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WQ0039924_2021 Residual Annual Report_20220224
Non-Discharge Branch Upload/Submittal Form �. NORTH CAROLINA EnWrvnmenfol Quoity Version 2-Revised June 23,2020 Initial Review Reviewer Thornburg,Nathaniel D Is this submittal an application?(Excluding additional information.)* Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2021 Permit Number(IR)* WQ0039924 Applicant/Permittee von Drehle Corporation Email Notifications Does this need review by the hydrogeologist?* Yes • No Regional Office Fayetteville CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence. ............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................ Name* Robert T.Branch Email Address* Phone Number* bbranch@branchrs.com 3363129007 Project Information Application/Document Type* New(Fee Required) Modification-Minor Modification-Major(Fee Required) Renewal Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1, Required) NDAR-2 Annual Report Residual Annual Report Additional Information Change of Ownership Other We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High-Rate Infiltration Other Wastewater Reclaimed Water Closed-Loop Recycle Residuals Single-Family Residence Wastewater Other Irrigation Permit Number:* WQ0039924 Has Current Existing permit number Applicant/Permittee Address* von Drehle 126 First Street Cordova,NC 28330 Facility Name* von Drehle Corporation Class A Residuals Program Please provide comments/notes on your current submittal below. At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form,Engineering Plans,Specifications,Calculations,Etc.) Class A 2021 Annual Report von Drehle.pdf 10.66MB Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre-review until the fee(if required)has been received by the Non- Discharge Branch.Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order(as specified by the application). Mail payment to: NCDEQ—Division of Water Resources Attn:Non-Discharge Branch 1617 Mail Service Center Raleigh,NC 27699-1617 Signature d Submission Date 2/24/2022 2021 ANNUAL REPORT VON DREHLE CORPORATION FIBER CLAY RESIDUAL CORDOVA,NORTH CAROLINA CLASS A PERMIT#WQ0039924 Prepared For: Von Drehle Corporation 126 First Street Cordova,N.C. 28330 Prepared By: 1114 Branch Residuals& Soils, LLC 1735 Heckle Blvd. Suite 103-291 Rock Hill SC,29732 February 2022 BRANCH RESIDUALS & SOILS, LLC 1735 Heckle Blvd,Suite 103-291,Rock Hill,SC 29732 PHONE (336)312-9007 February 10, 2022 North Carolina Department of Environmental Quality Division of Water Resources 1617 Mail Service Center Raleigh,North Carolina 27699-1617 Reference: 2021 CLASS A LAND APPLICATION ANNUAL REPORT Von Drehle Corporation. Cordova,North Carolina Permit No. WQ0039924 BR&S Project No. 2014-110 Information Processing Unit: Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced permit on behalf of Von Drehle Corporation for their facility in Cordova, North Carolina. This report includes: Distribution and Marketing Certification and Summary Form. Distributions were made from January to April and November— December during 2021. These distributions totaled 26,568.51 wet tons (9,958.53 dry tons). These applications were surface spread and incorporated into the soil. This is a reminder that Permit WQ0005135 the Class B permit for von Drehle was rescinded and an annual report was submitted for that permit earlier in 2021. Application activities were not performed during 2021 this permit. Immediately following this page is the no application certification form for this Class B permit. If any further information is required regarding this land application program, please do not hesitate to contact me at (336) 312-9007. Sinc rely, /1 ii; Robert T. Branch, L.S.S. Land Application/Residuals Operator #15676 RTB Enclosures ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0005135 County: _ Richmond Year: 2021 Facility Name(as shown on permit): von Drehle Corporation Land Application Operator: Bio-Nomic Services,Inc Phone: (704)529-0000 Land application of residuals as allowed by the permit occurred during the past calendar year? Cl Yes E] No -If No,skip Part A,and Part B and proceed to Part C. Also,If residuals were generated but not land applied,please attach an explanation on how the residuals were handled. Part A-Residuals Application Summary: Total number of application fields in the permit: 18 Total number of fields utilized for land application during the year: 0 Total amount of dry tons applied during the year for all application sites: 0.00 Total number of acres utilizes for land application during the year: 0.00 Part B-Annual Comniance Statement: Facility was compliant during calendar year 2021 with all conditions of the land application permit (including but not limited to items 1-13 below)issued by the Division of Water Quality. ❑ Yes 0 No If no please,provide a written description why the facility was not compliant,the dates,and explain corrective action taken. I) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)copies of laboratory results are attached. 4) Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1105(a)or the Pollutant Loading Rates in 15A NCAC 02T.1105(b)(applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or,in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals,as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C-Certification: "I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate, and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." Mr.Justin Dawkins,Cordova Plant Manager Permittee .in; and Ti pe or print) nature of Permittee Date C (2-11/t- Signatu - of Preparers` Date attire of Land Applier Date~ (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T.1102(26) DENR FORM ACF(12/2006) TABLE OF CONTENTS SECTION NO. TITLE I Distribution and Marketing Certification and Summary Forms II Annual Residual Sampling Summary Form III Residual Analysis Lab Sheets IV Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report V Pathogen and Vector Attraction Reduction Forms VI Pathogen and Vector Attraction Reduction Documentation DISTRIBUTION AND MARKETING CERTIFICATION AND SUMMARY FORM W O 0 0 O au 0 0 0 0 00 ... nl 'O 'II -0 •a b b 'C 'O 'O •b St 1 err Q) W O d 0 0 Q) d 0 N 1) 4 '.'. •.'. e oa oo 0000 a000 : _ o T. .S our a. z .4 a D conp A $ e o O N 1G M N 0 N N 1D .-. 0 . m 3 Y 2 lE m Noo 010ora oo, cMno o `� C o O qw `..� 00 tC leiT d' c D 7 M el Cn o cr O gl Q d C ❑ W #• e) .�N.."b � OO�i,o�o�� Mp � °r; NKO M v] `� O IIaN •-. ^ NN •� N � LY .I3 .�H A A re CI U A4 `' 8 ''' 48 U 4Q ,Z >+ Z e1; S 2 o O a '" \a Ai d 8 6 o 1...1 g .r am .� 'a �. a ... o N COH r- 01 cc l� AO Mco en ti M R p '�a 04 w.. W Q.[ Qi C�0.❑ U DO 4C 41 T_ 01 M !h l- C cn $ �j 1r •� •a \1 0 V U O i�i 'D VN'1� b O a ono..... p .M-. ,-.co N in r. o T +' ea C y �444 ^ 'V N ^ N N N N N cal x' et •iy L=' D .1.•qee o owe-. N Ci'd mi.° 4.r •,� w 1. ++ N �p M [� O l- I- 1G ,-. M M b Q O. 4.. C c'• �. , 7,1 N co l� 01 0o n d: d' O oN en a p dp: by r O O m un aL,0 'O o Nn � � privMef en oo[� o `net -48 *t v A ..�. 0 ,,. 'i7 " „. —, O O O'000 .�, p N h O M 44 O oq OP4 .-i •� N N •� .r N N N N N•�-• N W (� A V Pits C v� S ' ' 2 .� �J' v a ?°i > A � w a "3 ry -f O N Ci ua u ep ea 8 Q a '� o �° o�' O O O O ,� 1i ��„ r: 'o Q � � L 3 � � F �, ,; N O � � �,C a U z � � d o a. z r. 1: .� 8. V h E-1 c� U a .S u s 5a 4 ,, V rrI� w ill 0 m _al y 4" •3 a c. •S d VI el ›, •� We C V ts �* V y a m � or2 o 1.1 AHh.UA 4I O ti . a En 8 a. ! a ,o o > �, 44 -8 l'D G4 C. Q=G 49 ti Q V Z E r V M Cn* I31 rat Mt•-: C * ANNUAL RESIDUAL SAMPLING SUMMARY FORM co NO h c O T.,..en NI ciN ¢ M - O eet �p iv et V 44 — IV en 6i = e o m I O O O y 7 O O O •� C°7 sa- M z ry s M = Q a , ca _ re [V n A [C N ci $ Q N g S C• g O to C Y� M CV z t+f h ea154 ..n 7 ge . C Li ., N O N 8 o Oi 'V ao r: el p .d4 t a ry S R N • v v a `en n V r' a $ V e~' v •r•-• h M v; 0 4.4 40 3 rl rm era d• en N N p p �j O O O �o O r O S O O v w Ci Q M M N sp Q M e !''1 Cy \p ,p o0 (�( n O — •M 6 fA O 0 M V v z `o o N — •v r- `^ 8 a C •C ° o CzI , O R es $Q N ri el C` c v i 7 ea >s �o vVNZ dofcN n c a IA " mI. o ' dO Q• �7 0 rs M V v eV C e O V .O • -• y �i co 4gr l0 i� V _ a .. _ = 1) y p • �Q .O M p O t0 m g rf Q M r7Q. cl cl o u? • V g ,i 0 y 4 h V V M aa ° Q+ C4 y i C .O , C. V — N V N r V 0e0 O CC C603 O� C p p �p^n CV CA C M V 'g w O co h N v7 ri m P. '" ep as DO O S S O M g nit ,-,- est 'O > n V $ N z O o �d o _ r •V. `.. N• „' -0 a `0 O o ++ C [r3C G x A M g = ¢Q is," n 5 Q o e n n c h y op O p it 0 o Cs •ge,74 ye� C C M wi Q b N °I Q r OM G ono N �NNy p . • tri $ 0 ,° C M V O N z V 9 M •O h $ 1-1 V . S Q ev0 I. in it let m ''�' 3pA. aiUz � o�og2o� '%� rNgg ¢ ¢ ¢ ¢ o ° _ \ a, g Z Z.) uz V v -• � zzzz e v pt 3 A •• c "0 e o k r. ° e o, ,� 6j w EEA ■•1 y •� O W +� a C Ca Ts El ON • ema a au j zaEoss 4' 'j V .-• 0.)i i.�c b VE 0 Ell al Y C H rn * RESIDUAL ANALYSIS LAB SHEETS Waypoint -_) 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 1/26/2021 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC,29732 Ref: Analytical Testing Lab Report Number:21-018-0041 Client Project Description: Sludge Testing von Drehle Cordova Project#2014-110 Dear Mr. Bob Branch: Waypoint Analytical, LLC.received sample(s)on 1/16/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.Where the laboratory was not responsible for the sampling stage(refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017)and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters,where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters(chlorine, pH,dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of sampling. Usually,but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated.This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option,repeating the analysis in question at laboratory's expense,or the refund of the charges paid for performance of said analysis. Page 1 of 9 ,r,.! 0 .. • . I !aypoo Dt. 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Certification Summary Laboratory ID:WP MTN:Waypoint Analytical,LLC.,Memphis,TN State Program Lab ID Expiration Date _ J Alabama State Program 40750 02/28/2021 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 06/30/2021 Florida State Program-NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program-NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2021 Louisiana State Program-NELAP LA037 12/31/2021 Louisiana State Program-NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program-NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program-NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program-NELAP 460181 09/14/2021 Page 1 of 1 00001/21-018-0041 Page 2 of 9 • 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-018-0041 Client Project Description: Sludge Testing von Drehle Cordova Project# 2014-110 Lab No Client Sample ID Matrix Date Collected Date Received 86780 Sludge Solids 01/13/2021 01/16/2021 Page 3 of 9 Waypoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Client: Branch Residuals and Soils LLC CASE NARRATIVE Project:Sludge Testing Lab Report Number:21-018-0041 Date: 1/26/2021 Metals Analysis Method 6010D Sample 86954 Analyte:Aluminum QC Batch No:L532610 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte:Arsenic QC Batch No: L532610 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Calcium QC Batch No:L532349 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Cadmium QC Batch No: L532349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Copper QC Batch No: L532349 The matrix spike,matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Iron QC Batch No: L532610 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L532610 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Magnesium QC Batch No: L532349 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Manganese Page 4 of 9 V 'aypoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com QC Batch No: L532349 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte:Molybdenum QC Batch No: L532349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte:Sodium QC Batch No: L532349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Nickel QC Batch No: L532349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Phosphorus QC Batch No: L532349 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Lead QC Batch No:L532349 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Selenium QC Batch No: L532349 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Zinc QC Batch No: L532349 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Page 5 of 9 ,...447:7-6 • , t\y f s ] O!nt -A 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr.Bob Branch Report Date: 01/26/2021 1735 Heckle Blvd Information: von Drehle Cordova Received:01/16/2021 Suite 103-291 Project#2014-110 Rock Hill, SC 29732 Report Number:21-018-0041 REPORT OF Lab No: 86780 Matrix: Solids Sample ID:Sludge Sampled: 1/13/2021 0:00 Test Results Units MOL DF Date I Time By Analytical Analyzed Method Moisture 60.4 % 0.010 1 01/18/21 17:00 FMM 2540G-2011 Ammonia Nitrogen 462 mg/Kg-dry 63.1 1 01/25/21 10:30 JPJ 4500NH3C-2011 Nitrate(NO3-N) <2.53 mg/Kg-dry 2.53 1 01/21/21 15:38 BKN 9056A Nitrite(NO2-N) <2.53 mg/Kg-dry 2.53 1 01/21/21 15:38 BKN 9056A Nitrate+Nitrite-N <2.53 mg/Kg-dry 2.53 1 01/21/21 15:38 9056A Organic N 575.8 mg/Kg-dry 126.3 1 01/25/21 10:30 CALCULATION pH 7.5 s.u. 1 01/25/21 15:16 CxC 9045D Total Solids 39.6 % 0.010 1 01/18/21 17:00 FMM 2540G-2011 Total Volatile Solids 41.5 % 0.010 1 01/18/21 17:00 FMM 2540G-2011 Total Kjeldahl Nitrogen 1040 mg/Kg-dry 126 1 01/25/21 15:55 CLP 4500NORGD-2011 Phosphorus 144 mg/Kg-dry 12.6 1 01/21/21 06:42 US 6010D Aluminum 2630 mg/Kg-dry 12.6 1 01/21/21 06:42 TJS 6010D Arsenic <1.26 mg/Kg-dry 1.26 1 01/21/21 18:54 DADS 6010D Cadmium <0.253 mg/Kg-dry 0.253 1 01/21/21 06:42 TJS 6010D Calcium 192000 mg/Kg-dry 2530 20 01/21/21 18:59 DADS 6010D Copper 25.8 mg/Kg-dry 1.26 1 01/21/21 06:42 TJS 6010D Iron 1050 mg/Kg-dry 25.3 1 01/21/21 06:42 DADS 6010D Lead <0.757 mg/Kg-dry 0.757 1 01/21/21 06:42 TJS 6010D Magnesium 2210 mg/Kg-dry 12.6 1 01/21/21 06:42 TJS 6010D Manganese 41.7 mg/Kg-dry 1.26 1 01/21/21 06:42 TJS 6010D Mercury <0.0371 mg/Kg-dry 0,0371 1 01/22/21 10:39 DDB 7471A Molybdenum 3.61 mg/Kg-dry 0.631 1 01/21/21 06:42 TJS 6010D Nickel 0.866 mg/Kg-dry 0.631 1 01/21/21 06:42 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 6 of 9 �J1y VVayp oin 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr.Bob Branch Report Date: 01/26/2021 1735 Heckle Blvd Information: von Drehle Cordova Received:01/16/2021 Suite 103-291 Project#2014-110 Rock Hill, SC 29732 Report Number:21-018-0041 REPORT OF ANALYSIS Lab No: 86780 Matrix: Solids Sample ID:Sludge Sampled: 1/13/2021 0:00 Test Results Units MCL DF Date I Time By Analytical Analyzed Method Potassium 66.7 mg/Kg-dry 25.3 1 01/21/21 06:42 JADS 6010D Selenium 4.52 mg/Kg-dry 1.26 1 01/21/21 06:42 T]S 6010D Sodium 598 mg/Kg-dry 63.1 1 01/21/21 06:42 T]S 6010D Zinc 72.2 mg/Kg-dry 3.16 1 01/21/21 06:42 TB 6010D Neutralizing Value(%CCE) 52.9 % 0.1 1 01/25/21 10:03 DXT AOAC 955.01 Qualifiers/ OF Dilution Factor L Limit Exceeded Definitions Page 7 of 9 (0- Wayp 'nt 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400*Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:22972 Customer Name: Branch Residuals and Soils LLC Report Number: 21-018-0041 Shipping Method Fed Ex US Postal Lab Other: UPS Client Courier Thermometer ID: fT99 Shipping container/cooler uncompromised? Yes No Number of coolers/boxes received r 1 Custody seals intact on shipping container/cooler? Yes No • Not Present Custody seals intact on sample bottles? Yes No • Not Present Chain of Custody(COC)present? • Yes No COC agrees with sample label(s)? • Yes No COC properly completed • Yes No Samples in proper containers? • Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test(s)? Yes No All samples received within holding time? • Yes No Cooler temperature in compliance? • Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water-Sample containers properly preserved Yes No • N/A Water-VOA vials free of headspace Yes No • N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035—compliance criteria met Yes No • N/A High concentration container(48 hr) Low concentration EnCore samplers(48 hr) High concentration pre-weighed (methanol-14 d) Low conc pre-weighed vials(Sod Bis-14 d) Special precautions or instructions included? Yes • No Comments: Signature: Summer Harrison Date&Time: 1 18 2021 09:44:33 Page 8 of 9 I he follo►►mng parameters need to be analyzed on the sample liar on Drehle Regular Nutrient and Metal Residuals Anah.s s Arsenic Cadmium Copper Lead Mercury Mot}bdenum Nickel Selenium Zinc Aluminum Ammonia-Nitrogen Nitrate-Nitrite Nitrogen %'total Solids pl t Phosphorus Potassium TKN CCE. Calcium Magnesium Sodium Iron Certification required by: NC'DEQ Immediately notiliy me if this certification is not valid. Collected on. 1 13 2021 State to he used for Compliance North Carolina Collected by: Bob Branch Project: on Drehle Cordova Branch Residuals& Soils Project No 2014-1 10 336 3 1 2-9007 Bill Branch Residuals& Soils for Payment '1 Robert Branch Account number 22972 I t/1 Li 17- I (0 Ca f I�allllhllllllllll � 2t Ul&0 , Br.tncn Rseirrals.inrl Sods LLCl ll�ll�l�llll�Dl Ia 202I 5lurine Teshrm 09 39 3 t Page 9 of 9 'a of nt l 2790 Whitten Road,Memphis,TN 38133 y� Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 3/19/2021 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC,29732 Ref: Analytical Testing Lab Report Number:21-062-0168 Client Project Description:Von Drehle Cordova Biosolids Testing Project#2014-110 Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s)on 3/3/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.Where the laboratory was not responsible for the sampling stage(refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017)and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters,where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters(chlorine, pH,dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of sampling. Usually, but not always,any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated.This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, QOro `_)— Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option,repeating the analysiss in question at laboratory's expense,or the refund of the charges paid for performance of said analysis. ly tof Page 1 of 8 • Waypo I■ ■t. 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalyticai.com Certification Summary Laboratory ID:WP MTN:Waypoint Analytical,LLC., Memphis,TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2021 Florida State Program-NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program-NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2021 Louisiana State Program-NELAP LA037 12/31/2021 Louisiana State Program-NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program-NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program-NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program-NELAP 460181 09/14/2021 Page 1 of 1 00001/21-062-0168 Page 2 of 8 ° Wa tC J co'nt' 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanaiytical.com Sample Summary Table Report Number: 21-062-0168 Client Project Description: Von Drehle Cordova Biosolids Testing Project#2014-110 Lab No Client Sample ID Matrix Date Collected Date Received 88200 VD Solids 02/28/2021 16:13 03/03/2021 Page 3 of 8 -Th853) 2790 Whitten Road,Memphis,TN 38133 VVaypoiflt.. Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Von Drehle Cordova Mr.Bob Branch Report Date: 03/19/2021 1735 Heckle Blvd Information: Blosolids Testing Received:03/03/2021 Suite 103-291 Project#2014-110 Rock Hill, SC 29732 Report Number:21-062-0168 REPORT OF ANALYSIS Lab No: 88200 Matrix: Solids Sample ID:VD Sampled: 2/28/2021 16:13 Test Results Units MOL DF Date/Time By Analytical Analyzed Method Moisture 60.6 % 0.010 1 03/05/21 15:48 FMM 2540G-2011 Ammonia Nitrogen <254 mg/Kg-dry 254 1 03/10/21 15:00 JP] 4500NH3C-2011 Nitrate(NO3-N) <2.54 mg/Kg-dry 2.54 1 03/08/21 17:01 JCA 9056A Nitrite(NO2-N) <2.54 mg/Kg-dry 2.54 1 03/08/21 17:01 JCA 9056A Nitrate+Nitrite-N <2.54 mg/Kg-dry 2.54 1 03/08/21 17:01 9056A pH 8.1 s.u. 1 03/09/20 16:00 ADM 9045D Total Solids 39.4 % 0.010 1 03/05/21 15:48 FMM 2540G-2011 Total Kjeldahl Nitrogen 454 mg/Kg-dry 127 1 03/09/21 16:16 CLP 4500NORGD-2011 Phosphorus 140 mg/Kg-dry 12.7 1 03/10/21 00:02 DADS 6010D Aluminum 2080 mg/Kg-dry 12.7 1 03/10/21 22:35 DADS 6010D Arsenic 3.71 mg/Kg-dry 1.27 1 03/10/21 00:02 JADS 6010D Cadmium <0.254 mg/Kg-dry 0.254 1 03/10/21 00:02 DADS 6010D Calcium 231000 mg/Kg-dry 12700 100 03/10/21 22:55 DADS 6010D Copper 19.0 mg/Kg-dry 1.27 1 03/10/21 00:02 ]ADS 6010D Iron 1480 mg/Kg-dry 25.4 1 03/10/21 00:02 lADS 6010D Lead 1.08 mg/Kg-dry 0.761 1 03/10/21 00:02 DADS 6010D Magnesium 2520 mg/Kg-dry 12.7 1 03/10/21 00:02 LADS 6010D Mercury <0.0368 mg/Kg-dry 0.0368 1 03/08/21 12:04 DDB 7471A Molybdenum 6.42 mg/Kg-dry 0.634 1 03/10/21 00:02 ]ADS 6010D Nickel 1.69 mg/Kg-dry 0.634 1 03/10/21 00:02 DADS 6010D Potassium 63.5 mg/Kg-dry 25.4 1 03/10/21 00:02 DADS 6010D Selenium i.70 mg/Kg-dry 1.27 1 03/10/21 22:35 DADS 6010D Sodium 840 mg/Kg-dry 63.5 1 03/10/21 00:02 DADS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 8 • f Wa o'nt '� 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Von Drehle Cordova Mr.Bob Branch Report Date: 03/19/2021 1735 Heckle Blvd Information: Biosolids Testing Received:03/03/2021 Suite 103-291 Project#2014-110 Rock Hill, SC 29732 Report Number:21-062-0168 REPORT OF ANALYSIS Lab No: 88200 Matrix: Solids Sample ID:VD Sampled: 2/28/2021 16:13 Test Results Units MOL DF Date l Time By Analytical Analyzed Method Zinc 85.5 mg/Kg-dry 3.17 1 03/10/21 00:02 ]ADS 6010D Neutralizing Value(%CCE) 55.2 % 0.1 1 03/08/21 11:45 DXT AOAC 955.01 Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 5 of 8 Waypo i nt � 1— 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:22972 Customer Name: Branch Residuals and Soils LLC Report Number: 21-062-0168 Shipping Method Fed Ex US Postal Lab Other: • UPS Client Courier Thermometer ID: 1ff101 Shipping container/cooler uncompromised? • Yes No Number of coolers/boxes received r 1 Custody seals intact on shipping container/cooler? Yes No • Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of Custody(COC)present? • Yes No COC agrees with sample label(s)? • Yes No COC properly completed • Yes No Samples in proper containers? i♦ Yes No Sample containers intact? • Yes No Sufficient sample volume for indicated test(s)? t♦ Yes No All samples received within holding time? • Yes No Cooler temperature in compliance? • Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water-Sample containers properly preserved Yes No • N/A Water-VOA vials free of headspace Yes No • N/A Trip Blanks received with VOAs Yes No t♦ N/A Soil VOA method 5035—compliance criteria met Yes No f♦ N/A High concentration container(48 hr) Low concentration EnCore samplers(48 hr) High concentration pre-weighed (methanol-14 d) Low conc pre-weighed vials(Sod Bis-14 d) Special precautions or instructions included? Yes i♦ No Comments: Signature: KristinaA.McAdams Date&Time: 3 03 2021 15:45:57 Page 6 of 8 6 a 3 E E E N n , > ,a o C N ` I' -Ir c o on u al i tr e N N11 >' 0 z t o^H v 2 E c :. 0, o gir�r' aY, E o .. _ c '� Vp `,' (� 4 oS n p Vp 1Y7 Q, d 0.1•' 0 . O N Z 2 N I p N > v V I z z 2 = T V 4-, n• y 3 '141 2 `f1 c o,x, ��(., W L, W L. 6C7 Q14 > > > ( cc cc ce '( N 4 N H J M l7 49 9 I.. i in =U. .o a � �� 3 1 d � s N a a • 4 MICA ® ° • a, u K Q R c Siv E E EY SDZ _. —" Q N L 9 1.a Cl D Y a E E E7 E E O w � t Y ' Y I ME - > Q P i- h o U ,� o. 7 L x U - o tV ,o n IDa a _ 'v o m o 0 m �¢ r jp s u p r ilt�cP'(c% J_ 4 jd q N > u d -.Si W W a, ,� N Y d z z ze s is 1 I i -43 a3,sodwo)))Jo gei)g) U z r r p t a )Aap al Ja}aa)ruleyq a c G n ;• 91L siauIe3uoa fo iagwnN N z c n 12 2 - .. t� C u c p 9 a m `Q o .• ,c "z i �a c c M G O V ,x '� f '1l C ' ~ !e EEC \i' Y d .L. ; r °i,, ti 9 C______ c, u. IIN z a_ ZS c C A L 0J - - 9 C� Z , , v tt " v�J • -...... —U _ ar. _ �C �- o d, E ,E \ - T • J r3 ? c al z , C C\p Y Q Y :� 74 4 I f 3,.. m Uti ZnA a 4 Page 7 of 8 The folloNN ing parameters need to be analy,ed on the sample tier%on Drehle Regular Nutrient and Metal Residuals Analysis Arsenic Cadmium Copper Lead Mercury Molybdenum Nickel Selenium Zinc Aluminum Ammonia-Nitrogen Nitrate-Nitrite Nitrogen Total Solids p1•I Phosphorus Potassium TKN CCE Calcium Magnesium Sodium Iron Certification required by: NCDEQ Immediately notitiy me if this certification is not valid. Collected on: 2/28/2021 State to he used for Compliance North Carolina Collected by: Bob Branch Project: von Drehle Cordova Branch Residuals & Soils Project No 2014-I 10 336 312-9007 Bill Branch Residuals & Soils fir Payment Robert Branch Account number 27972 I IIIIII III 11IBranch rIL11II AI11!II11N 111111I Ij 1i.uals and Sok 3 L11 02" Vun Orehle Cordova 15 45 18 Page 8 of 8 Waypoint 2790 Whitten Road,Memphis,TN 38133 a Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 3/30/2021 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill,SC,29732 Ref: Analytical Testing Lab Report Number:21-078-0132 Client Project Description: Sludge Testing Project#2014-110 Dear Mr. Bob Branch: Waypoint Analytical, LLC.received sample(s)on 3/19/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.Where the laboratory was not responsible for the sampling stage(refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations,instrumentation maintenance and calibration for all parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017)and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters,where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters(chlorine,pH,dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of sampling. Usually,but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated.This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Cc)On,LoOS-Q_ ().3—,--Q- Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option,repeating the analysis in question at laboratory's expense,or the refund of the charges paid for performance of said analysis. - risa Page 1 of 8 d 'avo• vik';' 2790 Whitten Road,Memphis,TN 38133 i nt. Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.corn Certification Summary Laboratory ID:WP MTN:Waypoint Analytical,LLC.,Memphis,TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2021 Florida State Program-NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program-NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2021 Louisiana State Program-NELAP LA037 12/31/2021 Louisiana State Program-NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program-NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program-NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program-NELAP 460181 09/14/2021 Page 1 of 1 00001/21-078-0132 Page 2 of 8 WaYPOint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-078-0132 Client Project Description: Sludge Testing Project#2014-110 Lab No Client Sample ID Matrix Date Collected Date Received 97035 VD Solids 03/17/2021 14:25 03/19/2021 Page 3 of B Waypoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Client: Branch Residuals and Soils LLC CASE NARRATIVE Project: Sludge Testing Lab Report Number:21-078-0132 Date: 3/30/2021 Metals Analysis Method 6010D Sample 97043 Analyte:Aluminum QC Batch No:L543893 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Iron QC Batch No: L543893 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No:L544305 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97035(VD) Analyte: Potassium QC Batch No: L544305/L543453 Target analyte(s)was identified in the method blank associated with this project. Per laboratory protocol any associated affected sample result is flagged"B"to indicate that it was detected in the method blank. Anions by Ion Chromatography Method 9056A Sample 97616 Analyte: Nitrate-N QC Batch No: L544088 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Page 4 of 8 0off. Y Way;. Dint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400 1'Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr.Bob Branch Report Date: 03/30/2021 1735 Heckle Blvd Information: Project#2014-110 Received:03/19/2021 Suite 103-291 Rock Hill, SC 29732 Report Number:21-078-0132 REPORT OF ANALYSIS Lab No: 97035 Matrix: Solids Sample ID:VD Sampled: 3/17/2021 14:25 Test Results Units MOL DF Date/Time By Analytical Analyzed Method Moisture 60.5 % 0.010 1 03/22/21 15:55 FMM 2540G-2011 Ammonia Nitrogen 322 mg/Kg-dry 253 1 03/29/21 09:00 JPJ 4500NH3C-2011 Nitrate(NO3-N) <2.53 mg/Kg-dry 2.53 1 03/26/21 12:21 JCA 9056A Nitrite(NO2-N) <2.53 mg/Kg-dry 2.53 1 03/26/21 12:21 JCA 9056A Nitrate+Nitrite-N <2.53 mg/Kg-dry 2.53 1 03/26/21 12:21 9056A Organic N 394.9 mg/Kg-dry 253.2 1 03/29/21 09:00 CALCULATION pH 7.8 s.u. 1 03/25/21 16:30 ADM 9045D Total Solids 39.5 % 0.010 1 03/22/21 15:55 FMM 2540G-2011 Total Volatile Solids 43.2 % 0.010 1 03/22/21 15:55 FMM 2540G-2011 Total Kjeldahl Nitrogen 716 mg/Kg-dry 127 1 03/30/21 15:49 CLP 4500NORGD-2011 Phosphorus 142 mg/Kg-dry 12.7 1 03/27/21 01:05 TJS 6010D Aluminum 2320 mg/Kg-dry 12.7 1 03/29/21 23:53 TJS 60100 Arsenic <1.27 mg/Kg-dry 1.27 1 03/27/21 01:05 TJS 6010D Cadmium <0.253 mg/Kg-dry 0.253 1 03/27/21 01:05 TJS 6010D Calcium 204000 mg/Kg-dry 12700 100 03/29/21 23:58 TJS 6010D Copper 27.8 mg/Kg-dry 1.27 1 03/27/21 01:05 TJS 6010D Iron 1370 mg/Kg-dry 25.3 1 03/27/21 01:05 TJS 6010D Lead <0.759 mg/Kg-dry 0.759 1 03/27/21 01:05 TJS 6010D Magnesium 1980 mg/Kg-dry 12.7 1 03/27/21 01:05 TJS 6010D Manganese 45.1 mg/Kg-dry 1.27 1 03/27/21 01:05 TJS 6010D Mercury <0.0359 mg/Kg-dry 0.0359 1 03/24/21 13:46 DDB 7471A Molybdenum 4.58 mg/Kg-dry 0.632 1 03/27/21 01:05 TJS 6010D Nickel 0.681 mg/Kg-dry 0.632 1 03/27/21 01:05 TJS 6010D Qualifiers/ B Analyte detected in blank OF Dilution Factor Definitions L Limit Exceeded MQL Method Quantitation Limit Page 5 of 8 T 4 f £ V4/aypoi nt Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr.Bob Branch Report Date: 03/30/2021 1735 Heckle Blvd Information: Project#2014-110 Received:03/19/2021 Suite 103-291 Rock Hill, SC 29732 Report Number:21-078-0132 REPORT OF ANALYSIS Lab No: 97035 Matrix: Solids Sample ID:VD Sampled: 3/17/2021 14:25 Test Results Units MIL DF Date/Time By Analytical Analyzed Method Potassium 57.2 B mg/Kg-dry 25.3 1 03/29/21 23:53 TJS 60100 Selenium 1.58 mg/Kg-dry 1.27 1 03/27/21 01:05 TJS 6010D Sodium 603 mg/Kg-dry 63.3 1 03/27/21 01:05 TJS 6010D Zinc 97.7 mg/Kg-dry 3.16 1 03/27/21 01:05 TJS 6010D Qualifiers/ B Analyte detected in blank DF Dilution Factor Definitions L Umit Exceeded MQL Method Quantitation Umit Page 6 of 8 • vE2 Vaypoi nt 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:22972 Customer Name: Branch Residuals and Soils LLC Report Number: 21.078-0132 Shipping Method Fed Ex US Postal Lab Other: • UPS Client Courier Thermometer ID: l#101 Shipping container/cooler uncompromised? • Yes No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No • Not Present Chain of Custody(COC)present? • Yes No COC agrees with sample label(s)? • Yes No COC properly completed • Yes No Samples in proper containers? • Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test(s)? • Yes No All samples received within holding time? • Yes No Cooler temperature in compliance? • Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water-Sample containers properly preserved Yes No • N/A Water-VOA vials free of headspace " Yes No • N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035—compliance criteria met Yes No • N/A High concentration container(48 hr) Low concentration EnCore samplers(48 hr) High concentration pre-weighed (methanol-14 d) Low conc pre-weighed vials(Sod Bis-14 d) Special precautions or instructions included? Yes • No Comments: Signature: o Philli s Date&Time: 03 19 2021 13:46:42 Page 7 of 8 I I I 1 E E o 0 r ' F--, 3 0.. 