WQ0000543_Residual Annual Report 2021_20220224

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0000543
Applicant/Permittee City of Sanford
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office Raleigh
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Lysa Finnerty
Email Address* Phone Number*
[e-mail] 14105376150
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0000543
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court,Ste 100,Baltimore MD 21220
Facility Name* City of Sanford Class B Residuals Program
Please provide comments/notes on your current submittal below.
2021 Annual Report for City of Sanford,NC
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
Sanford NC 2021 Annual Report FINAL.pdf 31.59MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature Lp
Ja TM/WO
Submission Date 2/24/2022

435 Williams Court,Suite 100
Baltimore,MD 21220 SYNAG R
www.synagro.com
FEBRUARY 24,2022
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2021 Annual Report for Permit No.WQ0000543
Dear NCDEQ:
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Sanford, NC.
If you have any questions or need additional information,please do not hesitate to contact Scott
Siletzky at(919) 775-8305 or Chris Wynne at(336) 909-8627.
Sincerely,
l e't ic& Sfiiva'c 25
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Chris Wynne, Synagro
Scott Siletzky, City of Sanford
YOUR PARTNER FORA CLEANER,GREENER WORLD

CITY OF SANFORD
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0000543
2021 ANNUAL REPORT

City of Sanford, NC
Residuals Land Application Program
2021 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00000543 County Lee Year 2021
Facility Name(as shown on permit)City of Sanford WWTP NPDES No.NC0024147
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO,skip Part A,and Part B and proceed to Part C. Also,if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A—Residuals Application Summary:
Total number of application fields in the permit: 43
Total number of fields utilized for land application during the year: 23
Total amount of dry tons applied during the year for all application sites: 933.71
Total number of acres utilized for land application during the year: 422.03
Part B—Annual Compliance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit(including but not limited to items
1-13 below)issued by the Division of Water Quality X YES NO.
If no,please provide a written description why the facility was not compliant,the dates,and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three(3)copies of
laboratory results are attached.
4. Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1105(a)or the Pollutant Loading
Rates in 15A NCAC 02T.1105(b)(Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or,in the case of a deviation,prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals,as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C—Certification:
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate,and complete. I
am aware that there are significant penalties for submitting false info :tion,including the possibility of fines and imprisonment for
knowing violations."
Hal Hegwer,Public City Manager ! SW --
Permittee Name and Title(type or print) Signa'i re of P. i ee Date
��. 2/9/2022
Signature of Preparer* Date Sig:4 e of Land s plier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T.1102(26) DENR FORM ACF(12/2006)

OPERATIONS SUMMARY-LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES -ALL SITES
DATE RANGE: 1/1/2021 - 11/16/2021
SANFORD,NC
SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG. LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
January 2021 471,200.00 G 100.80 D 91.43
April 2021 1,550,000.00 G 262.90 D 238.45
May 2021 415,400.00 G 48.85 D 44.31
June 2021 446,400.00 G 52.49 D 47.61
July 2021 688,200.00 G 88.04 D 79.86
August2021 1,190,400.00 G 171.75 D 155.78
September 2021 496,000.00 G 71.56 D 64.91
October 2021 620,000.00 G 72.65 D 65.89
November 2021 551,800.00 G 64.66 D 58.65
TOTAL 6,429,400.00 G 933.71 D 846.87
Units Key: D-Dry Tons; G—Gallons;W—Wet Tons;Y—Cubic Yards
Report Date: 1/28/2022 10:22:56 AM

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed.The parameters can be reported in FORM RSSF-B
WQ Permit Number: WQ0000543 Laboratory:
Facility Name: SANFORD,NC PACE ANALYTICAL
Residual Source WQ#or
NPDES#: NC0024147
WWTP Name: BUFFALO CREEK WWTP
Residual Analysis Data
Product Type AEDLIQ AEDLIQ AEDLIQ AEDLIQ
Sample or Composite Date 01/05/21 04/05/21 07/14/21 10/05/21
Parameter(mg/kg dry weight) Ceiling Conc.
Limit
Percent Solids(%) NA 5.13 2.82 3.46 2.81
Arsenic 75 3.9 9.2 8.6 7.7
Cadmium 85 0.74 2.2 2 2.4
Copper 4300 190 540 420 540
Chromium NA 41 100 60 61
Lead 840 15 37 29 31
Mercury 57 <0.35 0.88 <0.56 <0.67
Molybdenum 75 8.7 22 18 22
Nickel 420 23 62 39 48
Selenium 100 3.5 5.3 7.6 9.8
Zinc 7500 490 1300 1000 1300
Total Phosphorus NA 14000 36000 34000 50000
TKN NA 33000 87000 96000 72000
Ammonia-Nitrogen NA 7600 20000 20000 14000
Nitrate and Nitrite NA 82 69 178.7 590
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable.Reference the individual permit for metals limits.
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the
possibility of fines and imprisonment for knowing violations."
- ' 4- sz)cslla.cia<9.,..
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15 A NCAC 2T.1102(26) DENR FORM RSSF(12/2006)
Printed:1/26/2022 3:33:59 PM For:2039 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM -B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0000543 Laboratory:
Facility Name: SANFORD,NC PACE ANALYTICAL
Residual Source
NPDES#or WQ#: NC0024147
WWTP Name: BUFFALO CREEK WWTP
Residual Analysis Data
Product Type AEDLIQ AEDLIQ AEDLIQ AEDLIQ
Sample or Composite Date 01/05/21 04/05/21 07/14/21 10/05/21
Parameters(mg/kg dry weight)
Aluminium 8400 22000 19000 24000
Calcium 8300 23000 19000 24000
Magnesium 2800 6900 7800 9400
pH(s.u.) 7.50 6.90 7.10 7.20
Potassium 3800 9200 11000 11000
Sodium 1400 2600 2900 3400
PAN 11502 30169 32979 24990
SAR(Ratio) 0.7657 0.6464 0.8292 0.7869
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted.I am aware that there are significant penalties for submitting false information,including the
possibility of fines and imprisonment for knowing violations."
.:::: eisi-61--A ' alocil b,.a.g._
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15 A NCAC 2T.1102(26)
Printed:2/4/2022 4:21:15 PM For:2039 01 DENR FORM RSSF-B(12/2006)

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Sanford VWVTP
Lot Number:WA06023
Date Completed:01/26/2021
01/26/2021 11:21 AM
Approved and released by:
Project Manager II: Lucas Odom
MILB
Q PCCR�c��
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDeORA16,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WA06023
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
TKN
Reduced volume was used for samples due to sludge matrix.
Phosphorus
The method blank for analytical batch 80524 contained the analyte total phosphorus greater than the
method acceptance criteria. The associated sample contained detections for this analyte at
concentrations greater than 10X the value found in the method blank; therefore sample results are not
impacted. The data has been reported.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WA06023-001
Description:Sanford WWTP Matrix:Solid
Date Sampled:01/05/2021 1300 % Solids: 5.13 01/07/2021 0115
Date Received:01/06/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (% Solids)SM 2540G 1 01/07/2021 0115 MOM 78694
1 350.1 (Ammonia-N )350.1 10 01/08/2021 1034 DRD 78739
1 (Nitrate-N )9056A 1 01/08/2021 1542 AMR 79020
1 (Nitrite-N )9056A 1 01/08/2021 1542 AMR 79022
3 (Phosphorus)365.1 20 01/22/2021 1530 DMA 01/13/2021 2032 79352
1 (Soil pH meas)9045D 1 01/08/2021 2154 AAB 78948
3 351.4 (TKN)351.2 2 01/21/2021 1222 DMA 01/19/2021 1952 79979
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
% Solids SM 2540G 5.13 % 1
Ammonia-N (gas diffusion) 350.1 7600 190 100 mg/kg 1
Nitrate-N (soluble) 9056A 57 9.7 1.9 mg/kg 1
Nitrite-N (soluble) 9056A 25 3.9 1.9 mg/kg 1
Phosphorus 7723-14-0 365.1 14000 1900 390 mg/kg 3
Soil pH measured in water @ 18°C 9045D 7.5 su 1
TKN 351.2 33000 970 970 mg/kg 3
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/07/2021 0903 JAB2 01/07/2021 0614 78704
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 1.4 0.35 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/13/2021 1356 KSH2 01/11/2021 0946 78716
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 8400 130 48 mg/kg 1
Arsenic 7440-38-2 6010D 3.9 J 4.8 1.6 mg/kg 1
Cadmium 7440-43-9 6010D 0.74 J 1.6 0.40 mg/kg 1
Calcium 7440-70-2 6010D 8300 1600 200 mg/kg 1
Chromium 7440-47-3 6010D 41 3.2 0.80 mg/kg 1
Copper 7440-50-8 6010D 190 3.2 1.4 mg/kg 1
Iron 7439-89-6 6010D 11000 32 15 mg/kg 1
Lead 7439-92-1 6010D 15 3.2 1.4 mg/kg 1
Magnesium 7439-95-4 6010D 2800 1600 200 mg/kg 1
Manganese 7439-96-5 6010D 740 4.8 1.9 mg/kg 1
Molybdenum 7439-98-7 6010D 8.7 J 13 3.2 mg/kg 1
Nickel 7440-02-0 6010D 23 13 3.4 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3of7

Client:Synagro Laboratory ID:WA06023-001
Description:Sanford WWTP Matrix:Solid
Date Sampled:01/05/2021 1300 % Solids: 5.13 01/07/2021 0115
Date Received:01/06/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/13/2021 1356 KSH2 01/11/2021 0946 78716
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Potassium 7440-09-7 6010D 3800 1600 200 mg/kg 1
Selenium 7782-49-2 6010D 3.5 J 6.4 2.6 mg/kg 1
Sodium 7440-23-5 6010D 1400 J 1600 200 mg/kg 1
Zinc 7440-66-6 6010D 490 16 4.0 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4of7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

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Shealy Environr•nen12il Servrine.s, Inc,
N Chain Of Custody Record �'D Vantage POdnl �iir
s West Columbia; South Carolina?f8172 Number
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PACE ANALYTICAL SERVICES, LLC
SamplasReceipt Cher-Mist(SRC){ME13013C•1S1 I S !9/29f2020
/.- .r7 1 ;l1)cat' Iss-drq Authority:Pace EN tiV- :0I. I I, f I ?:
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Sample Receipt Ch .c list S C) fi4O6023
Ci;Jlt: Cooler:inspected uyjlaLa: r % k3 _ Lot .�,ia
:Vic-zits errs race [:.ien1 L'P5 Fedi:LK Oi]ur:
Yes_; :N 1. WeCe Cklgocty sval,s re;e it on the cooler?
•LiYO, ❑N a rINA 2_ If ci: tndy srstla were paeseiIL,wrrc they intact=4 lu.6rokw,9
pH Strip lD: 7 Clalori_ia Strip 117_ i ted by: Ir- -
r rnlal tp pera y6re'upt rcr i.pt Kivill&l:rorreir.Cte.in e,ature upon receipt %Solid Snap-Cup ID; T.
i4$et ioc©'Temperature§Lainik Hergiin t Bottles. JR Cron IL): IR Gun CL]r rtz.1 ion Var:tor'
Method o_f coolant; Li-Wet Teo Er Ice Packs El .Cry Ice None
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Y o 5_ Word propea cnslrady 1xx�c dt res(relirtq'xiaficdr5cceik d)lollowo�?
y -- Li No t. Ware sample lDs Iislrxlon the COC?
•
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. es II No 7. Ware sam r iC IDS IfSI eel oil all sample cor ain�r7a ;I
i 'Cs L R. Was cal_ecd on_1aiii&time listed on tine CSC?
Y-s, n 9. Was cal:cm-icn date&thin.L ted ail ill yamPJc`colltainei_,?
EI Yes: F.T.To 10,Did all container lahel information.(ID,date,time)agree wit]the COC?
., es I NO II.Were tests to be performed listed cm the COC? _
Kees e ❑I n 12-Did u31 a�Lmplca arTive in rhis pr a„iuiners for each test and/cr in good condition
(unbroken. Iidi un,ate.)?
is No_13.Was adequate sartnpJ$volume avai:ab[o7
[Yes IN N, 14, Weae all samples r:ccived within the holding time or 4E hours,whichever conies first?
f Yes C1 1tiU 15. Were ery Rarnples containers rnisainVexcess(circle one)samples Not listed on COC?
16. For VOA and 1. :c-E7 samples,were bubbles pr seiit ca-s:ze'{'f,"or 6mm at diameter)
�]Y ❑TTo r`I A .to 9t.-1y of the VOA vials?
■ Yes No •_"A 17. Were all CRGlmctals!riuLrierA:tm]ples received n1 a pH of<2?
Yes El No E_ A ls. Were all cyanide sailrplcs received at- a pH_> 12 am:blade.Sun:talcs received at a pH 9'?
Yes El No �A 19.Were al'applicable N k TKN.?rvani d°hTp; aciG' a,il6U _= (<O.5m.grZ)samples Crest of
res'. le chloi e?
❑Yes ❑NLr A 20. Were Client reriarksfrr,]rests(i.e_requested dihruoris,NIS/MSD designations,etc.._)
conreeny transcribed from 1he COC into Cie comment section in LIM ? _
loin G•NoIIIM 21_ Was t3�c quote number listed on tt a r...p tgiflcr lane l?1f yes, ote it
ample PrE i 'p ation (1.lust be compicted for any sample(s) incuinel ly preserved N.with head,p .j
Sample(s) - iwcro re-eoved incorrectly preserved rt(rwcro adjusted eicoantritigi.y
.in sample receiving t ith rtiL of ciru]c one: 1.12504,TINO;,HCl,NaOki using SR rr
Titufi of preservation _ l f more than one preservative is needed,please note in the comment.:blow~.
S2.r P]e(s) _�. —
vibe receiiiod with bubbles>b men:il io ctcr,
5amplcs(s) fV, wcre rece;,...i.wit:,TH.c-,o.-5 mg/L(4019isno)andv,ere
,adjusted accordingiy ii sample recelyng with sodium LJhiosulfa ( Iu2St0;)with Sienjy ID; 7 J— ,
5lt'oa-eocle labels applirxi by: — . ..1
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Comments;;
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Sanford VWVTP
Lot Number:WD08037
Date Completed:04/19/2021
04/19/2021 3:20 PM
Approved and released by:
Project Manager II: Lucas Odom
MILB
Q PCCR�c��
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDeORA16,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WD08037
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low percent solids, sample-001 has been digested using three grams of sample. The LOQs have
been changed to reflect the additional disestion mass.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WD08037-001
Description:Sanford WWTP Matrix: Solid
Date Sampled:04/05/2021 1330 %Solids: 2.82 04/09/2021 0019
Date Received:04/08/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (%Solids)SM 2540G 1 04/09/2021 0019 MOM 88462
1 350.1 (Ammonia-N)350.1 20 04/13/2021 1504 KFE 88830
1 (Nitrate-N)9056A 1 04/13/2021 1117 AMR 88909
1 (Nitrite-N)9056A 1 04/13/2021 1117 AMR 88910
2 (Phosphorus)365.1 25 04/13/2021 1544 DMA 04/10/2021 1429 88601
1 (Soil pH meas)9045D 1 04/09/2021 1256 NBW 88539
1 351.4 (TKN)351.2 2 04/15/2021 1006 DMA 04/10/2021 1429 88598
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
%Solids SM 2540G 2.82 % 1
Ammonia-N (gas diffusion) 350.1 20000 710 370 mg/kg 1
Nitrate-N (soluble) 9056A 43 18 3.6 mg/kg 1
Nitrite-N (soluble) 9056A 26 S 7.1 3.6 mg/kg 1
Phosphorus 7723-14-0 365.1 36000 4400 890 mg/kg 2
Soil pH measured in water @ 20.4° C 9045D 6.9 su 1
TKN 351.2 87000 1800 1800 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 04/14/2021 1514 CMS2 04/14/2021 1203 88719
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B 0.88 J 2.9 0.69 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/10/2021 1435 KSH2 04/09/2021 0845 88488
2 3050B 6010D 1 04/12/2021 1138 KSH2 04/09/2021 0845 88488
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 22000 230 87 mg/kg 1
Arsenic 7440-38-2 6010D 9.2 8.7 2.9 mg/kg 1
Cadmium 7440-43-9 6010D 2.2 J 2.9 0.73 mg/kg 1
Calcium 7440-70-2 6010D 23000 2900 360 mg/kg 1
Chromium 7440-47-3 6010D 100 5.8 1.4 mg/kg 1
Copper 7440-50-8 6010D 540 5.8 2.6 mg/kg 1
Iron 7439-89-6 6010D 34000 58 26 mg/kg 2
Lead 7439-92-1 6010D 37 5.8 2.6 mg/kg 1
Magnesium 7439-95-4 6010D 6900 2900 360 mg/kg 1
Manganese 7439-96-5 6010D 2100 8.7 3.4 mg/kg 1
Molybdenum 7439-98-7 6010D 22 J 23 5.8 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:WD08037-001
Description:Sanford WWTP Matrix: Solid
Date Sampled:04/05/2021 1330 %Solids: 2.82 04/09/2021 0019
Date Received:04/08/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 04/10/2021 1435 KSH2 04/09/2021 0845 88488
2 3050B 6010D 1 04/12/2021 1138 KSH2 04/09/2021 0845 88488
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Nickel 7440-02-0 6010D 62 23 6.1 mg/kg 1
Potassium 7440-09-7 6010D 9200 2900 360 mg/kg 1
Selenium 7782-49-2 6010D 5.3 J 12 4.7 mg/kg 1
Sodium 7440-23-5 6010D 2600 J 2900 360 mg/kg 1
Zinc 7440-66-6 6010D 1300 29 7.2 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

87
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PACE ANALYTICAL SERVICES, LLC
Sarr►pIeReaaipt Checklist{SRC)(MEDO1 C•15) P.r}vi5e:::::)i29{2O2C
/.20,1,rr,-*givn !ssicingAuthority;PacxENV-WCQL rage 4o' 1
Sample Receipt Checklist (SRC)
client: r .1 f C tiler Ins oek'd byfdate; 'iF'JL_{_' fm! _
11
I McziIts al-receipt: • Pace C]ient ]FS fedfix • Other
D Yes r l,r� Wcrc custody seals.present on the cooler'? _Li .
3'es �,J N o I- N A 7. If custody N Is were present,we a;I i_ Enact aridunhrukn$
.pH Strip ID:_. 1\f� Chlorine Strap if . l Tested by; '71— , ..
0dg!na1 tern:nemturc upon receipt i Deivee: Correctec kom eI tutu u .poL rceeipl %Solid Snap-Cup 11 _Zr- (3
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1dJedtad;❑I'crrrpetature elk lErkgairisi.Bottles IR Crum ID: As IR Gun Correction Factor O °C
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PM was Notified by: phone./cmai]1 ihco-t0-ace(elm lc orrG).
7 yes •NO'_•NA 4. 15 the Commercial courier's packing slip attached to thi:farm?
Ellj es. ri Nic 5. W rc proper custody proced;ryes(NI sip d)followee
a '•s J No 6- Were sample]Ds listed On the COC?
C Yes' N{r 7- Were sample Ms listed On all sati- Prirnioers? ..
NEE
R. Was collection date Ii time listed on the COC?MEM
/•- i 9, Was collection dale&0rne listed on ill sample ul u rs"? _ -
•
r�`s' 10.13id all ounrniner label infortr-ation(1D,c1trti,time)agree with the COC2
Yes: • NU' 1.1-Were tests to be performed listed on the OOC?
, 'f Yes AND
t2- h i€I all samples arrive in the proper containers for each test andfar in goad rol,ciitinrl
,
(unbroken,lids on,cic-)? _
,rrYes 1J,..No 13.Was adequate sample valr.me available? - .
Yen 14-Were all sa mpl� received .;the within' e holding lime or 48 hours,Whichever comes G'st?
Yes No 15.Warr any soon lesoonkaincrs.hissing'-xc. ss(circle one).samples of listed onCk ?
16. For VOA and RSK-I 75 san1ple .were bobbies}u+escnt›:"pea-size 4.'or 6rnrn in diameter)
El Yes ATo N i
- n any of;.'he VOA vitals?
Yes El No rtN, 17. Were all DROIrietalainutriqit srrn oles received at a p]] of c 2't I
Yes I]Ye. � � 18. Were an c}anid�sarnPle�s rernivc1l all a I113: 12 and sulfide samples ruceivcd of a ph>9?
El Yes 1*10 1A 19.Were 911 applicable ]H T�1 1CNle}artiee,p]idol/62 -I rfi0t-3[.i 05rn rrt)samples tree of
,-a[dual chior:nc?
2fF. Were elicnl rrrmarl�slrecu dilutions,ests(i.e.requested MS/MSD designnliruiw,ex---)
©YEs ❑ ° ' —'NA co--ectly transcribed Lam the COC into the onmment wetitm.in UM ?
0 Ye; If tCo 21.Wnis the quote number Tined crs the auntainer label?If urns,Cr,cc 4
;Sa mirk Lime realion. (hi.in5tbconvicted far any sarnple(s,)incorrcetly Preserved or with headspaee,)
received incorrectly and were adjusted accordingly 'i
Sample(s) ...vr�err. Y�`5�'�'ed �
in Mtn ple receiving with mL of ciro]M one;H2S0.4,HNO3,l I i 1,Nall H using SR#
,Tirnc o:preservation_ . If more than Krre prei•eivativa:s need l,please no-g in the cope,»lents below.
I5umple(s) were received with bubbles6~rm 111 dismeter.
5arnple5(5) tiwuc received wally TRC:0.5 mg/I..(If 419 is rta)and were
adjust'd sleeordingly in sample receiving with sodium 11-insu Am(Na25903)with Shealy 11};_ _.
SR barcade la eels applied by: — r ill
-
-r, l ... -. i r
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Sanford VWVTP
Lot Number:WG16063
Date Completed:07/27/2021
07/28/2021 10:28 AM
Approved and released by:
Project Manager II: Lucas Odom
MILB
Q PCCR�c��
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDeORA16,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WG16063
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low percent solids, sample-001 had an initial weight that is 3x greater than standard procedure:
WG16063-001. The LOQ has been adjusted accordingly.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: WG16063
Sample Number Sample ID Matrix Date Sampled Date Received
001 Sanford WWTP Solid 07/14/2021 1130 07/16/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 9

