WQ0004609_Residual Annual Report 2021_20220224

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0004609
Applicant/Permittee Wayne Farms LLC
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Lysa Finnerty
Email Address* Phone Number*
[e-mail] 14105376150
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0004609
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court,Ste 100,Baltimore,MD 21220
Facility Name* Wayne Farms Class B Residuals Program
Please provide comments/notes on your current submittal below.
2021 Annual Report for Wayne Farms,L.L.C.-Dobson,NC
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
Wayne Farms NC 2021 Annual Report FINAL.pdf 20.5MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature Lp
Ja rotivit5
Submission Date 2/24/2022

435 Williams Court,Suite 100
Baltimore,MD 21220 SYNAG R
www.synagro.com
FEBRUARY 24,2022
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2021 Annual Report for Permit No.WQ0004609
Dear NCDEQ:
Synagro is submitting one electronic copy of the above referenced report on behalf of the
Wayne Farms, L.L.C.-Dobson, NC.
If you have any questions or need additional information,please do not hesitate to contact Paul
Nordin at(336)386-8151 or Alex Fox at(336) 703-8681.
Sincerely,
l e't ic& Sfiiva'c 25
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Paul Nordin,Wayne Farms, L.L.C.-Dobson
Alex Fox, Synagro
YOUR PARTNER FORA CLEANER,GREENER WORLD

WAYNE FARMS, L.L.C. , NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0004609
2021 ANNUAL REPORT

Wayne Farms, L.L.C. - Dobson, NC
Residuals Land Application Program
2021 Annual Report
TABLE OF CONTENTS
1. Certification Form & Annual Operations Summary
2. Annual Residual Sampling Summary Forms
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Control of Possible Nuisance Conditions
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00004609 County Surry Year 2021
Facility Name(as shown on permit)Wayne Farms NPDES No.NC0006548
Land Application Operator Svnazro Phone# (33>998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES_NO. If NO,sldp Part A,and Part B and proceed to Part C. Also,if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled,
Part A—Residuals Application Summary:
Total number of application fields in the permit: 26
Total number of fields utilized for land application during the year: 5
Total amount of dry tons applied during the year for all application sites: 71.92
Total number of acres utilized for land application during the year: 85.00
Part B—Annual Compliance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit(including but not limited to items
1-I3 below)issued by the Division of Water Quality X YES NO.
If no,please provide a written description why the facility was not compliant,the dates,and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three(3)copies of
laboratory results are attached.
4. Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1105(a)or the Pollutant Loading
Rates in 15A NCAC 02T.1105(b)(Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in I5A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or,in the case of a deviation,prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations arc
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals,as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C—Certification:
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate,and complete. I
am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing violations."Matthew Wooten,Complex Manager I/ l I1.90412
Permittee Name and Title(type or print) Signature!f P rmittee Date
• 2/18/2022
Signature of Prepare?' Date �I .ture of d Applier Date
(if different from Permittee) (if differ•nt from Permit ee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T.1102(26) DENR FORM ACF(12/2006)

OPERATIONS SUMMARY-LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES -ALL SITES
DATE RANGE: 1/1/2021 - 12/31/2021
WAYNE FARMS,L.L.C.,NC
WAYNE FARMS LLC,NC FOOD PROCESSING LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
May 2021 644,800.00 G 40.87 D 37.07
September 2021 229,400.00 G 14.54 D 13.19
October 2021 260,400.00 G 16.51 D 14.97
TOTAL 1,134,600.00 G 71.92 D 65.23
Units Key: D-Dry Tons; G—Gallons;W—Wet Tons;Y—Cubic Yards
Report Date: 12/6/2021 12:51:34 PM

