WQ0030998_Residual Annual Report 2021_20220224

Non -Discharge Branch Upload/Submittal Form
NORTH CAROLINA
EnWrvnmemfal Qualify
Version 2 - Revised June 23, 2020
Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?*
Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0030998
Applicant/Permittee Triple S Farms and Cleaning, Inc.
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office
CO Reviewer
Admin Reviewer
Wilmington

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name*
Robert T. Branch
Email Address* Phone Number*
[e-mail] 3363129007
Project Information
Application/Document Type *
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Permit Number: *
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
WQ0030998
Has Current Existing permit number
Applicant/Permittee Address* Triple S Farms PO Box 709 Beulaville NC 28518
Facility Name*
High -Rate Infiltration
Reclaimed Water
Residuals
Other
Triple S Farms and Cleaning Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Triple S Farms 2021 AR Final.pdf 11.68MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/24/2022

2021 ANNUAL REPORT
TRIPLE S FARMS & CLEANING, INC.
LAND APPLICATION PROGRAM
PERMIT #WQ0030998
Prepared For:
Triple S Farms & Cleaning, Inc.
Post Office Box 709
Beulaville, NC 28518
Prepared By:
Branch Residuals & Soils, LLC
1735 Heckle Blvd. Suite 103-291
Rock Hill, SC 29732
February 2022

BRANCH RESIDUALS & SOILS, LLC
1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732
PHONE [phone]
February 24, 2022
North Carolina Department of Environmental Quality
Division of Water Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2021 LAND APPLICATION ANNUAL REPORT
Triple S Farms & Cleaning, Inc.
Permit No. WQ0030998
Branch Residuals & Soils Project No. 2007-70
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced
permit on behalf of the Triple S Farms & Cleaning, Inc. This data includes: 1) Certification Forms and Facility
Information, 2) Annual Residual Sampling Summary Forms, 3) Annual Metals Field Loading Summary Forms,
4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7)
Pathogen & Vector Attraction Forms, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils
Lab Data 10) 2021 Application Summary Table, and 11) 2021 Application Condition Summaries.
A total of 5,720,002.28 gallons (479.97 dry tons) of Class B lime -stabilized biosolids or Class B fecal and
injected/incorporated biosolids were land applied to 102.45 acres in 2021. This material was divided as
follows:
• 240,000 gallons (12.31 dry tons) from Beulaville WWTP,
• 2,722,002.28 gallons (199.94 dry tons) from Clayton Little Creek WRF,
• 66,000 gallons (2.97 dry tons) from Kenansville WWTP,
• 0 gallons (0 dry tons) from Rose Hill WWTP,
• 400,000 gallons (41.20 dry tons) from Warsaw WWTP,
• 48,000 gallons (2.56 dry tons) from Southwest Plantation WWTP, and
• 2,244,000 gallons (220.99 dry tons) from Wallace WWTP.
If any further information is required regarding this land application program, please do not hesitate to contact
me at [phone].
Robert T. Branch, L.S.S.
Land Application/Residuals Operator
#15676
RTB
Enclosures
cc: Town of Beulaville Town of Kenansville
Town of Rose Hill Town of Warsaw
Southwest Plantation Town of Wallace
Town of Clayton

TABLE OF CONTENTS
SECTION NO. TITLE
I Certification Forms and Facility Information
II Annual Residual Sampling Summary Forms
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Forms
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Reports
X 2021 Application Summary Table
XI 2021 Application Condition Summaries

CERTIFICATION FORMS AND FACILITY INFORMATION

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0030998 County:
Facility Name (as shown on permit):
Land Application Operator:
Duplin Year: 2021
Triple S Farms & Cleaning
Triple S Farms & Cleaning Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
© Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part Application Summarj
Total number of application fields in the permit: I 10
Total number of fields utilized for land application during the year: I 8
Total amount of dry tons applied during the year for all application sites:
479.97
Total number of acres utilizes for land application during the year: I 102.45
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to Items 1-13 below) issued by the Division of Water Quality. © Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of tines and imprisonment for knowing violations."
Mr. Eric R. Smith, Owner
Permittee Name and Title (type or print)
Signature of Permittee
i4D
Date
See Attached
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF BEULAVILLE
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. E i Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of taw, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
rc , �i..r...7
a -
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF CLAYTON
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. Cl Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the pennit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete.1 am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
/ tf nxNn..wa mss.o.,, o.T.o..wcI.n=ft
tr1" William Simpson
0.11f?ELL' Date: 201202 le 111e3e-09.7
Signature of Prepay Date
(if different from rmittec)
* Preparer is del ed in 40 CFR Part 503.9 (r) and 15A NCAC 021' .1102 (26)

ANNUAL. t AND APP1'i:IC'A►ION CM111.1cAlIC►N 1,0ItM
i OWN t►1i KV.NANSYll;1,t+.
I'RYt li - Aum►pt_i'mpi9,11s£tittottrocnt• permit
Facility was compliant during t iilenttat )cat 0..) I with ad c nonillions of th' land application 1 �a
(including but not limited to items '1.l`1 below) issued by the division of Waits duality.
l�l Yes
If no pleads, pruritic a written tt4vet 1pli+►n why the facility was ► of compliant, the dates, and explain corrective
nctibii taken.
1) Only residuals nppirived (cat this pet out were applied to the peimitied mti.4
2) Sail pis was adjusted ns sped led in the permit anti hum was applied (it needed) to achieve, a soil pis of at lea°•t 6 0 or
the limit specified in the permit.
3) Annual soils analysis weie,performed on each site receiving residuals dump, the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual Tay analysis (if required) was performed and three (3) copies of certified laboratory results at and three
5) All other monitonng was performed in accordance with the permit and reported during the year as required
(3) copies of certified laboratory results are attached. or the Pollutant
6) The facility did not exceed any of the Pollutant Concentration Limits in 15ANCAC 02T .1105(a)
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities). (applicable to 40 CPR Part
8) All monitoring and reporting requirements in 15ANCAC 02T .1111 were complied with
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of Tay knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature of Prcparer*
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Date

ANNUAL LAND APPLICATION CERTIFICATION FORM
SOUTHWEST PLANTATION
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. r❑ Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil p1I was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual'I'CLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the pen -rut were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. 1 am : ware that there are significant penalties for submitting false information, including the
possibility of 4 d imprisonment for knowing violations."
Signatur- .f' =parer* ate
(if diff nt from Permittee)
* Pre.: er is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF WALLACE
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. p Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 I) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
V r6,,za 2- !o-2022-
Signature of Preparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL LAND APPLICATION CERTIFICATION FORM
TOWN OF WARSAW
Part B - Annual Comniance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
c9-/1' 2z
Signattrt'e of Pfeparer* Date
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)

ANNUAL RESIDUAL SAMPLING SUMMARY FORMS

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
WQ0030998
Triple S Farms & Cleaning
NC0026018
Town of Beulaville WWTP
Laboratory: 1) Environmental Chemists
2)
3)
4)
5)
Parameter
(mg kg)
Conc.
Limit
(mpg)
Sample or Composite Date
sr_4i2o21
Percent Solids (%)
NA
1.23
Arsenic
75
<30.8
Cadmium
85
<30.8
Copper
4,300
657.00
Chromium
NA
35.40
Lead
840
44.40
Mercury
57
1.80
Molybdenum
75
<30.8
Nickel
420
<30.8
Selenium
100
<30.8
Zinc
7,500
1,930.00
Total Phosphorus
NA
19,500
TKN
NA
54,600
Ammonia -Nitrogen
NA
455
Nitrate and Nitrite
NA
3
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
WQ0023178
Town of Clayton
NC0025453
Little Creek Water Reclamation Facility
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
n alYYaa naaaajuau avwaa.
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite Date
1 / 12/2021
5/20/2021
7/22/2021
,
10/21/2021
Percent Solids (%)
NA
1.65
1.93
1.70
1.97
Arsenic
75
<29.40
<26.30
_
<29 40
<25.00
Cadmium
85
<5.88
<5.26
<5.88
<5.00
Copper
4,300
258.00
168.00
219.00
206.00
Chromium
NA
36.60
18.30
21.20
22.60
Lead
840
<17.60
<15.80
<17.6
<15.00
Mercury
57
<0.882
<0.821
<0.900
<0.720
Molybdenum
75
<14.7
<13.20
'14 70
<12.50
Nickel
420
22 20
15.10
<14.70
<12.50
Selenium
100
<29.4
<26.3
<29.4
<25.00
Zinc
7,500
982.00
507.00
735.00
790.00
Total Phosphorus
NA
53,600
29,400
35,100
34,000
TKN
NA
95.900
76,300
80,000
97,500
Ammonia -Nitrogen
NA
3,600
12,600
6,880
9.150
Nitrate and Nitrite
NA
1,990
<256A0
3.650
755
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there arc significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
William Simpson ON"="""� ""w"
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and l 5A NCAC 2T .1102 (26)
Datc
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to he analyzed. 7 he parameters tan he reported in FORM
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
VYWTP Name:
Residual. Analysis Data
Parameter
(rnglkg)
Pea cut Solids (%)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
WQ0030998
Laboratory: l) Err. rrarmrnentai C:l 1st
Triple S Farms & Cleaning 2)
NC0036668
3)
4)
Town of Kenansville W'W'IP 5)
Conc. Sample or Composite Date
Limit
(mg/klg)
NA
75
85
4,300
NA
PAO
57
75
420
6/2/2021
1.08
<44.1
<44.1
522.00
<44.1
<4-4.1
<1.59
<44.1
<44.1
Selenium
Zinc
Total Phosphorus
TKN
100
<44.1
7,500
Ammonia -Nitrogen
Nitrate and Nitrite
f _
NA
795.00
10,100
NA
NA
NA
43,500
1,100
"I certify, under penalty of law, that this document was prepared under my direction or super%°ision in accordance nab a stets designed
to assure that qualified personnel properly gathered and evaluated the information subinitted. 1 atn IPA are that there are significant
penalties far submitting false information, including the possibility of fines and imprisonment for knowing, Niulatiaus,"
Signature of Prep rer''
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC: 2 i' .1102 (26)
Date
DENR FORs,i RSSF (12t2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
WQ0030998
Triple S Farms & Cleaning
W Q0029601
Southwest Plantation WWTP
Laboratory: 1) Environmental Chemists
2)
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
(mg/kg)
Sample or Composite Date
'/17/2021
,
Percent Solids (%)
NA
1.28
_
Arsenic
75
20.70
Cadmium
85
<19.4
Copper
4,300
130.00
Chromium
NA
19.60
Lead
840
<19.4
Mercury
57
<1.31
Molybdenum
75
<19.4
Nickel
420
<19.4
Selenium
100
<19.4
Zinc
7,500
1,010.00
Total Phosphorus
NA
12,600
TKN
NA
38,100
Ammonia -Nitrogen
NA
2,420
Nitrate and Nitrite
NA
15
"I certify, under pen of law that this document was prepared under my direction or supervision in accordance with a system designed
to assure that q
nnel properly gathered and evaluated the information submitted. I am aware that there a
Signature ,. Preparer
•Preparer is defined in 40 CFR Pa 03.9(r) and 15A NCAC 2T 1 102 (26)
'Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
WQ0030998
Triple S Farms & Cleaning
NC0003450
Town of Wallace Regional WWTP
Laboratory: 1) Environmental Chemists, Inc.
2)
3)
4)
i(Csluuau tlivalral.7 LJilt&
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite Date
1/22/2021
4/19/2021
7/21/2021
10/4/2021
Percent Solids (%)
NA
1.80
2.71
2.09
2.71
Arsenic
75
38.10
22.00
<35.7
<18.1
Cadmium
85
<27.2
<19.9
<35.7
<18.1
Copper
4,300
783.00
601.00
722.00
775.00
Chromium
NA
35.70
28.00
<35.7
28.20
Lead
840
51.30
38.00
39.60
35.80
Mercury
57
2.23
2.84
1.33
1.00
Molybdenum
75
<27.2
<19.9
<35.7
<18.1
Nickel
420
<27.2
<19.9
<35.7
19.30
Selenium
100
<27.2
<19.9
<35.7
<18.1
Zinc
7,500
1320.00
1070.00
_
1390.00
1410.00
Total Phosphorus
NA
27,500
25,400
23,300
21,600
TKN
NA
48,600
53,800
61,800
49,500
Ammonia -Nitrogen
NA
841
2,050
6,570
2,160
Nitrate and Nitrite
NA
2,050
4
1,760
11
,
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
peznties for submitting false information, including the possibility of fines and imprisonment for knowing violations. "
9
Signature of Preparer
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
f-1D-2f?c'.Z.
G
Date
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
WQ003 0998
Triple S Farms & Cleaning
NC0021903
Town of Warsaw WWTP
Laboratory: 1) Environmental Chemists
2)
3)
4)
5)
ffliAMLILILWILL r aaakyaaa 11Jraa.a
Parameter
(mg/kg)
Conc.
Limit
(mpg)
Sample or Composite Date
8/31/2021
Percent Solids (%)
NA
2.47
Arsenic
75
<13.4
Cadmium
85
<13.4
Copper
4,300
249.00
Chromium
NA
20.60
Lead
840
25.10
Mercury
57
0.76
Molybdenum
75
<13.4
Nickel
420
<13.4
Selenium
100
<13.4
Zinc
7,500
721.00
Total Phosphorus
NA
12,900
TKN
NA
27,800
Ammonia -Nitrogen
NA
907
Nitrate and Nitrite
NA
4,820
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
pen 'es for'tting false information, including the possibility of fines and imprisonment for knowing violations."
Signature o Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T .1102 (26)
Date
DENR FORM RSSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORMS

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Triple S Farms Total Dry Tons Applied (Annual):
WQ0030998 Cation Exchange Capacity (non 503 only):
Eric Smith Owner: Eric Smith Predominant Soil Series NoA
188.57
n/a
34.2 Acres Permitted: 34.2 Site #: 1 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
SWP 2021 3-21 :1-013-0004 WL1-2021-(BL2021-14WL2-2021 C3-21-207•WL3-2021-C4-21295-SWP2021:C4-21-295 KV2021-01BL202l-
Sample
or Com-
posite
Date
2/17/21
1/12/21
1/22/21
8/24/21
4/19/21
7/22/21
7/21/21
10/21/21
2/17/21
10/21/21
6/2/21
8/24/21
% Solids
1.28
1.65
1.80
1.23
2.71
1.70
2.09
1.97
1.28
1.97
1.08
1.23
Arsenic
20.70
29.40
38.10
30.80
22.00
29.40
35.70
25.00
20.70
25.00
44.10
30.80
Cadmium
19.40
5.88
27.20
30.80
19.90
5.88
35.70
5.00
19.40
5.00
44.10
30.80
Chromium
19.60
36.60
35.70
35.40
28.00
21.20
35.70
22.60
19.60
22.60
44.10
35.40
Copper
130.00
258.00
783.00
657.00
601.00
_
219.00
722.00
206.00
130.00
206.00
522.00
657.00
Lead
19.40
17.60
51.30
44.40
38.00
17.60
39.60
15.00
19.40
15.00
44.10
44.40
Mercury
1.31
0.88
2.23
1.80
2.84
0.90
1.33
0.72
1.31
0.72
0.00
1.80
Molyb-
denum
19.40
14.70
27.20
30.80
19.90
14.70
35.70
12.50
19.40
12.50
44.10
30.80
Nickel
19.40
22.20
27.20
30.80
19.90
14.70
35.70
12.50
19.40
12.50
44.10
30.80
Selenium
19.40
29.40
27.20
30.80
19.90
29.40
35.70
25.00
19.40
25.00
44.10
30.80
Zinc
1010.00
982.00
1320.00
1930.00
1070.00
735.00
1390.00
790.00
1010.00
790.00
795.00
1930.00
Total
Phos-
phorus
12,600
53,600
27,500
19,500
25,400
35,100
23,300
34,000
12,600
34,000
10,100
19,500
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total DT/Ac./
Yr./Application
Event
0.04
0.57
1.16
0.12
0.81
0.73
0.46
0.85
0.02
0.55
0.09
0.12
y
°g
F
Arsenic
0.00
0.03
0.09
0.01
0.04
0.04
0.03
0.04
0.00
0.03
0.01
0.01
0.33
Cadmium
0.00
0.01
0.06
0.01
0.03
0.01
0.03
0.01
0.00
0.01
0.01
0.01
0.18
Chromiutr
0.00
0.04
0.08
0.01
0.05
0.03
0.03
0.04
0.00
0.02
0.01
0.01
0.32
Copper
0.01
0.29
1.81
0.16
0.98
0.32
0.66
0.35
0.00
0.23
0.09
0.16
5.07
Lead
0.00
0.02
0.12
0.01
0.06
0.03
0.04
0.03
0.00
0.02
0.01
0.01
0.34
Mercury
0.00
0.00
0.01
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.02
Molyb-
denum
0.00
0.02
0.06
0.01
0.03
0.02
0.03
0.02
0.00
0.01
0.01
0.01
0.23
Nickel
0.00
0.03
0.06
0.01
0.03
0.02
0.03
0.02
0.00
0.01
0.01
0.01
0.23
Selenium
0.00
0.03
0.06
0.01
0.03
0.04 _
0.03
0.04
0.00
0.03
0.01
0.01
0.30
Zinc
0.08
1.11
3.06
0.46
1.74
_
1.08
1.28
1.35
0.04
0.87
0.14
0.46
11.66
Total
Phos-
phorus
0.94
60.75
63.74
4.68
41.29
51.44
21.38
58.00
0.47
37.25
1.76
4.68
346.37
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
inng the possib)Jity of fines and imprisonment for knowing violations"
c
LY/
Signature of Land Applier
Author Daryl D. Merritt
D.te DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Triple S Farms Total Dry Tons Applied (Annual):
WQ0030998 Cation Exchange Capacity (non 503 only):
Eric Smith Owner: Eric Smith Predominant Soil Series FoA
36.40
n/a
8.48 Acres Permitted: 8.48 Site #: 1 Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C 1-21-013-0004 2021-15014 WL2-20214 WL 3-2021 C 3-21-207-
Sample
or Com-
posite
Date
1/12/21
8/31/21
4/19/21
7/21/21
7/22/21
% Solids
1.65
2.47
2.71
2.09
1.70
Arsenic
29.40
13.40
22.00
35.70
29.40
Cadmium
5.88
13.40
19.90
35.70
5.88
Chromium
36.60
20.60
28.00
35.70
21.20
Copper
258.00
249.00
601.00
722.00
219.00
Lead
17.60
25.10
38.00
39.60
17.60
Mercury
0.88
0.76
2.84
1.33
0.90
Molyb-
denum
14.70
13.40
19.90
35.70
14.70
Nickel
22.20
13.40
19.90
35.70
14.70
Selenium
29.40
13.40
19.90
35.70
29.40
Zinc
982.00
721.00
1070.00
1390.00
735.00
Total
Phos-
phorus
53,600
12,900
25,400
23,300
35,100
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total DT/Ac./
Yr./Application
Event
0.73
0.43
1.84
0.49
0.80
Totals:
Arsenic
0.04
0.01
0.08
0.04
0.05
0.22
Cadmium
0.01
0.01
0.07
0.04
0.01
0.14
Chromium
0.05
0.02
0.10
0.04
0.03
0.24
Copper
0.38
0.21
2.21
0.71
0.35
3.86
Lead
0.03
0.02
0.14
0.04
0.03
0.25
Mercury
0.00
0.00
0.01
0.00
0.00
0.02
Molyb-
denum
0.02
0.01
0.07
0.04
0.02
0.16
Nickel
0.03
0.01
0.07
0.04
0.02
0.18
Selenium
0.04
0.01
0.07
0.04
0.05
0.21
Zinc
1.44
0.61
3.94
1.37
_
1.18
8.54
Total
Phos-
phorus
78.51
10.97
93.42
22.99
56.34
262.22
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the
ossibiliy of fines and imprisonment for knowing violations"
k
-'Cc
e
a_
Signature of Land Applier Author Daryl D. Merritt
t
DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 51.78
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 13.73 Acres Permitted: 13.73 Site #: 1 Field #: 3A
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
WR 2021-15014 2021-06258 SWP 2021 3 C 2-21-144 C 3 21-207- WL 3-2021 C 4-21-295-
Sample
or Com-
posite
Date
8/31/21
4/19/21
2/17/21
5/20/21
7/22/21
7/21/21
10/21/21
% Solids
2.47
2.71
1.28
1.93
1.70
2.09
1.97
Arsenic
13.40
22.00
20.70
26.30
29.40
35.70
25.00
Cadmium
13.40
19.90
19.40
5.26
5.88
35.70
5.00
Chromium
20.60
28.00
19.60
18.30
21.20
35.70
22.60
Copper
249.00
601.00
130.00
168.00
219.00
722.00
206.00
Lead
25.10
38.00
19.40
15.80
17.60
39.60
15.00
Mercury
0.76
2.84
1.31
0.82
0.90
1.33
0.72
Molyb-
denum
13.40
19.90
19.40
13.20
14.70
35.70
12.50
Nickel
13.40
19.90
19.40
15.10
14.70
35.70
12.50
Selenium
13.40
19.90
19.40
26.30
29.40
35.70
25.00
Zinc
721.00
1070.00
1010.00
507.00
735.00
1390.00
790.00
Total
Phos-
phorus
12,900
25,400
12,600
29,400
35,100
23,300
34,000
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total DT/AcJ
YrJApplication
Event
0.43
1.04
0.05
0.21
1.02
0.38
0.65
H
g
H
Arsenic
0.01
0.05
0.00
0.01
0.06
0.03
0.03
0.19
Cadmium
0.01
0.04
0.00
0.00
0.01
0.03
0.01
0.10
Chromium
0.02
0.06
0.00
0.01
0.04
0.03
0.03
0.18
Copper
0.21
1.25
0.01
0.07
0.45
0.55
0.27
2.81
Lead
0.02
0.08
0.00
0.01
0.04
0.03
0.02
0.19
Mercury
0.00
0.01
0.00
0.00
0.00
0.00
0.00
0.01
Molyb-
denum
0.01
0.04
0.00
0.01
0.03
0.03
0.02
0.13
Nickel
0.01
0.04
0.00
0.01
0.03
0.03
0.02
0.13
Selenium
0.01
0.04
0.00
0.01
0.06
0.03
0.03
0.19
Zinc
0.62
2.22
0.09
0.21
1.50
1.06
1.02
6.73
Total
Phos-
phorus
11.03
52.68
1.18
12.41
71.72
17.75
43.96
210.73
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
Including the ossibiljy of fines and imprisonment for knowing violations"
Signature of Land Applier
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)

Triple S Farms Total Dry Tons Applied (Annual): 33.79
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only):
Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 7.27 Acres Permitted: 7.27 Site #: 1 Field #: 3B
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Operator:
n/a
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C 1-21-013-00042021-15014 WR2021-1
Sample
or Com-
posite
Date
1/12/21
8/31/21
8/31/21
% Solids
1.65
2.47
2.47
Arsenic
29.40
13.40
13.40
Cadmium
5.88
13.40
13.40
Chromium
36.60
20.60
20.60
Copper
258.00
249.00
249.00
Lead
17.60
25.10
25.10
Mercury
0.88
0.76
0.76
Molyb-
denum
14.70
13.40
13.40
Nickel
22.20
13.40
13.40
Selenium
29.40
13.40
13.40
Zinc
982.00
721.00
721.00
Total
Phos-
phorus
53,600
12,900
12,900
nual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total DT/AcJ
YrJApplication
Event
1.35
2.24
1.06
H
m
1A
Arsenic
0.08
0.06
0.03
0.17
Cadmium
0.02
0.06
0.03
0.10
Chromium
0.10
0.09
0.04
0.23
Copper
0.69
1.11
0.53
2.34
Lead
0.05
0.11
0.05
0.21
Mercury
0.00
0.00
0.00
0.01
d nlmn
0.04
0.06
0.03
0.13
Nickel
0.06
0.06
0.03
0.15
Selenium
0.08
0.06
0.03
0.17
Zinc
2.64
3.23
1.53
7.40
Total
Phos-
phorus
144.33
57.75
27.41
229.50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the p sibof fines and imprisonment for knowing violations"
Signature of Land Applier
Author Daryl D. Merritt
ate DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 11.76
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 4.14 Acres Permitted: 4.14 Site #: 1 Field #:
4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C 1-21-013-0004:1-013-0004 WR2021-15
Sample
or Cotn-
posite
Date
1/12/21
1/12/21
8/31/21
% Solids
1.65
1.65
2.47
Arsenic
29.40
29.40
13.40
Cadmium
5.88
5.88
13.40
Chromium
36.60
36.60
20.60
Copper
258.00
258.00
249.00
Lead
17.60
17.60
25.10
Mercury
0.88
0.88
0.76
Motyb-
denum
14.70
14.70
13.40
Nickel
22.20
22.20
13.40
Selenium
29.40
29.40
13.40
Zinc
982.00
982.00
721.00
Total
Phos-
phorus
53,600
53,600
12,900
nual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total DT/AcJ
YrJApplication
Event
1.85
0.49
0.50
y
o
m
N
Arsenic
0.11
0.03
0.01
0.15
Cadmium
0.02
0.01
0.01
0.04
Chromium
0.14
0.04
0.02
0.19
Copper
0.95
0.26
0.25
1.46
Lead
0.07
0.02
0.02
0.11
Mercury
0.00
0.00
0.00
0.00
Molyb-
denum
0.05
0.01
0.01
0.08
Nickel
0.08
0.02
0.01
0.12
Selenium
0.11
0.03
0.01
0.15
Zinc
3.63
0.97
0.72
5.32
Total
Phos-
phorus
198.22
53.02
12.84
264.07
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
ing thee ossib 'ty of fines and imprisonment for knowing violations"
Signature of Land Applier
Author Daryl D. Merritt
Date DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 33.50
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Srnith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 11.2 Acres Permitted: 11.2 Site #: 1 Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C 1-21-013-0004:1-013-0004 C 2-21-144 (WR 2021-I
Sample
or Com-
posite
Date
1/12/21
1/12/21
5/20/21
8/31/21
% Solids
1.65
1.65
1.93
2.47
Arsenic
29.40
29.40
26.30
13.40
Cadmium
5.88
5.88
5.26
13.40
Chromium
36.60
36.60
18.30
20.60
Copper
258.00
258.00
168.00
249.00
Lead
17.60
17.60
15.80
25.10
Mercury
0.88
0.88
0.82
0.76
Molyb-
denum
14.70
14.70
13.20
13.40
Nickel
22.20
22.20
15.10
13.40
Selenium
29.40
29.40
26.30
13.40
.
Zinc
982.00
982.00
507.00
721.00
Total
Phos-
phorus
53,600
53,600
29,400
12,900
ual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total DT/Ac./
Yr./Application
Event
1.14
0.79
0.56
0.51
0
a
N
Arsenic
0.07
0.05
0.03
0.01
0.16
Cadmium
0.01
0.01
0.01
0.01
0.04
Chromium
0.08
0.06
0.02
0.02
0.18
Copper
0.59
0.41
0.19
0.25
1.43
Lead
0.04
0.03
0.02
0.03
0.11
Mercury
0.00
0.00
0.00
0.00
0.01
Molyb-
denum
0.03
0.02
0.01
0.01
0.08
Nickel
0.05
0.03
0.02
0.01
0.12
Selenium
0.07
0.05
0.03
0.01
0.16
Zinc
2.24
1.54
0.57
0.73
5.08
Total
Phos-
phorus
122.07
84.19
33.01
13.05
252.32
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the Qossib of fines and imprisonment for knowing violations"
Signature of Land Applier
Author Daryl D. Merritt
Ddte DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted In Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 87.59
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only): n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soil Series FoA
Acres Used: 14.5 Acres Permitted: 14.5 Site #: 1 Field #: 7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C 1-21-013-0004:1-144-0002 WL22021-1W1 32021•W
420Z1
5...
!sill LoalltnSs
o . - - ---- - -�
Total DTIAcJ
Yr./Application
Event
0.72
0.07
1.82
1.19
2.24
Totals:
Arsenic
0.04
0.00
0.08
0.08
0.08
0.29
Cadmium
0.01
0.00
0.07
0.08
0.08
0.25
Chromium
0.05
0.00
0.10
0.08
0.13
0.37
Copper
0.37
0.02
2.19
1.72
3.48
7.78
Lead
0.03
0.00
0.14
0.09
0.16
0.42
Mercury
0.00
0.00
0.01
0.00
0.00
0.02
Molyb-
denum
0.02
0.00
0.07
0.08
0.08
0.26
Nickel
0.03
0.00
0.07
0.08
0.09
0.28
Selenium
0.04
0.00
0.07
0.08
0.08
0.28
Zinc
1.41
0.07
3.90
3.31
6.33
15.01
Total
Phos-
phorus
76.73
3.92
92.64
55.46
96.96
325.72
n
I cer6t
y, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the p sibili of fines and imprisonment for knowing violations"
Signature of Land Applier Author Daryl D. Merritt
Da e
DENR FORM MFLSF (7/2002)

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Triple S Farms Total Dry Tons Applied (Annual): 36.59
Permit #: WQ0030998 Cation Exchange Capacity (non 503 only):
n/a
Operator: Eric Smith Owner: Eric Smith Predominant Soh Series GoA
Acres Used: 8.93 Acres Permitted: 8.93 Site #: 1 Field #: 9
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
C 1-21-013-0004:1-144-0002 BL2021-14'WL2-2021 C321207C421295
Sample
or Com-
posite
Date
I/12/21
5/20/21
8/24/21
4/19/21
7/22/21
10/21/21
% Solids
1.65
1.93
1.23
2.71
1.70
1.97
Arsenic
29.40
26.30
30.80
22.00
29.40
25.00
Cadmium
5.88
5.26
30.80
19.90
5.88
5.00
Chromium
36.60
18.30
35.40
28.00
21.20
22.60
Copper
258.00
168.00
657.00
601.00
219.00
206.00
Lead
17.60
15.80
44.40
38.00
17.60
15.00
Mercury
0.88
0.82
1.80
2.84
0.90
0.72
Molyb-
denum
14.70
13.20
30.80
19.90
14.70
12.50
Nickel
22.20
15.10
30.80
19.90
14.70
12.50
Selenium
29.40
26.30
30.80
19.90
29.40
25.00
Zinc
982.00
507.00
1930.00
1070.00
735.00
790.00
Total
Phos-
phorus
53,600
29,400
19,500
25,400
35,100
34,000
nual Heavy Metal Field Loadings (Calculated in Ibs/ac
Total DT/Ac./
Yr./Application
Event
0.23
0.11
0.46
2.51
0.57
0.22
0
Ea-
.
••
Arsenic
0.01
0.01
0.03
0.11
0.03
0.01
0.20
Cadmium
0.00
0.00
0.03
0.10
0.01
0.00
0.14
Chromium
0.02
0.00
0.03
0.14
0.02
0.01
0.23
Copper
0.12
0.04
0.60
3.01
0.25
0.09
4.11
Lead
0.01
0.00
0.04
0.19
0.02
0.01
0.27
Mercury
0.00
0.00
0.00
0.01
0.00
0.00
0.02
Molyb-
denum
0,01
0.00
0.03
0.10
0.02
0.01
0.16
Nickel
0.01
0.00
0.03
0.10
0.02
0.01
0.16
Selenium
0.01
0.01
0.03
0.10
0.03
0.01
0.19
Zinc
0.45
0.11
1.77
5.36
0.84
0.35
8.89
Total
Phos-
phorus
24.80
6.36
17.92
127.29
40.12
15.01
231.50
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including theossib)1Ity of fines and imprisonment for knowing violations"
_A- LC_
Signature of Land Applier
Author Daryl 0. Merritt
Date DENR FORM MFLSF (7/2002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac) Nutrients (lbs/ac)
As — Arsenic
Cd — Cadmium
Cr — Chromium
Cu — Copper
Pb — Lead
Hg — Mercury
Mo — Molybdenum
Ni — Nickel
Se — Selenium
Zn — Zinc
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.

Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: WQ0030998 Field #:
Owner: Eric Smith nnual Dry Tons Applied: 188.57 Site #: 1
Predominat Soil Series
Crop I Max PAN: 299.00
Eric Smith
Crop 1 Name:
Bermudngrass
NoA
Crop 2 Name:
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
wheat • Crop 2 Max. PAN
34.20
34.20
NA
50.00
IDate or
Month
Specify
% Solids
Decimal
Volume
Applied per
Acre
(DT/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,(DIY
Cond.
et,
Moist)
Pt ecip.
Past 24m
Hrs.
kicks
b
a m
, o
'
2
_
+ i
=
*
0'
TKN
Infikg
z
dr
o
co
metke
Nitrite
and
Nitrite
MAE
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop
2
Gal.
Cu.Yd.
Totals
Report
Totalsetc.)
in Gal.
Per Acre
Crop 1
Crop 2
Crop 1
Crop 2
Mar-21
24,000
702
1.28
0.04
Southwest Floatation
S
0.50
030
38,100
2,420
,
15
0.89
X
Mar-21
281,686
8,236
1.65
0.57
Clayton Little Creek WRF
IN
1.00
030
95,900
3,600
1,990
37.72
X
Mar-21
528,000
15,439
1.80
1.16
Wallace WWrP
INC
1.00
030
48,600
841
2,050
39.91
X
Mar-21
80,000
2,339
1.23
0.12
Bentavrlle WWII'
S
0.50
030
54,600
455
3
3.95
X
Apr-21
246,000
7,193
2.71
0.81
WallaceWWTP
INC
1.00
0.30
53,800
2,050
4
28.58
X
Jul-21
353.500
10,336
1.70
0.73
Clayton tittle Creek WRF
IN
1.00
0.30
80,000
6,880
3,650
47.58
X
Aug-21
180,000
5,263
2.09
0.46
WelmceWWTP
INC
1.00
0.30
61,800
6,570
1,760
22.84
X
Oct-21
355,080
10,382
1.97
0.85
Clayton Little Creek WRF
IN
1.00
0.30
97,500
9,150
755
62.11
X
Oct-21
12,000
351
1.28
0.02
Southwest Plantation
S
0.50
0.30
38,100
2,420
15
0.45
X
Nov-21
228,080
6,669
1.97
0.55
Clayton Little Creek WRF
IN
1.00
0.30
97,500
9,150
755
39.89
X
Nov-2I
66,000
1,930
1.08
0.09
Keaansvilk WWII'
S
0.50
0.30
43,500
1,100
2,890
2.81
X
Nov-21
80,000
2,339
1.23
0.12
Beulnae WWrP
S
0.50
0.30
54,600
455
3
3.95
X
TOTALS:
71,180
. - ..
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annual lbs/acre
0.33
0.18
0.32
5.07
0.34
0.02
0.23
0.23
030
11.66
346.37
243.58
47.10
Date
lbs/ac
Current Cumulative lbs/acre
1.27
1.01
NA
52.68
4.79
0.10
NA
I.87
1.34
107.86
Prior Years Cumulative lbs/acre
0.94
0.83
NA
47.62
4.46
0.09
NA
1.64
1.04
96.21
Permitted C. P. L. R.****
36
34
NA
1,338
267
15
NA
374
89
2,498
. •
Permit PAN Limit lst/2nd Crop50.00-
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN- Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 03, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: WQ0030998 Field #: 1
Owner: Eric Smith nnual Dry Tons Applied: 36.40 Site #: 2
Operator: Eric Smith Predominat Soil Series
Crop 1 Max PAN: 276.00
Crop 1 Name:
Betmndagrass
FoA
Crop 2 Name:
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
Wheat Crop 2 Max. PAN
8.48
8.48
NA
50.00
Date or
Month
SpecifySite
°h Solids
Decimal
Volume
Applied per
Acre
(DT/Ac)
Residual Sources
(NPDES #, WQ#,
Fat., Animal Waste,
etc.)
Cond.
(DTY'
Moist)
Precip.
P
Past 24
Hrs.
Inches
Appli-cation
Method•
g
m .1
:
5
r g
*
='
TKN
fit;
z
5
g L.
Nitrate
and
Nitrite
MAR
PAN A lied
Applied
(lbs/acre)
Must Select
Crop ! or Crop
2
Gal.
Cu.Yd.
Totals
Report
Totals
in Gal.
Per Acre
Crop1
Crop2
1
CropCrop
2
Jan-21
90,260
10,644
1.65
0.73
Clayton tank Creek WBF
IN
1.00
0.30
95,900
3,600
1,990
48.75
X
Mar-21
35,000
4,127
2.47
0.43
Warsaw WW1?
S
0.50
0.30
27,800
907
4,820
11.34
X
Apr-2I
138,000
16,274
2.71
1.84
Wallace WWII'
INC
1.00
0.30
53,800
2,050
4
64.66
X
Sep-21
48,000
5,660
2.09
0.49
WaltaceWWTP
INC
1.00
0.30
61,800
6,570
1,760
24.57
X
Sep-21
96,000
11,321
1.70
0.80
Clayton tattle Creek wRF
IN
1.00
0.30
80,000
6,880
3,650
52.11
X
TOTALS:
48,026
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annual lbs/acre
0.22
0.14
0.24
3.86
0.25
0.02
0.I6
0.18
0.21
8.54
262.22
152.68
48.75
Date
lbs/ac
Current Cumulative lbs/acre
1.16
0.94
NA
44.42
4.15
0.11
NA
1.68
1.17
87.31 -:
Prior Years Cumulative lbs/acre
0.94
0.80
NA
40.56
3.89
0.09
NA
1.50
0.96
78.77
Permitted C. P. L. R.****
36
34
NA
1,338
267
15
NA
374
89
2,498 ::
0'
Permit PAN Limit t stand Crop276
K
6 50.00
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Facility Name:
Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
WQ Perrnit #: W00030998 Field #: 1
Site #: 3A
Triple S Farms
Eric Smith
.nnual Dry Tons Applied: 51.78
Eric Smith
Crop 1 Name:
Bennudagrass
Predominat Soil Series
Crop 1 Max PAN: 276.00
FoA
Crop 2 Name:
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
Wheat (Grain) Crop 2 Max. PAN
13.73
13.73
NA
50.00
IDate or
Month
Specify
%Solids
As
Decimal
Volume
Applied per
Acre
(DT/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)•
Cad
(Dry,
Wet,
Moist)
Prccip.
Past 24
Hrs.
inches
Appli-cation
Method*
2
11'
*• m
=
xi 3
e r,
: m
5-
o'
TKN
Ammonia
Nitrogen
Nitrate
and
Nitrite
PAN Applied
(lbs/acre)
Must Select
Crop1 or Crop
2
Gal.
Cu.Yd.
Totals
Report
Totals
in Gal.
Per Acre
Crop1
Crop2
Crop1Crop
2
Mar-21
57,000
4,151
2.47
0.43
Warsaw WW1?
S
-
0.50
0.30
27,800
907
4,820
11.41
X
Apr-21
126,000
9,177
2.71
1.04
Wallace WWrP
INC
1.00
0.30
53,800
2,050
4
36.46
X
May-21
12,000
874
1.28
0.05
Scu hwest Plantation
S
0.50
0.30
-38,100
2,420
15
1.11
X
Jun-21
36,000
2,622
1.93
0.21
Clayton Link Creek WRF
IN
1.00
0.30
76,300
12,600
256
13.49
X
Jul-21
197,880
14,412
1.70
' 1.02
Clayton Link Creak WRF
IN
1.00
030
80,000
6,880
3,650
66.34
X
Aug-21
60,000
4,370
2.09
0.38
Wallace WWTP
INC
1.00
0.30
61,800
6,570
1,760
18.97
X
Nov-21
108,050
7,870
1.97
0.65
Clayton blue Creek WRF
IN
1.00
0.30
97,500
9,150
755
47.08
X
TOTALS:
43,476
•: _ ::;:;::';:.
As
Cd
Cr
Cu
Pb ,
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annual lbs/acre
0.19
0.10
0.18
2.81
0.19
0.01
0.13
0.13
0.19
6.73
210.73
147.78
47.08
Date
Ibs/ac
Current Cumulative lbs/acre
0.70
0.48
NA
22.73
1.93
0.06
NA
0.83
0.73
47.71
2 7 6
Prior Years Cumulative lbs/acre
0.51
0.38
NA
19.92
1.74
0.05
NA
0.70
0.55
40.98
Permitted C. P. L. R.****
36
34
NA
1,338
267
15
NA
374
89
2,498
Permit PAN Limit lst/2nd Crop"
:... 2 6
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: WQ0030998 Field #: 1 Acres Utilized: 7.27
Owner: Eric Smith nnual Dry Tons Applied: 33.79 Site #: 3B Acres Permitted: 7.27
Operator:
Eric Smith
Crop 1 Name:
Fescue (Hay)
Predominat Soil Series FoA Cation Exchange Capacity (non 503):
Crop 1 Max PAN: 184.00 Crop 2 Name: #NrA Crop 2 Max. PAN
NA
#N/A
Date or
Month
Specify
Solids
As
Decimal
Volume
Applied per
Acre
(DT/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)
Site
Cond.
(�
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
Appli-cation
Method*
Volitila-zation
Rate**
!Mineral -nation
Rate***
TKN
me/ks
Anunonia
Nitrogen
Nitrate
and
Nitrite
me/kc
PAN Applied
bs/acre)
Must Select
Crop 1 or Crop
2
Gal.
Totals
Per Acre
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Jan-21
142,258
19,568
1.65
1.35
Clayton Link Creek WRF
IN
1.00
0.30
95,900
3,600
1,990
89.61
X
Jun-21
158,000
21,733
2.47
2.24
Warsaw WWTP
S
0.50
0.30
27,800
907
4,820
59.73
X
Sep-21
75,000
10,316
2.47
1.06
Warsaw WWTP
S
030
0.30
27,800
907
4,820
28.35
X
TOTALS: _
51,617
.
As
Cd
Cr
Cu
Pb
Hg ,
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annual lbs/acre
0.17
0.10
023
2.34
0.21
0.01
0.13
0.15
0.17
7.40
229.50
177.70
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.68
0.49
NA
22.26
1.95
0.06
NA
0.84
0.71
4839
Prior Years Cumulative lbs/acre
0.51
0.38
NA
19.92
1.74
0.05
NA
0.70
0.55
40.98
Permitted C. P. L. R.****
36
34
NA
1,338
267
15
NA
374
89
2,498
'Permit PAN Limit lst/2nd Crop184
1 #N/A
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Anaeroblcally Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Facility Name:
Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Triple S Farms WQ Permit #: WQ0030998 Field #: 1
nnual Dry Tons Applied: 11.76 Site #: 4
Predominat Soil Series
Crop 1 Max PAN: 184.00
Eric Smith
Eric Smith
Crop 1 Name:
Fescue (Hoy)
FoA
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
4.14
4.14
NA
C7
m
0
= c
''
::::
Specify
Gal.
,
/o Solids
Decimal
Volume
Applied per
Acre
(DT/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
etc.)
Site
Cond.
(Dry,
Wet,
Moist)
Preci p
Past 24
Hrs.
inches
3
E.-
# .
=
-,
0
0
m
% N
t ,�
- - - -
X
�, ,5,'
5. a
#
* go
al'
TKN
,
a
Z 3
i i3
2 E.
_ �.
...■
Nitrate
andCrop
Nitrite
up z. minx.
_
PAN
(lbs/acre)
rAl�l +Hivin
Applied
Must Select
1 or Crop
2
d
Cu.Yd.
Totals
_
Report
Totals
in Gal.
Per Acre
Crop 1
Crop 2
Crop 1
Crop 2
Jan-21
1
1,258
26,874
1.65
1.85
Clayton Little Creek WRF
IN
1.00
0.30
95,900
3,600
1,990
123.07
X
Mar-21
Sep-ZI
29,758
20,000
7,188
1.65
0.49
Clayton tittle creek WBF
IN
1.00
0.30
95,900
3,600
1,990
32.92
X
4,831
2.47
0.50
Warsaw Wwlr
S
0.50
0.30
27,800
907
4,820
13.28
X
TOTALS: _38,893
:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2'
0.00
Lime
Date
Applied
lbs/ac
Annual lbs/acre
0.15
0.04
0.19
1.46
0.11
0.00
0.08
0.12
0.15
5.32
264.07
169.27
Current Cumulative lbs/acre
0.43
0.25
NA
13.36
0.95
0.02
NA
0.74
0.44
39.18 ::
Prior Years Cumulative Ibs/acre
0.28
0.21
NA
11.90
0.85
0.02
NA
0.62
0.29
33.86
Permitted C. P. L. R****
36
34
NA
1,338
267
15
NA
374
89
2,498
..•.... .
Permit PAN Limit 1 st/2nd C'rnr,
184 #N/A
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false Information, including the possibility of fines and imprisonment for knowing violations."
L e
Signature of Land Applier
0- A -
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 03, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Facility Name:
Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Triple S Farms WQ Permit #: WQ0030998 Field #:
nnual Dry Tons Applied: 33.50
Predominat Soil Series
Crop 1 Max PAN: 184.00
Eric Smith
Eric Smith
Crop 1 Name:
Fescue (Hay)
Site #:
FoA
5
Crop 2 Name:
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
1120
1120
NA
red
....... ..sup Hann. 11U' m.in
Date or
Month
Specify
Gal.
°
�0 Solids
Asm
Decimal
Volume
Appliedluper
Acre
_ (DT/Ac)
Residual Sources
(NPDES #. WQ#,
Fed., Animal Waste,
etc.)
SitePrecip.
Cond.
wet,
Moist)
Past 24
Hrs.
hicks
a
3'0.
a _
b
9<
-:
#
a
I.
I.
i
}'r
TKN
z t
o
g m.
mew
Nitrate
and
Nitrite
mom
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop
2
Cu.Yd.
Totals
Totals Report
in Gal.
Per Acre
Crop 1
Crop 2
Crop 1
Crop 2
Jan-21
185,363
16,550
1.65
1.14
Clayton Link Creek WRF
IN
1.00
030
95,900
3,600
1,990
75.79
X
Feb-21
127,835
11.414
1.65
0.79
Clayton Little Creek WRF
S
0.50
0.30
95,900
3,600
1,990
49.44
X
Jun-21
78,120
6,975
1.93
0.56
Clayton Link Creek WRF
IN
1.00
0.30
76,300
12,600
256
35.89
X
Sep-21
55,000
4,911
2.47
0.51
Warsaw wWrr
S
0.50
0.30
27,800
907
4,820
13.50
X
TOTALS: -
39,850 :
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se r
Zn
P
PAN 1
PAN 2
Lime
Applied
Annual lbs/acre
0.16
0.04
0.18
1.43
0.11
0.01
0.08
0.12
0.16
5.08
25232
I74.62
0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.77
0.57
NA
25.25
2.35
0.07
NA
1.04
0.77
50.13
Prior Years Cumulative lbs/acre
0.61
033
NA
23.82
2.24
0.07
NA
0.93
0.61
45.05
Permitted C. P. L. R.****
36
34
NA
1,338
267
15
NA
374
89
2,498
Permit PAN Limit 1st/2nd Crop18
.............:....
( # /
i
rc I certify ender penalty of haw_ that this document was d
preps un er my direction or supervrston m accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: WQ0030998 Field #:
Owner: Eric Smith nnnal Dry Tons Applied: 8759 Site #: 7
Operator:
Eric Smith
Crop 1 Name:
BernardagTass
Acres Utilized:
Acres Permitted:
14.50
14.50
Predominat Soil Series FoA Cation Exchange Capacity (non 503): NA
Crop 1 Max PAN: 276.00 Crop 2 Name:
Wheat Crop 2 Max. PAN
50.00
Date or
Month
Specify
Totals
Per Acre
/ Solids
As
Decimaletc.)
Volume
Applied per
Acre
(DT/Ac)
Residual Bourses
(NPDES #, WQ#,
Fert., Animal Waste,
Site
Cond.
D
( ry'
Wet,
Moist)
Precip.
Past 24
Hrs.
tam
x .
g, _.
o 2
a c
'
<
_ 9.,
ar
w 4
* ..
a
'Mineral -nation
Rate***
TKN
MAX
s ?
o
'�° �.
a
RAC
Nitrate
and
Nitrite
mere
PAN Applied
(1bs/acre)
Must Select
Crop1 or Cr
Crop
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Feb-21
150,850
10,403
1.65
0.72
Clayton torte Cork WRF
IN
1.00
0.30
95,900
3,600
1,990
47.64
X
Jun-21
12,000
828
1.93
0.07
Clayton time Creek WRF
IN
1.00
0.30
76,300
12,600
256
4.26
X
Jun-21
234,000
16,138
2.71
1.82
Wallace Wwrn
INC
1.00
0.30
53,800
2,050
4
64.12
X
Aug-21
198,000
13,655
2.09
1.19
Wallace WWrP
INC
1.00
0.30
61,800
6,570
1,760
59.26
X
Oct-21
288,000
19,862
2.71
2.24
Wallace WWfP
INC
1.00
0.30
49,500
2,160
1 I
73.50
X
TOTALS:
60,886
•
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime
Date
Applied
lbs/ac
Annual lbs/acre
0.29
0.25
0.37
7.78
0.42
0.02
0.26
0.28
0.28
15.01
325.72
201.14
47.64
Current Cumulative lbs/acre
0.66
0.42
NA
15.63
0.93
0.04
NA
0.56
0.58
30.29
Prior Years Cumulative lbs/acre
0.37
0.17
NA
7.84
0.51
0.02
NA
0.28
0.30
15.27
Permitted C. P. L. R.****
36
34
NA
1,338
267
15
NA
374
89
2,498
Permit PAN Limit lst/2nd Crop
.......... ii 2 50.00
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for bmitting false information, including the possibility of fines and imprisonment for knowing violations."
2/011/31-
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volttilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Triple S Farms WQ Permit #: WQ0030998 Field #:
Owner: Eric Smith nnual Dry Tons Applied: 36.59 Site #: 9
Predominat Soil Series
Crop 1 Max PAN: 184.00
Eric Smith
Crop 1 Name:
Fescue (Hoy)
GoA
Crop 2 Name:
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
#N/A Crop 2 Max. PAN
8.93
8.93
NA
#N/A
Date or
Month
Sib'
Totals
Per Acre
/a , Solids
As
Decimal
Volume
Applied per
Acre
(DT/Ae)
Residual Sources
(NPDES #, WQ#,
Fert., Waste,
etc.)
Site
Cond.Precip.
(�y
Wet,
Moist)
Past 24
Hrs.
inches
Appli-cation
Method*
Volitila-zation
Rate**
5
0
* 16...
0
TKN
m
z
ao a
3 m.
mgag
Nitrate
and
Nitrite
e/
meta
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop1
Crop2
Crop1
Crop2
Mar 21
30,024
3,362
1.65
0.23
Clayton Link Creek WRF
IN
1.00
0.30
95,900
3,600
1,990
15.40
X
May-21
12,000
1,344
1.93
all
Clayton Link Cheek WRF
IN
1.00
0.30
76,300
12,600
256
6.91
X
May-21
80,000
8,959
1.23
0.46
seulaville WWTP
S
0.50
0.30
54,600
455
3
15.14
X
Jun-21
198,000
22,172
2.71
2.51
WaUoce WWII'
INC
1.00
0.30
53,800
2,050
4
88.09
X
Sep-21
72,000
8,063
1.70
0.57
Clayrn Link Cnxk WRF
IN
1.00
0.30
80,000
6,880
3,650
37.11
X
Oct-21
24,000
2,688
1.97
0.22
Clayton Little Cheek WRF
IN
1.00
0.30
97,500
9,150
755
16.08
X
TOTALS:
46,587 :
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime
Date
Applied
Ibs/ac
Annual lbs/acre
0.20
0.14
0.23
4.1I
0.27
0.02
0.16
0.16
.
0.19
8.89
231.50
178.73
0.00
Current Cumulative lbs/acre
0.55
0.49
NA
10.08
0.79
0.03
NA
0.52
0.56
23.46
Prior Years Cumulative lbs/acre
0.35
0.35
NA
5.97
0.52
0.02
NA
0.35
0.36
14.57
Permitted C. P. L. R.****
36
34
NA
1,338
267
15
NA
374
89
2,498
Permit PAN Limit 1 st/2nd Crop
184 I
#N/A
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for sub t tting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 03, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

RESIDUAL ANALYSIS LAB SHEETS

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Beulaville
Beulaville WWTP
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
BL 2021-14538
8/24/2021
9/20/2021
Annual 2021
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.230
Nitrogen (TKN)
5.460
54,600.000
Phosphorus
1.950
19,500.000
Potassium
0.503
5,030.000
Sulfur
0.000
0.000
Calcium
2.860
28,600.000
Magnesium
0.254
2,540.000
Sodium
0.689
6,890.000
Iron
---
Aluminum
---
11,500.000
Manganese
---
Copper
---
657.000
1,500
Zinc
---
1,930.000
2,800
Ammonia Nitrogen
0.046
455.000
Nitrate N / Nitrite N
---
2.570
Cadmium
---
30.800
39
Chromium
---
35.400
1,200
Nickel
---
30.800
420
Lead
---
44.400
300
Arsenic
---
30.800
41
Mercury
---
1.800
17
Selenium
---
30.800
100
pH
3.870
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.415
Molybdenum
---
30.800
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wastewater Treatment Plant
Beulaville WWTP
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2021
9/20/2021 Report No: BL 2021-14538
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
32.947
PAN Inj.
33.402
P
39.000
K
10.060
Lime (estimated)
0.000
Secondary Nutrients
Calcium
57.200
Magnesium
5.080
Sodium
13.780
SAR
1.160
Chloride
0.000
Iron
0.000
Alumium
23.000
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
1.23
pH
3.870
Min Rate
0.300
Metals
Arsenic
0.062
Cadmium
0.062
Chromium
0.071
Copper
1.314
Lead
0.089
Mercury
0.004
Molybdenum
0.062
Nickel
0.062
Seleniun
0.062
Zinc
3.860

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Town of Beulaville
PO Box 130
Beulaville NC
Attention: Angie Miller
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Sep 20, 2021
Customer PO #:
28518 Customer ID: 08100015
Report #: 2021-14538
Project ID: Sludge
Lab ID
21-36387
Test
Sample ID:
Site: Sludge
Method
8/24/2021
Collect Date/Time Matrix
Solid/Sludge
Results
Sampled by
Angie Miller
Date Analyzed
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
pH
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 353.2
SM 2540 B
SM 4500 H B
Result estimated ,outside calibration range.Analyzed out of 15 minutes hold time.
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
SM 4500 NH3 C
SM 4500 Org B
SM 4500 P F
SW848 7471B
11500 mg/kg 09/01/2021
<30.8 mg/kg 09/01/2021
<30.8 mg/kg 09/01/2021
28600 mg/kg 09/01/2021
35.4 mg/kg 09/01/2021
657 mg/kg 09/01/2021
44.4 mg/kg 09/01/2021
2540 mg/kg 09/01/2021
<30.8 mg/kg 09/01/2021
<30.8 mg/kg 09/01/2021
5030 mg/kg 09/01/2021
<30.8 mg/kg 09/01/2021
6890 mg/kg 09/01/2021
1930 mg/kg 09/01/2021
2.57 mg/kg 08/27/2021
1.23 % 08/25/2021
3.87 estunits 09/09/2021
455 mg/kg 08/26/2021
54600 mg/kg 08/31/2021
19500 mg/kg 08/29/2021
1.80 mg/kg 09/03/2021
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: . 1-46t-
Report #:: 2021-14538 Page 1 of 1

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
6602 Windmill Way Wilmington, NC 28406
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Town of Beulaville WWTP
PROJECT NAME: WWTP-3/week monitoring
REPORT NO: j tt (r 5
ADDRESS: Post Office Box 130
Permit Number: NC0026018
,(
PO NO:
Beulaville, NC 28518
REPORT TO: Angie Miller/Miller Utility
PHONE/FAX: [phone]
l r
72 11
COPY TO:
email: [e-mail]
Sampled By: ( .
= Intiuent. E = Effluent W =Well ST =Stream SO =Soil SL —
Sample Identification
`Y Collection
a
T
G.
E
h
Composite
or Grab
ma
`o
o d
"
Chlorine
mg/L
d
0
a
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
w
O
Z
-1
U
=
o
tp
_
"
?
_
=
O
$
o
W
W
w
S
o
Inf composite (3/week)
C
P
X
BOD,TSS
G
G
Eff composite (3/week)
C
P
X
BOD,TSS
G
G
Eff composite (3/week)
C
P
X
NH3
G
G
Jan,Apr,Jul,October
C
P
X
Total N (calc), Total P
G
G
(clue quarterly)
C
P
G
G
Eff grab (3/week)
C
P
X
Fecal Coliform
G
G
C
P
N/x.+r;enis -F- we4c, %S
G
G
S kkde.
`j
2411 i
c
P
�d Z. 3.5/
2u�oZl
G
G
Transfer
Relinquished By:
Date/Time
Received By:
DatelTime
1.
Delivered By:
Comments:
ccepted. Rejec Resa R nested:
Received By: Date: 7iI Time: 31.
TU NA OUND:

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms & Cleaning, Inc
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
C 1-21-013-0004
1/12/2021
1/28/2021
1st Quarter
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.65
Nitrogen (TKN)
9.590
95,900.000
Phosphorus
5.360
53,600.000
Potassium
1.390
13,900.000
Sulfur
1.490
14,900.000
Calcium
2.850
28,500.000
Magnesium
0.912
9,120.000
Sodium
0.422
4,220.000
Iron
---
19,600.000
Aluminum
---
25,400.000
Manganese
---
498.000
Copper
---
258.000
1,500
Zinc
---
982.000
2,800
Ammonia Nitrogen
0.360
3,600.000
Nitrate N / Nitrite N
---
1,990.000
Cadmium
---
5.880
39
Chromium
---
36.600
1,200
Nickel
---
22.200
420
Lead
---
17.600
300
Arsenic
---
29.400
41
Mercury
---
0.882
17
Selenium
---
29.400
100
pH
6.000
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
9.230
Molybdenum
---
14.700
75
Chloride
---
Boron
Available P205
Specific Gravity
8.340

Date Reported:
Wastewater Treatment Plant
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
1st Quarter
1/28/2021 Report No: C 1-21-013-0004
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
62.960
PAN Inj.
66.560
P
107.200
K
27.800
Lime (estimated)
0.000
Secondary Nutrients
Calcium
57.000
Magnesium
18.240
Sodium
8.440
SAR
0.713
Chloride
0.000
Iron
39.200
Alumium
50.800
Manganese
0.996
Boron
0.000
Sulfur
29.800
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
Physical Characteristics
% Solids
1.65
pH
6.000
Min Rate
0.300
Metals
Arsenic
0.059
Cadmium
0.012
Chromium
0.073
Copper
0.516
Lead
0.035
Mercury
0.002
Molybdenum
0.029
Nickel
0.044
Seleniun
0.059
Zinc
1.964
2018
2019
2020
2021
0.30
55.38
2022
0.15
19.38
2023
0.08
8.24
2024
0.04
3.81
2025
2026
2027
2028

Waypoint.
ANALYTICAL
1/28/2021
Town Of Clayton
POB 879
Clayton, NC, 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 21-013-0004
Project Description: Holding Tank
Waypoint Analytical Virginia, Inc. received sample(s) on 1/13/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Tawit Gioarer
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

Waypoint...
ANALYTICAL
Report Number: 21-013-0004
Client Project Description: Holding Tank
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
74665 HT #2 Solids 01/12/2021 01/13/2021
74665 HT #2 Solids 01/12/2021 01/13/2021 SM-4500-NH3C WP MTN
74665 HT #2 Solids 01/12/2021 01/13/2021 9045D WP MTN
74665 HT #2 Solids 01/12/2021 01/13/2021 4500NO3F-2011 WP MTN
74665 HT #2 Solids 01/12/2021 01/13/2021 6010D WP MTN
74665 HT #2 Solids 01/12/2021 01/13/2021 SW-7471B WP MTN
74665 HT #2 Solids 01/12/2021 01/13/2021 SM-4500-NH3C-TKN WP MTN
74665 HT #2 Solids 01/12/2021 01/13/2021 SM-2540G WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

