WQ0014452_Residual Annual Report 2021_20220224

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0014452
Applicant/Permittee Town of Bladenboro
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office Fayetteville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Lysa Finnerty
Email Address* Phone Number*
[e-mail] 14105376150
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0014452
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court,Ste 100,Baltimore,MD 21220
Facility Name* Town of Bladenboro Class B Residuals Program
Please provide comments/notes on your current submittal below.
2021 Annual Report for Town of Bladenboro,NC
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
Bladenboro NC 2021 Annual Report FINAL.pdf 5.66MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature Lp
Ja TM/WO
Submission Date 2/24/2022

435 Williams Court,Suite 100
Baltimore,MD 21220 SYNAG R
www.synagro.com
FEBRUARY 24,2022
NCDEQ
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2021 Annual Report for Permit No.WQ0014452
Dear NCDEQ:
Synagro is submitting one electronic copy of the above referenced report on behalf of the
Town of Bladenboro, NC.
If you have any questions or need additional information,please do not hesitate to contact
Andrew Coleman at 910-234-2371 or Matthew Carter at 336-705-9886.
Sincerely,
1 e't iC& Sfiiva'c 25
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Andrew Coleman,Town of Bladenboro
Matthew Carter,Synagro
YOUR PARTNER FORA CLEANER,GREENER WORLD

TOWN OF BLADENBORO, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0014452
2021 ANNUAL REPORT

Town of Bladenboro, NC
Residuals Land Application Program
2021 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms & Residuals Analysis
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00014452 County Bladen Year 2021
Facility Name(as shown on permit)Bladenboro WWTP NPDES No.NC0026352
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO,skip Part A,and Part B and proceed to Part C. Also,if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A—Residuals Application Summary:
Total number of application fields in the permit: 4
Total number of fields utilized for land application during the year: 1
Total amount of dry tons applied during the year for all application sites: 12.42
Total number of acres utilized for land application during the year: 9_9
Part B—Annual Compliance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit(including but not limited to
items 1-13 below)issued by the Division of Water Quality X YES NO.
If no,please provide a written description why the facility was not compliant,the dates,and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three(3)copies of
laboratory results are attached.
4. Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1105(a)or the Pollutant Loading
Rates in 15A NCAC 02T.1105(b)(Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503
regulated facilities).
8, All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or,in the case of a deviation,prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C—Certification:
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate,and complete. I
am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations,"
1,44.4ii Town Administrator /5 FA,D1
Pei"mittee Name 4nd Title(type or print) Signature of Penn' ee Date
V4.15 4_ Lb1,A.47I 2/15/2022
ignatuit of PreparerT Date Si o Lan pplier Date
(if different from Permittee) (if different om Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T.1102(26) DENR FORM ACF(12/2006)

OPERATIONS SUMMARY-LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES -ALL SITES
DATE RANGE: 1/1/2021 - 12/31/2021
BLADENBORO,NC
BLADENBORO,NC AEROBICALLY DIGESTED LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
July 2021 322,400.00 G 12.42 D 11.27
TOTAL 322,400.00 G 12.42 D 11.27
Units Key: D-Dry Tons; G—Gallons;W—Wet Tons;Y—Cubic Yards
Report Date: 1/6/2022 11:34:35 AM

SECTION 2

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Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Nate Roth
Project Name: Bladenboro
Lot Number:WD22023
Date Completed:05/11/2021
—
05/11/2021 11:04 AM
Approved and released by:
Project Manager II: Lucas Odom
MILB
Q PCCR�c��
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WD22023
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low% solid the initial amount of sample -002 was 3 times the standard procedure amount per
PM's request. The LOQ has been adjusted accordingly.
TCLP VOCs
The following sample was analyzed outside of analytical holding time: WD22023-001. This sample was
over-looked when loading based off of holding-times.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2 of 10