SECTION 2

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Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Wayne Farms
Lot Number:WA14019
Date Completed:01/29/2021
02/01/2021 10:26 AM
Approved and released by:
Project Manager II: Lucas Odom
MILB
Q PCCR�c��
'ye )
ANSI NatonalAccredltatlon Board
ACCREDITEDORA1O,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WA14019
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix and low percent solids, the initial sample amount used for sample -001 was 3X more
than the standard procedure. The LOQ has been adjusted accordingly.
TKN
The method blank for analytical batch 80781 contained the analyte: Total Kjeldahl Nitrogen (TKN) greater
than the acceptance criteria. The associated samples, contained detections for this analyte at
concentrations greater than 10X the value found in the method blank; therefore sample results are not
impacted. The data has been reported.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WA14019-001
Description:Wayne Farms Matrix:Solid
Date Sampled:01/12/2021 1115 % Solids: 1.52 01/20/2021 0110
Date Received:01/14/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 (% Solids)SM 2540G 1 01/20/2021 0110 AAB 79998
1 350.1 (Ammonia-N )350.1 2 01/19/2021 1341 DRD 79842
1 (Nitrate-N )9056A 1 01/19/2021 1334 AMR 79937
1 (Nitrite-N )9056A 1 01/19/2021 1334 AMR 79944
2 (Phosphorus)365.1 5 01/27/2021 1018 DMA 01/26/2021 1924 80750
1 (Soil pH meas)9045D 1 01/14/2021 1817 AAB 79516
1 351.4 (TKN)351.2 2 01/26/2021 1520 DMA 01/21/2021 1755 80265
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Solids SM 2540G 1.52 % 2
Ammonia-N (gas diffusion) 350.1 3500 130 68 mg/kg 1
Nitrate-N (soluble) 9056A 70 33 6.6 mg/kg 1
Nitrite-N (soluble) 9056A ND 13 6.6 mg/kg 1
Phosphorus 7723-14-0 365.1 14000 1600 330 mg/kg 2
Soil pH measured in water @ 17.9° C 9045D 7.0 su 1
TKN 351.2 73000 3300 3300 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/21/2021 1241 JAB2 01/20/2021 1110 79538
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 5.1 1.2 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/20/2021 0849 KSH2 01/19/2021 0905 79720
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 11000 1200 440 mg/kg 1
Arsenic 7440-38-2 6010D ND 44 15 mg/kg 1
Cadmium 7440-43-9 6010D ND 15 3.7 mg/kg 1
Calcium 7440-70-2 6010D 13000 J 15000 1800 mg/kg 1
Chromium 7440-47-3 6010D 23 J 29 7.4 mg/kg 1
Copper 7440-50-8 6010D 360 29 13 mg/kg 1
Iron 7439-89-6 6010D 15000 290 130 mg/kg 1
Lead 7439-92-1 6010D ND 29 13 mg/kg 1
Magnesium 7439-95-4 6010D 14000 J 15000 1800 mg/kg 1
Manganese 7439-96-5 6010D 720 44 17 mg/kg 1
Molybdenum 7439-98-7 6010D ND 120 29 mg/kg 1
Nickel 7440-02-0 6010D ND 120 31 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3of7