Waypoint.
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank
Information :
Report Number : 21-013-0004 REPORT OF ANALYSIS
Lab No : 74665
Sample ID : HT #2
Report Date : 01/28/2021
Received : 01/13/2021
(float✓
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 1/ 12/ 2021 0:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture 98.3 0/0
Test Results Units
0.010
MQL
1 01/14/21 16:11 FMM SM-2540G
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen 3600 mg/Kg - dry 1470 1 01/19/21 15:37 JPJ SM-4500-NH3C
Nitrate+Nitrite-N 1990 mg/Kg - dry 271 1 01/19/21 14:26 ZBD 4500NO3F-2011
Organic N 92400 mg/Kg - dry 14700 1 01/19/21 10:00 CALCULATION
pH 6.0 s.u. 1 01/20/21 15:36 CxC 9045D
Total Solids 1.65 % 0.010 1 01/14/21 16:11 FMM SM-2540G
Total Kjeldahl Nitrogen 95900 mg/Kg - dry 14700 1 01/19/21 10:00 JP] >M-4500-N1-13C-TKP
Phosphorus 53600 mg/Kg - dry 294 1 01/19/21 06:52 TJS 6010D
Aluminum 25400 mg/Kg - dry 294 1 01/19/21 06:52 TJS 6010D
Arsenic <29.4 mg/Kg - dry 29.4 1 01/19/21 06:52 TJS 6010D
Calcium 28500 mg/Kg - dry 2940 1 01/19/21 06:52 TJS 6010D
Cadmium <5.88 mg/Kg - dry 5.88 1 01/19/21 06:52 TJS 6010D
Chromium 36.6 mg/Kg - dry 14.7 1 01/19/21 06:52 TJS 6010D
Copper 258 mg/Kg - dry 29.4 1 01/19/21 06:52 TJS 6010D
Iron 19600 mg/Kg - dry 588 1 01/19/21 06:52 TJS 6010D
Lead <17.6 mg/Kg - dry 17.6 1 01/19/21 06:52 TJS 6010D
Magnesium 9120 mg/Kg - dry 294 1 01/19/21 06:52 TJS 6010D
Manganese 498 mg/Kg - dry 29.4 1 01/19/21 06:52 TJS 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 3 of 6

Waypoint.
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
Report Number : 21-013-0004
Lab No : 74665
Sample ID : HT #2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank
Information :
REPORT OF ANALYSIS
Report Date: 01/28/2021
Received : 01/13/2021
?Quylc m� Gloact/
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 1/12/2021 0:00
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Mercury <0.882 mg/Kg - dry 0.882 1 01/21/21 11:20 DDB SW-7471B
Molybdenum <14.7 mg/Kg - dry 14.7 1 01/19/21 06:52 TJS 6010D
Nickel 22.2 mg/Kg - dry 14.7 1 01/19/21 06:52 TJS 6010D
Potassium 13900 mg/Kg - dry 588 1 01/19/21 06:52 TJS 6010D
Selenium <29.4 mg/Kg - dry 29.4 1 01/19/21 06:52 TJS 6010D
Silver <14.7 mg/Kg - dry 14.7 1 01/19/21 06:52 TJS 6010D
Sodium 4220 mg/Kg - dry 1470 1 01/19/21 06:52 TJS 6010D
Zinc 982 mg/Kg - dry 73.5 1 01/19/21 06:52 TJS 6010D
Sulfur 14900 mg/Kg - dry 588 1 01/19/21 06:52 TJS 6010D
Sodium Absorption Ratio <5.00 Ratio 5.00 1 01/19/21 06:52 CALCULATION
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 6

Waypoint.
ANALYTICAL
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 21-013-0004
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytica I.com
Shipment Receipt Form
Shipping Method
Fed Ex 0 US Postal 0 Lab Other :
• UPS 0 Client n Courier Thermometer ID: l
Shipping container/cooler uncompromised?
• Yes 0No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? Yes
No • Not Present
Custody seals intact on sample bottles? _ Yes No • Not Present
Chain of Custody (COC) present?
• Yes No
COC agrees with sample label(s)?
• Yes No
COC properly completed
• Yes No
Samples in proper containers?
Sample containers intact?
• Yes No
• Yes No
Sufficient sample volume for indicated test(s)? • Yes No
All samples received within holding time?
• Yes O No
Cooler temperature in compliance?
• Yes n No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes (J No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
n Yes
0 Yes
f1 No
n No
• •
N/A
N/A
Trip Blanks received with VOAs 0 Yes
0No •N/A
Soil VOA method 5035 — compliance criteria met
n Yes (J No • N/A
High concentration container (48 hr)
Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) I Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
(`) Yes
• No
Signature: ;Samantha Clarke Date & Time: ;01/13/2021 14:03:22
Page 5 of 6

Client Name/Address
71i)N eF Gl'atilon)
fQ 6ax •7q
etcat tO/t! NC c9752
Client Project Manager/Contact
Billing Information
ez/sa
For Laboratory Use Only
,
r
Project Description
111IIII81111111111
Project/Site Location
III`IIIII„��IIIIII�II��`II�`III�IIIIIIIIIIII
(City i t...t
barges ,ipp1Y
n t(0
pt13� 1
Method of Shipment
Fed Ex
!_
❑ Other Courier 1
{JI'S USPS
Client Drop Olt
Matnx Key
WW - Wastewater GW -Groundwater
ng
P Product 1 fvtw�tisc ater S Sod/Solid O-Od
I4D'_57
Project Number Town 01 Clayton
Holding Tank
_
Purchase Order Number
;(,,.z 1 — a.-Ci--
Site/Facility ID 11
Waypoint
7021 Wiulepme
ki.ltnx,nd,
(NO I) 271 n•I•It.
ANALYTICAL
Raab
k.\ 2123—
Unless noted. all containers
per Table II of 40 CFR Part
136
i
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A Cool < 10C Na2S203 (Micro Only)
0 Cool <_ 6C
C H2504 pH<2
D None Requited
E Na0H pH>10
F HNO3 pH<2
G HCL H<2
H HCLp H<2
P
I Coot <_ 5C NA2S203
Date
Time
Sample Identification
Required
Analysis / Preservative
Comments/Notes
1,42.1171.
w
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ate
✓�
/
.1V'+
1
-
-
.
Y
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Remarks/Comments
For LaboratoryUse OnlySampled
P by(Name - Print)
Client
Ice
Custody
Seals
tab Comments
( /t fl(--i-e( as
� ��
0/ N
Y/N
I GQi
p
1if
11 ishe y: (SIGNATURE)
Date Time
ilfzj i'1ls
Received by: (SIGNATURE)
Date Time
Blank/Cooler Temp
Relinquished by: (SIGNATURE)
Date Time
wed by: (S
�eIA ju.PbiA
NAT E
lilt 0.0
Date Time
I43 -Z! 1.1.,CIP
Relinquished by: (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time
Y1
up
44
0
11,
(el
a

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms & Cleaning, Inc
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
C 2-21-144-0002
5/20/2021
6/2/2021
2nd Quarter 2021
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.93
Nitrogen (TKN)
7.630
76,300.000
Phosphorus
2.940
29,400.000
Potassium
1.160
11,600.000
Sulfur
0.000
Calcium
3.040
30,400.000
Magnesium
0.558
5,580.000
Sodium
0.466
4,660.000
Iron
---
Aluminum
---
9,950.000
Manganese
---
Copper
---
168.000
1,500
Zinc
---
507.000
2,800
Ammonia Nitrogen
1.260
12,600.000
Nitrate N / Nitrite N
---
256.000
Cadmium
---
5.260
39
Chromium
---
18.300
1,200
Nickel
---
15.100
420
Lead
---
15.800
300
Arsenic
---
26.300
41
Mercury
---
0.821
17
Selenium
---
26.300
100
pH
7.100
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
6.370
Molybdenum
---
13.200
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wastewater Treatment Plant
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
2nd Quarter 2021
6/2/2021 Report No: C 2-21-144-0002
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
51.332
PAN Inj.
63.932
P
58.800
K
23.200
Lime (estimated)
0.000
Secondary Nutrients
Calcium
60.800
Magnesium
11.160
Sodium
9.320
SAR
0.893
Chloride
0.000
Iron
0.000
Alumium
19.900
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
Physical Characteristics
% Solids
1.93
pH
7.100
Min Rate
0.300
Metals
Arsenic
0.053
Cadmium
0.011
Chromium
0.037
Copper
0.336
Lead
0.032
Mercury
0.002
Molybdenum
0.026
Nickel
0.030
Seleniun
0.053
Zinc
1.014
2018
2019
2020
2021
0.30
38.22
2022
0.15
13.38
2023
0.08
5.69
2024
0.04
2.63
2025
2026
2027
2028

Waypoint.
ANALYTICAL
6/2/2021
Town Of Clayton
POB 879
Clayton, NC, 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 21-144-0002
Project Description: Sludge 2nd Qtr
Waypoint Analytical Virginia, Inc. received sample(s) on 5/24/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

Waypoi ntx
ANALYTICAL
pit 6,„„, /
Pauric McGroary
Agronomist
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 2 of 7

Waypoint.
ANALYTICAL
Report Number: 21-144-0002
Client Project Description: Sludge 2nd Qtr
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
76468 holding tank #1 Solids 05/20/2021 09:30 05/24/2021 SM-4500-NH3C WP MTN
76468 holding tank #1 Solids 05/20/2021 09:30 05/24/2021 SM-4500-NH3C-TKN WP MTN
76468 holding tank #1 Solids 05/20/2021 09:30 05/24/2021 4500NO3F-2011 WP MTN
76468 holding tank #1 Solids 05/20/2021 09:30 05/24/2021 6010D WP MTN
76468 holding tank #1 Solids 05/20/2021 09:30 05/24/2021 SW-7471B WP MTN
76468 holding tank #1 Solids 05/20/2021 09:30 05/24/2021 9045D WP MTN
76468 holding tank #1 Solids 05/20/2021 09:30 05/24/2021 SM-2540G WP MTN
WP MTN - Memphis, TN: Waypoint Analytical -TN, Memphis, TN
Page 3 of 7

Waypoint.
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyticai.com
Project Sludge 2nd Qtr
Information :
Report Number :21-144-0002 REPORT OF ANALYSIS
Original Report Date : 06/04/2021
Revised Report Date: 07/27/2021
Received : 05/24/2021
Lab No : 76468 Matrix: Solids
Sample ID : holding tank #1 Sampled: 5/20/2021 9:30
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Total Solids 1.93 % 0.010 1 05/25/21 16:25 FMM SM-2540G
Total Kjeldahl Nitrogen 76300 mg/Kg - dry 13200 1 06/01/21 10:00 JPJ ;M-4500-NH3C-TKP
Phosphorus 29400 mg/Kg - dry 263 1 05/29/21 05:02 TJS 6010D
Potassium 11600 mg/Kg - dry 526 1 06/01/21 13:41 TJS 6010D
Calcium 30400 mg/Kg - dry 2630 1 05/29/21 05:02 TJS 6010D
Magnesium 5580 mg/Kg - dry 263 1 05/29/21 05:02 TJS 6010D
Sodium 4660 mg/Kg - dry 1320 1 05/29/21 05:02 TJS 6010D
Copper 168 mg/Kg - dry 26.3 1 05/29/21 05:02 TJS 6010D
Zinc 507 mg/Kg - dry 65.8 1 05/29/21 05:02 TJS 6010D
Nitrate+Nitrite-N <256 mg/Kg - dry 256 1 05/26/21 14:04 ZBD 4500NO3F-2011
Nickel 15.1 mg/Kg - dry 13.2 1 05/29/21 05:02 TJS 6010D
Mercury <0.821 mg/Kg - dry 0.821 1 05/26/21 14:41 DDB SW-7471B
Selenium <26.3 mg/Kg - dry 26.3 1 05/29/21 05:02 TJS 6010D
pH 7.1 s.u. 1 05/27/21 16:16 CxC 9045D
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen 12600 mg/Kg - dry 5260 1 06/01/21 16:00 JPJ SM-4500-NH3C
Aluminum 9950 mg/Kg - dry 263 1 05/29/21 05:02 TJS 6010D
Arsenic <26.3 mg/Kg - dry 26.3 1 05/29/21 05:02 TJS 6010D
Cadmium <5.26 mg/Kg - dry 5.26 1 05/29/21 05:02 TJS 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 7

Waypoint.
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Sludge 2nd Qtr
Information :
Report Number :21-144-0002 REPORT OF ANALYSIS
Original Report Date : 06/04/2021
Revised Report Date: 07/27/2021
Received : 05/24/2021
Lab No : 76468 Matrix: Solids
Sample ID : holding tank #1 Sampled: 5/20/2021 9:30
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Chromium 18.3 mg/Kg - dry 13.2 1 05/29/21 05:02 TJS 6010D
Lead <15.8 mg/Kg - dry 15.8 1 05/29/21 05:02 TJS 6010D
Molybdenum <13.2 mg/Kg - dry 13.2 1 05/29/21 05:02 TJS 6010D
Silver <13.2 mg/Kg - dry 13.2 1 05/29/21 05:02 TJS 6010D
Analytical Method: SM-2540G
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Moisture
98.1
%
0.010 1 05/25/21 16:25 FMM L555046
Qualifiers/
Definitions
DF Dilution Factor MQL Method Quantitation Limit
Page 5 of 7

Waypoint
ANALYTICAL
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 21-144-0002
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
• UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
• Yes 0 No
Number of coolers/boxes received 1 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0Not Present
Custody seals intact on sample bottles? 0 Yes 0 No • Not Present
Chain of Custody (COC) present? • Yes 0 No
COC agrees with sample label(s)? • Yes 0 No
COC properly completed
• Yes 0No
Samples in proper containers?
• Yes 0 No
Sample containers intact?
• Yes 0 No
Sufficient sample volume for indicated test(s)?
• Yes 0 No
All samples received within holding time?
• Yes 0No
Cooler temperature in compliance?
• Yes 0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
• Yes 0 No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
O Yes
O Yes
O No
O No
• •
N/A
N/A
Trip Blanks received with VOAs 0 Yes
O No • N/A
Soil VOA method 5035 — compliance criteria met
O Yes 0 No 0 N/A
j High concentration container (48 hr) [ Low concentration EnCore samplers (48 hr)
1 High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
O Yes • No
Signature:
Brandi Watson Date & Time:
Page 6 of 7
05/24/2021 12:52:25

Client Name/Address
Town of Clayton
PO BOX 879
Clayton, NC 27528
Client Project Manager/Contact
William Simpson
Town of Clayton WRI-
PO Box 879
Clayton, NC 27528
Billing Information
Town of Clayton
PO BOX 879
Clayton, NC 27528
Protect Description
Sludge 2nd QTR
Project Number
Project/Site Location (City/State)
Town of Clayton Holding
Tank #1
Protect Manager Phone 11
9195531535
RUSFI — Additional charges apply
Special Detection Ltmtt(sl
Date Results Needed
Project Manager Email
2021-WRF
4
I 1111 li 11111111111111111111111111111111011111111h111111181i;2 �
Torre OI Clavinn 07 43 13
Shrdee :rid C11r
Method of Ship
nFed fx Irs�r
❑ Courier D (bent Drop Otr
Other
Purchase Order Number
2021-WRF
OW Drinking ,'.'.iter soil/So,nl 0 Oil
P Product M Misr:
Site/Facility ID 1t
Waypoint 0
ANALYTICAL
u1 1t'huynnc
ROImencl. V 1 `i_
(slit)'71 1,116
Unless noted, all containers
per Table II of 40 CFR Part
136
Date
Tune
0930
Sample Identification
Holding Tank #1
Number of Containers
2
Matrix (Refer to Key)
ww
0
E
`
m
u
C
M
N
0
.a
N
A
0
C
D
0
H
Cool • 10C Na2S2O3 (Micro Only)
Cool < 6C
H2SO4 pH<2
None Required
NaOH pH>t0
HNO3 pM<2
t1CL pH<2
H3PO4 pH<2
Cool <, 6C NA25203
✓ Y
For Laboratory Use Only
Ice
Y/N
Custody
Seals
Y/N
Blank/Cooler Temp
Lab Comments
•
Sampled by (Name — Print)
Required Analysis / Preservative
William Simpson
✓ ✓
60.#
111,
Comments/Notes
11
•
(tent Remarks/Comments P/,e.&,- . sjs i� DO%e' ir,sc.& vJ1t,f
Oilt.14. w, t2. £,44r071 po777u f°oi .✓rssci g,is.✓r
Rellnqu hed by: (SIGNATURE)
Relinquished b . (SIGNATURE)
Date Time
s1% 1GJ.'
Date Time
Received by: (SIGNATURE)
Received by: (SIGNATURE)
Date Time
Date Time
Relinquished by: (SIGNATURE)
Date Time
_6orypa Ta. _0r6ke.-,nr01I t� —
Received by: (SIGNATURE)
'512-1/ /
Date lime

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms & Cleaning, Inc
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
C 3-21-207-0004
7/22/2021
8/3/2021
3rd Quarter 2021
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.70
Nitrogen (TKN)
8.000
80,000.000
Phosphorus
3.510
35,100.000
Potassium
1.030
10,300.000
Sulfur
1.310
13,100.000
Calcium
2.080
20,800.000
Magnesium
0.600
6,000.000
Sodium
0.547
5,470.000
Iron
---
Aluminum
---
18,400.000
Manganese
---
Copper
---
219.000
1,500
Zinc
---
735.000
2,800
Ammonia Nitrogen
0.688
6,880.000
Nitrate N / Nitrite N
---
3,650.000
Cadmium
---
5.880
39
Chromium
---
21.200
1,200
Nickel
---
14.700
420
Lead
---
17.600
300
Arsenic
---
29.400
41
Mercury
---
0.900
17
Selenium
---
29.400
100
pH
6.300
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
7.312
Molybdenum
---
14.700
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wastewater Treatment Plant
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
3rd Quarter 2021
8/3/2021 Report No: C 3-21-207-0004
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
58.052
PAN Inj.
64.932
P
70.200
K
20.600
Lime (estimated)
0.000
Secondary Nutrients
Calcium
41.600
Magnesium
12.000
Sodium
10.940
SAR
1.117
Chloride
0.000
Iron
0.000
Alumium
36.800
Manganese
0.000
Boron
0.000
Sulfur
26.200
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
Physical Characteristics
% Solids
1.70
pH
6.300
Min Rate
0.300
Metals
Arsenic
0.059
Cadmium
0.012
Chromium
0.042
Copper
0.438
Lead
0.035
Mercury
0.002
Molybdenum
0.029
Nickel
0.029
Seleniun
0.059
Zinc
1.470
2018
2019
2020
2021
0.30
43.87
2022
0.15
15.36
2023
0.08
6.53
2024
0.04
3.02
2025
2026
2027
2028

Waypoint.
ANALYTICAL
8/3/2021
Town Of Clayton
POB 879
Clayton, NC, 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 21-207-0004
Project Description: Holding Tank #1
Waypoint Analytical Virginia, Inc. received sample(s) on 7/26/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
plc Graver
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

Waypoint..
ANALYTICAL
Report Number: 21-207-0004
Client Project Description: Holding Tank #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
77254 Holding Tank #1 Solids 07/22/2021 10:15 07/26/2021
77254 Holding Tank #1 Solids 07/22/2021 10:15 07/26/2021 SM-4500-NH3C WP MTN
77254 Holding Tank #1 Solids 07/22/2021 10:15 07/26/2021 9045D WP MTN
77254 Holding Tank #1 Solids 07/22/2021 10:15 07/26/2021 4500NO3F-2011 WP MTN
77254 Holding Tank #1 Solids 07/22/2021 10:15 07/26/2021 6010D WP MTN
77254 Holding Tank #1 Solids 07/22/2021 10:15 07/26/2021 SW-7471B WP MTN
77254 Holding Tank #1 Solids 07/22/2021 10:15 07/26/2021 SM-4500-NH3C-TKN WP MTN
77254 Holding Tank #1 Solids 07/22/2021 10:15 07/26/2021 SM-2540G WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

Waypoint.
ANALYTICAL
46546
Town Of Clayton
P0B 879
Clayton , NC 27528
Report Number : 21-207-0004
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank #1
Information :
REPORT OF ANALYSIS
Report Date : 08/03/2021
Received : 07/26/2021
�gcurc r}� G�oaO
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 77254 Matrix: Solids
Sample ID : Holding Tank #1 Sampled: 7/22/2021 10:15
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Total Solids 1.70 % 0.010 1 07/27/21 16:43 FMM SM-2540G
Total Kjeldahl Nitrogen 80000 mg/Kg - dry 14700 1 08/02/21 09:00 JPJ ;M-4500-NH3C-TKI'
Phosphorus 35100 mg/Kg - dry 294 1 07/30/21 23:08 JTR 6010D
Potassium 10300 mg/Kg - dry 588 1 07/30/21 23:08 JTR 6010D
Sulfur 13100 mg/Kg - dry 588 1 07/30/21 23:08 JTR 6010D
Calcium 20800 mg/Kg - dry 2940 1 07/30/21 23:08 JTR 6010D
Magnesium 6000 mg/Kg - dry 294 1 07/30/21 23:08 JTR 6010D
Sodium 5470 mg/Kg - dry 1470 1 07/30/21 23:08 JTR 6010D
Copper 219 mg/Kg - dry 29.4 1 07/30/21 23:08 JTR 6010D
Zinc 735 mg/Kg - dry 73.5 1 07/30/21 23:08 JTR 6010D
Nitrate+Nitrite-N 3650 mg/Kg - dry 288 1 07/28/21 15:58 ZBD 4500NO3F-2011
Nickel <14.7 mg/Kg - dry 14.7 1 07/30/21 23:08 JTR 6010D
Mercury <0.900 mg/Kg - dry 0.900 1 07/29/21 13:04 DDB SW-7471B
Selenium <29.4 mg/Kg - dry 29.4 1 07/30/21 23:08 JTR 6010D
pH 6.3 s.u. 1 07/30/21 14:36 DRS 9045D
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sodium Absorption Ratio <294 mg/Kg - dry 294 1 07/30/21 23:08 CALCULATION
Ammonia Nitrogen 6880 mg/Kg - dry 5880 1 08/02/21 15:00 JPJ SM-4500-NI3C
Aluminum 18400 mg/Kg - dry 294 1 07/30/21 23:08 JTR 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 3 of 6

Waypoint.
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Holding Tank #1
Information :
Report Number :21-207-0004 REPORT OF ANALYSIS
Report Date : 08/03/2021
Received : 07/26/2021
Icuttic �C G�oatir
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 77254 Matrix: Solids
Sample ID : Holding Tank #1 Sampled: 7/22/2021 10:15
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Arsenic <29.4 mg/Kg - dry 29.4 1 07/30/21 23:08 JTR 6010D
Cadmium <5.88 mg/Kg - dry 5.88 1 07/30/21 23:08 JTR 6010D
Chromium 21.2 mg/Kg - dry 14.7 1 07/30/21 23:08 JTR 6010D
Lead <17.6 mg/Kg - dry 17.6 1 07/30/21 23:08 JTR 6010D
Molybdenum <14.7 mg/Kg - dry 14.7 1 07/30/21 23:08 JTR 6010D
Silver <14.7 mg/Kg - dry 14.7 1 07/30/21 23:08 JTR 6010D
Analytical Method: SM-2540G
Test Results Units !VOL DF Date / Time By Analytical
Analyzed Batch
Moisture 98.3
0.010 1 07/27/21 16:43 FMM L565949
Qualifiers/
Definitions
DF Dilution Factor MQL Method Quantitation Limit
Page 4 of 6

Waypoint
ANALYTICAL
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 21-207-0004
0 Fed Ex
*% UPS
0 US Postal
0 Client
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Shipping Method
0 Lab
Courier
Other :
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes No
Number of coolers/boxes received I 1
Custody seals intact on shipping container/cooler? 0 Yes
O No * Not Present
Custody seals intact on sample bottles? 0 Yes
O No * Not Present
Chain of Custody (COC) present?
* Yes 0 No
COC agrees with sample label(s)?
*Yes 0No
COC properly completed
* Yes 0 No
Samples in proper containers?
Sample containers intact?
*Yes 0 No
(� Yes (J No
Sufficient sample volume for indicated test(s)?
* Yes JNo
All samples received within holding time?
*Yes 0No
Cooler temperature in compliance?
* Yes 0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
* Yes JNo
Water - Sample containers properly preserved
Water - VOA vials free of headspace
U Yes
0 Yes
O No
fl No
C N/A
C N/A
Trip Blanks received with VOAs 0 Yes
O No I N/A
Soil VOA method 5035 — compliance criteria met
0 Yes (0 No * N/A
High concentration container (48 hr)
Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) j Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
(1 Yes
*No
Signature: ;Brandi Watson ; Date & Time: :07/26/2021 11:04:56
Page 5 of 6

ClItrit
Name/Address
l✓e 6, Cf' fit i l
Po. b°K �7f
tin, rve Z75-Zr
Project Description
Client Project Manager/Contact
(i A,w. S(rweSO al‘"
-rGuh 0 C/ .t wgr—
O f% fl g 79 c1/414, We 275i
Project/Site ocation (City/State)
11�✓1 O11 C' A7rt
f-fo (d ►'� t\-
Billing Information
Sc+..' C
RUSH — Additional charges apply
Special Detection Unit(s)
Date Results Needed
Method of Shipmen
ED Fed Ex
Courser u
Other
For Laboratory Use Only
! III I� III IIII I II0 I III III 1II 1II 1II III 21 :27
Town OI Clavlor 11 03 57
Holdtaq Lmk 111
1
Project Number
Project Manager Phone li
(1 I) 5:51-153C
-
Project Manager Email
1NS;mes0A6:4<i+,.n04. nc.o y
Purchase Order Number
Z 0 2 rr ' wt2 l
Site/Facility ID tl
`-/
Waypoint
'' l Wink.
lii.6n(.nnl
(atl i l ' tad
p �,nt
ANALYTICAL.
pint Rudd
\ 1 ' S t'
In
Unless noted, all container.,
per Table II of 40 CrR Part
136
INumber of Containers
Matrix (Refer to Key)
(G)rab or (C)omposite
1 1
�}
ti 4n 4
ZJ
4,
!�
O>.-
'O
S.-
y ` \
('.
' o
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o '�
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i
�
^i
'` Che`\
C ,
�. " 1
1
��
`
C�
A Cool < IOC Na2S203 (Micro Only)
B Cool <= 6C
0 H2SO4pHc2
0 None Required
F HNO3pH<2B
G HCI. PH<2
H H3PO4 pHa2
I Cool c- 6C NA25203
Ci•.:Ie
ne
Sample identification
,
Analysis / Preservative
Comments/Notes
7/z2 /Z(
/O�$
0#0/C11vti �.n i /V
'I
� '
C
,/
✓
i
t,
)
For LaboratoryUse OnlyI
Sampled by
ir,. SG /Vet
(Name— Print)
r
/07 a,14( (4 62,0 TR—
Client Remarks/Comments
/caSc Sh:CoOlrr,Ict ?��ks
Q.,ek t� " �" lCigp4
Ice
Y / N
Custody
Seals
Y / N
Lab Comments
Re " ishe by: IGNATT E) ,
U,rr �d / 1/1620 J1
Date Time
Received by: (SIGNATURE)
Date Time
Blank/Cooler Temp
Relinquished by: (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time
Relinquished by: (SIGNATURE)
Date Time
Received by: (SIGNATURE)
Date Time

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms & Cleaning, Inc
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
C 4-21-295-0003
10/21/2021
11/2/2021
4th Quarter 2021
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.97
Nitrogen (TKN)
9.750
97,500.000
Phosphorus
3.400
34,000.000
Potassium
0.880
8,800.000
Sulfur
0.000
0.000
Calcium
2.570
25,700.000
Magnesium
0.605
6,050.000
Sodium
0.486
4,860.000
Iron
---
Aluminum
---
16,700.000
Manganese
---
Copper
---
206.000
1,500
Zinc
---
790.000
2,800
Ammonia Nitrogen
0.915
9,150.000
Nitrate N / Nitrite N
---
755.000
Cadmium
---
5.000
39
Chromium
---
22.600
1,200
Nickel
---
12.500
420
Lead
---
15.000
300
Arsenic
---
25.000
41
Mercury
---
0.720
17
Selenium
---
25.000
100
pH
6.600
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
8.835
Molybdenum
---
12.500
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wastewater Treatment Plant
Clayton Little Creek WRF
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
4th Quarter 2021
11/2/2021 Report No:
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
63.670
PAN Inj.
72.820
P
68.000
K
17.600
Lime (estimated)
0.000
Secondary Nutrients
Calcium
51.400
Magnesium
12.100
Sodium
9.720
SAR
0.992
Chloride
0.000
Iron
0.000
Alumium
33.400
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
C 4-21-295-0003
Physical Characteristics
% Solids
1.97
pH
6.600
Min Rate
0.300
Metals
Arsenic
0.050
Cadmium
0.010
Chromium
0.045
Copper
0.412
Lead
0.030
Mercury
0.001
Molybdenum
0.025
Nickel
0.025
Seleniun
0.050
Zinc
1.580
2018
2019
2020
2021
0.30
53.01
2022
0.15
18.55
2023
0.08
7.89
2024
0.04
3.65
2025
2026
2027
2028