Client:Synagro Laboratory ID:WD22023-001
Description:Bladenboro WWTP Matrix: Solid
Date Sampled:04/20/2021 1030 %Solids: 1.33 04/24/2021 1436
Date Received:04/22/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 (%Solids)SM 2540G 1 04/24/2021 1436 AAB 90126
1 (Flashpoint() 1010B 1 04/26/2021 1239 KMC 90241
1 (Reactive Cya)7.3.3 1 04/26/2021 1758 KFE 04/23/2021 2131
1 (Reactive Sul)7.3.4 1 04/27/2021 2225 GDC 04/23/2021 2131
1 (Soil pH meas)9045D 1 04/26/2021 2209 NBW 90278
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
%Solids SM 2540G 1.33 % 2
Flashpoint(Pensky-Martens Closed-Cup) 1010B >140 140 0 ° F 1
Reactive Cyanide 7.3.3 ND 50 50 mg/kg 1
Reactive Sulfide 7.3.4 ND 50 50 mg/kg 1
Soil pH measured in water @ 18.8° C 9045D 6.9 su 1
TCLP Volatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/5030B 8260D 10 05/09/20211645 TML 91772 05/05/2021 2224
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Benzene 71-43-2 8260D ND H 0.050 0.0040 mg/L 1
2-Butanone(MEK) 78-93-3 8260D ND H 0.10 0.020 mg/L 1
Carbon tetrachloride 56-23-5 8260D ND H 0.050 0.0040 mg/L 1
Chlorobenzene 108-90-7 8260D ND H 0.050 0.0040 mg/L 1
Chloroform 67-66-3 8260D ND H 0.050 0.0040 mg/L 1
1,2-Dichloroethane 107-06-2 8260D ND H 0.050 0.0040 mg/L 1
1,1-Dichloroethene 75-35-4 8260D ND H 0.050 0.0040 mg/L 1
Tetrachloroethene 127-18-4 8260D ND H 0.050 0.0040 mg/L 1
Trichloroethene 79-01-6 8260D ND H 0.050 0.0040 mg/L 1
Vinyl chloride 75-01-4 8260D ND H 0.010 0.0040 mg/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Bromofluorobenzene H 101 70-130
1,2-Dichloroethane-d4 H 106 70-130
Toluene-d8 H 108 70-130
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 05/09/2021 0449 SCD 05/06/2021 1712 91446 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,4-Dichlorobenzene 106-46-7 8270E ND 0.040 0.0050 mg/L 1
2,4-Dinitrotoluene 121-14-2 8270E ND 0.080 0.0050 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 10

Client:Synagro Laboratory ID:WD22023-001
Description:Bladenboro WWTP Matrix: Solid
Date Sampled:04/20/2021 1030 %Solids: 1.33 04/24/2021 1436
Date Received:04/22/2021
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 05/09/2021 0449 SCD 05/06/2021 1712 91446 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachlorobenzene 118-74-1 8270E ND 0.040 0.0050 mg/L 1
Hexachlorobutadiene 87-68-3 8270E ND 0.040 0.0050 mg/L 1
Hexachloroethane 67-72-1 8270E ND 0.040 0.010 mg/L 1
2-Methylphenol 95-48-7 8270E ND 0.040 0.010 mg/L 1
3+4-Methylphenol 106-44-5 8270E ND 0.040 0.015 mg/L 1
Nitrobenzene 98-95-3 8270E ND 0.040 0.015 mg/L 1
Pentachlorophenol 87-86-5 8270E ND 0.20 0.020 mg/L 1
Pyridine 110-86-1 8270E ND 0.040 0.0050 mg/L 1
2,4,5-Trichlorophenol 95-95-4 8270E ND 0.040 0.0050 mg/L 1
2,4,6-Trichlorophenol 88-06-2 8270E ND 0.040 0.0050 mg/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
2-Fluorobiphenyl 84 37-129
2-Fluorophenol 50 24-127
Nitrobenzene-d5 79 38-127
Phenol-d5 73 28-128
Terphenyl-d14 78 10-148
2,4,6-Tribromophenol 66 41-144
TCLP Herbicides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/8151 A 8151A 1 05/06/2021 2107 JPB 05/06/2021 0041 91294 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2,4-D 94-75-7 8151A ND 0.020 0.0050 mg/L 1
2,4,5-TP(Silvex) 93-72-1 8151A ND 0.0050 0.0013 mg/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
DCAA 81 50-112
TCLP Pesticides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081B 1 05/07/2021 1633 DAL1 05/06/2021 1537 91422 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
gamma-BHC(Lindane) 58-89-9 8081B ND 0.00040 0.00017 mg/L 1
Chlordane 57-74-9 8081B ND 0.0040 0.0015 mg/L 1
Endrin 72-20-8 8081B ND 0.00040 0.00015 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 10