Inorganic non-metals
Client:Synagro Laboratory ID:WG16063-001
Description:Sanford WWTP Matrix: Solid
Date Sampled:07/14/2021 1130 %Solids: 3.46 07/18/2021 2036
Date Received:07/16/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 350.1 (Ammonia-N)350.1 25 07/19/2021 1407 KFE 99305
1 (Nitrate-N)9056A 1 07/20/2021 1608 AMR 99555
1 (Nitrite-N)9056A 1 07/20/2021 1608 AMR 99558
1 (Phosphorus)365.1 25 07/23/2021 1226 DMA 07/21/2021 1635 99611
1 (Soil pH meas)9045D 1 07/18/2021 1716 NBW 99241
1 351.4 (TKN)351.2 5 07/27/2021 1427 DMA 07/21/2021 1523 99586
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Ammonia-N (gas diffusion) 350.1 20000 720 380 mg/kg 1
Nitrate-N (soluble) 9056A 170 14 2.9 mg/kg 1
Nitrite-N (soluble) 9056A 8.7 5.8 2.9 mg/kg 1
Phosphorus 7723-14-0 365.1 34000 B 3600 720 mg/kg 1
Soil pH measured in water @ 19.3° C 9045D 7.1 su 1
TKN 351.2 96000 B 7200 3600 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 9

CVAA
Client:Synagro Laboratory ID:WG16063-001
Description:Sanford WWTP Matrix: Solid
Date Sampled:07/14/2021 1130 %Solids: 3.46 07/18/2021 2036
Date Received:07/16/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 07/22/2021 1500 CMS2 07/21/2021 1058 99301
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 2.3 0.56 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 9

ICP-AES
Client:Synagro Laboratory ID:WG16063-001
Description:Sanford WWTP Matrix: Solid
Date Sampled:07/14/2021 1130 %Solids: 3.46 07/18/2021 2036
Date Received:07/16/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 07/22/2021 1648 JMH 07/21/2021 0347 99256
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 19000 180 68 mg/kg 1
Arsenic 7440-38-2 6010D 8.6 6.8 2.3 mg/kg 1
Cadmium 7440-43-9 6010D 2.0 J 2.3 0.57 mg/kg 1
Calcium 7440-70-2 6010D 19000 2300 280 mg/kg 1
Chromium 7440-47-3 6010D 60 4.5 1.1 mg/kg 1
Copper 7440-50-8 6010D 420 4.5 2.0 mg/kg 1
Iron 7439-89-6 6010D 22000 45 21 mg/kg 1
Lead 7439-92-1 6010D 29 4.5 2.0 mg/kg 1
Magnesium 7439-95-4 6010D 7800 2300 280 mg/kg 1
Manganese 7439-96-5 6010D 1800 6.8 2.7 mg/kg 1
Molybdenum 7439-98-7 6010D 18 18 4.5 mg/kg 1
Nickel 7440-02-0 6010D 39 18 4.8 mg/kg 1
Potassium 7440-09-7 6010D 11000 2300 280 mg/kg 1
Selenium 7782-49-2 6010D 7.6 J 9.1 3.7 mg/kg 1
Sodium 7440-23-5 6010D 2900 2300 280 mg/kg 1
Zinc 7440-66-6 6010D 1000 23 5.7 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 9

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4,Laboratory R date j TThe -
Note;All saniplegare retained for six weeks from renerptunfps other !ergLI,gFOFJLY (/ NecciotToms, ;Temp,took '
arrangeiments are apace r;eCEF. d on Ica{ChBdti 71 N .ice F+sck ' ` L 'c I❑ y 0 -. I
Eifeatfue date oG.2T.2912

PACE ANALYTICAL SERVICES, LLC
Samples Receipt rhec[[ditt(S }lM t_,r
k0012C-15i Ri4ed:9i2:4f202.0
� RC
e r 7d:yt1Cal Ism.: Authority:Pace LNV-%VCOL Page 1 of 1
Sample Ileceipt Checklist (SRC)
(.'Iicnt: 5311at70_ Cooler Inspected b Mac: alga i O'7116f2LI2I 1.or4: WGI6063
liMean of script: ■ PPcc' Client ❑UPS ri FcdF,-x • Other. -
Y No 1-Were cu€tad sea ra ls ,5en rim❑r [- i ti,Ier?
Yvs NoIr4I2.ifcustuoy seo.h mere resent,werethry intact ind WIhIukeu"
pH Strip 1! f iIrrrine Strip Ili_ Tested by
Original temperatu re upon receipt?Derived(Corrcctcd)Lsmperutuve upou receipt %Solid Snap-Cup Eat-t4 5 --
3..i. 13,2 o-' N . {J 1A. bc NA r Nf. CC Ik . NA 6.c
Method-.❑Teinperaturc 13Iank 0 .• inst E1 Liles IRGur]D: 5 JI4 [gun Corm:Liort Factor: 0 _uC '
Method paced:ant: ❑ Wet Try • ice Pak El Dry' lee ❑ NOW: —_ .
Y E ❑NoNA 3- If Lemperattn n of any cooler exceeded b.CPC,was l'rujut:l Munugcr Notified?FM was Notified by: plane/email;face-to-face(vim IL une). _ _.
LiYcs El Na E]NA d- is tiles t.lrnreerrsia]courier's packing slip atiachcd 7o this torm?
0 Yes I I No 15. v4rei+e proper c.lis-rody pr4cethir (rCLrgLlrthedIrezeived)fal'owod?
✓ Yes I.-..INa I 6. Were sample IDs listed on the coc7
A YeS Ti Nu I. LWcre sulr!ple IDs li tied pit all sample coiltethcrs? -
I-1 Yes Li Ne 8, W as colkel Ion date&time listed on thil COC?
Q Yes Erik: 9_ Was collection date&timc lislad an all bamp'.e Corttiiners? _
F4 Yes ale III Did�Il container label inform ttioiti([Tn. dare, lime)agree with the COC? —
n Yet II Na 11, Were tests to be performed listed an thy;CC)C? -- -
l^_. i)id all samples arrive in Lie proper kontainr:rs ter cx.ch IDA UAW in goad inrd'ririn
Z Y ❑No
(unbroken.,]ids on,cic.)? _.- _—.-
a
❑f Y es LJ No 13, 14\hs arlecl,i we sample w lint e available? -i
2 Yes El No ]4. Were.ail sampics ccoivcd Within '..5 the 1 old'uig tune or 413 hours,whichever comes first?
❑Yam k I No 15, Were any Szmple contairiers trissincfexcesa(circic onr~)surnp[es Not listed au COC?
16- vur VOA an,!RSK-175 aainplcs,wdre bubbly pn senL>'pea-size"(l4"or 6rnin in J is ne1er)
::17Y ❑Ala, + ' in arty of the VOA vial? .
ON, NA 17. Were all DRO}metalsinutrient samples received at a pH of=2
V r..4 I I ,k r ,E NA 12, Wore all G iiiiidr,sum lots received at apt!> I'2 and sulfide stun l s recc['ued at a H>97
❑ 0 }' I' ..� of p " C�
; 9. Wei-e al[applicrlli'le N143,71 lc}ranid phena11655.1/603 3( 1k m t L.j samples frcc of
❑Ycs FIND; ❑J N� Ii+cs[dual ehlorne7
❑Ye5 ❑No DNA 24, \Ycrc cl:cnt rcciarkSirequeSts(i,e.requested dilutions, NIS?MU)fIesignzliLrns,etc...)
correctly transcribed frorr.:he COC into the c.nlule:rt section in LIKES?
Yea [ I N0 2 i. Was the vote n um bET 1 i d ed or.L11e corLLnintr killer [f yes,Quote 4 --
'Sample Preseivntion (Must he c^inpletnd for env mample(s)indorreutly preterued or with Bads ACC-)
Samples) NA were received incur ctly praseryed ur1c were adjuster accordingly
in sample re.eivirig witls NA niLofoi:cic oLit: 1-E2 04, PIN03,1-1(1,MOJ-E using SR fl N.A .--_. _
Tin ofpre.servailnr. NA . If more than one pre. ervaiive is needed.please note:i5 the comments below.
Sample(3) Nr4 _were received with bubb'es 6 min in dim rteLcr.
5arnples(s) NA were received-.Nit]TRC>0.5 np.alL(If#19 is'Wp)irrrrl wcru
udjustrki.;ccardingly in sample receiving with audiurn thinsulfale(NazS,O3)with Shealy gip_ NA ,
—
SR barcude labels applicd by; J R.G2 Dam.: ('7i 16+??2 L
Comments; --
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 9 of 9

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Chris Wynne
Project Name: Sanford VWVTP
Lot Number:WJ08069
Date Completed:10/22/2021
10/25/2021 11:03 AM
Approved and released by:
Project Manager II: Lucas Odom
MILB
Q PCCR�c��
'ye I ANSI NatonalAccredltatlon Board
ACCREDITEDeORA16,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WJ08069
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non-Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W"qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, the initial sample amount of the following samples is 3x greater than the
standard procedure: WJ08069-001. The LOQ has been elevated to reflect the dilution.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WJ08069-001
Description:Sanford WWTP Matrix: Solid
Date Sampled:10/05/2021 1330 %Solids: 2.81 10/12/2021 0017
Date Received:10/06/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (%Solids)SM 2540G 1 10/12/2021 0017 NBW 18402
1 350.1 (Ammonia-N)350.1 25 10/17/2021 0031 DAK 19108
1 (Nitrate-N)9056A 10 10/15/2021 1244 AMR 19074
1 (Nitrite-N)9056A 10 10/15/2021 1244 AMR 19075
1 (Phosphorus)365.1 50 10/15/2021 1748 ATH 10/15/2021 1139 18956
2 (Soil pH meas)9045D 1 10/20/2021 1456 NBW 19580
1 351.4 (TKN)351.2 2 10/13/2021 1525 ATH 10/13/2021 0945 18598
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
%Solids SM 2540G 2.81 % 1
Ammonia-N (gas diffusion) 350.1 14000 890 460 mg/kg 1
Nitrate-N (soluble) 9056A 300 180 36 mg/kg 1
Nitrite-N (soluble) 9056A 290 71 36 mg/kg 1
Phosphorus 7723-14-0 365.1 50000 S 8900 1800 mg/kg 1
Soil pH measured in water @ 19.4° C 9045D 7.2 su 2
TKN 351.2 72000 3600 1800 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 10/13/2021 1524 CMS2 10/12/2021 1313 18311
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 2.8 0.67 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 10/13/2021 1814 KSH2 10/13/2021 0143 18303
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 24000 230 87 mg/kg 1
Arsenic 7440-38-2 6010D 7.7 J 8.7 2.9 mg/kg 1
Cadmium 7440-43-9 6010D 2.4 J 2.9 0.73 mg/kg 1
Calcium 7440-70-2 6010D 24000 2900 360 mg/kg 1
Chromium 7440-47-3 6010D 61 5.8 1.5 mg/kg 1
Copper 7440-50-8 6010D 540 5.8 2.6 mg/kg 1
Iron 7439-89-6 6010D 27000 58 27 mg/kg 1
Lead 7439-92-1 6010D 31 5.8 2.6 mg/kg 1
Magnesium 7439-95-4 6010D 9400 2900 360 mg/kg 1
Manganese 7439-96-5 6010D 2300 8.7 3.4 mg/kg 1
Molybdenum 7439-98-7 6010D 22 J 23 5.8 mg/kg 1
Nickel 7440-02-0 6010D 48 23 6.1 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:WJ08069-001
Description:Sanford WWTP Matrix: Solid
Date Sampled:10/05/2021 1330 %Solids: 2.81 10/12/2021 0017
Date Received:10/06/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 10/13/2021 1814 KSH2 10/13/2021 0143 18303
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Potassium 7440-09-7 6010D 11000 2900 360 mg/kg 1
Selenium 7782-49-2 6010D 9.8 J 12 4.7 mg/kg 1
Sodium 7440-23-5 6010D 3400 2900 360 mg/kg 1
Zinc 7440-66-6 6010D 1300 29 7.3 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit Q=Surrogate failure
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