Client:Synagro Laboratory ID:WA14019-001
Description:Wayne Farms Matrix:Solid
Date Sampled:01/12/2021 1115 % Solids: 1.52 01/20/2021 0110
Date Received:01/14/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/20/2021 0849 KSH2 01/19/2021 0905 79720
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Potassium 7440-09-7 6010D 7700 J 15000 1800 mg/kg 1
Selenium 7782-49-2 6010D ND 59 24 mg/kg 1
Sodium 7440-23-5 6010D 8000 J 15000 1800 mg/kg 1
Zinc 7440-66-6 6010D 860 150 37 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4of7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
Samples Receipt Checklist t5RC)iME0139.RC-is} Revised:9/290020
,i1r20...e.nAgical issuing Authority:Pace ENV-+NC41 Page I.of 1
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Sample Receipt Checklist (SRC)
Cheat: srwro Cooler Inspected b 'relate: KSC I Ci1'.4{21221 Lot,#' V/AMO
NJ i am 4freceipt:_ •• J LIPS
S -FedP r:■ Other
j yeAl I.Wore cunLttidy seals prks:nt On the cooler?
=Yes! ['No 7NA 2,)f r~.4Lvtodly seals werf I,resent,were than.intact and unbroken,"
cH Strip iD: ,Chloride Strip ID: NA ... Tcsled by!NA
Original temperature open receip=±Derived(Corrcx:Lk-(1)temperature upon receipt %Solid 5n p p la 2"75
23 �2,3 3c NA ...NA ac NA .NA 'r.: NA iNA nc
Method:F1Ternperaarre lila:1k []Against Sott:es IR Gun If): s IR Gods Correction Far,tor. {) °C .
Method of cnnlr]n1 El Wet Ice ❑ ire Pack; El L).ry]ce ❑ None
Yes I ]*fo ❑NA I3. IFe of any cooler ei ecdcd -0°C„wrii Prr�ject Manager Notified?
In PM was Notified by;phone!email I faua-to-Ca (circle one).
E. Ye_fi ❑No LINA 4, is tim tr.mmercia]courier's pocking slap attached to ri,is Conti?
prCe=
Yes El No 5- Ware.proper custody prorcd e:
urrs(relinquishatetvCd) Followed?
ND. 6. Were sample]Ds:isted in the C C?
es ❑Na 7, Were septic liJs listed au all sample containers?
Yes •Na N. Was_o]loctitiii[1aLe<&.time:fisted on the COC7 _I
ay..., nNo 9- Was collootion date&time listed ten.II].sample containP.r0 -
Yos fl o 1D.Did all n mLseiam:label inrormatiwn(CD,date,Lime)agree with Cie COO?
Yes IT No 1 t.werg Lois Du be per xurmed li•,etd on Ike CO C.? •
12.Did al]samples arrive in the proper conlrinurs for tech test and/or is good ca;tdit:on
Yes FINo (unbook.on,lids ort,etc.)?
n Ycs UNo 1 i. 1 r:s adequate swank volume available?
,r Yes •No _ 14. Wore all samples r000ivatl within !•4 the holding time or 48 hoirm.mrhicleeter comes first?
O Yr U'No is, Were any samples containers missinglexcess(circle one)s:miple8 Net Blvd on COC?
n 0 16. Far VOA and RSK-175 samples,were bubbles proscnt 7"pea-size"(Y.':or&run in d ameter)
❑Yes 'No NA iri h of the VOA vials? -
Res Li No �NA 17, Wore all DROrm etalsrnutriCtll Satriples recei vcL at a pI- of<21 .H
Yea LJ Nu' 1, NA 18. %Verret all eiyan ids salnp]ca re.oiv'ed at a p1!> 12 and nul1�ie samples receiv cJ t a p14>97
19, were all applicably NHy'l'ICNicyaiuoecna {-11608-3 .ii;1-)yeuvpks freeof I
El Yes ❑Na n A residual chlorine? _. _
20.Were chant remarks/requests(i.e,requested dilutions,l+ S±MST)designations,etc..-)
❑Yes ❑N' OVA con-ectly transcr:led from the CUC into the comment sorti{m i i 1,lbMS?
I]Yes C.1 N4 12E.Was the rote number listed on the_cnntairo label'?if s:Quote tt .
Sample Preservation (Must be completed for any sample(s)ineorr ;:tiy preserved or with headspacc,)
Samples) NA were received incorrt!cl:y preserved and wL1-c U..9.1 to I ace wdini{ly
;in Fampie receiving with th N mT.,of circle one:1•128O4.HNO3-AC].NaOH tiling SR 14 NFL
'Time of I+r'w:rvr rirni N ... , If more than one pros rv'I tLve:s needed,please note in lhv conimellts below,
Sampla(s) NA _. _ — _were_x3cci��ad with babbles>6 tram in diameter.
Samples(s) x, _were received v igi l TRC 0-S mgtL(If 419 is no)and were
adjusted accordingly in sample re oivirig with sodium tl:iosutiate(1.42,S2O0 with Shealy 1f3: NA
1.btu-code labels applied hy: -. 1-1641" ialto:. Ot+L4f2L121 ._.
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Comments;
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