Client:Synagro Laboratory ID:WD22023-001
Description:Bladenboro WWTP Matrix: Solid
Date Sampled:04/20/2021 1030 %Solids: 1.33 04/24/2021 1436
Date Received:04/22/2021
TCLP Pesticides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081B 1 05/07/2021 1633 DAL1 05/06/2021 1537 91422 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Heptachlor 76-44-8 8081B ND 0.00040 0.00015 mg/L 1
Heptachlor epoxide 1024-57-3 8081B ND 0.00040 0.00016 mg/L 1
Methoxychlor 72-43-5 8081B ND 0.0016 0.00021 mg/L 1
Toxaphene 8001-35-2 8081B ND 0.0080 0.0030 mg/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Decachlorobiphenyl 82 20-131
Tetrachloro-m-xylene 97 26-132
TCLP Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3010A 6010D 1 05/05/2021 0733 KSH2 05/04/2021 2321 91152 05/03/2021 1721
1 1311/7470A 7470A 1 05/05/2021 1404 CMS2 05/05/2021 1100 91210 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Arsenic 7440-38-2 6010D ND 0.15 0.025 mg/L 1
Barium 7440-39-3 6010D 0.051 J 0.25 0.031 mg/L 1
Cadmium 7440-43-9 6010D ND 0.050 0.0060 mg/L 1
Chromium 7440-47-3 6010D ND 0.10 0.013 mg/L 1
Lead 7439-92-1 6010D ND 0.10 0.047 mg/L 1
Mercury 7439-97-6 7470A ND 0.0020 0.00091 mg/L 1
Selenium 7782-49-2 6010D ND 0.20 0.085 mg/L 1
Silver 7440-22-4 6010D ND 0.10 0.021 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 10

Client:Synagro Laboratory ID:WD22023-002
Description:Bladenboro WWTP Matrix: Solid
Date Sampled:04/20/2021 1030 %Solids: 0.924 04/24/2021 1436
Date Received:04/22/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 (%Solids)SM 2540G 1 04/24/2021 1436 AAB 90126
1 350.1 (Ammonia-N)350.1 2 04/26/2021 1408 DRD 90225
3 (Nitrate-N)9056A 1 04/30/2021 1202 AMR 90829
1 (Nitrite-N)9056A 1 04/28/2021 1221 AMR 90631
1 (Phosphorus)365.1 10 04/26/2021 1446 DMA 04/24/2021 1139 90119
1 (Soil pH meas)9045D 1 04/26/2021 2210 NBW 90278
1 351.4 (TKN)351.2 1 04/26/2021 1318 DMA 04/24/2021 1116 90116
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
%Solids SM 2540G 0.924 % 2
Ammonia-N (gas diffusion) 350.1 9000 S 220 110 mg/kg 1
Nitrate-N (soluble) 9056A 160 54 11 mg/kg 3
Nitrite-N (soluble) 9056A 34 22 11 mg/kg 1
Phosphorus 7723-14-0 365.1 25000 S 5400 1100 mg/kg 1
Soil pH measured in water @ 18.7° C 9045D 6.9 su 1
TKN 351.2 51000 2700 2700 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 04/30/2021 1520 CMS2 04/30/2021 1104 90505
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 7.9 1.9 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/23/2021 1943 KSH2 04/23/2021 0253 89959
2 3050B 6010D 1 04/23/2021 1206 KSH2 04/23/2021 0253 89959
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 22000 720 270 mg/kg 1
Arsenic 7440-38-2 6010D 11 J 27 9.0 mg/kg 1
Cadmium 7440-43-9 6010D 3.4 J 9.0 2.3 mg/kg 1
Calcium 7440-70-2 6010D 25000 9000 1100 mg/kg 1
Chromium 7440-47-3 6010D 57 18 4.5 mg/kg 1
Copper 7440-50-8 6010D 700 18 8.1 mg/kg 1
Iron 7439-89-6 6010D 34000 180 82 mg/kg 2
Lead 7439-92-1 6010D 48 18 8.1 mg/kg 1
Magnesium 7439-95-4 6010D 3500 J 9000 1100 mg/kg 1
Manganese 7439-96-5 6010D 250 27 11 mg/kg 1
Molybdenum 7439-98-7 6010D ND 72 18 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 10