Waypoint
ANALYTICAL
11/2/2021
Town Of Clayton
POB 879
Clayton, NC, 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Ref: Analytical Testing
Report Number: 21-295-0003
Project Description: Sludge Disposal 4th Quarter
Waypoint Analytical Virginia, Inc. received sample(s) on 10/25/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
TI•c
plc brow/
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° fax [phone]
www.waypointanalytical.com
Sample Summary Table
Report Number: 21-295-0003
Client Project Description: Sludge Disposal 4th Quarter
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
55224 holding tank Solids 10/21/2021 11:40 10/25/2021
55224 holding tank Solids 10/21/2021 11:40 10/25/2021 SM-4500-NH3C WP MTN
55224 holding tank Solids 10/21/2021 11:40 10/25/2021 9045D WP MTN
55224 holding tank Solids 10/21/2021 11:40 10/25/2021 4500NO3F-2011 WP MTN
55224 holding tank Solids 10/21/2021 11:40 10/25/2021 6010D WP MTN
55224 holding tank Solids 10/21/2021 11:40 10/25/2021 SW-7471B WP MTN
55224 holding tank Solids 10/21/2021 11:40 10/25/2021 SM-4500-NH3C-TKN WP MTN
55224 holding tank Solids 10/21/2021 11:40 10/25/2021 SM-2540G WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 6

Waypoint,
ANALYTICAL
46546
Town 0f Clayton
POB 879
Clayton , NC 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Sludge Disposal 4th Quarter
Information :
Report Number :21-295-0003 REPORT OF ANALYSIS
Report Date : 11/02/2021
Received : 10/25/2021
�ctwit � 6.„„„r
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 55224 Matrix: Solids
Sample ID : holding tank Sampled: 10/21/2021 11:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture 98.0 % 0.010 1 10/27/21 16:57 FMM SM-2540G
Total Kjeldahl Nitrogen 97500 mg/Kg - dry 12500 1 11/01/21 10:00 JPJ ;M-4500-NH3C-TKP
Potassium 8800 mg/Kg - dry 500 1 10/30/21 04:05 TJS 6010D
Calcium 25700 mg/Kg - dry 2500 1 10/30/21 04:05 JADS 6010D
Aluminum 16700 mg/Kg - dry 250 1 10/30/21 04:05 )ADS 6010D
Copper 206 mg/Kg - dry 25.0 1 10/30/21 04:05 DADS 6010D
Zinc 790 mg/Kg - dry 62.5 1 10/30/21 04:05 JADS 6010D
Nickel <12.5 mg/Kg - dry 12.5 1 10/30/21 04:05 )ADS 6010D
Arsenic <25.0 mg/Kg - dry 25.0 1 10/30/21 04:05 ]ADS 6010D
Silver <12.5 mg/Kg - dry 12.5 1 10/30/21 04:05 )ADS 6010D
Test
Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sodium Absorption Ratio 50.0 mg/Kg - dry 50.0 1 10/30/21 04:05 CALCULATION
pH 6.6 s.u. 1 10/29/21 15:10 DRS 9045D
Lead <15.0 mg/Kg - dry 15.0 1 10/30/21 04:05 JADS 6010D
Magnesium 6050 mg/Kg - dry 250 1 10/30/21 04:05 JADS 6010D
Selenium <25.0 mg/Kg - dry 25.0 1 10/30/21 04:05 ]ADS 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 3 of 6

Waypoint.
ANALYTICAL
46546
Town Of Clayton
POB 879
Clayton , NC 27528
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project Sludge Disposal 4th Quarter
Information :
Report Number : 21-295-0003 REPORT OF ANALYSIS
Report Date : 11/02/2021
Received : 10/25/2021
?µWIC lC G�oa�/
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 55224 Matrix: Solids
Sample ID : holding tank Sampled: 10/21/2021 11:40
Total Solids 1.97 % 0.010 1 10/27/21 16:57 FMM SM-2540G
Phosphorus 34000 mg/Kg - dry 250 1 10/30/21 04:05 JADS 6010D
Sodium 4860 mg/Kg - dry 1250 1 10/30/21 04:05 DADS 6010D
Ammonia Nitrogen 9150 mg/Kg - dry 5000 1 11/01/21 15:00 JPJ SM-4500-NH3C
Nitrate+Nitrite-N 755 mg/Kg - dry 250 1 10/28/21 16:01 ZBD 4500NO3F-2011
Cadmium <5.00 mg/Kg - dry 5.00 1 10/30/21 04:05 JADS 6010D
Chromium 22.6 mg/Kg - dry 12.5 1 10/30/21 04:05 JADS 6010D
Mercury <0.720 mg/Kg - dry 0.720 1 10/29/21 14:05 JW2 SW-7471B
Molybdenum <12.5 mg/Kg - dry 12.5 1 10/30/21 04:05 JADS 6010D
Qualifiers/
Definitions
B Analyte detected in blank DF Dilution Factor
H Beyond holding time MQL Method Quantitation Limit
Page 4 of 6

Waypoint
ANALYTICAL
Customer Number: 46546
Customer Name: Town Of Clayton
Report Number: 21-295-0003
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Shipping Method
O Fed Ex 0 US Postal 0 Lab Other :
C` UPS 0 Client 0 Courier Thermometer ID: 1
Shipping container/cooler uncompromised?
Ci Yes No
Number of coolers/boxes received I 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present
Custody seals intact on sample bottles? 0 Yes 0 No n Not Present
Chain of Custody (COC) present?
COC agrees with sample label(s)?
L Yes
* Yes
O No
O No
COC properly completed
Yes O No
Samples in proper containers?
*'Yes 0No
Sample containers intact?
* Yes 0 No
Sufficient sample volume for indicated test(s)? L Yes 0 No
All samples received within holding time?
*Yes ONo
Cooler temperature in compliance?
* Yes 0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
( Yes (9 No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
Trip Blanks received with VOAs
0 Yes
O Yes
i jYes
O No
O No
O No
• N/A
• N/A
L' N/A
Soil VOA method 5035 — compliance criteria met
0Yes ONo '4)N/A
High concentration container (48 hr) r Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) r Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes No
Comments:
Signature: iBrandi Watson Date & Time:
10/25/2021 07:30:57
Page 5 of 6

Client Name/Address
Town of Clayton
Little Creek WRF
PO Box 879
Clayton. NC 27528
Client Project Manager/Contact
William Simpson
919-553-1536
wsi mpson@ townof cla ytonnC.org
Billing Information
Town of Clayton
Little Crock WRF
PO Box 879
Clayton. NC 27528
Project Description
Sludge Disposal 4th
Quarter
Project Number
Waypoint
Ynt
ANALYTICAL
"ti21 \\'hai:pine Road
Ri.hnu.tiJ. \ A 2 t21
ON) 271-441h
Project/Site Location (City/State)
Project Manager Phone $
Unless noted. all containers
per Table II of 40 CFR Part
136.
Date
1ia2t 21
Time
1140
Sample Identification
Holding Tank
cL
00
e
Z
4
ww
r..a
RUSH - Additional charges apply
Special Detection limits)
Date Results Needed
Project Manager Email
2022-115
)rab or (C)omposite
Req
Method of Shipmc
El Fed Ex �✓
❑ Courier ❑
Other
Purchase Order Number
2022-115
I�aIIIIIt1IIOIIIIOftNIII1IIII�II1IIIlIIII1 L95Sio 03
Twat Qf Clavion 07 29 38
Sludue Disuos.il 41h 0uarlei
Site/Facility ID tl
A
e
C
0
E
0
H
Cool < IOC Na252O3 (Micro Only)
Cool m GC
H2SO4pH<2
None Required
NaOH pH.10
HNO3 pHc2
HCIpH<2
H3PO4 pH<2
Cool <= GC NA252O3
ulred Analysis / Preservative
Comments/Notes
W
0
v
rd
01
w
For laboratory Use Only
Ice
Y/N
Custody
Seals
Y/N
Blank/Cooler Temp
Lab Comments
Sampled by (Name - Print)
Relinquished by: (SIGNATURE)
Client Remarks/Comments
Please return Cooler and ice packs with empty bottles for next event
FSos g12/f2(
Date Time
Received by: (SIGNATURE)
Received by: (SIGNATURE)
Date Time
Date Time
Relinquished by: (SIGNATURE}
Date Time
Received by: (SIGNATURE)
Date Time

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Kenansville
Kenansville WWTP
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
KV 2021-08913
6/2/2021
7/1/2021
Annual 2021
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.080
Nitrogen (TKN)
4.350
43,500.000
Phosphorus
1.010
10,100.000
Potassium
0.419
4,190.000
Sulfur
0.000
Calcium
1.580
15,800.000
Magnesium
0.220
2,204.000
Sodium
0.972
9,720.000
Iron
---
Aluminum
---
8,130.000
Manganese
---
Copper
---
522.000
1,500
Zinc
---
795.000
2,800
Ammonia Nitrogen
0.110
1,100.000
Nitrate N / Nitrite N
---
2,890.000
Cadmium
---
44.100
85
Chromium
---
44.100
1,200
Nickel
---
44.100
420
Lead
---
44.100
300
Arsenic
---
44.100
75
Mercury
---
0.000
17
Selenium
---
44.100
100
pH
6.840
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
4.240
Molybdenum
---
44.100
75
Chloride
---
Boron
Available P205
Specific Gravity
8.340

Date Reported:
Wastewater Treatment Plant
Kenansville WWTP
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2021
7/1/2021 Report No: KV 2021-08913
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
32.320
PAN Inj.
33.420
P
20.200
K
8.380
Lime (estimated)
0.000
Secondary Nutrients
Calcium
31.600
Magnesium
4.408
Sodium
19.440
SAR
1.990
Chloride
0.000
Iron
0.000
Alumium
16.260
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
1.08
pH
6.840
Min Rate
0.300
Metals
Arsenic
0.088
Cadmium
0.088
Chromium
0.088
Copper
1.044
Lead
0.088
Mercury
0.003
Molybdenum
0.088
Nickel
0.088
Seleniun
0.088
Zinc
1.590

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Town of Kenansville
PO Box 370
Kenansville
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
NC 28349
Date of Report: Jul 01, 2021
Customer PO #:
Customer ID: 09020018
Report #: 2021-08913
Project ID: Sludge
Lab ID
21-22184
Test
Sample ID:
Site: sludge
Method
Collect Date/Time Matrix Sampled by
6/2/2021
10:10 AM Solid/Sludge Client
Results
Date Analyzed
Total Solids (%)
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychlor (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenol (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1,1-Dichloroethylene (TCLP)
1,2-Dichloroethane (TCLP)
Benzene (TCLP)
SM 2540 B
SW 846 Method 8081 B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 method 8270/3510
SW 848 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 848 method 8270/3510
SW 846 method 8270/3510
SW848 Method 8151A
SW846 Method 8151A
SW846 Method 8260/5030
SW848 Method 8260/5030
SW846 Method 8260/5030
1.08 % 06/14/2021
<0.02 mg/L 06/09/2021
<0.0005 mg/L 06/09/2021
<0.0005 mg/L 06/09/2021
<0.0005 mg/L 06/09/2021
<0.0005 mg/L 06/09/2021
<0.0005 mg/L 06/09/2021
<0.05 mg/L 06/09/2021
<0.050 mg/L 06/11/2021
<0.050 mg/L 06/11/2021
<0.050 mg/L 06/11/2021
<0.050 mg/L 06/11/2021
<0.050 mg/L 06/11/2021
<0.050 mg/L 06/11/2021
<0.050 mg/L 06/11/2021
<0.050 mg/L 06/11/2021
<0.050 mg/L 06/11/2021
<0.050 mg/L 06/11/2021
<0.050 mg/L 06/11/2021
<0.250 mg/L 06/11/2021
<0.050 mg/L 06/11/2021
<0.003 mg/L 06/10/2021
<0.003 mg/L 06/10/2021
<0.01 mg/L 06/09/2021
<0.01 mg/L 06/09/2021
<0.01 mg/L 06/09/2021
Report #:: 2021-08913 Page 1 of 3

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Kenansville
PO Box 370
Kenansville NC 28349
Attention:
Date of Report: Jul 01, 2021
Customer PO #:
Customer ID: 09020018
Report #: 2021-08913
Project ID: Sludge
Carbon Tetrachloride (TCLP)
Chlorobenzene (TCLP)
Chloroform (TCLP)
Methyl ethyl ketone (TCLP)
Tetrachloroethylene (TCLP)
Trichloroethylene (TCLP)
Vinyl Chloride (TCLP)
RCI
Cyanide
Sulfide
Ignitability
pH
SW848 Method 8260/5030
SW848 Method 8280/5030
SW846 Method 8260/5030
SW846 Method 8280/5030
SW846 Method 8260/5030
SW848 Method 8260/5030
SW846 Method 8260/5030
SM 4500 CN D
SM 4500 S D
SW 846 method 1010
SW 846 Method 9045D
Result estimated. Analyzed out of 15 minutes hold time.
<0.01 mg/L 06/09/2021
<0.01 mg/L 06/09/2021
<0.01 mg/L 06/09/2021
<0.05 mg/L 06/09/2021
<0.01 mg/L 06/09/2021
<0.01 mg/L 06/09/2021
<0.01 mg/L 06/09/2021
<1.0 mg/kg 06/08/2021
0.11 mg/kg 06/08/2021
>200 °F 06/18/2021
6.84 units 06/30/2021
Sludge Residuals
Aluminum EPA200.7 8130mg/kg 06/18/2021
Arsenic EPA 200.7 <44.1 mg/kg 06/09/2021
Cadmium EPA200.7 <44.1 mg/kg 06/09/2021
Calcium EPA 200.7 15800 mg/kg 06/09/2021
Chromium EPA 200.7 <44.1 mg/kg 06/09/2021
Copper EPA 200.7 522 mg/kg 06/09/2021
Lead EPA 200.7 <44.1 mg/kg 06/09/2021
Magnesium EPA 200.7 <2204 mg/kg 06/09/2021
Molybdenum EPA 200.7 <44.1 mg/kg 06/09/2021
Nickel EPA 200.7 <44.1 mg/kg 06/09/2021
Potassium EPA 200.7 4190 mg/kg 06/09/2021
Selenium EPA200.7 <44.1 mg/kg 06/09/2021
Sodium EPA 200.7 9720 mg/kg 06/09/2021
Zinc EPA 200.7 795 mg/kg 06/09/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 2890 mg/kg 06/10/2021
Ammonia Nitrogen SM 4500 NH3 C 1100 mg/kg 06/04/2021
Repoli # : 2021-08913 Page 2 of 3

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info u environmentalchemists.com
Town of Kenansville
PO Box 370
Kenansville NC 28349
Attention:
Date of Report: Jul 01, 2021
Customer PO #:
Customer ID: 09020018
Report #: 2021-08913
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN) SM 4500 Org B
Total Phosphorus SM 4500 P F
Mercury SW846 74718
TCLP Metals
Arsenic EPA 200.7
Barium EPA 200.7
Cadmium EPA 200.7
Chromium EPA 200.7
Lead EPA 200.7
Selenium EPA 200.7
Silver EPA 200.7
Mercury EPA 245.1
43500 mg/kg 06/04/2021
10100 mg/kg 06/10/2021
<1.59 mg/kg 06/09/2021
<1.0 mg/L 06/15/2021
<1.0 mg/L 06/15/2021
<1.0 mg/L 06/15/2021
<1.0 mg/L 06/15/2021
<1.0 mg/L 06/15/2021
<1.0 mg/L 06/15/2021
<1.0 mg/L 06/15/2021
<0.0002 mg/L 06/09/2021
Comment: Sludge residuals reported on a dry weight basis.
Reviewed by: .' ,(t'l
Report #:: 2021-08913 Pape 3 of 3

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
CLIENT: Town of Kenansville
PROJECT NAME: Annual Sludge
REPORT NO:
ADDRESS:
CONTACT NAME: Garry Benson
PO NO:
pc-t"
(3
R
REPORT TO:
PHONE/FAX:
COPY TO:
email:
Sampled By:
SAMPLE TYPE: I = Influent. E = Effluent W = Well ST = SO = Soil SL = Slud a Other
Sample Identification
Collection
E a
(n
Composite
or
Grab
a o
a
4'
r E
"
LAB ID
NUMBER ;
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
W
z
Z
u
=
e
0
_
n
o
_
0
_
o
m
o
Sludge
,-02^al
lD•, In
lb'-,
SI
C
P
221
Full TCLP/RCl/Nutrients/Metals
G
G
C
P
G
G
C
P
G
G
C
P
G
G
_
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
R inquished By:
Date/Time
Received By:
DatefTime
1.
C #1ir�1..—
/ b4
t� iZ -021 / it.
2.
t V /
/)
emperature when Recety
Delivered By:
cceptea:
Resample Requested:
Received By: Date: 6--2-- �( Time:
Comments: TURNAROUND:

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Southwest Plantation
Jacksonville, North Carolina
Triple S Farms
Jacksonville WWTP
SWP 20213-21
2/17/2021
3/2/2021
Annual 2021
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
1.280
Nitrogen (TKN)
3.810
38,100.000
Phosphorus
1.260
12,600.000
Potassium
0.705
7,050.000
Sulfur
0.000
Calcium
1.370
13,700.000
Magnesium
0.374
3,740.000
Sodium
1.720
17,200.000
Iron
---
Aluminum
---
2,520.000
Manganese
---
Copper
---
130.000
1,500
Zinc
---
1,010.000
2,800
Ammonia Nitrogen
0.242
2,420.000
Nitrate N / Nitrite N
---
14.500
Cadmium
---
19.400
39
Chromium
---
19.600
1,200
Nickel
---
19.400
420
Lead
---
19.400
300
Arsenic
---
20.700
41
Mercury
---
1.310
17
Selenium
---
19.400
100
pH
6.720
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
3.568
Molybdenum
---
19.400
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Jacksonville WWTP
Southwest Plantation
Jacksonville, North Carolina
Triple S Farms
Annual 2021
3/2/2021 Report No: SWP 2021 3-21
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
23.857
PAN Inj.
26.277
P
25.200
K
14.100
Lime (estimated)
0.000
Secondary Nutrients
Calcium
27.400
Magnesium
7.480
Sodium
34.400
SAR
3.790
Chloride
0.000
Iron
0.000
Alumium
5.040
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
1.28
pH
6.720
Min Rate
0.300
Metals
Arsenic
0.041
Cadmium
0.039
Chromium
0.039
Copper
0.260
Lead
0.039
Mercury
0.003
Molybdenum
0.039
Nickel
0.039
Seleniun
0.039
Zinc
2.020

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Environmental Services
PO Box 1054
Jacksonville NC 28541
Attention:
Date of Report: Mar 02, 2021
Customer PO #:
Customer ID: 14110017
Report #: 2021-02832
Project ID: Bear Trail Golf Course
Lab ID
21-06818
Test
Sample ID:
Site: Sludge
Method
Collect Date/Time
2/17/2021 5:30 PM
Matrix Sampled by
Solid/Sludge Sonny Scozzari
Results Date Analyzed
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
pH
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
EPA 200 7
EPA2007
EPA 200.7
EPA2007
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200,7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 353.2
SM 2540 B
SM 4500 H B
SM 4500 NH3 C
SM 4500 Org B
SM 4500 P F
SW846 7471B
2520 mg/kg
20.7 mg/kg
<19.4 mg/kg
13700 mg/kg
19.6 mg/kg
130 mg/kg
<19.4 mg/kg
3740 mg/kg
<19.4 mg/kg
<19.4 mg/kg
7050 mg/kg
<19.4 mg/kg
17200 mg/kg
1010 mg/kg
14.5 mg/kg
1.28%
6.72 units
2420 mg/kg
38100 mg/kg
12600 mg/kg
<1.31 mg/kg
02/24/2021
02/24/2021
02/24/2021
02/24/2021
02/24/2021
02/24/2021
02/24/2021
02/24/2021
02/24/2021
02/24/2021
03/01/2021
02/24/2021
03/01/2021
02/24/2021
02/23/2021
02/22/2021
02/23/2021
02/22/2021
02/22/2021
02/25/2021
02/24/2021
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: LaJ0
Report #:; 2021-02832 Page 1 of 1

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT:
ENVIRONMENTAL SERVICES
PROJECT NAME: Bear Trail Golf
REPORT NO: 2,I-02 2jZ
ADDRESS:
103 Troy Avenue
CONTACT NAME: Sonny Scozzari
PO NO:
Jacksonville. NC 28540
REPORT TO: Sonny Scozzari / Alberta Y. Okamoto
PHONE/FAX: [phone]
COPY TO:
cnanes.scozzan(dlusmc.md
email: alberta.okamotoCdfusmc mil
Sampled By:
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
/ Collection
Semple
Type
E a o
o
t o
`"
I i
"
LAB ID
NUMBER
PRESERVATION .
ANALYSIS REQUESTED
/
Date
Time
Temp
2
x
=
_
g
_
o
gg
Bear Trail Golf
j.7121
1 / 3'0
SL
C
�p
G
E�\�
X
Aluminum, Arsenic, Cad ium, Calcium,
Chromium, Copper, Lead, Magnesium,
.
1P
r--0A- g ( PO—
Molybdenym, Nickel, Potassium,
Selenium,, Sodium, Zinc, Ammonia
G
G
1 LC
•
C
p
Nitrogen, Total Kjeldahl Nitrogen (TKN),
Nitrate+Nitrite-Nitrogen, Total Solids(%),
G
G
C
p
pH, Total Phosphorus, Mercury
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
nquished By:
Date/Time
Received By:
i Date/Time
eV
'/
4
41 /Z-t 0 T30
•
2.
/
,
Temperature when Received: (J I C Accepted: Resample Reques ed:
Delivered By: Received p—^=D 7- Date: 21g�-Time: \
Comments:
TURNAROUND:

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Wallace WWTP
Wallace, North Carolina
Triple S Farms
Wallace WWT,P
2021-01193
1/22/2021
2/18/2021
1st Quarter 2021
Type of Stabilization: Non
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
1.80
Nitrogen (TKN)*
4.860
48,600.000
Phosphorus
2.750
27,500.000
Potassium
0.426
4,260.000
Sulfur
0.000
Calcium
2.440
24,400.000
Magnesium
0.342
3,420.000
Sodium
0.382
3,820.000
Iron
---
Aluminum
---
12,900.000
Manganese
---
Copper
---
783.000
1,500
Zinc
---
1,320.000
2,800
Ammonia Nitrogen*
0.084
841.000
Nitrate N / Nitrite N*
---
2.050.000
Cadmium
---
27.200
39
Chromium
---
35.700
1,200
Nickel
---
27.200
420
Lead
---
51.300
300
Arsenic
---
38.100
41
Mercury
---
2.230
17
Selenium
---
27.200
100
pH
6.430
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
4.776
Molybdenum
---
27.200
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wallace WWTP
Wallace, North Carolina
Triple S Farms
1st Quarter 2021
2/18/2021 Report No: WL 1-2021-01193
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
33.596
PAN Inj.
34.437
P
55.000
K
8.520
Lime (estimated)
0.000
Secondary Nutrients
Calcium
48.800
Magnesium
6.840
Sodium
7.640
SAR
0.812
Chloride
0.000
Iron
0.000
Alumium
25.800
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
1.80
pH
6.430
Min Rate
0.300
Metals
Arsenic
0.076
Cadmium
0.054
Chromium
0.071
Copper
1.566
Lead
0.103
Mercury
0.004
Molybdenum
0.054
Nickel
0.054
Seleniun
0.054
Zinc
2.640

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Feb 18, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2021-01193
Project ID: WWTP Sludge
Chlorobenzene (TCLP)
Chloroform (TCLP)
Methyl ethyl ketone (TCLP)
Tetrachloroethylene (TCLP)
Trichloroethylene (TCLP)
Vinyl Chloride (TCLP)
RCI
Cyanide
Sulfide
Ignitability
pH
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
SW846 Method 8260/5030
SW846 Method B260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SM 4500 CN D
SM 4500 S D
SW 846 method 1010
SW 846 Method 9045D
EPA 200.7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA2007
EPA 200 7
EPA2007
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 353 2
SM 2540 B
SM 4500 NH3 C
SM 4500 Org B
<0.01 mg/L 01/29/2021
<0.01 mg/L 01/29/2021
<0.05 mg/L 01/29/2021
<0.01 mg/L 01/29/2021
<0.01 mg/L 01/29/2021
<0.01 mg/L 01/29/2021
<1.0 mg/kg 02/01/2021
0.15 mg/kg 02/01/2021
>200 °F 02/16/2021
6.43 units 02/16/2021
12900 mg/kg 01/29/2021
38.1 mg/kg 01/29/2021
<27.2 mg/kg 01/29/2021
24400 mg/kg 01/29/2021
35.7 mg/kg 01/29/2021
783 mg/kg 01/29/2021
51.3 mg/kg 01/29/2021
3420 mg/kg 01/29/2021
<27.2 mg/kg 01/29/2021
<27.2 mg/kg 01/29/2021
4260 mg/kg 01/29/2021
<27.2 mg/kg 01/29/2021
3820 mg/kg 01/29/2021
1320 mg/kg 01/29/2021
2050 mg/kg 01/29/2021
1.80 % 01/25/2021
841 mg/kg 01/25/2021
48600 mg/kg 01/25/2021
Report * 2021.01193 Page 2 of 4

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Feb 18, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2021-01193
Project ID: WWTP Sludge
Total Phosphorus
Mercury
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
SM 4500 P F
SW846 7471 B
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200 7
EPA 200 7
EPA 245 1
27500 mg/kg
2.23 mg/kg
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<0.0002 mg/L
01/29/2021
01/25/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
01/29/2021
Lab ID
21-02951
Test
Sample ID:
Site: 1
Collect Date/Time Matrix
1/22/2021 9:50 AM Solid/Sludge
Method Results
Sampled
In Young
by
Seo
Date Analyzed
Total Solids (%)
Fecal Density
Lab ID
21-02952
Test
Sample ID:
Site: 2
SM 2540 B
SM 9221C E MPN 24 hr 503
Method
1.98%
2273 MPN/g
Collect Date/Time Matrix
1/22/2021 9:50 AM Solid/Sludge
Results
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
01/25/2021
01/22/2021
Sampled
In Young
by
Seo
Date Analyzed
1.88%
2394 MPN/g
01/25/2021
01/22/2021
Lab ID
21-02953
Test
Sample ID:
Site: 3
Total Solids (%)
Fecal Density
Collect Date/Time
1/22/2021 9:50 AM
Method
Matrix
Solid/Sludge
Results
Sampled by
In Young Seo
Date Analyzed
SM 2540 B
SM 9221C E MPN 24 hr 503
1.90%
1053 MPN/g
01/25/2021
01/22/2021
Report 8 2021 01193 Page 3 of 4

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Wallace WWTP
Wallace, North Carolina
Triple S Farms
Wallace WWTP
2021-06258
4/19/2021
4/30/2021
2nd Quarter 2021
Type of Stabilization: ENon
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.71
Nitrogen (TKN)*
5.380
53,800.000
Phosphorus
2.540
25,400.000
Potassium
0.432
4,320.000
Sulfur
0.000
Calcium
1.980
19,800.000
Magnesium
0.300
3,000.000
Sodium
0.331
3,310.000
Iron
---
Aluminum
---
9,850.000
Manganese
---
Copper
---
601.000
1,500
Zinc
---
1,070.000
2,800
Ammonia Nitrogen*
0.205
2,050.000
Nitrate N / Nitrite N*
---
4.040
Cadmium
---
19.900
39
Chromium
---
28.000
1,200
Nickel
---
19.900
420
Lead
---
38.000
300
Arsenic
---
22.000
41
Mercury
---
2.840
17
Selenium
---
19.900
100
pH
7.400
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.175
Molybdenum
---
19.900
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wallace WWTP
Wallace, North Carolina
Triple S Farms
2nd Quarter 2021
4/30/2021 Report No: WL 2-2021-0625g
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
33.108
PAN Inj.
35.158
P
50.800
K
8.640
Lime (estimated)
0.000
Secondary Nutrients
Calcium
39.600
Magnesium
6.000
Sodium
6.620
SAR
0.951
Chloride
0.000
Iron
0.000
Alumium
19.700
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
2.71
pH
7.400
Min Rate
0.300
Metals
Arsenic
0.044
Cadmium
0.040
Chromium
0.056
Copper
1.202
Lead
0.076
Mercury
0.006
Molybdenum
0.040
Nickel
0.040
Seleniun
0.040
Zinc
2.140

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
info'! environmentalchemists.com
Branch Residuals/Bob Branch
Attention: Bob Branch
Date of Report: Apr 30, 2021
Customer PO #:
Customer ID: 15060009
Report #: 2021-06258
Project ID: Wallace WWTP
Lab ID
21-15552
Sample ID:
Site: Sludge
Collect Date/Time Matrix Sampled by
4/19/2021 9:25 AM Solid/Sludge Sean Pistorino
Test Method Results Date Analyzed
Sludge Residuals
PAN
Used 30% Mineralization Rate.
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
pH
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
Calculation
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 353.2
SM 2540 B
SM 4500 H B
SM 4500 NH3 C
SM 4500 Org B
SM 4500 P F
SW846 74716
16500 mg/kg 04/30/2021
9850 mg/kg 04/20/2021
22.0 mg/kg 04/20/2021
<19.9 mg/kg 04/20/2021
19800 mg/kg 04/20/2021
28.0 mg/kg 04/20/2021
601 mg/kg 04/20/2021
38.0 mg/kg 04/20/2021
3000 mg/kg 04/20/2021
<19.9 mg/kg 04/20/2021
<19.9 mg/kg 04/20/2021
4320 mg/kg 04/26/2021
<19.9 mg/kg 04/20/2021
3310 mg/kg 04/22/2021
1070 mg/kg 04/20/2021
4.04 mg/kg 04/23/2021
2.71 % 04/19/2021
7.40 units 04/27/2021
2050 mg/kg 04/21/2021
53800 mg/kg 04/21/2021
25400 mg/kg 04/27/2021
2.84 mg/kg 04/21/2021
Report # 2021-06258 Page 1 of 3