SECTION 3

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Wayne Farms, L.L.C.,NC Total Dry Tons Applied(Annual): 4.72
Permit#: WQ0004609 Cation Exchange Capacity(non 503 only):
Operator: James Walter Johnson Owner: James Walter Johnson Predominant Soil Series: Braddock
Acres Used: 30.4 Acres Permitted: 30.4 Site#: NC SU 00013 Field#: SU 00013 0006
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 11 I2 3 4j 51 61 71 LJ 91 101 111 i 121
Com-
posite
Date 1/12/21
%Solids 1.52
Arsenic 15
Cadmium 3.7
Copper 360
Chromium 23
Lead 13
Mercury 1.2
Molyb- 29
denum
Nickel 31
Selenium 24
Zinc 860
Total
Phos- 14000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 121 31 41 5 j 6 7 81 91 110 11 ] 12
DT/Ac./ o
App.
Event 0.16
Arsenic 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Cadmium 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001
Copper 0.112 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.112
Chromium 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007
Lead 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000
Molyb- 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009
denum
Nickel 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010
Selenium 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007
Zinc 0.267 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.267
Total
Phos- 4.340 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.340
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment o knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Wayne Farms, L.L.C., NC Total Dry Tons Applied(Annual): 26.33
Permit#: WQ0004609 Cation Exchange Capacity(non 503 only):
Operator: Davis Family Properties Owner: Davis Family Properties Predominant Soil Series: Fairview
Acres Used: 20.5 Acres Permitted: 20.5 Site#: NC SU 00020 Field#: SU 00020 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 ; 21 13; 4 5 ; 6; 7 ; 8; 9I 10 I11I 12
Com-
posite
Date 1/12/21
%Solids 1.52
Arsenic 15
Cadmium 3.7
Copper 360
Chromium 23
Lead 13
Mercury 1.2
Molyb- 29
denum
Nickel 31
Selenium 24
Zinc 860
Total
Phos- 14000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 11 Ji 3 ; 4 5 6 7 81 91 10 111 1 12
DT/Ac./ o
App. ig
Event 1.29 "
Arsenic 0.039 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.039
Cadmium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010
Copper 0.926 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.926
Chromium 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.059
Lead 0.033 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.033
Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Molyb 0.075 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.075
denum
Nickel 0.080 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.080
Selenium 0.062 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.062
Zinc 2.212 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.212
Total
Phos- 36.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 36.008
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment fo knowing violations".
---7) .- Q,/1 iiitZ-
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Wayne Farms, L.L.C., NC Total Dry Tons Applied(Annual): 15.72
Permit#: WQ0004609 Cation Exchange Capacity(non 503 only):
Operator: Ben Watson Owner: Ben Watson Predominant Soil Series: Clifford
Acres Used: 12.8 Acres Permitted: 12.8 Site#: NC SU 00022 Field#: SU 00022 0001
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 12 3 " 41 5 6 71 8 91 101 1111 12
Com-
posite
Date 1/12/21
%Solids 1.52
Arsenic 15
Cadmium 3.7
Copper 360
Chromium 23
Lead 13
Mercury 1.2
Molyb- 29
denum
Nickel 31
Selenium 24
Zinc 860
Total
Phos- 14000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 2 j 3! 4 5 61 7 81 9i 101 11 121
DT/Ac./
App. I
Event 1.23
Arsenic 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037
Cadmium 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009
Copper 0.884 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.884
Chromium 0.056 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.056
Lead 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032
Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Molyb 0.071 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.071
denum
Nickel 0.076 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.076
Selenium 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.059
Zinc 2.112 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.112
Total
Phos- 34.384 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 34.384
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
Attig
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Wayne Farms, L.L.C., NC Total Dry Tons Applied(Annual): 7.47
Permit#: WQ0004609 Cation Exchange Capacity(non 503 only):
Operator: Ben Watson Owner: Ben Watson Predominant Soil Series: Clifford
Acres Used: 7.6 Acres Permitted: 7.6 Site#: NC SU 00022 Field#: SU 00022 0002
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 1 2 31 4 51 61 7 8 9 101 111 12
Com-
posite
Date 1/12/21
%Solids 1.52
Arsenic 15
Cadmium 3.7
Copper 360
Chromium 23
Lead 13
Mercury 1.2
Molyb- 29
denum
Nickel 31
Selenium 24
Zinc 860
Total
Phos- 14000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 12 j 3 4 51 6: 7 81 91 10, 1'11 1 12
DT/Ac./
App. m
Event 0.98
Arsenic 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029
Cadmium 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007
Copper 0.707 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.707
Chromium 0.045 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.045
Lead 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.057 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.057
denum
Nickel 0.061 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.061
Selenium 0.047 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.047
Zinc 1.689 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.689
Total
Phos- 27.496 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 27.496
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprison ent for knowing violations".
11 .� 2.A lit 2,
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Wayne Farms, L.L.C., NC Total Dry Tons Applied(Annual): 17.69
Permit#: WQ0004609 Cation Exchange Capacity (non 503 only):
Operator: Max&Peggy Wall Owner: Max&Peggy Wall Predominant Soil Series: Braddock
Acres Used: 13.7 Acres Permitted: 13.7 Site#: NC SU 00023 Field#: SU 00023 0001
Residual Analysis Data(Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 L23 3' 41 51 6 L7 8' 9 101 11 121
Com-
posite
Date 1/12/21
%Solids 1.52
Arsenic 15
Cadmium 3.7
Copper 360
Chromium 23
Lead 13
Mercury 1.2
Molyb- 29
denum
Nickel 31
Selenium 24
Zinc 860
Total
Phos- 14000
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total L 21 31 4 51 6 71 8 9 10, 111 i121
DT/Ac./ o
App.
Event 1.29
Arsenic 0.039 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.039
Cadmium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.010
Copper 0.930 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.930
Chromium 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.059
Lead 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034
Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Molyb 0.075 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.075
denum
Nickel 0.080 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.080
Selenium 0.062 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.062
Zinc 2.222 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 _ 2.222
Total
Phos- 36.176 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 36.176
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonme t for know' violations".
C)71..--- 2//$.:/Z'
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