Client:Synagro Laboratory ID:WD22023-002
Description:Bladenboro WWTP Matrix: Solid
Date Sampled:04/20/2021 1030 %Solids: 0.924 04/24/2021 1436
Date Received:04/22/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/23/2021 1943 KSH2 04/23/2021 0253 89959
2 3050B 6010D 1 04/23/2021 1206 KSH2 04/23/2021 0253 89959
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Nickel 7440-02-0 6010D 38 J 72 19 mg/kg 1
Potassium 7440-09-7 6010D 6500 J 9000 1100 mg/kg 1
Selenium 7782-49-2 6010D ND 36 15 mg/kg 1
Sodium 7440-23-5 6010D 2900 J 9000 1100 mg/kg 1
Zinc 7440-66-6 6010D 1200 90 22 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 8 of 10

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
Samples Rec iptCheeklat15RC1lMEC01rC-Z5J Revi5ed:9129/2020
CeAr..4.t '3J Issuing.4Jth oil ty:Pare ENV• 'A+col Page 1 f 1!
Sample Receipt Checklist (SRC}
Client: 5Y NAGRO Coofe inspe4ced b. /dam: Mr.N r l 3n V2D2,t I-0I if; R'l)-L..t:'=
4e4i01_5OfreCeipl- El face Client ,f L;I'S FedEx Catxm
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MENIMER0 NA '. I f custody Seals were present.WCrh;tile)...hitact and I_InlJ oken?
11 pH `a trip ID: " _ C liorine Strip la "ATYs[Cd by:^a — 1
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''ts I�No 7. Were sample IDs]isied are 11 sample con taineis'�
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1?cT j No I I. WerG.tests to Esc peh 'armed listed on the COC'
El YeS ❑h`la 12-Did ail sartp]cs arrive itt thir prlaperr ontaijien5 for each test anclior in goal cnrtdi==cln
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LI Yot No l5-Were at s-ertpies euntuirtersmiss[ngr'exce s(eircle mete)samples Not lisre4on COC?
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 10 of 10

SECTION 3

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SECTION 4

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Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Nate Roth
Project Name: Bladenboro
Lot Number:WD22023
Date Completed:05/11/2021
—
05/11/2021 11:04 AM
Approved and released by:
Project Manager II: Lucas Odom
MILB
Q PCCR�c��
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDe0_RAt°,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WD22023
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low% solid the initial amount of sample -002 was 3 times the standard procedure amount per
PM's request. The LOQ has been adjusted accordingly.
TCLP VOCs
The following sample was analyzed outside of analytical holding time: WD22023-001. This sample was
over-looked when loading based off of holding-times.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2 of 10