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
info@environmentalchem ists.com
Client: Branch Residuals/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: ,;7c) .2 I— v t • 2.5V"
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, Public Works
PO NO:
R
REPORT TO:
PHONE/FAX: [phone]
COPY TO: Lisa Cottle, ORC
email: [e-mail]
Sampled By: (,, P hv,
SAMPLE TYPE: 1= Influent. E = Effluent W = Well ST = SO =Soil SL = Slud a Other•
Sample Identification
Collection
Et
A
'"
Composite
or
Grab
Container I
(P or G)
o f
"
LAB ID
NUMBER •
PRESERVATION
9,
REQUESTED
Date
Time
Temp
Z
z
-,
=
o
2_
8
o
z
o
~
Li
o
Sludge
C
P
r�1
15�
X
nutrients/metals
4 -(1-ZI
'.1 Z5
G
G
1)
C
P
5�3�
)
X
fecal density/ %TS
it-Iq -21
9• Z 5
G
G
2)
C
P
1 59'
X
fecal density/ %TS
4-1'1-11
el : 25
G
G
3)
C
P
)5541
X
fecal density/ %TS
4 - IK -ZI
6r. 2,5
G
G
4)
l y� i
X
fecal density/ %TS
Lt - IK - 21
9.15
G
G
5)
C
P
I -51'3
X
fecal density/ %TS
(-1.- Pt -U
9. a 5
G
G
6)
C
P
1 `4
X
fecal density/ %TS
4- IK - 21
ci- Z 5
G
G
7)
C
P
) 550
X
fecal density/ %TS
4-i9 -2.1
q: Z5
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
ic.A.. P ,m—
4 - «- Z i
2.
_ s'
it
emperature when Keceived:
ccepted:
R ' cted: Resample
sted:
qu
Delivered By: Received By: Date: Time:
Comments: TURNA - OUND:

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Wallace WWTP
Wallace, North Carolina
Triple S Farms
Wallace WWTP
2021-12254
7/21/2024
9/14/2024
3rd Quarter 2021
Type of Stabilization:
7-�
vNon:
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.09
Nitrogen (TKN)*
6.180
61,800.000
Phosphorus
2.330
23,300.000
Potassium
3.770
37,700.000
Sulfur
0.000
Calcium
19.400
194,000.000
Magnesium
2.780
27,800.000
Sodium
0.612
6,120.000
Iron
---
Aluminum
---
92.800.000
Manganese
---
Copper
---
722.000
1,500
Zinc
---
1,390.000
2,800
Ammonia Nitrogen*
0.657
6,570.000
Nitrate N / Nitrite N*
---
1.760.000
Cadmium
---
35.700
39
Chromium
---
35.700
1,200
Nickel
---
35.700
420
Lead
---
39.600
300
Arsenic
---
35.700
41
Mercury
---
1.330
17
Selenium
---
35.700
100
pH
7.620
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.523
Molybdenum
---
35.700
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wallace WWTP
Wallace, North Carolina
Triple S Farms
3rd Quarter 2021
9/14/2021 Report No: WL 3-2021-12254
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
43.228
PAN Inj.
49.798
P
46.600
K
75.400
Lime (estimated)
0.000
Secondary Nutrients
Calcium
388.000
Magnesium
55.600
Sodium
12.240
SAR
0.496
Chloride
0.000
Iron
0.000
Alumium
185.600
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
2.09
pH
7.620
Min Rate
0.300
Metals
Arsenic
0.071
Cadmium
0.071
Chromium
0.071
Copper
1.444
Lead
0.079
Mercury
0.003
Molybdenum
0.071
Nickel
0.071
Seleniun
0.071
Zinc
2.780

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Sep 14, 2021
Customer PO #:
Customer ID: 15060009
Report #: 2021-12254
Project ID: Wallace WWTP
Lab ID
21-30536
Test
Sample ID:
Site: Sludge
Method
Collect Date/Time Matrix Sampled by
7/21/2021 9:40 AM Solid/Sludge client
Results
Date Analyzed
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Nitrate+Nitrite-Nitrogen
Total Solids (%)
pH
EPA 200 7
EPA 200 7
EPA 200.7
EPA 200 7
EPA 200.7
EPA 200 7
EPA2007
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 353.2
SM 2540 B
SM 4500 H B
Result estimated. Analyzed out of 15 minutes hold time.
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
SM 4500 NH3 C
SM 4500 Org B
SM 4500 P F
SW846 7471 B
92800 mg/kg 07/26/2021
<35.7 mg/kg 07/28/2021
<35.7 mg/kg 07/28/2021
194000 mg/kg 07/26/2021
<35.7 mg/kg 07/28/2021
39.6 mg/kg 07/28/2021
27800 mg/kg 07/26/2021
<35.7 mg/kg 07/28/2021
<35.7 mg/kg 07/28/2021
37700 mg/kg 07/26/2021
<35.7 mg/kg 07/28/2021
6120 mg/kg 08/03/2021
1760 mg/kg 07/27/2021
2.09 % 07/23/2021
7.62 units 07/28/2021
6570 mg/kg 07/26/2021
61800 mg/kg 07/23/2021
23300 mg/kg 07/30/2021
1.33 mg/kg 07/29/2021
Lab ID
21-30536A
Test
Sample ID:
Site: Sludge
Method
Collect Date/Time
7/21/2021 9:40 AM
Matrix Sampled by
Solid/Sludge client
Results Date Analyzed
Copper
Zinc
EPA 200.7
EPA 200.7
722 mg/kg
1390 mg/kg
07/28/2021
07/28/2021
Report #:: 2021-12254 Page 1 of 3

Analytical 8, Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
info@envi ronmentalchem ists.com
Client: Branch Residuals/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: •c:)1. — I Tug'
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, Public Works
PO NO:
REPORT TO:
PHONE/FAX: [phone]
COPY TO: Lisa Cottle, ORC
email: [e-mail]
Sampled Bv:
eo
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other.
Sample Identification
Collection
!A
in ~
Composite
or
Grab
Container
(P or G)
a m
tom'. E
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
W
o
Z
-.
u
$
2
=
=
=
=
/
o
W
x
o
Sludge
17-^'-I- !
Q? yv
C
P
30 s-3
clf
nutrients/metals
G
G
1)
''" -'f
pgIto
c
P
-53-Ca.
X
fecal density/ %TS
G
G
2)
Y)-)I'ii
°GI 40C
P
�
30✓)
X
fecal density/ %TS
G
G
3)
`9-21-11
G q 1 ,
C
P
X
fecal density/ %TS
G
G
4)
7-}i-'4
°CNC'
C
P
J
Jr
X
fecal density/ %TS
G
G
5)
7-4'1
CA uo
c
P
j L)
X
fecal density/ %TS
G
G
6)
1'y1-7/
OCI4C
C
P
C
X
fecal density/ %TS
G
G
7)
i-14--�
ogyc,
C
P-,/
3
X
fecal density/ %TS
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
2.
Temperature when Received:
Delivered By:
,7,�aLlwi ;ec
t
,42
Accepted:
Comments:
-)-
Resample Requested:
Received By: _ Date: Z. �
Time:
TURNAROUND: �(1�
! `

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Triple S Farms
Wallace WWTP
Wallace, North Carolina
Triple S Farms
Wallace WWTP
2021-17320
10/4/2021
10/29/2021
4th Quarter 2021
Type of Stabilization: on }r k
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.71
Nitrogen (TKN)*
4.950
49,500.000
Phosphorus
2.160
21,600.000
Potassium
0.439
4,390.000
Sulfur
0.000
Calcium
2.570
25,700.000
Magnesium
0.366
3,660.000
Sodium
0.513
5,130.000
Iron
---
Aluminum
---
10,500.000
Manganese
---
Copper
---
775.000
1,500
Zinc
---
1,410.000
2,800
Ammonia Nitrogen*
0.216
2,160.000
Nitrate N / Nitrite N*
---
10.600
Cadmium
---
18.100
39
Chromium
---
28.200
1,200
Nickel
---
19.300
420
Lead
---
35.800
300
Arsenic
---
18.100
41
Mercury
---
1.000
17
Selenium
---
18.100
100
pH
7.400
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
4.734
Molybdenum
---
18.100
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wallace WWTP
Wallace, North Carolina
Triple S Farms
4th Quarter 2021
10/29/2021 Report No: WL 4-2021-17320
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
30.585
PAN Inj.
32.745
P
43.200
K
8.780
Lime (estimated)
0.000
Secondary Nutrients
Calcium
51.400
Magnesium
7.320
Sodium
10.260
SAR
1.302
Chloride
0.000
Iron
0.000
Alumium
21.000
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
2.71
pH
7.400
Min Rate
0.300
Metals
Arsenic
0.036
Cadmium
0.036
Chromium
0.056
Copper
1.550
Lead
0.072
Mercury
0.002
Molybdenum
0.036
Nickel
0.039
Seleniun
0.036
Zinc
2.820

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infojenvironmentalchemists.com
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Date of Report: Oct 29, 2021
Customer PO #:
Customer ID: 15060009
Report #: 2021-17320
Project ID: Wallace WWTP
Lab ID
21-43460
Test
Sample ID:
Site: Sludge
Method
Collect Date/Time Matrix Sampled by
10/4/2021 7:15 AM Solid/Sludge Sean Pistorino
Results Date Analyzed
Sludge Residuals
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Aluminum
Chromium
Nitrate+N itrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7, Rev. 4.4, 1994
EPA 200.7, Rev. 4.4, 1994
EPA 353.2
SM 2540 B
SM 4500 NH3 C-2011
SM 4500 Norg B-2011
SM 4500 P F-2011
pH SW 846 Method 9045D
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-846 7471 B
<18.1 mg/kg 10/15/2021
<18.1 mg/kg 10/15/2021
25700 mg/kg 10/15/2021
775 mg/kg 10/20/2021
35.8 mg/kg 10/15/2021
3660 mg/kg 10/15/2021
<18.1 mg/kg 10/15/2021
19.3 mg/kg 10/15/2021
4390 mg/kg 10/15/2021
<18.1 mg/kg 10/15/2021
5130 mg/kg 10/15/2021
1410 mg/kg 10/15/2021
10500 mg/kg 10/15/2021
28.2 mg/kg 10/15/2021
10.6 mg/kg 10/05/2021
2,71 % 10/04/2021
2160 mg/kg 10/05/2021
49500 mg/kg 10/05/2021
21600 mg/kg 10/07/2021
7.40 units 10/26/2021
1.00 mg/kg 10/19/2021
Report*. 2021-17320 Page 1 of 3

Analytical 8 Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Branch Residuals/Bob Branch
PROJECT NAME:
REPORT NO: 'i' I 7T-ZO
ADDRESS: 1735 Heckle Blvd.
Site:
PO NO:
Suite 103-291
REPORT TO: Bob Branch
PHONE/FAX:
Rock Hill, SC 29732
COPY TO:
email:
Sampled By: Sem
SAMPLE TYPE: 1= Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
Sample Type
Composfte
or Grab
c
3 o
o n
c, —
c
c o,
L E
'
`o
xn
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
NONE
HCL
o
H
...
c
z
x
NAOH
THIO
FILTERED
OTHER
1) Feco..1 Or S-5 tk)
x
fecal density, % total solids
IO-4-LI
'7; 15
a
G
2) Fccoi Dc,- sl (I)
C
Q
(41162
x
fecal density, % total solids
t0-4-lt
.7: 13
)
G
1
3) �cc&\ D ,1 C3)
C
"I-341.3
x
fecal density, % total solids
lv-'4-Z(
7.1 5
5
G
4) F�,� ��5 �H�
c
4U
3U16-I
x
fecal density, % total solids
1p-y-Z1
7� 1 5
Q
G
5) Ft Dt ns,% l5,
" 3\45
x
fecal density, % total solids
to-- 4 - z1
15
®
G
6) Ftaj ki (6
C
e
l)
v`�
x
fecal density, % total solids
(0-4 -11
7-.1-.1-
6)
G
7) ( rj j ei)
C
(0
L
`-4/(4"�
x
fecal density, % total solids
10-4 - ?A-7:
15
©
G
Nui-r;MI) /NA-O S
C
(ED
�
`,"> '
�I3°
10-ti-zt
1 :15
Q
G
Transfer
Relinquished By:
Date/Time
• ceived By:
Date/Time
1.
,Dt,o~
I9
10 - LI - Z.l
1
/Cl/ t4f,
;,.--
2.
Temperature when Rece
Delivered By:
Comments:
ved °C: -f1G
Accepted: ✓ Rejected:
Received By: (A
Resam pl��� Requested:
Date: Time: Th Nig"
TURNAROUND:

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Town of Warsaw
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
WR 2021-15014
8/31/2021
10/6/2021
Annual 2021
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
2.470
Nitrogen (TKN)
2.780
27,800.000
Phosphorus
1.290
12,900.000
Potassium
0.283
2,830.000
Sulfur
0.000
Calcium
2.080
20,800.000
Magnesium
0.139
1,390.000
Sodium
0.198
1,980.000
Iron
---
Aluminum
---
10,900.000
Manganese
---
0.000
Copper
---
249.000
1,500
Zinc
---
721.000
2,800
Ammonia Nitrogen
0.091
907.000
Nitrate N / Nitrite N
---
4,820.000
Cadmium
---
13.400
39
Chromium
---
20.600
1,200
Nickel
---
13.400
420
Lead
---
25.100
300
Arsenic
---
13.400
41
Mercury
---
0.761
17
Selenium
---
13.400
100
pH
5.650
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
2.689
Molybdenum
---
13.400
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

Date Reported:
Wastewater Treatment Plant
Warsaw WWTP
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2021
10/6/2021 Report No: WR 2021-15014
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
26.683
PAN Inj.
27.590
P
25.800
K
5.660
Lime (estimated)
0.000
Secondary Nutrients
Calcium
41.600
Magnesium
2.780
Sodium
3.960
SAR
0.563
Chloride
0.000
Iron
0.000
Alumium
21.800
Manganese
0.000
Boron
0.000
Sulfur
0.000
Physical Characteristics
% Solids
2.47
pH
5.650
Min Rate
0.300
Metals
Arsenic
0.027
Cadmium
0.027
Chromium
0.041
Copper
0.498
Lead
0.050
Mercury
0.002
Molybdenum
0.027
Nickel
0.027
Seleniun
0.027
Zinc
1.442

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ihfo@a cnvironmentalchenlists.com
Town of Warsaw
PO Box 464
Warsaw NC 28398
Attention: Angie Miller
Date of Report: Oct 08, 2021
Customer PO #:
Customer ID: 09070029
Report #: 2021-15014
Project ID: Wastewater
Lab ID Sample ID:
21-37582 Site: Sludge
Test
Method
Collect Data/Time Matrix Sampled by
8/31/2021 Solid/Sludge Greg Hughes
Results Date Analyzed
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Llndane (TCLP)
Methoxychlor (TCLP)
Toxaphene (TCLP)
1,4-Dlchlorobenzene (TCLP)
2,4,5-Trichtorophenol (TCLP)
2,4,6-Trichiorophenol (TCLP)
2,4-Dlnitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1,1-Dichloroethylene (TCLP)
1,2-Dichioroethane (TCLP)
Benzene (TCLP)
Carbon Tetrachloride (TCLP)
SW 848 Method 80518/3510
SW 845 Method 80818/3510
SW 845 Method 8081913510
SW 84e Method 008te/3510
SW 845 Method 80818/3510
SW 848 Method 80818/3510
SW 848 Method 8081S/3510
SW 848 method 8270/3510
SW 848 method 8270/3510
SW 848 method 8270/3510
SW 845 method 8270/3510
SW 646 method 8270/3510
SW 840 method 8270/3510
SW 848 method 8270/3510
SW 845 method 8270/3510
SW 848 method 8270/3510
SW 848 method 8270/3510
SW 848 method 8270/3510
SW 845 method 8270/3510
SW 848 method 8270/3510
SW848 Method 8151A
SW848 Method 8161A
SW848 Method 0250/5030
SW848 Method 8280/5030
SW846 Method 8280/5030
SW848 Method 8280/6030
<0.02 mg/L 09/14/2021
<0.0005 mg/L 09/14/2021
<0.0005 mg/L 09/14/2021
<0.0005 mg/L 09/14/2021
<0.0005 mg/L 09/14/2021
<0.0005 mg/L 09/14/2021
<0.05 mg/L 09/14/2021
<0.060 mg/L 09/0812021
<0.050 mg/L 09/08/2021
<0,050 mg/L 09/08/2021
<0.050 mg/L 09/08/2021
<0.050mg/L 09/08/2021
<0.050 mg/L 09/08/2021
<0.050 mg/L 09/08/2021
<0.050 mg/L 09/08/2021
<0.050 mg/L 09/08/2021
<0.050 mg/L 09/08/2021
<0.050 mg/L 09/08/2021
<0.250 mg/L 09/08/2021
<0.050 mg/L 09/08/2021
<0.003 mg/L 09/13/2021
<0.003 mg1L 09/13/2021
<0.01 mg/L 09/09/2021
<0.01 mg/L 09/0912021
<0.01 mg/L 09/09/2021
<0.01 mg/L 09/09/2021
Report 0:: 2021.16014 Pepe 2 of 4

ANALYTICAL a CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lob • 910.392.4424 Fax
710 t3owserlotvn Road, Monleo, NC 27954 ° 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info@environmenlalcbc nists.com
Town of Warsaw
PO Box 464
Warsaw NC 28398
Attention: Angie Miller
Date of Report: Oct 06, 2021
Customer PO #:
Customer ID: 09070029
Report #: 2021-15014
Project ID: Wastewater
Chlorobenzene (TCLP) swim Method 62em5030 <0.01 mg!L 09/09/2021
Chloroform (TCLP) SW846 Method 6260/5030 <0.01 mglL 09/09/2021
Methyl ethyl ketone (TCLP) SW846 Method 6260/5030 <0.05 mg!L 09/09/2021
Telrachloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg!L 09/09/2021
Trichloroethylene (TCLP) SW846 Method 826015030 <0.01 mglL 09/09/2021
Vinyl Chloride (TCLP) SW846 Method 8280/5030 <0.01 mglL 09/09/2021
RCI
Cyanide SM 4500 CN 0 <1.0 mg/kg 09/09/2021
Sulfide SM 4500 S D <0.05 mg/kg 09/13/2021
IgnItabllity SW 846 method 1010 >195°F 09/13/2021
Sludge Residuals
Aluminum EPA200.7 10900 mg/kg 09/20/2021
Arsenic EPA 200.7 <13.4 mg/kg 09/20/2021
Cadmium EPA200.7 <13.4mg/kg 09/20/2021
Calcium EPA200.7 20800mg/kg 09120/2021
Chromium EPA200.7 20.6mg/kg 09/20/2021
Copper EPA200.7 249mg/kg 09/20/2021
Lead EPA 200.7 25.1 mg/kg 09/20/2021
Magnesium EPA200.7 1390mg/kg 09/20/2021
Molybdenum EPA200.7 <13.4 mg/kg 09/20/2021
Nickel EPA200.7 <13.4mg/kg 09/20/2021
Potassium EPA200.7 2830 mg/kg 09/20/2021
Selenium EPA200.7 <13.4 mg/kg 09/20/2021
Sodium EPA 200.7 1980 mg/kg 09/22/2021
Zinc EPA200.7 721 mg/kg 09/20/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 4820 mg/kg 09/02/2021
Total Solids (%) SM 2540 s 2.47 % 09/01/2021
pH SM 4500 H 9 5.65 units 09/09/2021
Result estimated. Analyzed out of 16 minutes hold time.
Ammonia Nitrogen SM 4500 NH3 C 907 mg/kg 09/03/2021
Report IC: 2021.15014
Page 3 of 4

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manioc), NC 27954 • 252.473.5702 Lab/Pax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Warsaw Date of Report: Oct 06, 2021
PO Box 464 Customer PO #:
Warsaw NC 28398 Customer ID: 09070029
Attention: Angie Miller Report #: 2021-15014
Project ID: Wastewater
Total Kjetdahl Nitrogen (TKN) SM45000rge 27800 mg/kg 09/09/2021
Total Phosphorus SM 4500 P F 12900 mg/kg 09/08/2021
Mercury 8W64574710 0.7810mg/kg 09/10/2021
TCLP Metals
Arsenic EPA 200.7 <1.0 mglL 09/16/2021
Barium EPA 200.7 <1.0 mg/L 09/15/2021
Cadmium EPA 200.7 <1.0 mglL 09/16/2021
Chromium EPA200.7 <1.0mg/L 09/15/2021
Lead EPA 200.7 <1.0 mg/L 09/15/2021
Selenium EPA200.7 <1.0mglL 09/15/2021
Silver EPA 200.7 <1.0 mglL 09/15/2021
Mercury EPA 245.1 <0.0002 mg/L 09/10/2021
Comment: Sludge residual, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: -11
_, imAic
ReportA:: 2021.16014 Page 4 of 4

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COL
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
info@environmentalchem ists.com
Client: Town of Warsaw WWTP
PROJECT NAME: WWTP-3/week monitoring
REPORT NO: , - 4 -o
ADDRESS: Post Office Box 464
SITE:
PO NO:
Warsaw, NC 28398
REPORT TO: Greg Hughes, Town of Warsaw
PHONE/FAX: [phone]
COPY TO: Stanley/Angie Miller (Miller Utility)
email: [e-mail]
Sampled By:
AMPLE TYPE: 1= Influent_ E = Effluent W = Well ST =Stream SO = 5oil SL -
Sample Identification
Collection
Sample Type
Composite
or Grab
Container
(P or G)
d
o f
m
x
c
o.
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
z
z
fo
=
p
=
Q
z
o
~
w
c
Inf composite (3/week)
(t3?
P
1(X
BOD,TSS
$-31-2-1
MO
G
G
Eff composite (3/week)
m
P
�i►
o
f
X
BOD TSS
31- Z.c1'(
G
G
Eff composite (3/week)
©
P
£. 6
X
c--
NH3
« 3)- za
OP -to
G
G
Jan,Apr,Jui3October
C
P
X
Total N (calc), Total P
G
G
(due quarterly)
C
P
G
G
Eff grab (3/week)
C
P
L??5"-0
X
Fecal Coliform
ce j
OVy .
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
2. - -- .
. ,. 7
Delivered By:
Comments:
�-- Accepted:
Received By:
ed:
Resample Requested:
Date: Time: 1!)1"6:)
TURNAROUND:

TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORTS

A TCLP ANALYSIS IS REQUIRED FOR THE FOLLOWING FACILITIES:
TOWN OF WALLACE
TCLP DATA IS REQUIRED ONCE PER PERMIT CYCLE
FOR THE OTHER FACILITIES

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info environmentalchemists.com
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Feb 18, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2021-01193
Project ID: WWTP Sludge
Lab ID
21-02950
Test
Sample ID:
Site: Sludge
Method
Collect Date/Time Matrix Sampled by
1/22/2021 9:50 AM Solid/Sludge In Young Seo
Results Date Analyzed
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychior (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenol (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol (TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1,1-Dichloroethylene (TCLP)
1,2-Dichloroethane (TCLP)
Benzene (TCLP)
Carbon Tetrachloride (TCLP)
SW 846 Method 8081B/3510
SW 846 Method 8081/3/3510
SW 846 Method 808113/3510
SW 846 Method 8081 B/3510
SW 846 Method 8081B/3510
SW 846 Method 8081/3/3510
SW 846 Method 8081 B/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW846 Method 8151A
SW846 Method 8151A
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
<0.02 mg/L 02/04/2021
<0.0005 mg/L 02/04/2021
<0.0005 mg/L 02/04/2021
<0.0005 mg/L 02/04/2021
<0.0005 mg/L 02/04/2021
<0.0005 mg/L 02/04/2021
<0.05 mg/L 02/04/2021
<0.050 mg/L 02/03/2021
<0.050 mg/L 02/03/2021
<0.050 mg/L 02/03/2021
<0.050 mg/L 02/03/2021
<0.050 mg/L 02/03/2021
<0.050 mg/L 02/03/2021
<0.050 mg/L 02/03/2021
<0.050 mg/L 02/03/2021
<0.050 mg/L 02/03/2021
<0.050 mg/L 02/03/2021
<0.050 mg/L 02/03/2021
<0.250 mg/L 02/03/2021
<0.050 mg/L 02/03/2021
<0.003 mg/L 02/01/2021
<0.003 mg/L 02/01/2021
<0.01 mg/L 01/29/2021
<0.01 mg/L 01/29/2021
<0.01 mg/L 01/29/2021
<0.01 mg/L 01/29/2021
Report #. 2021-01193 Page 1 of 4

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Feb 18, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2021-01193
Project ID: WWTP Sludge
Chlorobenzene (TCLP)
Chloroform (TCLP)
Methyl ethyl ketone (TCLP)
Tetrachloroethylene (TCLP)
Trichloroethylene (TCLP)
Vinyl Chloride (TCLP)
RCI
Cyanide
Sulfide
Ignitability
pH
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 8260/5030
SW846 Method 6260/5030
SW846 Method 8260/5030
SM 4500 CN D
SM 4500 S D
SW 846 method 1010
SW 846 Method 9045D
EPA 200.7
EPA 200 7
EPA 200 7
EPA 200 7
EPA2007
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 3532
SM 2540 B
SM 4500 NH3 C
SM 4500 Org B
<0.01 mg/L 01/29/2021
<0.01 mg/L 01/29/2021
<0.05 mg/L 01/29/2021
<0.01 mg/L 01/29/2021
<0.01 mg/L 01/29/2021
<0.01 mg/L 01/29/2021
<1.0 mg/kg 02/01/2021
0.15 mg/kg 02/01/2021
>200 °F 02/16/2021
6.43 units 02/16/2021
12900 mg/kg 01/29/2021
38.1 mg/kg 01/29/2021
<27.2 mg/kg 01/29/2021
24400 mg/kg 01/29/2021
35.7 mg/kg 01/29/2021
783 mg/kg 01/29/2021
51.3 mg/kg 01/29/2021
3420 mg/kg 01/29/2021
<27.2 mg/kg 01/29/2021
<27.2 mg/kg 01/29/2021
4260 mg/kg 01/29/2021
<27.2 mg/kg 01/29/2021
3820 mg/kg 01/29/2021
1320 mg/kg 01/29/2021
2050 mg/kg 01/29/2021
1.80 % 01/25/2021
841 mg/kg 01/25/2021
48600 mg/kg 01/25/2021
Report # 2021.01193 Page 2 of 4

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Feb 18, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2021-01193
Project ID: WWTP Sludge
Total Phosphorus
Mercury
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
SM4500PF
SW846 7471B
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200.7
EPA 200.7
EPA 200 7
EPA 200 7
EPA 245 1
27500 mg/kg
2.23 mg/kg
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<0.0002 mg/L
Lab ID
21-02951
Test
Sample ID:
Site: 1
Method
01/29/2021
01/25/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
01/29/2021
Collect Date/Time Matrix Sampled by
1/22/2021 9:50 AM Solid/Sludge In Young Seo
Results
Date Analyzed
Total Solids (%)
Fecal Density
Lab ID
21-02952
Test
Sample ID:
Site: 2
SM 2540 B
SM 9221C E MPN 24 hr 503
1.98%
2273 MPN/g
01/25/2021
01/22/2021
Method
Collect Date/Time Matrix Sampled by
1/22/2021 9:50 AM Solid/Sludge In Young Seo
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
Lab ID
21-02953
Test
Sample ID:
Site: 3
Method
1.88%
2394 MPN/g
01/25/2021
01/22/2021
Collect Date/Time Matrix Sampled by
1/22/2021 9:50 AM Solid/Sludge In Young Seo
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.90%
1053 MPN/g
01/25/2021
01/22/2021
Report 4 2021 01193 Page 3 of 4

PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORMS

PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The Town of Beulaville, Town of Kenansville, Town of Warsaw, and Southwest Plantation meet
pathogen reduction and vector attraction reduction requirements through lime stabilization. The
Town of Wallace met pathogen reduction through fecal density and vector attraction reduction
through injection or incorporation. The Town of Clayton met pathogen reduction and vector
attraction reduction through fecal density and injection and in one instance by SOUR (February
11-23, 2021.)
The forms for these facilities are marked appropriately.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town ofBeulaviIle WWTP
Monitoring Period: From 1/1/2021
To
WQ Permit Number: WQ0030998
NPDES Number: NC0026018
12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed•
Class A:
Alt. A (time/temp) •
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)
❑
=::':: ;`
.................. '
Ait.D (No Prior
Test) •
Process to Further Reduce Pathogengs
•
•
If applicable to alternative
.
performed (Class A onh) indicate "Process to Further Reduce Pathogens":
Compost •
Heat Drying ❑
Heat Treatment 0
Thennophilic •
Beta Ray ■
Gamma Ray
•
Pasteurization •
Class B:
Alt. (1) Fecal Density
Alt. (2) Process to Significantly
Reduce Pathogens I I
•
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
o
Air Drying
•
Composting ❑
Aerobic Digestion ■
Anaerobic Digestion
•
I ::
If applicable to alternative performed (Class A or Class 16) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
-Number of
Excey
dences
Frequency
of
of Analysis
Sample
T e
Type
Analytical
Tech -
niaue
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
chon (15A NCAC 02T .1107) -
-
Alt.1 (VS reduction)
•
Alt. 2 (40-day bench) •
Alt. 3 (30-day bench) •
Alt. 4 (Spec. 02 uptake)
■
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) •
Alt. 8 (Drying - Unstable)
•
Alt. 9 (Injection)
•
Alt. 10 (Incorporation) •
No vector attraction reduction alternatives were performed
•
ERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Stanley Miller, WWTP ORC
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature,pf Preparer*
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Clayton
WWTP Name: Little Creek Water Reclamation Facility
Monitoring Period: From 1/1/2021 To
WQ Permit Number
NPDES Number:
3/31/2021
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and a
WQ0023178 &
WQ0030998
NC0025453
Class A:
Alternative 1 ❑
Alternative
Alternative
2 •
3 •
Alternative 4 •
Alteniative 5 •
Alternative 6 ■
If applicable to alternative
performed (Class
A only) indicate "Process to Further
Reduce Pathogens":
Compost •
Heat Drying 0
Heat Treatment ■
herntophilic •
Beta Ray 0
Gamma Ray
■
Pasteurization
0
Class B:
Alterative
Alternative
1 v
2 •
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
•
Air Drying •
Composting
Aerobic Digestion
•
•
Anaerobic Digestion 0
I
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number of
Excee-
rienre,
Frequency
of Anal
Analysis
Sample
Type
Anal tfcal
Tech -
ninue
SM18
9221 E
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
20,000
40,626
81 000
MPN/
Gram
0
Quarterl y
Grab
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
eduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
0
Alt. 3 (30-day bench) •
Alt. 4 (Spec. 02 uptake)
o
Alt. 5 (14-Day Aerobic)
•
Alt. 6 (Alk. Stabilization
•
Alt. 8 (Drying - Unstable)
Alt 7 (Drying - Stable) •
•
Alt. 9 (Injection)
0
Alt. 10 (Incorporation)
•
No vector attraction reduction alternatives were performed
•
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
El
Mr. William Simpson, WRF ORC
Preparer Name and Title (type or print)
Digitally signed by William Simpson
William Simpson ON: cn=WIRWmSimpson,o=TownofC
Resources. emaN=wslmpso05'00' oNl
�r° °a=Wa'e` Eric R Smith
aytannaorg.c=US
Signature of Preparer* Date
Mr. Eric R. Smith, Land Applier ORC
Land Applier Name and Title (if applicable)(type or print)
Digitally signed by Eric R Smith
DN: cn=Eric R Smith, o=Triple S Farms and Cleaning Inc.,
ou-Land Applier, email=Tripiesfarms@yahoocam, c=US
aeteri!RU.0439 DR.N.59 R5'RR'
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Clayton
WWTP Name: Little Creek Water Reclamation Facility
Monitoring Period: From 4/1/2021
WQ0023178 &
WQ Permit Number: WQ0030998
NPDES Number: NC0025453
To 6/30/2021
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 0
Alternative 2 ■
Alternative 3 ■
......
Alternative 4 0
Alternative 5 ■
Alternative 6 0
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost •
Heat Dryings
Heat Treatment ■
Thennophilic ■
.
Class B:
Alternative 1 El
Alternative 2 ■
• '
If applicable to alternative performed (Class B only) indicate "Process to Significantly
.............
Reduce Pathogens":
Lime Stabilization ■
Air Drying •
Composting ■
Aerobic Digestion •
Anaerobic Digestion •
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dents
Frequency
of Analysis
Sample
Type
Anal 'ttcat
Tech -
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
240,000
419,633
1,000,000
MPN/
Gram
0
Quarterly
Grab
SM18
9221E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction
(40 CFR 503 33) - Please indicate option performed:
Alt. 1 (VS reduction) •
Alt. 2 (40-day bench) •
Alt. 3 (30-day bench) •
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic)
•
Alt. 6 (Alk. Stabilization
■
Alt 7 (Drying - Stable) •
Alt. 8 (Drying - Unstable) ■
Alt. 9 (Injection) ail
Alt. 10 (Incorporation) •
No vector attraction reduction alternatives were performed •
ERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
© "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. William Simpson, WRF ORC
Preparer Name and Title (type or print)
William Simpson
Digitally signed by William Simpson
DN: cn.Willem Simpson,. -Town of
Resources, email.w,impson@townolc
Signature of Preparer* Date
eytonncorg, c.US
Mr. Eric R. Smith, Land Applier ORC
Land Applier Name and Title (if applicable)(type or print)
Digitally signed by Eric R Smith
DN: cn=Eric R Smith, o=Triple S Farms and Cleaning Inc.,
au=Land Applier, email=[e-mail], c=US
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
OENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Clayton
WQ0023178 &
W00030998
NC0025453
WQ Permit Number:
NPDES Number:
To 9/30/2021
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
WWTP Name: Little Creek Water Reclamation Facility
Monitoring Period: From 7 1 2021
Class A:
Alternative
Alternative
s
Alternative
1 ■
2 t
3 ■
Alternative 4 isI
Alternative 5 •
Alternative 6 ■
If applicable to alternative performed (Class A only) indicate "Process
to Further
Reduce Pathogens":
Compost •
Heat Drying ■
Heat Treatment
Thermophilic■
i
•
Beta Ray ■
Gamma Ray
■
Pasteurization 0
Class B:
Alternative 1 a
Alternative 2 •
If applicable to alternative performed (Class B only) indicate "Process to Significantly
Reduce
Pathogens":
Lime Stabilization 0
Air Drying •
Composting
Aerobic Digestion
•
•
Anaerobic Digestion •
I
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
in Sludgede
Pathogen Density
Number of
cec _
deuces
Frequency
of Anal
Analysis
Sample
Type
Analytical
Tech -
niaue
SM18
9221 E
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
130,000
154,347
210,000
MPN/
Gram
0
Quarterly
Grab
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in Lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
eduction (40 CFR 503 33) - Please i
Alt.1 (VS reduction)
•
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. O_ uptake)
Alt. 2 (40-day bench) •
•
Alt. 5 (14-Day Aerobic)
■
Alt. 6 (Alk. Stabilization■
Alt. 8 (Drying - Unstable)
Alt 7 (Drying - Stable) ■
•
Alt. 9 (Injection)
v
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives
were performed
•
CERTIFICATION STATEMENT (please check the appropriate statement)
p "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. William Simpson, WRF ORC
Preparer Name and Title (type or print)
Digitally signed by Wiliam Simpson
William Simpson DN: rn=Wlllam mps:n,:=Town:(Oayron,:u=Water
Resources, emaH=,vsimpsan@tawnalcWytonncorg, c.US
0ate: 2022.02.23 0828.17 .05'00'
Signature of Preparer*
Mr. Eric R. Smith, Land Applier ORC
Land Applier Name and Title (if applicable)(type or print)
Digitally signed by Eric 8 Smith
Dee cn.Enc 8 Smith, o.Tdpl. S Farms and Cleaning Inc.
u=Land Applier, email=Triples([e-mail] c=US
Date:2022.02.23 08,18:10 -05'00'
Eric R Smith
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Clayton
WWTP Name: Little Creek Water Reclamation Facility
Monitoring Period: From 10/1/2021
WQ0023178 &
WQ Permit Number: WQ0030998
NPDES Number: NC0025453
To 12/31/2021
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 •
Alternative 2 •
Alternative 3 ■
:.... _ . .•.
Alternative 4 0
Alternative 5 •
Alternative 6 0
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ■
Heat Drying •
Heat Treatment •
Thertnoplulic 0
Beta Ray •
Ganuna Raz
■
Pasteurization
■
Class B:
Alternative 1 0
Alternative 2
•
If applicable to alternative performed (Class B only) indicate "Process to Significantly
Reduce Pathogens":
Lime Stabilization 0
Air Drying ■
Composting ■
Aerobic Digestion •
Anaerobic Digestion •
I .
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excec-
rtf aces
Frequency
of Analysis
Sample
Type
Anatydcat
Tech -
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
140,000
242,042
450,000
M:PMPN
Gram
0
Quarterly
Grab
SN118
9221E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 M:PN per 4 grams
total solid (dry
weight)
ector Attraction Keduction (40 CFR 503 33) - Please indicate option performed:
Alt.1 (VS reduction)
•
Alt. 2 (40-day bench)
•
Alt. 3 (30-day bench) •
Alt. 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
•
Alt. 6 (Alk. Stabilization
■
Alt 7 (Drying - Stable) •
Alt. 8 (Drying - Unstable)
■
Alt. 9 (Injection)
o
Alt. 10 (Incorporation)
•
No vector attraction reduction alternatives were performed
•
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. William Simpson, WRF ORC
Preparer Name and Title (type or print)
Digitally signed by William Simpson
DN: cn=William Simpson, o=Town of Clayton, eu:Water
Resources, email=wdmpson®townofclaytonncorg, c-US
0a3e:20210223 0828:44 -05'00'
William Simpson
Signature of Preparer* Date
Mr. Eric R. Smith, Land(Applier ORC
Land Applier Name and Title (f2plibable?(type or print)
Eric R Smith
DN: cn=Edc 0 Smith, .Triple 5 Farms and Cleaning Inc,
ou=Land Applier, email=[e-mail], c=US
Darr 2022 02 23 08'40'47 -05'00'
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

t ,S1.1A1 P VIM-H•1 -. 11't I i 14111 A I 111,1( I1111N R1, IAl( 110N FORM On l&fes11J 8
lief) Potful! N li rullor:
1 pi MI't NOW: �{'!1(� @ S_ 1 117c 1k f 1,.., \},e.
+rpllT ' ?y{rrl{er: i'tf'l> 3�ifil,R
�� W 1 t'!Annie: Town r*f >� an alle_,—_. 'tt It t I' ,1 1 1 11 { ; 1 ! • 1� 1 t
ltnl{ilnring retina from l 1
S_ N(• iki • 1i1' 1 .I 1l1h Mow hulk -ate Ir{ rl >ar lelrai°rl Rttrl Rlia'rppiivt! >tt'r r,> rlrrt
; 1 All ( (Prior f ret1F1�1T
I'nllto,cn IZ r4itttlirtrt i i 1c!r _ .
i11 .'1 lino:. lr!nill 1 .1 Ai! 11 (Ate I refitment (I <.: ,
l`Isrca A: l`1:: rRA In I ortl!• r l l 1LP Probv-ri ,
if m _ ttr-R1slr to t►tte+ noti• r 1,1 Ifmom] It Inac '1 ,jtili ii{r114 eti,' ' nett caw In 1 urrhri ltvilt" r 1'oih'11{�n+° -
��_ ] It r,1 1 i isi1,'-,II 1 1 I hrr!1'-r.1,11111=.
Lilt..., t i }}eAli 1►,'>,,r"--�'. I l
•-.`� 1 1 I'1, ,!, 1t1 t Isilll,l! 1 1 •
7 , `,11r,I1::1t 11• Pratt(a l'o11-r,en : I
.�..i k.11 1 ..• .11 l?,•).0,01 i 1 All ) I im, o. t' f. - ...
t 1t l_ .... to nllrrnRti►. pc' tut ttt{ r1 [S lr►+c li •rti11 It1414 ati "i'i IA rat 141 5nFly f�rt1itre f',�tht► ens
lible
Lime StxL+il,rat,.,t1
.1 Alt 111AI11�Z1 i ,s1:1 N,.11nE : 1 Iscrt3btC T)i 4esit:rir _°
yw , n Frequency Santple
It applicable to aiternnti► r trtfoi mrd lav4 A or (11s+�.i rran plate the followin monitorir+ R s'ta: Tex!?
411c�►►°attic Level Pathogen 13c•ltsli•y•
Fxcce• vSAnalysis anipl
in Sludge 1 1 ntn;un (. eo. Mean MaxitfUn l Tow, .de/acx
AiP 1111111111 111111111111114
iliallallIMINIIIIII
Please indicate aiternat'e erformed:
❑ r}[]-d bench) ❑ 0 Alt- 8 (Drying - Unstable)
Alt 7 (i7ryiog - grable)
No vector attraction reduction operatics were performed ❑
PnrantC4er
Fecal Colif trm
t 1Dtothe
6th Nova
lets at
total so1id<
lttt trouper gram
of total solid (dry
yeti ht
Salmonella ba teria 3 MPN per 4 grams
(in lieu of fecal total solid (dry
:olift}rre wei :1st
Vector Attraction Reduction (15A NCAC 02T .1107)
Alt. 2 ( ay
Alt 5 (14 Flay Aerobic) 0 A 6 (Alk. Stabilization ID
❑ Alt 10 (Inca • oration) ❑
A': 1 (A'S reduction)
Alt. 3 (30-day bench)
At. 94 b'}ed'on} appropriate statement)
CERTIFICATION STATEMENT (please check the
"% certify, under penalty of law, that the pathogen requirements in ISA NCAC OZT .1106 and the
El
vector attraction reduction r uirement in ISA NCAC 02T .1107 have been met. -
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
0 vector attraction reduction requirementNCAC 02T 1107 almet one or both of theve not been met." pase note
if you check this statement attach an explanation why you have not
r uirernents.} t rectlata an • supervision n acco • >Itttce wit t 1 e system
ryl � etc1, nation as � een made under my 1
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction nrequirem is have
been en met. 1 am aware that there are
significant penalties for false certification including
[ i J
Alt 4 (Spec 0: uptake)
❑
❑
Mr. Gary if, er, W WTP ORC
Preparer Name and Title (type or print)
Land Applier Name and Title (if applicable)(type or Print}
_
_._ iicabie
Signature Prepay
- pate Signature of Land Applier (if app )
*Preparer is defined in 40 FR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DPNR FORM PVRF 02T (12t2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Southwest Plantation WWTP
Monitoring Period: From
1 /1 /2021
WQ Permit Number: WQ0030998
NPDES Number: WQ0029601
To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
•
Alt B (Alk Treatment)
■
I Alt. C (Prior Testing)
•
A
Alt.D (No Prior Test) ■
Process to Further Reduce Pathogengs ■
If applicable to alternative performed (Class A only) indicate
"Process to Further Reduce Pathogens":
Compost 0
Heat Drying ■
Heat Treatment ■
Thennophilic ■
Beta Ray •
Gamma Ray
0
Pasteurization •
Class B:
Alt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens
•
o
If applicable to alternative performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization l9
Air Drying ❑
Composting •
Aerobic Digestion ■
Anaerobic Digestion ■
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
PathogenDensityNumber
of
Excee-
deuces
Frequency
of Analysis
Sample
Type
Analytical
Tech -
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x lO to the
6th power
per gram of
total solids
MPN
C'FU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per grams
total solid (day
weight)
Vector Attraction Reduction (1SA NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
0
Alt. 2 (40-day bench)
❑
Alt. 3 (30-day bench) •
Alt. 4 (Spec. U, uptake)
■
Alt. 5 (I4-Day Aerobic)
•
Alt. 6 (Alk. Stabilization
o
Alt 7 (Drying - Stable) •
Alt. 8 (Drying - Unstable)
•
Alt. 9 (Injection)
■
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
•
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant pena for false certification including fine and imprisonment."
Mr. S
Preparer
ozzari, WWTP ORC
d Title (type or print)
Land Applier Name and Title (if applicable)(type or print)
Sig e o re. •t r* t Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
r)FNR FflRM PVRF f19T 112/7lt1R1

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Fadlity Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPDES Number: NC0003450
Monitoring Period: From 1/1/2021 To 3/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:4mt.mtimettemp, ❑ I Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing) 0
............ iAIt.D (No Prior Test) C2 [ Process to Further Reduce Pathogengs C]
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Heat Treatment 0 Thermo ' ' 'tic L]
Pasteurization ;.;;:::.:::.1::j.........
i
or Alt. (2) Process to Significantly Reduce Pathogens ::
COu.s t 0
Beta Ray •
r
Heats in ❑
Gamma Ray
Class B: ,Alt. (1) Fecal Density la
If applicable to alternative performed (Class B only) indicate "process to Significantly Reduce Pathogens":
Lime Stabilization C] Air Drying 0
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the followinS monitoring data: of atytrosf
Number Frequency Sample
Allowable Level Exc Tech -
in Sludge denc..n of Analysis Type „
(lam SM 9221 C
E
Pathogen
Density
i inirnu i
Geo. Mean
axim . '
Units
MPN/
1,016
111111111111
1,710
2,632
Gram
MIME
MEM
Alt. 2 (40-day bench) ❑
Alt. 6 (Alk. Stabilization ❑
r
Fecal Coliform
2x 10 to the
6th power
per gram of
total solids
MPN
CFI
1000 men per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid On,
coliform) weit¢n)
Vector Attraction Reduction (1'.
Alt.1(VS reduction) 0
Alt. 5 (14-Day Aerobic) D
Alt. 9 (Injection)
Composting 0 ]Aerobic Di$estion 0
Alt. 3 (30-day beach)
Alt 7 (Drying - Stable) 0
Alt. 10Sncorporation) 0 lNo vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements In 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 1SA NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
If you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Lisa Cottle, WWTP ORC Mr. Eric R. Smith, Land Applier ORC
Preparer Name and Title (type or print) Land A pier Name d Title (if applicable)(type or print)
����,, `ri n n _ zo1L N , C° -1�1.1aZ 2
:�7'',(�"� �r� j 10' Date
Signature of Preparers` Date Signature of Land Applier (if applicable)
"Preparer is defined in 40 CFR Pert 503.9(r) and 15A NCAC 2T .1102 (26)
0
Quarterly
.11u7) - Pease lndkate alternative ercormea:
D Alt. 4 (Spec. 02 uptake) 0
Alt. 8 (Drying -Unstable) p
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (0ZT Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town of Wallace WWTP
Monitoring Period: From 4/1/2021
WQ Permit Number: WQ0030998
NPDES Number: NC0003450
To 6/30/2021
Pathoien Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment) 0 Alt. C (Prior Testing) ❑ :. >r•
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Thermephilic
Class A:
Compost ❑
Beta Ray C]
A1t.D (No Prior Test) 0 , Process to Further Reduce Pathogcngs 0
Heat Drying ❑
Gamma Ray 0
Heat Treatment ❑
Pasteurization ❑
Class B: Alt. (1) Fecal Density Alt. (21 Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0 1 Air Drying C] 1 Composting 0 j Aerobic Digestion C]
Anaerobic Digestion ❑ 1
If applicable to alternative performed (Class A or Class B) complete the followingmonitorini data:
Parameter
Fecal Coliform
Salmonella bacteria
(in lieu of fecal
conform)
Allowable Level
in Sludge
2xt0tothe
6th power
per gram of
total solids
MPN
CFU
Pathogen Density
'Minim Geo. Mena
1000 mpn per gram
of total solid (dry
weight)
122,3781 379,114
Maximum
1,908,128
Units
MPN/
Gram
Number
Excee-
dences
0
Frequency
of Analysis
Quarterly
3 Nag per grams
total solid (dry
weigh,_
.rn Reductron {i5A NCA( 1T .1107) - Please lnd Bate alternative performed:
Sample
Type
Grab
Analytical
Tech -
niece
SM 9221 C
E
Alt.l (VS reduction) 0
Alt 2 (40-day bench) C]
Alt. 3 (30-day bench) ti
Alt. 4 (Spec. OZ uptake) 0
Alt. 5 (14-Day Aerobic) 0
Alt. 6 (Alk. Stabilization 0
Alt 7 (Drying - Stable) ■
Alt. 8 (Drying - Unstable) 0
Alt. 9 (Injection) El
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed CI
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
53
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction redaction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Lisa Cottle, WWTP ORC
Prep Natne and Title (type or print)
60412.e
Signature of Preeparer*
Mr. Eric R. Smith, Land Applier ORC
Land Applier d Title (if applicableXtype or print)
7-/D•IOZZ. -ace , d- 14 a;b2
Date Signature of Land Applier (if applicable) Date
*Prepare[ is defined in 40 CFR Part 503.9(r) and 1 SA NCAC 2T .1102 (26)
DENR FORM PVRF 02T (1212008)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facllty Name: Triple S Farms & Cleaning
WWTP Name: Town of Wallace WWTP
Monitoring Period: From 7/1/2021
To
WQ Permit Number: WQ0030998
NPDES Number: NC0003450
9/30/2021
1106) - Please indicate level achieved and alternative p erformed:
Class A:
Alt. A ctimahemp) 1 Alt B (Alk Treatment) • l
Alt. C (Prior Testing) CI.,......i..
::.. ' . .
AIt.D (No Prior Test) C1 [ Process to Further Reduce Pathogengs • 1
if applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost •
Heat Drying ❑ `
Heat Treatment ❑
Thermopluhc ❑
: :. .:
.
..:`•.
Beta Ray C1
Gamma Ray 0
Pasteurization CI
_
Class B:
Alt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens❑ �:' .`;
If applicable to alternative performed (Class B only) Indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ I Air Drying ❑
Composting
..
• '
Aerobic Digestion
■
Anaerobic Digestion • -I.
• • • ' ''
If applicable to alternative performed (Class A or Class B) complete the followin
monitoring data:
'
Analytx�t
Tech -
ramie
SM 9221
CE
Parameter
Allowable Level
in Sludge
Pathogen Density
Ner °
ama!
d �
Frequency
ofAnalysis
Sample
Type
Minimum
Geo. MeanMaxi
muxn
Units
L.
Fecal Coliform
2 x 10
6t
per gram of
total solids
MPN
78
179
2,554
MPI4/
Gram
0
Quarterly
Grab
CFU
1000 mpn per gram
of total solid (dry
weight)
,
Salmonella bacteria
(in lieu of fecal
colifbnn)
3 MPN per 4 grams —
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC lRT .111f1) - crease mmcate ai iernanve envrmuR.
Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) CI
Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) C]
No vector attraction reduction alternatives were performed ❑
Alt.1 (VS reduction) ❑
Alt. 5 (14-Day Aerobic) 0
Alt. 9 (Injection)
Alt. 2 (40-day bench) ❑
Alt. 6 (A1k. Stabilization Cl
Alt. 10 (Incorporation) ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
❑ vector attraction reduction requirement in 1SA NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
Ms. Lisa Cottle, WWTP ORC Mr. Eric R. Smith, Land Applier ORC
Preparer Name and Title (type or print) Land Applier Nam Title (if applicable)(type or print)
OQI 240.202 2.. a / - _
Signature of Preparer* Date Signature of Land Applier (if applicable) Date •
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

ignature of Preparers
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning WQ Permit Number: WQ0030998
WWTP Name: Town of Wallace WWTP NPDES Number: NC0003450
Monitoring Period: From 10/1/2021 To 12/31/2021
Pathogen Reduction (1SA NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) Of
Alt B (Alk Treatment) CI t
Alt. C (Prior Testing) 0
'
• AIt.D o Prior Test) 0 Process to Further Reduce Patho C3
If applicable to alternativeperformed (Class A only) indicate "Process to Further Reduce Pathogens": '
Compost • Heat Drying ■
Heat Treatment •
Thermoohilic 0
Beta Rat 0
u Gamma Ray •
•
Pasteurization •
'
Class B:
Alt. (1) Fecal Density Ca
Alt. (2) Process to Significantly Reduce Pathogens El
If applicable to alternative performed (aass B on10 indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization • Air Drying. 0 I
Composting •
Aerobic Digestion 0
Anaerobic Digestion • • • ..
If applicable to alternative performed (Class A or Class B) complete the following
Kumber Ali`
dcrlces
monitoring
Frequency
ofAnalysis
data:
Sample
Type
A toyybcat
Tech -
niaua
Parameter
Allowable Level
in Sludge
Pathogei Density
Minitnum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
63
76
163
MI'N!
GramC
0
Quarterly
Grab
SM 9221
E
C1=u
1000 tnpa per grain
of total solid (dry
iteei�ht)
Salmonella bacteria
(in lieu of fecal
ooliform)
3 MPNper 4 grams
total solid (dry
weight)
Vector Attraction Reduction (1SA NCAC 02T .1107) - Please indicate niternadve performed:
Alt.1(VS reduction)
0
Alt. 2 (40-day bench)
CI
Alt. 3 (30-day bench) 0
Alt 4 (Spec. 03 uptake)
0
Alt. 5 (14-Day Aerobic)
•
Alt. 6 (Alk. Stabilization
•
Alt 7 (Drying - Stable) 0
Alt. 8 (Drying - Unstable)
•
Alt 9 (Injection)
El
Alt. 10 (Incorporation)
C]
No vector attraction reduction alternatives were performed
■
CERTIFICATION STATEMENT (please check the appropriate statement)
EI "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
Q "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the Information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprieonment."
Ms. Lisa Cottle, WWTP ORC Mr. Eric R. Smith, Land Applier ORC
darer Name and Title (type or print) plier Name Title (if applicablextype or print)
2
} — Io Zo7.2. Lac �L k
. G
Date Signature of Land Applier (if applicable)
•Preparer is defined in 40 CFR Pert 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (1212006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Triple S Farms & Cleaning
WWTP Name: Town of Warsaw WWTP
Monitoring Period: From 1/1/2021
WQ Permit Number: WQ0030998
NPDES Number: WQ0021903
To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
• I
Alt B (A1k Treatment)
•
Alt. C (Prior Testing) •
A1t.D (No Prior Test) • I
Process to Further Reduce Pathogengs ■
If applicable to alternative performed (Class A only) indicate
"Process to Further Reduce Pathogens":
• , •: , ,
Compost ■
Heat Drying •
Heat Treatment
•
Ther nopl�ilic 0
:::
•• • -••
Beta Ray •
Gamma Ray ■
Pasteurization
•
•,•
1
Class B:
Alt. (1) Fecal Density • I
Alt. (2) Process to Significantly Reduce Pathogens El
[::::::::::::
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 11
I Air Drying ■
I Composting 0
Aerobic Digestion
•
Anaerobic Digestion •
•
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Patho en Densi
g ty
Number of
Excee-
dences
Frequency
of Analysis
Sample
Type
Anal ical
Tech -
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt,1 (VS reduction)
•
Alt. 2 (40-day bench)
•
Alt. 3 (30-day bench) •
Alt. 4 (Spec. 02 uptake)
■
Alt. 5 (14-Day Aerobic)
•
Alt. 6 (A1k. Stabilization
In
Alt 7 (Drying - Stable) Cl
Alt. 8 (Drying - Unstable)
•
Alt. 9 (Injection)
•
Alt. 10 (Incorporation)
•
No vector attraction reduction alternatives were performed
•
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Greg Hughes, WWTP ORC
Preer Natiyfe old Title (type or print)
Signatu'Ee of ireparer*
Land Applier Name and Title (if applicable)(type or print)
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION

PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The Town of Beulaville, Town of Kenansville, Town of Warsaw, and Southwest Plantation meet
pathogen reduction and vector attraction reduction requirements through lime stabilization. The
Town of Wallace met pathogen reduction through fecal density and vector attraction reduction
through injection or incorporation. The Town of Clayton met pathogen reduction and vector
attraction reduction through fecal density and injection and in one instance by SOUR (February
11-23, 2021.)
Documentation of these activities are found in the following section.