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Moto:All samples are rEta,ined for six weeks from receipt a li less other LT
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PACE ANALYTICAL SERVICES, LLC
I
' Samples RectEnt Checklist{SRek(M£001;�C-15) Revis2d:5f 9J Ot0
ceFr:ary7ie�,! Issuing Authcrlty-Pace E V-WCO€ I Page Z of 1
Sample Receipt Choc list(SRC) 1
CI:cnt;..s9" Lr'' U Cooler',ispec4cd byfdate: 3 H1 ; •19;1 �a21 �iN: w10845
h'leans afreceipt: M • '[[en' 151 UPS - FeclEx •I other 1
Yes / NE. I. Were Glasrody seals:�raien[on the cooler? — i
IU Y, •No E2 NA 2-If custody sea]x webs men],were they iheact a unbroken? �..
H Strip]D; NA Chloride Strict ICI NA I Tested by_i^
rEgii a]temperature upon raccipt 1 f}er1vcd(Corm:L.0 [.rnperature ubor receipt Moat Snap-Cup]D: 2I-!`
di f4,7 0C NA 1 NA off: NA +miry o - TtiA JNA o -
Method;f Temperanrre Blank ❑Agains!Bottles IR Gun ID; 5 - IR(Ion Correctiut Pac;,or: 0 DC
M1 I-.nd of ei olum:. El Wei I r..r!. ❑ Ice Packs ❑ Iry ra_ED cjn
n Y [ No i�]A I. ff lei r• Inure of al ender exce [bed 6.:Pc was Project Manager�7+lnlinedp
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. PM wos Notified by,phone lemon?lea #o-tace(c.irc]z.one),
o Ves ■No ■NA 1, is the commercial eaJricr'5 paekiii%slip i ac#iedtolfhlx lean? 1
J '',' N Ci No 5, Wax proper c.ir iixly p,ucexJuna(re[ir~cO5hedfie4eivle.j)-COI[owcd 1
0 Ye Na 6- Were sample IL]s fisted tN'I the CO(2? I .
FA Yes ENo 7. Were Sample Ms listed on all trernple cor4ainen7 1
J Ye• .0Na S. Was col!eu'irm date& Ciit a listed on the :.)C? • I -
EYes ❑No,. 4. Was colJecci On datr&time lined oil all s u,rp I:'containers& I •
.j Yes El No ['J-Did all container label info(mullion op,date.doe)agree:it.iv,lc. C? •
J`Yes. . No —11.Were tests to hu performed]fisted on the LOC?
Y n 1_2: Did a][aaunplcs arrive in tho Drove txmtginers for eieh tryst aniVorlin good condition
(urtbrnkcn: lids on, ete:)? _- I I
i
12'Yes L,hv Mil [3- Wi•wl-icquate sofa frlr.vv:u[ne minable?' _
• IR Yes _•No 14.Wero aIr a.Ixlpies reccive�within Y the[iu]ding time or 481tours, 1)iehewc.r Mettles ETV?
Eyes ., NO 15. \Vera any same:es conta.ine[s mks in Pie ess(C role one)samples IStot]i ted on COC?
16: For 'C1 . and RS K-115 samples,were or[bbies DMIeri >'`paa-^.i..E Off or burin in el IA:ratca')I ❑Yes �7Jir ErTIA in anti of[IIC VOA vials? j' J
•Y !No 7I\J r\ 17- Weee rxl l 1.#E10hnetalsrnu#rient s�npIcs rl ei lied la a pFi of<2? i
.m I..]No_j NA J S. Welt:all cyanide samples received:rr a p I> 12 Nod su[f cIe samp4 received at a pH 47
❑Yes Tfr �TIA 19. Were all fpplicableNH3JT TN/ey�arida+p eilili 5-llbl}8.3 (.0.5iriE/L)samples freed-
residual e.hforine?
❑ye, c No DNA 26-Were r.lier-d r��..Ina:kstrcqueaa(I-C.tequest�ed Jilt Eons, MS.'1r1Sl7 d igriatiur[s,etc,...)cowec41y trar.scribcsl from the COC iota the cJu['rrent sectirrn in L1MSt
EL:reS. I/I No 21. Vial the note number listed on the con[r3#ner!abe
anromp
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Srlrlr.Yr�eserreiti a (Must he ro i1plefeCl for any sa:np[e(s)incorrectly�prcgcrved or with]fe4paee,)
Srmple(s) NA •
ws[+c received inc a ![} prcxenedand are adRls'ed tic oi-4irg'y
in Semple receiving.W'ttli NA mL of cirGly one: R2504,IJN03, J-EC[,NaOH using SR# N `
irne ufPrt sorvation bA = If more Chao one preservaliwo is neddera,plcalse note in the comments bek w.
I
arnple(s) HA were ra~ei veil with bubbrd > min is d i[irr,v[er,
Sampics(s) NA were receiw:ed with TRC>0.5 vtdL:(Ike#19 is rye)yard were •
urikisted accordin l}' in trample rime Eying with sodium Ihiasui Rae 041a2 ];)w h SE[e [y+ID: N'°`-
R h:rcode.la eL9 xpp[ied f ; 1S]i ryatc,_ Ica78r3O2I , n
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00049-0-0004- ACRES UTILIZED:11.5
LAND OWNER:HENRY STINSON ANNUAL DRY TONS APPLIED:10.17 SITE#:NC CH 00049 ACRES PERMITTED:11.5
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:CID CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:141 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site
Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 *Crop 2
10/4/2021 86,800.00 (G) 2.810 0.882 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 44.089 FSP
Oct-21 86,800.00 (G)
Total 0.882 Total 44.089 0.000
AS CD CU CR PB HG MO* NI SE ZN P Lime Applied
Annual Ibs/acre Applied 0.014 0.004 0.953 0.108 0.055 0.001 0.039 0.085 0.017 2.294 88.213 Date Lbs/Ac
Cumulative Ibs/acre Applied 0.014 0.004 0.953 I 0.108 I 0.055 0.001 0.039 0.085 0.017 2.294 1
Permit PAN Limit(lbs/acre) 1st Crop4 141
Federal C.P.L.R.(Ibs/acre)**** 36.6 34.8 1,339.0 11111.1111 267.9 15.0 SIM 3750 89.0 2,500.0
11111111.1111.111
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant pen es r in. ' g false information,including the possibility of fines and impris ment r knowing violations."
Z 11 Lv ZZ.
SIGN OF LAND APPLIER D TE
NR=Not Reported or Not Requi el *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface, INJ-Injection,SURIN-Incorporation **** C.P.L.R. :Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00049-0-0005- ACRES UTILIZED:5.6
LAND OWNER:HENRY STINSON ANNUAL DRY TONS APPLIED:10.94 SITE 4:NC CH 00049 ACRES PERMITTED:5.6
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:CID CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:141 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
7/14/2021 93,000.00 (G) 2.820 1.963 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 118.469 FSP
Jul-21 93,000.00 (G)
Total 1.963 Total 118.469 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.036 0.009 2.120 0.393 0.145 0.003 0.086 0.243 0.021 5.105 141.366 Date Lbs/Ac
***** *..**
emulative Ibs/acre Applied 0.036 0.009 2.120 0.393 0.145 0.003 0.086 0.243 0.021 5.105
cre) 1st Crop ... , I
Permit PAN Limit(Ibs/a 141
Federal C.P.L.R.(Ibs/acre)**** 36.6 34.8 1,339.0 M 15.0 375.0 89.0 2,500.0 I -
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTPAEROB.DIG.LIQUID
"I certify,under penalty of law,that this document as prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant pe,:ties -• u mi ing false information,including the possibility of fines and impris nment or knowing violations."
1`f Ltd 22
SIG E OF LAND APPLIER ATE
NR=Not Reported or Not Req ' *"* Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation ""** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00049-0-0006- ACRES UTILIZED:7.3
LAND OWNER:HENRY STINSON ANNUAL DRY TONS APPLIED:16.77 SITE#:NC CH 00049 ACRES PERMITTED:7.3
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:CID CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:141 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip , Volati- Mineral. Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
7/13/2021 124,000.00 (G) 2.820 1.987 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 119.868 FSP
7/14/2021 18,600.00 (G) 2.820 0.298 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 17.980 FSP
Jul-21 142,600.00 (G)
Total 2.285 Total 137.848 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.042 0.010 2.467 0.457 0,169 0.004 0.101 0.283 0.024 5.940 164.491 Date Lbs/Ac
*****
Cumulative Ibs/acre Applied 0.138 0.039 8.982 2.295 0.559 0.012 T--0.323 1.253 0.104 17.522
Permit PAN Limit(lbs/acre) 1st Crop, 141
Federal C.P.L.R.(Ibs/acre)**** 36.6 34.8 a 1,339.0 267.9 15.0 375.0 89.0 2,500.0
MN
SBCAEDL=SANFORD,NC BUFFALO CREEK W WTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant a ti r s bmi ' g false information,including the possibility of fines and imprisoi ent f knowing violations."
Z (1 0 2
G E OF LAND APPLIER DA E
NR=Not Reported or Not Req ' *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022 DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME:SANFORD,NC WQ PERMIT A WQ0000543 FIELD#:NC-CH-00049-0-0007- ACRES UTILIZED:18.9
LAND OWNER:HENRY STINSON ANNUAL DRY TONS APPLIED:38.04 SITE#:NC CH 00049 ACRES PERMITTED:13.9
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:CID CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:141 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
M Gallons(G) _ Site 1 Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite ' (Ibs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
7/26/2021 49,600.00 (G) 2.820 0.309 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 18.660 FSP
7/29/2021 49,600.00 (G) 3.460 0.379 SBCAEDL DRY "0-<1/Z" SUR 0.5 0.30 96,000.00 20,000.00 178.70 25.027 FSP
7/30/2021 124,000.00 (G) 3.460 0.949 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 62.568 FSP
7/31/2021 49,600.00 (G) 3.460 0.379 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 25.027 FSP
Jul-21 272,800.00. (G)
Total 2.016 Total 131.282 0.000
AS CD - CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.035 0.008 1.768 0.267 0.122 0.002 0.075 0.172 0.029 4.219 138.378 a Date Lbs/Ac
Cumulative lbs/acre Applied 0.147 0.042 9.631 2.560 0.587 I 0.012 1 0.348 1.317 0.123 1 18.123 1'
Permit PAN Limit(lbs/acre) 1st Crop,l 141
{Federal C.P.L.R.(Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document was repared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant penalti ram' false information,including the possibility of fines and impriso ent f knowing violations."
SIGNATU E F LAND APPLIER D E
NR=Not Reported or Not Required *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 **'** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00049-0-0008- ACRES UTILIZED:9.4
LAND OWNER:HENRY STINSON ANNUAL DRY TONS APPLIED:19.68 SITE If:NC CH 00049 ACRES PERMITTED:9.4
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:CID CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:141 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- 1 Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate*" Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
7/31/2021 43,400.00 (G) ' 3.460 0.663 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 43.752 FSP
Jul-21 43,400.00 (G)
8/2J2021 86,800.00 (G) 3.460 1.327 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 ' 178.70 87.503 FSP
8/5/2021 6,200.00 (G) 3.460 0.095 SBCAEDL DRY 0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 6.250 FSP
Aug-21 93,000.00 (G) ! --
Total 2.085 Total 137.505 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.036 0.008 1.751 0.250 0.121 0.002 0.075 0.163 0.032 4.170 141.763 Date Lbs/Ac
CumulativeIbs/acre Applied
0.120 0.034 7.510 1.893 0.461 0.010 0.268 1.019 0.102 14.076
Permit PAN Limit(Ibs/acre) 1st Crop, ,
_ 141
Feder-ar
SBCAEDLP SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG•LIQUID
1,339.0
( ) 267.9 15.0 375.0 89.0 2,500.0
"I certify,under penalty of law,that this document s prepared under my direction or supervision in accordance with a system d signed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant pe ' s ubmi ing false information,including the possibility of fines and impriso ent fo knowing violations."
I`I f
1.) 22
SIG U OF LAND APPLIER DA E
NR=Not Reported or Not Re ire *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00066-0-0001- ACRES UTILIZED:31.7
LAND OWNER:STINSON,JR HENRY ANNUAL DRY TONS APPLIED:56.36 SITE#:NC CH 00066 ACRES PERMITTED:31.7
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:NANFORD-BADIN CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:135 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site -� Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
8/11/2021 74,400.00 (G) 3.460 0.339 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 22.328 FSP
8/12/2021 173,600.00 (G) 3.460 0.790 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 52.099 FSP
8/19/2021 74,400.00 (G) 3.460 0.339 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 22.328 FSP
8/23/2021 68,200.00 (G) 3.460 0.310 SBCAEDL DRY 0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 20.467 FSP
Aug-21 390,600.00 (G)
Total 1.778 Total 117.222 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
[ -Annual lbs/acre Applied 0.031 0.007 1.493 0.213 0.103 ' 0.002 0.064 0.139 0.027 3.555 120.853 Date Lbs/Ac
Cumulative Ibs/acre Applied 0.148 0.046 10.975 3.081 0.657 0.015 0.395 1.445 0.137 19.388
Permit PAN Limit(Ibs/acre) 1st Crop 135
Federal C.P.L.R.(lbs/acre)*'** 36.6 34.8tl tl1,33,9.0 I 267.9 15.0 ,I375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document was prep ed under my direction or supervision in accordance with a system d signed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant pena ' s r su fal information,including the possibility of fines and impriso ent fo knowing violations."
,--
1-2-
AT E D APPLIER DA E
NR=Not Reported or Not Required *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,I -Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 *""** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME:SANFORD,NC WQ PERMIT#:W00000543 FIELD#:NC-CH-00066-0-0002- ACRES UTILIZED:20.0
LAND OWNER:STINSON,JR. HENRY ANNUAL DRY TONS APPLIED:47.41 SITE#:NC CH 00066 ACRES PERMITTED:20.0
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:NANFORD-BADIN CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE HAY(FSH) CROP 1 MAX.PAN:180 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
8/5/2021 12,400.00 (G) ) 3.460 0.090 SBCAEDL DRY ''0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 5.906 FSH
8/6/2021 68,200.00 (G) 3.460 0.492 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 32.484 FSH
8/9/2021 68,200.00 (G) 3.460 0.492 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 32.484 FSH
8/23/2021 55,800.00 (G) 3.460 0.403 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 26.578 FSH
8/24/2021 99,200.00 (G) 3.460 0.716 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 47.249 FSH
8/25/2021 f 12,400.00 (G) 3.460 0.090 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 5.906 FSH
8/27/2021 12,400.00 (G) 3.460 0.090 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 5.906 FSH
Aug-21 328,600.00 (G)
Total 2.373 Total 156.513 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual Ibs/acre Applied 0.041 0.010 1.993 0.285 0.138 0.003 0.085 0.185 0.036 4.746 161.359 Date Lbs/Ac
Cumulative lbs/acre Applied 0.137 0.042 10.049 2.730 0.615 0.015 0.364 1.282 0.127- I 18.296
Permit PAN Limit(lbs/acre)
1st Crop
180
k
[Federal C.P.L.R.(Ibs/acre)**** 36.6 34.8 1,339.0 I I 267.9 , 15.0 [ I 375.0 I 8.9.0 I 2,500.0 g
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTPAEROB.DIG.LIQUID
"I certify,under penalty of law,that this document w..prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant p f s sub.'tf g false information,including the possibility of fines and impriso ent fo knowing violations."
14 24 n
SIGN;7 OF LAND APPLIER DA E
NR=Not Reported or Not Required *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 **"** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME:SANFORD,NC WQ PERMIT#:W00000543 FIELD#:NC-CH-00066-0-0003- ACRES UTILIZED:16.9
LAND OWNER:STINSON,JR. HENRY ANNUAL DRY TONS APPLIED:25.05 SITE#:NC CH 00066 ACRES PERMITTED:16.9
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:NANFORD-BADIN CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:135 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site - _ Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization ` TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 'Crop 2
8/25/2021 86,800.00 (G) 3.460 0.743 , SBCAEDL DRY "0-0/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 49.022 FSP
8/27/2021 49,600.00 (G) 3.460 0.425 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 28.013 FSP
8/30/2021 37,200.00 (G) 3.460 0.319 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 21.010 FSP
Aug-21 173,600.00 (G)
Total 1.487 Total 98.045 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.026 0.006 1.249 0.178 0.086 0.002 0.054 0.116 0,023 2.973 101.081 Date Lbs/Ac
****. *....
Cumulative lbs/acre Applied 0.131 0.041 9.683 2.696 0.582 I 0.014 I 0.353 1.261 l 0.123 17.251 !
Permit PAN Limit(lbs/acre) 1st Crop
_ 135
Federal C,P.LR.(Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document wa prepared under my direction or supervision in accordance with a system esigned to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant penal' or mittin false information,including the possibility of fines and impriso ent f knowing violations."
LrLfwz2
IG OF LAND APPLIER D E
NR=Not Reported or Not Require *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME:SANFORD,NC WQ PERMIT#:W00000543 FIELD#:NC-CH-00066-0-0004- ACRES UTILIZED:30.9
LAND OWNER:STINSON,JR. HENRY ANNUAL DRY TONS APPLIED:51.88 SITE#:NC CH 00066 ACRES PERMITTED:30.9
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:NANFORD-BADIN CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN: 135 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site
Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate'** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 ° Crop 2
8/31/2021 74,400.00 (G) 3.460 0.348 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 22.928 FSP
Aug-21 74,400.00 (Gj
9/7/2021 74,400.00 (G) 3.460 0.348 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 22.928 FSP
9/8/2021 80,600.00 (G) 3.460 0.377 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 24.839 FSP
9/9/2021 12,400.00 (G) 3.460 0.058 SBCAEDL DRY "0-0/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 3.821 FSP
9/10/2021 117,800.00 (G) 3.460 0.550 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 36.303 FSP
Sep-21 285,200.00. (G)
Total 1.681 Total 110.819 0.000
AS CD CU CR
PB HG * MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.029 0.007 1.411 0.202 0.097 0.002 0.060 0.131 0.026 3.360 114,252 Date Lbs/Ac
Cumulative lbs/acre Applied 0.106 0.033 7.780 2.146 0.475 0.011 0.288 _ 0.989 0.099 14.255
Permita PAN Limit(lbs/acre) 1st Crop 135
Federal C.P.L.R.(lbs/acre)**** 36.6 34,8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document wa prepared under my direction or supervision in accordance with a system esigned to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant pen ie for mitt g false information,including the possibility of fines and impriso eat r knowing violations."
�� Zozz
SIGN O.9.'F LAND APPLIER D TE
* NR=Not Reported or Not Require *** Mineralization Rates:Compost-0.1,Anaerobically digested-0-2,Aerobically digested-0.3,Raw Sludge-0.4
Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L_R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022 DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00066-0.0005- ACRES UTILIZED:14.0
LAND OWNER:STINSON,JR. HENRY ANNUAL DRY TONS APPLIED:30.41 SITE#:NC CH 00066 ACRES PERMITTED:14.0
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:NANFORD-BADIN CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE HAY(FSH) CROP 1 MAX.PAN:180 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site 1 Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches ' Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
9/10/2021 24,800.00 (G) 3.460 0.256 SBCAEDL DRY "0-<1/2" SUR 0.5 0,30 96,000.00 20,000.00 178.70 16.870 FSH
9/16/2021 93,000.00` (G) 3.460 0.959 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 63.262 FSH
9/17/2021 62,000.00. (G) 3.460 0.639 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 42.174 FSH
9/20/2021 24,800.00 (G) 3.460 0.256 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 16.870 FSH
9/21/2021 6,200.00 (G) 3.460 0.064 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 4.217 FSH
Sep-21 210,800.00 (G) 1
Total 2.174 I Total 143.393 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.037 0.009 1.826 0.261 0.126 0.002 0.078 0.170 0.033 4.348 ' 147.834 Date Lbs/Ac
Cumulative lbs/acre Applied 0.037 0.009 1.826 0.261 0.126 0.002 0.078 0.170 0.033 4.348
Permit PAN Limit(lbs/acre) 1st Crop: 180
Federal C.P.L.R.(lbs/acre)**** 36.6 I 34.8 1,339.0 { , , I 267.9 1 15.0 I j 375.0 89.0 1 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that thi current w.s prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant pe tie ubmitt;i g false information,including the possibility of fines and impri so ent f knowing violations."
f Zv LZ
S N* OF LAND APPLIER D E
NR=Not Reported or Not Requ *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00066-0-0006- ACRES UTILIZED:21.7
LAND OWNER:CYNTHIA/ANGELA STORY/EADES ANNUAL DRY TONS APPLIED:58.33 SITE#:NC CH 00066 ACRES PERMITTED:21.7
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:CID CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE HAY(FSH) CROP 1 MAX.PAN:189 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist inches Method* Rate*" Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
6/25/2021 74,400.00 (G) 2.820 0.404 SBCAEDL DRY 0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 24.349 FSH
6/28/2021 130,200.00 (G) 2.820 0.706 SBCAEDL DRY "0-<112" SUR 0.5 0.30 87,000.00 20,000.00 69.00 42.612 FSH
6/29/2021 117,800.00. (G) 2.820 0.639 SBCAEDL DRY "0-<112" SUR 0.5 0.30 87,000.00 20,000.00 69.00 38.553 FSH
6/30/2021 124,000.00 (G) 2.820 0.673 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 40.582 FSH
Jun-21 446,400.00 (G)
7/1/2021 49,600.00 (G) 2.820 0.269 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 16.233 FSH
Jul-21 49,600.00 (G)
Total 2.691 Total 162.329 0.000
AS CD CU CR PB HG MO NI SE Mal P Lime Applied
Annual lbs/acre Applied 0.050 0.012 2.906 0.538 0.199 0.005 0.118 0.334 0.029 MEM 193.705 Date Lbs/Ac
Cumulative Ibs/acre Applied 0.157 0.045 10.689 2.851 0.656 0.015 0.405 1.378 0.128 20.508
. �... 9 _
Permit PAN Limit(lbs/acre) 1st Crop
189
Federal C.P.L.R.(Ibs/acre)*"** 36.6 1 34.8 1,339.0 gg 267.9 15.0 375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document w prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant pe ie fo ub itti g false information,including the possibility of fines and impriso nt fo knowing violations."
r L Pi 2-0 ZZ
SIGN OF LAND APPLIER DA E
NR=Not Reported or Not Requ *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00066-0-0008- ACRES UTILIZED:6.2
LAND OWNER:CYNTHIA/ANGELA STORY/EADES ANNUAL DRY TONS APPLIED:10.21 SITE it:NC CH 00066 ACRES PERMITTED 6.2
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:CID CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE HAY(FSH) CROP 1 MAX.PAN:189 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, ' Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
7/1/2021 86,800.00 (G) 2.820 1.654 SBCAEDL DRY "0-<1/2" '" SUR 0.5 0.30 87,000.00 20,000.00 69.00 99.818 FSH
Jul-21 86,800.00 (G)
Total 1.654 Total 99.818 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.030 0.007 1.787 0.331 0.122 0.003 0.073 0.205 0.018 4.301 119,111 Date Lbs/Ac
Cumulative Ibs/acre Applied 0.160 0.047 11.140 3.128 w 0.670 0.015 0.398 1.549 0.126 20.677
Permit PAN Limit(Ibs/acre) 1st Crop: I 189
Federal C.P,L.R.(Ibs/acre)**** 36.6 34.8 ,339.0 267.9 15.0 [ 375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document w s prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant p a ties su mi ng false information,including the possibility of fines and impriso ent for owing violations."
c
Z lc- 2 U 2-2-
SIG E OF LAND APPLIER DAT
NR=Not Reported or Not Req *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00066-0-0011- ACRES UTILIZED:7.1
LAND OWNER:STINSON,JR HENRY ANNUAL DRY TONS APPLIED:18.79 SITE#:NC CH 00066 ACRES PERMITTED:7.1
OPERATOR:HENRY STINSON PREDOMINANT SOIL SERIES:CID CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:189 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, I Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method" [ Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
8/2/2021 37,200.00 (G) 3.460 0.753 rSBCAEDL DRY "0-<1/2" t SUR 0.5 0.30 96,000.00 20,000.00 178.70 49.651 FSP
8/5/2021 93,000.00 (G) 3.460 1.882 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 96,000.00 20,000.00 178.70 124.128 FSP
Aug-21 130,200.00 (G)
Total 2.635 Total 173.779 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.045 0.011 2.213 0.316 0.153 0.003 0.095 0.206 0.040 5.269 179.161 Date Lbs/Ac
Cumulative lbs/acre Applied 0.156 0.043 9.671 2.437 0.597 0.012 ( 0.347 1.318 0.131 l 18.329
Permit PAN Limit(lbs/acre) 1st Crop!, — 11 189
Fed eral C.P.L.R.(Ibs/acre)**** 36.6 34.8 �'' 1,339.0 267.9 15.0 T 375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document we prepared under my direction or supervision in accordance with a system d signed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant pen e fo bm'ti g false information,including the possibility of fines and impriso ent fo knowing violations."
1 2-
SIGN E OF LAND APPLIER DA E
NR=Not Reported or Not Requ a *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00077-0-0004- ACRES UTILIZED:53.9
LAND OWNER:PAUL&LUCY PRICE ANNUAL DRY TONS APPLIED:42.14 SITE#:NC CH 00077 ACRES PERMITTED:53.9
OPERATOR:PAUL&LUCY PRICE PREDOMINANT SOIL SERIES:NANFORD BADIN CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:128 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization 1 ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
10/26/2021 124,000.00 (G) 2.810 0.270 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 13.473 FSP
10/27/2021 124,000.00 (G) 2.810 0.270 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 13.473 FSP
10/28/2021 93,000.00 (G) 2.810 0.202 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 10.105 FSP
Oct-21 341,000.00 (G)
11/1/2021 18,600.00 (G) 2.810 0.040 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 2.021 FSP
Nov-21 18,600.00 (G)
Total 0.782 Total 39.072 0.000
AS CD CU CR
allallaga. MO NI 1.11.I ZN P Lime Applied
Annual lbs/acre Applied 0.012 0.004 0.844 0.095 0.048 0.001 0.034 0.075 0.015 2.033 78.176 Date Lbs/Ac
Cumulative.lbs/acre Applied 0.042 0.011 2.731 0.503 0.169 0.003 0.112 0.272 0.053 6.321
/Permit PAN Limit(lbs/acre)
1st Crop a 128
Federal C.P.L.R.(lbs/acre)**** 36.6 I 34.8 ' 1,339,0 '267.9 15.0 _1 375.0-1 89.0 - 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK W WTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that di' doc ent w prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted,I am
aware that there are significant pe ties f sit tti g false information,including the possibility of fines and impriso ent r knowing violations."
_ Z t¢ PI zz
SIGNA -- OF LAND APPLIER TE
NR=Not Reported or Not Requi *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R. :Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00077-0-0005- ACRES UTILIZED:15.6
LAND OWNER:PAUL&LUCY PRICE ANNUAL DRY TONS APPLIED:63.15 SITE#:NC CH 00077 ACRES PERMITTED:15.6
OPERATOR:PAUL&LUCY PRICE PREDOMINANT SOIL SERIES:CID LIGNUM CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:CORN SILAGE(CSI) CROP 1 MAX.PAN:224 CROP 2 NAME:MIXED COOL SEASON CROP 2 MAX.PAN:50
RESIDUAL SOURCE(S):*See list at bottom of report
(ranee thArer_1
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) °/" Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Act Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
4/19/2021 148,800.00' (G) 5.130 2.040 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 33,000.00 7,600.00 82.00 46.939 CSI
4/20/2021 111,600.00 (G) 2.820 0.841 p SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 50.759 CSI
4/21/2021 74,400.00 (G) 2.820 0.561 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 33.840 CSI
Apr-21 334,800.00 (G)
10/6/2021 24,800.00 (G) 2.810 0.186 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 9.310 MCSG
10/7/2021 55,800.00 (G) 2.810 0.419 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 20.948 MCSG
Oct-21 80,600.00 (G)
Total 4.047 Total 131.538 30.258
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.051 0.012 2.943 0.522 0.203 0.005 0.124 0.326 0.041 7.219 218.625 Date Lbs/Ac
Cumulative lbs/acre Applied 0.131 0.037 MENIIMIla 0.537 0.010 0.338 0.984 0.103 18.500
Permit PAN Limit(lbs/acre) 1st Crop 224
2nd Crop . , _ . .-. 50
Federal C.P.L.R.(lbs/acre)**** 36.6 34.8 1,339.0 I 267.9 15.0 '375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this docume t was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant lti r su itting false information,including the possibility of fines and impriso 't fo knowing violations."
s
2if 24 22
SI URE OF LAND APPLIER DA E
* NR=Not Reported or Not R red *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-O.3,Raw Sludge-0.4
Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R. :Cumulative Pollutant Loading Rate
** Volatilization Rate; Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:W00000543 FIELD#:NC-CH-00077-0-0006- ACRES UTILIZED:15.0
LAND OWNER:PAUL&LUCY PRICE ANNUAL DRY TONS APPLIED:55.71 SITE#:NC CH 00077 ACRES PERMITTED:15.0
OPERATOR:PAUL&LUCY PRICE PREDOMINANT SOIL SERIES:CID LIGNUM CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:142 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method" Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
1/21/2021 136,400.00 (G) 5.130 1.945 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 33,000.00 7,600.00 82.00 44.749 FSP
1/22/2021 124,000.00 (G) 5.130 1.768 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 33,000.00 7,600.00 82.00 40.681 FSP
Jan-21 260,400.00 (G)
Total 3.713 Total 85.430 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
EAnnual /acre Applied 0.029 0.006 1.411 0.305 0.111 0.003 0.065 0.171 0.026 3.639 103.983 Date Lbs/Ac
***** *****
Cumulative lbs/acre Applied 0.029 0.006 I 1.411 0.305 0.111 0.003 0.065 0.171 I 0.026 I 3.639
Permit PAN Limit(lbs/acre) 1st Crop! " 142
Federal C.P.L.R.(lbs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
1
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document was .repared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant penaltie or u 'ttin, false information,including the possibility of fines and impriso ent f r knowing violations."
1+ 4.0
ON' d- .F LAND APPLIER D TE
NR=Not Reported or Not Requi . *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME:SANFORD,NC WQ PERMIT#:W00000543 FIELD#:NC-CH-00077-0-0007- ACRES UTILIZED:23.4
LAND OWNER:PAUL&LUCY PRICE ANNUAL DRY TONS APPLIED:63.38 SITE#:NC CH 00077 ACRES PERMITTED:23.4
OPERATOR:PAUL&LUCY PRICE PREDOMINANT SOIL SERIES:CID LIGNUM CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:CORN SILAGE(CSI) CROP 1 MAX.PAN:224 CROP 2 NAME:MIXED COOL SEASON CROP 2 MAX.PAN:50
(_RAcc rndren)
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site !Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM - Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
4/22/2021 93,000.00 (G) 2.820 0.467 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 28.200 CSI
4/23/2021 55,800.00 (G) 2.820 0.280 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 16.920 CSI
4/26/2021 136,400.00 (G) 2.820 0.685 SBCAEDL DRY "0-c1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 41.359 CSI
4/27/2021 142,600.00 (G) 2.820 0.717 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 43.239 CSI
Apr-21 427,800.00 (G)
10/7/2021 12,400.00 (G) 2.810 0.062 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 3.103 MCSG
10/8/2021 6,200.00 (G) 2.810 0.031 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 1.552 MCSG
10/25/2021 93,000.00 (G) 2.810 0.466 SBCAEDL DRY "O-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 23.276 MCSG
Oct-21 111,600.00 (G)
Total 2.708 Total 129.718 27.931
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.048 0.012 2.925 0.498 0.194 0.005 0.119 0.320 0.034 7.043 210.674 Date Lbs/Ac
Cumulative lbs/acre Applied 0.128 0.037 8.118 1.647 0.528 0.010 0.336 (1964 0.096 18.338
Permit PAN Limit(Ibs/acre) 1st Crop 224
2nd Crop,
50
(lbs/acre)***" 366 348 13390 2
,Federal C.P.L.R. Ibs/acre*'** . . , . 67.9 15.0 375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are signifies • f• s i mating false information,including the possibility of fines and imprison ent fo knowing violations."
l‘f U2z
'II TURE OF LAND APPLIER DA E
NR=Not Reported or Not ired *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
*` Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CIi-00077-0-0008-A ACRES UTILIZED:12.4
LAND OWNER:PAUL&LUCY PRICE ANNUAL DRY TONS APPLIED:22.60 SITE#:NC CH 00077 ACRES PERMITTED:12.4
OPERATOR:PAUL&LUCY PRICE PREDOMINANT SOIL SERIES:NANFORD BADIN CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:CORN SILAGE(CSI) CROP 1 MAX.PAN:231 CROP 2 NAME: CROP 2 MAX,PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site __. - Name of Crop Type
or Cubic Yards(Y) Cond. Precip Vorati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre) Application
Month Amount UOM t Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
5/1/2021 31,000.00 (G) 2.820 0.294 SBCAEDL DRY 0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 17.738 CSI
5/2/2021 136,400.00 (G) 2.820 1.294 SBCAEDL DRY 0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 78.049 CSI
5/3/2021 24,800.006 (G) 2.820 0.235 SBCAEDL DRY 0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 14.191 CSI
May-21 192,20 .00 (G)
Total 1.823 Total 109.978 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual Ibs/acre Applied 0.034 0.008 . 1.969 0.365 0,135 0.003 0.080 0.226 0.019 4.739 131.235 Date Lbs/Ac
**.** *****
Cumulative Ibs/acre Applied 0.034 0.008 1.969 0.365 0.135 0.003 0.080 0.226 0.019 4.739
Permit PAN Limit(lbs/acre) 1st Crop -
23.1
'FederalC.P.L.R.(Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 N' 375.0 89.0 2,500.0 1
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document w:s prepared under my direction or supervision in accordance with a system esigned to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant pen re f ubmi g false information,including the possibility of fines and impriso ent f knowing violations."
2_ r�f ZvZZ
SIGNA ka OF LAND APPLIER D E
NR=Not Reported or Not Repoli',. . *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00077-0-0008-B ACRES UTILIZED:19.3
LAND OWNER:PAUL&LUCY PRICE ANNUAL DRY TONS APPLIED:87.26 SITE#:NC CH 00077 ACRES PERMITTED:19.3
OPERATOR:PAUL&LUCY PRICE PREDOMINANT SOIL SERIES:NANFORD BADIN CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:135 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site ,
Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) °!o Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry TonslAc Source Moist Inches Method* Rate** J Rate*** mg/kg mg/kg mg/kg I Crop 1 1 Crop 2 Crop 1 Crop 2
1/23/2021 186,000.00 (G) 5.130 ' 2.062 SBCAEDL DRY 0-<1/2" SUR 0.5 III 0.30 33,000.00 7,600.00 82.00 47.426 FSP
1/24/2021 24,800.00 (G) 5.130 0.275 SBCAEDL DRY 0-<112" SUR 0.5 0.30 33,000.00 7,600.00 82.00 6.323 FSP
Jan-21 210,800.00 (G)
4/7/2021 105,400.00 (G) 5.130 1.168 SBCAEDL DRY 0-<1/2" SUR 0.5 0.30 33,000.00 7,600.00 82.00 26.874 FSP
4/8/2021 37,200.00 (G) 5.130 0.412 SBCAEDL DRY 0-<112" SUR 0.5 0.30 33,000.00 7,600.00 82.00 9.485 FSP
4/28/2021 99,200.00 (G) 2.820 0.604 SBCAEDL DRY 0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 36.470 FSP
Apr-21 241,800.00 (G)
Total 4.521 Total 126.578 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.042 0.008 2.141 0.442 0.162 0.004 0.095 0.255 0.034 5.410 153.197 Date Lbs/Ac
Cumulative lbs/acre Applied 0.042 I 0.008J 2.141 0.442 0.162 0.004 0.095 1 0.255 0.034 5.410
!Permit PAN Limit(lbs/acre) 1st Crop
135
Federal ( ) 1,339.0 267.9 15.0 375.0 89.0 2,500.0
SBCAEDL.:=::-SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document w prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant penal' s o bmitt' g false information,including the possibility of fines and impriso nt f r knowing violations."
if - u--
SIG E F LANDAPPLIER D TE
NR=Not Reported or Not Rep 'red *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00077-0-0009- ACRES UTILIZED:21.2
LAND OWNER:PAUL&LUCY PRICE ANNUAL DRY TONS APPLIED:116.72 SITE#:NC CH 00077 ACRES PERMITTED:21.2
OPERATOR:PAUL&LUCY PRICE PREDOMINANT SOIL SERIES:CID SILT LOAM CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:134 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
4/8/2021 55,800.00 (G) 5.130 0.563 SBCAEDL DRY "0-<112" SUR 0.5 0.30 33,000.00 7,600.00 82.00 12.953 FSP
4/9/2021 86,800.00 (G) 5.130 0.876 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 33,000.00 7,600.00 82.00 20.148 FSP
4/12/2021 111,600.00 (G) 5.130 1.126 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 33,000.00 7,600.00 82.00 25.905 FSP
4/13/2021 161,200.00 (G) 5.130 1.627 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 33,000.00 7,600.00 82.00 37.418 FSP
4/14/2021 86,800.00 (G) 5.130 0.876 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 33,000.00 7,600.00 82.00 20.148 FSP
4/15/2021 43,400.00 (G) 5.130 0.438 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 33,000.00 7,600.00 82.00 1 10.074 FSP
Apr-21 545,600.00 (G)
Total 5.506 Total 126.646 0.000
AS CD algallIMISIIIIMI HG MO Mal SE ZN Line Applied
Annual lbs/acre Applied 0.043 0.008 2.092 0.451 0.165 0.004 0.096 0.253 0.039 5.395 MICIIIIIIIIIIIIII Date Lbs/Ac
Cumulative lbs/acre Applied 0.043 0.008 I 2.092 0.451 0.165 0.004 0.096 0.253 0.039 5.395
Permit PAN Limit(lbs/acre) 1st Crop
.
134
Federal C.P.L.R.(lbs/acre)**** 36.6 I. 34.8 1 1,339.0 267.9 15.0 375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document w prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant penalt' for itt' g false information,including the possibility of fines and impriso ent or knowing violations,"
- Z I` 2- 22_,
SIGNA OF LAND APPLIER TE
NR=Not Reported or Not Requir d *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00077-0-0012- ACRES UTILIZED:14.4
LAND OWNER:PAUL&LUCY PRICE ANNUAL DRY TONS APPLIED:26.15 SITE#:NC CH 00077 ACRES PERMITTED:14.4
OPERATOR:PAUL&LUCY PRICE PREDOMINANT SOIL SERIES:CID SILT LOAM CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:133 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site
Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (Ibs/acre' Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
11/9/2021 68,200.00 (G) 2.810 0.555 SBCAEDL DRY "0-<1/2" 1 SUR 0.5 0.30 72,000.00 14,000.00 590.00 27.737 FSP
11/10/2021 31,000.00 (G) 2.810 0.252 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 12.608 FSP
11/11/2021 124,000.00 (G) 2.810 1.009 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 50.431 FSP
Nov-21 223,200.00 (G)
Total 1.816 Total 90.776 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.028 0.009 1.962 0.222 0.113 0.002 0.080 0.174 0.036 4.722 181.624 Date Lbs/Ac
Cumulative Ibs/acre Applied 0.034 0.011 I 2.420 J 0.360 0.141 I 0.003 0.102 1 0.239 0.041 5.693
Permit PAN Limit(lbs/acre) 1st Crop 133
Federal C.P.L.R.(Ibs/acre)**** 36.6 34.8 1,339.0 267.9 I 15.0 ,.! 375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document as prepared under my direction or supervision in accordance with a syste designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant pena ' fo mi 'ng false information,including the possibility of fines and impriso ent r knowing violations."
1 Z�ZZ
SI E OF LAND APPLIER TE
* NR=Not Reported or Not Rey' -. *** Mineralize ion Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CFI-00077-0-0013- ACRES UTILIZED:15.4
LAND OWNER:PAUL&LUCY PRICE ANNUAL DRY TONS APPLIED:21.80 SITE#:NC CH 00077 ACRES PERMITTED:15.4
OPERATOR:PAUL&LUCY PRICE PREDOMINANT SOIL SERIES:CID SILT LOAM CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:FESCUE PASTURE(FSP) CROP 1 MAX.PAN:133 CROP 2 NAME: CROP 2 MAX.PAN:
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type
or Cubic Yards(Y) Cond. Precip Volati- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
11/15/2021 74,400.00 (G) 2.810 0.566 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 28.294 FSP
11/16/2021 111,600.00 (G) 2.810 0.849 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 42.441 FSP
Nov-21 186,000.00 (G)
Total 1.415 Total 70.735 0.000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.022 0.007 1.528 0.173 0.088 0.002 0.062 0.136 0.028 3.680 141.525 Date Lbs/Ac
**.** ****.
1Cumulative lbs/acre Applied 0.067 0.017 4.302 0.772 0.264 0.005 0.176 0.426 0.083 9.983
Permit PAN Limit(lbs/acre) 1st Crop
133
Federal C.P.L.R.(lbs/acre)**** 3,6.6 I 34.8 f 1,339.0 I 267.9 15.0 375.0 89.0 2,500.0�
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTP AEROB.DIG.LIQUID
"I certify,under penalty of law,that this document wa prepared under my direction or supervision in accordance with a system esigned to assure that qualified personnel properly gathered and evaluated the information submitted.lam
aware that there are significant penalz
fo 7tti g false information,including the possibility of fines and imprison ent f knowing violations."
I`f ZoZ2N U OF LAND APPLIER D E
NR=Not Reported or Not Requi *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
* Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:1/26/2022
DENR FORM FSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page:1
FACILITY NAME:SANFORD,NC WQ PERMIT#:WQ0000543 FIELD#:NC-CH-00077-0-0016- ACRES UTILIZED:30.3
LAND OWNER:PAUL&LUCY PRICE ANNUAL DRY TONS APPLIED:40.78 SITE#:NC CH 00077 ACRES PERMITTED 30.3
OPERATOR:PAUL&LUCY PRICE PREDOMINANT SOIL SERIES:CID LIGNUM CATION EXCHANGE CAPACITY(NON-503):
CROP 1 NAME:CORN SILAGE(CSI) CROP 1 MAX,PAN:224 CROP 2 NAME:SORGHUM GRAIN(SGR) CROP 2 MAX.PAN:50
RESIDUAL SOURCE(S):*See list at bottom of report
Gallons(G) Site Name of Crop Type--
or Cubic Yards(Y) Cond. Precip Valet- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Date or or Wet Tons(W) % Residual Dry,Wet, Past 24 Hrs. Application lization ization TKN Nitrogen and Nitrite (lbs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method* Rate** Rate*** mg/kg mg/kg rig/kg Crop 1 Crop 2 Crop 1 Crop 2
5/12/2021 18,600.00 (G) 2.820 0.072 SBCAEDL DRY "0-<1/2" 1 SUR 0.5 0.30 87,000.00 20,000.00 69.00 4.356 CSI
5/14/2021 167,400.00 (G) 2.820 0.650 SBCAEDL DRY "0-<1/2" i SUR 0.5 0.30 87,000.00 20,000.00 69.00 39.200 CSI
5/15/2021 37,200.00 (G) 2.820 0.144 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 87,000.00 20,000.00 69.00 8.711 CSI
May-21 223,200.00 (G)
11/1/2021 124,000.00 (G) 2.810 0.480 SBCAEDL DRY "0-<1/2" SUR 0.5 0.30 72,000.00 14,000.00 590.00 23.967 SGR
Nov-21 124,000.00 (G)
Total 1.346 Total 52.267 23.967
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Annual lbs/acre Applied 0.023 0.006 1.453 0.232 0.094 0.002 0.059 0.153 0.019 3.499 110.323 Date Lbs/Ac
Cumulative lbs/acre Applied 0.116 0.035 7.458 1.570 0.481 0.008 0.309 0.905 0.090 1 16.558
Permit PAN Limit Ohs/acre) 1st Crop 224
2nd Crop;
50
_ . 1 ..Federal C.P.LR.(Ibs/acre)**** 36.6 34.8 1,339.0111.11111=11 15.0 375.0 89.0 2,500.0
SBCAEDL=SANFORD,NC BUFFALO CREEK WWTPAEROB.DIG.LIQUID
"I certify,under penalty of law,that this document as prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant penal' f sub ',' g false information,including the possibility of fines and imprisonm nt fo knowing violations."
/ 2- f`{ 2°ZZ
SI e if OF LAND APPLIER D E
* NR=Not Reported or Not Req *** Mineralization Rates:Compost-0.1,Anaerobically digested-0.2,Aerobically digested-0.3,Raw Sludge-0.4
Application Method:SUR-Surface,INJ-Injection,SURIN-Incorporation **** C.P.L.R.:Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH&Lime Application Records Section of Report
Printed:2/4/2022 DENR FORM FSF(12/2006)