Client:Synagro Laboratory ID:WD22023-001
Description:Bladenboro WWTP Matrix:Solid
Date Sampled:04/20/2021 1030 % Solids: 1.33 04/24/2021 1436
Date Received:04/22/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 (% Solids)SM 2540G 1 04/24/2021 1436 AAB 90126
1 (Flashpoint() 1010B 1 04/26/2021 1239 KMC 90241
1 (Reactive Cya)7.3.3 1 04/26/2021 1758 KFE 04/23/2021 2131
1 (Reactive Sul)7.3.4 1 04/27/2021 2225 GDC 04/23/2021 2131
1 (Soil pH meas)9045D 1 04/26/2021 2209 NBW 90278
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Solids SM 2540G 1.33 % 2
Flashpoint(Pensky-Martens Closed-Cup) 1010B >140 140 0 °F 1
Reactive Cyanide 7.3.3 ND 50 50 mg/kg 1
Reactive Sulfide 7.3.4 ND 50 50 mg/kg 1
Soil pH measured in water @ 18.8° C 9045D 6.9 su 1
TCLP Volatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/5030B 8260D 10 05/09/2021 1645 TML 91772 05/05/20212224
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Benzene 71-43-2 8260D ND H 0.050 0.0040 mg/L 1
2-Butanone(MEK) 78-93-3 8260D ND H 0.10 0.020 mg/L 1
Carbon tetrachloride 56-23-5 8260D ND H 0.050 0.0040 mg/L 1
Chlorobenzene 108-90-7 8260D ND H 0.050 0.0040 mg/L 1
Chloroform 67-66-3 8260D ND H 0.050 0.0040 mg/L 1
1,2-Dichloroethane 107-06-2 8260D ND H 0.050 0.0040 mg/L 1
1,1-Dichloroethene 75-35-4 8260D ND H 0.050 0.0040 mg/L 1
Tetrachloroethene 127-18-4 8260D ND H 0.050 0.0040 mg/L 1
Trichloroethene 79-01-6 8260D ND H 0.050 0.0040 mg/L 1
Vinyl chloride 75-01-4 8260D ND H 0.010 0.0040 mg/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Bromofluorobenzene H 101 70-130
1,2-Dichloroethane-d4 H 106 70-130
Toluene-d8 H 108 70-130
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 05/09/2021 0449 SCD 05/06/2021 1712 91446 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
1,4-Dichlorobenzene 106-46-7 8270E ND 0.040 0.0050 mg/L 1
2,4-Dinitrotoluene 121-14-2 8270E ND 0.080 0.0050 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 10

Client:Synagro Laboratory ID:WD22023-001
Description:Bladenboro WWTP Matrix:Solid
Date Sampled:04/20/2021 1030 % Solids: 1.33 04/24/2021 1436
Date Received:04/22/2021
TCLP Semivolatiles
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 05/09/2021 0449 SCD 05/06/2021 1712 91446 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachlorobenzene 118-74-1 8270E ND 0.040 0.0050 mg/L 1
Hexachlorobutadiene 87-68-3 8270E ND 0.040 0.0050 mg/L 1
Hexachloroethane 67-72-1 8270E ND 0.040 0.010 mg/L 1
2-Methylphenol 95-48-7 8270E ND 0.040 0.010 mg/L 1
3+4-Methylphenol 106-44-5 8270E ND 0.040 0.015 mg/L 1
Nitrobenzene 98-95-3 8270E ND 0.040 0.015 mg/L 1
Pentachlorophenol 87-86-5 8270E ND 0.20 0.020 mg/L 1
Pyridine 110-86-1 8270E ND 0.040 0.0050 mg/L 1
2,4,5-Trichlorophenol 95-95-4 8270E ND 0.040 0.0050 mg/L 1
2,4,6-Trichlorophenol 88-06-2 8270E ND 0.040 0.0050 mg/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 84 37-129
2-Fluorophenol 50 24-127
Nitrobenzene-d5 79 38-127
Phenol-d5 73 28-128
Terphenyl-d14 78 10-148
2,4,6-Tribromophenol 66 41-144
TCLP Herbicides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/8151A 8151A 1 05/06/20212107 JPB 05/06/2021 0041 91294 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
2,4-D 94-75-7 8151A ND 0.020 0.0050 mg/L 1
2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 0.0013 mg/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
DCAA 81 50-112
TCLP Pesticides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081B 1 05/07/2021 1633 DAL1 05/06/2021 1537 91422 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
gamma-BHC(Lindane) 58-89-9 8081B ND 0.00040 0.00017 mg/L 1
Chlordane 57-74-9 8081B ND 0.0040 0.0015 mg/L 1
Endrin 72-20-8 8081B ND 0.00040 0.00015 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 10