Triple S Farms WQ0030998
Lime Stabilization Documentation
Faclkv Name Town of Bculavlle
month 41.0. x o t7' 1
Teak/{L�
N0.
approximate
Grams
Lime
%
Prior to Lime Addition
> 12 pH
2
Hours After >12 pH
24 Horns After >I2 pH
Dates)
Heeled
Temp
.ord
Corr
Time
urn zed
Temp
a.I.ear
Carr
Trine
.
oars
WA
Standard
Temp
pH
actual
Temp.
Corr
Tine
Pll
anemia
ars
Stardnd
Temp
PH
utear
Tens.
Corr
Time
pil
aIm..d
EPA
SemdaN
Date
11,
I
11661,0
c
la
5;41
6,40
7u 5
1:°
13
atii'-
a
q:.'15
! 4.
12.00
/ 4
AO
/003
f1.7°!
Mat
moo
I
41,4
ay.3,1
iia;A
usj.y
Ins°
.3-11
Signature of C1p(rator
* EPA 40 CFR Part 503 far lime stabilization requires lime mixed with sewage sludge to have n pH of 12 or greater after 2 hours and maintain a pH of 11.5 for the followtng22 hours.
pH auwt = actual pH values that hove not been temperature corrected.
pH mnvd = pH values have been temperature corrected.
Al temperature units are in Celsius.
0
1
r
tT
tT
re-3
C;
00
co:
10
O
Crl
Cr'I
10
M
to
�rn
C'rl
t-'
N
M
("1
t+'I
tV
N
00
C
N_
O
as
Csl
CO
N
O
O
1/40
N
O
O
O
rn
O
O
N
1/40
O
C
r
N
O
O
N
N
{V
N
rn
O
t
0
N
00
C
N
N
N
O
O
M
O
OS
M
r;1t
O
e
to
. f.
O
Cs 00 t- co t/1 -t M CV
.--t r -- e--4

Triple S Farms WQ0030998
Lime Stabilization Documentation
Facility Name Town of Beulaville
Month
aaaf
Dart
Tale
No.
Approximate
Gadm o
Lime
116
Added
Prior to Lime Addition
> 12 pH
2
Hours After M12 pH
24 Hours After >12 pH
Dates)
Hauled
Temp
pH
.nailTi
Temp.
Carr
me
PH
amnia!
Temp
pH
x aat
Temp.
Corr
Tlmc
pH
amnia
EPA.
Stamina
Temp
pH
mi
Temp.
Corr
Tee
pH
emend
EPA
Staadat4
Temp
pH
.mast
Teem
Carr
Time
pH
errand
EPA
etmdad
,(
s.2.i-.1
I
%tot)1500
a3
3F1121..;;le
(I,'1)
,.ib5
.Zti
424
z:4?
%Ai3O
12;e23
.12.00
,,,z9
al54:03
/IND
472
12.00
..ii'f
i/'16:03
/0)1)4I,'75
u.so
.1-2(d''41
Signature of Operator
Acvtlizet
EPA 40 CFR Part 503 for lime stabilization requires lirne mixed with sewage sludge to have a pH of 12 or greater after 2 hours and maintain a pH of 11.5 for the following 22 hears.
pH arma9 = actual pH values that have not been temperature corrected.
pFl can Jul = pH values have been temperature corrected.
All temperate units are in Celsius
Correction
Factor
v't
tt
c;
c.
�f
a
01
en
O
en
C
Cr)
Cr)
G
O
0'1
O
0.27
0.24
.-4
N
0
CO
r--t
0
an
^
6
N
^4
O
CA
v
V
O
0
M
O
0
O
O
0
M
O
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\O
O
O
ON
O
O
[V
".-,
O
WI
"-,
O
00
r"'
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r-+
N
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-0.30 I
e5
M
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‘.0
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01
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0
eV
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0
in
`d'
0
Temp C
O
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on
cat-
M
Nam^-+
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00
N
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to
I 24
en
N
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O
O1
1$
t�
l9.
in
^t
M
C'1
—+
'4'
en
M
en
en
en
en
en
M
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en
CV
N
N
N
CV
hl
N
N
(4
. -1
--1
^'
` "1
ri
" 4
a"-t
r"
r"I
.l
—

Triple S Fanns WQ0030998
Lime Stabilization Documentatiun
Facility Name Town of Beulaville
Month
Dare
Teals
No.
Approximate
Gallons
Lime
f `j S
Added
Prior to Lime Addition
> 12 pH
2 Hours After >12 pH
24 Hours After >12 pH
Date(s)
Hailed
Temp
pH
••• 1
Temp.
Corr
Time
pH
esmew
Temp
pH
meal
Thaw
Corr
Time
pH
wormed
EPA
&mime
Temp
pH
mml
Tamp.
Corr
Time
pH
eeneekd
etA
Sid
Temp
pH
nmmd
Temp.
Car
Time
pH
meeeded
IPA
aerdm d
ij`saL
1
$©.cO
a440
IP-
4-11cN2
/o.c t:
3,T3
a.►
42,5.
z, ..,i
i1:30
i.2.t4
1100
f :(:
OA
',•:M3lc
f,' e✓
ia.13
12.00
iiscl
1:415
3.46_
/1;3
110-
11.50
j1-9t1
/
ure of0 r
Signature
EPA 40 CFR Part 503 for lime atabdization requires lime nixed with sewage sludge to have a pH of 12 or greater after 2 hours and maintain a pH of 115 for the following I2 hours.
pH maw = actual pH values that have not been temperature comcted.
pH canoes m pH values have been temperature corrected.
All temperature units are in Celsius
S to
tel
N
�'
' ON
M
\p
e•
0.33 J
' O
c+l
N
N 1
0.24 I
I --I
N
0.18
• l
.-+
CV
r-e
ON
p
0.06
M
O
O
en
O
O
C1
O
I N
r-+
' In
•- t
00
.-'i
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(V
N
N
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-0.33
I -0.36 1
O
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06
N
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In
'8
wocococ'
o
600
006Qc'6r
`
600.o0
et
00
h
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rM
32
—r
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en
CV
' •-,
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0'
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'et
en
CV
.--1
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en
M
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M
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en
CV
N
N
N
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CV
[V
NO.en
r-+
v--+
^-1
v—'
•—'
•"
^'
•'"'
Eil
1
s,
�

Triple S Farms
Clayton Little Creek Water Reclamation Facility
WQ0030998
Jan-21
Environment 1, Inc.
, • -
Lab ' 'i!:.a
• — •
:Date , iia 0
.
04t PIO . OA." '' '.::
pp:::::::
rkr#
::*::i:Log
:.: •::
HT-1
1/19/21
51,000
4.708
HT-2
1/19/21
20,000
4.301
HT-3
1/19/21
32,000
4.505
HT-4
1/19/21
30,000
4.477
HT-5
1/19/21
47,000
4.672
HT-6
1/19/21
49,000
4.690
HT-7
1/19/21
81,000
4.908
Total
Average
Most Probable Number / Gram
Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

TTWITDIE
gia, rinnungtto4
Drinking Wpter IDt 17715
We:ebeweter /DI 10
114 OAKMON i .DRIVE PHONE [phone]
GREENVILLE, N,C, 27858 FAX [phone]
TOWN OF CLAYTON
MR. JAMES WARREN
P.O. BOX 879
CLAYTON ,NC 27528
PARAMETERS
ID#: 890 I
DATE COLLECTED: 01/19/21
DATE REPORTED : 01/27/21
REVIEWED BY:
•
Sample Sample Sample Sample Sample Analysis Method
#1 #2 #3 #4 #5 Date Analyst Code
Total Residue, mg/I 15767 16233 15533 16633 16667 01/21/21 JMS 2540B-11
Fecal Coliibrm (MPN), /gram Solids 51000 20000 32000 30000 47000 01/19/21 KDS 9221E-06

[LliE;YJaC�Vf�liil iS 1.1U ilUIC:J rt° lath MU11
11411116111.1116011111160111011111.141101001.60010101100
Vlnkirtg Wa ar IRf 57715
Wastewater XDt 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N C 27858 FAX (252) 7 8-O633
ID1t: 890 X
TOWN OF CLAYTON
MR. JAMES WARREN
P.O. BOX 879 DATE COLLECTED: 01/19/21
CLAYTON ,NC 27528 DATE REPORTED : 01/27/21
PARAMETERS
REVIEWED BY:
Sample Sample Analysis Method
N6 //7 bate Analyst Code
Total Residue, mg/I 16233 16033 01/21/21 JMS 254013-11
Fecal Cnliform (MPN). /gram Solids 49000 81000 01/19/21 KDS 9221E-06

Environment I, Me.
130 Box 7O;i5- .1l4 iD i.sninn Dr.
i''ircerville. NC 27S58
CHALN OF CUSTODY RECORD
Page .__ __1._. of ._._.
environment I Inc.{: urn
Phone (=_i=, 7Sfs-b?e`;:� • Fax t'N2)
890 I
CLIENT:
TOWN OF CLAYTON
MR. DAMES WARREN
P.O.BOX 879
CLAYTON NC 27528
[phone]
'1 f3 •tlCi
Week: 7
I ?:ilSC.tiPECi'iON i
_ Ir—
. t::iiLi)xtt? iE
.
—,
G� is
Imo'
r _.._..____ _
CHLORINE NEUTRALIZED AT LL"cGra,
I.
1
pH CHECK (LAB)
P i
P
{
fit
co N AINERTYPE,Pfii
A
A
(
C=c1EMICALPRESERVATION
AA -NONE D-i+iADH
C • H.SO4 r• 7_!t :: AC,cTAT E/NAO 7
G-NATHOSULFATE
sC
`ii:i
TEMPERATURE, 'C
AT COLLECTION
0
_
-u:
Total Residue _ J
L
:7
J
f y
j
k
t
i
t
i
vs -
cc
j
-
a_
.'
it)! LE IO�1 i -J -
;
SAMPLE + OCATiON
DAM'
1191E a
i.
Sample #i
/ ;g %T
/l p r! 7/
i
i t ,S h i
E.
2
•z.
,,,,.t
i}
CLASSIFICATION:
i WA5 i avATER NPD^,EES1
_
i DRINKING WATER
I D'rr
Sample #2
Jr/ -t 7b{
I
? / •-r'r' I
I7-
2`+
",,
.
—
Sample #3
•
/I �'itG!
.1 1 l
J
2"
5.
'
Sample #4
ihf to
_u
t
i
i
2
, ::,
„>
x2
Sample #5
r
i
2
M,x
SCUD WASTE SECTION
Sample #6
P
r ...`
! ,1/r i
; ✓
i 2.
.
3, .�
Sample #7
ti
t. �
'/I 7f
, , �, !
r 7
,,.y
i ti
2
�,..
CHAIN OF CUSTODY_
(SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
r
_.
J
r
i
;
SAMPLES COLLECTED B" .
(Plpasa Print)
G.-
i
---
;
r
I
''
SAMPLES RECEIVED INLAB AT .-_ _°C
REP. y ASH D ` ISiG. ;5+4SP ERi
JH7Eri ir!F i tom•- 4" .�.,lr�
t .'�''.;
D TETME
of
MMENTS: /' , Z
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t1A9E � REC=''
cD BY (SKI)
DATE?IME
11101
; : 50
i
AEI:WJISHEDBY(SiG.'
DAT:,TiMc" 1 RECEIVED3Y(SIG.)
I
DA4 .;;ME
PLEASE READ Instructions for completing this form on the reverse me.
FORM 4%
Sampler must place a'C," for composite sample or e "C-" for
Grab sample ir, the blocks above for each parameter requested. E u 389065

Triple S Farms
Clayton Little Creek Water Reclamation Facility
WQ0030998
May-21
Environment 1, Inc.
e lia p
0 pi! • ,,,::i:
it. gram
HT-1
5/20/21
510,000
5.708
HT-2
5/20/21
260,000
5.415
HT-3
5/20/21
400,000
5.602
HT-4
5/20/21
250,000
5.398
HT-5
5/20/21
720,000
5.857
HT-6
5/20/21
240,000
5.380
HT-7
5/20/21
1,000,000
6.000
Most Probable Number / Gram
Total
Average
Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

1[MWniTEENgna inoilp®rgod
RIMIIIMIllnimpionuoir wow -Ter
ist3alc ng Wntet Ut: - 1 41
Wnatewntes ID: 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
TOWN OF CLAYTON
MR. JAMES WARREN
P.O. BOX 879
CLAYTON, NC 27528
PARAMETERS
ID#: 890 I
DATE COLLECTED: 05/20/21
DATE REPORTED : 05/26/21
REVIEWED BY:
Sample Sample Sample Sample Sample Analysis Method
#1 #2 #3 #4 115 Date Analyst Code
Total Residue, mg/1 15533 18833 19800 19267 18133 05/21/21 BLV 2540B-11
Fecal Coliform (MPN), /gram Solids 510000 260000 400000 250000 720000 05/20/21 KDS 9221E-06

O
ado o11MINE `Ecarp©Tak
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
TOWN OF CLAYTON
MR. JAMES WARREN
P.O. BOX 879
CLAYTON, NC 27528
PARAMETERS
Total Residue, mg/I
Fecal Coliform (MPN), /gram Solids
Sample
116
Sample
117
..suir-
iir1'sikir.:q Natax ID.< i7715
Waotewater IDs l0
PHONE [phone]
FAX [phone]
ID#: 890 I
DATE COLLECTED: 05/20/21
DATE REPORTED : 05/26/21
REVIEWED BY:
Analysis Method
Date Analyst Code
20233 18067 05/21/21 BIN 2540B-11
240000 1000000 05/20/21 KDS 9221E-06

.Environment .1, Inc.
13oz 7085, 114 Oakmont Dr.
Greenville, NC 27858
CIi.1IN OF CUSTODY RECORD
Page 1 of —_.....1
cnm°ironnient I Inc.ci nt
Phtxte (2_52) 756-6208 • Fax
8901
CLIENT:
:
TOWN OF CLAYTON
MR. JAIVIES WARREN
P.O. BOX 879
CLAYTON NC 27528
[phone]
(252) 756-(1633
Week: 1
DISlN1
❑
E( I ION
C1IL(7ltl'iI
uv
NON
CHLURINENEUTRALIZEDATCOLLECTIQN
Li
pH CHECK (LAB)
Ej
P
P
CONTAINER TYPE, P'G
A
A
CHEMICAL
PRESERVATION
A - NONE D - NAOH
B-HNO E -HCL
C - H SO, F -7_INC ACETATE'NAOH
G - NATHIOSULFATE
TOTAL CHLORINE, mg I
OR ug%I AT COLLECTION
TEMPERATURE, rf,
AT COLLECTION
# OF CONTAINERS
Total Residue
a
'~
v
irU.
PARAMETERS,TESTS 1
COLLECTION
SAMPLE LOCATION
DATE
TIME
Sample #1
—Sample
1
5�
2
�..,.
'r� '':
CLASSIFICATION:
I:IWASTEWATER (NPDES)
#2
Sample #3
?'
t /
,
2
Air
;
«sF
`yr%
p
2
1*-
Ul DRINKING WATER
Sample #4
—Sample
_
Jr ` -1
2
"' : —
f,,:
j DWRiGW
j SOLID WASTE SECTION
#5
J3,'
2
`.
Sample #6
2
#
,.
,
�°
�'"
Sample #7
S
Sl Yd`1
(2-I 0
2
4
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
4110 N
SAMPLES COLLECTED BY:
(Please
' \f Pant) (�
V I " . 1.1('C.
r Q T.-C.--
SAMPLES RECEIVED IN LABAT- C/ _ °C
RELIN 1 D B (SIG.) (SAMPLER)
------
DATE/TIME
,/0,:elsl I
RECEII,
r
ED BY (SIG)
DATE/TIME
5/''1vr
, :f.
5
COMMENTS:
RELIT oHED BY (SIG)
DATE/TIME
I
RECEIVED BY (SIG)
DATEri1ME
1
RELINQUISHED BY (SIG.)
DATE/TIME
I
RECEIVED BY (SIG.)
DATE
I
TIME
FORM 45
rLEASE READ Instructions for completing this form on the reverse side.
Sampler must place a "C" for composite sample or a "G' for
Grab sample in the blocks above for each parameter requested
N-395352

Triple S Farms
Clayton Little Creek Water Reclamation Facility
WQ0030998
Jul-21
Environment 1, Inc.
HT-1
7/22/21
140,000
5.146
HT-2
7/22/21
210,000
5.322
HT-3
7/22/21
150,000
5.176
HT-4
7/22/21
200,000
5.301
HT-5
7/22/21
130,000
5.114
HT-6
7/22/21
130,000
5.114
HT-7
7/22/21
140,000
5.146
Most Probable Number / Gram
Total
Average
Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

U
_ENTNTggi
Drinking Water ID: 'J7,15
Wastewater ID: 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 890 I
TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879 DATE COLLECTED: 07/22/21
CLAYTON, NC 27528 DATE REPORTED : 07/30/21
PARAMETERS
REVIEWED BY:
Sample Sample Sample Sample Sample Analysis Method
#1 #2 #3 #4 #5 Date Analyst Code
Total Residue, mg/I 17067 16567 16533 17300 17900 07/26/21 CAW 254011-11
Fecal Coliform (1PN), /gram Solids 140000 210000 150000 200000 130000 07/22/21 EDS 9221E-06

! i7_ -URI is
_U
ECIaTpUiThe,.
prinking Water ID: 37735
Wastewater ID, 10
119 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 890 I
TOWN OP CLAYTON
MR. BILL SIMPSON
P.O. BOX 879 DATE COLLECTED: 07/22/21
CLAYTON, NC 27528 DATE REPORTED : 07/30/21
REVIEWED BY:
PARAMETERS
Sample Sample Analysis Method
#6 #7 Date Analyst Code
Total Residue. mg/I 18533 17300 07/26/21 CAW 2540B-11
Fecal Coliform (MPN). /gram Solids 130000 140000 07/22/21 KDS 9221E-06

Environment .[, Inc.
P.O. [3ox 7085, 114 Oakmont Dr.
Gr enviIIe. NC 27SS8
CHAIN OF CUSTODY RECORD)
Pace 1 of 1
environment I jne.com
Phone [phone] • Fax (252)
CLIENT: 890 I
TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879
CLAYTON NC 27528
[phone]
751i t}hip
Weck:I
DIS1NI4.("1'IO;`
uiiC'1-IL01Z1NL
L.
L NO\
Qi
CHLORINE NEUTRALIZED AT COLLECTION
pH CHECK (LAB)
P
P
CONTAINER TYPE; P/G
A
A
CHEMICAL
PRESERVATION
A -NONE D-NAOH
B-HNO3 E -HCL
C - H,SO= F - ZINC ACETATE/NAOH
G - NA THIOSULFATE
TOTAL CHLORINE, mg.
OR ug l AT COLLECTION
TEMPERATURE,°C
AT COLLECTION
# OF CONTAINERS
Total Residue
FC/Gram
[ PARAMETERS/TESTS
COLLECTION
SAMPLE LOCATION
DATE
TIME
Sample #I
7/22/2f
l000
2
,:v ,
�:-�
���
,.x
CLASSIFICATION:
Li WASTEWATER(NPDES)
Sample 112
7/j 2/
!t,
2
Y,`../
�3
Sample #3
7/22/21
t o0q
2
',4's
Ij DRINKING WATER
DWR/GW
Sample #4
2
�,a�r�
Sample #5
7/23l2l
Io0�'
2
`.. ,
'
D SOLID WASTE SECTION
Sample 116%/Z
Z/Z/
2
:
,:
^"
Sample 117
7/2z/z)
lo)2,
2
'''.4
-
z %
CHAIN
OF CUSTODY (SEAL) MAINTAINED
DURINGSHIIPP}MENT/DELIVERY
Y
�\ 1 N
SAMPLES COLLECTED BY:
Print)
h / / %
Chi
C d (Na // 2 /'C
SAMPLES RECEIVED IN LAB AT C'%.Y.___'C
RELLIINOUIsHED BY (I ,) (SAMPLER)
DATETIME
7/24/2/
FCEIVED BY (SI
a 4'e)—-'
DATE/11ME
7/#41
l'iLt3
COMMENTS.
RELINQUISHED BY (SIG)
DATETIME
I
RECEIVED BY (S t
DATE/T1ME
RELINQUISHED BY (SIG.)
DATE/TIME
RECEIVED BY (SIG)
DATE/11ME
I
FORM #5
rPLcASE READ Instructions for completing this form on the reverse side.
Sampler must place a "C" or composite sample or a "G" for
Grab sample in the blocks above for each parameter requested.
w 98555

Triple S Farms
Clayton Little Creek Water Reclamation Facility
WQ0030998
Nov-21
Environment 1 Inc.
•Lj
pergram:','
HT-1
10/21/21
450,000
5.653
HT-2
10/21/21
170,000
5.230
HT-3
10/21/21
450,000
5.653
HT-4
10/21/21
170,000
5.230
HT-5
10/21/21
270,000
5.431
HT-6
10/21/21
140,000
5.146
HT-7
10/21/21
220,000
5.342
Most Probable Number / Gram
Total
Average
.........................
Fecal Coliform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

Q
IERc
rrarigir
114 OAKMONT DRIVE
GREENVILLE N C 27858
AOC@ Fi'fftar[f
TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879
CLAYTON, NC 27528
PARAMETERS
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 890 I
DATE COLLECTED: 10/21/21
DATE REPORTED : 11/01/21
REVIEWED BY:
Sample Sample Sample Sample Sample Analysis Method
11 112 113 114 115 Date Analyst Code
Total Residue, nig/I 20367 20367 20367 20767 19800 10/25/21 CAW 2540B-15
Fecal Colit'orm (NIPN), /gram Solids 450000 170000 450000 170000 270000 10/21/21 DNS 9221E-14

Vim-mg—1
.JQ
'1.d©T
Tm:tad
Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE PHONE {252) 756-6208
GREENVI! LE, N.0 27858 FAX [phone]
TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879
CLAYTON, NC 27526
ID#: 890 I
DATE COLLECTED: 10/21/21
DATE REPORTED : 11/01/21
./ `
REVIEWED BY:
PARAMETERS
Sample Sample Analysis Method
116 /17 Date Analyst Code
Total Residue, mg/1 20033 20300 10/25/21 CAW 2540B-15
Fecal Coliform (MPN), /gram Solids 140000 220000 10/21/21 DNS 9221E-14

Page
1 o1` I
LIENT: 890 I
TOWN OF CLAYTON
MR. BILL SIMPSON
P.O. BOX 879
CLAYTON NC 27528
[phone]
Week:l
DISINFECTION
jCHLORINE
NON
CHLORINE NEUTRALIZED AT COLLECTION
pH CHECK (LAB)
ary
LI
P
P
CONTAINER TYPE. P/G
J
A
A
CHEMICAL
PRESERVATION
A -NONE D-NAOH
8-HN0 E•HCL
C - H2SO4 F - ZINC ACETATENAOH
G - NATHIOSULFATE
TOTAL CHLORINE, mg,'I
OR 41 AT COLLECTION
TEMPERATURE`C
AT COLLECTION
OF CONTAINERS
.54
b
6
IX
a
o
F"
E
LI
J
U
;L.
IPARAP?METERS [ESTS
COLLECTION
SAMPLE LOCATION
DATE
TIME
Sample #1
2
.,:
CLASSIFICATION:
X WASTENATER(NPDES)
#2 Sample pIvlafl
,�
2
:::�
Sample N3
jD/2 !hi
1135
2
Y
.V
(
to DRINKING WATER
Li DWRIGW
SampleH4
10/UIJZ(
2137
2
„
,..
.
Sample #5
1 a f 2 1/21
113 C
.2
h
,
it >.
LI SOLID WASTE SECTION
Sample 116
/oJ2//z)
If LI i
2
>? 4
v.
Sample #7
/ %
��`LJ`
t�
f j r
2
.
CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT'DELIVERY
N
SAMPLES
(Please�
.
SAMPLES
COLLECTED BY:
Pant)
4iaao/ t/QIvtez9 SL
RECEIVED IN LAB AT )"I.6 "C
RELIN I. BY(G MP _RI
E ���G
DATETIME
'qvb!
L..rt c,
GEIVEDBY(SIIG.)
(.,A,,- .
DATETIME
10/21ia I
: 1 r(
COMMENTS
RELINQUISHED BY (SIG.)
DATES
1ME
1
RECEIVED BY (SIG.)
DATETIME
1
RELINQUISHED BY (SIG.)
DATE/TIME
RECEIVED BY (SIG)
DATE/TIME
rORM fi5
PLEASE READ Instructions for completing this form on the reverse side
Sampler must place a "C" for composite sample or a "G" for
Grab sample in the blocks above for each parameter requested.
W 398550

Triple S Farms
Clayton Little Creek Water Reclamation Facility
WQ0030998
Jan-21
SOUR*
mg oxygen/Or
1/19/2021
0.45
1/19/2021
0.47
1/19/2021
0.37
1/19/2021
0.41
1/19/2021
0.25
1/19/2021
0.40
1/19/2021
0.40
* SOUR = Specific Oxygen Uptake Rate
Total
Average
SOUR values are less than 1.5 mg oxygen/gram/hour and meets the 40 CFR Part
503.33 Option 4 for Vector Attraction Reduction.
SOUR values provided by Town of Clayton WRF

Total Solids mg/ =Dill gm x 1000
Sample Vol ml
Date: ///9/Z/
Time In:
Town of Clayton
Total Solids at 103 - 105° C
SM 2540 B 18th ed.
f/ r-�-
•
%RPD = 2(A-B)x100
A + B
B
Blank
g
-3
Z7
4
Z
Dish WET gm
97 g5-3
9, 9'7yy
/Da, /17/
9e,g3'70
Iva 3SSza
Dish Empty gm
'z `797'7
7Y, 89z0
7,57 3743
7y345 `/
?.s- 8 ®93
Sample Vol. ml
'Z'+, G,8 76
,5; o,3//e
x '7H0q
25", R/391
2.9,,-/q/40
'7% 7'0.3
Azi,YIp,5-7
'7 3.2-9I
Dish Dry .gm
73..Z3b0
75-, 33 7i
Dish Empty gm
72,(743 9'7
'7e-/,egg.$
'X
74b3445-z7
•7 R95
Residual gm
, y 7?- s
o , ttqc16
.?'743
0 , 41.374)
O. LR 7?
,,
a Y3g1
%,
%SOLIDS
/, 7
/ • 7 /
1, `77
/, f% l
% RPD
Date:/ / f/ /
Time rn: , rc
•
H
Holding tank 1
,,r'
/Z.- Dup
Dish WET gm
q6, 75.-/j
/ty, /y4n
Dish Empty gm
72, /Y/0
74, yOk0
Sample Vol. ml
X 4/4i/*'
/, 7W..3O
Dish Dry .gm
17,2 , 574i. 3
'1�), + 1/6 0
Dish Empty gm
Residual gm
LO' e1 wi/.
e , Lill
%SOLIDS
), 7 9
1, 7R
% RPD

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By -
Total Solids•
Beginning Temperature:
End Temperature:
Time Dissolved Oxygen Level
(minutes) (mg/I)
0
2
4
5 8.13
6 8.04
7 7.97
8 7.89
9
10 774
11 7.66
12 7.6
13 7.52
14 7.45
15 7.36
8.76
8.46
8.34
8.28
8.21
7.81
Slope: 0.08
Intercept: 8.6
Correlation Coefficient: 0.99
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Dry Solids
degrees Celsius
degrees Celsius
4.93 mg Oxygen/hr
0.28 mg Oxygen/hr/g
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rate:
1
0.45[
mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature.
Sampling Date/Time.
Sampled By
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
Town of Clayton
W00023178
MIND
1 /19/2021�
133,
01/19/21 1340
WRS
01/19/21 1345
WRS
1.77 % Dry Solids
12.9 degrees Celsius
End Temperature. 13.9 degrees Celsius
Dissolved Oxygen Level
Slope: 0.09
Intercept: 8.7
Correlation Coefficient: 0.97
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
5.15 mg Oxygen/hr
0.29 mg Oxygen/hr/g
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rate:
0.41
mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope.
Intercept.
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
Town of Clayton
W 00023178
1/19/2021
13
01/19/21 1415
WRS
01/19/21 1420
WRS
1.77
12.9
13.9
0.07
8.4
0.98
Dry Solids
degrees Celsius
degrees Celsius
4.10 mg Oxygen/hr
0.23 mg Oxygen/hr/g
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rater 0.37
mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/I)
Town of Clayton
WO0023178
1 / 19/2021
13
8.8
8.66
8.58
8.49
8.42
IN
8.33
8.25
ININO
N W
O
8.19
8.1
8.04
7.96
7.89
7.83
7.75
7.69
7.6
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
01/19/21 1445
WRS
r
01 /19/21 1450
WRS
1.79 % Dry Solids
12.5 degrees Celsius
13.7degrees Celsius
0.08
8.7
1.00
4.58 mg Oxygen/hr
0.26 mg Oxygen/hr/g
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rate
0.41
mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/I)
7.6
8.7
8.61
8.54
Town of Clayton
W 00023178
1/19/2021
13
01/19/21 1505
WRS
01/19/21 1510
WRS
1.79
12.7
13.7
Dry Solids
degrees Celsius
degrees Celsius
8.46
IND
e
8.4
8.32
8.26
8.18
8.11
8.03
7.95
7.89
7.81
7.74
7.68
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.05
8.5
0.65
2.83 mg Oxygen/hr
0.16 mg Oxygen/hr/g
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rate:
0.25
mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature.
End Temperature:
tz y
Town of Clayton
W 00023178
1/19/2021
13
01 /19/21 1525
WRS
01/19/21 1530
WRS
1.79 % Dry Solids
12.7 degrees Celsius
13.7 degrees Celsius
Time Dissolved Oxygen Level
(minutes) _(mg/I)
0 8.71
1 8.58
2 8.51
3 8.43
7
4 8.36
5 8.28
6
8
9
10
11 --
12
13 7.71
14 7.63
15 7.n
8.21
8.13
8.06
7.99
7.91
7.84
7.77
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.07
8.7
1.00
4.45 mg Oxygen/hr
0.25 mg Oxygen/hr/g
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rate:
0.40
mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(m9/1)
8.73
Town of Clayton
W Q0023178
1/19/2021
13
01 /19/21 1545
WRS
01/19/21 1550
WRS
11/1111111110.
8.57
8.5
8.42
8.35
8.27
8.19
8.12
MIL
8.04
7.97
7.9
7.83
7.76
7.69
7.63
7.57
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
N
1.78 % Dry Solids
12.5 degrees Celsius
13.6 degrees Celsius
0.07
8.7
1.00
4.47 mg Oxygen/hr
0.25 mg Oxygen/hr/g
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rate:
0.40
mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Pomutce: Tj-y o)e �'fl r171 S
ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Batch Size (gallons) 66 000 Lbs. of Lime i 3Ub
pH
4.21
Temp •C
roillcipH
Corr. Corrected
Fodor to pH
T
Thmc
pH
t5513.
Temp•C
IS.3
>12 pH
Carr.
Fedor+
Corrected
px
13.11
Time pH
Pi 135
Date rn9 -a 1
Temp•C
2JHour pH
Corr. Carrected
Parlor+f pH
1a
Time
13,i
Land Application Permit No: j• Q n n 3 b 99S
Operator
pH Temp •C Corr. Corrected Time initials
Factor+l pH
ri$ 11 i9 q."b �11
'N,V'P To wn Rena di ( lc_
6al-m }A43.r Q e.r"

TripkSFarms WQ0030998
Lime Stabilization Documentation
Facility Name Southwest Plantation! Bear Trail
Month
2021
Date
Teats
N o.
Approximate
COON N
lime
Added
Prior to Lome Addltim
>12 pH
-' 2 Hears Alter>12 di
24 Home After>12
Date(s)
Tea,
pH
.mat
Temp
Cover
lee r
pH
—
Temp
pH
sari
Temp.
Carr
Time
pH
onnwod
SPA
Omani
Temp
p
PH
earl
el
'item,
anred
r
Cr
lime
PM
a
RA
emir'
Temp
PH
soul
TM,.
Csiv
Time _
PH
mowed
tar
Ord.Hauled
31Vk4
j11LOagyp
111.11.15
-.33
17o0
t,.85
it{ 0
12
-033
IB9O
12,5
12.60
)I O
124'0
-3.1
27)00
-rs
12.00
fy.Zlz41
13
o
I1•75
11.50
30(L/
Y/2fh)
qfrgiZ,
12. latlr3
1160
14-0
'[,T3
-.11
110 0
I,.14,
1 i1.Z
It.4l-o.T1
IR ID
I2.l.y
I211
1 Lb
1121
:2,-1
2p3o
11.'11
IZa
ISA
11.11
:2.7
O * DD
II 9011511
5II11z(
‘2,1.0
yoozu
14.4
'.uq
%lop
145
22;4
17,14
:09
do o
1243
It00
11.1
12.3c
:01
1-100
12.so
1Znp
ILI
Iwo
- 04
100p
11.44
11.5b419/z4
ilz110
12 if4
'V
24.1
1.1,1
o3
nob
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:03
icoD
12.I4
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Al.%
12.11
:0l,
Z12P
1Z.lI
120011,1
II.91J
`pC.
o'i' S
tttt
ile
109/u
n
Signettro
• EPA 4 CPR Part 503 for lime stabilization requites lime mixed with sewage sludge to have a pH of 12 or grater for 2 boots and maintain a pH of 11.5 for the following 22 hours.
pH cool pH values that have not been tcn clone corrected.
pH - pH values have been temps anme corrected.
All temperance mots are in Celsius.
in
N
V-
CT
en
ko
on
en
art
O
col
t--
N
er
N
.--i
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k.o
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en
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.-1
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er'i
en
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en
v%
r t
N
vl
G1.
ti
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tj
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0
0
0
0
0
0
0
0
0
0
0
0
0
i
0
•
0
t
0
t
0
1
0
•
0
•
0
•
0
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0
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0
•
0
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C
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•
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•
Temp C
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00
t--
t.b
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in
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en
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en
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en
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•--1
•--1
.--1
.i
.-ti
•--u
.-1
...t
.--1
.t