SECTION 4

S
a i' Summit Environmental Technologies,Inc.
inIrg 3310 Win St.
ENVIRONMENTAL TECHNO LOCiES,INC Cuyahoga Falls,Ohio 44223
rralyt�cal L9boraIi rlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com
January 13,2021
Alex Fox
Synagro
284 Boger Rd.
Mocksville,NC 27028
TEL:
FAX:
RE: WWTP
Dear Alex Fox: Order No.: 21010192
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/6/2021 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results,please feel free to call the
laboratory.
Sincerely,
/.....?-74424f4 177��
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls,Ohio 44223
Arkansas 88-0735,California 2943,Colorado,Connecticut PH-0108,Florida NELAC E87688,Idaho OH00923,Illinois 200061,Indiana C-OH-13,Kansas
E-10347,Kentucky(Underground Storage Tank)3,Kentucky 90146,Maryland 339,Michigan 9988,Minnesota 1780279,Nevada OH009232020-1,New
Hampshire 2996,New Jersey OH006,New York 11777,North Carolina 39705 and 631,North Dakota R-201,Ohio DW,Ohio VAP CL0052,Oklahoma
2019-155,Oregon OH200001, Pennsylvania 011,Rhode Island LA000317,South Carolina 92016001,Texas T104704466-19-16,Utah OH009232020-12,
Virginia VELAP 10381,West Virginia 9957C
Page 1 of 37