Client:Synagro Laboratory ID:WD22023-001
Description:Bladenboro WWTP Matrix:Solid
Date Sampled:04/20/2021 1030 % Solids: 1.33 04/24/2021 1436
Date Received:04/22/2021
TCLP Pesticides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081E 1 05/07/2021 1633 DAL1 05/06/2021 1537 91422 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Heptachlor 76-44-8 8081E ND 0.00040 0.00015 mg/L 1
Heptachlor epoxide 1024-57-3 808113 ND 0.00040 0.00016 mg/L 1
Methoxychlor 72-43-5 8081E ND 0.0016 0.00021 mg/L 1
Toxaphene 8001-35-2 8081E ND 0.0080 0.0030 mg/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl 82 20-131
Tetrachloro-m-xylene 97 26-132
TCLP Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3010A 6010D 1 05/05/2021 0733 KSH2 05/04/2021 2321 91152 05/03/2021 1721
1 1311/7470A 7470A 1 05/05/2021 1404 CMS2 05/05/2021 1100 91210 05/03/2021 1721
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Arsenic 7440-38-2 6010D ND 0.15 0.025 mg/L 1
Barium 7440-39-3 6010D 0.051 J 0.25 0.031 mg/L 1
Cadmium 7440-43-9 6010D ND 0.050 0.0060 mg/L 1
Chromium 7440-47-3 6010D ND 0.10 0.013 mg/L 1
Lead 7439-92-1 6010D ND 0.10 0.047 mg/L 1
Mercury 7439-97-6 7470A ND 0.0020 0.00091 mg/L 1
Selenium 7782-49-2 6010D ND 0.20 0.085 mg/L 1
Silver 7440-22-4 6010D ND 0.10 0.021 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 10

Client:Synagro Laboratory ID:WD22023-002
Description:Bladenboro WWTP Matrix:Solid
Date Sampled:04/20/2021 1030 % Solids: 0.924 04/24/2021 1436
Date Received:04/22/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 (% Solids)SM 2540G 1 04/24/2021 1436 AAB 90126
1 350.1 (Ammonia-N )350.1 2 04/26/2021 1408 DRD 90225
3 (Nitrate-N )9056A 1 04/30/2021 1202 AMR 90829
1 (Nitrite-N )9056A 1 04/28/2021 1221 AMR 90631
1 (Phosphorus)365.1 10 04/26/2021 1446 DMA 04/24/2021 1139 90119
1 (Soil pH meas)9045D 1 04/26/2021 2210 NBW 90278
1 351.4 (TKN)351.2 1 04/26/2021 1318 DMA 04/24/2021 1116 90116
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Solids SM 2540G 0.924 % 2
Ammonia-N (gas diffusion) 350.1 9000 S 220 110 mg/kg 1
Nitrate-N (soluble) 9056A 160 54 11 mg/kg 3
Nitrite-N (soluble) 9056A 34 22 11 mg/kg 1
Phosphorus 7723-14-0 365.1 25000 S 5400 1100 mg/kg 1
Soil pH measured in water @ 18.7° C 9045D 6.9 su 1
TKN 351.2 51000 2700 2700 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 04/30/2021 1520 CMS2 04/30/2021 1104 90505
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 7.9 1.9 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/23/2021 1943 KSH2 04/23/2021 0253 89959
2 3050B 6010D 1 04/23/2021 1206 KSH2 04/23/2021 0253 89959
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 22000 720 270 mg/kg 1
Arsenic 7440-38-2 6010D 11 J 27 9.0 mg/kg 1
Cadmium 7440-43-9 6010D 3.4 J 9.0 2.3 mg/kg 1
Calcium 7440-70-2 6010D 25000 9000 1100 mg/kg 1
Chromium 7440-47-3 6010D 57 18 4.5 mg/kg 1
Copper 7440-50-8 6010D 700 18 8.1 mg/kg 1
Iron 7439-89-6 6010D 34000 180 82 mg/kg 2
Lead 7439-92-1 6010D 48 18 8.1 mg/kg 1
Magnesium 7439-95-4 6010D 3500 J 9000 1100 mg/kg 1
Manganese 7439-96-5 6010D 250 27 11 mg/kg 1
Molybdenum 7439-98-7 6010D ND 72 18 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 10

