analytical Method:SM 4500-52-F-2011 Preparation Method:SW-846 7,3,4.2 Pace Analytical Services-Greensburg Sulfide,Reactive ND mg/kg 10.1 1 10/08/21 15:48 10/08/21 16:05 Q REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/25/2021 05:04 PM without the written consent of Pace Analytical Services,LLC. 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J a7 ry ry m Ln r-I cr .7 LO ,,.i tD ry m pnp 8 ip N O S , P p 8 co C N " Q = , E 0 0 •4 0 0 O O L ,0 V J « J 16 T ❑ ° II II II 11 II II II II II II II III II• .0 TS C .0 '~ 41 E ei 0 0 0 0 0 0 asa E 00de-, ❑ 00040o' S $ 8800000000 a 2 0 M a o 0 o a o No c t d Al __.8r1 r1 r-1 r-1 ey e-I ri tti .-1 r-1 ey ri r-I a ^, J ❑ ° -a -IDa a a a a a a a 'CS '0 v a ° _ 0 $ L ed w a a a+ m m d a m a m CO a ti E va a ,v_ at � � � ,v_ a ❑ �° E `m E °c ° 7 7 7 7 7 7 7 > > 7 7 7 �atl ~ ❑ y ❑ �' N o 'o •o 'o a a 6 'a 'a 6 6 'a o E; w E wTo .11i L (V 0 @ i a O 7 +-' O ry c0 O e-1 O ID N Q e-I O O N a 3 ra 3 �-' .cE RN r.] O e-I O v to v ui O r-I n y E -17 ry O Lp O •ry m , rK m N y I.L. N co W N ❑ LL C ILL Q J = ,_ F. al:. 'a = G] 0 a• u E N Iy t Ia m Ly .0 Y . L r.+ = rN-1 rN-I ,, rN-1 ,-1 rN-1 rNi .N-1 r-I r-I .- rN-1 ,1 N y O p p d a 0 0 0 0 0 p 4 d y m y o v o 0 0i_n 0 o a at) = M i C .i O o O O O o a 0 v o 0 v O . C u O o O o 0 0 0 0 C i w U a C U a U a .y. �' �° �° �° 3° 3E a2 �' 3 3' �° 3E 3° y e e e e i e e ate. a a 0 ? 'E O a +• N N N N N N N N N N N N N +, N N N N N N N N Y a VI ey ey 14 e-I ri ri ei .4 r-I r-1 r-1 r-I rl v e-1 r-1 rti wi 94 .-1 .-1 e-1 C1 i CJ ' Q) ' W • a s a . a a _ _ _ . . . . . J J J +• ad'c=�'= = = = = 3d 'c7d + EESEEEEE c = c 6 o p o 0 D _ N ''1 O v N m N m N O m ry ''' °O m cr N - N Cl 00 Tr ca N 0 ct a ca ,eten 0 L 2 a _ m +a, +a, 7 •d 'C O1 NE E N 7 N ro E ra p '' :: 'p E ro = a £ E c a 2 2 2 1- ¢ L a [_ to c c 3 3 E `- v N E E a ac+ aci aci CU s° > > 0. = E 7 ¢ = TarLi = 3 u 40 a7 m m m Q 7 „ -DE m c rII o _, 0 Ol o = dl 0 � .. .. �_ , a Q OC m m 0 _ Q d U U U '2 2 a Lri In [J �2 . 2 2 Z Z 21 4 0. Ian s ca LL a Sodium Absorption Ration (SAR) 2021 9/30/2021 Results Ca — 1,190 mg/I Mg — 85.8 mg/I Na — 58.3 mg/I You have to know the valence of each of the compounds (can be found ❑n the periodic table) s❑ you can convert mg/i (mg/kg) to megii. Ca has 2 electrons, and the molar mass is 40.4. Mg has 2 electrons, and the molar mass is 24.3. Na has 1 electron, and the molar mass is 22.9. Ca concentration = (1 ,190 mg/kg x 2) 140 = 59.5 Mg concentration = (85 8 mg/kg x 2) / 24.3 = 7.06 Na concentration = (58.3 divided by 22.9) = 2.54 meq/L SAR is: Concentration ❑f Na in meg1L divided by the square root of 1/2 x (concentration of Mg in meq/L + concentration of Ca in meq/L) Sum of Ca and Mg = 66.56, half of that is 33.28 Square root of 33.28 = 5.77 Na is 2.54 The SAR results is: 2.5415.77 = .0.439 meg/L Analytical Results STATESVILLE ANALYTICAL Pace Analytical 9800 Kincey Suite 100 Huntersville, NC 