SECTION 4

S a i' Summit Environmental Technologies,Inc.
17:4u 331 Win St.
ENVIRONMENTAL TECIiNOLOd',iES,INC Cuyahoga Falls,Ohio 44223
ArralyUcal Laboralorfas TEL:[phone] FAX.-[phone]
Website:http://www.settek.com
August 21,2019
Nate Roth
Synagro
284 Boger Rd.
Mocksville,NC 27028
TEL: [phone]
FAX: [phone]
RE: Wayne Farms
Dear Nate Roth: Order No.: 19071834
Summit Environmental Technologies, Inc. received 1 sample(s) on 7/26/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results,please feel free to call the
laboratory.
Sincerely,
177.4e€441°1--
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls,Ohio 44223
Arkansas 88-0735,California 07256CA,Colorado,Connecticut PH-0108,Delaware,Florida NELAC E87688,Georgia E87688,Idaho OH00923,Illinois
200061,Indiana C-OH-13,Kansas E-10347,Kentucky(Underground Storage Tank)3,Kentucky 90146,Louisiana 04061,Maryland 339,Minnesota
409711,New Hampshire 2996,New Jersey OH006,New York 11777,North Carolina 39705 and 631,North Dakota R-201,Ohio DW,Ohio VAP
CL0052,Oklahoma 9940,Oregon OH200001, Pennsylvania 010,Rhode Island LA000317,South Carolina 92016001,Texas T104704466-11-5,Utah
OH009232011-1,Virginia VELAP 9456,Washington C891
Page 1 of 36

5 M�'� Summit Environmental Technologies,Inc. Case Narrative
mu 331 Ohio Wm St.
AnalENVIRONMENTAL calLaoraloriNO LOGI ,INC. Cuyahoga Falls, 44223 WO#: 19071834rrafyt�caf iaboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com Date: 8/21/2019
CLIENT: Synagro
Project: Wayne Farms
WorkOrder Narrative:
19071834: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain-of-Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc.,Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19071834-001A TCLP-SVOC 8270E: Surrogate recovery was outside of the laboratory established
acceptance criteria for: p-Terphenyl-d14. All other surrogates exhibited recoveries within the
acceptance criteria.
Original
Page 2 of 36

� 3M m 1 or Summit Environmental Technol31oogies,In.
Wm s Qualifiers and Acronyms
Ekiwll�ONMEU1'AL TECHN❑LOGiES,INC Cuyahoga Falls,Ohio 442 WO#: 19071834
4rraly0cal Laboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.co, Date: 8/21/2019
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25%difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low(-)or high(+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low(-)or high(+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low(-)or high(+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low(-)or high(+).
S The spike result was outside of accepted recovery limits.
Z Deviation;A deviation from the method was performed;Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLvl Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 36