5 M�'� Summit Environmental Technologies,Inc. Case Narrative
mu 331 Ohio Wm St.
AnalENVIRONMENTAL calLaoraloriNO LOGI ,INC. Cuyahoga Falls, 44223 WO#: 21010192rrafyt�caf iaboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com Date: 1/13/2021
CLIENT: Synagro
Project: WWTP
WorkOrder Narrative:
21010192: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain-of-Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Original
Page 2 of 37

•
17 S
Mm iT Summit Environmental Techno3310Wlogies,Ins
Qualifiers and Acronyms
EkiwllxsStJM@N1'nLTecriw❑LOG{ES.INC Cuyahoga Falls,Ohio 442 WO#: 21010192
4rraly0cal Laboralorlas TEL:[phone] FAX. [phone]E
Website:http://www.settek.co Date: 1/13/2021
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25%difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low(-)or high(+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low(-)or high(+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low(-)or high(+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low(-)or high(+).
S The spike result was outside of accepted recovery limits.
Z Deviation;A deviation from the method was performed;Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 37

S t�' Summit Environmental Technologies,Inc. Workorder
I'll3310 Win St.
111 MI ENVIRONMENTAL TECHNQI. oiEs,iric, Cuyahoga Falls,Ohio 44223 Sample Summary
4rralyt�cai iaboralorlas TEL:[phone] FAX [phone] WO#: 21010192
Website:http://www.settek.com 13-Jan-21
CLIENT: Synagro
Project: WWTP
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
21010192-001 Sanford WWTP 1/5/2021 1:00:00 PM 1/6/2021 11:10:00 AM Sludge
Page 4 of 37

SUMMIT
Summit Environmental Technologies,Inc. DATES REPORT
MN 33hi Win St.
Anal Neat La oratorL iNO LOi,I S,INC Cuyahoga Falls, Ohio 44223 WO#: 21010192
�a�}lkai iaboralorlas TEL:[phone] FAX:[phone]
Website:http://www.settekcom 13-Jan-21
Client: Synagro
Project: WWTP
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
21010192-001A Sanford WWTP 1/5/2021 1:00:00 PM Sludge Ignitability of Solids(SW-846: 1030) 1/13/2021 11:15:56 AM
Percent Solids by SM2540Mod 1/12/2021 10:05:00 AM
pH(SW9045D) 1/7/2021 11:00:00 AM
Reactive Cyanide(9014/7.3.3.2)-Solid 1/7/2021 4:50:00 PM
Reactive Sulfide(9034)/7.3.4.2 1/7/2021 4:50:00 PM
TCLP Herbicides by EPA 8321B 1/9/2021 9:33:00 PM
TCLP Mercury Analysis(SW1311/7471/7/2021 3:30:00 PM 1/11/2021 10:05:00 AM 1/11/2021 2:02:00 PM
TCLP Metals Analysis(SW1311/6010:1/7/2021 3:30:00 PM 1/8/2021 10:25:00 AM 1/11/2021 12:00:29 PM
TCLP Pesticides Analysis(SW1311/8(1/7/2021 3:30:00 PM 1/8/2021 12:00:00 PM 1/11/2021 11:20:00 PM
TCLP Pesticides Analysis(SW1311/8(1/7/2021 3:30:00 PM 1/8/2021 12:00:00 PM 1/11/2021 11:20:00 PM
TCLP Semi-Volatiles Analysis 1/7/2021 3:30:00 PM 1/7/2021 12:15:00 PM 1/9/2021 1:06:00 AM
(SW1311/8270)
TCLP Volatiles Analysis 1/7/2021 3:30:00 PM 1/8/2021 10:05:00 PM
Original
Page 5 of 37

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENb1R01JMENTAL TECliK10LOG1ES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 21010192
Website:http://www.settek.com Date Reported: 1/13/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/5/2021 1:00:00 PM
Lab ID: 21010192-001A
Project: WWTP
Client Sample ID Sanford WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: ERA
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND 0.00200 mg/L 1 1/11/2021 2:02:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW6010D SW3010A Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 1/11/2021 12:00:29 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 1/11/2021 12:00:29 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 1/11/2021 12:00:29 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 1/11/2021 12:00:29 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 1/11/2021 12:00:29 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 1/11/2021 12:00:29 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 1/11/2021 12:00:29 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8270 SW3510C Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.200 mg/L 2 1/9/2021 1:06:00 AM
2,4,5-Trichlorophenol ND 0.500 mg/L 2 1/9/2021 1:06:00 AM
2,4,6-Trichlorophenol ND 0.500 mg/L 2 1/9/2021 1:06:00 AM
2,4-Dinitrotoluene ND 0.100 mg/L 2 1/9/2021 1:06:00 AM
Cresols,Total ND 10.0 mg/L 2 1/9/2021 1:06:00 AM
Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 1/9/2021 1:06:00 AM
Hexachlorobenzene ND 0.100 mg/L 2 1/9/2021 1:06:00 AM
Hexachloroethane ND 0.200 mg/L 2 1/9/2021 1:06:00 AM
Nitrobenzene ND 0.200 mg/L 2 1/9/2021 1:06:00 AM
Pentachlorophenol ND 0.500 mg/L 2 1/9/2021 1:06:00 AM
Pyridine ND 0.500 mg/L 2 1/9/2021 1:06:00 AM
Surr:2-Fluorophenol 81.1 10-157 m %Rec 2 1/9/2021 1:06:00 AM
Surr: Phenol-d6 77.5 10-169 %Rec 2 1/9/2021 1:06:00 AM
Surr: Nitrobenzene-d5 85.6 32.1 -130 %Rec 2 1/9/2021 1:06:00 AM
Surr:2,4,6-Tribromophenol 102 45.4-166 %Rec 2 1/9/2021 1:06:00 AM
Surr:2-Fluorobiphenyl 86.4 35.7-130 %Rec 2 1/9/2021 1:06:00 AM
Surr:p-Terphenyl-d14 114 74.7-145 %Rec 2 1/9/2021 1:06:00 AM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 6 of 37

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECliK10LOG1ES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 21010192
Website:http://www.settek.com Date Reported: 1/13/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/5/2021 1:00:00 PM
Lab ID: 21010192-001A
Project: WWTP
Client Sample ID Sanford WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane,total ND 0.0250 mg/L 1 1/11/2021 11:20:00 PM
Toxaphene ND 0.0500 mg/L 1 1/11/2021 11:20:00 PM
Endrin ND 0.00250 mg/L 1 1/11/2021 11:20:00 PM
gamma-BHC ND 0.00250 mg/L 1 1/11/2021 11:20:00 PM
Heptachlor ND 0.00250 mg/L 1 1/11/2021 11:20:00 PM
Heptachlor epoxide ND 0.00250 mg/L 1 1/11/2021 11:20:00 PM
Methoxychlor ND 0.00250 mg/L 1 1/11/2021 11:20:00 PM
Surr:TCMX 66.0 10-119 %Rec 1 1/11/2021 11:20:00 PM
Surr: DCB 82.3 10-119 %Rec 1 1/11/2021 11:20:00 PM
TCLP HERBICIDES BY EPA 8321B SW8321A Analyst: JPG
2,4-D ND 0.500 mg/L 50 1/9/2021 9:33:00 PM
2,4,5-TP ND 0.500 mg/L 50 1/9/2021 9:33:00 PM
Surr:2,4-Dichlorophenylacetic aci 101 70-130 %Rec 50 1/9/2021 9:33:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8260 SW1311M Analyst: SLV
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.250 mg/L 50 1/8/2021 10:05:00 PM
1,2-Dichloroethane ND 0.250 mg/L 50 1/8/2021 10:05:00 PM
MEK ND 5.00 mg/L 50 1/8/2021 10:05:00 PM
Benzene ND 0.250 mg/L 50 1/8/2021 10:05:00 PM
Carbon tetrachloride ND 0.250 mg/L 50 1/8/2021 10:05:00 PM
Chlorobenzene ND 2.50 mg/L 50 1/8/2021 10:05:00 PM
Chloroform ND 0.250 mg/L 50 1/8/2021 10:05:00 PM
Tetrachloroethene ND 0.250 mg/L 50 1/8/2021 10:05:00 PM
Trichloroethene ND 0.250 mg/L 50 1/8/2021 10:05:00 PM
Vinyl chloride ND 0.100 mg/L 50 1/8/2021 10:05:00 PM
Surr:4-Bromofluorobenzene 92.4 70-130 %Rec 50 1/8/2021 10:05:00 PM
Surr: Dibromofluoromethane 105 70-130 %Rec 50 1/8/2021 10:05:00 PM
Surr:Toluene-d8 97.6 70-130 %Rec 50 1/8/2021 10:05:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 7 of 37

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENb1R01JMENTAL TECtiNOLOGIES,IN'C Cuyahoga Falls, Ohio 44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WON: 21010192
Website:http://www.settek.com Date Reported: 1/13/2021
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/5/2021 1:00:00 PM
Lab ID: 21010192-001A
Project: WWTP
Client Sample ID Sanford WWTP
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9014 Analyst: MS
REACTIVE CYANIDE(9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.495 mg/Kg 1 1/7/2021 4:50:00 PM
IGNITABILITY OF SOLIDS(SW-846: 1030) SW1030 Analyst: SEE
Ignitability nonflammable mm/sec 1 1/13/2021 11:15:56 AM
PERCENT SOLIDS BY SM2540MOD A2540B Analyst: MMA
Percent Solids 3.15 % 1 1/12/2021 10:05:00 AM
RCI SW9045D Analyst: DHC
PH (SW9045D)
pH 7.2 s.u.@19.0C 1 1/7/2021 11:00:00 AM
RCI SW9034 Analyst: MS
REACTIVE SULFIDE(9034)/7.3.4.2
Sulfide, Reactive 30.0 25.0 mg/Kg 1 1/7/2021 4:50:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 8 of 37

it SUMMIT
Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7teS RenOrt
MI ENVIRONMENTAL TECHNaLOGES,INCCuyahoga Falls,Ohio 44223 J Y
rral}'t�cai iaboralorlas TEL:[phone] FAX [phone] WO#: 21010192
Website:http://www.settek.com 13-Jan-21
Client: Synagro State: NW
Project: WWTP Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
21010192-001A Sludge Ignitability of Solids(SW-846: 1030) Ignitability A
Sludge Percent Solids by SM2540Mod Percent Solids N
Sludge pH(SW9045D) Hydrogen Ion(pH) A
Sludge Reactive Cyanide(9014/7.3.3.2)-Solid Cyanide,Reactive N
Sludge Reactive Sulfide(9034)/7.3.4.2 Sulfide,Reactive N
Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A
Sludge TCLP Herbicides by EPA 8321B 2,4-D A
Sludge TCLP Mercury Analysis(SW1311/7470) Mercury A
Sludge TCLP Metals Analysis(SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis(SW1311/6010) Barium A
Sludge TCLP Metals Analysis(SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis(SW1311/6010) Chromium A
Sludge TCLP Metals Analysis(SW1311/6010) Lead A
Sludge TCLP Metals Analysis(SW1311/6010) Selenium A
Sludge TCLP Metals Analysis(SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis(SW1311/8081) Chlordane,total A
Sludge TCLP Pesticides Analysis(SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis(SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis(SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 1,4-Dichlorobenzene N
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,5-Trichlorophenol N
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,6-Trichlorophenol N
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4-Dinitrotoluene N
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Cresols,Total N
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobenzene N
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobutadiene N
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachloroethane N
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Nitrobenzene N
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pentachlorophenol N
Key Key
NC WW SCM A Accredited NC WW SCM N Not Accredited
Original#1
Page 9 of 37

S UMM IT Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7tes Report
EN ENWIRONM@NtAL TECHN❑LociEs,i Cuyahoga Falls,Ohio 44223 Analytes
rral}'tiicaf iaboralorlas TEL:[phone] FAX [phone] WO#: 21010192
Website:http://www.settek.com 13-Jan-21
Client: Synagro State: NW
Project: WWTP Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
21010192-001A Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pyridine N
Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
Key Key
NC WW SCM A Accredited NC WW SCM N Not Accredited
Original#1
Page 10 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: 47177
Sample ID: 21010089-001AMS SampType: MS TestCode: TCLP-SVOC_ Units: mg/L Prep Date: 1/7/2021 RunNo: 122338
Client ID: BatchQC Batch ID: 47177 TestNo: SW8270 SW3510C Analysis Date: 1/8/2021 SegNo: 3149456
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene 0.676 0.200 0.8000 0 84.5 15.2 124
2,4,5-Trichlorophenol 0.788 0.500 0.8000 0 98.5 30.6 152
2,4,6-Trichlorophenol 0.805 0.500 0.8000 0 101 27.6 150
2,4-Dinitrotoluene 0.716 0.100 0.8000 0 89.6 58 141
o-Cresol 0.792 0.500 0.8000 0 99.0 26.9 132
Cresols,Total ND 10.0 1.600 1.030 91.8 27.6 132
Hexachloro-1,3-butadiene 0.649 0.0400 0.8000 0 81.1 10 156
Hexachlorobenzene 0.746 0.100 0.8000 0 93.2 54.3 142
Hexachloroethane 0.676 0.200 0.8000 0 84.5 1.92 131
Nitrobenzene 0.759 0.200 0.8000 0 94.9 21 135
Pentachlorophenol 0.832 0.500 0.8000 0 104 47.4 134
Pyridine ND 0.500 0.8000 0 16.4 10 130 mQMR
Surr:2-Fluorophenol 0.898 1.000 89.8 9.77 146
Surr: Phenol-d6 0.914 1.000 91.4 20.7 130
Surr: Nitrobenzene-d5 0.870 1.000 87.0 13.9 156
Surr:2,4,6-Tribromophenol 1.02 1.000 102 27.3 183
Surr:2-Fluorobiphenyl 0.860 1.000 86.0 21.4 153
Surr: p-Terphenyl-d14 1.10 1.000 110 54.8 154
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 11 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: 47177
Sample ID: 21010089-001AMSD SampType: MSD TestCode: TCLP-SVOC_ Units: mg/L Prep Date: 1/7/2021 RunNo: 122338
Client ID: BatchQC Batch ID: 47177 TestNo: SW8270 SW3510C Analysis Date: 1/8/2021 SegNo: 3149457
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene 0.584 0.200 0.8000 0 73.0 15.2 124 0.6760 14.5 30
2,4,5-Trichlorophenol 0.740 0.500 0.8000 0 92.5 30.6 152 0.7880 6.28 30
2,4,6-Trichlorophenol 0.745 0.500 0.8000 0 93.1 27.6 150 0.8052 7.79 30
2,4-Dinitrotoluene 0.803 0.100 0.8000 0 100 58 141 0.7164 11.4 30
o-Cresol 0.761 0.500 0.8000 0 95.2 26.9 132 0.7924 4.02 30
Cresols,Total ND 10.0 1.600 1.030 79.8 27.6 132 0 0 30
Hexachloro-1,3-butadiene 0.584 0.0400 0.8000 0 73.0 10 156 0.6488 10.4 30
Hexachlorobenzene 0.758 0.100 0.8000 0 94.8 54.3 142 0.7456 1.65 30
Hexachloroethane 0.576 0.200 0.8000 0 72.0 1.92 131 0.6760 15.9 30
Nitrobenzene 0.680 0.200 0.8000 0 85.1 21 135 0.7592 10.9 30
Pentachlorophenol 0.816 0.500 0.8000 0 102 47.4 134 0.8320 1.89 30
Pyridine ND 0.500 0.8000 0 29.2 10 130 0 0 30 Rm
Surr:2-Fluorophenol 0.748 1.000 74.8 9.77 146 0
Surr: Phenol-d6 0.824 1.000 82.4 20.7 130 0
Surr: Nitrobenzene-d5 0.832 1.000 83.2 13.9 156 0
Surr:2,4,6-Tribromophenol 1.07 1.000 107 27.3 183 0
Surr:2-Fluorobiphenyl 0.828 1.000 82.8 21.4 153 0
Surr: p-Terphenyl-d14 1.15 1.000 115 54.8 154 0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 12 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: 47177
Sample ID: MB-47177 SampType: MBLK TestCode: TCLP-SVOC_ Units: mg/L Prep Date: 1/7/2021 RunNo: 122260
Client ID: PBS Batch ID: 47177 TestNo: SW8270 SW3510C Analysis Date: 1/7/2021 SegNo: 3147025
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene ND 0.100
2,4,5-Trichlorophenol ND 0.250
2,4,6-Trichlorophenol ND 0.250
2,4-Dinitrotoluene ND 0.0500
o-Cresol ND 0.250
Cresols,Total ND 5.00
Hexachloro-1,3-butadiene ND 0.0200
Hexachlorobenzene ND 0.0500
Hexachloroethane ND 0.100
Nitrobenzene ND 0.100
Pentachlorophenol ND 0.250
Pyridine ND 0.250
Surr:2-Fluorophenol 0.856 1.000 85.6 10 109 m
Surr: Phenol-d6 0.775 1.000 77.5 10 109
Surr: Nitrobenzene-d5 0.918 1.000 91.8 19 120
Surr:2,4,6-Tribromophenol 1.03 1.000 103 10 120 m
Surr:2-Fluorobiphenyl 0.832 1.000 83.2 22 117
Surr: p-Terphenyl-d14 1.03 1.000 103 34 116
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 13 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: 47177
Sample ID: LCS-47177 SampType: LCS TestCode: TCLP-SVOC_ Units: mg/L Prep Date: 1/7/2021 RunNo: 122260
Client ID: LCSS Batch ID: 47177 TestNo: SW8270 SW3510C Analysis Date: 1/7/2021 SegNo: 3147026
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene 0.670 0.100 0.8000 0 83.8 36.4 130
2,4,5-Trichlorophenol 0.745 0.250 0.8000 0 93.2 31.7 132
2,4,6-Trichlorophenol 0.783 0.250 0.8000 0 97.8 31.1 133
2,4-Dinitrotoluene 0.829 0.0500 0.8000 0 104 43.3 130
o-Cresol 0.800 0.250 0.8000 0 100 32.9 130
Cresols,Total ND 5.00 1.600 0 98.3 31.7 130
Hexachloro-1,3-butadiene 0.620 0.0200 0.8000 0 77.4 31.4 130
Hexachlorobenzene 0.764 0.0500 0.8000 0 95.6 43.1 130
Hexachloroethane 0.643 0.100 0.8000 0 80.4 36.5 130
Nitrobenzene 0.756 0.100 0.8000 0 94.5 39.5 130
Pentachlorophenol 0.850 0.250 0.8000 0 106 34 130
Pyridine 0.285 0.250 0.8000 0 35.6 10 130 m
Surr:2-Fluorophenol 0.982 1.000 98.2 17.1 130 m
Surr: Phenol-d6 0.911 1.000 91.1 10 130
Surr: Nitrobenzene-d5 0.897 1.000 89.7 32.6 130
Surr:2,4,6-Tribromophenol 1.09 1.000 109 4.43 130
Surr:2-Fluorobiphenyl 0.945 1.000 94.5 41.8 130
Surr: p-Terphenyl-d14 1.08 1.000 108 36.4 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 14 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: 47188
Sample ID: MB-47188 SampType: MBLK TestCode: TCLP-VOC-M Units: mg/L Prep Date: 1/7/2021 RunNo: 122301
Client ID: PBS Batch ID: 47188 TestNo: SW8260 SW1311M Analysis Date: 1/8/2021 SegNo: 3148165
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,1-Dichloroethene ND 0.250
1,2-Dichloroethane ND 0.250
MEK ND 5.00
Benzene ND 0.250
Carbon tetrachloride ND 0.250
Chlorobenzene ND 2.50
Chloroform ND 0.250
Tetrachloroethene ND 0.250
Trichloroethene ND 0.250
Vinyl chloride ND 0.100
Surr:4-Bromofluorobenzene 2280 2500 91.0 70 130
Surr: Dibromofluoromethane 2640 2500 106 70 130
Surr:Toluene-d8 2490 2500 99.4 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 15 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: 47205
Sample ID: 21010092-001ams SampType: MS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 1/8/2021 RunNo: 122365
Client ID: BatchQC Batch ID: 47205 TestNo: SW8081 SW3510C Analysis Date: 1/11/2021 SegNo: 3150630
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Endrin 0.00799 0.000500 0.0100 0 79.9 10 224 m
Methoxychlor 0.0100 0.000500 0.0100 0 100 10 251
Sample ID: 21010092-001amsd SampType: MSD TestCode: TCLP-SVOC- Units: mg/L Prep Date: 1/8/2021 RunNo: 122365
Client ID: BatchQC Batch ID: 47205 TestNo: SW8081 SW3510C Analysis Date: 1/11/2021 SegNo: 3150631
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Endrin 0.00746 0.000500 0.0100 0 74.6 10 224 0.00799 6.93 30 m
Methoxychlor 0.00896 0.000500 0.0100 0 89.6 10 251 0.0100 11.0 30
Sample ID: LCS-47205 SampType: LCS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 1/8/2021 RunNo: 122365
Client ID: LCSS Batch ID: 47205 TestNo: SW8081 SW3510C Analysis Date: 1/11/2021 SegNo: 3150641
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Endrin 0.00659 0.000500 0.0100 0 65.9 10 130 m
Methoxychlor 0.00925 0.000500 0.0100 0 92.5 10 178
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 16 of 37