28078 Receive Date: 09/30/2021 Reported: 12/08/2021 For: Town of Boiling Springs Comments: GEOMETRIC MEAN: 125,032 MPNIg Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 2 1 0 93 0-2 0-0 1 Fecal Coliforms 1 102410 MPNIg SM92210E-2006 09/30/2021 MD 210930-20-01 Percent Solids 1 1.66 ova SM2540s-2011 10/01/2021 MD 210930-20-02 Fecal Coliforms 2 101796 MPNIg SM92210E-2006 09/30/2021 MD 210930-20-02 Percent Solids 2 1.67 % sM254os-2011 10/01/2021 MD 210930-20-03 Fecal Coliforms 3 136905 MPNIg SM92210E-2006 09/30/2021 MD 210930-20-03 Percent Solids 3 1.68 % S45408.2011 10/01/2021 MD 210930-20-04 Fecal Coiiforms 4 137725 MPNIg sM92210E-2006 09/30/2021 MD 210930-20-04 Percent Solids 4 1.67 % SM25406.2011 10/01/2021 MD 210930-20-05 Fecal Coliforms 5 178571 MPN/g sM92210E-2o06 09/30/2021 MD 210930-20-05 Percent Solids 5 1.68 % sM25408-2011 10/01/2021 MD 210930-20-06 Fecal Coliforms 6 100592 MPNIg SM92210E-2006 09/30/2021 MD 210930-20-06 Percent Solids 6 1.69 % SM2540B-2011 10/01/2021 MD 210930-20-07 Fecal Coliforms 7 135294 MPNIg 5M92210E-2006 09/30/2021 MD 210930-20-07 Percent Solids 7 1.70 % sM2540a-2011 10/01/2021 MD Respectfully submitted, Melissa Myers NC Cert#440, NCDW Cert#37755, EPA#NC00909 PO Box 228• Statesville, NC 28687 •704/872/4597 Page 1 of rage 3 of 6 ",=�;1 s r, :•r_+. _ • •-r.sr:r.cN... 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X 600ft.Approx) = 11,780 gal/acre or 3.8 loads/acre Year: 2021 r Weather Soil Volume Drivers Date Ph %solids Location Field condition condition gallons initials Rain 3/8/21 6.7 1.8 Petty JP1 Sunny Dry 12000 JG 0.0 3/9/21 ‘.7 /. c44.y P I S Orr 'Xy. j �(,... 0.0• 3/10/21 �- '7 /-S" �p}C./47 TRI �c�,.wr T Del 2..00aC) co 0_0 - 3/11/21 6 -7 1.g ikr-447 r,Q1 54 (I 'r v 1 Z600 7 G d_o 3fJ ltiz/ ��1 -17 /• f c� F}� _ 7�>♦ r�kr, pry 6600 T(4- -O L//3/z/ I .2 /. 0 64 4`{ Ty/ S4r,e dr? R 7/a/z1 7 I. 01� ,1 Q I .sw,wq %)f i / Ov C O.O 10/l1/Z1 70 l. � rc. d f't s /N Cr- I�fez f-1 7 _ j .1 eI S64�.• Pr r '( Q.o. Plivzir 7 a 7 % d P pry _ stow° k+.ST 0.0, J l/3,yzr 1 pcJ- . _ a et_ .Sk,y D y t �.G OO d Gr 0.0 izjc/z.i C"6 !' ec,tfy • 7' Skrw?' d)r'y ILi6da rj(r G I1-/%-/at C Tp2- S — of 2"kk) d 0 12/37- (- . I-Y ec.,d47 J P l2/r I / a Cr o .o t 2.'G'i! ‘ .Ia I.Y 'c, �i�Z s �►N �-Y o t' yCO , I1 - 0- ,a PATHOGEN & VECTOR ATTRACTION REDUCTION FORMS ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Town of Boiling Springs WQ Permit Number: WQ00183352 WWTP Name: Town of Boiling Springs WWTP NPDES Number: NC0071943 Monitoring Period: From 1/1/2021 To 12/31/2021 Pathogen Reduction (40 CFR 503.32)-Please indicate level achieved and alternative performed: Class A: Alternative I J Alternative 2 Alternative 3 J Alternative 4 J Alternative 5 J Alternative 6 J If applicable to alternative performed (Class A only) indicate"Process to Further Reduce Pathogens": Compost D Heat Drying 0 Heat Treatment I Therntophilic J Beta Ray I Gamma Ray ❑ Pasteurization J Class B: Alternative 1 J _ Alternative 2 J If applicable to alternative performed (Class B only) indicate"Process to Significantly Reduce Pathogens": Lime Stabilization I Air Drying_] Composting ._I Aerobic Digestion J Anaerobic Digestion I. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Patho en DensityNumber of' Analytical g Frequency Sample Parameter Tech- in Sludge Excee- of Analysis g Minimum Geo. Mean Maximum Units dences y Type niaue 2 x 10 to the MPN 100592 125032 178571 MPN/g 0 7/year Grab SM9221 6th power per gram of CFU Fecal Coliform total solids 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid(dry coliform) weight) Vector Attraction Reduction (40 CFR 503.33)-Please indicate option performed: Alt.1 (VS reduction) I Alt. 2(40-day bench) J Alt. 3 (30-day bench) I Alt. 4(Spec. 0, uptake) El• Alt. 5 (14-Day Aerobic) ! Alt. 6(AIL. Stabilization J Alt 7(Drying- Stable) Alt. 8(Drying- Unstable) Alt. 9(Injection) El Alt. 10(Incorporation) No vector attraction reduction alternatives were performed rj CERTIFICATION STATEMENT(please check the appropriate statement) t l "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mike Gibert/Public Works Director _ Todd Humphries/Wastewater Supervisor Preparer Name and Title(type or print) Land Applier Name nd Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) DENR FORM PVRF 503 (12/2006) Annual Pathogen and Vector Reduction Summary Town of Boiling Springs permit # WQ0018352 2021 Fecal Coliform - Class B There were seven (7) test results provided by Pace Analytical Services in Huntersville. The calculated Geo Mean for the Fecal Coliform samples was 125032 MPN/g. Vector Attraction Reduction Option 4 - Sour test results are reported in the attached data showing seven (7) test results at 1.02 mg Oxygenlglhr or less for Specific Oxygen Uptake Rate. End temperature for each test result was under 30 Degrees Celsius and the percent solids were under 2% for each result. Specific Oxygen Uptake Rate SOUR Facility Name: Town of Boiling Springs,NC Biosolids Permit Number: WQ0018352 Date: 9/30/21 Digester Temperature: 22 Sampling DaterTime: 9/30/21 Sampled By: Todd Humphries Analysis Date/Time: 9/30/2021 /6:00:00 AM A Analyzed By: Todd Humphries Sample Volume: 300 milliliters Total Solids: 1.66 % Dry Solids Beginning Temperature: 22 degrees Celsius End Temperature: 21 degrees Celsius Time Dissolved Oxygen Level (minutes) (mgll) 0 7.03 1 6.89 2 6.71 3 6.60 4 6.52 5 6.55 6 6.44 7 6.35 8 6.27 9 6.22 10 6.13 11 6.08 12 6.00 13 5.94 14 5.88 15 5.80 Slope: 0.1 Intercept: 6.9 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 4.53 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.91 mg Oxygen/g/hr Average Temperature: 22 degrees Celsius Temperature Correction Factor: 0.907029478 Temperature Corrected Specific Oxygen Uptake Rate: 0.83 mg Oxygenlglhr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. {1) 