S
t�'T Summit Environmental Technologies,Inc. Workorder
3310 Win St.
MP ENVIRONMENTAL TECHriawc,3ES,iric, Cuyahoga Falls,Ohio 44223 Sample Summary
4rralyt�cai iaboralorlas TEL:[phone] FAX [phone] WO#: 19071834
Website:http://www.settek.com 21-Aug-19
CLIENT: Synagro
Project: Wayne Farms
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
19071834-001 Wayne Farms 7/25/2019 9:00:00 AM 7/26/2019 9:50:00 AM Sludge
Page 4 of 36

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a.7
w S IP it I Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
ENVIRONMENTAL TECHNOLOGIES,IF'C Cuyahoga Falls, Ohio 44223 (base report)
Mil 4rraly0cal Laboralorfas TEL:[phone] FAX..[phone] WON: 19071834
Website:http://www.settek.com Date Reported: 8/21/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 7/25/2019 9:00:00 AM
Lab ID: 19071834-001A
Project: Wayne Farms
Client Sample ID Wayne Farms
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS(SW1311/7470)
TCLP Mercury ND 0.00500 mg/L 1 8/2/2019 5:29:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW6010D SW3010A Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 8/5/2019 6:03:12 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 8/5/2019 6:03:12 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 8/5/2019 6:03:12 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 8/5/2019 6:03:12 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 8/5/2019 6:03:12 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 8/5/2019 6:03:12 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 8/5/2019 6:03:12 PM
FLASHPOINT DETERMINATION (1010) SW1010 Analyst: TAH
Flashpoint(140°F) ND °F 1 7/31/2019 12:01:41 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8270 SW3510C Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.200 mg/L 2 8/6/2019 6:13:00 PM
2,4,5-Trichlorophenol ND 0.500 mg/L 2 8/6/2019 6:13:00 PM
2,4,6-Trichlorophenol ND 0.500 mg/L 2 8/6/2019 6:13:00 PM
2,4-Dinitrotoluene ND 0.100 mg/L 2 8/6/2019 6:13:00 PM
Cresols,Total ND 10.0 mg/L 2 8/6/2019 6:13:00 PM
Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 8/6/2019 6:13:00 PM
Hexachlorobenzene ND 0.100 mg/L 2 8/6/2019 6:13:00 PM
Hexachloroethane ND 0.200 mg/L 2 8/6/2019 6:13:00 PM
Nitrobenzene ND 0.200 mg/L 2 8/6/2019 6:13:00 PM
Pentachlorophenol ND 0.500 mg/L 2 8/6/2019 6:13:00 PM
Pyridine ND 0.500 mg/L 2 8/6/2019 6:13:00 PM
Surr:2-Fluorophenol 20.7 10-109 %Rec 2 8/6/2019 6:13:00 PM
Surr: Phenol-d6 26.9 10-109 %Rec 2 8/6/2019 6:13:00 PM
Surr: Nitrobenzene-d5 24.2 19-120 %Rec 2 8/6/2019 6:13:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 6 of 36