U��' Summit Environmental Technologies,Inc. QC SUMMARY REPORT
OM5 T 33hi Win St.
ENVIRONMENTAL rmy' 'LaboTtorfas LOi,I S,INC Cuyahoga Falls, Ohio 44223 WO#: 21010192�a�}'t�caf iaboralorlas TEL:[phone] FAX:[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: 47205
Sample ID: MB-47205 SampType: MBLK TestCode: TCLP-SVOC- Units: mg/L Prep Date: 1/8/2021 RunNo: 122365
Client ID: PBS Batch ID: 47205 TestNo: SW8081 SW3510C Analysis Date: 1/11/2021 SegNo: 3150643
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Endrin ND 0.000500
Methoxychlor ND 0.000500
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 17 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: 47205
Sample ID: 21010092-001ams SampType: MS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 1/8/2021 RunNo: 122364
Client ID: BatchQC Batch ID: 47205 TestNo: SW8081 SW3510C Analysis Date: 1/11/2021 SegNo: 3150607
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
gamma-BHC 0.00840 0.000500 0.0100 0 84.0 10 192 P
Heptachlor 0.00895 0.000500 0.0100 0 89.5 10 197 P
Heptachlor epoxide 0.00964 0.000500 0.0100 0 96.4 10 208 P
Surr:TCMX 14.5 20.00 72.5 10 157 P
Surr: DCB 17.4 20.00 87.0 10 194 P
Sample ID: 21010092-001amsd SampType: MSD TestCode: TCLP-SVOC- Units: mg/L Prep Date: 1/8/2021 RunNo: 122364
Client ID: BatchQC Batch ID: 47205 TestNo: SW8081 SW3510C Analysis Date: 1/11/2021 SegNo: 3150608
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
gamma-BHC 0.00769 0.000500 0.0100 0 76.9 10 192 0.00840 8.85 30 P
Heptachlor 0.00812 0.000500 0.0100 0 81.2 10 197 0.00895 9.75 30 P
Heptachlor epoxide 0.00867 0.000500 0.0100 0 86.7 10 208 0.00964 10.7 30 P
Surr:TCMX 13.2 20.00 66.0 10 157 0 P
Surr: DCB 15.6 20.00 78.1 10 194 0 P
Sample ID: LCS-47205 SampType: LCS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 1/8/2021 RunNo: 122364
Client ID: LCSS Batch ID: 47205 TestNo: SW8081 SW3510C Analysis Date: 1/11/2021 SegNo: 3150618
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 18 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: 47205
Sample ID: LCS-47205 SampType: LCS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 1/8/2021 RunNo: 122364
Client ID: LCSS Batch ID: 47205 TestNo: SW8081 SW3510C Analysis Date: 1/11/2021 SegNo: 3150618
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
gamma-BHC 0.00848 0.000500 0.0100 0 84.8 10 130
Heptachlor 0.00899 0.000500 0.0100 0 89.9 10 130
Heptachlor epoxide 0.00953 0.000500 0.0100 0 95.3 10 130
Surr:TCMX 14.2 20.00 71.1 10 130
Surr: DCB 17.4 20.00 87.0 10 130
Sample ID: MB-47205 SampType: MBLK TestCode: TCLP-SVOC- Units: mg/L Prep Date: 1/8/2021 RunNo: 122364
Client ID: PBS Batch ID: 47205 TestNo: SW8081 SW3510C Analysis Date: 1/11/2021 SegNo: 3150620
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Chlordane,total ND 0.00250
Toxaphene ND 0.00500
gamma-BHC ND 0.000500
Heptachlor ND 0.000500
Heptachlor epoxide ND 0.000500
Surr:TCMX 13.2 20.00 65.9 10 119
Surr: DCB 16.7 20.00 83.3 10 119
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 19 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: 47220
Sample ID: MB-47220 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM Prep Date: 1/11/2021 RunNo: 122334
Client ID: PBS Batch ID: 47220 TestNo: SW7470A SW7470A Analysis Date: 1/11/2021 SegNo: 3149401
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID: LCS-47220 SampType: LCS TestCode: HG_TCLP(74 Units: PPM Prep Date: 1/11/2021 RunNo: 122334
Client ID: LCSS Batch ID: 47220 TestNo: SW7470A SW7470A Analysis Date: 1/11/2021 SegNo: 3149402
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury 0.00410 0.00200 0.00400 0 103 80 120
Sample ID: 21010240-001AMS SampType: MS TestCode: HG_TCLP(74 Units: PPM Prep Date: 1/11/2021 RunNo: 122334
Client ID: BatchQC Batch ID: 47220 TestNo: SW7470A SW7470A Analysis Date: 1/11/2021 SegNo: 3149407
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury 0.00448 0.00200 0.00400 0.000395 102 75 125
Sample ID: 21010240-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 1/11/2021 RunNo: 122334
Client ID: BatchQC Batch ID: 47220 TestNo: SW7470A SW7470A Analysis Date: 1/11/2021 SegNo: 3149408
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury 0.00451 0.00200 0.00400 0.000395 103 75 125 0.00448 0.667 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 20 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: 47220
Sample ID: 21010240-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 1/11/2021 RunNo: 122334
Client ID: BatchQC Batch ID: 47220 TestNo: SW7470A SW7470A Analysis Date: 1/11/2021 SegNo: 3149408
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sample ID: TCLP Blank1 1-8-21 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM Prep Date: 1/11/2021 RunNo: 122334
Client ID: PBS Batch ID: 47220 TestNo: SW7470A SW7470A Analysis Date: 1/11/2021 SegNo: 3149412
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 21 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122210
Sample ID: LCS-R122210 SampType: LCS TestCode: pH_NPW(450 Units: s.u.@20.4C Prep Date: RunNo: 122210
Client ID: LCSW Batch ID: R122210 TestNo: SW9045D Analysis Date: 1/7/2021 SegNo: 3145887
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Sample ID: 21010146-001ADUP SampType: DUP TestCode: pH_NPW(450 Units: s.u.@21.2C Prep Date: RunNo: 122210
Client ID: BatchQC Batch ID: R122210 TestNo: SW9045D Analysis Date: 1/7/2021 SegNo: 3145889
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH 6.0 6.0 0 5 H
Sample ID: PH 7 CHECK SampType: LCS TestCode: PH_NPW(450 Units: s.u.@20.1C Prep Date: RunNo: 122210
Client ID: LCSW Batch ID: R122210 TestNo: SW9045D Analysis Date: 1/7/2021 SegNo: 3145893
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Sample ID: PH 7 CHECK SampType: LCS TestCode: PH_NPW(450 Units: s.u.@19.2C Prep Date: RunNo: 122210
Client ID: LCSW Batch ID: R122210 TestNo: SW9045D Analysis Date: 1/7/2021 SegNo: 3146033
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH 7.0 7.0 0 99.6 98.6 101.4
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 22 of 37

U��' Summit Environmental Technologies,Inc. QC SUMMARY REPORT
OM5 T 33hi Win St.
ENVIRONMENTAL rmy' 'LaboTtorfas LOi,I S,INC Cuyahoga Falls, Ohio 44223 WO#: 21010192�a�}'t�caf iaboralorlas TEL:[phone] FAX:[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122210
Sample ID: PH 7 CHECK SampType: LCS TestCode: PH_NPW(450 Units: s.u.@19.2C Prep Date: RunNo: 122210
Client ID: LCSW Batch ID: R122210 TestNo: SW9045D Analysis Date: 1/7/2021 SegNo: 3146033
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 23 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122266
Sample ID: 21010091-001AMS SampType: MS TestCode: Sulfide,React Units: mg/Kg Prep Date: RunNo: 122266
Client ID: BatchQC Batch ID: R122266 TestNo: SW9034 Analysis Date: 1/7/2021 SegNo: 3147244
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive 2980 25.0 3010 40.00 97.7 80 120
Sample ID: 21010091-001AMSD SampType: MSD TestCode: Sulfide,React Units: mg/Kg Prep Date: RunNo: 122266
Client ID: BatchQC Batch ID: R122266 TestNo: SW9034 Analysis Date: 1/7/2021 SegNo: 3147245
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive 2940 25.0 3010 40.00 96.3 80 120 2980 1.35 30
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 24 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122266
Sample ID: MB-R122266 SampType: MBLK TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 122266
Client ID: PBW Batch ID: R122266 TestNo: SW9034 Analysis Date: 1/7/2021 SegNo: 3147220
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-R122266 SampType: LCS TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 122266
Client ID: LCSW Batch ID: R122266 TestNo: SW9034 Analysis Date: 1/7/2021 SegNo: 3147221
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive 2880 25.0 3010 0 95.7 85 115
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 25 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
AnalENVIRONMENTAL catLabratorf NO LOi,I S,IF1C Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122270
Sample ID: 21010091-001AMS SampType: MS TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 122270
Client ID: BatchQC Batch ID: R122270 TestNo: SW9014 Analysis Date: 1/7/2021 SegNo: 3147444
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive 9.63 0.490 10.00 0 96.3 75 125
Sample ID: 21010091-001AMSD SampType: MSD TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 122270
Client ID: BatchQC Batch ID: R122270 TestNo: SW9014 Analysis Date: 1/7/2021 SegNo: 3147445
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive 9.49 0.485 10.00 0 94.9 75 125 9.628 1.39 10
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 26 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
Anal ON M cat Lab ratorf NO LOi,I S,IF1C Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122270
Sample ID: Blank SampType: MBLK TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 122270
Client ID: PBW Batch ID: R122270 TestNo: SW9014 Analysis Date: 1/7/2021 SegNo: 3147429
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive ND 0.495
Sample ID: LCS SampType: LCS TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 122270
Client ID: LCSW Batch ID: R122270 TestNo: SW9014 Analysis Date: 1/7/2021 SegNo: 3147430
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive 9.46 0.495 10.00 0 94.6 85 115
Sample ID: RLCheck SampType: RLC TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 122270
Client ID: BatchQC Batch ID: R122270 TestNo: SW9014 Analysis Date: 1/7/2021 SegNo: 3147432
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive ND 0.485 0.5000 0 77.2 65 135
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 27 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122312
Sample ID: MB SampType: MBLK TestCode: TCLP-SVOC- Units: mg/L Prep Date: RunNo: 122312
Client ID: PBS Batch ID: R122312 TestNo: SW8321A Analysis Date: 1/8/2021 SegNo: 3148878
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D ND 0.0100
2,4,5-TP ND 0.0100
Surr:2,4-Dichlorophenylacetic acid 1.03 1.000 103 70 130
Sample ID: LCS SampType: LCS TestCode: TCLP-SVOC- Units: mg/L Prep Date: RunNo: 122312
Client ID: LCSS Batch ID: R122312 TestNo: SW8321A Analysis Date: 1/8/2021 SegNo: 3148879
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D 0.357 0.0100 0.3000 0 119 60.5 141
2,4,5-TP 0.304 0.0100 0.3000 0 102 68.3 144
Surr:2,4-Dichlorophenylacetic acid 3.01 3.000 100 70 130
Sample ID: LCSD SampType: LCSD TestCode: TCLP-SVOC- Units: mg/L Prep Date: RunNo: 122312
Client ID: LCSS02 Batch ID: R122312 TestNo: SW8321A Analysis Date: 1/8/2021 SegNo: 3148880
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D 0.287 0.0100 0.3000 0 95.6 60.5 141 0.3571 21.8 30
2,4,5-TP 0.249 0.0100 0.3000 0 82.9 68.3 144 0.3045 20.2 30
Surr:2,4-Dichlorophenylacetic acid 2.44 3.000 81.5 70 130 0 0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 28 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122312
Sample ID: 21010089-001AMS SampType: MS TestCode: TCLP-SVOC- Units: mg/L Prep Date: RunNo: 122312
Client ID: BatchQC Batch ID: R122312 TestNo: SW8321A Analysis Date: 1/8/2021 SegNo: 3148881
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D 16.9 0.500 15.00 0 112 60.5 141
2,4,5-TP 14.4 0.500 15.00 0 96.2 68.3 144
Surr:2,4-Dichlorophenylacetic acid 143 150.0 95.0 70 130
Sample ID: 21010089-001AMSD SampType: MSD TestCode: TCLP-SVOC- Units: mg/L Prep Date: RunNo: 122312
Client ID: BatchQC Batch ID: R122312 TestNo: SW8321A Analysis Date: 1/8/2021 SegNo: 3148882
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D 17.9 0.500 15.00 0 119 60.5 141 16.87 5.67 30
2,4,5-TP 15.4 0.500 15.00 0 102 68.3 144 14.43 6.28 30
Surr:2,4-Dichlorophenylacetic acid 151 150.0 101 70 130 0 0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 29 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122377
Sample ID: MB-R122377 SampType: MBLK TestCode: PctSolid_S(2 Units: % Prep Date: RunNo: 122377
Client ID: PBS Batch ID: R122377 TestNo: A2540B Analysis Date: 1/12/2021 SegNo: 3151031
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Percent Solids ND 0 0
Sample ID: 21010161-001ADUP SampType: DUP TestCode: PctSolid_S(2 Units: % Prep Date: RunNo: 122377
Client ID: BatchQC Batch ID: R122377 TestNo: A2540B Analysis Date: 1/12/2021 SegNo: 3151033
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Percent Solids 10.6 0 0 9.965 6.15 5 R
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 30 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,IF1C Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122408
Sample ID: LCS-R122408 SampType: LCS TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: LCSS Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152374
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability 6.87 7.240 0 94.9 70 130
Sample ID: 21010307-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152376
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability <2.2 0 0 20
Sample ID: 21010307-002ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152379
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability <2.2 0 0 20
Sample ID: 21010307-003ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152382
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 31 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,IF1C Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122408
Sample ID: 21010307-003ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152382
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sample ID: 21010307-004ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152384
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Sample ID: 21010307-005ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152386
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Sample ID: 21010307-006ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152388
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability <2.2 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 32 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122408
Sample ID: 21010307-008ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152394
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability <2.2 0 0 20
Sample ID: 21010307-009ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152397
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability <2.2 0 0 20
Sample ID: 21010307-010ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152400
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability <2.2 0 0 20
Sample ID: 21010192-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: Sanford WWTP Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152403
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 33 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,IF1C Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122408
Sample ID: 21010192-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: Sanford WWTP Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152403
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sample ID: 21010278-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152405
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Sample ID: 21010279-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152407
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Sample ID: 21010280-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152409
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 34 of 37

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' 'LaboTtorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 21010192
4na/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 13-Jan-21
Client: Synagro
Project: WWTP BatchlD: R122408
Sample ID: 21010359-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152411
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Sample ID: 21010360-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 122408
Client ID: BatchQC Batch ID: R122408 TestNo: SW1030 Analysis Date: 1/13/2021 SegNo: 3152413
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 35 of 37

i Summit Environmental Technologies, Inc, Analysis Request/Chain of Custody
i 3310 Win Street
Cuyahoga Falls,Ohio 44223 Tel:330,253.8211 Fax: [phone] For Summit Environmental Technologies,Inncc.use only
Page
Company Name (Please Print) Project{`fame f �_1 � f a8T Na ,
reGkr rci Vv yy1-�)� Analytical P eters and Methods 1
_ !
Company Address Project Address s 1 - -
art-
L J 1 I
� � x - Pi bckvilleeP c.rily' i it i " #
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Client Phone No. 33 1*` 1
(p eto q 6(a2-7 Report to T - .0
Client not N . fi Rmt hF[ 0POOs I •
If .z;
' Client ambit Please Email lRraults J ( Quoit No. g
C.rvVhrtcWS-1rutn-cogq _ -
Contact Pelson, `� rr�+ y
K S W rt+tiL It
Sampled by a kr-, 1 K k c Check if Ohio VA?samples,r ❑ ilf 1 R] E ,1 VI
_ 1" I"
# Sample Identification
a 1 1
Collected Collected a I x vs c z 14-
Fir.arch Box of
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j 4CW/4n:4 MAITP 1 424 ' I:C. eel x .sL x i A
. �.
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■ I Mil
-
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I�dl ed bp: time ; �oeked by: Dar Nai&comments: /+ T
Cliris rut [ i i far $DR vi�Pi 1,Lid7_,__yq v
J �0 _ [FkTIF'w'1.770N xfU NO
kLPofT•roS1At'E(DWOM- ES No
ved _` �{� r� If 34.S,plem pens PWS.STU,h MP
V in lab hY: bale Time
Requested
By: mai be approved "1.bun,n Ill...MI,Ent.
Rush ii� uesgcd _ �} I. (` 4' •WIFY,n FYl9 L%ahlc.,u
^ ti.. q Dale by lab manager y � � y_ - .,,aV[yR.v1 FOL.iVAlili li, i„ A
CO 4./ lAll L q
CD Whitt and yellow pages should acc«nputy samples w the laboratory.The client r -ns pin page. ~� 3
W IG
o Page 1 of 1
CO

;74700,1summIT Summit Environmental Techn3310ologiesW,in Inc.St.
II a
ENVIRONMENTAL TECliNOL4GaS.INC Cuyahoga Falls, Ohio 44223 Sample Log-In Check List
ArrafyOcaf Laborator/as TEL:[phone] FAX. [phone]
Website:http:/Aiww.settek.com
Client Name: SYN-NC-27028 Work Order Number: 21010192 RcptNo: 1
Logged by: Jacqueline Rasile 1/6/2021 11:10:00 AM
Completed By: Jacqueline Rasile 1/7/2021 9:20:55 AM
Reviewed By: Jennifer Woolf 1/7/2021 11:14:58 AM (...710‘7*.?1' M''oaL011,--
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? FedEx
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0°C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s)in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
g. Are samples(except VOA and ONG)properly preserved? Yes ❑d No ❑
10.Was preservative added to bottles? Yes ❑ No ❑d NA ❑
it Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials V
12.Were any sample containers received broken? Yes ❑ No ❑d
13. Does paperwork match bottle labels? Yes ❑d No ❑
(Note discrepancies on chain of custody)
14.Are matrices correctly identified on Chain of Custody? Yes ❑d No ❑
15. Is it clear what analyses were requested? Yes ❑d No ❑
16. Were all holding times able to be met? Yes ❑d No ❑
(If no,notify customer for authorization.)
Special Handling(if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA V
Person Notified: I Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18.Additional remarks:
Cooler Information
Cooler No Temp°C Condition Seal Intact Seal No Seal Date Signed By
1 1.5 Good Not Present
Page 37 of 37