Client:Synagro Laboratory ID:WD22023-002
Description:Bladenboro WWTP Matrix:Solid
Date Sampled:04/20/2021 1030 % Solids: 0.924 04/24/2021 1436
Date Received:04/22/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050E 6010D 1 04/23/2021 1943 KSH2 04/23/2021 0253 89959
2 3050E 6010D 1 04/23/2021 1206 KSH2 04/23/2021 0253 89959
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Nickel 7440-02-0 6010D 38 J 72 19 mg/kg 1
Potassium 7440-09-7 6010D 6500 J 9000 1100 mg/kg 1
Selenium 7782-49-2 6010D ND 36 15 mg/kg 1
Sodium 7440-23-5 6010D 2900 J 9000 1100 mg/kg 1
Zinc 7440-66-6 6010D 1200 90 22 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 8 of 10

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106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
Samples Receipt Cheeklat 15 1 iiviEo01$C-15J RQvi5ed:9/29/2020
Ceksf.:Tical Issuing.+:Itharily:Pare ENV• 'NCOL Page 1 of 1
!
Sample Receipt Checklist (SRC)
Ciicrtt: 5YNAGR 4 , Mp.N r 04/22+2D2.E 41'I?2ZL'23
r►Irler ln.pe4oed a? ,dsFe; I.0#f;
^
4ex?>_sofreceipt: El race Client ,f L;fS Fe.lEx Chu:
.m IL No I1. Were t:ustody seals present on the cooler? .
VIM NL J NAP. If custody stalls were presort,were tiler hrtact and I n.laroken? _
l] `'tri ID: "� Ill: R nA
R p — . __ C:rlurine Strip TYstcd by!
0rigina]tenaperautlre upon receipt 1 Derived(C;oarectoti)temperature upon receipt %Solid Snap-Cup Ili: 21'443
19 .04.9 ',c F . /NA eC NA iNA o-- NA t+tA ac
4ethot•QTtvnperature Blank E [ant Bottles ER Gun ID_ 6 IR Gin Correction Factor: 111 'C
Method ofcoolar.t, ❑ Wet Ice 0 Ice Recker ty] Mime _
Ecs - It temperature of any cooler exceexitdaG.0cC,was]'-eject ManagerNotifiad?
! 1'M was Notified by.: phone.'ernai]i face-tc-fave(circle one)_
• 11 ' 1 CGS ElNn AIA.L, IS E11LI cc]m rcin;Courier's pacing slip I-ac tied to•LI-Li Fonn7
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�Yes' DNO 5. Wer4 proper custody procedures(re tinquisl-tc ,'reoived)folhow d?
M Yes U Na C.. W rG sample IDs Iisted to t}lo.COC?
'ts IE No 7. Were sample IDs listed are all sample containers')
L
12 Yes NO S. Was col lecdon date&time listed on Ile COC4
0 Yes LiNo V. War collection dale rt Ire listed on all sample con[dinars? •
•
. 7 11 Yes i No 10. Did all ca,nrainer label inform:Won(ID,date.tine)awes•with thu COC? —
1 Yt j No I I. Wero tests to Ese NJ-formed listed on the CDC'}
El YeS ❑h`la I2_Did all sar.tp]cs arrive iu the properr ontautier for:ach test anclior in goad coldi_'on
(Unbroken,lids on,Ne_)? _
'Yes Nol 13, Was integrate sarnplo volutie avai[ah1e?
J Yes No H. Were PHsaonplew w received .h in LFL C R holding time or hours,w h ichever corraes first?
L I Y LT.GLI No 15_Were any s-.m,pies euntuiaars tnissingr'exc s(eir+c Ie cane)samples Not hued on COC?
•!7 n No �N.q ]6. For VOA aiid RSK-l75 samples, wero bubbles present>`•pca-size"(V or 6 rrnn l D diarneLT)
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i J tics LI N4 ✓ NA is.VI/LTC all cyan=de sresect!plus race iveil at a pH` 12 and Sulfide srhmples received at a rFt -9?
1 1ias, LE7wu J NA 19. Were all applicab:s N]];fl•'] Cystnideipheflo1i60S.3(<b rrig L)sam et of
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❑ I �—r 20. Were them remar[csfrcc]uests(i.e.letliieited dilutions,JvlS/MSD destgnH ions,etc,._.)
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I _ oon-ettIy transcribed from the COC into the aotaMtent scctinn In LI MS?
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rime I f preservation NA. - ({'more than one preservative:.S.seeded,please nolxt in the comtnenrs below,
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'amplus(s) NA • were received with I RC> 1
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 10 of 10