a.7
w 5 IP it I Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
ENVIRONMENTAL TECHNOLOGIES,IF'C Cuyahoga Falls, Ohio 44223 (base report)
Mil 4rrafy0caf Laboralorfas TEL:[phone] FAX. [phone] WON: 19071834
Website:http://www.settek.com Date Reported: 8/21/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 7/25/2019 9:00:00 AM
Lab ID: 19071834-001A
Project: Wayne Farms
Client Sample ID Wayne Farms
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8270 SW3510C Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr:2,4,6-Tribromophenol 27.0 10-120 %Rec 2 8/6/2019 6:13:00 PM
Surr:2-Fluorobiphenyl 24.7 22-117 %Rec 2 8/6/2019 6:13:00 PM
Surr:p-Terphenyl-d14 25.9 34-116 S %Rec 2 8/6/2019 6:13:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: MES
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane,total ND 0.0250 mg/L 10 8/6/2019 4:13:00 PM
Toxaphene ND 0.0500 mg/L 10 8/6/2019 4:13:00 PM
Endrin ND 0.00500 mg/L 10 8/6/2019 4:13:00 PM
gamma-BHC ND 0.00500 mg/L 10 8/6/2019 4:13:00 PM
Heptachlor ND 0.00500 mg/L 10 8/6/2019 4:13:00 PM
Heptachlor epoxide ND 0.00500 d mg/L 10 8/6/2019 4:13:00 PM
Methoxychlor ND 0.00500 d mg/L 10 8/6/2019 4:13:00 PM
Surr:TCMX 47.1 10-119 %Rec 10 8/6/2019 4:13:00 PM
Surr: DCB 50.1 10-119 %Rec 10 8/6/2019 4:13:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8151A SW8151A Analyst: MES
TCLP HERBICIDES ANALYSIS (SW1311/8151)-SOLID
2,4-D ND 0.0100 d mg/L 1 8/13/2019 5:34:00 PM
2,4,5-TP ND 0.00500 mg/L 1 8/13/2019 5:34:00 PM
Surr: DCAA 99.9 20-140 %Rec 1 8/13/2019 5:34:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8260 Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.250 mg/L 50 8/5/2019 2:00:00 PM
1,2-Dichloroethane ND 0.250 mg/L 50 8/5/2019 2:00:00 PM
MEK ND 5.00 mg/L 50 8/5/2019 2:00:00 PM
Benzene ND 0.250 mg/L 50 8/5/2019 2:00:00 PM
Carbon tetrachloride ND 0.250 mg/L 50 8/5/2019 2:00:00 PM
Chlorobenzene ND 2.50 mg/L 50 8/5/2019 2:00:00 PM
Chloroform ND 0.250 mg/L 50 8/5/2019 2:00:00 PM
Tetrachloroethene ND 0.250 mg/L 50 8/5/2019 2:00:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 7 of 36

a.7
w S IP it I Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
ENVIRONMENTAL TECHNOLOGIES,IF'C Cuyahoga Falls, Ohio 44223 (base report)
Mil 4rrafy0caf Laboralorfas TEL:[phone] FAX. [phone] WON: 19071834
Website:http://www.settek.com Date Reported: 8/21/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 7/25/2019 9:00:00 AM
Lab ID: 19071834-001A
Project: Wayne Farms
Client Sample ID Wayne Farms
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8260 Analyst: CTB
TCLP VOLATILES ANALYSIS
Trichloroethene ND 0.250 mg/L 50 8/5/2019 2:00:00 PM
Vinyl chloride ND 0.100 mg/L 50 8/5/2019 2:00:00 PM
Surr:4-Bromofluorobenzene 93.9 70-130 %Rec 50 8/5/2019 2:00:00 PM
Surr: Dibromofluoromethane 97.3 70-130 %Rec 50 8/5/2019 2:00:00 PM
Surr:Toluene-d8 97.0 70-130 %Rec 50 8/5/2019 2:00:00 PM
RCISOLID-W/IGNITABILITY1030 SW9014 Analyst: MS
REACTIVE CYANIDE(9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.490 mg/Kg 1 7/31/2019 12:26:00 PM
RCI-SOLID-W/IGNITABILITY1030 SW9045D Analyst: WK
PH (SW9045D)
pH 6.7 s.u.@20.0C 1 7/29/2019 3:21:02 PM
RCI-SOLID-W/IGNITABILITY1030 SW9034 Analyst: MS
REACTIVE SULFIDE(9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 7/31/2019 12:26:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 8 of 36