2 3 4 5 6 7 Circle Test# PH 7.90 Specific Oxygen Uptake Rate SOUR Facility Name: Town of Boiling Springs,NC Biosolids Permit Number: WQ0018352 Date: 9/30/21 Digester Temperature: 22 Sampling Date/Time: 9/30121 Sampled By: Todd Humphries Analysis Date/Time: 9/30/2021 6:15 Analyzed By: Todd Humphries Sample Volume: 300 milliliters Total Solids: 1.67 % Dry Solids Beginning Temperature: 22 degrees Celsius End Temperature: 21 degrees Celsius Time ❑issolved Oxygen Level (minutes) (mgll) 0 6.94 1 6.80 2 6.77 3 6.65 4 6.63 5 6.55 6 6.43 7 6.39 8 6.35 9 6.28 10 6.22 11 6.17 12 6.12 13 6.07 14 6.03 15 4.52 Slope: 0.1 Intercept: 7.0 Correlation Coefficient: 0.8 Oxygen Uptake Rate: 5.66 mg Oxygen/hr Ambient Specific❑xygen Uptake Rate: 1.13 mg Oxygenlglhr Average Temperature: 22 degrees Celsius Temperature Correction Factor: 0.907029478 Temperature Corrected Specific Oxygen Uptake Rate:: 1.02 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 (2) 3 4 5 6 7 Circle Test# Specific Oxygen Uptake Rate SOUR Facility Name: Town of Boiling Springs,NC Biosolids Permit Number: WQ0018352 Date: 9/30/21 Digester Temperature: 22 Sampling Date/Time: 9/30/21 Sampled By: Todd Humphries Analysis Date/Time: 9/30/2021 /6:30:00 AM Analyzed By: Todd Humphries Sample Volume: 300 milliliters Total Solids: 1.68 % Dry Solids Beginning Temperature: 22 degrees Celsius End Temperature: 21 degrees Celsius Time Dissolved Oxygen Level (minutes) (mgll) 0 6.52 1 6.41 2 6.35 3 6.33 4 6.30 5 6.28 6 6.26 7 6.20 8 6.15 9 6.11 10 6.08 11 6.04 12 5.98 13 5.93 14 5.89 15 5.85 Slope: 0.0 Intercept: 6.5 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 2.46 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.49 mg Oxygen/g/hr Average Temperature: 22 degrees Celsius Temperature Correction Factor: 0.907029478 Temperature Corrected Specific Oxygen Uptake Rate: 0.44 mg Oxygenlglhr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 (3) 4 5 6 7 Circle Test# Specific Oxygen Uptake Rate SOUR Facility Name: Town of Boiling Springs,NC Biosolids Permit Number: WQ0018352 Date: 9/30/21 Digester Temperature: 22 Sampling Date/Time: 9/30121 Sampled By: Todd Humphries Analysis Date/Time: 9/30/21 16:45 AM Analyzed By: Todd Humphries Sample Volume: 300 milliliters Total Solids: 1.67 % Dry Solids Beginning Temperature: 22 degrees Celsius End Temperature: 21.0 degrees Celsius Time Dissolved Oxygen Level (minutes) (mg/I) 0 6.38 1 6.33 2 6.29 3 6.26 4 6.24 5 6.21 6 6.18 7 6.14 8 6.09 A 9 6.05 10 6.01 11 5.95 12 5.91 13 6.10 14 5.98 15 5.89 Slope: 0.0 Intercept: 6.4 Correlation Coefficient: 0.9 Oxygen Uptake Rate: 1.82 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.36 mg Oxygen/g/hr Average Temperature: 22 degrees Celsius Temperature Correction Factor: 0.907029478 Temperature Corrected Specific Oxygen Uptake Rater 0.331mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 3 (4) 5 6 7 Circle