0 ~ i, I:c3-1 h f y O O O vV O . p ON 2 c+ VI V N N r n P m 3 sa v v =p n a$ v V CU u re O o po ppp o 2 31 in � V u S 2 2 2 S S u D4 n C u Z. Y u ME « ^ 33 � �� Lf Soo. In Qmu0 W+. US _ ¢ c ce Z Q L r 1 =tn 417.7 a _ U. 11' V u D ti E y c Em Z ? am Id u ..... Ri y w m Y u' m L. o at 0 o E El: E E a Z 7 s M r '= r H cSI r d': U O . a �. \ C s « ❑❑ a M d R ^ N T u o� e c _ '^ _ M Va N a 9— 0') /d cc tz cc `V 2 E. c�.l o n cyra+r-.�op►t/V _ o to N L 5� ono m I l a aksodwo)�)ao geJ(9) t.l Z a I a3.Ni v r Z )Aap of aajatl)xlaleW J y - 'S r. h E `^Cl E .E siauieluoo jo iagwnN y h c a c m n N U } is 2 m v lat8 15 0 C io a. 4 u G 2 mN roQ � ..0 IC � `o u+ ^, r2 cp a o 'c 0 It p d N ca -� a u o Q `M' TE ^ "0 a a L vi 10 a ,Ng =r o. p ' u j� p 71 a EL. C -.4 .:4 3 IA 3.. irt: ,- 1:tt I 0 N Iri ih 0 Page 8 of 8 • '3'i Wap t lit 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanaiytical.com 4/20/2021 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC,29732 Ref: Analytical Testing Lab Report Number:21-099-0173 Client Project Description: Sludge Testing Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s)on 4/9/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.Where the laboratory was not responsible for the sampling stage(refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017)and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters,where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters(chlorine,pH, dissolved oxygen,sulfite...)are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated.This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, � d �'4,rJLL` d 1. AVAW— Randy Thomas Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option,repeating the analysis in question at laboratory's expense,or the refund of the charges paid for performance of said analysis. Page 1 of 9 tf o Waypoint. "- ; • r 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Certification Summary Laboratory ID:WP MTN:Waypoint Analytical,LLC., Memphis,TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2021 Florida State Program-NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program-NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2021 Louisiana State Program-NELAP LA037 12/31/2021 Louisiana State Program-NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program-NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program-NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program-NELAP 460181 09/14/2021 Page 1 of 1 00001/21-099-0173 Page 2 of 9 Waypoint, 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-099-0173 Client Project Description: Sludge Testing Lab No Client Sample ID Matrix Date Collected Date Received 90362 VD Solids 04/06/2021 13:36 04/09/2021 Page 3 of 9 D 2790 Whitten Road,Memphis,TN 38133 VV Vt�y��'�t Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Client: Branch Residuals and Soils LLC CASE NARRATIVE Project: Sludge Testing Lab Report Number:21-099-0173 Date:4/20/2021 Metals Analysis Method 6010D Analyte:Aluminum QC Batch No: L547526 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte:Arsenic QC Batch No:L547240 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Calcium QC Batch No: L547526 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Copper QC Batch No: L547240 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Iron QC Batch No: L547526 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L547240 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Magnesium QC Batch No: L547240 The matrix spike,matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Manganese QC Batch No: L547526 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 9 0 4 eV faYPOInt 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Analyte: Molybdenum QC Batch No: L547240 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Nickel QC Batch No: L547240 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Lead QC Batch No: L547240 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte:Zinc QC Batch No: L547240 The matrix spike,matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Page 5 of 9 C ,t) \aYpOint `_- 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr.Bob Branch Report Date: 04/20/2021 1735 Heckle Blvd Information : Received:04/09/2021 Suite 103-291 Rock Hill, SC 29732 Report Number:21-099-0173 REPORT OF ANALYSIS Lab No: 90362 Matrix: Solids Sample ID:VD Sampled:4/6/2021 13:36 Test Results Units MOL DF Date!Time By Analytical Analyzed Method Neutralizing Value(%CCE) 8.3 % 0.1 1 04/16/21 15:02 DXT AOAC 955.01 Moisture 59.8 % 0.010 1 04/13/21 16:13 FMM 2540G-2011 Ammonia Nitrogen 604 mg/Kg-dry 249 1 04/16/21 16:00 JP) 4500NH3C-2011 Nitrate(NO3-N) <2.49 mg/Kg-dry 2.49 1 04/12/21 21:59 JCA 9056A Nitrite(NO2-N) <2.49 mg/Kg-dry 2.49 1 04/12/21 21:59 JCA 9056A Nitrate+Nitrite-N <2.49 mg/Kg-dry 2.49 1 04/12/21 21:59 9056A Organic N 11340 mg/Kg-dry 828.4 1 04/16/21 16:00 CALCULATION pH 7.6 s.u. 1 04/16/21 15:18 CxC 9045D Total Solids 40.2 % 0.010 1 04/13/21 16:13 FMM 2540G-2011 Total Volatile Solids 44.6 % 0.010 1 04/13/21 16:13 FMM 2540G-2011 Total Kjeldahl Nitrogen 11900 mg/Kg-dry 828 1 04/19/21 17:38 CLP 4500NORGD-2011 Phosphorus 103 mg/Kg-dry 12.4 1 04/14/21 20:54 DADS 6010D Aluminum 1680 mg/Kg-dry 12.4 1 04/14/21 20:54 JADS 6010D Arsenic <1.24 mg/Kg-dry 1.24 1 04/14/21 20:54 JADS 6010D Cadmium <0.249 mg/Kg-dry 0.249 1 04/14/21 20:54 DADS 6010D Calcium 43000 mg/Kg-dry 622 5 04/15/21 17:11 JADS 6010D Copper 19.3 mg/Kg-dry 1.24 1 04/14/21 20:54 JADS 6010D Iron 1270 mg/Kg-dry 24.9 1 04/14/21 20:54 DADS 6010D Lead 2.38 mg/Kg-dry 0.746 1 04/14/21 20:54 JADS 6010D Magnesium 1930 mg/Kg-dry 12.4 1 04/14/21 20:54 JADS 6010D Manganese 37.3 mg/Kg-dry 1.24 1 04/14/21 20:54 JADS 6010D Mercury <0.0368 mg/Kg-dry 0.0368 1 04/13/21 12:45 DDB 7471A Molybdenum 2.96 mg/Kg-dry 0.621 1 04/14/21 20:54 JADS 6010D Qualifiers/ DF Dilution Factor L Umit Exceeded Definitions MQL Method Quantitation Umit Page 6 of 9 • 0'°, VVaypount _ 2ep1 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr.Bob Branch Report Date: 04/20/2021 1735 Heckle Blvd Information: Received:04/09/2021 Suite 103-291 Rock Hill, SC 29732 Report Number:21-099-0173 REPORTOFANALYSIS Lab No: 90362 Matrix: Solids Sample ID:VD Sampled: 4/6/2021 13:36 Test Results Units MOL DF Date/Time By Analytical Analyzed Method Nickel 1.13 mg/Kg-dry 0.621 1 04/14/21 20:54 DADS 6010D Potassium 47.8 mg/Kg-dry 24.9 1 04/14/21 20:54 DADS 6010D Selenium <1.24 mg/Kg-dry 1.24 1 04/14/21 20:54 JADS 6010D Sodium 858 mg/Kg-dry 62.2 1 04/14/21 20:54 JADS 6010D Zinc 86.3 mg/Kg-dry 3.11 1 04/14/21 20:54 DADS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions Page 7 of 9 Waypo'nt 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:22972 Customer Name: Branch Residuals and Soils LLC Report Number: 21-099.0173 Shipping Method Fed Ex US Postal Lab Other: • UPS Client Courier Thermometer ID: fri01 Shipping container/cooler uncompromised? • Yes No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? Yes No • Not Present Custody seals intact on sample bottles? Yes No • Not Present Chain of Custody(COC)present? • Yes No COC agrees with sample label(s)? • Yes No COC properly completed • Yes No Samples in proper containers? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test(s)? • Yes No All samples received within holding time? • Yes No Cooler temperature in compliance? Yes No Cooler/Samples arrived at the laboratory on ice. 5 Yes No Samples were considered acceptable as cooling process had begun. Water-Sample containers properly preserved Yes No N/A Water-VOA vials free of headspace Yes No f• N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035—compliance criteria met Yes No • N/A High concentration container(48 hr) Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol-14 d) Low conc pre-weighed vials(Sod Bis-14 d) Special precautions or instructions included? Yes • No Comments: Signature: Maka la Weaver Date&Time: 04.'09/2021 16:12:35 Page 8 of 9 , \!) G y u u I E E F- 1= G .J 3 1 N a '9 dqqd, o trs V vl e c ,,, e 0Y Q+�' c- c P. aagis �S.`U E a� V/ O an ��� � 3 � prim, a$_ - L C S N O 9,G d T J -_ s uuxzzxxzu S Y 3 u ..r A 3 3 , 2 co 23 o a N Qmuo ,.�,. l9x _ W W O U Lt a II. x sit 71 a i v a tri DJ V � =LmI $1ij NM a _ I v o v Y V 4 i 4. o ` o L x E E N E E a L n' r m C P. ~ cc � a � o uZ 'as !NoLN1; ,41 a o 0 0 '6 H 'qd PO'St/ 0 ..2.- a I sr 2, ` 3D3'spies Ie)o) • E: .. U C CV - - C n W ej'Iv'eN'64J'eO 03rngar O^1 - -6 t, v W 4f (�\ W W O 7 O C 1 , z -C 1.1 k d 4l.uc UA 41., � Q Q c M N u m U a` 2 , 2 2 u.7-1 C _ 1 t7 g o ea U 5 vnt V co _ �� g ..,. a it m Q I ' I a aiisodwo(7)JO gei(9) V Z `1 a aa- (Aap oliajaa)rlJleyy N -0 ..CM I Ns a O Fa I siauleluo)in iagwnN N Fa N € c I 2 cc et oU a N ov t• C o z S �'! ' < • m .. A V E ?m 0 2 '^ z n ,e E a „ 3 G tiY ,^ F- E e.0 a, L u M i „ 0 t O o O e y c 13 u m a`V d CO'! D 03 w al G j E r a 0 "i . - a O C=' 0 o A E < a v a a $ Z E " • / _, I $ eaG 2 L: ' 0 2 Q 1 4 �+ a e a 47, Y ! 01/ u es. - v a Page 9 of 9 Arit Waypoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 6/7/2021 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC,29732 Ref: Analytical Testing Lab Report Number:21-145-0029 Client Project Description: Sludge Testing Von Dizehie Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s)on 5/25/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.Where the laboratory was not responsible for the sampling stage(refer to the chain of custody)results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations,instrumentation maintenance and calibration for all parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017)and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters,where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters(chlorine, pH,dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option,repeating the analysis in question at laboratory's expense,or the refund of the charges paid for performance of said analysis. #o Page 1 of 9 •',Ill % Iaypo'nt 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated.This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Randy Thomas Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option,repeating the analysis in question at laboratory's expense,or the refund of the charges paid for performance of said analysis. Page 2 of 9 Waypoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Certification Summary Laboratory ID:WP MTN:Waypoint Analytical,LLC., Memphis,TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2021 Florida State Program-NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program-NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2021 Louisiana State Program-NELAP LA037 12/31/2021 Louisiana State Program-NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program-NELAP 68-03195 05/31/2022 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program-NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2021 Virginia State Program-NELAP 460181 09/14/2021 Page 1 of 1 00001/21-145-0029 Page 3 of 9 i�f Waypoint. 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-145-0029 Client Project Description: Sludge Testing Von Dizehle Lab No Client Sample ID Matrix Date Collected Date Received 88943 VD1 Solids 05/20/2021 14:30 05/25/2021 Page 4 of 9 Way point 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Client: Branch Residuals and Soils LLC CASE NARRATIVE Project:Sludge Testing Von Dizehle Lab Report Number:21-145-0029 Date:6/7/2021 Metals Analysis Method 6010D Sample 88943(VD1) Analyte:Aluminum QC Batch No: L555691/L555326 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L555691/L555326 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 9 .____ v \P%yp oint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Von Dizehle Mr.Bob Branch Report Date: 06/07/2021 1735 Heckle Blvd Information: Received:05/25/2021 Suite 103-291 Rock Hill, SC 29732 Report Number:21-145-0029 REPORT OF ANALYSIS Lab No: 88943 Matrix: Solids Sample ID:VD1 Sampled: 5/20/2021 14:30 Test Results Units MQL DF Date/Time By Analytical Analyzed Method Neutralizing Value(%CCE) 52.6 % 0.1 1 05/27/21 00:00 DXT AOAC 955.01 Moisture 60.9 % 0.010 1 05/25/21 16:25 FMM 2540G-2011 Ammonia Nitrogen 312 mg/Kg-dry 256 1 06/02/21 15:00 JPJ 4500NH3C-2011 Nitrate(NO3-N) <2.56 mg/Kg-dry 2.56 1 06/01/21 16:36 JCA 9056A Nitrite(NO2-N) <2.56 mg/Kg-dry 2.56 1 06/01/21 16:36 JCA 9056A Nitrate+Nitrite-N <2.56 mg/Kg-dry 2.56 1 06/01/21 16:36 9056A Organic N 4445 mg/Kg-dry 639.4 1 06/02/21 15:00 CALCULATION pH 7.4 s.u. 1 06/01/21 15:30 ADM 9045D Total Solids 39.1 °yo 0.010 1 05/25/21 16:25 FMM 2540G2011 Total Volatile Solids 45.8 % 0.010 1 05/25/21 16:25 FMM 2540G-2011 Total Kjeldahl Nitrogen 4760 mg/Kg-dry 639 1 06/04/21 10:00 JPJ iM-4500-NH3C-TKO Phosphorus 175 mg/Kg-dry 12.8 1 05/28/21 02:25 TJS 6010D Aluminum 1770 mg/Kg-dry 12.8 1 05/28/21 02:25 TJS 6010D Arsenic <1.28 mg/Kg-dry 1.28 1 05/28/21 02:25 TJS 6010D Cadmium <0.256 mg/Kg-dry 0.256 1 05/28/21 02:25 TJS 6010D Calcium 186000 mg/Kg-dry 1280 10 05/28/21 23:42 TJS 6010D Copper 31.5 mg/Kg-dry 1.28 1 05/28/21 02:25 TJS 6010D Iron 1610 mg/Kg-dry 25.6 1 05/28/21 02:25 TJS 6010D Lead 1.93 mg/Kg-dry 0.767 1 05/28/21 02:25 TJS 6010D Magnesium 1870 mg/Kg-dry 12.8 1 05/28/21 02:25 TJS 6010D Manganese 45.0 mg/Kg-dry 1.28 1 05/28/21 02:25 TJS 6010D Mercury <0.0361 mg/Kg-dry 0.0361 1 06/01/21 12:00 DDB 7471A Molybdenum 4.60 mg/Kg-dry 0.639 1 05/28/21 02:25 TJS 6010D Qualifiers/ DF Dilution Factor L Umit Exceeded Definitions MQL Method Quantitation Umit Page 6 of 9 _:::: • ,,` 1 2790 Whitten Road,Memphis,TN 38133 VVayp 01�� Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Von Dizehle Mr.Bob Branch Report Date: 06/07/2021 1735 Heckle Blvd Information: Received:05/25/2021 Suite 103-291 Rock Hill, SC 29732 Report Number:21-145-0029 REPORT OF ANALYSIS Lab No: 88943 Matrix: Solids Sample ID:VD1 Sampled: 5/20/2021 14:30 Test Results Units MIL DF Date/Time By Analytical Analyzed Method Nickel 1.40 mg/Kg-dry 0.639 1 05/28/21 02:25 T)S 6010D Potassium 62.9 mg/Kg-dry 25.6 1 05/28/21 02:25 TJS 6010D Selenium <1.28 mg/Kg-dry 1.28 1 05/28/21 02:25 TJS 6010D Sodium 481 mg/Kg-dry 63.9 1 05/28/21 02:25 TJS 6010D Zinc 116 mg/Kg-dry 3.20 1 05/28/21 02:25 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions Page 7 of 9 Waypoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:22972 Customer Name: Branch Residuals and Soils LLC Report Number: 21-145-0029 Shipping Method Fed Ex US Postal Lab Other: • UPS Client Courier Thermometer ID: (T102 Shipping container/cooler uncompromised? • Yes No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? Yes No • Not Present Custody seals intact on sample bottles? Yes No • Not Present Chain of Custody(COC) present? Yes No COC agrees with sample label(s)? • Yes No COC properly completed • Yes No Samples in proper containers? • Yes No Sample containers intact? • Yes No Sufficient sample volume for indicated test(s)? • Yes No All samples received within holding time? Yes No Cooler temperature in compliance? Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water-Sample containers properly preserved Yes No • N/A Water-VOA vials free of headspace Yes No • N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035—compliance criteria met Yes No N/A High concentration container(48 hr) Low concentration EnCore samplers(48 hr) High concentration pre-weighed(methanol-14 d) Low conc pre-weighed vials (Sod Bis-14 d) Special precautions or instructions included? Yes • No Comments: Signature: Maka la Weaver Date&Time: 5 25 2021 11:44:45 Page 8 of 9 I v u E E Y E = o 0 3 i. .-_ F.N p '0 O ���� o 2 n re_ o a o av� 1 ul N M N i 1 N 9 >. l7 `" 2 n a ry v 2 Y v j C M o o r x x , c`at E c, n 2 a v v p t =M n g v 3 8 a^ 3 c rL O o O N o ORIl U rn O 7 QN+') �.� .a. r.V x Z 2 I x x t� �1r1��f'f d y y E. _ - rr NQ T x Y o O t �_ 'ice Q " s j nL ---- Hit _ 1 I I . C E E a =s ' u d 7 ` ' z N c a 10 ____ a' = - d ` - m W. o u' v o` if 4. : E E n £ E .c v O c `Immili a`: r:� c 1 7. i a v C O I I o 1�"t u j — ._ I _ .. . o NI x 1 R, c a E' 1i ' _° Z W �y a �//v 1 9" _ d it + W W la fU Xry 3 f / cc cc c a a a m I , - alisodwop)io geilD) C..) 2 p $ a N^ 9 (Aag of Nay)■uleW -J v `�+-1, . 1c S. T. _ al'"-*- siau1e1ua)to iigwnN n a It ¢ ` CJ n u u I y a c ff at t o d o u S " c ct a" `u o u o E \ cv) — o d au C ! C 0 C y I . x. n a V p • m u n 9 Lil in A a I V C:a' T 1:- r. C N ta E O< �• q. a- A. i 4: C! •YrN u r� a_ cc. „, st 1 10 : w z p � 0 Page 9 of 9 Waypoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 7/7/2021 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC,29732 Ref: Analytical Testing Lab Report Number: 21-175-0082 Client Project Description: Sludge Testing Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s)on 6/24/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.Where the laboratory was not responsible for the sampling stage(refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017)and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'-'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters,where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters(chlorine, pH,dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of sampling. Usually, but not always,any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated.This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, A4/4.11 ). )4444- Randy Thomas Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option,repeating the analysis in question at laboratory's expense,or the refund of the charges paid for performance of said analysis. 4acistee Page 1 of 7 fIay •-t of nt. Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.corn Certification Summary Laboratory ID:WP MTN:Waypoint Analytical,LLC., Memphis,TN State Pro ram Lab ID _ _ _ Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2022 Florida State Program-NELAP E871157 06/30/2022 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program-NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2022 Kentucky State Program KY90047 12/31/2021 Louisiana State Program-NELAP LA037 12/31/2021 Louisiana State Program-NELAP 04015 06/30/2022 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program-NELAP 68-03195 05/31/2022 South Carolina State Program 84002 06/30/2022 South Carolina State Program 84002 06/30/2021 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program-NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2022 Virginia State Program-NELAP 460181 09/14/2021 Page 1 of 1 00001/21-175-0082 Page 2 of 7 %a o m t 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-175-0082 Client Project Description: Sludge Testing Lab No Client Sample ID Matrix Date Collected Date Received 86373 VD Solids 06/23/2021 14:00 06/24/2021 Page 3 of 7 VVaypo'�� Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanaiytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr.Bob Branch Report Date: 07/07/2021 1735 Heckle Blvd Information: Received:06/24/2021 Suite 103-291 Rock Hill, SC 29732 Report Number:21-175-0082 REPORT OF ANALYSIS Lab No: 86373 Matrix: Solids Sample ID:VD Sampled: 6/23/2021 14:00 Test Results Units MQL DF Date/Time By Analytical Analyzed Method Neutralizing Value(%CCE) 54.4 % 0.1 1 06/28/21 14:00 DXT AOAC 955.01 Moisture 62.8 % 0.010 1 06/24/21 16:28 FMM 2540G-2011 Ammonia Nitrogen 973 mg/Kg-dry 269 1 06/30/21 15:00 JP] 4500NH3C-2011 Nitrate(NO3-N) <2.69 mg/Kg-dry 2.69 1 06/29/21 15:11 )CA 9056A Nitrite(NO2-N) <2.69 mg/Kg-dry 2.69 1 06/29/21 15:11 JCA 9056A Nitrate+Nitrite-N <2.69 mg/Kg-dry 2.69 1 06/29/21 15:11 9056A Organic N <384.4 mg/Kg-dry 384.4 1 06/30/21 15:00 CALCULATION pH 7.1 s.u. 1 06/30/21 16:20 DRS 9045D Total Solids 37.2 % 0.010 1 06/24/21 16:28 FMM 2540G-2011 Total Volatile Solids 47.9 % 0.010 1 06/24/21 16:28 FMM 2540G-2011 Total Kjeldahl Nitrogen 1160 mg/Kg-dry 384 1 07/01/21 15:11 CLP 4500NORGD-2011 Phosphorus 115 mg/Kg-dry 13.4 1 06/30/21 20:21 TJS 6010D Aluminum 2190 mg/Kg-dry 13.4 1 07/02/21 21:42 T]S 6010D Arsenic <1.34 mg/Kg-dry 1.34 1 06/30/21 20:21 T]S 6010D Cadmium <0.269 mg/Kg-dry 0.269 1 06/30/21 20:21 TJS 6010D Calcium 184000 mg/Kg-dry 1340 10 07/02/21 21:47 TJS 6010D Copper 23.9 mg/Kg-dry 1.34 1 06/30/21 20:21 TJS 6010D Iron 1430 mg/Kg-dry 26.9 1 06/30/21 20:21 TJS 6010D Lead 1.25 mg/Kg-dry 0.806 1 06/30/21 20:21 TJS 60100 Magnesium 2060 mg/Kg-dry 13.4 1 06/30/21 20:21 TJS 6010D Manganese 42.2 mg/Kg-dry 1.34 1 06/30/21 20:21 TJS 6010D Mercury <0.0425 mg/Kg-dry 0.0425 1 06/30/21 12:45 DDB 7471A Molybdenum 4.41 mg/Kg-dry 0.672 1 06/30/21 20:21 -OS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 Waypoint '\• 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr.Bob Branch Report Date: 07/07/2021 1735 Heckle Blvd Information: Received:06/24/2021 Suite 103-291 Rock Hill, SC 29732 Report Number:21-175-0082 REPORT OF ANALYSIS Lab No: 86373 Matrix: Solids Sample ID:VD Sampled: 6/23/2021 14:00 Test Results Units MQL DF Date/Time By Analytical Analyzed Method Nickel 0.876 mg/Kg-dry 0.672 1 06/30/21 20:21 TJS 6010D Potassium 66.7 mg/Kg-dry 26.9 1 06/30/21 20:21 TJS 6010D Selenium <1.34 mg/Kg-dry 1.34 1 06/30/21 20:21 TJS 6010D Sodium 565 mg/Kg-dry 67.2 1 06/30/21 20:21 TJS 6010D Zinc 160 mg/Kg-dry 3.36 1 06/30/21 20:21 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions Page 5 of 7 W Npoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:22972 Customer Name: Branch Residuals and Soils LLC Report Number: 21.175.0082 Shipping Method Fed Ex US Postal Lab Other: • UPS Client Courier Thermometer ID: It99 Shipping container/cooler uncompromised? • Yes No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? Yes No • Not Present Custody seals intact on sample bottles? Yes No • Not Present Chain of Custody(COC) present? • Yes No COC agrees with sample label(s)? • Yes No COC properly completed • Yes No Samples in proper containers? • Yes No Sample containers intact? • Yes No Sufficient sample volume for indicated test(s)? • Yes No All samples received within holding time? • Yes No Cooler temperature in compliance? • Yes No Cooler/Samples arrived at the laboratory on ice. • Yes No Samples were considered acceptable as cooling process had begun. Water-Sample containers properly preserved Yes No • N/A Water-VOA vials free of headspace Yes No • N/A Trip Blanks received with VOAs Yes No • N/A Soil VOA method 5035—compliance criteria met Yes No • N/A High concentration container(48 hr) Low concentration EnCore samplers(48 hr) High concentration pre-weighed(methanol-14 d) , Low conc pre-weighed vials (Sod Bis-14 d) Special precautions or instructions included? Yes • No Comments: Signature: Maka la Weaver Date&Time: 6 24 2021 11:11:47 Page 6 of 7 _ o Y Y+— 2111110 i E E •E {--•:. O 0 i- i- i= > Z it O —\ Q n O a o 2 �J J." M R. 'I ', .i w So aZv rOV d E�C = � mQ �s = ab O , in . a v �. vaaQv `� t a, .,. V v x 2 2 x x x v EAt i D o \ i i`'- ea, II ra C O a. N 4 C u a '.. .� 0 2 - �11pp W 7 Cc W CC .0 MI Q Q Q J i t.7 0 2 tr - V IQ o „ - asaw a. a o�1 a o ~ U Y al V E cc cc r : 1r.at g a; E E E E Y C K r '2I�"� i0 fC o 74DO t2 �L u � o a Q v Y 1 71 i J Y —� 5 _. w tJ 4 o g ` i. �?, `n N tilt t+'A! f�i :� zr n j /❑ -)p� (f a 2 2 5 .— '' -a }�'lr r• I' Y t Lt t�14\ 7, t? S. CO Y n�' = = m' m a° at!Sadwol7�io geil9l V z t t� a CI ' 1 m d V ( i oliafaa)■uteyy y! Q > V,Lel n c •c s,auleluop fo iagwnp, ° �� c� c I V 2. C - u° Z 1 a `m . ''� L v V C. i r a o I:4G ,. Y , 2 a Y.Y c �, c c Y 7 ,'� -, co o Y = °d u 1 NI a 1i) e Tv u o. e j n. O I o 1 1 0 -Y r '�2 a U v l Y Y u 2 E t )1111 'i — N• u ;� o n c O 2 73` = _ _C7 z a (~ , c � 4. e �c�q r Q ..��1 Y �,..y co f PP Page 7 of 7 ��sO� • rY V (aypO'lit 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 7/27/2021 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Lab Report Number: 21-197-0162 Client Project Description: Sludge Testing Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s) on 7/16/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'--'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters,where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 4746 )• )14042- Randy Thomas Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 7 • VV Wa1pO'■ ■t 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Certification Summary Laboratory ID:WP MTN:Waypoint Analytical, LLC., Memphis,TN State _ Program _ Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2022 Florida State Program-NELAP E871157 06/30/2022 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program-NELAP 200078 10/10/2021 Kentucky State Program 80215 06/30/2022 Kentucky State Program KY90047 12/31/2021 Louisiana State Program-NELAP LA037 12/31/2021 Louisiana State Program-NELAP 04015 06/30/2022 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program-NELAP 68-03195 05/31/2022 South Carolina State Program 84002 06/30/2022 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program-NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2022 Virginia State Program-NELAP 460181 09/14/2021 Page 1 of 1 00001/21-197-0162 Page 2 of 7 w Waypoint. 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-197-0162 Client Project Description: Sludge Testing Lab No Client Sample ID Matrix Date Collected Date Received 90282 VD Solids 07/14/2021 14:30 07/16/2021 Page 3 of 7 YY� Waypoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr. Bob Branch Report Date: 07/27/2021 1735 Heckle Blvd Information : Received :07/16/2021 Suite 103-291 Rock Hill , SC 29732 Report Number:21-197-0162 REPORT OF ANALYSIS Lab No: 90282 Matrix: Solids Sample ID:VD Sampled: 7/14/2021 14:30 Test Results Units MQL DF Date/Time By Analytical Analyzed Method Neutralizing Value(%CCE) 42.7 % 0.1 1 07/26/21 13:00 DXT AOAC 955.01 Moisture 59.8 % 0.010 1 07/21/21 15:50 FMM 2540G-2011 Ammonia Nitrogen <249 mg/Kg-dry 249 1 07/23/21 15:00 JPJ 4500NH3C-2011 Nitrate(NO3-N) <2.49 mg/Kg-dry 2.49 1 07/20/21 22:29 JCA 9056A Nitrite(NO2-N) <2.49 mg/Kg-dry 2.49 1 07/20/21 22:29 JCA 9056A Nitrate+Nitrite-N <2.49 mg/Kg-dry 2.49 1 07/20/21 22:29 9056A Organic N 1244 mg/Kg-dry 248.8 1 07/22/21 16:10 CALCULATION pH 7.7 s.u. 1 07/22/21 16:10 DRS 9045D Total Solids 40.2 % 0.010 1 07/21/21 15:50 FMM 2540G-2011 Total Volatile Solids 48.3 % 0.010 1 07/21/21 15:50 FMM 2540G-2011 Total Kjeldahl Nitrogen 1240 mg/Kg-dry 135 1 07/22/21 16:10 CLP 4500NORGD-2011 Phosphorus 111 mg/Kg-dry 12.4 1 07/20/21 20:56 TJS 6010D Aluminum 2220 mg/Kg-dry 12.4 1 07/20/21 20:56 TJS 6010D Arsenic <1.24 mg/Kg-dry 1.24 1 07/20/21 20:56 TJS 6010D Cadmium <0.249 mg/Kg-dry 0.249 1 07/20/21 20:56 TJS 6010D Calcium 166000 mg/Kg-dry 1240 10 07/22/21 00:03 JTR 6010D Copper 25.1 mg/Kg-dry 1.24 1 07/20/21 20:56 TJS 6010D Iron 908 mg/Kg-dry 24.9 1 07/20/21 20:56 TJS 6010D Lead 1.31 mg/Kg-dry 0.746 1 07/20/21 20:56 TJS 6010D Magnesium 1740 mg/Kg-dry 12.4 1 07/20/21 20:56 TJS 6010D Manganese 34.3 mg/Kg-dry 1.24 1 07/20/21 20:56 TJS 6010D Mercury 0.0438 mg/Kg-dry 0.0363 1 07/21/21 10:47 DDB 7471A Molybdenum 3.43 mg/Kg-dry 0.621 1 07/20/21 20:56 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 a VIayp oi nt. 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr. Bob Branch Report Date: 07/27/2021 1735 Heckle Blvd Information: Received :07/16/2021 Suite 103-291 Rock Hill, SC 29732 Report Number:21-197-0162 REPORTOFANALYSIS Lab No: 90282 Matrix: Solids Sample ID:VD Sampled: 7/14/2021 14:30 Test Results Units MOL DF Date/Time By Analytical Analyzed Method Nickel 0.932 mg/Kg-dry 0.621 1 07/20/21 20:56 TJS 6010D Potassium 66.7 mg/Kg-dry 24.9 1 07/20/21 20:56 TJS 6010D Selenium <1.24 mg/Kg-dry 1.24 1 07/20/21 20:56 TJS 6010D Sodium 677 mg/Kg-dry 62.2 1 07/20/21 20:56 TJS 6010D Zinc 52.5 mg/Kg-dry 3.11 1 07/20/21 20:56 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions Page 5 of 7 Waypo 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:22972 Customer Name: Branch Residuals and Soils LLC Report Number: 21-197-0162 Shipping Method Fed Ex 0 US Postal 0 Lab 0 Other : .... .. . ... . . . UPS 0 Client 0 Courier Thermometer ID: JT102 Shipping container/cooler uncompromised? *Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No OQ Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody(COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed *Yes 0 No Samples in proper containers? *Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? *Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? J Yes 0 No Cooler/Samples arrived at the laboratory on ice. *Yes 0 No Samples were considered acceptable as cooling process had begun. Water-Sample containers properly preserved 0 Yes 0 No OQ N/A Water-VOA vials free of headspace 0 Yes 0 No * N/A Trip Blanks received with VOAs 0 Yes 0 No * N/A Soil VOA method 5035—compliance criteria met 0 Yes 0 No c N/A High concentration container(48 hr) Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis-14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: Makayla Weaver Date&Time: 07/16/2021 15:38:16 Page 6 of 7 ,- M o NA i E E E" cs �b n 0 0 } f- -4_ il pQ'y�� v_ 0 N NO,fl p V VIL a, 4f - RNsn _� o p 0 2 V1 N N ,: . 1 N a N Y - 2 N N 2 L MOS . `guaySxvnw E liN3 a v v 0 d =,a, ag v u° s 0 8 S '" I o c a o U C N O N 2 V to p J Y M vox 22xx xu so�Al C 7 U. elimilm Nmararm f Cl. 34 • H oa in amuou t7s _ _ I 1 i o�c -a.� v O _ ID z gilmmn t y ..,. i 71 J]a a v v 0 t N y ? ,n a id Ci E u u re cc E m Z - O. 2 co a - a< a,us m o a,2 E x E. - E E O W j L_ on 2 1- • F- 11 t u. v O .0 a n.a N n v at L f Q Z I "; �� �i itsl� ! 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Waypo� � 2790 Whitten Road,Memphis,TN 38133 i�t Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 8/25/2021 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Lab Report Number: 21-229-0067 Client Project Description: Sludge Testing Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s)on 8/17/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters,where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated.This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 44,0 9. Akrlel,— Randy Thomas Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. ice- 4 Page 1 of 7 a YV Waypoint, 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalyticaicom Certification Summary Laboratory ID:WP MTN:Waypoint Analytical, LLC., Memphis,TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2022 Arkansas State Program 88-0650 02/07/2022 California State Program 2904 06/30/2022 Florida State Program- NELAP E871157 06/30/2022 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program-NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2022 Kentucky State Program KY90047 12/31/2021 Louisiana State Program-NELAP LA037 12/31/2021 Louisiana State Program-NELAP 04015 06/30/2022 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2021 Oklahoma State Program 9311 08/31/2021 Pennsylvania State Program-NELAP 68-03195 05/31/2022 South Carolina State Program 84002 06/30/2022 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021 Texas State Program-NELAP T104704180 09/30/2021 Virginia State Program 00106 06/30/2022 Virginia State Program-NELAP 460181 09/14/2021 Page 1 of 1 00001/21-229-0067 Page 2 of 7 • Y rQ I (aypoi n t - 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-229-0067 Client Project Description: Sludge Testing Lab No Client Sample ID Matrix Date Collected Date Received 92141 VD Solids 08/16/2021 13:45 08/17/2021 Page 3 of 7 o Waypoi ft 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr.Bob Branch Report Date: 08/25/2021 1735 Heckle Blvd Information : Received : 08/17/2021 Suite 103-291 Rock Hill, SC 29732 Report Number:21-229-0067 REPORT OF ANALYSIS Lab No: 92141 Matrix: Solids Sample ID:VD Sampled: 8/16/2021 13:45 Test Results Units MOL DF Date/Time By Analytical Analyzed Method Neutralizing Value(%CCE) 47.7 % 0.1 1 08/23/21 11:15 DXT AOAC 955.01 Moisture 61.7 % 0.010 1 08/20/21 16:27 FMM 2540G-2011 Ammonia Nitrogen 491 mg/Kg-dry 261 1 08/24/21 11:00 JPJ 4500NH3C-2011 Nitrate(NO3-N) <2.61 mg/Kg-dry 2.61 1 08/23/21 19:28 JCA 9056A Nitrite(NO2-N) <2.61 mg/Kg-dry 2.61 1 08/23/21 19:28 JCA 9056A Nitrate+Nitrite-N <2.61 mg/Kg-dry 2.61 1 08/23/21 19:28 9056A Organic N 412.5 mg/Kg-dry 261.1 1 08/24/21 11:00 CALCULATION pH 7.4 s.u. 1 08/23/21 15:35 DRS 9045D Total Solids 38.3 % 0.010 1 08/20/21 16:27 FMM 2540G-2011 Total Volatile Solids 46.7 % 0.010 1 08/20/21 16:27 FMM 2540G-2011 Total Kjeldahl Nitrogen 903 mg/Kg-dry 145 1 08/25/21 15:45 CLP 4500NORGD-2011 Phosphorus 131 mg/Kg-dry 13.1 1 08/23/21 21:23 JTR 6010D Aluminum 1540 mg/Kg-dry 13.1 1 08/23/21 21:23 JTR 6010D Arsenic <1.31 mg/Kg-dry 1.31 1 08/23/21 21:23 JTR 6010D Cadmium <0.261 mg/Kg-dry 0.261 1 08/23/21 21:23 JTR 6010D Calcium 176000 mg/Kg-dry 1310 10 08/24/21 12:29 TJS 6010D Copper 22.6 mg/Kg-dry 1.31 1 08/23/21 21:23 JTR 6010D Iron 1100 mg/Kg-dry 26.1 1 08/23/21 21:23 JTR 6010D Lead 6.37 mg/Kg-dry 0.783 1 08/23/21 21:23 JTR 6010D Magnesium 2370 mg/Kg-dry 13.1 1 08/23/21 21:23 JTR 6010D Manganese 39.2 mg/Kg-dry 1.31 1 08/23/21 21:23 JTR 6010D Mercury <0.0392 mg/Kg-dry 0.0392 1 08/20/21 11:48 TJS 7471A Molybdenum 2.74 mg/Kg-dry 0.652 1 08/23/21 21:23 JTR 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 7 w Waypoint. 