SUMMIT Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7teS RenOrt
MP ENVIRONMENTAL TECHN❑LociEs,i Cuyahoga Falls,Ohio 44223 J Y
rral}'ticaf iaboralorlas TEL:[phone] FAX [phone] WO#: 19071834
Website:http://www.settek.com 21-Aug-19
Client: Synagro State: NW
Project: Wayne Farms Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
19071834-001A Sludge Flashpoint Determination(1010) Flashpoint(140°F) A
Sludge pH(SW9045D) Hydrogen Ion(pH) A
Sludge Reactive Cyanide(9014/7.3.3.2)-Solid Cyanide,Reactive U
Sludge Reactive Sulfide(9034)/7.3.4.2 Sulfide,Reactive U
Sludge TCLP Herbicides Analysis(SW1311/8151)-solid 2,4,5-TP A
Sludge TCLP Herbicides Analysis(SW1311/8151)-solid 2,4-D A
Sludge TCLP Mercury Analysis(SW1311/7470) Mercury A
Sludge TCLP Metals Analysis(SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis(SW1311/6010) Barium A
Sludge TCLP Metals Analysis(SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis(SW1311/6010) Chromium A
Sludge TCLP Metals Analysis(SW1311/6010) Lead A
Sludge TCLP Metals Analysis(SW1311/6010) Selenium A
Sludge TCLP Metals Analysis(SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis(SW1311/8081) Chlordane,total A
Sludge TCLP Pesticides Analysis(SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis(SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis(SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 1,4-Dichlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,5-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Cresols,Total A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pyridine A
Key Key
NC WW SCM A Accredited NC WW SCM U Unavailable
Version#2
Page 9 of 36

S u M t
• Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal�7 teS Report
2.7 ENWIRONM@NtAL TECHNaLOGES,iri Cuyahoga Falls,Ohio 44223 Analytes
rral}'Ocaf iaboralorlas TEL:[phone] FAX [phone] WO#: 19071834
Website:http://www.settek.com 21-Aug-19
Client: Synagro State: NW
Project: Wayne Farms Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
19071834-001A Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
Key Key
NC WW SCM A Accredited NC WW SCM U Unavailable
Version#2
Page 10 of 36

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Page 35 of 36

SUMMIT
Summit Environmental Technologies,Inc.
OMrg 3310 Win St.
ArraitOt al Lab L7farios OGi S,IF# Cuyahoga Falls, Ohio 44223 Sample Log-In Check List
�irrafytica�LaboralarJas TEL:[phone] FAX. [phone]
Website:http://www.settek.com
Client Name: SYN-NC-27028 Work Order Number: 19071834 RcptNo: 1
Logged by: John A.Semenik 7/26/2019 9:50:00 AM
Completed By: Jacqueline Rasile 7/26/2019 11:18:05 PM
Reviewed By: Jennifer Woolf 7/29/2019 2:54:58 PM (...710‘7*.?1' )7700aA/01"i•-
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? FedEx
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0°C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s)in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
g. Are samples(except VOA and ONG)properly preserved? Yes ❑d No ❑
10. Was preservative added to bottles? Yes ❑ No ❑d NA ❑
it Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials V
12. Were any sample containers received broken? Yes ❑ No ❑d
13. Does paperwork match bottle labels? Yes ❑d No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody? Yes ❑d No ❑
15. Is it clear what analyses were requested? Yes ❑d No ❑
16. Were all holding times able to be met? Yes ❑d No ❑
(If no, notify customer for authorization.)
Special Handling(if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA V
Person Notified: I Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18.Additional remarks:
Cooler Information
Cooler No Temp°C Condition Seal Intact Seal No Seal Date Signed By
1 4.5 Good Not Present
Page 36 of 36

SECTION 5

Wayne Farms Land Application Program
Permit #WQ0004609
Calendar Year 2021
Animal processing wastewater residuals were land applied in
two events in the year 2021. The biosolids were sampled at the
beginning of the year to cover the entire year since we hauled
less than 300 dry tons per year.
The biosolids land applied in 2021 had sufficient lime added to
raise the pH of the uniform mixture to a pH of 10 for thirty
minutes prior to being surface land applied. This was
performed to control possible nuisance conditions (see Section
II, Item 7 in permit #WQ0004609).

SECTION 6

Agricultural Lime Application Log
Year: 2021
Project: Wayne farms
Field Soil Lime Requirement Tons/Acre Date Applied
(state-county-site-field) pH (from soil analysis) Applied(CCE Eq.)
SU-13-6 6.9 0.0T/Ac.
SU-20-1 5.6 0.0 T/AC
SU-22-1 6.8 0.0T/Ac.
SU-22-2 6.7 0.0T/Ac.
SU-23-1 5.7 0.0T/Ac.
Lime is in the sludge

SECTION 7

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