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: City of Sanford WQ Permit Number: WQ0000543
WWTP Name: Big Buffalo WWTP NPDES Number: NC0024147
Monitoring Period: From 01/01/21 To 03/31/21
Pathogen Reduction(40 CFR 503.32/15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt. I/A(time/temp) Alt.2/B(Alk Treatment) Alt.3/C(Prior Testing)
Alt.4/D(No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density X Alt.(2)Process to Significantly Reduce Pathogens
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo.Mean Maximum Units dences Analysis
Fecal 2x10to the 6th CFU 29900 39200 60700 CFU/g 0 Quarterly Grab SM9222D
Coliform power per gram -MF
of total solids
MPN MPN/g
1000 MPN per gram of MPN/g
total solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) X (40-day bench) (30-day bench) (Spec.02 uptake)
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization) (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T:1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met."(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky,WWTP Superintendent
Preparer Name and Title(typ or print) Land Applier Name and Title(if applicable)(type or print)
Signature of Preparer* D e Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)

Cameron Testing Services, Inc. Laboratory Report NC OE NRq«
NC PHI-ES n7799
US EPA 191
Client: Synagro CT$ Proj. 2101-02 D&Cell 4£799
Project: Sanford WWTP Regulatory As
SampleSample information
Sampled C. Wynne De.te 01/04Q1 REiceived M. Sms m 01m4/21
Analyses and Results
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Project Wanner D
219 S.SkvIc Str. 919-208 Aq
Sanford NC 2732 cb a_ .mm

219S, SweaieStr- Cameron Testing Services, Inc. Chain of Custody
Sanford,NC 27330 Page!of
Rtane:919-208-4240 NC WINIG cert. 65t NC PHHS Cart 0 37799 US EPA NC01918 - -
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.Sample Intofrnation 1 Number of bottles - preservative Required TestinglAnalysis i CTS
;- x . - . Presomatives-(U)rIproserved, H(CkL
Client Sample 0 ia • 2 EL o I { & , Sample
F! A C `° q, ew -I g H2(S)O4, H(N}01(NalrhiOSUIrata, In
i, ''' I "' co pr Mar0) 1, IP}hasphonc,Dew(X),radicirte
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C11.NI 1; lAll ift/I-4 r-j-' / L., d i/if...,„/ Vlio.4 1 I -Lis no
- -
Check-in I
Rush work will require prior approval- Additional charges will apply -

3$% Reporl
Project: Sanford VONTP I 38% Volatiles Reduction T Proj. 2103-116
Client: Synagro (EPA 6251R-921013, Appendix D) Regulatory
Sampled Received Ref. Methods Std. Meth- 19th ed.
By C Winne By M. Sims 2540 G-TS
Crate 03/11121 Date 03f11121 Requested 2540 C -VS
—
Type Grab Matrix Sludge y Analysis
Sample ID Lab ID TS (%) VS (%) Analysis ' AnaFyat Date _
In 01 1.50% 915% 01 -
Out 02 6.55% 80 7% 02 FVSR (VK) 61.0% 'Pass > 38' °
I
/t 9/1‘,/1-41,
Project Mgr. !Ms
Notes:
Page 1

21QS-Steele EEr Cameron Testing Services, Inc. Chain of Custody
sartford. NC 27330
Phc ne; 91 -2C18 424O NG 11wv ;`r Cor; f654 NC PHHS Crei Al 377 9 VS EPA NCd1918 Page of
C�_ ' <1 co il- C I . W
Contact: -‘4%%`11;_ t.,r; - Phone: g ?Le 0 7 61
Addr {City, 4 -1� "g.. Fez:
Notes!
P i c', 1 ,ca 4- N1w,v l l Rush Orli1.1 Due!
. S,am---h torn ation Nurnbero t I Li- preservative -Required Testing/Analyefe -
I
Client Sample 2 e a- 3 a t7 a , ltres ��J}r�preservee. N({�I, 81r41�}I[+
_ w L S a N2(8JO4, +3(h1,09,{Na�Thiosutrate,
I — 0C9g. ,h___7 N4�(O�1I. {P}nospFwt►'Ft oth.r(x).ii-dia. ID
GIs -TI72!, 141.4Pi 1- I., 1 g- vs _ /
il Vj10 41 Vicm C I- . t
t 1
1
P.
I
1
Re No - Rime ived- taFr —
R - --
. - .7"--.. • uf,
- ~ It 21 10_ Zo
Cheok�#ri — - - -.- -
_ — — - - - --
Rush work waili requoro prior approval. Additional charges will apply

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: City of Sanford WQ Permit Number: WQ0000543
WWTP Name: Big Buffalo WWTP NPDES Number: NC0024147
Monitoring Period: From 04/01/21 To 06/30/21
Pathogen Reduction(40 CFR 503.32/15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A(time/temp) Alt.2/B(Alk Treatment) Alt.3/C(Prior Testing)
Alt.4/D(No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density X Alt.(2)Process to Significantly Reduce Pathogens
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo.Mean Maximum Units dences Analysis
Fecal 2x10to the 6th CFU <23300 27300 48200 CFU/g 0 Quarterly Grab SM9222D
Coliform power per gram -MF
of total solids
MPN MPN/g
1000 MPN per gram of MPN/g
total solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) X (40-day bench) (30-day bench) (Spec.02 uptake)
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization) (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T:1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met"(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky,WWTP Superintendent
Preparer Name and Tit e(type or print) Land Applier Name and Title(if applicable)(type or print)
- A. , 9)a9_
Signature of Prepar-y' / Ditto Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)

Cameron Testing Services, Inc. Laboratory Report NC DE NRk«
NC PhIHSk9g
U EPA i98
Client: Synagro CTS of 2104-023 D&Cert■22m
Project: Sanford WWTP Regulatory Yes
Sample In rmation
Sampled C. WynleAteD4/05/21 Received J. c,mesn Date /05e!
Analyses and Results
Lb SmogO i ƒ / ATI
© t ® k ka k hs
# 3 ` ' 2 Reference
k
21 -0 -01 q m FCC Ar-s 25500 ®A 25500 04/05121 RL 922D -ME
-02 <25500 ®A 25300
e] 25700 @q 2572
g4 <25500 em 25500
-05 48200 ek 24100
-06 ‹23300 @m 233oo
-07 <23400 Jm 2400
_en0
21043 -01 _@ a TS IN 3.S.2% o01 0445/21 FiL 2540G.TS
-02 4.21% _
22 &90% _
-04 I % 0.01
-05 415\ Ckai
-06 4 % aal
-07 4 % am
'
g / 01 610/
Review ` _
Lab Director
239 S.Slott Sir. 919-208-4240
Sanford NC2730 & _ em

219 S.Steele Str, Chain of Custody
s>re.Nc �o Cameron Testing Services, Inc.
NC 1GW Cart i16$4 NC PHilS Cad 0 37799 US EPA NC4191 E Page of
p�. e q7 a.20B�240 WJ•,
Corntxany; Synagro Email: - 1N kke S 111-4.Toi-c.N.wk CTSlab use On!
Sample TernpICI
Lab I D .Contact: Pl�q+>�: .,
284 Boer Ind. � - (co(YlN1
Address(City, --- -- .
State, k Mocksville, NC 27028 NOm; Permit MN)
I
Project: , v i-.MJrt Rush(YIN( , Due•
r.
Coilncted: Name: C Lb. it Kt— Sigiatute. Ca646
Sample Information Number of bottles Requested Analysis
4s Cr. � �" � rL � � Prellsrwati�+es={U)nprosErrved, NO, Lab
Sample ID m H2(s}a4. H{N}O3,{Na}Tiiiosulfoie, Na{0�1-, ID
U I °then?7C},Irhdirule
t -F
7- 1 11 z 1 I , , St +1t -
- -
1 . . , i . -1 '
Dateffiene
elin u hail: --
[ ei,it---1
__ . - ag-. ...iggeo 11/5/Z i 3 D PM
Rush work will require prior approval. Additional charges will apply

38% Report
Project: Sanford IMAirp 38% Volatiles Reduction 1 CTSProj. 2104-022
Client: Synagro (EPA 6251R-92/013, Appendix D) Regulatory
Sampled Received Ref- Methods Std. Meth_ W9i'ed.
. -By C. Wynne By J. Cameron 2540 C-T
Date 04/05/21 Date Q4/05/2 Requested 2540(a-VS
Type I Grab Matrix Sludge
Analysis
Sample ID Lab ID TS (%) VS ( ) Analygis
Analyst
2104-022-01 I-I 0 2.2'',: 6.8' ,
2104-022-02 Oul D 85"••:. 6r 2'r:. try-:;,' FVSR IVK) 38.1% 'Pass > 38%'
I _
.L... j277,:mer,
4P61////c710.,A
f
Lab Director Date:
Notes:
Page I

219 S. sleek Sir" Chain of Custody
s 21130
Cameron Testing Services, Inc
Phone 91•9-238-4240i NC WMpLa r Cell- 654 NC PHIIS Cede 37799 U$EPA f1C01918 Page of__""
cr _1r z ir — -- kwr, , ji .ci CT #abuses. -
Li,..
Address }} 284 Boger Rd. a r'' '
s .,
, .=' M_ ocksvi „ IBC 7 _ Perrriit(Yilio .____
P . _-• as 4 rrmij • -the. — -
C011,- .a 4 C Narki1' 0;g 6.1 14.14-C., Sigr11i2eJrta
ii
.Sample 11001:rrilicJAMMINK.Nur ber of bottles - ft
Requested Analysis
I
d d o_ xi .lc . a a c O 0. Pri erYalivirA:{uirrp,eserw d. f I Cia,
Em R 1. H2tsio4, WrnO3,(�)Tiosuffate. Na.0
iki ;
ID
ample ID j + , r Other(X).Indeale
- 16+11 .,
1111 1 coL4f 34 'Pen , Si. _ N l 1 38 NJ P- 3-ik , chc+-)
I
I . • -1 -' - .1 E
. ,
1 1 1
i ,
_1. j .._ _ _
11 •
ce"- _ _
I
Rush work will require prior approval" Additional charges will apply

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: City of Sanford WQ Permit Number: WQ0000543
WWTP Name: Big Buffalo WWTP NPDES Number: NC0024147
Monitoring Period: From 07/01/21 To 09/30/21
Pathogen Reduction(40 CFR 503.32/15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A(time/temp) Alt.2/B(Alk Treatment) Alt.3/C(Prior Testing)
Alt.4/D(No Prior Test) Alt.5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density X Alt.(2)Process to Significantly Reduce Pathogens
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo.Mean Maximum Units dences Analysis
Fecal 2x10to the 6th CFU 23200 73212 1520000 CFU/g 0 Quarterly Grab SM9222D
CoIiform power per gram -MF
of total solids
MPN MPN/g
1000 MPN per gram of MPN/g
total solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) X (40-day bench) (30-day bench) (Spec.02 uptake)
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization) (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T:1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met."(Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky,WWTP Superintendent
Preparer Name and Title^type or print) Land Applier Name and Title(if applicable)(type or print)
A. a dg aa.
Signature of Preparer Da e Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)

Cameron Testing Services, Inc. Laboratory Report NC DENR#654
NC PHHS#37799
US EPA#NC01918
Synagro CTS Proj. 2107-0094 DW Geri#37799
, Sanford WVVTP Regulatory Yes
Sample Information
C. Wynne Date 07/12/21 Received E. Puckett Date 07/12/21
Analyses and Results
2 .1 Std.Methods
- ID I Result el
a ii Reference
2107-0094 -03 Sludge Gr Fec.Coliform-5 23700 CFUI0 23700 07/13/21 RL 9222D-MF
-04 23400 0FUte 23400
-05 23200 CFU/g 23200
-06 828000 cFuig 23600
-07 1520000 CFU/g 23400
-08 29500 CFUlp 28500
-09 23600 CFUN 23500
Geomean
2107-0094 -03 3Iudge Gr TS(%) 4.23% 001 07/13/21 RL 2540 G-TS
-04 4.27%
-05 4.30% cc,
-06 4.23% 0 co
-07 4.27% 001
-08 3.39% 001
-09 4.24% 0.01
Report
Review /(:)11/ce4r)
Lab Director Date
219 S.Steele Sir.
919-2011-4240
Sanford NC 27330 chnsVcarnerontesung corn

219 S.Steele Str. Cameron TestingServices, Inc.
Sanford,NC 27330Chain of Custody
Phone:[phone] NC WWJGW Cert.#654 NC PtitlS Cert#37799 US EPA NCO1918 Page___of
Company: kJ YO Email {1 k Co: .v ws-�
CTS lab use
Contact: 'Phone: ,36, G O, LJ 6 2 # Sample ems Prod.fi3
Address(city., i
State,Zip) _ ._M_ . ___.
INS., Permit n
Project a i ,e �r' „r-r'' P gush(Y/N1 a Due:
Sample
Cotten/on: Name: C if k s M`.`,4(4+°.4t.- Signature;
Sample information Number of bottles+ pros xve Required Testing/Analysis
Client Sample 2 4) ' cl., I .'_< N z -; 1 o. ti. 2- ) Preservatives:(U)npreserved, t-t{Cjl, Sample
ID (1, C? �' ¢ H2(S)04, ht(N) 33,(Na)Thsasulfate, SaCn le
c� '� m ' 1 O O •\ Na(0)h, (P)hosphoric,Other(X),Indicate )
4,1 liititi ii 1 SI
._ so it.. ,
,, ss.
.n i i
tif i ;
iI E �_.__ ..__
r Relinquished: Received. - Date/Time
. \ 1 1.
Rush work will require prior approval. Additional charges will apply

38% Report
Project: 2108-0133 38% Volatiles Reduction CTS Proj. 2108-0133
Client: Synagro - Sanford (EPA 6251R-921013, Appendix D) Regulatory
+
Sampled Received Ref. Methods Std. Meth. 19th ed.
By C. Wynne By R. Lloyd Requested 2540 G -TS
Date 08/13/21 Date 08/13/21 2540 G-VS
Type Grab Matrix Sludge Analysis
Sample ID Lab ID TS(%) VS(%) A ni is Analyst
01 In 0.40% 70.1% In
02 Out 1.56% 53.7% Out FVSR ON 50.6% 'Pass> 38%
/5 c//
Project Mgr. Date:
Notes:
Page 1

219 S.Steele Sir. Cameron Testing Services, Inc. Chain of Custody
Sanford NC 27330 NC WWIGW Cert.#654 NC PHFHS Cert#37799 US EPA NC01918 Page _of___
Phone:[phone]
Company: �� bt7 Email: [,v 1 UL ce.s i[ `} -C a 6r� CTS lab use
J Sample Temp
Contact: Phone: 3 �j 05 6r L 2-7 SampleProj.ID
•Address(City, Fax: Ice(YIN)
State,Zip)
Notes: Permit(YIN)
SA C= I
Project: �� (�c t i
Rush(YIN) Due:
Sample
Collecion: Name: C -
I`Lz5 (t � Signature:
F e�
Sam pie Information Number of bottles+ preservative Required Testing/Analysis. CTS
Client Sample vo el • IL m a a 45 Preservatives:(U)npreserved, li(C)I,
I� Sample
t 0 N ; Q . _1 : ¢ H2(S)©4, H(N)O3,(Na)Thiosulfate,
ID En ~ �] N ' `'' "' m r P I o? Na(0)!i, (P)hosphoric,Other(X),Indicate IR.
\(' - �-ut S 1 42 I(•g3A , C Si- 2/
i.) 3- V 5 � e�g
v5Z, o(,.,- - 10121 11:36.4i G 5L 6 1 . ?.. VsR 12
Relinquished: Received: Date/Time
Check-in
Rush work w:(I require prior approval. Additional charges will apply

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: City of Sanford WQ Permit Number: WQ0000543
WWTP Name: Big Buffalo WWTP NPDES Number: NC0024147
Monitoring Period: From 10/01/21 To 12/31/21
Pathogen Reduction(40 CFR 503.32/1SA NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A(time/temp) Alt.2/B(Alk Treatment) Alt.3/C(Prior Testing)
Alt.4/D(No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt.6(Equivalent to PFRP)
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt.(1)Fecal Density X Alt.(2)Process to Significantly Reduce Pathogens
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density No.of Frequency Sample Analytical
Excee- of Type Technique
Minimum Geo.Mean Maximum Units dences Analysis
Fecal 2x10to the 6th CFU <23900 <24000 <24200 CFU/g 0 Quarterly Grab SM9222D
Coliform power per gram -MF
of total solids
MPN MPN/g
1000 MPN per gram of MPN/g
total solids(dry weight)
Salmonella 3 MPN per 4 grams total
bacteria(in solids(dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction(40 CFR 503.33/15A NCAC 02T.1107)-Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt.4
(VS reduction) X (40-day bench) (30-day bench) (Spec.02 uptake)
Option/Alt.5 Option/Alt.6 Option/Alt.7 Option/Alt.8
(14-Day Aerobic) (Alk Stabilization) (Drying—Stable) (Drying—Unstable)
Option/Alt.9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT(please check the appropriate statement)
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met.' (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky,WWTP Superintendent
Preparer Name and Title(ty e or print) Land Applier Name and Title(if applicable)(type or print)
cE ) - % a1 t;./223'a g.
Signature of Preparer* I bate Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)

Cameron Testing Services, Inc. Laboratory Report NC DENR#654
NC PHHS#37799
US EPA#NC01918
Client: Synagro CIS Proj. 2110038 DW Cert#37799
Project: Sanford WWTP Regulatory Yes
Sample Information
• Sampled C. Wynne , Rate: .; 10/05/21 Received J. Cameron Date 10/05/21
Analyses and Results
Lab ID Sample ID ri o L° Analyte Inuit i m .4 c Std.Methods
2 0 i7 m CZ n g C Reference
2110-0038 -01 Sludge Gr Fee.Coliform-S <23900 CFUrg 23900 10/06/21 RL 9222D-MF
-02 <23900 CFU/g 23900
-03 <24200 CFUrg 24200
-04 <24000 CFU/g 24000
-05 <24100 GFU/g 24100
-06 <23900 CFUrg 23900
-07 <24200 CFUrg 24200
Geomean <24000 24000
2110038 -01 Sludge Gr TS(%) 4.18% 0.01 10/05/21 RL 2540 G-TS
-02 4.18% 0.01
-03 4.14% 0,01
-04 4.16% 0,01
-05 4.15% 0.01
-06 4.18% 0,01
-07 4.14% 0.01
Report Review /P////cV2_/
Lab Director Date
219 S.Steele Str. 919-208-4240
Sanford NC 27330 [e-mail]

219 S.Steele Str. Cameron Testing Services, Inc. Chain of Custody
Sanford,NC 27330 NC WWIGW Cert.#654 NC PHHS Cert#37799 US EPA NC01918 Page of
Phone:[phone]
ll
I Company: Synagro Email: G synagro.com I CTS lab use only
K l".e..� 'Phone: Sample Temp
Contact:_
Oy Ck S1 kJ/ 336 909 8627 (C) : Lab ID � �d _
Address(City, 284 Boger Rd.
Fax: Ice(YIN)
State,Zip) 1
Mocksville, NC 2702$ Notes: Permit(WTI)
i
Project: : Rush(YIN) Due:
Collected: Name pi- c ti s lAJ y yt ;_c_ Signature: Ce:e/ ,�
Sample Information Number of bottles j� Requested Analysis
a Preservatives:(U)npreserved, H(C)I, CTS Lab
Sample ID T E2 CD E L } 0 o : ¢ I C7 L H2(S)O4, H(N)03,(Na)Thiosulfate, Na(0)H, ID
} v M m I � I r o I Other(X),Indicate
Dg-a-1-1 foI� �j j _ :'�t L' �L I �r
- 1ca� C�i, ���--c���
! ell
' - .015--
r �7
-- r- - ---- -- -'h - -- -.
1
--r i -
1 ,
. •
Relinquished: Received Date/Time
L..,iet vi., ii\j rt ii_e_--
i L...4 _,/ LL,_i „.._ ! .
Rush work will require prior approval. Additional charges will apply
ya.- • - _ �'''i.- a " '-. fr!.