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400°Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Sludge Testing Mr.Bob Branch Report Date: 08/25/2021 1735 Heckle Blvd Information: Received :08/17/2021 Suite 103-291 Rock Hill, SC 29732 Report Number:21-229-0067 REPORT OF ANALYSIS Lab No: 92141 Matrix: Solids Sample ID:VD Sampled: 8/16/2021 13:45 Test Results Units MOL DF Date/Time By Analytical Analyzed Method Nickel 1.04 mg/Kg-dry 0.652 1 08/23/21 21:23 JTR 6010D Potassium 52.2 mg/Kg-dry 26.1 1 08/23/21 21:23 JTR 6010D Selenium <1.31 mg/Kg-dry 1.31 1 08/23/21 21:23 JTR 6010D Sodium 789 mg/Kg-dry 65.3 1 08/23/21 21:23 JTR 6010D Zinc 70.2 mg/Kg-dry 3.26 1 08/23/21 21:23 JTR 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions Page 5 of 7 • vv Waypoint 2790 Whitten Road,Memphis,TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:22972 Customer Name: Branch Residuals and Soils LLC Report Number: 21-229-0067 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other : ® UPS 0 Client 0 Courier Thermometer ID: r102 Shipping container/cooler uncompromised? 0 Yes No Number of coolers/boxes received T1 Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody(COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes ❑No Samples in proper containers? 0 Yes 0 No Sample containers intact? Q Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes Q No Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No Samples were considered acceptable as cooling process had begun. Water-Sample containers properly preserved 0 Yes 0 No 0 N/A Water-VOA vials free of headspace 0 Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A i High concentration container(48 hr) r Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) r Low cone pre-weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: Emily M. Peterson Date&Time: 08/17/2021 12:30:08 Page 6 of 7 r 0 ch o, t 0.1 N �� f?c' r PIS C! N NO` 3.- ■ E E 1 o P. P. P. m m Oa0 a c 0 z ,1 0 0 - N N M INEd R Y.13 Q G O L1 `d- � xQxx "Vne E o, a v Uo o v A g o o = o o Q 'o -91 o $ « o 4' z u r. o 1111 N VUXZZSMSV u _ G u r ,_ s C 4f N Q tJ O W W U' S W W W �_�� di . AM 4 qd V CC . =L IIM 8 z z z m V3 I 1 w N 7 , > > • a .0 .o, , a a a is c `, u u u a II, a E cc cc ■ • "33 E E Z — — W 1 a • u a -- L a Y " 4 2 '° 3 E E v o w o a o. u OV. IA. W L It w ❑O o La. V O C O A ci ' NQ .3 -A, • - . a % C m Nd - 7 C' � S . I �o y r C o d N o 0 z Wei ,> N�hjjN 14�1 r} ' . z nil• v2 +l n = 4y a a a O" x ii „ g ..,�i t 6 z z O V n a` ` as�sodwo(3)Jo qe�(9) '° .4) a a TEI '+a z > w tea, (Aa„of ia4ay)xuley4 v \ _ E. S. v auieluo3)o Jag �wnN -. y .. tm u Tu CC L « ) ... c �' 3s n C• ] Y ., 3 E. L 'F p ,cf L• Vti O u p NI ISD t O G \)y ^� n -0 ° .-. �' w CJ Vo S.? O V E o• M a �. o c▪ r., c > `-' 3 `'� O. a 7 a a, e 0 3 m m a N 0 > I +� `o 1�• 11+' a aa y l ^ E g e, .E. A i . '. 2 =r' T n it a 3` 1 a -3 ^ a V IT Page 7 of 7 w Waypoint, 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 9/23/2021 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Report Number: 21-258-0002 Project Description:Von Drehle Cordova Project#2014-110 Dear Bob Branch: Waypoint Analytical Virginia, Inc. received sample(s) on 9/15/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated.This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 1)aµir'c MC &tear Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 -ii VV Waypoint. 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-258-0002 Client Project Description: Von Drehle Cordova Project#2014-110 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 77715 VD Solids 09/09/2021 14:00 09/15/2021 SM-2540G WP MTN 77715 VD Solids 09/09/2021 14:00 09/15/2021 SM-4500-NH3C WP MTN 77715 VD Solids 09/09/2021 14:00 09/15/2021 SM-4500-NH3C-TKN WP MTN 77715 VD Solids 09/09/2021 14:00 09/15/2021 4500NO3F-2011 WP MTN 77715 VD Solids 09/09/2021 14:00 09/15/2021 6010D WP MTN 77715 VD Solids 09/09/2021 14:00 09/15/2021 SW-7471B WP MTN 77715 VD Solids 09/09/2021 14:00 09/15/2021 9045D WP MTN 77715 VD Solids 09/09/2021 14:00 09/15/2021 AOAC 955.01 WP MTN WP MTN-Memphis,TN: Waypoint Analytical-TN,Memphis,TN Page 2 of 8 11i Waypo nt. �_.� 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von Drehle Cordova Bob Branch Report Date: 09/23/2021 1735 Heckle Blvd Information : Project#2014-110 Received :09/15/2021 Suite 103-291 Rock Hill , SC 29732 l q cuvic pjt G/oar REPORT OF Pauric Mc Groary Ph.D.,CPA Report Number:21-258-0002 Agronomist Lab No: 77715 Matrix: Solids Sample ID :VD Sampled: 9/9/2021 14:00 Test Results Units MOL DF Date/Time By Analytical Analyzed Method Total Solids 36.8 % 0.010 1 09/16/21 15:54 FMM SM-2540G Total Kjeldahl Nitrogen 5490 mg/Kg-dry 679 1 09/21/21 10:00 JPJ ;M-4500-NH3C-TKP Phosphorus 144 mg/Kg-dry 13.6 1 09/18/21 03:07 JTR 6010D Potassium 67.7 mg/Kg-dry 27.2 1 09/18/21 03:07 JTR 6010D Calcium 210000 mg/Kg-dry 13600 100 09/20/21 20:07 JTR 6010D Magnesium 2460 mg/Kg-dry 13.6 1 09/18/21 03:07 JTR 6010D Sodium 658 mg/Kg-dry 67.9 1 09/18/21 03:07 JTR 6010D Copper 39.1 mg/Kg-dry 1.36 1 09/18/21 03:07 JTR 6010D Zinc 115 mg/Kg-dry 3.40 1 09/18/21 03:07 JTR 6010D Nitrate+Nitrite-N 59.0 mg/Kg-dry 13.0 1 09/23/21 14:48 ZBD 4500NO3F-2011 Nickel 1.26 mg/Kg-dry 0.679 1 09/18/21 03:07 JTR 6010D Mercury <0.0421 mg/Kg-dry 0.0421 1 09/21/21 12:11 TJS SW-7471B Selenium <1.36 mg/Kg-dry 1.36 1 09/18/21 03:07 JTR 6010D pH 7.6 s.u. 1 09/21/21 15:07 DRS 9045D Calcium Carbonate Equivalent 16.0 % 0.1 1 09/22/21 09:15 DXT AOAC 955.01 Test Results Units MOL DF Date/Time By Analytical Analyzed Method Ammonia Nitrogen 302 mg/Kg-dry 272 1 09/22/21 12:00 JPJ SM-4500-NH3C Aluminum 2340 mg/Kg-dry 13.6 1 09/18/21 03:07 JTR 6010D Arsenic 3.72 mg/Kg-dry 1.36 1 09/18/21 03:07 JTR 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of B rs,--.... .a.01 Wa i point _) 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von Drehle Cordova Bob Branch Report Date: 09/23/2021 1735 Heckle Blvd Information : Project#2014-110 Received :09/15/2021 Suite 103-291 Rock Hill , SC 29732 Tam c plc &o.r. REPORT OF Pauric Mc Groary Ph.D.,CPA�/ Report Number:21-258-0002 Agronomist Lab No: 77715 Matrix: Solids Sample ID :VD Sampled: 9/9/2021 14:00 Test Results Units MQL DF Date/Time By Analytical Analyzed Method Cadmium <0.272 mg/Kg-dry 0.272 1 09/18/21 03:07 JTR 6010D Lead <0.815 mg/Kg-dry 0.815 1 09/18/21 03:07 JTR 6010D Molybdenum 3.89 mg/Kg-dry 0.679 1 09/18/21 03:07 JTR 6010D Analytical Method: SM-2540G Test Results Units MQL DF Date/Time By Analytical Analyzed Batch Moisture 63.2 % 0.010 1 09/16/21 15:54 FMM L574461 Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 4 of 8 w Waypoi nt. 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Client: Branch Residuals and Soils LLC CASE NARRATIVE Project:Von Drehle Cordova Lab Report Number: 21-258-0002 Date: 9/23/2021 Metals Analysis Method 6010D Sample 77720 Analyte: Calcium QC Batch No: L574862/L574543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Cadmium QC Batch No: L574862/L574543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Copper QC Batch No: L574862/L574543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L574862/L574543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Magnesium QC Batch No: L574862/L574543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Molybdenum QC Batch No: L574862/L574543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Sodium QC Batch No: L574862/L574543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Nickel QC Batch No: L574862/L574543 Page 5 of 8 WayprY�?i ft, 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Lead QC Batch No: L574862/L574543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Selenium QC Batch No: L574862/L574543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Zinc QC Batch No: L574862/L574543 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Solids Total Mercury Analysis-CVAA Method 7471A Sample 77719 Analyte: Mercury QC Batch No: L575182/L574935 The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control acceptance ranges. Matrix interference is suspected Page 6 of 8 vv Wayioint 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:46368 Customer Name: Branch Residuals and Soils LLC Report Number: 21-258-0002 Shipping Method 0 Fed Ex 0 US Postal 0 Lab Other : 0 UPS 0 Client 0 Courier Thermometer ID: I Shipping container/cooler uncompromised? *Yes " No Number of coolers/boxes received �1 Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody(COC) present? J Yes 0 No COC agrees with sample label(s)? J Yes 0 No COC properly completed *Yes 0 No Samples in proper containers? *Yes 0 No Sample containers intact? *Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No Samples were considered acceptable as cooling process had begun. Water-Sample containers properly preserved 0 Yes 0 No @ N/A Water-VOA vials free of headspace 0 Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes 0 No * N/A Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol-14 d) Low conc pre-weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: Brandi Watson Date&Time: 09/15/2021 12:39:16 Page 7 of 8 ^, o / V ,,,) r „` ,N v E. "� 3 1 ) egg _ Li o n Q I? Z� m 9 �v 2 i 3 .. mi W t. -<.• Cl 7- f+' is a - O eT as a o 9 r ^ < 3 a .AI 9 (•� 3 90 , N R q' v o a I C7'4 fl ..6.) I. 2. ;73 1N-,'1-,'1 ^; ,0 2 r ; t " - , N L e e n r 3 Number o(Canta:nr rs n n S l� < Matrix(Refer to Rex) a a . 2 ^ io I I f S ;,x g uJ ' •+ (G)reb or(C(omposrce o 11 1 gD D /t tl 3.3 3 p _ 1 C 8 8' 8' 5— z•-• Ell II 1KK - R n n mieA" NIA CC4 f.- 3 v Li p aD -4 o anV D A a,, mom I i IJ% < a n € OO nQn g.,..:I t ni , e to n :n Nn n O N 3 3 n n n w z Le r w O rl o. a El •g g g < m— oN T N N N - - N O z Cl Cl � 03 �� 8 c c r aD a = 0 0 T T _ o . 9 0* 3 of . < x '-� = ' -< C ^W to - 8 Q g K. F A E m s £ � Az�^.. n r� AN n o W 1 Z.2 o n Y O� Y El Elt M N O q 4 R O C. Y G -.Iq_q� O a n S n MIN 4 .n, O r J ry W N W O p ti IV ,_ Page 8 of 8 �a Waypoint 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 10/7/2021 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Report Number: 21-270-0002 Project Description:Von Dreble Cordova Project#2014-110 Dear Bob Branch: Waypoint Analytical Virginia, Inc. received sample(s)on 9/27/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH,dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated.This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 1gcyrc &toa r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 6 vv Waypoi lit, 7621 Whitepine Road,Richmond,VA 23237 (� Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-270-0002 Client Project Description: Von Dreble Cordova Project#2014-110 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 77888 VD Solids 09/23/2021 14:30 09/27/2021 SM-2540G WP MTN 77888 VD Solids 09/23/2021 14:30 09/27/2021 SM-4500-NH3C WP MTN 77888 VD Solids 09/23/2021 14:30 09/27/2021 SM-4500-NH3C-TKN WP MTN 77888 VD Solids 09/23/2021 14:30 09/27/2021 4500NO3F-2011 WP MTN 77888 VD Solids 09/23/2021 14:30 09/27/2021 6010D WP MTN 77888 VD Solids 09/23/2021 14:30 09/27/2021 SW-7471B WP MTN 77888 VD Solids 09/23/2021 14:30 09/27/2021 9045D WP MTN 77888 VD Solids 09/23/2021 14:30 09/27/2021 AOAC 955.01 WP MTN WP MTN-Memphis,TN: Waypoint Analytical-TN, Memphis,TN Page 2 of 6 YV VVaypoi nt 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von Dreble Cordova Bob Branch Report Date: 10/07/2021 1735 Heckle Blvd Information : Project#2014-110 Received :09/27/2021 Suite 103-291 Rock Hill , SC 29732 law,c PIc 6,roa3/ Report Number:21-270-0002 REPORT OF ANALYSIS Pauric Mc Groary Ph.D.,CPA Agronomist Lab No: 77888 Matrix: Solids Sample ID :VD Sampled: 9/23/2021 14:30 Test Results Units MQL DF Date/Time By Analytical Analyzed Method Moisture 56.7 % 0.010 1 09/28/21 16:15 FMM SM-2540G Total Kjeldahl Nitrogen 3190 mg/Kg-dry 577 1 10/04/21 14:00 JPJ iM-4500-NH3C TKI` Potassium 68.1 mg/Kg-dry 23.1 1 10/06/21 00:32 DADS 6010D Calcium 205000 mg/Kg-dry 11500 100 10/04/21 14:44 TJS 6010D Sodium 695 mg/Kg-dry 57.7 1 09/30/21 03:08 JTR 6010D Iron 1010 mg/Kg-dry 23.1 1 09/30/21 03:08 JTR 6010D Aluminum 1870 mg/Kg-dry 11.5 1 09/30/21 03:08 JTR 6010D Zinc 53.3 mg/Kg-dry 2.89 1 09/30/21 03:08 JTR 6010D Nickel 1.29 mg/Kg-dry 0.577 1 09/30/21 03:08 JTR 6010D Arsenic <1.15 mg/Kg-dry 1.15 1 09/30/21 03:08 JTR 6010D Calcium Carbonate Equivalent 67.8 % 0.1 1 10/04/21 09:35 DXT AOAC 955.01 Test Results Units MQL DF Date/Time By Analytical Analyzed Method pH 8.6 s.u. 1 09/30/21 15:14 DRS 9045D Lead 1.42 mg/Kg-dry 0.692 1 09/30/21 03:08 JTR 6010D Magnesium 2820 mg/Kg-dry 11.5 1 09/30/21 03:08 JTR 6010D Selenium <1.15 mg/Kg-dry 1.15 1 09/30/21 03:08 JTR 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 6 w \A/aypOl nt_. 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von Dreble Cordova Bob Branch Report Date: 10/07/2021 1735 Heckle Blvd Information: Project#2014-110 Received :09/27/2021 Suite 103-291 Rock Hill, SC 29732 lcuwc Int & oar REPORT Pauric Mc Groary Ph.D.,CPA Report Number:21-270-0002 Agronomist Lab No: 77888 Matrix: Solids Sample ID:VD Sampled: 9/23/2021 14:30 Total Solids 43.3 % 0.010 1 09/28/21 16:15 FMM SM-2540G Phosphorus 136 mg/Kg-dry 11.5 1 09/30/21 03:08 JTR 6010D Sulfur 891 mg/Kg-dry 23.1 1 09/30/21 03:08 JTR 6010D Copper 32.6 mg/Kg-dry 1.15 1 09/30/21 03:08 JTR 6010D Ammonia Nitrogen 245 mg/Kg-dry 231 1 10/01/21 10:30 JPJ SM-4500-NH3C Nitrate+Nitrite-N 31.6 mg/Kg-dry 11.5 1 10/04/21 15:01 ZBD 4500NO3F-2011 Cadmium <0.231 mg/Kg-dry 0.231 1 09/30/21 03:08 JTR 6010D Mercury <0.0367 mg/Kg-dry 0.0367 1 09/29/21 12:18 TJS SW-7471B Molybdenum 1.91 mg/Kg-dry 0.577 1 09/30/21 03:08 JTR 6010D Qualifiers/ B Analyte detected in blank DF Dilution Factor Definitions H Beyond holding time MQL Method Quantitation Limit Page 4 of 6 • Wa4poInt 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:46368 Customer Name: Branch Residuals and Soils LLC Report Number: 21-270-0002 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other : ! 0 UPS 0 Client 0 Courier Thermometer ID: Shipping container/cooler uncompromised? 0 Yes No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present Custody seals intact on sample bottles? Q Yes 0 No 0 Not Present Chain of Custody(COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed ®Yes Q No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 1 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No Samples were considered acceptable as cooling process had begun. Water- Sample containers properly preserved 0 Yes 0 No 0 N/A Water-VOA vials free of headspace 0 Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A High concentration container (48 hr) T Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis-14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: Brandi Watson Date&Time: 09/27/2021 14:29:47 Page 5 of 6 ;v N= 0 n �1 • 3 n T O - � is , UJ r3o s_ •_4 - A� 1 A c- 1 ' 2 7, O. .+ L _y c) < r rt h P. L .elli ' U. p. t.' O' r 0 O '1 li. 1 tn -o n ri F U V ? (` 3 V .2 3 o A _ a rr c Nil 3 �' V 1 7 = a _ 7 A 0 n w OT d r ^ 0 ^ r •o r` ^ V cu T ; � s ,. s N d o n 7 7 �` w rr A 7 \) O n H _ ( - < o >v r. m n 7D •-' Number of Containers f m 3' 3 ( �, `v G il s "\_1 (.'l (� Matrix(Refer to Key) b • - cr cr e .e N� d (1 (G)rab or(C)omposite Cr- c,,,)- a I I w co 7, 5 ,- z z ,..._ z �(3,��Crj(of 3 A et/K f.Y f� M MI RI LI a ( 1 l�\' 3' z a o - o ii 1� W O g g V m r v J o. 3, o • a , y; o v L �, o. D 7 d .. o• 0+ m n Z C. DD 3 Ln' N R N A o o �A A A A S o n T S S w -44 7 C a a rr 01 ? o o < co'— �3 f. m m A Q �� a RI a �9a v. f)5: 10° • < Cr '' i 110.1.11M c o N O n T 1 2 2 2 y� r CU C C C o = CT 0 al 1,1 ITI - 2 ai .. m a r 0�� D * C Ca C I g e S S S 2 2 3 3 d < C W Z G• p N000mo �CC ry VI r1 A 9 W Z A p G c 0 O u S y 9 n v = a s n3 9'= Ns v c n _ % ° 7 I. N A N A�1 In Cl K • N.tr. IA C tJ N N -.I r 1 AI O./Y e� O W NJ o 3 A a A N N p C 7 1 1 - d 13 e N C 1 ti O 1 _ Page 6 of 6 w Waypoint 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 11/10/2021 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Report Number: 21-300-0011 Project Description:Von Drehle Dear Bob Branch: Waypoint Analytical Virginia, Inc. received sample(s)on 10/27/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012)and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 4 l•c MC &fear Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 6 1;I�;J IP/a'yp oi n� 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-300-0011 Client Project Description: Von Drehle Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 55382 Von Drehle Solids 10/26/2021 14:00 10/27/2021 SM-2540G WP MTN 55382 Von Drehle Solids 10/26/2021 14:00 10/27/2021 SM-4500-NH3C WP MTN 55382 Von Drehle Solids 10/26/2021 14:00 10/27/2021 SM-4500-NH3C-TKN WP MTN 55382 Von Drehle Solids 10/26/2021 14:00 10/27/2021 4500NO3F-2011 WP MTN 55382 Von Drehle Solids 10/26/2021 14:00 10/27/2021 6010D WP MTN 55382 Von Drehle Solids 10/26/2021 14:00 10/27/2021 SW-74716 WP MTN 55382 Von Drehle Solids 10/26/2021 14:00 10/27/2021 9045D WP MTN 55382 Von Drehle Solids 10/26/2021 14:00 10/27/2021 AOAC 955.01 WP MTN WP MTN-Memphis,TN: Waypoint Analytical-TN,Memphis,TN Page 2 of 6 _,. VVaypoint. 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch Report Date: 11/10/2021 1735 Heckle Blvd Information: Received : 10/27/2021 Suite 103-291 Rock Hill, SC 29732 Taws c tilt &,,,,, / REPORTOFANALYSIS Pauric Mc Groary Ph.D.,CPA Report Number:21-300-0011Agronomist Lab No: 55382 Matrix: Solids Sample ID:Von Drehle Sampled: 10/26/2021 14:00 Test Results Units MQL DF Date/Time By Analytical Analyzed Method Moisture 59.7 % 0.010 1 10/28/21 16:05 FMM SM-2540G Potassium 61.8 mg/Kg-dry 24.8 1 11/09/21 04:01 TJS 6010D Calcium 195000 mg/Kg-dry 12400 100 11/09/21 19:33 JADS 6010D Sodium 769 mg/Kg-dry 62.0 1 11/09/21 04:01 TJS 6010D Aluminum 1740 mg/Kg-dry 12.4 1 11/09/21 04:01 TJS 6010D Nickel 1.56 mg/Kg-dry 0.620 1 11/09/21 04:01 TJS 6010D Arsenic 1.71 mg/Kg-dry 1.24 1 11/09/21 04:01 TJS 6010D Test Results Units MQL DF Date/Time By Analytical Analyzed Method pH 6.9 s.u. 1 11/02/21 15:09 DRS 9045D Total Solids 40.3 % 0.010 1 10/28/21 16:05 FMM SM-2540G Copper 30.0 mg/Kg-dry 1.24 1 11/09/21 04:01 TJS 6010D Lead 1.26 mg/Kg-dry 0.744 1 11/09/21 04:01 TJS 6010D Magnesium 2150 mg/Kg-dry 12.4 1 11/09/21 04:01 TJS 6010D Selenium <1.24 mg/Kg-dry 1.24 1 11/09/21 04:01 TJS 6010D Total Kjeldahl Nitrogen 4240 mg/Kg-dry 620 1 11/01/21 10:00 JPJ ;M-4500-NH3C-TKP Qualifiers/ B Analyte detected in blank DF Dilution Factor Definitions H Beyond holding time MQL Method Quantitation Limit Page 3 of 6 C"*. * VVaypo I nt. 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch Report Date: 11/10/2021 1735 Heckle Blvd Information : Received : 10/27/2021 Suite 103-291 Rock Hill , SC 29732 10.14/1c Plc 610aK/ REPORT Pauric Mc Groary Ph.D.,CPA Report Number:21-300-0011 Agronomist Lab No: 55382 Matrix: Solids Sample ID:Von Drehle Sampled: 10/26/2021 14:00 Phosphorus 134 mg/Kg-dry 12.4 1 11/09/21 04:01 TJS 6010D Zinc 143 mg/Kg-dry 3.10 1 11/09/21 04:01 TJS 6010D Ammonia Nitrogen <248 mg/Kg-dry 248 1 11/03/21 10:00 JP] SM-4500-NH3C Nitrate+Nitrite-N 15.8 mg/Kg-dry 11.6 1 11/03/21 15:36 ZBD 4500NO3F-2011 Cadmium <0.248 mg/Kg-dry 0.248 1 11/09/21 04:01 TJS 6010D Mercury <0.0359 mg/Kg-dry 0.0359 1 11/05/21 13:13 TJS SW-7471B Calcium Carbonate Equivalent 3.3 % 0.1 1 11/02/21 13:06 DXT AOAC 955.01 Molybdenum 4.84 mg/Kg-dry 0.620 1 11/09/21 04:01 TJS 6010D Qualifiers/ B Analyte detected in blank DF Dilution Factor Definitions H Beyond holding time MQL Method Quantitation Limit Page 4 of 6 vo Waipoint . 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:46368 Customer Name: Branch Residuals and Soils LLC Report Number: 21-300-0011 Shipping Method 0 Fed Ex 0 US Postal 0 Lab Other: 0 UPS 0 Client 0 Courier Thermometer ID: Shipping container/cooler uncompromised? 0 Yes No Number of coolers/boxes received r1 Custody seals intact on shipping container/cooler? 0 Yes i j No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody(COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No Samples were considered acceptable as cooling process had begun. Water- Sample containers properly preserved 0 Yes 0 No 0 N/A Water-VOA vials free of headspace 0 Yes 0 No 0 N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A 1 High concentration container(48 hr) I- Low concentration EnCore samplers (48 hr) I High concentration pre-weighed (methanol-14 d) Low conc pre-weighed vials (Sod Bis-14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: Brandi Watson Date&Time: 10/27/2021 13:58:22 Page 5 of 6 ., o rye o a t7,4 TJ z = s O t A ' tav — V` L .i-- n _ ' i 3 : :-= g /" >� -I .< I C z f- Cr �� * 3 a' o ...0 i_ 7..., • { . V z N a t'1 a Oil 0 o v 3 N .0 m • 3-d O N, ma.: a C N V 3 - o Go 3 P- m v' N wo ° N e c, N °' aw ' : ^ O n -.CD t T o o h N N d n nT21 .0 � �} 3 —` Number of Containers f9 3` c3 .o U- . T _N . LA Matrix(Refer to Key) o. o. 1 .., 3 m ti ) (G)rab or(C)omposite �- o 7 Z. o A' ov, 7J N z• z z Ai�CA ti �Iai d S t " CC.E' Di eo, . N 9 DO G TT A s • a Cl. N3 _ �� U' a, Z» m kvS � I N rug o 1 = c❑a a N N - G- _ N CI C � �� It z z 2 v--I --I -Di r-= - 2 Ctmm ' WM v 0 * d WEIS n o 1 " . _ el S eD 4. t� ^ F an K n x x x 2 O S .- Q 0 K o o E =99 s� . * C, 3 0-0 ,„, xx a '' fl 3, 0 Z N O N tV ggo N.) , V: C v. N ri1 iN 10 O O 0 0 0 u' r-' - O 0 d d d 3 --▪ 3 A A 4. N O S ii n 1 -i -I Q r� A3 A 30 1 m O - Page a oi: 6 �b Waypoi ft. 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 12/6/2021 Branch Residuals and Soils LLC Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Report Number: 21-327-0001 Project Description:Von Drehle Dear Bob Branch: Waypoint Analytical Virginia, Inc. received sample(s) on 11/23/2021 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as- received basis unless otherwise indicated.This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, al,cuuf c tit &tea / Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 6 vv Waypoi flT 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 21-327-0001 Client Project Description: Von Drehle Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 55587 VD Solids 11/22/2021 13:30 11/23/2021 SM-2540G WP MTN 55587 VD Solids 11/22/2021 13:30 11/23/2021 SM-4500-NH3C WP MTN 55587 VD Solids 11/22/2021 13:30 11/23/2021 SM-4500-NH3C-TKN WP MTN 55587 VD Solids 11/22/2021 13:30 11/23/2021 4500NO3F-2011 WP MTN 55587 VD Solids 11/22/2021 13:30 11/23/2021 6010D WP MTN 55587 VD Solids 11/22/2021 13:30 11/23/2021 SW-74718 WP MTN 55587 VD Solids 11/22/2021 13:30 11/23/2021 9045D WP MTN 55587 VD Solids 11/22/2021 13:30 11/23/2021 AOAC 955.01 WP MTN WP MTN-Memphis,TN: Waypoint Analytical-TN,Memphis,TN Page 2 of 6 � J Wapoint ) 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch Report Date: 12/06/2021 1735 Heckle Blvd Information : Received : 11/23/2021 Suite 103-291 Rock Hill, SC 29732 Iowa plc Grown REPORTOFANALYSIS Pauric Mc Groary Ph.D.,CPA Report Number:21-327-0001 Agronomist Lab No: 55587 Matrix: Solids Sample ID:VD Sampled: 11/22/2021 13:30 Test Results Units MOL DF Date/Time By Analytical Analyzed Method Total Kjeldahl Nitrogen 3940 mg/Kg-dry 653 1 12/02/21 09:00 JP] >M-4500-NH3C TKP Calcium 181000 mg/Kg-dry 2610 20 12/03/21 04:07 JADS 6010D Aluminum 1970 mg/Kg-dry 13.1 1 11/30/21 21:34 DADS 6010D Zinc 108 mg/Kg-dry 3.26 1 11/30/21 21:34 JADS 6010D Nitrate+Nitrite-N 14.2 mg/Kg-dry 12.2 1 12/01/21 14:25 ZBD 4500NO3F-2011 Lead 1.35 mg/Kg-dry 0.783 1 11/30/21 21:34 JADS 6010D Arsenic <1.31 mg/Kg-dry 1.31 1 11/30/21 21:34 JADS 6010D Mercury <0.0355 mg/Kg-dry 0.0355 1 12/03/21 15:38 JW2 SW-7471B Selenium 1.91 mg/Kg-dry 1.31 1 11/30/21 21:34 DADS 6010D Test Results Units MOL DF Date/Time By Analytical Analyzed Method Phosphorus 225 B mg/Kg-dry 13.1 1 11/30/21 21:34 DADS 6010D Chromium 2.79 mg/Kg-dry 0.652 1 11/30/21 21:34 JADS 6010D Molybdenum 3.89 mg/Kg-dry 0.652 1 11/30/21 21:34 JADS 6010D Qualifiers/ B Analyte detected in blank DF Dilution Factor Definitions L Limit Exceeded MQL Method Quantitation Limit Page 3 of 6 e•) \%'ypoint 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46368 Branch Residuals and Soils LLC Project Von Drehle Bob Branch Report Date: 12/06/2021 1735 Heckle Blvd Information : Received : 11/23/2021 Suite 103-291 Rock Hill, SC 29732 ti.w,c plc toay/ Report Number:21-327-0001 REPORT OF ANALYSIS Pauric Mc Groary Ph.D.,CPA Agronomist Lab No: 55587 Matrix: Solids Sample ID:VD Sampled: 11/22/2021 13:30 Analytical Method: SM-2540G Test Results Units MQL DF Date/Time By Analytical Analyzed Batch Moisture 61.7 % 0.010 1 11/29/21 17:15 FMM L587060 Total Solids 38.3 % 0.010 1 11/29/21 17:15 FMM SM-2540G Potassium 61.6 mg/Kg-dry 26.1 1 11/30/21 21:34 JADS 6010D Magnesium 2110 mg/Kg-dry 13.1 1 11/30/21 21:34 DADS 6010D Sodium 804 mg/Kg-dry 65.3 1 11/30/21 21:34 JADS 6010D Copper 46.2 mg/Kg-dry 1.31 1 11/30/21 21:34 JADS 6010D Ammonia Nitrogen <261 mg/Kg-dry 261 1 12/02/21 12:30 JPJ SM-4500-NH3C Cadmium <0.261 mg/Kg-dry 0.261 1 11/30/21 21:34 JADS 6010D Nickel 1.07 mg/Kg-dry 0.652 1 11/30/21 21:34 JADS 6010D pH 7.5 s.u. 1 12/01/21 15:59 ADM 9045D Calcium Carbonate Equivalent 58.5 % 0.1 1 12/01/21 09:36 DXT AOAC 955.01 Qualifiers/ B Analyte detected in blank DF Dilution Factor Definitions H Beyond holding time MQL Method Quantitation Limit Page 4 of 6 vo • Waypou lit 7621 Whitepine Road,Richmond,VA 23237 Main 804-743-9401°Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number:46368 Customer Name: Branch Residuals and Soils LLC Report Number: 21-327-0001 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other : ® UPS 0 Client 0 Courier Thermometer ID: I Shipping container/cooler uncompromised? Sj Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody(COC) present? c Yes 0 No COC agrees with sample label(s)? *Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? #Yes 0 No Cooler temperature in compliance? J Yes 0 No Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No Samples were considered acceptable as cooling process had begun. Water-Sample containers properly preserved 0 Yes 0 No # N/A Water-VOA vials free of headspace 0 Yes 0 No * N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A High concentration container(48 hr) Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) r- Low conc pre-weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: Brandi Watson Date&Time: 11/23/2021 13:08:55 Page 5 of 6 le le i h O ti - v � N ic y O 2 m � �I- r �/ G i W :• -T ^` C r, - -1 'fr..' r 3 5 - y7741,.,• c1 3 ma r c Z M K �� I 0 r, V IrD n t R. 9, rc ° rm ` �J o '7 = .^. �; �i C 3 ^ ° C �`i H Q s N '��.f c >> • = a 57'i 2 L/o r.,. W ^ . m a a ti d -. n tt r = x a "� -o 3• n � ft n m a N iT v, , y A n . A 3 Number of Containers A sS a (�" Matrix(Refer to Key) n. s < ' 2 < •e •• 3 (_' (G)rab or(C)omposite ` m Z Z CI • \ I di, C. i b 3 ry NI A^' ret X I r red Am(A4 AAA -ti bn, 2 n▪ . -+•..1 st, go I m A a I -o i- - - -- - �.._ ._ a+ a N d n c 19 �m w ` nT S S A -I "1 �' -r r. Z I 22, °N' - c a oa x a enm d Z a 44. ` T o A I t rl� z 72 70 3 3 ° :; n Q re n <CDC C 3• 3 Y 6 19 a A w 1 O{ �� a a a-c I = m�� VI Tit V1 . N �� fl m 5 I a__ 2 Z 2 I �� N IM110 m m m - S LI ++ m D r w > Vf N .... . r nu. 0�� k0 0.-.) r• r- f•1 S 2 S Z 2 .Tr r r1 . -c - EME 3 AI ^' = . 2c „ nr4i 00 =ES A Z N I''' p - N 2 ar N a N M N 0 0 C 0 - w s m 9. . 2" u R R 3 8 ' fs n N 0 g 0 j g 1 9 n 3 Y.ge 6 Lir-o TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORT M I C RO BAC R: Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KI A0090 Project Description Residuals Sample-Annual For: Mr.Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Administration Brittany Smith Tuesday,January 19,2021 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc.-Fayetteville. If you have any questions,comments,or require further assistance regarding this report,please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report.Analytical results are reported on a'as received'basis unless specified otherwise.Analytical results for solids with units ending in(dry)are reported on a dry weight basis. A statement of uncertainty for each analysis is available upon request.This laboratory report shall not be reproduced,except in full,without the written approval of Microbac Laboratories.The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 16 ( MICROBACP Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K1A0090 Von Drehle Corporation Project Name: Residuals Sample-Annual Mr.Chris Fowler Project/PO Number:2030767 126 First Street Received: 01/06/2021 Cordova, NC 28330 Reported: 01/19/2021 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Effluent K1A0090-01 Aqueous Grab 01/06/21 11:24 01/06/21 14:52 Page 2 of 16 { MICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K1A0090 Analytical Testing Parameters Client Sample ID: Effluent Sample Matrix: Aqueous Collected By: Wright Lab Sample ID: K1A0090-01 Collection Date: 01/06/2021 11:24 Analyses Subcontracted to:Microbac Laboratories Inc.,-Marietta,OH Metals TCLP by AA Result RL Units DF Note Prepared Analyzed Analyst EPA 7470A Mercury <0.00200 0.00200 mg/L 1 01/13/21 0607 01/13/21 1345 TMM Metals TCLP by ICP Result RL Units DF Note Prepared Analyzed Analyst EPA 6010D Arsenic <0.200 0.200 mg/L 1 01/13/21 0621 01/13/21 1640 KHL Barium 0.116 0.100 mg/L 1 01/13/21 0621 01/13/21 1640 KHL Cadmium <0.0200 0.0200 mg/L 1 01/13/21 0621 01/13/21 1640 KHL Chromium <0.0500 0.0500 mg/L 1 01/13/21 0621 01/13/21 1640 KHL Lead <0.200 0.200 mg/L 1 01/13/21 0621 01/13/21 1640 KHL Selenium <0.350 0.350 mg/L 1 01/13/21 0621 01/13/21 1640 KHL Silver <0.100 0.100 mg/L 1 01/13/21 0621 01/13/21 1640 KHL Volatile Organic Compounds TCLP Result RL Units DF Note Prepared Analyzed Analyst by GCMS EPA 8260E Benzene <50.0 50.0 ug/L 10 01/13/21 1609 EEA 2-Butanone <100 100 ug/L 10 01/13/21 1609 EEA Carbon tetrachloride <50.0 50.0 ug/L 10 01/13/21 1609 EEA Chlorobenzene <50.0 50.0 ug/L 10 01/13/21 1609 EEA Chloroform <50.0 50.0 ug/L 10 01/13/21 1609 EEA 1,2-Dichloroethane <50.0 50.0 ug/L 10 Y 01/13/21 1609 EEA 1,1-Dichloroethene <50.0 50.0 ug/L 10 Y 01/13/21 1609 EEA Tetrachloroethene <50.0 50.0 ug/L 10 01/13/21 1609 EEA Trichloroethene <50.0 50.0 ug/L 10 03 01/13/21 1609 EEA Vinyl chloride <100 100 ug/L 10 01/13/21 1609 EEA Surrogate:4-Bromofluorobenzene 118 Limit:86-115 %Rec 10 S1 01/13/21 1609 EEA Surrogate:Dibromofluoromethane 102 Limit:86-118 %Rec 10 01/13/21 1609 EEA Surrogate:1,2-Dichloroethane-d4 101 Limit:80-120 %Rec 10 01/13/21 1609 EEA Surrogate:Toluene-d8 101 Limit:88-110 %Rec 10 01/13/21 1609 EEA Herbicides TCLP by GC/ECD Result RL Units DF Note Prepared Analyzed Analyst EPA 8151A 2,4,5-TP(Silvex)[2C] <2.00 2.00 ug/L 1 01/14/21 1750 01/18/21 2119 ECL 2,4-D[2C] <20.0 20.0 ug/L 1 01/14/21 1750 01/18/21 2119 ECL Surrogate:2,4-Dichloropenylacetic acid 77.0 Limit:20-144 %Rec 1 01/14/21 1750 01/18/21 2119 ECL [2C] Microbac Laboratories. Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 16 1 ( MICROBAC ' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K1A0090 Client Sample ID: Effluent Sample Matrix: Aqueous Collected By: Wright Lab Sample ID: K1A0090-01 Collection Date: 01/06/2021 11:24 Pesticides TCLP by GC/ECD Result RL Units DF Note Prepared Analyzed Analyst EPA 8081A alpha-Chlordane <0.500 0.500 ug/L 1 01/12/21 0850 01/15/21 0220 ECL Endrin <0.500 0.500 ug/L 1 01/12/21 0850 01/15/21 0220 ECL gamma Chlordane <0.500 0.500 ug/L 1 01/12/21 0850 01/15/21 0220 ECL gamma-BHC(Lindane) <0.500 0.500 ug/L 1 01/12/21 0850 01/15/21 0220 ECL Heptachlor <0.500 0.500 ug/L 1 01/12/21 0850 01/15/21 0220 ECL Heptachlor epoxide <0.500 0.500 ug/L 1 01/12/21 0850 01/15/21 0220 ECL Methoxychlor <0.500 0.500 ug/L 1 01/12/21 0850 01/15/21 0220 ECL Toxaphene <10.0 10.0 ug/L 1 01/12/21 0850 01/15/21 0220 ECL Surrogate:2,4,5,6-Tetrachloro-m-xylene 66.4 Limit:20-130 %Rec 1 01/12/21 0850 01/15/21 0220 ECL Surrogate:Decachlorobiphenyl 16.9 Limit:25-140 %Rec 1 S2 01/12/21 0850 01/15/21 0220 ECL (BZ-209) Semivolatile Organic Compounds Result RL Units DF Note Prepared Analyzed Analyst TCLP by GCMS EPA 8270C 1,4-Dichlorobenzene <50.0 50.0 ug/L 1 Y 01/12/21 1600 01/14/21 1820 SCB 2,4-Dinitrotoluene <50.0 50.0 ug/L 1 Y 01/12/21 1600 01/14/21 1820 SCB Hexachlorobenzene <50.0 50.0 ug/L 1 Y 01/12/21 1600 01/14/21 1820 SCB Hexachlorobutadiene <50.0 50.0 ug/L 1 Y 01/12/21 1600 01/14/21 1820 SCB Hexachloroethane <50.0 50.0 ug/L 1 Y 01/12/21 1600 01/14/21 1820 SCB 2-Methylphenol <50.0 50.0 ug/L 1 Y 01/12/21 1600 01/14/21 1820 SCB 3-,4-Methylphenol <50.0 50.0 ug/L 1 Y 01/12/21 1600 01/14/21 1820 SCB Nitrobenzene <50.0 50.0 ug/L 1 Y 01/12/21 1600 01/14/21 1820 SCB Pentachlorophenol <250 250 ug/L 1 08,Y 01/12/21 1600 01/14/21 1820 SCB Pyridine <250 250 ug/L 1 Q3,Y 01/12/21 1600 01/14/21 1820 SCB 2,4,6-Trichlorophenol <50.0 50.0 ug/L 1 Y 01/12/21 1600 01/14/21 1820 SCB 2,4,5-Trichlorophenol <50.0 50.0 ug/L 1 Y 01/12/21 1600 01/14/21 1820 SCB Surrogate:2-Fluorobiphenyl 69.6 Limit:43-116 %Rec 1 01/12/21 1600 01/14/21 1820 SCB Surrogate:2-Fluorophenol 48.0 Limit:19-119 %Rec 1 01/12/21 1600 01/14/21 1820 SCB Surrogate:Nitrobenzene-d5 67.3 Limit:35-114 %Rec 1 01/12/21 1600 01/14/21 1820 SCB Surrogate:Phenol-d5 33.1 Limit: 10-120 %Rec 1 01/12/21 1600 01/14/21 1820 SCB Surrogate:p-Terphenyl-d14 74.6 Limit:10-130 %Rec 1 01/12/21 1600 01/14/21 1820 SCB Surrogate:2,4,6-Tribromophenol 115 Limit:22-142 %Rec 1 01/12/21 1600 01/14/21 1820 SCB Microbac Laboratories,Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 16 6) MICROBAC • Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K1A0090 Batch Log Summary Method Batch Laboratory ID Client(Source ID EPA 8081A B1A0490 B1A0490-BLK1 B1A0490-BS1 B 1 A0490-BSD 1 B1A0490-BS2 B1A0490-BLK2 K1A0090-01 Effluent Method _ _ Batch __...__ Laboratory ID Client I Souyce_�D EPA 8270C B1A0492 B1A0492-BLK1 B1A0492-BLK2 B1A0492-BS1 B1A0492-BSD1 K1A0090-01 Effluent Method Batch _ LaQtatolyJD Client 1 Source ID EPA 7470A B1A0554 B1A0554-BLK1 B1A0554-BLK2 B1A0554-BS1 K1A0090-01 Effluent B1A0554-MS1 M1A0484-01 B1A0554-MSD1 M1A0484-01 B1A0554-PS1 M1A0484-01 Method Batch Laboratory ID Client 1 Source ID EPA 6010D B1A0555 B1A0555-BLK1 B1A0555-BLK2 B1A0555-BS1 B1A0555-PS1 M1A0450-02 B1A0555-SRL1 M1A0450-02 B1A0555-MS1 M1A0484-01 B1A0555-MSD1 M1A0484-01 K1A0090-01 Effluent Method_ Batch Laboratory ID Client 1 Source ID EPA 8260E B1A0574 B1A0574-BLK1 B1A0574-BLK2 B 1 A0574-BS 1 B1A0574-BSD1 K1 A0090-01 Effluent B 1 A0574-MS 1 M1A0450-02 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 16 OMICROBAC'`' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KI A0090 Method Batch Laboratory ID Client 1 Source ID EPA 8151A B1A0598 B1A0598-BLK1 B1A0598-BS1 B1A0598-MRL1 B1A0598-BSD1 B1A0598-MS1 M1A0450-02 K1A0090-01 Effluent B1A0598-BLK2 B1A0598-BLK3 Batch Quality Control Summary: Microbac Laboratories Inc.,-Marietta,OH Spike Source %REC RPD Metals TCLP by AA Result RL Units Level Result %REC Limits RPD Limit Notes Batch B1A0554-EPA 245.1 &EPA 7470A-EPA 7470A Blank#684(B1A0554-BLK1) Prepared&Analyzed:01/13/2021 Mercury <0.00200 0.00200 mg/L Blank flt_bik(B1A0554-BLK2) Prepared&Analyzed:01/13/2021 Mercury <0.00200 0.00200 mg/L LCS(B1A0554-BS1) Prepared&Analyzed:01/13/2021 Mercury 0.00352 0.000200 mg/L 0.00400 88.0 80-120 Matrix Spike(B1A0554-MS1) Source:M1A0484-01 Prepared&Analyzed:01/13/2021 Mercury 0.0434 0.00200 mg/L 0.0400 ND 108 75-125 Matrix Spike Dup(B1A0554-MSD1) Source:M1A0484-01 Prepared&Analyzed:01/13/2021 Mercury 0.0438 0.00200 mg/L 0.0400 ND 110 75-125 0.986 20 Post Spike(B1A0554-PS1) Source:M1A0484-01 Prepared&Analyzed:01/13/2021 Mercury 1.09 ug/L 1.00 -0.0878 109 85-115 Spike Source %REC RPD Metals TCLP by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch B1A0555-3015A_6010-EPA 6010D Blank#684(B1 A0555-BLK1) Prepared&Analyzed:01/13/2021 Arsenic <0.200 0.200 mg/L Barium <0.100 0.100 mg/L Cadmium <0.0200 0.0200 mg/L Chromium <0.0500 0.0500 mg/L Lead <0.200 0.200 mg/L Selenium <0.350 0.350 mg/L Silver <0.100 0.100 mg/L Blank flt_blk(B1A0555-BLK2) Prepared&Analyzed:0.1/13/2021 Arsenic <0.200 0.200 mg/L Barium <0.100 0.100 mg/L Cadmium <0.0200 0.0200 mg/L Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 16 4VMICROBACw Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K1A0090 Spike Source %REC RPD Metals TCLP by ICP Result RL Units Level Result %REC Limits RPD Limit Notes Batch B1A0555-3015A 6010-EPA 6010D Blank flt_bik(B1A0555-BLK2) Prepared&Analyzed:01/13/2021 Chromium <0.0500 0.0500 mg/L Lead <0.200 0.200 mg/L Selenium <0.350 0.350 mg/L Silver <0.100 0.100 mg/L LCS(B1A0555-BS1) Prepared&Analyzed:01/13/2021 Arsenic 0.243 0.0250 mg/L 0.250 97.2 80-120 Barium 0.643 0.0125 mg/L 0.625 103 80-120 Cadmium 0.0317 0.00250 mg/L 0.0313 102 80-120 Chromium 0.320 0.00625 mg/L 0.313 102 80-120 Lead 0.320 0.0250 mg/L 0.313 102 80-120 Selenium 0.236 0.0438 mg/L 0.250 94.4 80-120 Silver 0.248 0.0125 mg/L 0.250 99.1 80-120 Matrix Spike(B1A0555-MS1) Source:M1A0484-01 Prepared&Analyzed:01/13/2021 Arsenic 2.00 0.200 mg/L 2.00 ND 100 75-125 Barium 5.25 0.100 mg/L 5.00 0.198 101 75-125 Cadmium 0.250 0.0200 mg/L 0.250 ND 99.8 75-125 Chromium 2.54 0.0500 mg/L 2.50 ND 102 75-125 Lead 2.48 0.200 mg/L 2.50 ND 99.3 75-125 Selenium 1.96 0.350 mg/L 2.00 ND 97.8 75-125 Silver 1.97 0.100 mg/L 2.00 ND 98.3 75-125 Matrix Spike Dup(B1A0555-MSD1) Source:M1A0484-01 Prepared&Analyzed:01/13/2021 Arsenic 2.02 0.200 mg/L 2.00 ND 101 75-125 0.993 20 Barium 5.38 0.100 mg/L 5.00 0.198 104 75-125 2.56 20 Cadmium 0.256 0.0200 mg/L 0.250 ND 102 75-125 2.57 20 Chromium 2.61 0.0500 mg/L 2.50 ND 104 75-125 2.60 20 Lead 2.53 0.200 mg/L 2.50 ND 101 75-125 2.01 20 Selenium 2.03 0.350 mg/L 2.00 ND 102 75-125 3.87 20 Silver 2.01 0.100 mg/L 2.00 ND 101 75-125 2.37 20 Post Spike(B1A0555-PS1) Source:M1A0450-02 Prepared&Analyzed:01/13/2021 Arsenic 0.197 mg/L 0.200 0.000342 98.4 80-120 Barium 0.515 mg/L 0.500 0.0168 99.5 80-120 Cadmium 0.0246 mg/L 0.0250 0.000540 96.1 80-120 Chromium 0.252 mg/L 0.250 0.00107 100 80-120 Lead 0.246 mg/L 0.250 0.000495 98.2 80-120 Selenium 0.190 mg/L 0.200 -0.00443 95.2 80-120 Silver 0.194 mg/L 0.200 -0.000351 97.2 80-120 Spike Source %REC RPD Volatile Organic Compounds Result RL Units Level Result %REC Limits RPD Limit Notes TCLP by GCMS Batch B1A0574-5030_8260-EPA 8260E Blank(B1 A0574-BLK1) Prepared&Analyzed:01/13/2021 Benzene <50.0 50.0 ug/L Mir robac Laboratories, Inc 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p 1 www.microbac.com Page 7 of 16 ,} MICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K1A0090 Spike Source %REC RPD Volatile Organic Compounds Result RL Units Level Result %REC Limits RPD Limit Notes TCLP by GCMS Batch B1A0574-5030_8260-EPA 8260B Blank(B1A0574-BLK1) Prepared&Analyzed:01/13/2021 2-Butanone <100 100 ug/L Carbon tetrachloride <50.0 50.0 ug/L Chlorobenzene <50.0 50.0 ug/L Chloroform <50.0 50.0 ug/L 1,2-Dichloroethane <50.0 50.0 ug/L 1,1-Dichloroethene <50.0 50.0 ug/L Tetrachloroethene <50.0 50.0 ug/L Trichloroethene <50.0 50.0 ug/L Vinyl chloride <100 100 ug/L Surrogate:4-Bromofluorobenzene 59.2 ug/L 50.0 118 86-115 S1 Surrogate:Dibromofluoromethane 51.1 ug/L 50.0 102 86-118 Surrogate:1,2-Dichloroethane-d4 50.0 ug/L 50.0 100 80-120 Surrogate:Toluene-d8 49.4 ug/L 50.0 98.9 88-110 Blank(B1A0574-BLK2) Prepared&Analyzed:01/13/2021 Benzene <50.0 50.0 ug/L 2-Butanone <100 100 ug/L Carbon tetrachloride <50.0 50.0 ug/L Chlorobenzene <50.0 50.0 ug/L Chloroform <50.0 50.0 ug/L 1,2-Dichloroethane <50.0 50.0 ug/L 1,1-Dichloroethene <50.0 50.0 ug/L Tetrachloroethene <50.0 50.0 ug/L Trichloroethene <50.0 50.0 ug/L Vinyl chloride <100 100 ug/L Surrogate:4-Bromofluorobenzene 58.2 ug/L 50.0 116 86-115 S1 Surrogate:Dibromofluoromethane 49.8 ug/L 50.0 99.6 86-118 Surrogate:1,2-Dichloroethane-d4 49.7 ug/L 50.0 99.4 80-120 Surrogate:Toluene-d8 50.0 ug/L 50.0 100 88-110 LCS(B1A0574-BS1) Prepared&Analyzed:01/13/2021 Benzene 17.1 5.00 ug/L 20.0 85.4 80-121 2-Butanone 16.6 10.0 ug/L 20.0 83.2 10-170 Carbon tetrachloride 17.0 5.00 ug/L 20.0 84.9 65-140 Chlorobenzene 17.8 5.00 ug/L 20.0 89.1 80-120 Chloroform 16.6 5.00 ug/L 20.0 82.8 80-125 1,2-Dichloroethane 17.5 5.00 ug/L 20.0 87.4 80-129 1,1-Dichloroethene 16.1 5.00 ug/L 20.0 80.3 80-132 Tetrachloroethene 16.7 5.00 ug/L 20.0 83.3 80-124 Trichloroethene 15.6 5.00 ug/L 20.0 77.9 80-122 Q3 Vinyl chloride 17.2 10.0 ug/L 20.0 85.8 50-170 Surrogate:4-Bromotluorobenzene 46.7 ug/L 50.0 93.4 86-115 Surrogate:Dibromofluoromethane 49.6 ug/L 50.0 99.3 86-118 Surrogate:1,2-Dichloroethane-d4 50.1 ug/L 50.0 100 80-120 Surrogate:Toluene-d8 47.4 ug/L 50.0 94.8 88-110 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 8 of 16 <75) MICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K1 A0090 Spike Source %REC RPD Volatile Organic Compounds Result RL Units Level Result %REC Limits RPD Limit Notes TCLP by GCMS Batch B1A0574-5030_8260-EPA 8260E LCS Dup(B1A0574-BSD1) Prepared&Analyzed:01/13/2021 Benzene 19.8 5.00 ug/L 20.0 98.9 80-121 14.7 20 2-Butanone 20.2 10.0 ug/L 20.0 101 10-170 19.1 20 Carbon tetrachloride 19.4 5.00 ug/L 20.0 97.0 65-140 13.3 20 Chlorobenzene 20.5 5.00 ug/L 20.0 103 80-120 14.2 20 Chloroform 18.9 5.00 ug/L 20.0 94.4 80-125 13.1 20 1,2-Dichloroethane 20.1 5.00 ug/L 20.0 101 80-129 13.9 20 1,1-Dichloroethene 18.7 5.00 ug/L 20.0 93.4 80-132 15.1 20 Tetrachloroethene 18.9 5.00 ug/L 20.0 94.6 80-124 12.7 20 Trichloroethene 18.2 5.00 ug/L 20.0 91.1 80-122 15.6 20 Vinyl chloride 18.8 10.0 ug/L 20.0 94.1 50-170 9.23 20 Surrogate:4-Bromofluorobenzene 50.3 ug/L 50.0 101 86-115 Surrogate:Dibromofluoromethane 51.1 ug/L 50.0 102 86-118 Surrogate:1,2-Dichloroethane-d4 51.1 ug/L 50.0 102 80-120 Surrogate:Toluene-d8 49.0 ug/L 50.0 98.0 88-110 Matrix Spike(B1A0574-MS1) Source:M1A0450-02 Prepared&Analyzed:01/13/2021 Benzene 204 50.0 ug/L 200 ND 102 80-121 2-Butanone 1030 100 ug/L 200 829 102 10-170 Carbon tetrachloride 203 50.0 ug/L 200 ND 102 65-140 Chlorobenzene 211 50.0 ug/L 200 ND 105 80-120 Chloroform 203 50.0 ug/L 200 ND 101 80-125 1,2-Dichloroethane 208 50.0 ug/L 200 ND 104 80-129 1,1-Dichloroethene 184 50.0 ug/L 200 ND 92.0 80-132 Tetrachloroethene 191 50.0 ug/L 200 ND 95.3 80-124 Trichloroethene 183 50.0 ug/L 200 ND 91.7 80-122 Vinyl chloride 156 100 ug/L 200 ND 78.1 50-170 Surrogate:4-Bromofluorobenzene 53.9 ug/L 50.0 108 86-115 Surrogate:Dibromofluoromethane 51.8 ug/L 50.0 104 86-118 Surrogate:1,2-Dichloroethane-d4 52.2 ug/L 50.0 104 80-120 Surrogate:Toluene-d8 50.4 ug/L 50.0 101 88-110 Spike Source %REC RPD Herbicides TCLP by GC/ECD Result RL Units Level Result %REC Limits RPD Limit Notes Batch B1A0598-8151_WATER-EPA 8151A Blank(B1A0598-BLK1) Prepared:01/14/2021 Analyzed:01/18/2021 2,4,5-TP(Silvex) <2.00 2.00 ug/L 2,4,5-TP(Silvex)[2C] <2.00 2.00 ug/L 2,4-D <20.0 20.0 ug/L 2,4-D[2C] <20.0 20.0 ug/L Surrogate:2,4-Dichloropenylacetic acid 21.5 ug/L 50.0 43.0 20-144 Surrogate:2,4-Dichloropenylacetic acid 12C,1 23.4 ug/L 50.0 46.7 20-144 Blank(B1A0598-BLK2) Prepared:01/14/2021 Analyzed:01/18/2021 2,4,5-TP(Silvex)[2C] <2.00 2.00 ug/L 2,4-D[2C] <20.0 20.0 ug/L Microbac Laboratories,Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 9 of 16 < MICROBAC ' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K1A0090 Spike Source %REC RPD Herbicides TCLP by GC/ECD Result RL Units Level Result %REC Limits RPD Limit Notes Batch B1A0598-8151 WATER-EPA 8151A Blank(B1A0598-BLK2) Prepared:01/14/2021 Analyzed:01/18/2021 Surrogate:2,4-D(chloropenylacetic acid(2CJ 23.0 ug/L 50.0 46.1 20-144 Blank(B1A0598-BLK3) Prepared:01/14/2021 Analyzed:01/18/2021 2,4,5-TP(Silvex)[2C] <2.00 2.00 ug/L 2,4-D[2C] <20.0 20.0 ug/L Surrogate:2,4-Dichloropenylacetic acid(2CJ 39.2 ug/L 50.0 78.4 20-144 LCS(B1A0598-BS1) Prepared:01/14/2021 Analyzed:01/18/2021 2,4,5-TP(Silvex)[2C] 0.252 0.200 ug/L 0.500 50.4 25-120 2,4-D[2C] 2.47 2.00 ug/L 5.00 49.3 20-110 Surrogate;2,4-Dlchloropenylacetic acid(2C) 2.47 ug/L 5.00 49.3 20-144 LCS Dup(B1A0598-BSD1) Prepared:01/14/2021 Analyzed:01/18/2021 2,4,5-TP(Silvex)[2C] 0.337 0.200 ug/L 0.500 67.3 25-120 28.7 30 2,4-D[2C] 3.26 2.00 ug/L 5.00 65.2 20-110 27.8 30 Surrogate:2,4-Dichloropenylacehc acid 12CJ 3.23 ug/L 5.00 64.6 20-144 Matrix Spike(B1A0598-MS1) Source:M1A0450-02 Prepared:01/14/2021 Analyzed:01/18/2021 2,4,5-TP(Silvex)[2C] <2.00 2.00 ug/L 5.00 ND 26.7 25-120 2,4-D[2C] <20.0 20.0 ug/L 50.0 ND 24.8 20-110 Surrogate:2,4-Dichloropenylacetic acid(2CJ 12.4 ug/L 50.0 24.9 20-144 Spike Source %REC RPD Pesticides TCLP by GCIECD Result RL Units Level Result %REC Limits RPD Limit Notes Batch B1A0490-3510C_8081 -EPA 8081A Blank(B1A0490-BLK1) Prepared:01/12/2021 Analyzed:01/14/2021 alpha-Chlordane <0.500 0.500 ug/L Endrin <0.500 0.500 ug/L gamma Chlordane <0.500 0.500 ug/L gamma-BHC(Lindane) <0.500 0.500 ug/L Heptachlor <0.500 0.500 ug/L Heptachlor epoxide <0.500 0.500 ug/L Methoxychlor <0.500 0.500 ug/L Toxaphene <10.0 10.0 ug/L Surrogate:2,4,5,6-Tetrachloro-m-xylene 1.73 ug/L 2.00 86.6 20-130 Surrogate:Decachloroblphenyl (BZ-209) 1.78 ug/L 2.00 88.8 25-140 Blank(B1A0490-BLK2) Prepared:01/12/2021 Analyzed:01/14/2021 alpha-Chlordane <0.500 0.500 ug/L Endrin <0.500 0.500 ug/L gamma Chlordane <0.500 0.500 ug/L gamma-BHC(Lindane) <0.500 0.500 ug/L Heptachlor <0.500 0.500 ug/L Heptachlor epoxide <0.500 0.500 ug/L Methoxychlor <0.500 0.500 ug/L Toxaphene <10.0 10.0 ug/L Surrogate:2,4,5,6-Tetrachloro-m-xylene 1.82 ug/L 2.00 91.0 20-130 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p 1 www.microbac.com Page 10 of 16 OMICROBAC ' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K1 A0090 Spike Source %REC RPD Pesticides TCLP by GC/ECD Result RL Units Level Result %REC Limits RPD Limit Notes Batch B1A0490-3510C 8081 -EPA 8081A Blank(B1A0490-BLK2) Prepared:01/12/2021 Analyzed:01/14/2021 Surrogate:Decachlorobiphenyl (BZ-209) 0.998 ug/L 2.00 49.9 25-140 LCS(B1A0490-BS1) Prepared:01/12/2021 Analyzed:01/14/2021 alpha-Chlordane 5.32 0.500 ug/L 5.00 106 40-120 Endrin 5.89 0.500 ug/L 5.00 118 40-138 gamma Chlordane 5.06 0.500 ug/L 5.00 101 40-136 gamma-BHC(Lindane) 5.86 0.500 ug/L 5.00 117 30-134 Heptachlor 5.74 0.500 ug/L 5.00 115 40-130 Heptachlor epoxide 5.26 0.500 ug/L 5.00 105 40-120 Methoxychlor 5.18 0.500 ug/L 5.00 104 40-150 Surrogate:2,4,5,6-Tetrachloro-m-xylene 1.96 ug/L 2.00 98.0 20-130 Surrogate:Decachlorobiphenyl (BZ-209) 1.70 ug/L 2.00 84.9 25-140 LCS(B1A0490-BS2) _ Prepared:01/12/2021 Analyzed:01/14/2021 Toxaphene 18.4 10.0 ug/L 20.0 92.0 41-126 Surrogate:2,4,5,6-Tetrachloro-m-xylene 1.88 ug/L 2.00 93.8 20-130 Surrogate-Decachlorobiphenyl (BZ-209) 1.80 ug/L 2.00 89.8 25-140 LCS Dup(B1A0490-BSD1) Prepared:01/12/2021 Analyzed:01/14/2021 alpha-Chlordane 5.57 0.500 ug/L 5.00 111 40-120 4.54 30 Endrin 6.09 0.500 ug/L 5.00 122 40-138 3.42 30 gamma Chlordane 5.28 0.500 ug/L 5.00 106 40-136 4.35 30 gamma-BHC(Lindane) 6.04 0.500 ug/L 5.00 121 30-134 3.08 30 Heptachlor 5.96 0.500 ug/L 5.00 119 40-130 3.69 30 Heptachlor epoxide 5.43 0.500 ug/L 5.00 109 40-120 3.11 30 Methoxychlor 5.35 0.500 ug/L 5.00 107 40-150 3.40 30 Surrogate:2,4,5,6-Tetrachloro-m-xylene 1.83 ug/L 2.00 91.4 20-130 Surrogate Decachlorobiphenyl (BZ-209) 1.54 ug/L 2.00 76.8 25-140 Spike Source %REC RPD Semivolatile Organic Result RL Units Level Result %REC Limits RPD Limit Notes Compounds TCLP by GCMS Batch B1A0492-3510C_8270-EPA 8270C Blank(B1A0492-BLK1) Prepared:01/12/2021 Analyzed:01/14/2021 1,4-Dichlorobenzene <50.0 50.0 ug/L 2,4-Dinitrotoluene <50.0 50.0 ug/L Hexachlorobenzene <50.0 50.0 ug/L Hexachlorobutadiene <50.0 50.0 ug/L Hexachloroethane <50.0 50.0 ug/L 2-Methylphenol <50.0 50.0 ug/L 3-,4-Methylphenol <50.0 50.0 ug/L Nitrobenzene <50.0 50.0 ug/L Pentachlorophenol <250 250 ug/L Pyridine <250 250 ug/L 2,4,6-Trichlorophenol <50.0 50,0 ug/L 2,4,5-Trichlorophenol <50.0 50.0 ug/L Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 11 of 16 OMIICROBAC ` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K1 A0090 Spike Source %REC RPD Semivolatile Organic Result RL Units Level Result %REC Limits RPD Limit Notes Compounds TCLP by GCMS Batch B1A0492-3510C 8270-EPA 8270C Blank(B1A0492-BLK1) Prepared:01/12/2021 Analyzed:01/14/2021 Surrogate:2-Fluorobiphenyl 324 ug/L 500 64.8 43-116 Surrogate:2-Fluorophenol 463 ug/L 1000 46.3 19-119 Surrogate:Nitrobenzene-d5 328 ug/L 500 65.7 35-114 Surrogate:Phenol-d5 304 ug/L 1000 30.4 10-120 Surrogate:p-Terphenyl-d14 475 ug/L 500 95.0 10-130 Surrogate:2,4,6-Tribromophenol 1040 ug/L 1000 104 22-142 Blank(B1A0492-BLK2) Prepared:01/12/2021 Analyzed:01/14/2021 1,4-Dichlorobenzene <50.0 50.0 ug/L 2,4-Dinitrotoluene <50.0 50.0 ug/L Hexachlorobenzene <50.0 50.0 ug/L Hexachlorobutadiene <50.0 50.0 ug/L Hexachloroethane <50.0 50.0 ug/L 2-Methylphenol <50.0 50.0 ug/L 3-,4-Methylphenol <50.0 50.0 ug/L Nitrobenzene <50.0 50.0 ug/L Pentachlorophenol <250 250 ug/L Pyridine <250 250 ug/L 2,4,6-Trichlorophenol <50.0 50.0 ug/L 2,4,5-Trichlorophenol <50.0 50.0 ug/L Surrogate:2-Fluorobiphenyl 349 ug/L 500 69.9 43-116 Surrogate:2-Fluorophenol 514 ug/L 1000 51.4 19-119 Surrogate:Nitrobenzene-d5 362 ug/L 500 72.4 35-114 Surrogate:Phenol-d5 317 ug/L 1000 31.7 10-120 Surrogate:p-Terphenyl-d14 478 ug/L 500 95.5 10-130 Surrogate:2,4,6-Tribromophenol 1030 ug/L 1000 103 22-142 LCS(B1A0492-BS1) Prepared:01/12/2021 Analyzed:01/14/2021 1,4-Dichlorobenzene 371 50.0 ug/L 500 74.2 29-112 2,4-Dinitrotoluene 532 50.0 ug/L 500 106 57-128 Hexachlorobenzene 463 50.0 ug/L 500 92.6 53-125 Hexachlorobutadiene 442 50.0 ug/L 500 88.4 22-124 Hexachloroethane 346 50.0 ug/L 500 69.2 21-115 2-Methylphenol 414 50.0 ug/L 500 82.7 30-120 3-,4-Methylphenol 372 50.0 ug/L 500 74.4 20-130 Nitrobenzene 439 50.0 ug/L 500 87.9 40-120 Pentachlorophenol 467 250 ug/L 500 93.4 35-138 Pyridine <250 250 ug/L 500 10-100 Q3 2,4,6-Trichlorophenol 465 50.0 ug/L 500 93.1 50-135 2,4,5-Trichlorophenol 472 50 0 ug/L 500 94.4 53-123 Surrogate:2-Fluorobiphenyl 390 ug/L 500 78.0 43-116 Surrogate:2-Fluorophenol 533 ug/L 1000 53.3 19-119 Surrogate:Nitrobenzene-d5 389 ug/L 500 77 7 35-114 Surrogate:Phenol-d5 345 ug/L 1000 34.5 10-120 Surrogate:p-Terphenyl-d14 432 ug/L 500 86.3 10-130 Surrogate:2,4,6-Tribromophenol 1100 ug/L 1000 110 22-142 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p 1 www.microbac.com Page 12 of 16 ( M CROBAC: Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KIA0090 Spike Source %REC RPD Semivolatile Organic Result RL Units Level Result %REC Limits RPD Limit Notes Compounds TCLP by GCMS Batch B1A0492-3510C 8270-EPA 8270C LCS Dup(B1A0492-BSD1)._............_..._.. Prepared_01/12/2021 Analyzed:01/14/2021............_._......._........_........_................._...._..._....__...._....._.._..._._ 1,4-Dichlorobenzene 376 50.0 ug/L 500 75.2 29-112 1.43 30 2,4-Dinitrotoluene 526 50.0 ug/L 500 105 57-128 1.18 30 Hexachlorobenzene 477 50.0 ug/L 500 95.3 53-125 2.87 30 Hexachlorobutadiene 447 50.0 ug/L 500 89.3 22-124 0.998 30 Hexachloroethane 349 50.0 ug/L 500 69.8 21-115 0.840 30 2-Methylphenol 428 50.0 ug/L 500 85.6 30-120 3.46 30 3-,4-Methylphenol 383 50.0 ug/L 500 76.5 20-130 2.87 30 Nitrobenzene 447 50.0 ug/L 500 89.4 40-120 1.68 30 Pentachlorophenol 476 250 ug/L 500 95.3 35-138 1.99 30 Pyridine <250 250 ug/L 500 41.1 10-100 78.1 30 R1 2,4,6-Trichlorophenol 466 50.0 ug/L 500 93.2 50-135 0.149 30 2,4,5-Trichlorophenol 472 50.0 ug/L 500 94.4 53-123 0.0420 30 Surrogate:2-Fluorobiphenyl 392 ug/L 500 78.5 43-116 Surrogate:2-Fluorophenol 547 ug/L 1000 54.7 19-119 Surrogate:Nitrobenzene-d5 401 ug/L 500 80.3 35-114 Surrogate:Phenol-d5 348 ug/L 1000 34.8 10-120 Surrogate:p-Terphenyl-d14 446 ug/L 500 89.3 10-130 Surrogate:2,4,6-Tribromophenol 1130 ug/L 1000 113 22-142 Definitions mg/L: Milligrams per Liter Q3: LCS recovery is below acceptance limits.The reported value is estimated. Q8: CCV recovery is below acceptance limits.The reported value is estimated. R1: Duplicate RPD is outside of acceptance limits. RL: Reporting Limit RPD: Relative Percent Difference S1: Surrogate recovery is above acceptance limits. S2: Surrogate recovery is below acceptance limits. uglL: Micrograms per Liter ug/mL: Micrograms per Milliliter Y: This analyte is not on the laboratory's current scope of accreditation. Cooler Receipt Log Cooler ID: Default Cooler Temp: 6.7°C Microbac Laboratories.Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 13 of 16 ( MICROBAC Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K1 A0090 Cooler Inspection Checklist Ice Present or not required? Yes Shipping containers sealed or not required? Yes Custody seals intact or not required? Yes Chain of Custody(COC)Present? Yes COC includes customer information? Yes Relinquished and received signature on COC? Yes Sample collector identified on COC? Yes Sample type identified on COC? Yes Correct type of Containers Received Yes Correct number of containers listed on COC? Yes Containers Intact? Yes COC includes requested analyses? Yes Enough sample volume for indicated tests received? Yes Sample labels match COC(Name,Date&Time?) Yes Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes VOA vials have zero headspace,or not recd.? Yes Project Requested Certification(s) Microbac Laboratories Inc.,-Marietta,OH 583 NC Dept.of the Environment and Natural Resources Microbac Laboratories,Inc.-Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to �),� applicable accreditation standard unless otherwise noted. �/\ The data and information on this,and other accompanying documents,represents only the sample(s)analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith present and an authorized signature is included.The services were provided under and Administration subject to Microbac's standard terms and conditions which can be located and Reported: 01/19/2021 16:30 reviewed at<https://www.microbac.com/standard-terms-conditions>. Microbac Laboratories,Inc. 2592 Hope Mills Rd I Fayetteville,NC 28306 1 910.864.1920 p 1 www.microbac.com Page 14 of 16 nnmoaGFayettovlre ie O✓^` 2592 Hope Nils Rd. CHAIN OF CUSTODY RECORDo `K1A0090' C''p Fayetteville,NC 26306 Number Ins+BE COSP.Ens on :D ,,7ip'y15 MIME f[,i(7i�■a��y}py Lab Report Address Invoice Address Turnaround Time TO BE COMPLETED 9Y MlCROBAC rillG NIjBtt(5itlj$((ri'f(II'yyI 1P Chem Name: Vc vDNAW Corp. Client Name: (i Routine(5 to 7 business days) Temperature Upon Receipt FC)`-7 []RUSH.(notify lab) Therm ID Address: 129 First Steel Address: Holding Time City,State,Zip: Cordova.NC 25330 City,State,Zip: (needed by) Samples Received on 1- tli'No NIA Contact: Chris Fowler Contact: Repon Type Custody Sealslnta Y No WA Telephone No.: 910-410-9131 Telephone No.: (]Results Only[(Level l []Level 2()Level ()level 4()EDD Send Report vim (I Mel (]Fax ()e+na:l(address) Send Invoke via: ()Mal ()Fax (1 a ttol address) Project Annual Loutkn: MANHOLE IN WOODS PO No.: Compliance()AgauaylWogramgrarn ring? I)Yes [)No Sampled by(PRINT): Wright Sampler Sampler Phone 910-759.mg1 Signature: No.. •Matrix Types SolSofd(SI Sludge,Oa W1pe Drinking Water(0W),Groundwater(OW)Surtax Water(SW).Waste Water(MN)Other(apeyd) Preservative Types (1)HM03.(2)H2SO4(3)HCI,(4)NaOH.(51 Zinc Acetate.(a)Methanol,(7)Sedum emulate(a)Sedum TNostMate WI Hexane)U)Unpreservsd REQUESTED ANALYSIS 1 A t uo ti Date Time o $ Preservativ a. Lab ID Client Sample ID Collected Collected 1 =S a .Types" P. Additional Notes c...1 EFFLUENT l/6[1 i jf:t° 2 KW C U Fled pH' Field Tem Possible Hazard Identification (I Hammon ()Nen-Harmdoue [I Radioactive Sample Disposition [1 Oopdso as appropriate (]Return ()Archive Comment. Relinquln B ( , Recei B-)sgn�ure) Date e I .` �l e/ , .,>, ,Purl ��-- CQ r`a i Li. '.S gWshed By spnalu ) Date/Time Received By(signature) Datemme Relinquished By(signature) Date/Time Received By(signature) Date/Time rev 12/252017 Page I or 2 • Sample Acceptance Policy for Environmental Chemistry and Microbiology RE r T: _ Chain of Custody A chain of custody MUST accompany all samples received at the laboratory The following information on the Chain of Custody must be complete client name and address,sample collectors name,sample description/identification,matrix,date and time of collection,number of containers,preservative and requested analysis Any missing receipt information will be documented in the final report.The laboratory will analyze those target analyses identified by the client on a project-specific basis.If project-specific information is not available,then the laboratory's default reference methods and target list of analyses will be used Page 15 of 16 Sample Containers Nicrn0ac-Fayeeeetle M I C R o B A C 2592 Hope Nulls Rd. CHAIN OF CUSTODY RECORD "K 1 A0090" Fayetteville,NC 283e6 Number Msatxlbns on back MU NI{'rp''W! �j� p Lab Report Address Imeice Address Turnaround Tuns TO BECO.twLETEO BYMICROBAC hi-PIl pggt ... .+' Client Name: VonoreNe Corp. Client Name: 1)Routine(5 to 7 business days) Temperature Upon Receipt('C)`.7 "'LLLtt11111111 ff6b HHH::: Ar7 ()RUSH'(notify lab) Therm ID / Address: 126 First Street Address: Holding Time City,State,Zip: Cordova,NC 219330 City,State,Zip: (needed by) Samples Received on I els No NIA Contact: Chris Fowler Contact: Report Type Custody Seals Intact( No WA Telephone No.: 910-410-9131 Telephone No.: ()Results Only()level 1 ((Level 2()Levela ()Level 4 nEDD Send Report via: (j Mail ((Fax ()e-mail(adyresa) Send Invoice via ()Mail ()Fax (I e-mail(address) Project: Annual Location: MANHOLE IN WOODS PO No.: Compliance Monitoring? [I Yes (I No ()Agoncyrpregram Sampled by(PRINT): Wright Sampler Sampler Phone 910.75943291 Signature: No.: 'Meta Types Su05did(5).Se+092.00 Hope DnNdng Water(OW),Grp:ntater(GW)Sufaco Water(SW).Waste Water(WW).Mr(spay) 'FreservafNe Types(1)HNO3(2)i.OSO4(3)HO(4)NaOH.(5)Zre Acela'.e.(6)Methanol(7)soctum El su."a:e.(B)Salem 1 hiosufete(s:.Hexane(U)Unpreserveo REQUESTED ANALYSIS e t) t) Date Tne 5 Preserwtiv g Lab ID Client Sample ID Collected Collected i 3 t e Types'• Addrfional MOMSCA EFFLUENT 1/6/7 i II:t`f 2 MAV C U Field pH Fia:d Temp Possible Hazard Identification (I He:arde.% (1 Non-Hazardous (I Radioactive Sample Disposition (I Dapose as appropriate (I Reuan I Amine Comments r )Relinqu ( Dot me Recer '"tnatur Dot ,e j 6/2/ ,1-,t- e t1,i di ►Lt 15 . elinquished By signata j DateRime Received By(signature) Datelime Relinquished By(signature) Datemme Received By(signature) Date/Time rev 12E6/2017 Page 1 of 2 Sample Acceptance Policy for Environmental Chemistry and Microbiology REV i= Chain of Custody A chain of custody MUST accompany all samples received at the laboratory.The fol owing information on the Chain of Custody must be complete:client name and address,sample co:lectoi's name,sample description/identification,matrix,date and time of collection,number of containers,preservative and requested analysis. My missing receipt information will be documented in the final report The laboratory will analyze those target analyses identified by the client on a project-specific basis.If project-specific Information is not available,then the laooratory's default reference methods and target list of analyses will be used Page 16 of 16 Sample Containers PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION The current permit, WQ0039924, does not have vector attraction requirements but does have Class A requirements for pathogens. These forms are marked to reflect these requirements. PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 1/1/2021 To 1/31/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: ' Alt A(time/temp) ❑ Alt B(Alk Treatment) 0 Alt C(Prior Testing) 0 = AltD(No Prior Test) 0 I Process to Further Reduce Pathogens ❑ =. :- If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens": Compost Cl Heat Drying 0 Heat Treatment❑ Thermophilic❑ Beta Ray ❑ Gamma Ray 0 Pasteurization 0 Class B: )Alt. (I)Fecal Density ❑ I Alt (2)Process to Significantly Reduce Pathogens ❑ - , If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization 0 1 Air Drying 0 I Composting 0 Aerobic Digestion 0 Anaerobic Digestion 0 If applicable to alternative performed(Class A or Class B)complete the following monitoring data: Parameter Allowable Level Pathogen Density Nunioerot Frequency Sample 'al3't"a' Tech- in Sludge Minimum Geo.Mean Maximum Units d n c of Analysis Type n ne e 2x10tothe MPN 6th power per gram of Fecal Coliform total solids CRT 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid(dry <0.6 NA <0.6 MPN/4 0 Monthly Grab EPA c� oliforml _ weight) Grams 1682 Vector Attraction Reduction(15A NCAC 02T.1107)-Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt.2(40-day bench) ❑ Alt.3(30-day bench) ❑ Alt.4(Spec.O,uptake) 0 Alt. 5(14-Day Aerobic) ❑ Alt.6(Alk.Stabilizatiox Alt 7(Drying-Stable) 0 Alt.8(Drying-Unstable) 0 Alt.9(Injection) ❑ Alt. 10(Incorporation) 0 No vector attraction reduction alternatives were performed El CERTIFICATION STATEMENT(please check the appropriate statement) El "I certify, under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr.Chris Fowler,Facility Manager Mr.Chris Fowler,Land Application ORC Prep N and Title(type or print) Land App " Name and Title if applicable)(type or print) .,..2e Signature of Preparer* Date Sign e of Land Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) DFNR FORM PVRF 02T(12I20061 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 2/1/2021 To 2/28/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: Alt.A(time/temp) ❑ I Alt B(Alk Treatment) 0 ( Alt. C(Prior Testing) 0 AIt.D(No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed(CIass A only)indicate"Process to Further Reduce Pathogens": Compost ❑ Heat Drying❑ Heat Treatment❑ Thennophilic❑ Beta Ray 0 Gamma Ray 0 Pasteurization 0 , _ Class B: Alt. (1)Fecal Density ❑ I Alt. (2)Process to Significantly Reduce Pathogens 0 I; If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization 0 Air Drying 0 Composting 0 Aerobic Digestion❑ Anaerobic Digestion ❑ .......:......:. If applicable to alternative performed(Class A or Class B)complete the following monitoring data: Anaircar Allowable Level Pathogen Density Number or Frequency Sample Parameter in Sludge Minimum Geo.Mean Maximum Units lrxcee of Analysis TypeTech- Arnces nintle 2 x 10 to the MPN bth power per gram of Fecal Coliform total solids CFCT • 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid(dry <0.6 NA 0.8 MPN/4 0 Monthly Grab EPA colifonn) weiifhh Grains 1682 Vector Attraction Reduction(15A NCAC 02T.1107)-Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt.2(40-day bench) 0 Alt.3(30-day bench) ❑ Alt.4(Spec.02 uptake) ❑ Alt.5(14-Day Aerobic) 0 Alt.6(Alk.Stabilization❑ Alt 7(Drying-Stable) ❑ Alt. 8(Drying-Unstable) 0 Alt.9(Injection) 0 Alt. 10(Incorporation) 0 No vector attraction reduction alternatives were performed 17 CERTIFICATION STATEMENT(please check the appropriate statement) ❑ "I certify, under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler,Facility Manager Mr.Chris Fowler,Land Application ORC Preparer N d Title(type or print) Land Applier ► :i..