SECTION 5

ANNUAL PATHOGEN AND VECTOR A I IRACTTON REDUCTION FORM(02T Rules)
Facility Name: Town of Bladenboro WQ Permit Number. W 0014452
WWTP Name: Bladenboro WWTP NPDES Number. NC0026352
Monitoring Period: From 01/01/2021 To 12/31/2021
Pathogen Reduction(40 CFR 503.32/15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A(time/temp) Alt.2/B(Alk Treatment) Alt.3/C(Prior Testing)
Alt.4/D(No Prior Test) Alt.5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density X Alt.(2)Process to Significantly Reduce Pathogens
If applicable to alternative perfonned(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo.Mean Maximum Units dences Analysis
Fecal 2x10 to the 6th MPN MPN/g
Coliform power per gram
of total solids
CFU 27500 72200 176000 CFU/g 0 Annually Grab 9222D-
MF
1000 MPN per gram of MPN/g
total solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
coliform 1 1
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative perfonned:
Option/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) X (40-day bench) (30-day bench) (Spec.02 uptake)
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization) (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33715A NCAC 02T.1107 have been met."
"I certify,under penalty of law that the athogeen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33//15A NCAC 02T.1107 have not been met."(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Clint Ward.Waste Water ORC
Prep N e d ' e(type or print) Land Applier Name and Title(if applicable)(type or print)
OIL JZ-ly-zr'
Signature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)

Cameron Testing Services, Inc. Laboratory Report NC 54
NC PHHS#37737799
US EPA#NC01918
C� Synagro OQ], n 2104-165 DW Cert#37799
Bladenboro Or V Yes
Sample Information
' Om N. Roth = hats 4 04/20/21 re 3 J. Cameron 90t0 04/20/21
Analyses and Results
ra. ' Std.Methods
Lab ID Sample ID Analyte Result a E CI Reference
2104-165 -01 3Eudge Gr Fec.Coliform-S <31800 CFUrg 31800 04/20/21 RL 9222D-MF
-02 <32400 CFUrg 32400
-03 <27500 CFU/g 27500
-04 <176000 CFU/g 176000
-05 <B8800 CFU/g 68800
-06 <172000 CFU/g 172000
-07 <174000 Mfg 174000
Geomean <72200
2104-165 01 -01 sludge Gr TS(%) 3.14% 001 04/20/21 RL 2540 G-TS
-02 3.09% 001
-03 3.63% 001
-04 0.570% 0.01
-05 1.45% 0.01
-06 0.583% 0.01
-07 0.576% 0.01
Report
Review Q 7 1) //
Lab Director Date
219 S.Steele Str, 919-208-4240
Sanford NC 27330 [e-mail]

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SECTION 6

Agricultural Lime Application Log
Year 2021
Project Bladenboro
Fields Soil Lime Requirements Tons/Acre Date
(state-county-site-field) PH (from soil analysis) Applied Applied
BL-3-4 5.9 0 n/a n/a
*N/A pH value was at or above 6.0/Did not require lime

SECTION 7

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