38% Report
Project: Sanford VWVTP - Tank#1 38% Volatiles Reduction CTS Proj. 2111-0186
Client: Synagro (EPA 625/R-921013, Appendix D) Regulatory
Sampled Received Ref. Methods Std. Meth. 19th ed.
By N. Roth By M. Sims 2540 G -TS
Date 11/19/21 Date 11/19/21 Requested 2540 G -VS
Type Grab Matrix Sludge Analysis
Sample ID Lab ID TS(%) VS (%) Analysis Analyst
Date I
In -1 0.02% 100.0% In
Out -2 0.11% 51.2% Out FVSR(VK) 100.0% 'Pass > 38%'
•
///c71a/P0(7 -/
Project Manager Date.
Notes:
Page 1

219 S.Steele Str. Cameron Testing Services, Inc. Chain of Custody
Sanford, NC 27330
Phone: [phone] NC WW/GW Cert.#654 NC PHHS Cert#37799 US EPA NC01918 Page of
1
Company: Synagro Email: [e-mail] CTS lab use only
Contact: Sample Tempi
R.ROtII Phone: [phone] (C) Lab ID // ._, ,y046.
Address(City, 284 Boger Rd. Fax: Ice(YIN)
State,Zip) Mocksville, NC 27028 Notes: Permit(YIN) 1
Project: 1 Rush(YIN) Due:
Collected: Name: Nei 2 q- h. Signature: >ILA
Sample Information Number of bottles Requested Analysis
_ I
N ® I c �� .` } C7 4 4 : m` C7 4 y m Preservatives:(k3)npreserved, H(C)I, CTS Lab
Sample ID 0 • E (; m N M g g ' e- Oa H2(S)04, H(N)03, (Na}Thiasulfate, Na(0)H, ID
U V LO co 7 Other(X),Indicate
jr 4 CdUrrP.J 1)(1/�01:6i-. a S L. A), x. - -0 lA VSN I
s,,corS to i s�toc G S L g ii--- v
Ren hed: . Received: Date/Time
C! v1-0 ! j oOl Rush work will require prior approval. Additional charges will apply

SECTION 6

Agricultural Lime Application Log
Year: 2021
Project: Sanford WWTP
Field Soil Lime Requirement Tons/Acre Date Applied
(state-county-site-field) pH (from soil analysis) Applied
NC-CH-49-4 6.0 0.0 0.0
NC-CH-49-5 6.3 0.0 0.0
NC-CH-49-6 6.2 0.0 0.0
NC-CH-49-7 6.1 0.0 0.0
NC-CH-49-8 6.2 0.0 0.0
NC-CH-60-4 5.2 1.4 0.0
NC-CH-77-4 5.9 0.0 0.0
NC-CH-77-5 6.4 0.0 0.0
NC-CH-77-6 5.8 0.4 0.0
NC-CH-77-7 6.6 0.0 0.0
NC-CH-77-8A 6.0 0.0 0.0
NC-CH-77-8B 6.6 0.0 0.0
NC-CH-77-9 6.3 0.0 0.0
NC-CH-77-12 5.8 0.4 0.0
NC-CH-77-13 6.0 0.0 0.0
NC-CH-77-16 5.6 0.8 0.0
NC-CH-66-1 5.4 1.0 0.0
NC-CH-66-2 6.0 0.0 0.0
NC-CH-66-3 5.6 0.8 0.0
NC-CH-66-4 6.1 0.0 0.0
NC-CH-66-5 6.2 0.0 0.0
NC-CH-66-6 5.7 0.6 0.0
NC-CH-66-11 5.8 0.5 0.0
NC-CH-66-8 5.6 0.7 0.0
NC-CH-101-1 5.6 0.8 0.0
NC-CH-101-2 5.7 0.6 0.0
NC-CH-101-3 5.8 0.5 0.0
NC-CH-101-4 5.8 0.5 0.0
NC-CH-101-5 5.7 0.5 0.0
NC-CH-101-6 5.7 0.5 0.0
NC-CH-101-8 6.0 0.5 0.0
NC-CH-101-9 5.7 0.6 0.0
NC-CH-101-10 5.9 0.5 0.0

SECTION 7

WPage1 of 1
r 0
Report No: 22 035 0647
Account No: 46622 \I (a ,point,, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Advisor: Synagro Central LLC/Technical Client: Henry Stinson Farm:
Mary Brewer
284 Boger Road
Mocksville NC 27028 Date Received:02/04/2022
Date of Report:02/07/2022
Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-I K-I S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I CEC BS% Ca% Mg% ESP Na
09080 CH-49 4 MIN 6.0 1.3 183 48 0 0 8.2 85 61 21
Crop Recommendations: Rec Uom Lime(t/acre) N P205 KZO S Mn Zn Cu B Mg Last Crop
1 Pasture lb/acre 0.5 50 0 71 0
Comment:
Test result units=CEC and Na in meq/100cm3;NO3 N in mg/dm3;WA/in g/cm3
North Carolina Division of Water Quality Certification#257,Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines,Analysis prepared by:Waypoint Analytical Virginia,Inc.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL001066
,c.i 1t4+•.• Client: Henry(Jr)Stinson Advisor: Chris Wynne
' :Wk.., Predictive 904 Delphus Stinson Rd. Synagro LLC
_$ �� ,it ��
Goldston, NC 27252 284 Boger Road
1 , i. Soil Report Mehlich-3 Extraction Mocksville, NC27028
-::: li , '. Sampled County: Chatham
'66.y,i,.%;l '. Links to Helpful Information
Client ID: 130941 Advisor ID: 509090
Sampled: 07/05/2021 Received: 07/20/2021 Completed: 07/28/2021 Farm: CH-49
Sample ID: 5 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 30 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.46 0.95 13.0 90 1.4 6.3 300 59 70 18 41 383 242 797 797 899 0.2 2
Sample ID: 6 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 20 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.41 0.96 13.7 89 1.5 6.2 373 66 67 20 43 419 265 1249 1249 1030 0.1 1
e1 1orkh Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
.# k rThank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Totr7CiwTruskfLindCi iibIm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL001066
Henry(Jr)Stinson Page 2 of 3
Sample ID: 7 Recommendations: Lime Nutrients(Ib/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 90 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.36 1.09 9.6 86 1.3 6.1 291 24 66 19 40 232 155 456 456 450 0.1 1
Sample ID: 8 Recommendations: Lime Nutrients(Ib/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 80 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.41 1.04 9.9 88 1.2 6.2 297 27 65 21 41 238 157 490 490 464 0.1 1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL001066
Henry (Jr)Stinson Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If$, pH$, $pH, C or Z M-O mineral-organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmsfind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.. P205 phosphate
S-I sulfur index
Test Results SS-I soluble salt index
W/V weight per volume
Zn-Al zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO3-N (not routinely
www.ncagr.gov/agronomi/uyrst.htm
available)] indicate levels of plant nutrients or other fertility measurement. Visit

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL006534
,c.i 1t4+•.• Client: Henry(Jr)Stinson Advisor: Chris Wynne
' :Wk.., Predictive 904 Delphus Stinson Rd. Synagro LLC
_$ �� ,it ��
Goldston, NC 27252 284 Boger Road
1 , � Soil Report Mehlich-3 Extraction Mocksville, NC27028
'-''. , '. Sampled County: Chatham
'66.y,i,.%;l '. Links to Helpful Information
Client ID: 130941 Advisor ID: 509090
Sampled: 08/03/2021 Received: 09/30/2021 Completed: 10/12/2021 Farm: CH-66
Sample ID: 1 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 1.0 120-200 0 70 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.60 0.95 9.8 80 2.0 5.4 295 35 58 20 55 568 358 602 602 517 0.3 3
Sample ID: 2 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 60 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.46 1.02 13.0 89 1.4 6.0 368 41 63 25 52 566 356 722 722 633 0.4 3
e1 1orkh Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
.# k rThank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Totr7Ciwfrus!fLindCi iibIm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL006534
Henry(Jr)Stinson Page 2 of 3
Sample ID: 3 Recommendations: Lime Nutrients(Ib/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.8 120-200 0 0 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.60 0.93 10.2 80 2.0 5.6 275 103 58 17 56 749 466 832 832 674 0.1 1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL006534
Henry (Jr)Stinson Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If$, pH$, $pH, C or Z M-O mineral-organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmsfind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.. P205 phosphate
S-I sulfur index
Test Results SS-I soluble salt index
W/V weight per volume
Zn-Al zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO3-N (not routinely
www.ncagr.gov/agronomi/uyrst.htm
available)] indicate levels of plant nutrients or other fertility measurement. Visit

WPage1 of 1
r 0
Report No: 22 035 0650
Account No: 46622 \Ilafpoint,, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Advisor: Synagro Central LLC/Technical Client: Henry Stinson Farm:
Mary Brewer
284 Boger Road
Mocksville NC 27028 Date Received:02/04/2022
Date of Report:02/07/2022
Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-I K-I S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I CEC BS% Ca% Mg% ESP Na
09090 CH-66 4 MIN 6.1 1.2 196 52 0 0 8.6 86 62 21
Crop Recommendations: Rec Uom Lime(t/acre) N P205 K20 S Mn Zn Cu B Mg Last Crop
1-Pasture lb/acre 0.5 50 0 61 0
09091 CH-66 11 MIN 5.8 1.6 162 53 0 0 8.2 81 59 19
Crop Recommendations: Rec Uom Lime(t/acre) N P205 K20 S Mn Zn Cu B Mg Last Crop
1 Pasture lb/acre 0.5 50 0 59 0
Comment:
Test result units=CEC and Na in meq/100cm3;NO3 N in mg/dm3;WA/in g/cm3
North Carolina Division of Water Quality Certification#257,Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines,Analysis prepared by:Waypoint Analytical Virginia,Inc.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL019821
oci 11
4,,, Client: Henry(Jr)Stinson Advisor: Chris Wynne
k •
' *r " , Predictive 904 Delphus Stinson Rd. Synagro LLC
_$ ���`it ��
Goldston, NC 27252 284 Boger Road
1 , � Soil Report Mehlich-3 Extraction Mocksville, NC27028
- -•I , '. Sampled County: Chatham
'66.y,i,.%;l '. Links to Helpful Information
Client ID: 130941 Advisor ID: 509090
Sampled: 11/18/2021 Received: 11/24/2021 Completed: 01/20/2022 Farm: CH-66
Sample ID: 5 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.41 1.11 13.2 90 1.4 6.2 416 97 70 16 82 1374 838 1043 1043 1139 0.3 2
e1 1orkh Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
.# k rThank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Totr7CiwTruskfLindCi iibIm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL019821
Henry (Jr)Stinson Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If$, pH$, $pH, C or Z M-O mineral-organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmsfind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.. P205 phosphate
S-I sulfur index
Test Results SS-I soluble salt index
W/V weight per volume
Zn-Al zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO3-N (not routinely
www.ncagr.gov/agronomi/uyrst.htm
available)] indicate levels of plant nutrients or other fertility measurement. Visit

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL034244
,c.i 1t4+•.• Client: Henry(Jr)Stinson Advisor: Chris Wynne
' :Wk.., Predictive 904 Delphus Stinson Rd. Synagro LLC
_$ �� ,it ��
Goldston, NC 27252 284 Boger Road
1 , i. Soil Report Mehlich-3 Extraction Mocksville, NC27028
-::: li , '. Sampled County: Chatham
'66.y,i,.%;l '. Links to Helpful Information
Client ID: 130941 Advisor ID: 509090
Sampled: 06/15/2021 Received: 06/17/2021 Completed: 06/24/2021 Farm: CH-66
Sample ID: 6 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.6 120-200 0 80 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.41 1.06 9.7 80 1.9 5.7 322 27 61 18 55 660 413 650 650 737 0.1 1
Sample ID: 8 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.7 120-200 0 60 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.46 0.98 10.3 83 1.8 5.6 294 39 63 18 52 387 249 781 781 776 0.1 1
e1 1orkh Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
.# k rThank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Totr7CiwTruskfLindCi iibIm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL034244
Henry (Jr)Stinson Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If$, pH$, $pH, C or Z M-O mineral-organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmsfind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.. P205 phosphate
S-I sulfur index
Test Results SS-I soluble salt index
W/V weight per volume
Zn-Al zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO3-N (not routinely
www.ncagr.gov/agronomi/uyrst.htm
available)] indicate levels of plant nutrients or other fertility measurement. Visit

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL019816
,c.i 1t4+•.• Client: Paul Price Advisor: Chris Wynne
' :Wk.., Predictive 645 J. Cook Rd Synagro LLC
_$ �� ,it ��
Goldston, NC 27252 284 Boger Road
1 , i. Soil Report Mehlich-3 Extraction Mocksville, NC27028
-::: li , '. Sampled County: Chatham
'66.y,i,.%;l '. Links to Helpful Information
Client ID: 435848 Advisor ID: 509090
Sampled: Received: 11/24/2021 Completed: 01/20/2022 Farm: CH-77
Sample ID: 4 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
1.14 1.00 9.7 85 1.4 5.9 133 90 62 18 55 573 361 459 459 499 0.1 1
Sample ID: 12 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.4 120-200 0 40 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.51 0.96 10.0 83 1.7 5.8 205 52 58 22 41 534 337 466 466 506 0.1 1
e1 1orkh Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
.# k rThank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Totr7CiwTruskfLindCi iibIm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL019816
Paul Price Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If$, pH$, $pH, C or Z M-O mineral-organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmsfind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.. P205 phosphate
S-I sulfur index
Test Results SS-I soluble salt index
W/V weight per volume
Zn-Al zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO3-N (not routinely
www.ncagr.gov/agronomi/uyrst.htm
available)] indicate levels of plant nutrients or other fertility measurement. Visit

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL006535
oci 11
4,,, Client: Paul Price Advisor: Chris Wynne
k •
' *r " , Predictive 645 J. Cook Rd Synagro LLC
_$ ���`it ��
Goldston, NC 27252 284 Boger Road
1 , � Soil Report Mehlich-3 Extraction Mocksville, NC27028
- -•I , '. Sampled County: Chatham
'66.y,i,.%;l '. Links to Helpful Information
Client ID: 435848 Advisor ID: 509090
Sampled: 07/28/2021 Received: 09/30/2021 Completed: 10/12/2021 Farm: CH-77
Sample ID: 5 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 10 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.51 1.09 10.5 90 1.0 6.4 248 77 69 18 70 1438 874 618 618 810 0.3 3
e1 1orkh Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
.# k rThank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Totr7CiwTruskfLindCi iibIm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL006535
Paul Price Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If$, pH$, $pH, C or Z M-O mineral-organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmsfind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.. P205 phosphate
S-I sulfur index
Test Results SS-I soluble salt index
W/V weight per volume
Zn-Al zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO3-N (not routinely
www.ncagr.gov/agronomi/uyrst.htm
available)] indicate levels of plant nutrients or other fertility measurement. Visit

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL029141
,c.i 1t4+•.• Client: Paul Price Advisor: Chris Wynne
' :Wk.., Predictive 645 J. Cook Rd Synagro LLC
_$ �� ,it ��
Goldston, NC 27252 284 Boger Road
1 , i': Soil Report Mehlich-3 Extraction Mocksville, NC27028
'- ';, c, ` Sampled County: Chatham
-"x'w,i,.;+ '. Links to Helpful Information
Client ID: 435848 Advisor ID: 509090
Sampled: 01/05/2021 Received: 04/08/2021 Completed: 04/16/2021 Farm: CH-77
Sample ID: 6 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.4 120-200 0 0 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.56 1.05 10.5 84 1.7 5.8 130 79 61 19 52 666 417 372 372 386 0.1 1
Sample ID: 8 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.46 1.13 9.7 89 1.0 6.3 106 92 58 27 31 945 580 316 316 378 0.1 1
e1 1orkh Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
.# k rThank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Totr7Ciwfrus!fLindCi iibIm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL029141
Paul Price Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If$, pH$, $pH, C or Z M-O mineral-organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmsfind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.. P205 phosphate
S-I sulfur index
Test Results SS-I soluble salt index
W/V weight per volume
Zn-Al zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO3-N (not routinely
www.ncagr.gov/agronomi/uyrst.htm
available)] indicate levels of plant nutrients or other fertility measurement. Visit

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL031197
,c.i 1t4+•.• Client: Paul Price Advisor: Chris Wynne
' :Wk.., Predictive 645 J. Cook Rd Synagro LLC
_$ �� ,it ��
Goldston, NC 27252 284 Boger Road
1 , � Soil Report Mehlich-3 Extraction Mocksville, NC27028
'- ';, c, ` Sampled County: Chatham
-"x'w,i,.;+ '. Links to Helpful Information
Client ID: 435848 Advisor ID: 509090
Sampled: 04/26/2021 Received: 04/28/2021 Completed: 05/06/2021 Farm: CH-77
Sample ID: 7 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Corn, silage 0.0 180-220 0 110 0 0 pH$ 0 0 0 Note: 3 Note: $
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.32 1.06 9.5 92 0.8 6.6 180 43 71 19 51 1346 816 394 394 561 0.3 3
Sample ID: 16 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Corn, silage 0.8 180-220 0 20 0 0 0 0 0 0 Note: 3
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.60 1.01 10.6 82 1.9 5.6 288 107 61 16 44 518 328 975 975 711 0.1 1
e1 1orkh Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
.# k rThank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Totr7Ciwfrus!fLindCi iibIm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL031197
Paul Price Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If$, pH$, $pH, C or Z M-O mineral-organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmsfind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.. P205 phosphate
S-I sulfur index
Test Results SS-I soluble salt index
W/V weight per volume
Zn-Al zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO3-N (not routinely
www.ncagr.gov/agronomi/uyrst.htm
available)] indicate levels of plant nutrients or other fertility measurement. Visit

WPage1 of 1
r 0
Report No: 22 035 0649
Account No: 46622 \I (a ,point,, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Advisor: Synagro Central LLC/Technical Client: Paul Price Farm:
Mary Brewer
284 Boger Road
Mocksville NC 27028 Date Received:02/04/2022
Date of Report:02/07/2022
Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-I K-I S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I CEC BS% Ca% Mg% ESP Na
09088 CH-77 8A MIN 6.0 1.2 174 50 0 0 7.9 85 62 20
Crop Recommendations: Rec Uom Lime(t/acre) N P205 K20 S Mn Zn Cu B Mg Last Crop
1-Pasture lb/acre 0.5 50 0 66 0
09089 CH-77 13 MIN 6.0 1.3 185 41 0 0 8.6 85 62 21
Crop Recommendations: Rec Uom Lime(t/acre) N P205 K20 S Mn Zn Cu B Mg Last Crop
1 Pasture lb/acre 0.5 50 0 86 0
Comment:
Test result units=CEC and Na in meq/100cm3;NO3 N in mg/dm3;WA/in g/cm3
North Carolina Division of Water Quality Certification#257,Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines,Analysis prepared by:Waypoint Analytical Virginia,Inc.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL029147
,c.i 1t4+•.• Client: Paul Price Advisor: Chris Wynne
' :Wk.., Predictive 645 J. Cook Rd Synagro LLC
_$ �� ,it ��
Goldston, NC 27252 284 Boger Road
1 , i': Soil Report Mehlich-3 Extraction Mocksville, NC27028
'- ';, c, ` Sampled County: Chatham
-"x'w,i,.;+ '. Links to Helpful Information
Client ID: 435848 Advisor ID: 509090
Sampled: 04/05/2021 Received: 04/08/2021 Completed: 04/16/2021 Farm: CH-77
Sample ID: 9 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 30 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.46 1.03 9.0 89 1.0 6.3 112 58 69 17 43 1207 736 296 296 419 0.1 1
Sample ID: 10 Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Fescue/OGrass/Tim, M 0.0 120-200 0 30 0 0 0 0 0 0 Note: 12
2- 0.0
Test Results [units-WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.51 1.06 9.6 89 1.0 6.3 122 60 69 17 43 1390 846 338 338 473 0.1 1
e1 1orkh Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
.# k rThank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Totr7Ciwfrus!fLindCi iibIm

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL029147
Paul Price Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no-till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If$, pH$, $pH, C or Z M-O mineral-organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmsfind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.. P205 phosphate
S-I sulfur index
Test Results SS-I soluble salt index
W/V weight per volume
Zn-Al zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO3-N (not routinely
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available)] indicate levels of plant nutrients or other fertility measurement. Visit