- . , . le(if licable)(type or print) 2,3 Zti Z-4TZN Signature of Preparer* Date Sign. ' e of Land Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) DENR FORM PVRF 02T 112/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 3/1/2021 To 3/31/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: Alt.A(time/temp) 0 Alt B(Alk Treatment) ❑ Alt C(Prior Testing) t] AItD(No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat TreatmentO Thermo tic❑ Beta Ray ❑- Gamma Ray 0 Pasteurization CI Class B: Alt. (1)Fecal Density 0 Alt (2)Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed(Class B only)indicate`Process to Significantly Reduce Pathogens": Lime Stabilization ❑ I Air Drying 0 I Composting 0 'Aerobic Digestion❑ Anaerobic Digestion 0 If applicable to alternative performed(Class A or Class B)complete the followin monitoring data: Parameter Allowable Level Pathogen Density Number of Frequency Sample Analytical Tech- in Sludge Minimum Geo.Mean Maximum Unitsee- of Analysis Type n e P 2x10tothe MIN 6th power per gram of Fecal Coliform total solids CF[J 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid(dry <0.6 NA 1.6 MPN/4 0 Monthly Grab EPA coliform) weight) Grams 1682 Vector Attraction Reduction(15A NCAC 02T.1107)-Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt.2(40-day bench) 0 Alt.3(30-day bench) ❑ Alt.4(Spec.02 uptake) ❑ Alt.5(14-Day Aerobic) 0 Alt.6(Alk.Stabilization❑ Alt 7(Drying-Stable) ❑ ,Alt.8(Drying-Unstable) ❑ Alt.9(Injection) ❑ Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed 0 CERTIFICATION STATEMENT(please check the appropriate statement) ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify, under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler,Facility Manager Mr. Chris Fowler,Land Application ORC Preparer d Tit a(type or print) Land a and Title(if applicable)(type or print) Signature of Preparer* Date Si e of Land Applier(if applicable) Date *Preparer is defined in 40 CiR Part 503.9(r)and 15A NCAC 2T.1102(26) DENR FORM PVRF 02T(12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von Drehle Corporation. WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 4/1/2021 To 4/30/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: Alt A(time/temp) 0 1 Alt B(Alk Treatment) 0 Alt. C(Prior Testing) l l . . .. ......:.. . Alt.D(No Prior Test) ❑ Process to Further Reduce Pathogens ❑ ... . . If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens": • Compost ❑ Heat Drying❑ Heat Treatment❑ Thermophilic❑ Beta Ray ❑ Gamma Ray 0 Pasteurization ❑ ..... . Class B: Alt. (1)Fecal Density 0 I Alt. (2)Process to Significantly Reduce Pathogens ❑ .. . If applicable to alternative performed(Class B only)indicate'Process to Significantly Reduce Pathogens": Lime Stabilization 0 Air Drying ❑ Composting 0 'Aerobic Digestion 0 Anaerobic Digestion 0 1 If applicable to alternative performed(Class A or Class B)complete the following monitoring data: Parameter Allowable Level Pathogen Density Number or Frequenccee- y Sample `''nal�'� Tech- in Sludge Minimum Geo.Mean Maxi Units denc q of Analysis Type nin e 2x10tothe MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid(thy <0.7 NA <0.6 MPN/4 0 Monthly Grab EPA coliform) weight) Grams 1682 Vector Attraction Reduction(15A NCAC 02T.1107)-Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt.2(40-day bench) ❑ Alt.3(30-day bench) ❑ Alt.4(Spec.02 uptake) ❑ Alt.5(14-Day Aerobic) ❑ Alt. 6(Allc.Stabilization❑ Alt 7(Drying-Stable) 0 Alt.8(Drying-Unstable) 0 Alt.9(Injection) 0 Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed O CERTIFICATION STATEMENT(please check the appropriate statement) ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify, under penalty of law,that the pathogen requirements in 1SA NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr.Chris Fowler,Land Application ORC Pre er and Title(type or print) Land Ap " ame and Title(if applicable)(type or print) • Z-� .2______ v LZ i i� 72,,------5 ..___ 24-2te Signature of Preparer* Date Signf Land Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) DENR FORM PVRF 02T(12/20061 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 5/1/2021 To 5/31/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: Alt A(time/temp) ❑ I Alt B(Alk Treatment) ❑ Alt C(Prior Testing) El AltD(No Prior Test) ❑ f Process to Further Reduce Pathogens 0 If applicable to alternative performed(Class A only)indicate"Process to Farther Reduce Pathogens": Compost 0 Heat Drying 0 Heat Treatment❑ Thermoplulic❑ Beta Ray ❑ Gamma Ray❑ Pasteurization 0 .. . . Class B: Alt. (l)Fecal Density 0 Alt(2)Process to Significantly Reduce Pathogens ❑ �: ;:::::::::.� If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ 'Aerobic Digestion 0 Anaerobic Digestion 0 I If applicable to alternative performed(Class A or Class B)complete the following monitoring data: Allowable Level Patho DensityNumber of Analytical en Parameter g Frequency Sample Tech- in Sludge Minimum Geo.Mean'Maximum Units apn,a, of Analysis Type n a e 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CPU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams MPN/4 EPA (in lieu of fecal total solid(dry <0.8 NA <0•8 Grams 0 Monthly Grab 1682 coliform) weight) Vector Attraction Reduction(15A NCAC 02T.1107)-Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt.2(40-day bench) ❑ Alt.3(30-day bench) ❑ Alt.4(Spec.Oz uptake) ❑ Alt.5(14-Day Aerobic) 0 Alt.6(Alk.Stabilization❑ Alt 7(Drying-Stable) ❑ Alt. 8(Drying-Unstable) 0 Alt.9(Injection) 0 Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed El CERTIFICATION STATEMENT(please check the appropriate statement) ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler,Facility Manager Mr.Chris Fowler,Land Application ORC Prep N e and Title(type or print) Land Appli and (if applicable)(type or print) 2. ya attire of Preparer* Date Sign of Land Applier(if applicable) Date !Preparer is defined in 40 Cult Part 503.9(r)and 15A NCAC 2T.1102(26) DENR FORM PVRF 02T/12/20061 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number:. NA Monitoring Period: From 6/1/2021 To 6/30/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: Alt.A(time/temp) ❑ I Alt B(Alk Treatment) 0 I Alt C(Prior Testing) El `` _..,. Alt.D(No Prior Test) 0 I Process to Further Reduce Pathogens Cl If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens": Compost 0 Heat Drying 0 Heat Treatment❑ Thermophilic❑ Beta Ray 0 Gamma Raz 0 Pasteurization 0 . . ........ Class B: Alt. (1)Fecal Density 0 Alt. (2)Process to Significantly Reduce Pathogens ❑ . .:::::: If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization 0 Air Drying 0 Composting 0 Aerobic Digestion❑ Anaerobic Digestion 0 .. If applicable to alternative performed(CIass A or Class B)complete the followin_ monitoring data: Number o Analytical Allowable Level Pathogen Density Frequency le Sam Parameter Excee- ` Sample Sludge Minimum Geo. Mean Maximum Units dences of Analysis Type 1110llP. 2x10tothe MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams MPN/4 EPA (in lieu of fecal total solid(dry <0.6 NA <0.8 Grams 0 Monthly Grab coliform) weight) 1682 Vector Attraction Reduction(15A NCAC 02T.1107)-Please indicate alternative performed: Alt 1 (VS reduction) ❑ Alt.2(40-day bench) ❑ Alt.3(30-day bench) 0 Alt.4(Spec.02 uptake) 0 Alt 5(14-Day Aerobic) ❑ Alt.6(Alk.Stabilization❑ Alt 7(Drying-Stable) 0 Alt.8 (Drying-Unstable) 0 Alt.9(Injection) 0 Alt. 10(Incorporation) 0 No vector attraction reduction alternatives were performed 0 CERTIFICATION STATEMENT(please check the appropriate statement) ❑ "I certify, under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Mr. Chris Fowler,Facility Manager Mr. Chris Fowler,Land Application ORC Prep e and Title(type or print) Land Ap 'P Name and Title(if applicable)(type or print) - (,......9._.40_____ 2-924 2- -21• Signature of Preparers` Date Si e of Lan pplier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) DENR FORM PVRF 02T(12/20061 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number:_ NA Monitoring Period: From 7/1/2021 To 7/31/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: Alt.A(tune/temp) ❑ J AIt B(Alk Treatment) ❑ I Alt C(Prior Testing) El AIt.D(No Prior Test) 0 I Process to Further Reduce Pathogens ❑ .. . If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens": Compost ❑ Heat Drying❑ Heat Treatment❑ Thermophilic❑ r. Beta Ray ❑ Gamma Ray❑ Pasteurization ❑ • . . . ._ . Class B: Alt. (1)Fecal Density 0 I Alt (2)Process to Significantly Reduce Pathogens 0 If applicable to alternative performed(CIass B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization 0 Air Drying ❑ Composting 0 'Aerobic Digestion❑ Anaerobic Digestion ❑ If applicable to alternative performed(Class A or Class B)complete the followin: monitoring data: Parameter Allowable Level Pathogen Density Number or Frequency Sample Analytical . Units Excee- Tech- in SIudge Minimum Geo. Mean Maximum dames of Analysis Type niauP 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams MPN/4 (in lieu of fecal total solid(dry <0.6 NA <0.6 0 Monthly Grab EPA coliform) weight) Grams 1682 Vector Attraction Reduction(15A NCAC 02T.1107)-Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt.2(40-day bench) 0 Alt.3(30-day bench) 0 Alt.4(Spec.02 uptake) 0 Alt.5(I4-Day Aerobic) ❑ Alt.6(Alk.Stabilization0 Alt 7(Drying-Stable) ❑ Alt. 8(Drying-Unstable) 0 Alt 9(Injection) ❑ Alt.10(Incorporation) ❑ No vector attraction reduction alternatives were performed El CERTIFICATION STATEMENT(please check the appropriate statement) ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." CI "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr.Chris Fowler,Facility Manager Mr. Chris Fowler,Land Application ORC Prepay e and Title e or print) Land Ap ' ame and Title(if applicable)(type or print) • Z-cG.`21 _— Z-&-ZL Signature of Preparer* Date Si of Land Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) DFNR FORM PVRF 09T 119/9nosl ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von Dreble Corporation WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 8/1/2021 To 8/31/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: Alt.A(time/temp) 0 I Alt B(Alk Treatment) ❑ Alt. C(Prior Testing) El AIt.D(No Prior Test) ❑ I Process to Further Reduce Pathogens If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens": Compost 0 Heat Drying 0 Heat Treatment❑ Thermophilic❑ Beta Rav 0 Gamma Ray 0 Pasteurization 0 Class B: Alt. (1)Fecal Density 0 Alt. (2)Process to Significantly Reduce Pathogens 0 If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization 0 Air Drying 0 Composting ❑ 'Aerobic Digestion❑ Anaerobic Digestion CI _ . If applicable to alternative performed(Class A or Class B)complete the following monitoring data: Parameter Allowable Level Pathogen Density Number of Frequency Sample `Iyu cal Tech- in Sludge Minimum Geo.Mean Maximum Units genres of Analysis Type moue 2x10tothe ,N . 6th power per gram of Fecal Coliform total solids CPU 1000 mpn per gram of total solid (dry weight) • Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid(dry <0.6 NA 0.7 MPN/4 0 Monthly Grab EPA coliform) weight) Grams 1682 Vector Attraction Reduction(15A NCAC 02T.1107)-Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt.2(40-day bench) ❑ Alt.3(30-day bench) ❑ Alt.4(Spec.02 uptake) 0 Alt.5(14-Day Aerobic) 0 Alt.6(Alk.Stabilization❑ Alt 7(Drying-Stable) ❑ Alt.8(Drying-Unstable) 0 Alt.9(Injection) ❑ Alt. 10(Incorporation) 0 No vector attraction reduction alternatives were performed El CERTIFICATION STATEMENT(please check the appropriate statement) ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr.Chris Fowler,Facility Manager Mr.Chris Fowler,Land Application ORC Pr N and Title(type or print) Land Ap a and Title(if applicable)(type or print) 2•{i:L Z ature of Pr er* Date Sign d Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) fFNR FORM PVRF(19T[i9/9MR1 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 9/1/2021 To 9/30/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: Alt.A(time/temp) 0 Alt B(Alk Treatment) 0 Alt. C(Prior Testing) El : ....... Alt.D(No Prior Test) ❑ Process to Further Reduce Pathogens ❑ ..... , If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens": Compost 0 Heat Drying❑ Heat Treatment❑ Thermophilic❑ Beta Ray 0 Gamma Ray❑ Pasteurization 0 . Class B: Alt. (1)Fecal Density 0 Alt. (2)Process to Significantly Reduce Pathogens ❑ 1: : If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization ❑ J Air Drying ❑ Composting 0 Aerobic Digestion 0 Anaerobic Digestion 0 • . __ _ If applicable to alternative performed(Class A or Class B)complete the following monitoring data: Parameter Allowable Level Pathogen Density Number o Frequency Sample Analytical Excee- in Sludge Minimum Geo.Mean Maximum Units den,„ of Analysis Type Tech- IIlOrle 2x10tothe MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram - of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams MPN/4 EPA (in lieu of fecal total solid(dry <0.6 NA <0.8 0 Monthly Grab coliform) weight) Grams 1682 Vector Attraction Reduction(15A NCAC 02T.1107)-Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt.2(40-day bench) 0 Alt.3(30-day bench) ❑ Alt.4(Spec.02 uptake) ❑ Alt.5(14-Day Aerobic) ❑ Alt.6(Alk.Stabilization❑ Alt 7(Drying-Stable) 0 Alt.8(Drying-Unstable) 0 Alt.9(Injection) 0 Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed 0 CERTIFICATION STATEMENT(please check the appropriate statement) ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction redaction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify, under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr.Chris Fowler,Facility Manager Mr. Chris Fowler,Land Application ORC Prep a and Title type or print) Land A e and T' e(if applicable)(type or print) Z. 0 L 2�2� Signature of Prepar Date Signature of Land A ter(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) 11FNR FORM PVRF f17T f 17/7nflR1 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 10/1/2021 To 10/31/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: All A(time/temp) ❑ I Alt B(Alk Treatment) ❑ Alt. C(Prior Testing) El AItD(No Prior Test) 0 Process to Further Reduce Pathogens 0 If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens": Compost 0 Heat Drying❑ Heat Treatment❑ Thermophilic❑ Beta Ray__ _ ❑ Gamma Ray❑ Pasteurization❑.. . Class B: Alt. (1)Fecal Density ❑ Alt. (2)Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed(Class B only)indicate'Process to Significantly Reduce Pathogens": Lime Stabilization 0 Air Drying 0 Composting 0 Aerobic Digestion❑ _ Anaerobic Digestion 0 • If applicable to alternative performed(Class A or Class B)complete the following monitoring data: Allowable Level Pathogen Density Number otFrequency Sample Anatyncai Parameter Excee- Tech- in Sludge Minimum Geo.Mean Maximum Units den of Analysis Type ninue 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CPU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams MPNPA (in lieu of fecal total solid(dry <0.6 NA 0.7 /S 0 Monthly Grab coliform) weight) Vector Attraction Reduction(15A NCAC 02T.1107)-Please indicate alternative performed: Alt.1(VS reduction) ❑ Alt.2(40-day bench) 0 Alt.3(30-day bench) ❑ Alt.4(Spec.02 uptake) 0 Alt. 5(I4-Day Aerobic) 0 Alt.6(Alk. Stabilization❑ Alt 7(Drying-Stable) 0 Alt.8(Drying-Unstable) 0 Alt. 9(Injection) 0 Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed El CERTIFICATION STATEMENT(please check the appropriate statement) "I certify, under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the 0 vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler,Facility Manager Mr.Chris Fowler,Land Application ORC Prepare d Ti type or print) Land App ': ..s a and Ti a(if applicable)(type or print) -2_3-zz Signature of Preparer* Date Signa - • Land Applier(if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) DENR FORM PVRF 02T(12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von.Drehle Corporation WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 11/1/2021 To 11/30/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: Alt A(time/temp) ❑ I Alt B(Alk Treatment) ❑ I Alt C(Prior Testing) El Alt D(Na Prior Test) 0 Process to Further Reduce Pathogens ❑ If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens": Compost 0 Heat Drying 0 I Heat Treatment❑ Thermophilic❑ Beta Ray ❑- Gamma Ray 0 _ Pasteurization❑ Class B: lAlt. (1)Fecal Density ❑J Alt.(2)Process to Significantly Reduce Pathogens 0 If applicable to alternative performed(C7ass B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization 0 I Air Drying 0 Composting ❑ 'Aerobic Digestion❑ Anaerobic Digestion 0 If applicable to alternative performed(Class A or Class B)complete the following monitoring data: Parameter Allowable Level Pathogen Density Number of Excee- Frequency Sample Analytical Tech- in Sludge Minimum Geo.Mean Maximum Units den r of Analysis Type n o e 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid(dry <0.6 NA 0.7 MPN/4 0 Monthly Grab EPA coliform) weight) Grams 1682 Vector Attraction Reduction(1SA NCAC O*2T.1107)-Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt.2(40-day bench) ❑ Alt.3(30-day bench) ❑ Alt.4(Spec.02 uptake) ❑ Alt.5(14-Day Aerobic) ❑ Alt.6(Alk.Stabilization❑ Alt 7(Drying-Stable) ❑ Alt.8 (Drying-Unstable) ❑ Alt 9(Injection) 0 Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed 0 CERTIFICATION STATEMENT(please check the appropriate statement) ❑ "I certify, under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr.Chris Fowler,Facility Manager Mr.Chris Fowler,Land Application ORC Prep e d Titl r print) Land App ' ame and Title if applicable)(type or print) Z L2 Signature of Preparer* Date Sign o Land Appl (if applicable) Date *Preparer is defined in.40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) r1FNPFC]RM PVRFrorti7/7nosx ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0039924 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 12/1/2021 To 12/31/2021 Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: Class A: Alt.A(time/temp) ❑ I Alt B(Alk Treatment) 0 I Alt. C(Prior Testing) 17 :: :=:: : :: Alt D(No Prior Test) 0 Process to Further Reduce Pathogens 0 . If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens": Compost 0 Heat Drying 0 Heat Treatment❑ Thermophilic❑ Beta Ray 0 Gamma Ray❑ Pasteurization❑ ' • Class B: Alt. (1)Fecal Density 0 Alt. (2)Process to Significantly Reduce Pathogens 0 ,.._..is If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens": Lime Stabilization 0 Air Drying ❑ Composting 0 Aerobic Digestion 0 Anaerobic Digestion 0 If applicable to alternative performed(Class A or Class B)complete the following monitoring data: Parameter Allowable Level Pathogen Density Number of Frequency Sample Analytical in Sludge Minimum Geo.Mean Maximum Units rienne 1 C of Analysis Type Tech- 2 x 10 to the MPN gigue 6th power per gram of Fecal Coliform total solids CPU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grains MPN/4 EPA (in lieu of fecal total solid(dry <0.6 NA <0.7 Grams 0 Monthly Grab 1682 coliform) , weight) Vector Attraction Reduction(15A NCAC 02T.1107)-PIease indicate alternative performed: Alt.1 (VS reduction) ❑ Alt.2(40-day bench) 0 Alt.3(30-day bench) ❑ Alt.4(Spec.02 uptake) ❑ Alt.5(14-Day Aerobic) ❑ Alt. 6(Alk.Stabilization❑ Alt 7(Drying-Stable) 0 Alt.8(Drying-Unstable) 0 Alt. 9(Injection) ❑ Alt. 10(Incorporation) 0 No vector attraction reduction alternatives were performed C] CERTIFICATION STATEMENT(please cheek the appropriate statement) ❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify, under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler,Facility Manager Mr.Chris Fowler,Land Application ORC Pr N d Title{type or print) Land A - r e and Title(if applicable)(type or print) 7( hire of Preparer* Date Si of Land Appli(if applicable) Date *Preparer is defined in 40 CFIt Part 503.9(r)and 15A NCAC 2T.1102(26) !Inn FC)RM PVRF n9T M 2r2nn 1 PATHOGEN AND VECTOR ATTRACTION REDUCTION DOCUMENTATION PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION DOCUMENTATION The current permit, WQ0039924, does not have vector attraction requirements but does have Class A requirements for pathogens. Documentation is attached to reflect these requirements. Von ❑rehle Corporation Cordova,NC City of Rockingham IUP 0015 Jan-21 Biological Consulting Services lC at a c nal i=e 'rim. . ...atu...Salmonell ....Secoadar. ...a1Qe.$al0974.g a.. e a':. i1' '1!T. .. '.tl.. MIPN :eir4. �r. ............ . .......... ...................................... 2101210 1/14/21 < 0.07 <0.6 2101211 1/14/21 < 0.07 <0.6 2101212 1/14/21 < 0.07 < 0.6 2101213 1/14/21 < 0.07 < 0.6 2101214 1/14/21 < 0.07 <0.6 2101215 1/14/21 < 0.07 <0.6 2101216 1/14/21 < 0.07 <0.6 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. 0 BIOLOGICAL CONSULTING SERVICES j Inc. ...� OF NORTH FLORIDA, INC. J4,id4 l ZOZl January 19, 2021 I Robert Branch Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD-1,VD-2,VD-3,VD-4,VD-5,VD-6,VD-7 BCS ID: 2101210, 2101211, 2101212, 2101213, 2101214, 2101215, 2101216 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4(IS017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, -,;--2 . lit PQ„ Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2101210,2101211,2101212,2101213,2101214,2101215,2101216 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, IS017025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES jA4AB Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-1 Sample Date/Time:January 13, 2021 13:52 BCS Sample ID: 2101210 Sample Description: Biosolid Date Received: January 14, 2021 10:00 Amount Submitted:100 mL bottle %Solids: 42.4 Amount Analyzed: 30.10 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: January 14, 2021 11:23 Analysis Stop Date: January 19, 2021 11:00 Analyst: Wei-yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-2 Sample Date/Time:January 13, 2021 13:54 BCS Sample ID: 2101211 Sample Description: Biosolid Date Received: January 14, 2021 10:00 Amount Submitted:100 mL bottle %Solids: 42.0 Amount Analyzed: 30.08 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: January 14, 2021 11:23 Analysis Stop Date: January 19, 2021 11:00 Analyst: Wei-yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2101210,2101211,2101212,2101213,2101214,2101215,2101216 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES f la reifib (2T - Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-3 Sample Date/Time:January 13, 2021 13:56 BCS Sample ID: 2101212 Sample Description: Biosolid Date Received: January 14, 2021 10:00 Amount Submitted:100 mL bottle %Solids: 41.9 Amount Analyzed: 30.09 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: January 14, 2021 11:23 Analysis Stop Date: January 19, 2021 11:00 Analyst: Wei-yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-4 Sample Date/Time:January 13, 2021 13:58 BCS Sample ID: 2101213 Sample Description: Biosolid Date Received: January 14, 2021 10:00 Amount Submitted:100 mL bottle %Solids: 41.4 Amount Analyzed: 30.07 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: January 14, 2021 11:23 Analysis Stop Date: January 19, 2021 11:00 Analyst: Wei-yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report 13C5 ID 2101210,2101211,2101212,2101213,2101214,2101215,2101216 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-5 Sample Date/Time:January 13, 2021 14:00 BCS Sample ID: 2101214 Sample Description: Biosolid Date Received: January 14, 2021 10:00 Amount Submitted:100 mL bottle %Solids: 42.4 Amount Analyzed: 29.94 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: January 14, 2021 11:57 Analysis Stop Date: January 19, 2021 11:00 Analyst: Wei-yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-6 Sample Date/Time:January 13, 2021 14:02 BCS Sample ID: 2101215 Sample Description: Biosolid Date Received: January 14, 2021 10:00 Amount Submitted:100 mL bottle %Solids: 40.3 Amount Analyzed: 30.10 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: January 14, 2021 11:57 Analysis Stop Date: January 19, 2021 11:00 Analyst: Wei-yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2101210,2101211,2101212,2101213,2101214,2101215,2101216 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A,GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ~'�12t.G aAa -, ^.r i 1� A C Gnr rr.:r.n f'. Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-7 Sample Date/Time:January 13, 2021 14:04 BCS Sample ID: 2101216 Sample Description: Biosolid Date Received: January 14, 2021 10:00 Amount Submitted:100 mL bottle %Solids: 40.6 Amount Analyzed: 30.10 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: January 14, 2021 11:57 Analysis Stop Date: January 19, 2021 11:00 Analyst: Wei-yea Hsu, M.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2101210,2101211,2101212,2101213,2101214,2101215,2101216 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES lr.i 404 Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page6of8 Final Report BCS ID 2101210,2101211,2101212,2101213,2101214,2101215,2101216 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX.(352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative)and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety,and/or purity of any sample, batch,source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program,as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: January 19, 2021 Page 7 of 8 Final Report BCS ID 2101210,2101211,2101212,2101213,2101214,2101215,2101216 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422, PADEP: 68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AAIB DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence for the presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. • Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2101210,2101211,2101212,2101213,2101214,2101215,2101216 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES CHAIN OF CUSTODY RECORD BCS Laboratories www.microbioservices.com 4609 NW 6th street, Building A Ir'c. FL DOH Laboratory#E82924,EPA#FL01147 Gainesville, FL 32609 � n 1/ F� Tel.(352)377-9272,Fax.(352)377-5630 Client Name and Address: s1 ,3,d.-4'1 `. %L , 73s/�Bc4'HJIC)..-..5i lb_-ZQl Compliance Monitoring? FYesn No City/State/Zip:RoC.k 1-I fi i.fc 24 7-j2 Project ID: Z0I41-/1; Project Manager., I gjZ,4 mot^ Facility/Site: Oy,a�2 QeQ4 e_04dolsl Telephone Number. 3Yb Z•cia)./ Fax No.: Report To:Bab gut-wt.- Sampler Name:(Print) y ,2 L Email: !j//24upLei2401-4$.Cr Sampler Signature:e Invoice To:i-,]x.e Matrix Analysis N 2 m r V a a m 1/ 2 m om'- ? '.$ m u a v m a t i d o .P c th 10 1 X re c o m W iv E X W W U 4• c u =° a u a a it V O P O- a 9). 00 m o m a u .� is -g .Z^ m 'v E m a E m O 0 g m o i- E E oc v 8 = 4 c E r`3� p m _a d� ° 10 .S S m co 8 1Q1 2 .n ._ F in 1 8 a LL O P -- ti N m y C 9 g 3 N g t C O O m m U p E (p 1 • I-- p u m E Q u s V B G U '- U c c 5 m a o i E 9-m m E d t m 5 $ `m ry n T� E E o $ = 'or ci m m . a r y Sample ID/Description Z .. , o in 3 0 in o i-- U u i in - W a J J w` a > w z o 'z I - I 1 tirj).) //di2( Li i 'r Branch Residuals and Sails '( Branch Residuals and Soils \..%D Z t KO j Y Vo-1 012 5 2101210 Z101213 o . y ,./D.3""f� d.56 \ _I' ' 01/14/2021 10:00 \ A. 01114/2021 10:00 0 oo •./{t y 15$ r Branch Residuals and Soils S. Branch Residuals and Soils 2 t, '' And �/D"� Z,� VD-2 .Q V m p o 2101211 \ 210121214 N 7 �' L y 0' . L 7 4 1 ' 01/14/2021 10:00 Z. 01/1412021 10:00 re - c o U IA Z>k t r Branch Residuals and Soils k. Branch Residuals and Soils ' m VD3 VD-fi m` 2101212 2101215 01/1412021 10:00 01/14/2021 10:00 Special Instructions: Laboratory Comments: o :, r- Method of Shipment: "'"- 'C UP Postal FEDEX Other. Temp.@ recp't: '�G � �- Reli ish by: Die Time Received by: Date Time IR-I U. Corrected for IR E ,3 ( q•St? Custody Seal: Intact Broken CNIA dfliJ L G Presence of visable ice Y `" E32elinquished by: e Time Received by BCS Laboratories: Date lime Presence of ice packs N 4 'Hold Time �/ Von Drehle Corporation Cordova,NC City of Rockingham IUP 0015 Feb-21 Biological Consulting Services ... liumpuiraLab# Date Analyzed muPrimary l Value Salmonella ii00044#*Iy000,:i$000004#11 m*uranium mimimiumiumiumiumimimi .........................,.................................................................................... ................................................................per 4............grams...................... ............ 2102322 2/25/21 0.07 0.7 2102323 2/25/21 0.07 0.8 2102324 2/25/21 <0.07 <0.7 2102325 2/25/21 <0.07 <0.7 2102326 2/25/21 0.07 0.8 2102327 2/25/21 <0.07 <0.6 2102328 2/25/21 <0.07 <0.7 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. -� BIOLOGICAL CONSULTING SERVICES s Inc. �� OF NORTH FLORIDA, INC. rA gl e Z ZI March 04, 2021 / Robert Branch Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1,VD2,VD3,VD4,VD5,VD6,VD7 BCS ID: 2102322, 2102323, 2102324, 2102325, 2102326, 2102327, 2102328 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: 2014-120 Analysis :Method Salmonella EPA 1682; BCS SOP M-4 (15017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, /l.1 Bonnie Mull, MPH Laboratory Operations Manager Page l of 8 Final Report BCS ID 2102322,2102323,2102324,2102325,2102326,2102327,2102328 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A,GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AttlAB 4 ,/„1., •ems. .. Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-120 Client Sample ID: VD1 Sample Date/Time:February 24,2021 13:56 BCS Sample ID: 2102322 Sample Description: Biosolid Date Received: February 25, 2021 10:20 Amount Submitted:100 mL BCS Bottle %Solids: 39.0 Amount Analyzed: 29.95 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: February 25, 2021 12:35 Analysis Stop Date: March 04, 2021 11:50 Analyst: Robert Pimentel Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.7 Salmonella MPN/4 dry grams Analysis Notes: None Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-120 Client Sample ID: VD2 Sample Date/Time:February 24, 2021 13:58 BCS Sample ID: 2102323 Sample Description: Biosolid Date Received: February 25, 2021 10:20 Amount Submitted:100 mL BCS Bottle %Solids: 35.8 Amount Analyzed: 30.00 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: February 25, 2021 12:35 Analysis Stop Date: March 04, 2021 11:50 Analyst: Robert Pimentel Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.8 Salmonella MPN/4 dry grams Analysis Notes: None Page 2 of 8 Final Report BCS ID 2102322,2102323,2102324,2102325,2102326,2102327,2102328 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES r :01 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-120 Client Sample ID: VD3 Sample Date/Time:February 24, 2021 14:00 BCS Sample ID: 2102324 Sample Description: Biosolid Date Received: February 25, 2021 10:20 Amount Submitted:100 mL BCS Bottle %Solids: 36.4 Amount Analyzed: 30.10 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: February 25, 2021 12:35 Analysis Stop Date: March 04, 2021 11:50 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-120 Client Sample ID: VD4 Sample Date/Time:February 24, 2021 14:02 BCS Sample ID: 2102325 Sample Description: Biosolid Date Received: February 25, 2021 10:20 Amount Submitted:100 mL BCS Bottle %Solids: 36.8 Amount Analyzed: 30.10 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: February 25, 2021 12:35 Analysis Stop Date: March 04, 2021 11:50 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2102322,2102323,2102324,2102325,2102326,2102327,2102328 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, IS017025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 1sG=isI4EAAr .-. _,, _, Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-120 Client Sample ID: VD5 Sample Date/Time:February 24, 2021 14:04 BCS Sample ID: 2102326 Sample Description: Biosolid Date Received: February 25, 2021 10:20 Amount Submitted:100 mL BCS Bottle %Solids: 35.9 Amount Analyzed: 29.97 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: February 25, 2021 12:35 Analysis Stop Date: March 04, 2021 11:50 Analyst: Robert Pimentel Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.8 Salmonella MPN/4 dry grams Analysis Notes: None Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-120 Client Sample ID: VD6 Sample Date/Time:February 24, 2021 14:06 BCS Sample ID: 2102327 Sample Description: Biosolid Date Received: February 25, 2021 10:20 Amount Submitted:100 mL BCS Bottle %Solids: 40.3 Amount Analyzed: 30.10 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: February 25, 2021 12:35 Analysis Stop Date: March 04, 2021 11:50 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units - -- - Page 4 of 8 ----- - --- --- Final Report BCS ID 2102322,2102323,2102324,2102325,2102326,2102327,2102328 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �^ =y; � •ecneo .r— Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-120 Client Sample ID: VD7 Sample Date/Time:February 24, 2021 14:08 BCS Sample ID: 2102328 Sample Description: Biosolid Date Received: February 25, 2021 10:20 Amount Submitted:100 mL BCS Bottle %Solids: 38.9 Amount Analyzed: 29.99 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: February 25, 2021 11:10 Analysis Stop Date: March 04, 2021 11:50 Analyst: Robert Pimentel Qualifier: U Primary Value: <_0.07 Salmonella MPN/mL sample analyzed Secondary Value: <_0.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2102322,2102323,2102324,2102325,2102326,2102327,2102328 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES l.$C-1W .%YCJ.ifM+ Client: Branch Residuals and Soils Project: 2014-120 Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2102322,2102323,2102324,2102325,2102326,2102327,2102328 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES J,`l jJt�[] I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true,accurate,and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative)and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety, and/or purity of any sample, batch,source,or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. 1; CALL `l I L ):... Signature of LaboratoryDirector Authorized Rep. _ Date: March 04, 2021 g / P Page 7 of 8 Final Report BCS ID 2102322,2102323,2102324,2102325,2102326,2102327,2102328 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX.(352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES • �\ a c c n ,"t 8.: IN—... DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence for the presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BC5 ID 2102322,2102323,2102324,2102325,2102326,2102327,2102328 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A,GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO17025:2017 L2422,PADEP:68-03950,AZDHS:AZO82O, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 1110001---41) CHAIN OF CUSTODY RECORD BCS Laboratories www.microbioservices.com 4609 NW 6th street, Building A .,,,. ;-i; ._7 Inc- FL DOH Laboratory#E82924,EPA#FLO1147 Gainesville, FL 32609 / I Tel.(352)377-9272,Fax.(352)377-5630 t I I I • '' ' f, l i'" i'`' i'�''• Compliance Monitoring? CYes_No Client Name and Address. Kt?rIr\ } ,'' rI {; p g. City/State/Zip: (-'c-a.l•_i-r:iI, L.)5-' : Project ID: 7)c•t5-j1'a• Project Manager: R,i i;'..•;,E...(.. Facility/Site: , i`i_=.i•�': c. .•skip,- 1..x:: Telephone Number: ,_ 31<-4;t,o1 Fax No.: Report To: ..^.L,i-,i• 1 •.••?�- SamplerName:(Print) R. !,_I-..? 4-•' • Email: , i • •.,L '-'f,. ,,,l.r'S•s'•- Sampler Signature: "'-""-; C" Invoice To: • Matrix Analysis N 2 f0 U a O U .2 �` 3, d y N a �i m 1 Xx 2 m 92 a fi cc a o. m s m `= d E a a O x cl 9- v g 2 m m w 4 m m u a, to m .z m v E > E m 8 "8 2 m o li u- n E m m 11, o u �+ ? 'D c F. O A o c U U co ,1 u c $ n k v e E o $ . e s -z N a o s c 2 U _ CJ c c E F, .. ~ y m E o L° E d m a R2 -- y mg 5 a m m nl E E 'm c�i v § � � m m ¢ � L rA Sample ID/Description t Z I r7 o u) 3 m o 1- U u_ x rn 1- ui a �' -I w a } to z 0 ft D ? _t1 I;•',- t '- Branch Residuals and Soils VOS \:'ii i 1;j`.1 F T. ,. 2102326 \i 7.‘‘,3 I l ` .;, X. 02/2512021 10:20 . t 1 V}-'i I a',.-,,' I • 2• L Branch Residuals and Soils 2102327 till) 1.'4 !• 'r. 02/251202110.20 ~ j Branch Residuals and Soils Branch Residuals and Soils Branch Residuals and Soils Branch Residuals and Soils Branch Residuals and Soils VD7 Vol VD2 V03 • VD4 2102328 2102322 2102323 2102324 2102325 02/25f2021 10:20 02/25/2021 10:20 02/25/2021 10:20 02/25/2021 10:20 02125/2021 10:20 i' ' Method of Shipment: UPS Postal FEDEX Other: Temp.@ recp'l: 4,7 'f J 'C Relinquished by:- / Date Time Received by: Date Time IR Corrected for IR 4 /'r"•/ -- / G cl" !,;_A*:)/ �J, c.. Custody Seal: Intact Broken N i •L ,• Presence of visabie Ice Y ) Relinquished by: Date Time Received by BCS Laboratories: Date Time Presence of ice packs ( N J Hold Time �- Von Drehle Corporation Cordova,NC City of Rockingham IUP 0015 Mar-21 Biological Consulting Services Date,t nalyted.: ..:Pr m.. '.:.:.a[u .S lmQn 11..:.:. .$e0on4:40i: oo Salmo okii :.:.:.:.:.:.:........ 2103260 3/18/21 <0.07 <0.6 2101211 ' 1/14/21 <0.07 <0.6 2101212 1/14/21 <0.07 <0.7 2101213 1/14/21 <0.07 < 0.7 2101214 1/14/21 0.16 1.6 2101215 1/14/21 <0.07 <0.7 2101216 1/14/21 < 0.07 <0.7 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. Inc BIOLOGICAL CONSULTING SERVICES i.._...., OF NORTH FLORIDA, INC. ,A i/ � JV( 2zf March 25, 2021 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD-1,VD-2,VD-3,VD-4,VD-5,VD-6,VD-7 BCS ID: 2103260, 2103261, 2103262,2103263, 2103264, 2103265, 2103266 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4 (15017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2103260,2103261,2103262,2103263,2103264,2103265,2103266 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-1 Sample Date/Time:March 18, 2021 2:07 BCS Sample ID: 2103260 Sample Description: Biosolid Date Received: March 18, 2021 9:56 Amount Submitted:100 mL BCS Bottle %Solids: 41.3 Amount Analyzed: 30.10 g Receipt Temperature: 4.7 deg C Preserved: Yes Analysis Start: March 18, 2021 11:10 Analysis Stop Date: March 24, 2021 13:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 5.0.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-2 Sample Date/Time:March 18, 2021 2:10 BCS Sample ID: 2103261 Sample Description: Biosolid Date Received: March 18, 2021 9:56 Amount Submitted:100 mL BCS Bottle %Solids: 40.4 Amount Analyzed: 30.10 g Receipt Temperature: 4.7 deg C Preserved: Yes Analysis Start: March 18, 2021 11:10 Analysis Stop Date: March 24, 2021 13:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2103260,2103261,2103262,2103263,2103264,2103265,2103266 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422,PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOI IT THE WRITTEN CONSENT OF BCS LABORATORIES ilacalwRA Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-3 Sample Date/Time:March 18, 2021 2:13 BCS Sample ID: 2103262 Sample Description: Biosolid Date Received: March 18, 2021 9:56 Amount Submitted:100 mL BCS Bottle %Solids: 39.9 Amount Analyzed: 29.93 g Receipt Temperature: 4.7 deg C Preserved: Yes Analysis Start: March 18, 2021 11:10 Analysis Stop Date: March 24, 2021 13:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-4 Sample Date/Time:March 18, 2021 2:16 BCS Sample ID: 2103263 Sample Description: Biosolid Date Received: March 18, 2021 9:56 Amount Submitted:100 mL BCS Bottle %Solids: 38.3 Amount Analyzed: 30.10 g Receipt Temperature: 4.7 deg C Preserved: Yes Analysis Start: March 18, 2021 11:10 Analysis Stop Date: March 24, 2021 13:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2103260,2103261,2103262,2103263,2103264,2103265,2103266 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAx. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, IS017025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES + ti� ACC C. - rom Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-5 Sample Date/Time:March 18, 2021 2:19 BCS Sample ID: 2103264 Sample Description: Biosolid Date Received: March 18, 2021 9:56 Amount Submitted:100 mL BCS Bottle %Solids: 38.8 Amount Analyzed: 30.01 g Receipt Temperature: 4.7 deg C Preserved: Yes Analysis Start: March 18, 2021 11:10 Analysis Stop Date: March 24, 2021 13:30 Analyst: Robert Pimentel Qualifier: None Primary Value: 0.16 Salmonella MPN/mL sample analyzed Secondary Value: 1.6 Salmonella MPN/4 dry grams Analysis Notes: None Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-6 Sample Date/Time:March 18, 2021 2:22 BCS Sample ID: 2103265 Sample Description: Biosolid Date Received: March 18, 2021 9:56 Amount Submitted:100 mL BCS Bottle %Solids: 39.9 Amount Analyzed: 29.90 g Receipt Temperature: 4.7 deg C Preserved: Yes Analysis Start: March 18, 2021 11:10 Analysis Stop Date: March 24, 2021 13:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2103260,2103261,2103262,2103263,2103264,2103265,2103266 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A,GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-7 Sample Date/Time:March 18, 2021 2:25 BCS Sample ID: 2103266 Sample Description: Biosolid Date Received: March 18, 2021 9:56 Amount Submitted:100 mL BCS Bottle %Solids: 39.6 Amount Analyzed: 30.10 g Receipt Temperature: 4.7 deg C Preserved: Yes Analysis Start: March 18, 2021 11:10 Analysis Stop Date: March 24, 2021 13:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report 13C5 ID 2103260,2103261,2103262,2103263,2103264,2103265,2103266 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2103260,2103261,2103262,2103263,2103264,2103265,2103266 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL.WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES • tttu:,:4+In.XlfClr+ I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative) and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety,and/or purity of any sample, batch,source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. • mo• • Signature of Laboratory Director/Authorized Rep. `� Date: March 25, 2021 Page 7 of 8 Final Report BCS ID 2103260,2103261,2103262,2103263,2103264,2103265,2103266 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZO82O, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. 11 The sample matrix interfered with the ability to make any accurate determination. 12 No Quality Control criteria exist for the component. 13 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence forthe presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2103260,2103261,2103262,2103263,2103264,2103265,2103266 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 1 7025:201 7 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES cCn waurom CHAIN OF CUSTODY RECORD BCS Laboratories www.microbioservices.com 4609 NW 6th street, Building A Inc. FL DOH Laboratory#E82924,EPA#FLO1147 Gainesville, FL 32609 le L! Tel.(352)377-9272,Fax.(352)377-5630 Client Name and Address:F2A4c 1 12>0 s scA°le F0 4_, ,C Compliance Monitoring? Yesu No City/State/Zip: Rock L1 1, 5C. 21 73z Project ID:Zp(1-!-114 Project Manager: b a2A....)' Facility/Site: Veal0/Za.Ut Cph vR, k-i(° Telephone Number:3��3t-3tZ 9'a 1- Fax No.: Report To: b 3zi..Q Sampler Name:(Print) .Aob pZ¢.-e.L" Email: ,13 h A4,.a,4 0&N-944f, _-- Sampler Signature: re.6'22., Invoice To: j;,,,,, Matrix Analysis y 4 2 9y G b "J Branch Residuals and Soils w o a ,'S` o if/ 40 h d E x LU W U R VD-7 ea u m �a 1Q y E a 2 U X p O o- 21D3266 m v o $ ,Z. E °' c v € m € m m a u... 03/18120219:56 E c g m E ., E o c . m 2 . a E c o 6 6. o c m , u o � 'B - f iu m v $ t d ' 8 E v 'g m rA rn c E. LL m E e = °o' l v N o c c� c c oo . U c c u 3 2 ,0 01 F m E o aL° E w E v - ;b t 1y° .E y w m o. E E m d °1 E. 6, d E 2 ¢ - 2 vi Sample ID/Description ''d Z `� " a 1-- rnn 9 o u) m o I- ri i Cl) 1- ui o_ -1 a, c d } W Z O re VD-) 3joei 2.of k r 4 R, Branch Residuals and Soils r� ( VD-1 y \(17-Z t 2:ro 1 (, t Q 2103260 •o \l -3 1 Z:!j ` \e c p t 03/18/2021 9:56 V / l 9• ,p e Branch Residuals and Soils n ,.1 0 V -y 2:lI• A \ VD-2 1 g n a - �q-S' 2.:pi, t. t k. 2103261 'a}o N �7 k. 03/18/2021 9:56 0 a ,- t o y� 2$ y I. L Branch Residuals and Soils ?'L. VD- V. Branch Residuals and Soils Branch Residuals and Soils 2103262 m VD-5 V116 - D3/18/2021 9:56 - 2103264 2103265 I 1 1 Special Instructions: 03/1812021 9:56 03/18/2021 9:56 Laboratory Comments: -7 / -2 Method of Shipment: /UPS+ Postal FEDEX Other: Temp.@ recp't: ,`1 u 7 •C R hffq ' tilt,' Date Time1 Received by: L'- Date lime IR- (-i Corrected for IR 3f i 17i!' Z'{S Custody resenc Seal: Intact Broken (ll/// Presence of visable ice Y CD Relinquished by: Date lime Received by BCS Laboratories: Date lime Presence of Ice p s n N n 3/l iz q 1,3 [Hold:rime Von Drehle Corporation Cordova,NC City of Rockingham IUP 0915 Apr-21 Biological Consulting Services l ate 4A al €:prim o §0.0nel . econdar. ...alue.Sal nouella.. ............ . .......... ...................................... e ... . ra 2104055 4/8/21 <0.07 <0.7 2104056 4/8/21 <0.07 <0.7 2104057 4/8/21 <0.07 <0.7 2104058 4/8/21 <0.07 <0.6 2104059 4/8/21 <0.07 <0.6 2104060 4/8/21 <0.07 < 0.6 2104061 4/8/21 < 0.07 <0.6 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. Inc. 13 BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. P/Li April 14, 2021 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1,VD2,VD3,VD4,VDS,VD6,VD7 BCS ID: 2104055, 2104056, 2104057, 2104058, 2104059, 2104060, 2104061 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4(ISO17025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Q �, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2104055,2104056,2104057,2104058,2104059,2104060,2104061 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,W'THOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD1 Sample Date/Time:April 07, 2021 13:17 BCS Sample ID: 2104055 Sample Description: Biosolid Date Received: April 08, 2021 10:00 Amount Submitted:100 mL BCS Bottle %Solids: 36.9 Amount Analyzed: 30.10 g Receipt Temperature: 3.7 deg C Preserved: Yes Analysis Start: April 08, 2021 11:11 Analysis Stop Date: April 14, 2021 9:50 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD2 Sample Date/Time:April 07, 2021 13:20 BCS Sample ID: 2104056 Sample Description: Biosolid Date Received: April 08, 2021 10:00 Amount Submitted:100 mL BCS Bottle %Solids: 39.0 Amount Analyzed: 29.93 g Receipt Temperature: 3.7 deg C Preserved: Yes Analysis Start: April 08, 2021 11:11 Analysis Stop Date: April 14, 2021 9:50 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2104055,2104056,2104057,2104058,2104059,2104060,2104061 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD3 Sample Date/Time:April 07, 2021 13:23 BCS Sample ID: 2104057 Sample Description: Biosolid Date Received: April 08, 2021 10:00 Amount Submitted:100 mL BCS Bottle %Solids: 40.1 Amount Analyzed: 30.10 g Receipt Temperature: 3.7 deg C Preserved: Yes Analysis Start: April 08, 2021 11:11 Analysis Stop Date: April 14, 2021 9:50 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD4 Sample Date/Time:April 07, 2021 13:27 BCS Sample ID: 2104058 Sample Description: Biosolid Date Received: April 08, 2021 10:00 Amount Submitted:100 mL BCS Bottle %Solids: 41.7 Amount Analyzed: 30.10 g Receipt Temperature: 3.7 deg C Preserved: Yes Analysis Start: April 08, 2021 11:11 Analysis Stop Date: April 14, 2021 9:50 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2104055,2104056,2104057,2104058,2104059,2104060,2104061 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17O25:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES miAn -8 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD5 Sample Date/Time:April 07, 2021 13:30 BCS Sample ID: 2104059 Sample Description: Biosolid Date Received: April 08, 2021 10:00 Amount Submitted:100 mL BCS Bottle %Solids: 41.3 Amount Analyzed: 29.99 g Receipt Temperature: 3.7 deg C Preserved: Yes Analysis Start: April 08, 2021 11:11 Analysis Stop Date: April 14, 2021 9:50 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD6 Sample Date/Time:April 07,2021 13:35 BCS Sample ID: 2104060 Sample Description: Biosolid Date Received: April 08, 2021 10:00 Amount Submitted:100 mL BCS Bottle %Solids: 40.2 Amount Analyzed: 30.05 g Receipt Temperature: 3.7 deg C Preserved: Yes Analysis Start: April 08, 2021 11:11 Analysis Stop Date: April 14, 2021 9:50 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2104055,2104056,2104057,2104058,2104059,2104060,2104061 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAx.(352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT £TTHH�E�WRITTEN CONSENT OF BCS LABORATORIES 2T 'Fi AdA.ate G=.NIEZA i :;t Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD7 Sample Date/Time:April 07, 2021 13:38 BCS Sample ID: 2104061 Sample Description: Biosolid Date Received: April 08, 2021 10:00 Amount Submitted:100 mL BCS Bottle %Solids: 42.4 Amount Analyzed: 30.07 g Receipt Temperature: 3.7 deg C Preserved: Yes Analysis Start: April 08, 2021 11:11 Analysis Stop Date: April 14, 2021 9:50 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2104055,2104056,2104057,2104058,2104059,2104060,2104061 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 15.640 Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2104055,2104056,2104057,2104058,2104059,2104060,2104061 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate,and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative)and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety, and/or purity of any sample, batch,source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025,and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. 1 l�v�.��� Signature of Laboratory Director/Authorized Rep. - Date: April 14, 2021 Page 7 of 8 Final Report BCS ID 2104055,2104056,2104057,2104058,2104059,2104060,2104061 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A,GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 1 C*1's 1 .YNI DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. 11 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. 13 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence forthe presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2104055,2104056,2104057,2104058,2104059,2104060,2104061 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,W.THOUT THE WRITTEN CONSENT OF BCS LABORATORIES a C C CHAIN OF CUSTODY RECORD BCS Laboratories c . www.microbioservices.com 4609 NW 6th street, Building A kt �— inc. FL DOH Laboratory#E82924,EPA#FL01147 Gainesville, FL 32609 I , ! 1 Tel.(352)377-9272,Fax.(352)377-5630 Client Name and Address: giallajj r� r"s•J+.a-IS 6. Do I-1 Compliance Monitoring? CYesn No City/State/Zip: (133/I€ L Rivcl. 1.:le(03.291 WoCIC •-.11.k, C Z 93e Project ID: Rz? Zoly-ii0 Project Manager: Ko11,,4 ri5)zA,• . Facility/Site: verii2elya eo4-.doi,t pp Telephone Number:3343(Z•Qw r � V2,4�al Fax Report To: - Sampler Name:(Print) Pcbep--t "B, +�h Email: hi,¢43,ti.e.(.r•t?.b rt.4J-as.Cs- Sampler Signature: . Invoice To: .1,Qwe Branch Residuals and Soils Matrix Analysis VD5 2104059 2 04108/2021 10:00 o °' ' = ,..9 a o �V' U N ` O „yam„ N n u z c c s, X W U a Branch Residuals and Soils rn X 2 n w m E w o n. V06 m a w E_ o ° O 0 u 2104060 ai v o 10 2• c,' m E N E m 0 `^ o f u. 041081202110:00 Z. E o y y E L c .Q m m S c m m E Q E. t=o t to N c n °Q ii: . . E Q , u . r ._ s 0 o c-' c 0 o rg 0 c c v m v m I- . E o 2 o v ti E ? L .2 m g u°, a`, �a a E E m v .y. rn rn -_ m m Q 2 n y Sample ID/Description o P z LI c.) ii a r °8 ' o` ° = o Z m w m o e, o c in m o_ t o /� rR O m pm o i- U u x rn ui a -J - w o- - w z 0 r4 V D) t1/ 1 13.l7/ � p X ` . Branch Residuals and Soils _ VII Z" l3•2o It. lc2104055 — Al uD3 1 :23 l 4 04l0el202110:00 to V/p Li 13:27 4 )1 4 k. Branch Residuals and Soils m o `/D 5- 3:° I A k 2104056 a V/Dle )3.3 l Y R. St. 0410812021 10:00 z 0 N ia y D 1J/ 13.36' t y a g.. 4.., Branch Residuals and Soils eL a V03 5 Branch Residuals and Soils 2104057 VO4 04108/2021 10:00 2104058 y Special Instructions: 04108/2021 10:00 Laboratory Comments: /2 /,7 „ Method of Shipment: UPS ostai FEDEX Other: Temp.@ recp't: . •r 5- •C Relin�' >t�d at Time Received by:�� Date Time IR-(1 Corrected for IR /m/f / t li j I 7 61` Custody Seal: Intact Broken N/A /j ! / (/ C••' Presence of visable ice Y N Relinquished y: Date Time Received by BCS Laboratories: Date Time Presence of Ice packs Y N ,r am L(/°(/2l '(, 0 v Mold Ti -m.e ..,K,ctt. Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 May-21 Biological Consulting Services ............ . .......... .................... .................................................................................... ` lab i Dateal d i 111plo . ...aloe alo oowili.Se..ondar. ...aloe.Salmonella.. ................................................ ........................................ . ...................................... .. . ...... . .......... ........................................................................................................ ................................................ ........................................ ........................................ :.:.:::::::::.:.:.:.:.:.:::::::::::::::::::::.:::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::.:.:. ............ . .......... ...................................... 2105257 5/20/21 < 0.07 < 0.8 2105258 5/20/21 <0.07 <0.8 2105259 5/20/21 < 0.07 <0.8 2105260 5/20/21 <0.07 <0.8 2105261 5/20/21 < 0.07 <0.8 2105262 5/20/21 < 0.07 < 0.8 2105263 5/20/21 < 0.07 < 0.8 Exceedances U All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. s Inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. M A ft7 2 0 .I May 26, 2021 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1,VD2,VD3,VD4,VD5,VD6,VD7 BCS ID: 2105257, 2105258, 2105259, 2105260, 2105261, 2105262, 2105263 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4(IS017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, r-� }\ ( Bonnie Mull, MPH Laboratory Operations Manager Page l of 8 Final Report BCS ID 2105257,2105258,2105259,2105260,2105261,2105262,2105263 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES :,ter Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD1 Sample Date/Time:May 19, 2021 13:58 BCS Sample ID: 2105257 Sample Description: Biosolid Date Received: May 20, 2021 9:39 Amount Submitted:100 mL BCS Bottle %Solids: 31.5 Amount Analyzed: 30.10 g Receipt Temperature: 1.2 deg C Preserved: Yes Analysis Start: May 20, 2021 11:15 Analysis Stop Date: May 25, 2021 12:04 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD2 Sample Date/Time:May 19, 2021 14:01 BCS Sample ID: 2105258 Sample Description: Biosolid Date Received: May 20, 2021 9:39 Amount Submitted:100 mL BCS Bottle %Solids: 31.4 Amount Analyzed: 30.09 g Receipt Temperature: 1.2 deg C Preserved: Yes Analysis Start: May 20, 2021 11:15 Analysis Stop Date: May 25, 2021 12:04 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2105257,2105258,2105259,2105260,2105261,2105262,2105263 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD3 Sample Date/Time:May 19, 2021 14:04 BCS Sample ID: 2105259 Sample Description: Biosolid Date Received: May 20, 2021 9:39 Amount Submitted:100 mL BCS Bottle %Solids: 31.6 Amount Analyzed: 30.07 g Receipt Temperature: 1.2 deg C Preserved: Yes Analysis Start: May 20, 2021 11:15 Analysis Stop Date: May 25, 2021 12:04 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD4 Sample Date/Time:May 19, 2021 14:07 BCS Sample ID: 2105260 Sample Description: Biosolid Date Received: May 20, 2021 9:39 Amount Submitted:100 mL BCS Bottle %Solids: 33.0 Amount Analyzed: 30.10 g Receipt Temperature: 1.2 deg C Preserved: Yes Analysis Start: May 20, 2021 11:15 Analysis Stop Date: May 25, 2021 12:04 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2105257,2105258,2105259,2105260,2105261,2105262,2105263 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD5 Sample Date/Time:May 19, 2021 14:10 BCS Sample ID: 2105261 Sample Description: Biosolid Date Received: May 20, 2021 9:39 Amount Submitted:100 mL BCS Bottle %Solids: 31.8 Amount Analyzed: 29.99 g Receipt Temperature: 1.2 deg C Preserved: Yes Analysis Start: May 20, 2021 11:15 Analysis Stop Date: May 25, 2021 12:04 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD6 Sample Date/Time:May 19, 2021 14:13 BCS Sample ID: 2105262 Sample Description: Biosolid Date Received: May 20, 2021 9:39 Amount Submitted:100 mL BCS Bottle %Solids: 30.7 Amount Analyzed: 30.00 g Receipt Temperature: 1.2 deg C Preserved: Yes Analysis Start: May 20, 2021 11:15 Analysis Stop Date: May 25, 2021 12:04 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2105257,2105258,2105259,2105260,2105261,2105262,2105263 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, IS017025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD7 Sample Date/Time:May 19, 2021 14:16 BCS Sample ID: 2105263 Sample Description: Biosolid Date Received: May 20, 2021 9:39 Amount Submitted:100 mL BCS Bottle %Solids: 34.1 Amount Analyzed: 29.95 g Receipt Temperature: 1.2 deg C Preserved: Yes Analysis Start: May 20, 2021 11:15 Analysis Stop Date: May 25, 2021 12:04 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2105257,2105258,2105259,2105260,2105261,2105262,2105263 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,Dy EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES iIaC' i'• r `tr. .. • Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2105257,2105258,2105259,2105260,2105261,2105262,2105263 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative) and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety, and/or purity of any sample, batch,source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. -11\1 r Signature of Laboratory Director/Authorized Rep. ✓ Date: May 26, 2021 Page 7 of 8 Final Report BCS ID 2105257,2105258,2105259,2105260,2105261,2105262,2105263 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES !wQ i�Y •1Ti Aecnro DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence for the presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2105257,2105258,2105259,2105260,2105261,2105262,2105263 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX.(352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ♦e C n r.o.r t u CHAIN OF CUSTODY RECORD BCS Laboratories _rh, . -, www.microbioservices.com 4609 NW 6th street, Building A `� inc. ' 1.a - FL DOH Laboratory#E82924,EPA#FL01147 Gainesville, FL 32609 IN f ( 1 `� Tel.(352)377-9272,Fax.(352)377-5630 Client Name and Address:j,?1W;•fj t+BS•�t 1i.4114 S iS5/T�'' ttB�CI }' 3 G4 Compliance Monitoring? CYes❑No City/State/Zip: jcoG.k'.4-:!1-SC 2 913 Z Project ID: ZO('-Ito Project Manager: RA iRa4i;4• Facility/Site: vp,..t Dmt.kit Co 2_dova Telephone Number: 33•.3)Z-9oo1 Fax No.: Report To: &IL 152,4.4,1. Sampler Name:(Print) .'ob-siz4.acJs Email: hit WA-a-6 bea.w•{ -s•0-- Sampler Signature: `Z'..,r°7r:? Invoice To: 6fIM( Branch Residuals and Soils Matrix Analysis VD1 2105257 .° m 2 m d 05nOn0219:39 n o a .Y �_ _ $ m a n v V y .c X !r n r y co s _ c t9 (� = -y X a. Branch Residuals and Soils m c°i °i ii rn a' E �`' E t1 u VD2 c L m .. �, .. a n m 0 v g �, 2105259 E a G o o u d $ 'u o m m U c !r 05/2012021 9:39 co S °u .o LL o " co N 3 '' a g a o O d o g y m 0 E c .y a m o n n u y E 2 1 v o Y v U ° e c o U ._ U c c ° 5 o w = 3' E di B o m m E ' t6t m = ° 65 3 n T� E E m u ? rn , = m , ¢ r rn Sample ID/Description /0 I- z O ° 4- a iT B S I cn o m 8 ,2 6 LT s rn I°. ui a .°'i 23 w` a w z O z V D/ -5,/ 2/ I'Ss) ( 10 st° r { Branch Residuals and Soils VD 2."Ji I l _t r X. VD5 V D� 2.0 ( c �' 2105261 051 0/2021 9:39 Y D'( 2.'O7 I to r Y ,� Branch Residuals and Soils V OS- 2:10 ( `(CI Y 2105262 — v DL. 2.13 ) yO y 1' g no12021 9:39 'Ni D i 24 b I Y 1 Y Branch 05 Residuals and Soils VD7 Branch Residuals and Soils Branch Residuals and Soils 2105263 VD3 VD4 05/20/2021 9:39 2105259 2105260 Special Instructions: 05/2012021 9:39 05/2012021 9:39 Laboratory Comments: D.g sp i I.2 , 1 L �� Method or Shipment: UPS Postal FEDEX Other: Temp.@ recp't: 1 0 I,2 T 'C Reli pal d y i Date Time Received by: 'i Date Time IR-/c.r Corrected for IR ///914f q 5L Custody Seal: Intact / Broken i N/A J!' !�t ' Presence of visable ice Y N Relinquished by: Date lime Received by BCS Laboratories: Date Time Presence of Ice packs �� N .‹D f/..l at C )• 71 IH-old Time c/ Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Jun-21 Biological Consulting Services Analyzed:::::::Prima y Value::Salmonella:::::::Secondary Value::Salmonella::: ................................................ ........................................ . ...................................... ............ . .......... ....................... ................................................................................ ................................................ ........................................ ........................................ 2106271 6/23/21 <0.07 < 0.8 2106272 6/23/21 < 0.07 <0.7 2106273 6/23/21 < 0.07 <0.7 2106274 6/23/21 <0.07 <0.6 2106275 6/23/21 <0.07 <0.6 2106276 6/23/21 <0.07 <0.6 2106277 6/23/21 <0.07 < 0.6 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. s Inc. BIOLOGICAL CONSULTING SERVICES �� OF NORTH FLORIDA, INC. ✓ ,-.