Test# Specific Oxygen Uptake Rate SOUR Facility Name: Town of Boiling Springs,NC Biosolids Permit Number: WQ0018352 Date: 9/30/21 Digester Temperature: 22 Sampling Date/Time: 9/30/21 Sampled By: Todd Humphries Analysis Date/Time: 9/30/21 /7:15 AM Analyzed By: Todd Humphries Sample Volume: 300 milliliters Total Solids: 1.68 % Dry Solids Beginning Temperature: 22 degrees Celsius End Temperature: 21.0 degrees Celsius Time Dissolved Oxygen Level (minutes) (mg/I) 0 6.64 1 6.63 2 6.54 3 6.50 4 6.44 5 6.42 6 6.44 7 6.41 8 6.39 9 6.34 10 6.28 11 6.23 12 6.22 13 6.19 14 6.13 15 6.09 Slope: 0.0 Intercept: 6.6 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 2.08 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.41 mg Oxygen/g/hr Average Temperature: 22 degrees Celsius Temperature Correction Factor: 0.907029478 Temperature Corrected Specific Oxygen Uptake Rate: 0.371mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 3 4 (5) 6 7 Circle Test# Specific Oxygen Uptake Rate SOUR Facility Name: Town of Boiling Springs,NC Biosolids Permit Number: WQ0018352 Date: 9/30/21 Digester Temperature: 22 Sampling Date/Time: 9/30/21 Sampled By: Todd Humphries Analysis Date/Time: 9/30/21 /7:30 AM Analyzed By: Todd Humphries Sample Volume: 300 milliliters Total Solids: 1.69 % Dry Solids Beginning Temperature: 22 degrees Celsius End Temperature: 21.0 degrees Celsius Time Dissolved Oxygen Level (minutes) (mg/I) 0 6.44 1 6.42 2 6.38 3 6.32 4 6.28 5 6.27 6 6.26 7 6.20 8 6.14 9 6,10 10 6.05 11 6.01 12 5.95 13 5.90 14 5.87 15 5.82 Slope: 0 0 Intercept: 6.5 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 2.52 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.50 mg Oxygen/gfhr Average Temperature: 22 degrees Celsius Temperature Correction Factor: 0.907029478 Temperature Corrected Specific Oxygen Uptake Rate: 0.45mg Oxygenfgfhr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 1 2 3 4 5 (6) 7 Circle Test 4 Specific Oxygen Uptake Rate SOUR Facility Name: Town of Boiling Springs,NC Biosolids Permit Number: WQ0018352 Date: 9/30/21 Digester Temperature: 22 Sampling Date/Time: 9/30/21 Sampled By: " Todd Humphries Analysis Date/Time: 9/30/21 /7:45 AM Analyzed By: Todd Humphries Sample Volume: 300 milliliters Total Solids: 1.7 % Dry Solids Beginning Temperature: 22 degrees Celsius End Temperature: 21.0 degrees Celsius Time Dissolved Oxygen Level (minutes) (mg/I) 0 6.65 1 6.53 2 6.37 3 6.36 4 6.32 5 6.26 6 6.15 7 6.10 8 6.06 9 5.99 10 5.93 11 5.87 12 5.83 13 5.81 14 5.76 15 5.65 Slope: 0.1 Intercept: 6.6 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 3.64 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.71 mg Oxygen/g/hr Average Temperature: 22 degrees Celsius Temperature Correction Factor: 0.907029478 Temperature Corrected Specific Oxygen Uptake Rate: 0.65 mg Oxygen/gfhr Instructions: Enter Data in the Blue Boxes. 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