-i l,n!e 2 6 t/ June 30, 2021 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: T1,T2,T3,T4,T5,T6 BCS ID: 2106271, 2106272, 2106273, 2106274, 2106275, 2106276, 2106277 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis (Method Salmonella EPA 1682; BCS SOP M-4(IS017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, --- �, '‘ rL I t 0� Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2106271,2106272,2106273,2106274,2106275,2106276,2106277 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 VWVW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES >• ry Nam/ 1f7C. A4 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: T1 Sample Date/Time:June 22, 2021 14:00 BCS Sample ID: 2106271 Sample Description: Biosolid Date Received: June 23, 2021 11:19 Amount Submitted:100 mL BCS Bottle %Solids: 34.5 Amount Analyzed: 30.10 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: June 23, 2021 12:22 Analysis Stop Date: June 26, 2021 11:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: T2 Sample Date/Time:June 22, 2021 14:05 BCS Sample ID: 2106272 Sample Description: Biosolid Date Received: June 23, 2021 11:19 Amount Submitted:100 mL BCS Bottle %Solids: 38.9 Amount Analyzed: 29.95 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: June 23, 2021 12:22 Analysis Stop Date: June 26, 2021 11:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2106271,2106272,2106273,2106274,2106275,2106276,2106277 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: T3 Sample Date/Time:June 22, 2021 14:07 BCS Sample ID: 2106273 Sample Description: Biosolid Date Received: June 23, 2021 11:19 Amount Submitted:100 mL BCS Bottle %Solids: 37.0 Amount Analyzed: 30.01 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: June 23, 2021 12:22 Analysis Stop Date: June 26, 2021 11:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: T4 Sample Date/Time:June 22, 2021 14:10 BCS Sample ID: 2106274 Sample Description: Biosolid Date Received: June 23, 2021 11:19 Amount Submitted:100 mL BCS Bottle %Solids: 44.4 Amount Analyzed: 30.10 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: June 23, 2021 12:22 Analysis Stop Date: June 26, 2021 11:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2106271,2106272,2106273,2106274,2106275,2106276,2106277 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHO'T THE WRITTEN CONSENT OF BCS LABORATORIES ? lJ C__3Ak-7-*, i , � ' -ram Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: T5 Sample Date/Time:June 22, 2021 14:13 BCS Sample ID: 2106275 Sample Description: Biosolid Date Received: June 23, 2021 11:19 Amount Submitted:100 mL BCS Bottle %Solids: 42.1 Amount Analyzed: 29.93 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: June 23, 2021 12:22 Analysis Stop Date: June 26, 2021 11:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: T6 Sample Date/Time:June 22, 2021 14:16 BCS Sample ID: 2106276 Sample Description: Biosolid Date Received: June 23, 2021 11:19 Amount Submitted:100 mL BCS Bottle %Solids: 44.6 Amount Analyzed: 30.07 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: June 23, 2021 12:22- Analysis Stop Date: June 26, 2021 11:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2106271,2106272,2106273,2106274,2106275,2106276,2106277 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ilacARA Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: T6 Sample Date/Time:June 22, 2021 14:20 BCS Sample ID: 2106277 Sample Description: Biosolid Date Received: June 23, 2021 11:19 Amount Submitted:100 mL BCS Bottle %Solids: 44.6 Amount Analyzed: 29.94 g Receipt Temperature: 2.7 deg C Preserved: Yes Analysis Start: June 23, 2021 12:22 Analysis Stop Date: June 26, 2021 11:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2106271,2106272,2106273,2106274,2106275,2106276,2106277 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 VWVW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ecnr. o,-ram Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2106271,2106272,2106273,2106274,2106275,2106276,2106277 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, IS017025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ititAikA JAB _, , +ecnrn. I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true,accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative)and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety, and/or purity of any sample, batch,source,or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program,as applicable unless otherwise noted. (1r, 1'7 0-1 Signature of Laboratory Director/Authorized Rep. Date: June 30, 2021 — — — --4 -� Page 7 of 8 Final Report BCS ID 2106271,2106272,2106273,2106274,2106275,2106276,2106277 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 VWWV.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES „) • G`11 A erne DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence for the presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2106271,2106272,2106273,2106274,2106275,2106276,2106277 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx.(352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIESLf- Ajfik B ""Ijk aes. CHAIN OF CUSTODY RECORD BCS Laboratories www.microbioservices.com 4609 NW 6th street, Building A Inc. FL DOH Laboratory#E82924,EPA#FL01147 Gainesville, FL 32609 2 Tel.(352)377-9272,Fax.(352)377-5630 Client Name and Address: I)\—C,I' l Y,.,,,\J l„- , s ,,y I'V 3 1-1, UeR I,,d j.- y . ` 1 I Compliance Monitoring? EYes❑No City/State/Zip: 12,0,,1E i-I.t 1 SC Z`'1/52 Project ID: Z 1-(K /1 Project Manager: Pi,1) 1>4.,C L Facility/Site: V e.0 D,:=,-,1,t e C C"i c .' 44 (YC- Telephone Number:_3'' 7 z 9 o{ Fax No.: Report To: R:-1313;2,4..;y� Sampler Name:(Print) J ..b R2,q.,cI.. Email: h‘,F2i3.1c,1_L�tc',4 Ll--. c— SamplerSignature:,(1_1',t i' Invoice To: PPb R2„+. II Branch Residuals and Soils Matrix Analysis T6 2106276 u U `c =06/23/2021 11:19 2 if _ a m m '.' - c U \-, c m X a Branch Residuals and Sails rg m e fn w .4 E LLLLII p 0 Q T6 v c v o A i ' .2, m y € m m € m O w0 0 m Q LL 2106277 a a m '6, B c v m 12! U c K E E c ,illm _u m'f0 N / 2i - 'c o a o g m m c ,n F O6f231202111:19 C5 N Pi n u- g m E o y 8 lu. cn c H 2. U 0 u c QcQ To U V c c e v m t' °I u F 2 E c g i m m E 2 r, t 5 $ m Ti a R E E T, u 2. .2 0 m i Q 40 t N Sample ID/Description o i= 2 c" U ii o. g 3 o m .3 6 m o` lo- o a T u ro ui 8 °3 w a > w z O z T0 ,y2)Ll! r t �:) r 9 y St Branch Residuals and Soils 1 I G f/ T I ff lY 9 r g. T3 2106273 1 ? ` /y.CJ] i` 1 '� 06/23/2021 11:19 Branch Residuals and Soils 1 r' IL•�t7 .� 1. T4 1 S i 11-113 u > ,, 2106274 T C ( ly i 6 ,F ,,1 A- )- 06/23/2021 11:19 Branch Residuals and Soils T{: 4, 14 G, Y 't ' `/- T5 Branch Residuals and Soils Branch Residuals and Soils 2106275 T1 ' T2 06/23/2021 11:19 2106271 2106272 I Special Instructions: 06/2312021 11:19 06/23/2021 11:19 Laboratory Comments:Method of Shipment: (UPS. Postal FEDEX Other. Temp.@ recp't: 1. r q 7 .7 .0 Relinquished by." / Date Time Received by: '--' Date Time IR- Corrected tor,IR ���,/ '/l� 'J��i ({1b Custody Seal: Intact Broken MIA ! - ( l Presence of visable ice Y N Relinquished by: Date Time Received by BCS Laboratories Date Time Presence of ice packs (.Y N j , IHoldTime l� I __ �-�;'- .�r-^, �i_i 1«1 ,1. ,�� • o,rrn.,me,.... Von Drehle Corporation Cordova,NC City of Rockingham IUP 0015 Jul-21 Biological Consulting Services i at i Date A al yze i .€ P im aloe.Salmonella... Secondar. ...alue.Salmonella.. . ....... .. e . a ................................................ .. 2107449 7/15/21 <0.07 <0.7 2107450 7/15/21 < 0.07 <0.7 2107451 7/15/21 < 0.07 <0.7 2107452 7/15/21 < 0.07 <0.7 2107453 7/15/21 < 0.07 <0.6 2107454 7/15/21 <0.07 < 0.7 2107455 7/15/21 < 0.07 <0.7 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. 4 Inc. BIOLOGICAL CONSULTING SERVICES �/ OF NORTH FLORIDA, INC. ✓ 1 Jccy 23C1 July 20, 2021 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD7,VD1,VD2,VD3,VD4,VDS,VD6 BCS ID: 2107449, 2107450, 2107451, 2107452, 2107453, 2107454, 2107455 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Cordova NC Analysis ;Method Salmonella EPA 1682; BCS SOP M-4(15017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, . j 0.1,vrL<.{�, LLB Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2107449,2107450,2107451,2107452,2107453,2107454,2107455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES pos ile- r - -4AB r �'' •cr_n r.o.s.. xu..nawn _. Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD7 Sample Date/Time:July 14, 2021 14:10 BCS Sample ID: 2107449 Sample Description: Biosolid Date Received: July 15, 2021 9:44 Amount Submitted:100 mL BCS Bottle %Solids: 39.2 Amount Analyzed: 30.10 g Receipt Temperature: 2.6 deg C Preserved: Yes Analysis Start: July 15, 2021 10:55 Analysis Stop Date: July 20, 2021 9:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: <_0.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD1 Sample Date/Time:July 14, 2021 13:56 BCS Sample ID: 2107450 Sample Description: Biosolid Date Received: July 15, 2021 9:44 Amount Submitted:100 mL BCS Bottle %Solids: 39.5 Amount Analyzed: 29.90 g Receipt Temperature: 2.6 deg C Preserved: Yes Analysis Start: July 15, 2021 10:55 Analysis Stop Date: July 20, 2021 9:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 5_0.07 Salmonella MPN/mL sample analyzed Secondary Value: _5.0.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2107449,2107450,2107451,2107452,2107453,2107454,2107455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAx. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, IS017025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES iIBG,_-NIRA Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD2 Sample Date/Time:July 14, 2021 13:59 BCS Sample ID: 2107451 Sample Description: Biosolid Date Received: July 15, 2021 9:44 Amount Submitted:100 mL BCS Bottle %Solids: 40.1 Amount Analyzed: 30.03 g Receipt Temperature: 2.6 deg C Preserved: Yes Analysis Start: July 15, 2021 10:55 Analysis Stop Date: July 20, 2021 9:30 Analyst: Robert Pimentel Qualifier: U Primary Value: <_0.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD3 Sample Date/Time:July 14, 2021 14:01 BCS Sample ID: 2107452 Sample Description: Biosolid Date Received: July 15, 2021 9:44 Amount Submitted:100 mL BCS Bottle %Solids: 38.5 Amount Analyzed: 30.01 g Receipt Temperature: 2.6 deg C Preserved: Yes Analysis Start: July 15, 2021 10:55 Analysis Stop Date: July 20, 2021 9:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 5.0.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2107449,2107450,2107451,2107452,2107453,2107454,2107455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17O25:2017 L2422, PADEP: 68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ryry., lJ acArfA- Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD4 Sample Date/Time:July 14, 2021 14:03 BCS Sample ID: 2107453 Sample Description: Biosolid Date Received: July 15, 2021 9:44 Amount Submitted:100 mL BCS Bottle %Solids: 41.2 Amount Analyzed: 30.10 g Receipt Temperature: 2.6 deg C Preserved: Yes Analysis Start: July 15, 2021 10:55 Analysis Stop Date: July 20, 2021 9:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD5 Sample Date/Time:July 14, 2021 14:05 BCS Sample ID: 2107454 Sample Description: Biosolid Date Received: July 15, 2021 9:44 Amount Submitted:100 mL BCS Bottle %Solids: 39.6 Amount Analyzed: 30.10 g Receipt Temperature: 2.6 deg C Preserved: Yes Analysis Start: July 15, 2021 10:55 Analysis Stop Date: July 20, 2021 9:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 1]nal Report BCS ID 2107449,2107450,2107451,2107452,2107453,2107454,2107455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 1 ' AttlAB q .term:,.-rr: Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD6 Sample Date/Time:July 14, 2021 14:07 BCS Sample ID: 2107455 Sample Description: Biosolid Date Received: July 15, 2021 9:44 Amount Submitted:100 mL BCS Bottle %Solids: 39.8 Amount Analyzed: 30.09 g Receipt Temperature: 2.6 deg C Preserved: Yes Analysis Start: July 15, 2021 10:55 Analysis Stop Date: July 20, 2021 9:30 Analyst: Robert Pimentel Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2107449,2107450,2107451,2107452,2107453,2107454,2107455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES -la- of Client: Branch Residuals and Soils Project: Cordova NC Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2107449,2107450,2107451,2107452,2107453,2107454,2107455 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED.EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate,and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative)and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety,and/or purity of any sample, batch,source,or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025,and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. 1 i} Signature of Laboratory Director/Authorized Rep. Date: July 20, 2021 Page 7 of 8 Final Report BCS ID 2107449,2107450,2107451,2107452,2107453,2107454,2107455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX.(352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WI.HOUT THE WRITTEN CONSENT OF BCS LABORATORIES DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence for the presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2107449,2107450,2107451,2107452,2107453,2107454,2107455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES CHAIN OF CUSTODY RECORD BCS Laboratories 111111111iwww.microbioservices.com 4609 NW 6th street, Building A Ir,c- FL DOH Laboratory#E82924,EPA#FLO1147 Gainesville, FL 32609 _" i-r'? //{,c Lk I .-,.) Tel.(352)377-9272,Fax.(352)377-5630 Client Name and Address: 1);.4../k i`c, 6,t-il `-0 t, j;L. -t ' ' Compliance Monitoring? Yes No City/State/Zip: koCL (.l:il, ';(:. ,'Cf 732 Project ID: C',:JLI-X: Project Manager: R.:),`13::,..,,k_ Facility/Site: C;e .. k('• Telephone Number: ---i t,,-.31? 9tv/ Fax No.: Report To: iL b T.%i.. 7 Sampler Name:(Print) -L), 1?x.4. k Email: tat,r,q.,,I,13n4,.:,;.L' 5i.� Sampler Signature: r'>f<i( Invoice To: 54q Branch Residuals and Sails Matrix Analysis VD6 2107465 m •2 m •--ram a y 07H5120219:44 n o d 2 2 n v X .yd. m N `" V. (9 �^ c m X w cc a Branch Residuals and Soils m m "o w °d \ m E x w a�i ` n y e E a A U X . a+ 210V7449 c T ii S !° m E 4 Q u Y, - m�-' ` v € 3 m € m O 0 , c $ x u.. 07/15/2021 9:44 E E e _p y .2 c m m 3 u 3 S m o S m m ',{{ oa D ,n . F' cn u) O L 2. U. U N E N ,S ._ 32 n U $ V 4. CQQ U U 2 C p -8 N to I- R E m o , 'n E a `• `a ` c •R 8 To a •E E m $ a c c i5 " Q b 0 N Sample ID/Description ° g n r° r°n S rn 3 ° © o r°- ci iL I co Fo- ui a m v w a > tu z O cc v'l I 7/1414 13 57- \ � y , ,P Branch Residuals and Soils 1 _ Y V it 2 I I)fi ' ,' Y ? 2107450 VT)i ' HA 1 y Y. 07/15/20219:44 Branch Residuals and Soils vi LI ( it-I.:%3 \ r L Y VD2 V I)iv I 1 ti ,K N P 1 1` 2107451 V ill, I 1`i:6) 3 - 07/15/2021 9:44 T r -7 /.1).,'. iil, l,9:ly t Branch Residuals and Soils — V03 Branch Residuals and Soils Branch Residuals and Soils 2107452 VD4 V05 07/15/2021 9:44 — 2107453 2107454 Special Instructions: 07/15/2021 9:44 07/15/2021 9:44 Laboratory Comments: .— �, Method of Shipment: UPS Postal FEDEX Other- Temp.@ recp't: 1.0 (- .6 •C Relinqulshed,hy:/! Date lime Received by: Date lime IR- 'I i. Corrected' IR 1, ,, � �� 1� •{' Custody Seal: Intact ' Broken WA // "14/ ;IA t-IL f'J Presence of visable ice Y t Relinquished by: Date Time Received by BCS Laboratories: Die Time Presence of Ice p ks (Y-'') N L1YI-1 o7 �,'1 n` i, IHoid Time\ Von Drehle Corporation Cordova,NC City of Rockingham IUP 0015 Aug-21 Biological Consulting Services tali Date Anal zed Prim ry alue.Salmonella Secondary yaw Value.salmonella.. ............ . .......... ...................................... 2108449 8/27/21 < 0.07 <0.6 2108450 8/27/21 < 0.07 < 0.7 2108451 8/27/21 < 0.07 <0.7 2108452 8/27/21 0.07 0.70 2108453 8/27/21 < 0.07 <0.7 2108454 8/27/21 0.07 0.70 2108455 i 8/27/21 < 0.07 <0.6 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. A set of samples was collected on August 11,2021, one of these seven samples did not past the detection limit. A set of resamples were collected on August 26, 2021. These confirmation samples are all in compliance. I was not able to determine what Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. �e5,fJ6 S Inc. BIOLOGICAL CONSULTING SERVICES COF NORTH FLORIDA, /NC. � oz4 September 07,2021 Robert Branch f} S � OD) s � Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD-1,VD-2,VD-3,VD-4,VD-5,VD-6,VD-7 BCS ID: 2108449, 2108450, 2108451, 2108452, 2108453, 2108454, 2108455 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4(15017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, ll� Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2108449,2108450,2108451,2108452,2108453,2108454,2108455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES .Artu3 _, Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-1 Sample Date/Time:August 26, 2021 13:25 BCS Sample ID: 2108449 Sample Description: Biosolid Date Received: August 27, 2021 11:28 Amount Submitted:100 mL BCS Bottle %Solids: 40.8 Amount Analyzed: 29.99 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: August 27, 2021 13:00 Analysis Stop Date: September 02, 2021 11:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-2 Sample Date/Time:August 26, 2021 13:28 BCS Sample ID: 2108450 Sample Description: Biosolid Date Received: August 27, 2021 11:28 Amount Submitted:100 mL BCS Bottle %Solids: 40.1 Amount Analyzed: 30.10 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: August 27, 2021 13:00 Analysis Stop Date: September 02, 2021 11:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2108449,2108450,2108451,2108452,2108453,2108454,2108455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17O25:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ilacimkA AptAB • Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-3 Sample Date/Time:August 26, 2021 13:31 BCS Sample ID: 2108451 Sample Description: Biosolid Date Received: August 27, 2021 11:28 Amount Submitted:100 mL BCS Bottle %Solids: 40.1 Amount Analyzed: 29.96 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: August 27, 2021 13:00 Analysis Stop Date: September 02, 2021 11:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: <_0.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-4 Sample Date/Time:August 26, 2021 13:35 BCS Sample ID: 2108452 Sample Description: Biosolid Date Received: August 27, 2021 11:28 Amount Submitted:100 mL BCS Bottle %Solids: 40.2 Amount Analyzed: 30.10 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: August 27, 2021 13:00 Analysis Stop Date: September 07, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.7 Salmonella MPN/4 dry grams Analysis Notes: None Page 3 of 8 Final Report BCS ID 2108449,2108450,2108451,2108452,2108453,2108454,2108455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 VWVW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES \J+r.1, A ti ArLa , . '�^.^ rCnr.a.r rc Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-5 Sample Date/Time:August 26, 2021 13:39 BCS Sample ID: 2108453 Sample Description: Biosolid Date Received: August 27, 2021 11:28 Amount Submitted:100 mL BCS Bottle %Solids: 40.0 Amount Analyzed: 30.01 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: August 27, 2021 13:00 Analysis Stop Date: September 02, 2021 11:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-6 Sample Date/Time:August 26, 2021 13:44 BCS Sample ID: 2108454 Sample Description: Biosolid Date Received: August 27, 2021 11:28 Amount Submitted:100 mL BCS Bottle %Solids: 40.4 Amount Analyzed: 29.95 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: August 27, 2021 13:00 Analysis Stop Date: September 07, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.7 Salmonella MPN/4 dry grams Analysis Notes: None - Page 4 of 8 Final Report BCS ID 2108449,2108450,2108451,2108452,2108453,2108454,2108455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX.(352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT,THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD-7 Sample Date/Time:August 26, 2021 13:46 BCS Sample ID: 2108455 Sample Description: Biosolid Date Received: August 27, 2021 11:28 Amount Submitted:100 mL BCS Bottle %Solids: 40.2 Amount Analyzed: 29.97 g Receipt Temperature: 1.6 deg C Preserved: Yes Analysis Start: August 27, 2021 13:00 Analysis Stop Date: September 02, 2021 11:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2108449,2108450,2108451,2108452,2108453,2108454,2108455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 664E te r .�, ccnr.o..ro Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2108449,2108450,2108451,2108452,2108453,2108454,2108455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true,accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative)and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety, and/or purity of any sample, batch,source,or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program,as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. ' Date: September 07, 2021 Page 7 of 8 Final Report BCS ID 2108449,2108450,2108451,2108452,2108453,2108454,2108455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ice\ Acorn,-rn Mt.r1.ulYJutOT+ ..CO.. DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence for the presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2108449,2108450,2108451,2108452,2108453,2108454,2108455 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES -Pacirsoi '��` ,r c c1..1 CHAIN OF CUSTODY RECORD BCS Laboratories '' ' -----, www.microbioservices.com 4609 NW 6th street, Building A ,' ..--) 1,-,. FL DOH Laboratory#E82924,EPA#FL01147 Gainesville, FL 32609 I r I! I -- Ak7k�Blid Tel.(352)377-9272,Fax.(352)-37-7-5630 Client Name and Address: _ 444' 4S.GI.. ' .V ..lie i IC�- _ f( Compliance Monitoring? IYesn No City/State/Zip: So`,)_l4.(l, -SC 2c173a Project ID: Z ola-/io Project Manager: R.b /32q-/( Facility/Site: \(O.,!Daet•A2 Cc.-dw A,Al C Telephone Number: "31.'3/2'9(.07 Fax No.: Report To: -5A.- Sampler Name:(Print) Roh 4Y 2,1...,0.1-. Email: 61),,;;4,.i{''1,)0pncL 125 L Sampler Signature:�� Invoice To: 4,4..E Branch Residuals and Soils Matrix Analysis VD-6 0 on 2108454 5a m '> o 08127f202111:28 a g E.13 �+ = Q "V. '� 1't �'` w c�.t a. v. G - Branch Residuals and Soils y o w rn to \ 0 E X W 4 y m a w E a U a c c m ii 2108455 n a II R v ° ra a m O1 * m E E 8 uni m U R ,9 a E E w m d 3 D a ?, 3 'c o _ c _ CC 08/2712021 11:28 m w a - w L a a 3 c� a a a a t m o 8 a 2 o E E rn ti n) ,, a iZ u d¢ E °= °2 w c v —' U a u c COQ ._ r0 c c yy O c �D w 1- % E c F. c ,i m E m .c3 > c R, `m T. n 6 'E E Z. w c .4 6 _ O 1= z o o it I w 5 w 3 p` o $ o a" a d it o " 10 a agi c a m a O 'C Sample ID/Description o. I- rn u o m in o I- 0 L I v) I- ui a J J w a >- w z o re VD-I 4/4411 1.2} I ., se 4. Branch Residuals and Soils VD-1 V p'L 12 t Y 2108449 - VD'3 1.31 l Y' j `( -08/27/202111:28 in a i Branch Residuals and Soils m 1z p m 4 1/4[ I J Y 1. 2108450 •N - N q D I Li' i 1' ' ,� 08127/2021 11:28 iiia ,r iv J d Branch Residuals and Soils -r c VD i l.yd, \ r v VO4 6 2108451 2 Branch Residuals and Soils m VD-5 08/27/202111:28 ' 2108453 — Special Instructions: 08)27/2021 11:28 Laboratory Comments: ri, (//; Method of Shipment: )Postal FEDEX Other: Temp.@ recp't: O i `' I Y 'C Reli hod b // Dee lime Received by: Date lime IR- ( Corrected Jer-lFt i� OLAj 24", Pustody resence ofeal:v Intact Broken (44-- S Presence visable ice 'NN Relinquished by: Date lime Received by BCS Laboratone ; Date Time Presence of Ice pack N �j �) g/2 7/ZI I r 2-r1Hold Time V I BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. you4cj- 202 / August 20, 2021 Robert Branch du 6 : Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1,VD2,VD3,VD4,VDS,VD6,VD7 BCS ID: 2108175, 2108176, 2108177, 2108178, 2108179, 2108180, 2108181 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: 2014-110 Analysis IMethod Salmonella EPA 1682; BCS SOP M-4(15017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, • ) (iC Bonnie Mull, MPH Laboratory Operations Manager Page l of 8 Final Report BCS ID 2108175,2108176,2108177,2108178,2108179,2108180,2108181 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 VWVW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES , Arts 11 ilaCARA Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD1 Sample Date/Time:August 11, 2021 13:32 BCS Sample ID: 2108175 Sample Description: Biosolid Date Received: August 12, 2021 10:04 Amount Submitted:100 mL BCS Bottle %Solids: 39.2 Amount Analyzed: 30.00 g Receipt Temperature: 3.6 deg C Preserved: Yes Analysis Start: August 12, 2021 11:20 Analysis Stop Date: August 18, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD2 Sample Date/Time:August 11, 2021 13:34 BCS Sample ID: 2108176 Sample Description: Biosolid Date Received: August 12, 2021 10:04 Amount Submitted:100 mL BCS Bottle %Solids: 39.5 Amount Analyzed: 30.04 g Receipt Temperature: 3.6 deg C Preserved: Yes Analysis Start: August 12, 2021 11:20 Analysis Stop Date: August 18, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 F;ral Report BCS ID 2108175,2108176,2108177,2108178,2108179,2108180,2108181 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, IS017025:2017 L2422,PADEP:68-03950,AZDHS:AZO82O, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITrEN CONSENT OF BCS LABORATORIES maegitRA AptAB 4ecnr. Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD3 Sample Date/Time:August 11, 2021 13:36 BCS Sample ID: 2108177 Sample Description: Biosolid Date Received: August 12, 2021 10:04 Amount Submitted:100 mL BCS Bottle %Solids: 36.7 Amount Analyzed: 30.05 g Receipt Temperature: 3.6 deg C Preserved: Yes Analysis Start: August 12, 2021 11:20 Analysis Stop Date: August 20, 2021 11:45 Analyst: Robert Pimentel, B.S. Qualifier: None Primary Value: 1.0 Salmonella MPN/mL sample analyzed Secondary Value: 11.0 Salmonella MPN/4 dry grams Analysis Notes: None Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD4 Sample Date/Time:August 11, 2021 13:38 BCS Sample ID: 2108178 Sample Description: Biosolid Date Received: August 12, 2021 10:04 Amount Submitted:100 mL BCS Bottle %Solids: 38.9 Amount Analyzed: 30.10 g Receipt Temperature: 3.6 deg C Preserved: Yes Analysis Start: August 12, 2021 11:20 Analysis Stop Date: August 18, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2108175,2108176,2108177,2108178,2108179,2108180,2108181 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ilatT411,1 APiA13 ".` 'tip• �•.:1�,�1��.. ...,.uuu.ter.a Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD5 Sample Date/Time:August 11, 2021 13:40 BCS Sample ID: 2108179 Sample Description: Biosolid Date Received: August 12, 2021 10:04 Amount Submitted:100 mL BCS Bottle %Solids: 39.9 Amount Analyzed: 30.10 g Receipt Temperature: 3.6 deg C Preserved: Yes Analysis Start: August 12, 2021 11:20 Analysis Stop Date: August 18, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD6 Sample Date/Time:August 11, 2021 13:42 BCS Sample ID: 2108180 Sample Description: Biosolid Date Received: August 12, 2021 10:04 Amount Submitted:100 mL BCS Bottle %Solids: 39.2 Amount Analyzed: 30.09 g Receipt Temperature: 3.6 deg C Preserved: Yes Analysis Start: August 12, 2021 11:20 Analysis Stop Date: August 18, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: <_0.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2108175,2108176,2108177,2108178,2108179,2108180,2108181 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES .ren...,A Client: Branch Residuals and Soils Analysis: Salmonella Project Name: 2014-110 Client Sample ID: VD7 Sample Date/Time:August 11,2021 13:45 BCS Sample ID: 2108181 Sample Description: Biosolid Date Received: August 12, 2021 10:04 Amount Submitted:100 mL BCS Bottle %Solids: 39.6 Amount Analyzed: 30.00 g Receipt Temperature: 3.6 deg C Preserved: Yes Analysis Start: August 12, 2021 11:20 Analysis Stop Date: August 18, 2021 10:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2108175,2108176,2108177,2108178,2108179,2108180,2108181 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES SICA ffA Aptiu3 ' eene.o :ee Client: Branch Residuals and Soils Project: 2014-110 Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2108175,2108176,2108177,2108178,2108179,2108180,2108181 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ? lJ •tcn ro.:cn I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative)and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety, and/or purity of any sample, batch,source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025,and the FL DOH Environmental Laboratory Certification Program,as applicable unless otherwise noted. • .1 Wt. Signature of Laboratory Director/Authorized Rep. Date: August 20, 2021 Page 7 of 8 Final Report BCS ID 2108175,2108176,2108177,2108178,2108179,2108180,2108181 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, IS017025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES LJ ,` ce:, - DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence for the presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2108175,2108176,2108177,2108178,2108179,2108180,2108181 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES CHAIN OF CUSTODY RECORD BCS Laboratories ..m+- .. www.microbioservices.com 4609 NW 6th street, Building A V'kl'��t „-) Inc FL DOH Laboratory#E82924,EPA#F"L011�1�47 Gainesville, FL 32609 fJ I %�/� '` t f''Sf/cc ee RIF d Tel.(352)377-9272,Fax.(352)377-5630 Client Name and Address:gleXiaX fl�`9O44 .-b'!- .5 e/D3-2/} Compliance Monitoring? VYesE No City/State/ip: Fv� /.r+11, SC c?1 ?_ Project ID: 2t21L'I lfl fj Project Manager: � Dgot+.tel- Facility/Site: la)t4M �oe.'t�i 4 fJG Telephone Number:3r,�c 3/Z-9Do/ Fax No.: Report To: 7/l, P.A+-c-1" Sampler Name:(Print) po ); Email: bid?.A• eb aA^f0�Sampler Signature:r� / Invoice To: — Matrix Analysis ,� 2 m 2 4a a /� c _ X X R. Y y V' r] Y _ C 4 C O )Co. y 3 " u 's u E wo a Q a a�i v o 19 9 u .Z io %f m .2. 3 4x E_ m m € m 8 E s ` 3 H LL Ea m g 12 m m 2 m ii o. 3 J r7 r<i o a m ,2 'o m m o o c v' Q m a) o S. n lr 1 v U p c Egg U U c c f0 �.°- 3 = m E o 1 E i `° E I'u L m e ui t 76 Ti E t b $ d 'o+ .rn I. p m S o t v) Sample ID/Description o E= z cb 0 tL a ' 8 8 N 3 6 m o - U )i I rn r ui a . . w a > w z o g VD) j /l! /2- ' 7( .� se Y Branch Residuals and Soils 2108178 _,H 4D3 I 1,34. ( r ? Y -e 08/12/2021 10:04 _2 o v D q /': ? t 7" r tI Branch Residuals and Soils — A p m re v DS- l.'�D 1 /° 7 Y t VD5 N'N a ` �J y f 2108179 — a w V 7 r)�+'Z I r I 081121202110:04 _ _ vD 1 LI l;iiS 1 p r t e Branch Residuals and Soils —to _ Branch Residuals and Soils Branch Residuals and Soils Branch Residuals and Soils Vtl6 _ V01 VD2 - VD3 2108180 2108175 2108176 _ 2106177 08/12I2021 10:04 �_ OBl1212021 10:04 O8/121202110:04 08/121202110:04 Laborator Method of Shipment: UPS Postal FEDEX Other: Temp.©recp't: 2. ' 12, b •C rhecLbjr, at Time Received by: Date Time IR-rw CorrectedferIR L( /, r� Custody Seal: IntactBroken MA7 U X,z G. 7i Presence of visable ice Y v)' Relinquished by: Date Time Rece.ed BCS stories Date Time Presence of ice pac s 0 N ? /(�12, 10. �� Haid Time ( axscxnaa r.t ca Von Drehle Corporation Cordova,NC City of Rockingham 1UP 0015 Sep-21 Biological Consulting Services .. ... Lab# Date Analyzedililipegoodly00011$00.00411111$00440:valiii.smokaiolli.: 111111111i1111111ili111111111i111i111111111iMPN per nil MPN per 4gr4wPry. 2109081 9/8/21 < 0.07 < 0.6 2109082 9/8/21 < 0.07 <0.6 2109083 9/8/21 < 0.07 <0.6 2109084 9/8/21 < 0.07 <0.6 2109085 9/8/21 < 0.07 < 0.6 2109086 9/8/21 < 0.07 < 0.6 2109087 9/8/21 < 0.07 <0.8 Exceedances .. All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. 1C10inc. BIOLOGICAL CONSULTING SERVICES ' OF NORTH FLORIDA, INC. 59 IQ..t4..-L Z o z / .7. September 15, 2021 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD6,VD7,VD1,VD2,VD3,VD4,VD5 BCS ID: 2109081, 2109082, 2109083, 2109084, 2109085, 2109086, 2109087 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis (Method Salmonella EPA 1682; BCS SOP M-4 (15017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, \�L r i"- ' , ,/lt.rl cE. Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2109081,2109082,2109083,2109084,2109085,2109086,2109087 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD6 Sample Date/Time:September 07, 2021 13:58 BCS Sample ID: 2109081 Sample Description: Biosolid Date Received: September 08,2021 11:15 Amount Submitted:100 mL BCS bottle %Solids: 41.8 Amount Analyzed: 30.05 g Receipt Temperature: 2.8 deg C Preserved: Yes Analysis Start: September 08, 2021 12:31 Analysis Stop Date: September 14, 2021 14:13 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD7 Sample Date/Time:September 07, 2021 14:01 BCS Sample ID: 2109082 Sample Description: Biosolid Date Received: September 08,2021 11:15 Amount Submitted:100 mL BCS bottle %Solids: 41.8 Amount Analyzed: 30.08 g Receipt Temperature: 2.8 deg C Preserved: Yes Analysis Start: September 08, 2021 12:31 Analysis Stop Date: September 14, 2021 14:13 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2109081,2109082,2109083,2109084,2109085,2109086,2109087 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, IS017025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITH -"T THE WRITTEN CONSENT OF BCS LABORATORIES ac a ANAB ,ram_ Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD1 Sample Date/Time:September 07, 2021 13:42 BCS Sample ID: 2109083 Sample Description: Biosolid Date Received: September 08, 2021 11:15 Amount Submitted:100 mL BCS bottle %Solids: 41.7 Amount Analyzed: 30.10 g Receipt Temperature: 2.8 deg C Preserved: Yes Analysis Start: September 08, 2021 12:31 Analysis Stop Date: September 14, 2021 14:13 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD2 Sample Date/Time:September 07, 2021 13:45 BCS Sample ID: 2109084 Sample Description: Biosolid Date Received: September 08,2021 11:15 Amount Submitted:100 mL BCS bottle %Solids: 42.1 Amount Analyzed: 30.10 g Receipt Temperature: 2.8 deg C Preserved: Yes Analysis Start: September 08,2021 12:31 Analysis Stop Date: September 14, 2021 14:13 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2109081,2109082,2109083,2109084,2109085,2109086,2109087 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX.(352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES act Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD3 Sample Date/Time:September 07, 2021 13:48 BCS Sample ID: 2109085 Sample Description: Biosolid Date Received: September 08,2021 11:15 Amount Submitted:100 mL BCS bottle %Solids: 42.5 Amount Analyzed: 30.03 g Receipt Temperature: 2.8 deg C Preserved: Yes Analysis Start: September 08,2021 12:31 Analysis Stop Date: September 14, 2021 14:13 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD4 Sample Date/Time:September 07, 2021 13:52 BCS Sample ID: 2109086 Sample Description: Biosolid Date Received: September 08, 2021 11:15 Amount Submitted:100 mL BCS bottle %Solids: 41.9 Amount Analyzed: 30.10 g Receipt Temperature: 2.8 deg C Preserved: Yes Analysis Start: September 08, 2021 12:31 Analysis Stop Date: September 14, 2021 14:13 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2109081,2109082,2109083,2109084,2109085,2109086,2109087 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, IS017025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 'I� ��\ ccne.nre.0 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD5 Sample Date/Time:September 07, 2021 13:55 BCS Sample ID: 2109087 Sample Description: Biosolid Date Received: September 08,2021 11:15 Amount Submitted:100 mL BCS bottle %Solids: 31.0 Amount Analyzed: 30.02 g Receipt Temperature: 2.8 deg C Preserved: Yes Analysis Start: September 08, 2021 12:31 Analysis Stop Date: September 14, 2021 14:13 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2109081,2109082,2109083,2109084,2109085,2109086,2109087 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES „ acTIA ,`•e�,/.`. •`lam' - Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2109081,2109082,2109083,2109084,2109085,2109086,2109087 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422,PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate,and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative) and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety,and/or purity of any sample, batch,source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. September 15, 2021 Signature of Laboratory Director/Authorized Rep. Date: Page 7 of 8 Final Report BCS ID 2109081,2109082,2109083,2109084,2109085,2109086,2109087 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES r A / \� AtCeneo.sen DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. 11 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence for the presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2109081,2109082,2109083,2109084,2109085,2109086,2109087 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHO"T THE WRITTEN CONSENT OF BCS LABORATORIES CHAIN OF CUSTODY RECORD BCS Laboratories www.microbioservices.com 4609 NW 6th street, Building A Ir-t . FL DOH Laboratory#E82924,EPA#FL01 47 Gainesville, FL 32609 /)' —i-:l_//35 ie,,L'1i "�Y� Tet.(352)377-9272,Fax-f352)377-5 30 — Client Name and Address: �' & IN�'II '.KS•d`f i`fi''S :5.<.-1e l j•24! Compliance Monitoring? LYesn No City/State/Zip:A44-1 Ii,.1C Zii %-3Z Project ID: 2t>/L)-/I`c Project Manager: 17 h 1je'.4ru'-1- Facility/Site: t i.c,L J7 r.z (,4' Co2 e- , cov,a ki Telephone Number: 531-�/.'yt'b 1 Fax No.: Report To: 9t6;hz4...(2 Sampler Name:(Print) Ei),.,b 1Bha4.-�„L Email: t,1j a A-'4s.61)b12,4.--,1 L3.G..-...— Sampler Signature: `67''ye----( Invoice To: 3;3-.e• Branch Residuals and Soils Matrix Analysis VD5 ‘g 2109087 r� c, •> E0 U a. - 09l08)2021 11:15 c E a _ a f� .D m m P. 0 m - - \'i C N X X y m u N W of Branch Residuals and Soils c .• m E T' o - VD6 5 n i = = 0 E X Qtil LLl X Q 2109091 T `-° _ a m .D d 10 �°•jv �' co a - 'u •� o _ a o7 U o 091081202111:15 c: g u �3 r •o 5y�j O g < e m E a s :o - U NO u - o U _ () s e 22 9 .. ,- 7 la- m E o o m m E ''S. 2 t g O 8 22 2a' m w m o 8 m m c c7, 2 c¢- ` .2 en en Sample ID/Description o 1 F z r, a i- co 2 0 in ei O 1- ci u_ x rn 1- ui 0 3 3 w a > w z 0 0: \;})1 'IA/ 1_'y/L 1 y' I \,j T Branch Residuals and Soils li 1)2 vol -- ( �.ii ( 7 - v_ _ Y 2109093 .J1).3 I (. t / `T' m 09/0812021 11:15 \J j]y ).I2 ) y Y ' c r ,i, Branch Residuals and Soils 1II�i� VD2 5 1.5S I }' Y (' i G N ('� 2109084 �/�L i (+�1 l Ni; - 'I >o -t 09/08/2021 11:15 ` � r 2 O tv r%�f \, 0l i .r Y �,, CrCrc e 1 Branch ResidualsVD3 and Soils Branch Residuals and Soils m 2109085 VD4 re 09108/2021 11:15 2109086 . Special Instructions: 09108/2021 11:15 Laboratory Comments: r, .. Method of Shipment: (61PS}Postal FEDEX Other. Temp.@ recp't: -2.• 2•0 'C �Reelfi 4'sh b 7 Date Time Received by: ✓ Date Time IR-iZ Corrected for IR r11 .) Custody Seal: Intact Broken N (' , �l iizl 2 J Z Presence of visable Ice Y 1t Relinquished by: Date Time Received by BCS Laboratories: Date Time Presence of Ice packs CYO N y3 15 t kr, Mold Time Von Drehle Corporation Cordova,NC City of Rockingham IUP 0015 Oct-21 Biological Consulting Services ` I ate:Anal d ngoo Va�uo::00.000ella::ii H*..ondar. ....woi$4lmtiA011 . ............ . ............... .................. e .. a 2109346 10/1/21 < 0.07 < 0.6 2109347 10/1/21 < 0.07 < 0.6 2109348 10/1/21 < 0.07 0.700 2109349 10/1/21 < 0.07 < 0.6 2109350 10/1/21 0.07 0.7 2109351 10/1/21 < 0.07 < 0.6 2109352 10/1/21 < 0.07 < 0.6 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. —,� BIOLOGICAL CONSULTING SERVICES inc. OF NORTH FLORIDA, INC. z.)z i October 06, 2021 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1,VD2,VD3,VD4,VD5,VD6,VD7 BCS ID: 2109346, 2109347, 2109348, 2109349, 2109350, 2109351, 2109352 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4(15017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, - /I\It r) Bonnie Mull, MPH Laboratory Operations Manager Page l of 8 Final Report BCS ID 2109346,2109347,2109348,2109349,2109350,2109351,2109352 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ,,.,,,.t„ AAB F ilaCilitgA , ac cn Ao,A r.n Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD1 Sample Date/Time:September 23, 2021 13:48 BCS Sample ID: 2109346 Sample Description: Biosolid Date Received: September 24,2021 10:03 Amount Submitted:100 mL BCS Bottle %Solids: 42.8 Amount Analyzed: 30.02 g Receipt Temperature: 3.2 deg C Preserved: Yes Analysis Start: September 24, 2021 11:21 Analysis Stop Date: October 01, 2021 12:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD2 Sample Date/Time:September 23, 2021 13:55 BCS Sample ID: 2109347 Sample Description: Biosolid Date Received: September 24,2021 10:03 Amount Submitted:100 mL BCS Bottle %Solids: 42.6 Amount Analyzed: 30.00 g Receipt Temperature: 3.2 deg C Preserved: Yes Analysis Start: September 24,2021 11:21 Analysis Stop Date: October 01, 2021 12:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BC5 ID 2109346,2109347,2109348,2109349,2109350,2109351,2109352 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Nita . ate. \\r .e e _ . Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD3 Sample Date/Time:September 23, 2021 13:51 BCS Sample ID: 2109348 Sample Description: Biosolid Date Received: September 24,2021 10:03 Amount Submitted:100 mL BCS Bottle %Solids: 43.1 Amount Analyzed: 30.10 g Receipt Temperature: 3.2 deg C Preserved: Yes Analysis Start: September 24, 2021 11:21 Analysis Stop Date: October 05, 2021 12:30 Analyst: Robert Pimentel, B.S. Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.7 Salmonella MPN/4 dry grams Analysis Notes: None Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD4 Sample Date/Time:September 23, 2021 13:58 BCS Sample ID: 2109349 Sample Description: Biosolid Date Received: September 24, 2021 10:03 Amount Submitted:100 mL BCS Bottle %Solids: 42.1 Amount Analyzed: 29.95 g Receipt Temperature: 3.2 deg C Preserved: Yes Analysis Start: September 24, 2021 11:21 Analysis Stop Date: October 01, 2021 12:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2109346,2109347,2109348,2109349,2109350,2109351,2109352 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES INEE1 I ACC>t P. •- ,�r'�. —®._..tea— . ._ Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD5 Sample Date/Time:September 23, 2021 13:45 BCS Sample ID: 2109350 Sample Description: Biosolid Date Received: September 24,2021 10:03 Amount Submitted:100 mL BCS Bottle %Solids: 42.5 Amount Analyzed: 30.06 g Receipt Temperature: 3.2 deg C Preserved: Yes Analysis Start: September 24, 2021 11:21 Analysis Stop Date: October 05, 2021 12:30 Analyst: Robert Pimentel, B.S. Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.7 Salmonella MPN/4 dry grams Analysis Notes: None Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD6 Sample Date/Time:September 23, 2021 14:01 BCS Sample ID: 2109351 Sample Description: Biosolid Date Received: September 24, 2021 10:03 Amount Submitted:100 mL BCS Bottle %Solids: 42.5 Amount Analyzed: 29.97 g Receipt Temperature: 3.2 deg C Preserved: Yes Analysis Start: September 24, 2021 11:21 Analysis Stop Date: October 01, 2021 12:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2109346,2109347,2109348,2109349,2109350,2109351,2109352 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AdAB Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD7 Sample Date/Time:September 23, 2021 13:42 BCS Sample ID: 2109352 Sample Description: Biosolid Date Received: September 24,2021 10:03 Amount Submitted:100 mL BCS Bottle %Solids: 43.0 Amount Analyzed: 30.00 g Receipt Temperature: 3.2 deg C Preserved: Yes Analysis Start: September 24,2021 11:21 Analysis Stop Date: October 01, 2021 12:00 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2109346,2109347,2109348,2109349,2109350,2109351,2109352 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES -7 _ Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2109346,2109347,2109348,2109349,2109350,2109351,2109352 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES •ecnr.n.r rc I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative)and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety, and/or purity of any sample, batch,source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program,as applicable unless otherwise noted. P � ,t� �k- October 06, 2021 Signature of Laboratory Director/Authorized Rep. Date: Page 7 of 8 Final Report BCS ID 2109346,2109347,2109348,2109349,2109350,2109351,2109352 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950,AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Atecnentrrn �1,0G_1NRA DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence for the presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2109346,2109347,2109348,2109349,2109350,2109351,2109352 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES JIla6='MRAAdAB a C C MCRtW/N CHAIN OF CUSTODY RECORD BCS Laboratories am-� 4? ;.�,_,t,C--- www.microbioservices.com 4609 NW 6th street, Building v::L4�� ir'G' FL DOH Laboratory#E82924,EPA#FL01147 Gainesville, FL 32609 ~- —.-. Tell352)37-7-9272-,-Fax-(352)377-5630. Client Name and Address:V2rl..: f,2t5 1-y r 5),1> 1 7.J Week It)lj kid.u•:It (`'3.1 y 1 Compliance Monitoring? F—Yesn No City/State/Zip: ) ,.k p-.II SC 29752 Project ID: c2.:/44N Project Manager: fro)?R,Oit•t L Facility/Site: v.i Dee/J,' t1,41,dct,r4- 4f' Telephone Number: i.0 312.-Qot f Fax No.: Report To: h�?At-.a- Sampler Name:(Print) 3 :?Pa---1/4- Email: hb.2'h,,l-C-')0r_al'eiz----- Sampler Signature:X :c /r Invoice To: j.4-e Branch Residuals and Soils Matrix Analysis VD4 m 2109349 m m U w 0912412021 10:03 n 8 n Z S " y (O� U i .c m 1 .Y ... o 0 . .� X it 1 Branch Residuals and Soils " u _ 00 �, cet E w O a v taVD5 c m m m r n € a € 10 U 1-2 O �n C. u 2109350 e' w '6 y o u F. °i d f 'B 5 E b o m O a c Y 09/2412021 10:03 E E E .y m m ! 2 5 m m '- n, 3 ._ ._ m m E in _ Q F. o LL n o_ a a w y V �' c c U ._ U m Y a 16 3 43 S m E c L° o a `m E '$ L 0 Zi ❑` 4 t o Z' d W c 0 . L y m d b L ❑ Sample ID/Description ❑ 2 c' U <L . 4 rn 8 g m 8 � v v_ x rn r ui n- -J _I w a r w z o e: 1(D I -7�1/4/ 1•r'(j \ \P Q... -- Branch Residuals and Soils V h Z i I.3J i `f k. L. ;ir vol 2109346 up 3 \ . I'S•) 1 y St, i, 2, 09/2412021 10:03 \D`i \ S�)' 1 ,f 1 y' Branch Residuals and Soils 5- i•Yr I �c 21VD2 09347 . . U D/v 2.:t 1 I. .L 09124/2021 10:03 4 1L Branch Residuals and Soils ID 1 Z t Y VD3 2109348 09/24/2021 10:03 Special Instructions: Laboratory Comments: , S cY'Method of Shipment: UPS)Postal FEDEX Other. Temp.@ recp't: ��, v 3 U 'C Rel' ui ed by: Date Time Received by: Date Time IR- ) 3 Corrected for IR cii?'/ 7 Custody Seal: Intact Broken �fIA7 ' �/�� Z. i�` Presence of visable Ice 'Y .N� Relinquished by: Date Time Received/7 by BCS Laboratorrieti s: Date Time Presence of Ice pac s �/ N Branch Residualsand Soils Branch Residuals and Soils I/i�'�i (1 ?/2* 11c,:03 (Hold Time vol L'1 / �{A_t/ // 7 ........vP.m.�u.:..ar.,,.wc.�� 2109351 2109352 ,/''' 0912412021 10:03 09/24/2021 10:03 Von Drehle Corporation Cordova,NC City of Rockingham IUP 0015 Nov-21 Biological Consulting Services ial i4teale1' �m. . ...a[u...Salmonell ....Secoada . ...alue.SaUnoneUa.. 2110282 11/2/21 <0.07 <0.7 2110283 11/2/21 <0.07 <0.7 2110284 11/2/21 <0.07 < 0.7 2110285 11/2/21 < 0.07 < 0.7 2110286 11/2/21 < 0.07 < 0.6 2110287 11/2/21 0.07 0.70 2110288 11/2/21 <0.07 < 0.7 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. .--' BIOLOGICAL CONSULTING SERVICES ft S Inc. � 0" OF NORTH FLORIDA, INC. NoVe„bell- zvz1 November 03, 2021 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD1,VD2,VD3,VD4,VDS,VD6,VD7 BCS ID: 2110282, 2110283, 2110284, 2110285, 2110286, 2110287, 2110288 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4(IS017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, --;--,2 , 1\11 ( i. f Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2110282,2110283,2110284,2110285,2110286,2110287,2110288 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAx.(352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924.IS017025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ilk A JAB r Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD1 Sample Date/Time:October 26, 2021 13:09 BCS Sample ID: 2110282 Sample Description: Biosolid Date Received: October 27, 2021 9:36 Amount Submitted:100 mL BCS Bottle %Solids: 39.8 Amount Analyzed: 30.10 g Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Start: October 27, 2021 10:40 Analysis Stop Date: November 02, 2021 9:40 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD2 Sample Date/Time:October 26, 2021 13:13 BCS Sample ID: 2110283 Sample Description: Biosolid Date Received: October 27, 2021 9:36 Amount Submitted:100 mL BCS Bottle %Solids: 39.7 Amount Analyzed: 30.08 g Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Start: October 27, 2021 10:40 Analysis Stop Date: November 02, 2021 9:40 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2110282,2110283,2110284,2110285,2110286,2110287,2110288 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD3 Sample Date/Time:October 26, 2021 13:10 BCS Sample ID: 2110284 Sample Description: Biosolid Date Received: October 27, 2021 9:36 Amount Submitted:100 mL BCS Bottle %Solids: 39.6 Amount Analyzed: 30.02 g Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Start: October 27, 2021 10:40 Analysis Stop Date: November 02, 2021 9:40 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD4 Sample Date/Time:October 26, 2021 13:07 BCS Sample ID: 2110285 Sample Description: Biosolid Date Received: October 27, 2021 9:36 Amount Submitted:100 mL BCS Bottle %Solids: 39.3 Amount Analyzed: 30.10 g Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Start: October 27, 2021 10:40 Analysis Stop Date: November 02, 2021 9:40 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2110282,2110283,2110284,2110285,2110286,2110287,2110288 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD5 Sample Date/Time:October 26, 2021 12:56 BCS Sample ID: 2110286 Sample Description: Biosolid Date Received: October 27, 2021 9:36 Amount Submitted:100 mL BCS Bottle %Solids: 40.8 Amount Analyzed: 29.94 g Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Start: October 27, 2021 10:40 Analysis Stop Date: November 02, 2021 9:40 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD6 Sample Date/Time:October 26, 2021 12:59 BCS Sample ID: 2110287 Sample Description: Biosolid Date Received: October 27, 2021 9:36 Amount Submitted:100 mL BCS Bottle %Solids: 40.8 Amount Analyzed: 29.93 g Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Start: October 27, 2021 10:40 Analysis Stop Date: November 03, 2021 10:20 Analyst: Robert Pimentel, B.S. Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.7 Salmonella MPN/4 dry grams Analysis Notes: None Page 4 of 8 Final Report BCS ID 2110282,2110283,2110284,2110285,2110286,2110287,2110288 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES II�BGAdAB - Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD7 Sample Date/Time:October 26, 2021 13:03 BCS Sample ID: 2110288 Sample Description: Biosolid Date Received: October 27, 2021 9:36 Amount Submitted:N/A %Solids: 40.0 Amount Analyzed: 30.00 g Receipt Temperature: 1.8 deg C Preserved: Yes Analysis Start: October 27, 2021 10:40 Analysis Stop Date: November 02, 2021 9:40 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units • Page 5 of 8 Final Report BCS ID 2110282,2110283,2110284,2110285,2110286,2110287,2110288 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 1 47 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2110282,2110283,2110284,2110285,2110286,2110287,2110288 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17O25:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FU L,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative)and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality,safety,and/or purity of any sample, batch,source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. ti / • .1 '\1 (\ Signature of Laboratory Director/Authorized Rep. Date: November 03, 2021 Page 7 of 8 Final Report BCS ID 2110282,2110283,2110284,2110285,2110286,2110287,2110288 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950,AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 100, U'•.ti DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. 11 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence for the presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2110282,2110283,2110284,2110285,2110286,2110287,2110288 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ���F • CHAIN OF CUSTODY RECORD BCS Laboratories www.microbioservices.com 4609 NW 6th street, Building A lIIIi:rrc FL DOH Laboratory#E82924,EPA#FLO1147 Gainesville, FL 32609 n f Tel.(352)377-9272,Fax.(352)377-5630 Client Name and Address: ��2 7^fC� i 85 cLoii ` Si::�s 173 5/,Lkle l L i 5..L(u3 24f Compliance Monitoring? Yes❑No City/State/Zip: k,a,,,l i1.1,1 . c Z2 c±73 Z Project ID: 2 01.1-11 e Project Manager: /3,,b 2i y✓L Facility/Site: v0.iD 1eA it Co,z lcv,4 NC Telephone Number: `d i::: =112-ga,1 Fax No.: Report To: .;b fia_,.' Sampler Name:(Print) Rohs..t t'-?Z.4..*. Email: i,I),z.1-icl 1:-biz 1-,ct.es(.,--- Sampler Signature: T! Invoice To: ,);v. Analysis Branch Residuals and Soils Matrix VDs 2 2110287 . •� 19 1.5. in 1012712021 9:36 a ii Bi u • ,� ? c d o. y t XX H m 0 x `° X as Branch Residuals and Soils c �` B ry w u E x w o ov Q VD7 c g. c- .. m u x 2 v v m 2110288 n m m �' _ E f0 a E m U 0, m cQ i N To. o• `9 m E u >n n c u 0. d 31_ a c o_ m .P c m 2 '. 10127120219:]6 H "-- 01 N a 3 rn a S a ' L T. o 0 10 m . E 'g '_ F v) to c a Et 0 m E o .2. 5 m Y :o = d ii 8 c c o •_ ci c o m m 3 .. _ Sample ID/Description o 1= z (5 O 'z x m 7--- ' 0 8 o ' L m m o " m m m l d a — p p o I- `O u, m 0 t- v u x rn r- ui a J J w a } w Z 0 v71 1o12 21 13.0 1 '/ . 'l Branch Residuals and Soils v1)2 I \ :I3 1 •P _2. 2 - vol 2110282 y 7 3 RIp 1 y 1, 9,. k. 10127/2021 9:36 V j) `i 13 L? 1 7 t 1` k Branch Residuals and Soils VD2 V j 12. 4 \ 'l' 1. k 2110283 VD L 2.'9 1 ]' { 1. i. 10!27120219:36 Branch Residuals and Soils 1,P'l 4 i3 tot y .� C. -1 VD3 Branch Residuals and Soils Branch Residuals and Soils 2110284 VD4 1105 10127/2021 9:36 2110295 2110286 Special Instructions: 1012712021 9:36 1012712021 9:36 Laboratory Comments: Method of Shipment: I UPS)Postal FEDEX Other: Temp.@ recp't: 2. 1 CS 'C 3,1i,luish. ). y Date Time Received by: Date Time IR-\� Conected,.to IR iCustody Seal: Intact Broken 'N/A �f' �NZL�11 pi, v Presence of visable ice (Y, (d Relinquished by Date Time Received by BCS Laboratories: Date Time Presence of ice pgcks v(J N Kf_‘$.t•t'' 1°12.1121 �,3� IHoldTime 1-It,,l y.`j U t'l Von Drehle Corporation Cordova,NC City of Rockingham IUP 0015 Dec-21 Biological Consulting Services at I at A al e > i `mo . . ...aloe win0nella....ae..ondar. ...aloe.§alr oneUa.. 111111111111111111111111.. 1111111111111111111111 .................. .................... .................... ................. .............. 2111285 12/1/21 < 0.07 < 0.7 2111286 12/1/21 < 0.07 <0.7 2111287 12/1/21 < 0.07 <0.7 2111288 12/1/21 < 0.07 <0.7 2111289 12/1/21 < 0.07 <0.6 2111290 12/1/21 < 0.07 < 0.6 2111291 1 12/1/21 < 0.07 <0.7 Exceedances All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Monthly Pathogen and Vector Attraction Reduction Forms for Class A option. CS Inc BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. �L'�✓&� Z_02/ December 02, 2021 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd.Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD 1,VD 2,VD 3,VD 4,VD 5,VD 6,VD 7 BCS ID: 2111285, 2111286, 2111287, 2111288, 2111289, 2111290, 2111291 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4(15017025 and TNI Accredited) Following,you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, 1')Q- Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2111285,2111286,2111287,2111288,2111289,2111290,2111291 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX.(352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT �THE EWWRITTEN CONSENT OF BCS LABORATORIES 1G=t�F2AJAB -aa. Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 1 Sample Date/Time:November 22, 2021 13:10 BCS Sample ID: 2111285 Sample Description: Biosolid Date Received: November 23, 2021 9:46 Amount Submitted:100 mL BCS Bottle %Solids: 36.0 Amount Analyzed: 30.10 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: November 23, 2021 11:20 Analysis Stop Date: December 01, 2021 10:50 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 2 Sample Date/Time:November 22, 2021 13:12 BCS Sample ID: 2111286 Sample Description: Biosolid Date Received: November 23, 2021 9:46 Amount Submitted:100 mL BCS Bottle %Solids: 38.0 Amount Analyzed: 30.08 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: November 23, 2021 11:20 Analysis Stop Date: December 01, 2021 10:50 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2111285,2111286,2111287,2111288,2111289,2111290,2111291 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES r ACCIlentrro omits, Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 3 Sample Date/Time:November 22, 2021 13:14 BCS Sample ID: 2111287 Sample Description: Biosolid Date Received: November 23, 2021 9:46 Amount Submitted:100 mL BCS Bottle %Solids: 37.3 Amount Analyzed: 30.00 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: November 23,2021 11:20 Analysis Stop Date: December 01, 2021 10:50 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 4 Sample Date/Time:November 22, 2021 13:16 BCS Sample ID: 2111288 Sample Description: Biosolid Date Received: November 23,2021 9:46 Amount Submitted:100 mL BCS Bottle %Solids: 37.5 Amount Analyzed: 30.00 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: November 23, 2021 11:20 Analysis Stop Date: December 01, 2021 10:50 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2111285,2111286,2111287,2111288,2111289,2111290,2111291 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN F.LL,W.THOUT THE WRITTEN CONSENT OF BCS LABORATORIES ,,r ._ Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 5 Sample Date/Time:November 22, 2021 13:18 BCS Sample ID: 2111289 Sample Description: Biosolid Date Received: November 23, 2021 9:46 Amount Submitted:100 mL BCS Bottle %Solids: 40.3 Amount Analyzed: 30.10 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: November 23, 2021 11:20 Analysis Stop Date: December 01, 2021 10:50 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 6 Sample Date/Time:November 22,2021 13:20 BCS Sample ID: 2111290 Sample Description: Biosolid Date Received: November 23, 2021 9:46 Amount Submitted:100 mL BCS Bottle %Solids: 40.9 Amount Analyzed: 29.96 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: November 23, 2021 11:20 Analysis Stop Date: December 01, 2021 10:50 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2111285,2111286,2111287,2111288,2111289,2111290,2111291 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES f. ilac.„1...„-WA, PAW 0:4* c c n ot,.i.d:• a .. .n.ean. Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 7 Sample Date/Time:November 22, 2021 13:22 BCS Sample ID: 2111291 Sample Description: Biosolid Date Received: November 23,2021 9:46 Amount Submitted:100 mL BCS Bottle %Solids: 38.4 Amount Analyzed: 30.05 g Receipt Temperature: 0.5 deg C Preserved: Yes Analysis Start: November 23,2021 11:20 Analysis Stop Date: December 01, 2021 10:50 Analyst: Robert Pimentel, B.S. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected:Analyte was not detected in the sample analyzed;Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2111285,2111286,2111287,2111288,2111289,2111290,2111291 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP:68-03950,AZDHS:AZO82O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �fQi�Aelt ccn Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s)were received well preserved and in excellent condition. Sample(s)were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2111285,2111286,2111287,2111288,2111289,2111290,2111291 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL. (352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924,ISO 17025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES .ccnro. ro :,7~1•\:•' ,< .•.T I certify that I have examined and I am familiar with the information submitted herein.The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client.The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client(or client's representative) and it's/their condition at the time of analysis.The sample(s)were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch,source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices.The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. i; (.. �L' '-�, I Rt,l l". Signature of Laboratory Director/Authorized Rep. Date: December 02, 2021 Page 7 of 8 Final Report BCS ID 2111285,2111286,2111287,2111288,2111289,2111290,2111291 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, IS017025:2017 L2422, PADEP:68-03950,AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification or delayed delivery. Analysis performed outside of associated method required QC data set(1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit&the practical quantitation limit. J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component. J3 The data are questionable because of improper laboratory or field protocols. L Off scale high.Actual value is known to be greater than value given. N Presumptive evidence for the presence of material.There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected.The specified component was not detected.The reported value is the method detection limit. ✓ Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved sample;the data may not be accurate Too many colonies present(TNTC);the numeric value given represents the upper end of the value that can be determined based on the volume. Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. ^ Sampling container supplied by client.Sterility can not be confirmed by BCS. # BCS Lab specific qualifier.See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2111285,2111286,2111287,2111288,2111289,2111290,2111291 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET,STE.A, GAINESVILLE, FLORIDA 32609 TEL.(352)377-9272, FAX. (352)377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422,PADEP:68-03950,AZDHS:AZ082O, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED,EXCEPT IN FULL,WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES � Aikoi CHAIN OF CUSTODY RECORD BCS Laboratories 4609 NW 6th street, Building A www.microbioservices.com Inc. FL DOH Laboratory#E82924,EPA#FL01147 Gainesville, FL 32609 Tel.(352)377-9272,Fax.(352)377-5630 Client Name and Address: Compliance Monitoring? Yesu No City/State/Zip: Project ID: Project Manager: Facility/Site: Telephone Number. 112-9..QL71- Fax No.: Report To: Sampler Name:(Print) _ A b I a I-Alt'' Email: Sampler Signature: ' 7 Invoice To: Matrix Analysts Soils U, Residuals and 2 m •i~ U Branch d y VDT a ii c T ..$ L xx fa, 27 2111291 ;� w C9 v 1112312021 �, w '5 `, w 0 m n V X O a- Q d m % v ii `0 5 u .Z m a v € m ,� € m o `92 N° ° ~ E E = u u 5 ° 1.3 e R. 9 0 0 .c G O CO 0 ? U a m u -E m n m in .. I- y t0 `o a it u s E e g g s 13 3 2 u c C U _ U c 2 ? Z m [O m H m E 6 L° o m 'm c• 2 o �s ,4 is m n -8 E E d u rn 2. a: B 5 a t y Sample ID!Description z " n 1- o` in 3 m o I- U ti 5 rn I- u 0 J J W 0- } W Z 0 re r)^ 1 1 2 I 11 fD \ I .,d, Branch Residuals and Soils 2111288 t h.• J I /14• \ K. 1 1.111/23/2021 9:46 \l J -. is:''O [ i k i > I I I I t V7w1 4c l i X. 1 4 v. Branch Residuals and Soils VD 5 'f / 1 I. ;iy'� 'k �}' 1 $t 2111289 ,�rl l f 2 ' `zs. i A 11/23/2021 9:46 Branch Residuals and Soils Branch Residuals and Soils VD 1 - Branch Residuals and Soils _ VD 3 12111285 VD 2 2111287 - 2111286 11/23/2021 9:46 LaboratoryComments: 11/2372021 9:46 11123/2021 9.46 r .1 • ) A Method of Shipment: UPS !Postal FEDEX Other: Temp.@ recp't: 1 3 (_• ) •C Re ngl7is d by // Date Time Received by: \ Date Time IR-it( Corrected for IR JI Custody Seal: Intact Broken Fl/A { I Presence of visablo Ice Y �N Relinquished by. Dale Time Received by BCS Laboratories Date Time Presence of Ice packs L Y N Branch Residuals and Soils /lt I ' c•( ,t,, (Hold Time V06 r \i i.-1 7( ..+•.0j111.1c.dZnIto.,,1:0.4.. 2111290 11/23/2021 9:46