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NC0020702
Jan-21
Environmental Chemists, Inc.
••,•::•
.0
Date. 0Most
:::::::::: . ,• . .::::••••
ii;i!.
• , ... • .... • .. •:,:• • • ,,:f,,,,,
Probable 'ii:
per gram
... ,•••••• :„....
Log
1
1/22/21
2,273
3.357
2
1/22/21
2,394
3.379
3
1/22/21
1,053
3.022
4
1:22,21
2,487
3.396
5
1/22/21
2,632
3.420
6
1/22/21
1,124
3.051
7
1/22/21
1,016
3.007
Most Probable Number / Gram
Total
Average
Fecal Culiform/gram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Feb 18, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2021-01193
Project ID: WWTP Sludge
Total Phosphorus
Mercury
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
SM 4500 P F
SW846 7471B
EPA 200.7
EPA 200 7
EPA 200 7
EPA 200.7
EPA 200.7
EPA 200 7
EPA2007
EPA 245 1
27500 mg/kg
2.23 mg/kg
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<1.0 mg/L
<0.0002 mg/L
01/29/2021
01/25/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
02/02/2021
01/29/2021
Lab ID
21-02951
Test
Sample ID:
Site: 1
Method
Collect Date/Time Matrix Sampled by
1/22/2021 9:50 AM Solid/Sludge In Young Seo
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.98 %
2273 MPN/g
01/25/2021
01/22/2021
Lab ID
21-02952
Test
Sample ID:
Site: 2
Method
Collect Date/Time Matrix Sampled by
1/22/2021 9:50 AM Solid/Sludge In Young Seo
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.88 %
2394 MPN/g
01/25/2021
01/22/2021
Lab ID
21-02953
Test
Sample ID:
Site: 3
Method
Collect Date/Time Matrix Sampled by
1/22/2021 9:50 AM Solid/Sludge In Young Seo
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.90 %
1053 MPN/g
01/25/2021
01/22/2021
Report # 2021-01193 Page 3 of 4

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Town of Wallace
316 E. Murray Street
Wallace NC 28466
Attention: Brent Dean, ORC (WWTP)
Date of Report: Feb 18, 2021
Customer PO #:
Customer ID: 09010063
Report #: 2021-01193
Project ID: WWTP Sludge
Lab ID Sample ID:
21-02954 Site:4
Test
Total Solids (%)
Fecal Density
Method
SM 2540 B
Collect Date/Time Matrix
1/22/2021 9:50 AM Solid/Sludge
Results
SM 9221C E MPN 24hr503
Sampled by
In Young Seo
Date Analyzed
1.81 %
2487 MPN/g
01/25/2021
01/22/2021
Lab ID
21-02955
Test
Sample ID:
Site: 5
Method
Collect Date/Time Matrix
1/22/2021 9:50 AM Solid/Sludge
Results
Sampled by
In Young Seo
Date Analyzed
Total Solids (%)
Fecal Density
Lab ID
21-02956
Test
Sample ID:
Site: 6
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
1.71 %
2632 MPN/g
Method
Collect Date/Time Matrix
1/22/2021 9:50 AM Solid/Sludge
Results
Lab ID
21-02957
Test
Sample ID:
Site: 7
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
Method
01/25/2021
01/22/2021
Sampled by
In Young Seo
Date Analyzed
1.78 %
1124 MPN/g
01/25/2021
01/22/2021
Collect Date/Time Matrix Sampled by
1/22/2021 9:50 AM Solid/Sludge In Young Seo
SM 2540 8
SM 9221C E MPN 24 hr 503
Results
Date Analyzed
1.97
1016 MPN/g
01/25/2021
01/22/2021
Comment: *Sludge residual results, except pH, reported on a dry weight basis.
Reviewed by:
Report # 2021-01193 Page 4 of 4

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 WindmIll Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Branch Residuals/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: Z j 6h193
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, Public Works
PO NO:
REPORT TO:
PHONE/FAX: [phone]
COPY TO: Lisa Cottle, ORC
email: bdean1townofwallace.com
Sampled Bv:
.1ouna_e(3
SAMPLE TYPE: 1= Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
`
Identification
Collection
1"
a
O
i;
Container
(P or G)
-1Sample
o
E
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
W
o
=
3
_
o
_
_
o
1
°
e
Sludge
I-u -)-1
aq 5-0
c
P
,, �, v
`` -
X
Fut(T�P
nutrients/metals '� C _
G
G
1 j
) .. ->)
cU q' -O
C
P
X
fecal density/ %TS
G
G
2) _
1-s-3--yJ
aq t.c
C
P
a
X
fecal density/ %TS
G
G
3)
/ -D-)- >J
c' q 5C
C
P
07--.1S
X
fecal density/ %oTS
G
G
4)
I-yl--�/
oil C
C
P
4',,si
X
fecal density/ %TS
G
G
5)
I-)-z-'-(
0c 50
C
P
.6.
X
fecal density/ %TS
G
G
6)
1 ---)-)--)1
pc/q)
C
P
X
fecal density/ %TS
G
G
7)
1-z)---y)
o ci 4-0
C
P
"'
X
fecal density/ %TS
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
Zr1r0u1,9 sec
.
Temperature when Received: C
Delivered By: j/rb
Accepted: t Rejected:
Received By: (iro
Resample Requested:
Date: I /11//1 Time: (-7 0
Comments:
TURNAROUND:

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NC0020702
Apr-21
Environmental Chemists, Inc.
e:Attal e
os
`ralO4ble:ember.:€
........................... .
1............
4/19/21
264,151
5.422
2
4/19/21
491,229
5.691
3
4/19/21
1,908,128
6.281
4
4/19/21
122,378
5.088
5
4/19/21
535,118
5.728
6
4/19/21
161,404
5.208
7
4/19/21
430,108
5.634
1%lost Probable Number / Gram
Total
Average
Fecal Coliform
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab " 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 " 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info`aienvironmentalchemists.com
Branch Residuals/Bob Branch
Attention: Bob Branch
Date of Report: Apr 30, 2021
Customer PO #:
Customer ID: 15060009
Report #: 2021-06258
Project ID: Wallace WWTP
Lab ID Sample ID:
21-15557 Site: #1
Test
Method
Collect Date/Time Matrix Sampled by
4/19/2021 9:25 AM Solid/Sludge Sean Pistorino
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.65 % 04/19/2021
264151 MPN/g 04/19/2021
Lab ID
21-15560
Test
Sample ID:
Site: #2
Method
Collect Date/Time Matrix Sampled by
4/19/2021 9:25 AM Solid/Sludge Sean Pistorino
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.85% 04/19/2021
491229 MPN/g 04/19/2021
Lab ID Sample ID:
21-15561 Site: #3
Test
Method
Collect Date/Time Matrix Sampled by
4/19/2021 9:25 AM Solid/Sludge Sean Pistorino
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.83% 04/19/2021
1908128 MPN/g 04/19/2021
Lab ID Sample ID:
21-15562 Site:#4
Test
Method
Collect Date/Time Matrix Sampled by
4/19/2021 9:25 AM Solid/Sludge Sean Pistorino
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.86% 04/19/2021
122378 MPN/g 04/19/2021
Lab ID Sample ID:
21-15563 Site: #5
Test
Method
Collect Date/Time Matrix Sampled by
4/19/2021 9:25 AM Solid/Sludge Sean Pistorino
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.99% 04/19/2021
535118 MPN/g 04/19/2021
Report #:. 2021-06258
Page 2 of 3

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
inforl;environmentalchemists. com
Branch Residuals/Bob Branch
Attention: Bob Branch
Date of Report: Apr 30, 2021
Customer PO #:
Customer ID: 15060009
Report #: 2021-06258
Project ID: Wallace WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-15564 Site: #6 4/19/2021 9:25 AM Solid/Sludge Sean Pistorino
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E MPN 24 hr 503
2.85 % 04/19/2021
161404 MPN/g 04/19/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-15565 Site: #7 4/19/2021 9:25 AM Solid/Sludge Sean Pistorino
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E MPN 24 hr 503
2.79 % 04/19/2021
430108 MPN/g 04/19/2021
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: � O?
Report # 2021-06258 Page 3 of 3

Analytical 8 Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
info@environmentalchem ists.com
Client: Branch Residuals/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: ,;«J .2 I — 0 L 2...5
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, Public Works
PO NO:
REPORT TO:
PHONE/FAX: [phone]
COPY TO: Lisa Cottle, ORC
email: [e-mail]
Sampled By: (,,o,, P 4.
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
A g
cn
Composite
or
Grab
Container
(P or G)
N
t E
"
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
Z
Z
=
y
_
8
_
o
_
o
~
W
o
Sludge
C
P
�r�' 1
I 5
X
nutrients/metals
4-19-2.I
1 Z.5
G
G
1)
) 55`s .
X
fecal density/ %TS
it -let -2I
9* 2.5
G
G
2)
P
(0,0
X
fecal density/ %TS
`i'- 11-2.1
9: Z5
G
G
3)
C
P
156°
X
fecal density/ %TS
4 - I%-ZI
9'. 7,5
G
G
4)
C
P
6L
15°
X
fecal density/ %TS
(4- (rt-21
9 . 25
G
G
5)
C
P
1.351'3
X
fecal density/ %TS
4-lj-2.I
9. 1 5
G
G
6)
C
P
) 15 ��
X
fecal density/ %TS
4- Ft- 21
9- Z 5
G
G
7)
C
P
► 550
X
fecal density/ %TS
4-19 -2_1
q: Z5
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
.fa., P,„-
4 - «- zl
2.
-
if
Temperature when Received: T.2
Delivered By: &C
Accepted:
Received By:
Rejected: Resample
Date:
Comments: TURNA - OUND:

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NC0020702
Jul-21
Environmental Chemists, Inc.
• • : :
-Date : AflaIyzed.
:::•::
1I�$t:risAi4 ' '!. ' iiiii
•
r ...
1
7/21/21
78
1.892
2
7/21/21
78
1.892
3
7/21/21
80
1.903
4
7/21/21
750
2.875
5
7/21/21
80
1.903
6
7/21/21
80
1.903
7
7/21/21
2,554
3.407
Most Probable Number / Gram
Total
Average
Fecal Coliformlgram
Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab * 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Date of Report: Sep 14, 2021
Customer PO #:
Customer ID: 15060009
Report #: 2021-12254
Project ID: Wallace WWTP
Lab ID
21-30537
Test
Sample ID:
Site: 001
Collect Date/Time
7/21/2021 9:40 AM
Method
Matrix
Water
Results
Sampled by
client
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.33 %
<78 MPN/g
07/23/2021
07/21/2021
Lab ID
21-30539
Test
Sample ID:
Site: 002
Method
Collect Date/Time
7/21/2021 9:40 AM
Matrix
Water
Results
Sampled by
client
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.32%
<78 MPN/g
07/23/2021
07/21/2021
Lab ID
21-30540
Test
Sample ID:
Site: 003
Method
Collect Date/Time
7/21/2021 9:40 AM
Matrix
Water
Results
Sampled by
client
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.25 %
<80 MPN/g
07/23/2021
07/21/2021
Lab ID
21-30541
Test
Sample ID:
Site: 004
Method
Collect Date/Time
7/21/2021 9:40 AM
Matrix
Water
Results
Sampled by
client
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.67%
750 MPN/g
07/23/2021
07/21/2021
Lab ID
21-30542
Test
Sample ID:
Site: 005
Method
Collect Date/Time
7/21/2021 9:40 AM
Matrix
Water
Results
Sampled by
client
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
2.51 %
80 MPN/g
07/23/2021
07/21/2021
Report # 2021.12254
Page 2 of 3

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info:a environmentalchemists.com
Date of Report: Sep 14, 2021
Customer PO #:
Customer ID: 15060009
Report #: 2021-12254
Project ID: Wallace WWTP
Lab ID
21-30543
Test
Sample ID:
Site: 006
Method
Collect Date/Time
7/21/2021 9:40 AM
Matrix
Water
Results
Sampled by
client
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E MPN 24 hr 503
2.26%
<80 MPN/g
07/23/2021
07/21/2021
Lab ID
21-30544
Test
Sample ID:
Site: 007
Method
Collect Date/Time
7/21/2021 9:40 AM
Matrix
Water
Results
Sampled by
client
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221 C E MPN 24 hr 503
2.35%
2554 MPN/g
07/23/2021
07/21/2021
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: ( ATh
Report #:: 2021-12254 Page 3 of 3

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Branch Residuals/Bob Branch
PROJECT NAME: Sludge -Wallace WWTP
REPORT NO: :0)1 -- t fiZt
ADDRESS: CC: Town of Wallace
CONTACT NAME: Brent Dean, Public Works
PO NO:
REPORT TO:
PHONE/FAX: [phone]
COPY TO: Lisa Cottle, ORC
email: [e-mail]
Sampled Bv:
S7 ' 1W 1 '7eo
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other.
Sample Identification
Collection
E �:
to �-
Composite
or
Grab
Container
(P or G) I
d
`o
= E
`
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
w
o
Z
-.
u
=
$
a
z
=
3
o
w
x
Sludge
'1-3-1-1
Q? itC
C
P
30 3c
nutrients/metals
G
G
1)
,)_y/",.I
oclita
c
P
3LI.C3.
X
fecal density/ %TS
G
G
2)
)7-4."-(
(ML-t0
C
P
3
!
X
fecal density/ %TS
G
G
3)
9-4-1
UCj 40
C
P
O
X
fecal density/ %TS
G
G
4)
Jt
X
fecal density/ %TS
G
G
X
fecal density/ %TS
6)
3acel-3
X
fecal density/ %TS
G
G
7
n-1-1-�
oq
P
30"41/
X
fecal density/ %TS
Gc
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
Dlyenil Teo
9 -)-1 -Di
Temperature when Received:
Delivered By:
Accepted:
Received By:
cted:
Resample Requested:
Date: �2.1 Time:
Comments: TURNAROUND: 1

Town of Wallace
Wallace Wastewater Treatment Plant
NPDES Permit # NC0020702
Oct-21
Environmental Chemists, Inc,
Date i' n e
iiii::' . 4
to)** Nuniber:.:.:.'i'ii!
t: • .:.:.:
':!1"1.Log
:.:.:
1
10/04/21
72
1.857
2
10/04/21
63
1.799
3
10/04/21
67
1.826
4
10/04/21
163
2.212
5
10/04/21
69
1.839
6
10/04/21
63
1.799
7
10/04/21
67
1.826
Most Probable Number / Gram
Total
Average
.. • ..... •
• :•:• ' •:•:•"
Fecal Coliform/gram
Fecal Conform values are less than 2,000,000 and meets the Class B pathogen reduction
requirement
Data provided in this summary have been used for the values and geometric means
reported on the Annual Pathogen and Vector Attraction Reduction Form for this land
application event.

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Date of Report: Oct 29, 2021
Customer PO #:
Customer ID: 15060009
Report #: 2021-17320
Project ID: Wallace WWTP
Lab ID Sample ID:
21-43461 Site: Sludge 1
Test
Method
Collect Date/Time
10/4/2021 7:15 AM
Matrix Sampled by
Solid/Sludge Sean Pistorino
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
2.79 %
72 MPN/g
10/04/2021
10/04/2021
Lab ID
21-43462
Test
Sample ID:
Site: Sludge 2
Method
Collect Date/Time Matrix Sampled by
10/4/2021 7:15 AM Solid/Sludge Sean Pistorino
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
2.87%
<63 MPN/g
10/04/2021
10/04/2021
Lab ID Sample ID:
21-43463 Site: Sludge 3
Test
Method
Collect Date/Time Matrix Sampled by
10/4/2021 7:15 AM Solid/Sludge Sean Pistorino
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 8
SM 9221C E-2014
2.72 %
<67 MPN/g
10/04/2021
10/04/2021
Lab ID Sample ID:
21-43464 Site: Sludge 4
Test
Method
Collect Date/Time Matrix Sampled by
10/4/2021 7:15 AM Solid/Sludge Sean Pistorino
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
2.77 %
163 MPN/g
10/04/2021
10/04/2021
Lab ID Sample ID:
21-43465 Site: Sludge 5
Test Method
Collect Date/Time
10/4/2021 7:15 AM
Matrix
Solid/Sludge
Results
Sampled by
Sean Pistorino
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
2.64%
<69 MPN/g
10/04/2021
10/04/2021
Report# 2021-17320
Page 2 of 3

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Date of Report: Oct 29, 2021
Customer PO #:
Customer ID: 15060009
Report #: 2021-17320
Project ID: Wallace WWTP
Lab ID Sample ID:
21-43466 Site: Sludge 6
Test
Method
Collect Date/Time Matrix Sampled by
10/4/2021 7:15 AM Solid/Sludge Sean Pistorino
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
2.87 % 10/04/2021
<63 MPN/g 10/04/2021
Lab ID Sample ID:
21-43467 Site: Sludge 7
Test
Method
Collect Date/Time Matrix Sampled by
10/4/2021 7:15 AM Solid/Sludge Sean Pistorino
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
2.69% 10/04/2021
<67 MPN/g 10/04/2021
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report #:: 2021-17320 Page 3 of 3

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Branch Residuals/Bob Branch
PROJECT NAME:
REPORT NO:
"4'
17-37z)
ADDRESS: 1735 Heckle Blvd.
Site:
PO NO:
Suite 103-291
REPORT TO: Bob Branch
PHONE/FAX:
Rock Hill, SC 29732
COPY TO:
email:
Sampled By: Sean (340r0•o
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream
SO = Soil, SL = Slu
Sample Type I
Composite
or Grab
Container I
(P or G)
.
3NON 1
HCL
H2SO4
NAOH
THIO I
FILTERED
OTHER
Temperature when Rece
Delivered By:
Comments:
ved °C: : tic
Accepted: ✓ Rejected: Resample R gpested:
Date: "l j44 Time: O: `'i,S"
TURNAROUND:
Received By: (,M

Triple SFarms WQ0030998
Lime Stabilization Documentation
Name
Mouth / g4-/ :' Ro ZI
Tank.
No.
Approximate
Gallons
Lima
Added
Prior to Lune Addition
—Temp.
>12 pH
2 Haas After>12 pH
24 Homy After>12 pH
Date(p)
Heated
Temp
AI
` Cosy
Time
mimed a
Temp
a
Cam
Time
d
EPA
Seed rd
'map
pH
r
Temp.
t
Ups
me
p..eat
9emh.d
Temp
o r
Cesar
Tulle
pH
ssm Era
I ii
IS3
4
0 ao
133O
,(o_i`I
tC-1
12-41R
0.30
iv:o.
/ZcfG
12.00
61
12-62-
0.t1
/IP:a.'
12-3C
12.00
/5-1
1? 1
D 3.0
/
. :
1Zr51
11.50
v
7i Part 503 for time stabilization requires lime nixed with sewage sludge to have a pH of I2 or greater after hours and maimain a pH of 11.5 for the following 22 hones.
hrai pH values that have riot been temperature corrected
pH values have been temperature corrected.
rc writs rue in r.him
I Factor II
en
'V'
C;
N
'd'
C
Cif
tr)
C
lO
t*?
O
to
crl
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cr7
o
N
N
C
- t-
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O
--i
N
O
00
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O
►n
.--r
O
"O
N
r-e
O
a1
CI
O
k,e,
C7
C
rn
p
O
C
O
O
en
O
d
s
l4
O
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s
01
C
a
.
N
--+'
C
.
rn
,-+
C
.
00
,—u
C
r
,-r
N
e
9
'�
N
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.
t�
N
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s
0
trl
0
.
VI
Cr)
C
.
10
M
C
.
ON
to
O
e
N
'd-
e
9
en
Vt'
e
9
(Temp C
a:,a1
'd'
C
00
t+)
N
en
1p
en
M
vy-
M
cn
cr)
I 32
—1
(*PI
Cry
01
N
00
N
t`-
N
lO
N
rn
N
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N
on
N
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N
-^a
N
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N—
01
oo
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t -
,—i
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,-
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ct'
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eh
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1 -1
O
e-i

Jame . Ttm o W cse.5Q4.s
TripleSFarms WQ0030998
Lime Stabilization Documentation
Month
aa2,1
7imkx
Na
.tpproslmafo
Gallons
1Jme
Added
Prior toP Lime Addition
> 1Z PH
Z Hann After >12 pH
24 Homo After >12 H
H) I
Homed
Temp
aaoal
Time
mrp11
T
Team
Pli
aemd
Ttmp.
Corr
Timc
PH.
canceled
Qa
ataadam
Temp
pH
*rand
Temp.
Corr
Time
PH
manned
tots
Srmhmd
Temp
pH
end
Tip.
Corr
tins
phi
aerated
. vs
staged
lialik
laAa
.3
G 53
, 03
t t Do
ii.Qo
24-i
11.i.1
:D 3
Lo
j2a."s
12.00
2.�4
)Q.Sry
:al
/S°
iniC
moo
2.42
f2 1
3
ill 0
apt
use
iixil
•
t
Joi 941-
Zt Part 503 for lime soon requires lime mixed with sewage sludge to Lave a pH of 12 or greater after hums and maintain a pH of 11.5 for the following 22 hours.
Oral pH vales that have not born temperature coaetied.
pH values have ban tempaanue corrected.
zc units are in Celsius
c
;,
an
d-
N
%Ct.
C1
vfl
\D
Cr)
0.33
0.30
N
c3
0.24 1
.-i
N
CO
,--i
an
.-i
CV
—
Cti
O
\0
o
M
cp
O
o
M
C
%.0
o
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O
CA
r-r
to
,--a
00
,-+
,--t
N
cr'
CV
a
O
Cr1
M
c+)
'.0
Cr)
CA
tot
N
"et
✓t
'c1-
4-ar
6
C
C
O
C
O
O
O
O
C
O
O
C
O
O
O
C
G
C1
C
O
O
O
d
O
C
C
C
Temp C 1
O
C,
CO
t.•
l0
an
eh
1 33
(NI
•-+
O
0\
00
I 27
VD
to
ch
[ 23
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00
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t.0
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d'
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car
eer
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a—i
rt
a--1

game rl9tt)?1 W CLrQtr.i
Triple SFanny WQ0030998
Lime Stabilization Documentation
mouth SP�72 4 /
Tank
No.
Approximate
lime
Prior to Lime Addition
>12 pH
2 Hours After>12 pH
24 Hoots After>12 pH
Dote(s)
Hauled
Temp
PH
moms
TAR
Corry
phi
pH
aeons
Temp.
0:eer(�
Time
p11
unwed
unwee1d
:se
'So dem
Temp
pH
'emu
Tamp.
Car
imee
pH
mama
am
Smmnt
Tpnp
pH
corm
Temp,
Corr
Dos
pal.
a sme6
Me
So s
�+�Gallons
15o,oCo
)Added
!SO%
1q
7 p
-. i D
`Tune
%( O
�earned
4 ,o
`Teemp
J 1
to
c `"
O yv
�a.d4
12.00
�0
Ja
. )C
Og3Q
10-31
1240
Jo
t2da
. rs
073 o
nab
luso
L
R Part.503 for lime stabili=tion requires lime noted with sewage sludge to have a pH of 12 or greater ater2 hours and maiataim a pH of 11.5 for the following 22 hours.
mg pH values that have not been temperature corrected
pH values have be= temperance corrected.
are mots are in Crlab:.
`o
O
ei
' 1-
C
Cr)
O
Cr,
O
m
Cr)
O
o
M
O
S
N
O
-4-
CV
O
'-c
N
O
oo
+- i
O
an
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O
CV
r- t
O
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o
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asc
O
O
rn
O
O
o
O
O
en
O
O
r
k0
O
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r
01
O
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e
CV
--1'
C
r
to
.-I
C
e
00
+-+
C
e
v- 4
eV
C
e
"4"
N
C
s
N
O
t
o
en
O
e
M
en
C
e
en
O
s
0,
to
C
r
Crl
"d:
O
s
rn
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e
0.
05
Qa
4
C:1
"4'
CA
en
CO
en
en
en
en
en
en
en
Cr/
Cr)
C4
C
Cal
N
N
N
N
Cal
N
C'
•-+
d
'--i
---I
'-1
r+
'--I
OI-C

SOIL ANALYSIS REPORTS

SOIL SAMPLE ANALYSES
The Town of Beulaville, the Town of Warsaw, the Town of Clayton, the Town of Kenansville and
Southwest Plantation met pathogen reduction and vector attraction reduction requirements through
lime stabilization. The soil pH will continue to be raised through the continued application of lime
stabilized biosolids to these application fields.

Grower:
Triple S Farms
Farm:
Triple S Farm
Farm Sample ID
Dixie Chemical - Beulaville
1060 S. NC 41 & 111 Hwy Beulaville, NC 28518
910-298-3660

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364W. Park Drive I Warsaw, NC 28398- I Phone [phone]
''I11L11:YTy.tItrf Ci o-141 jt.
l,(1tt;1 Siten.cc."
HARVEYS-BEULAVILLE [60126] Grower. TRIPLE S FARMS
Farm: TRIPLE S FARM / FIELD 1
1060 S NC 418.111 LID: D2FF3586187
BEULAVILLE, NC 28518 Test Method: Mehiich III
'
Page 1
Target pH: 6
Received: 12/14/2021 Processed: 12/16/2021
Sample IDLab
ID
.. P-1
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-I
Zn-AI
Mn-I
Mn-AI
Cu-I Na
ESP
CEC BS (%) HM (%)
Soil Class
1
8933090W
222
70
10
54
5 3
2.6
51
716
716
47
38
450
0.2
2
81
68
1.16
Min
2
8933100W
495
95
7
67
5 6
2.4
56
1302
1302
53
42
838
0 2
2
10.8
78
1.70
Min
3
8933110W
551
48
8
74
5 3
1.8
63
2028
2028
50
40
955
0 2
2
11.4
84
0.96
Min
4
8933120W
450
57
7
77
5.7
1.4
54
1842
1842 ;
44
36
992
0.2
2
10 5
87
0 70
Min
5
8933130W
535
37
7
74
5.7
2.0
49
2486
2486
53
42
1038
0.2
2
11.4
82
0.42
Min
6
8933140W
571
64
8
75
5.9
1.6
56
1772
1772
53
42
835
0.2
1
11.0
85
0.64
Min
7
8933150W
500
60
7
75
5.3
1.8
69
1574
1574
38
33
935
0.2
2
11.3
84
1.05
Min
8
9
8933160W
352
441
46
69
6
8
68
50
5.3
5.1
1.8
2.6
42
51
916
774
916
774
62
66
47
50
550
505
0.1
0.1
2
2
7.6
7.0
76
63
0.89
0.43
Min
Min
8933170W
10
8933180W
449
38 _
6
68
5 4
2.2
I 46
1148
1148
50 40
748
0 1
1
8.9
75
0.56
Min
Explanation of Symbols - % (percent), -I (Index), Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
• NCDA Soil Fertility Recommendations (Ibs/A)
Sample ID
2
Crop
.1SOYBEANS444 "
Lime N
TonslAere Nitrogen
1.4
1.0
P205 K20
Phosallele Potash
20
Mg
Magnesium
S
Suitor
B
Boron
Zn
Zinc
Mn
Menge nese
Cu
Copper
See Note
3 .
3
SOYBEANS
3
SOYBEANS
1.0
40
3
4
SOYBEANS
0.5
40
3
5
SOYBEANS
07
70
3
6
7
___ SOYBEANS
SOYBEANS
0.3
1.0
30
30
3 __
3
8
SOYBEANS
1.0
50
25
3
9
SOYBEANS
1.6
20
3
10
SOYBEANS
1.1
60
3
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only n Is entirety Waters Agn x5 rd L±oratones has no control over be manner in *hob samples are taken therefore aralyes, s bused solely en d•e sarrrle as received Latcratory list her s hinted to the 'ee assessed on the refererced sortie

7-7
,. WATERS.A RlCUL, ORAL
LABOF/7O{tIE# INC
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364W. Park Drive I Warsaw, NC 28398- I Phone [phone]
rrIlJL/)3YT;'L11tJ 11}Y711't21.,..
1,01.th Sctt'rice"
HARVEYS-BEULAVILLE [60126) Grower. TRIPLE S FARMS Page 2
Farm: TRIPLE S FARM / FIELD 1
1060S NC 41 & 111 LID: D2FF3586187 Target pH: 6
BEULAVILLE, NC 28518 Test Method: Mehlich III Received: 12/14/2021 Processed: 12/16/2021
Sample ID Lab ID
11 ' 893319OW
P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-I
Zn-Al Mn-I
Mn-AI
Cud Na
ESP CEC BS (%) HM (%)
Soil Class
434
36
8
76
5 4
1.4
55
1071
1071 41
35
720
0 2
2 9 9
86
0 52
Min
12 893320OW
678
64
7
75
55
1.8
51
2260
2260 69
51
1025
0 2
2 11.4
84
0.33
Min
13 893321OW
592
48
7
71
5 8
2.0
49
1924
1924 66
50
1010
0 2
2 10 0
80
0 19
Min
Explanation of Symbols - 9e (percent). -I Index), Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic cenbmeters)
Abbreviations. Ac (Acid ty), CEC (Cabon Exchange Capacity). BS (Base Saturation) HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
Sample ID Crop
11
12
SOYBEANS
SOYBEANS
13
SOYBEANS
NCDA Soil Fertility Recommendations (Ibs/A)
Lime
TorelAcre
07
08
N
Nitrogen
05
P205
Phos Pluto
K20 'Mg
Potash Meg mesh=
70
30
Sulfur
B
Bonn
Zn
Zino
40
Mn Cu
Merge rose Copper
See Note
3
3
3
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWG Laboratory Certification Number 635
Ths document may be reprodteed only nits enlrety Waters Agr:cuu:ral Letcra:ones has no control over to manner .n whd samples are taken therefore analyn s 5 based solely m the sample as waved Labcretory hatrtty is anted to the lee assessed on the referenced sample

WATERS A 6RICULiTU RAL
LAITRA'id7.168, INC
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- 1 Phone [phone]
"/111.1'):-th;L1t (if tit11...
It/tt-11. St✓teit c;"
HARVEYS-BEULAVILLE [60126] Grower. TRIPLE S FARMS
Farm: TRIPLES FARM / FIELD 2
1060 S NC 41 & 111 LID: D2FF3586190
BEULAVILLE, NC 28518 Test Method: Mehlich III
Page 3
Target pH: 6
Received: 12/14/2021 Processed: 12/16/2021
Sample ID
Lab ID
P4
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-I
Zn-Al
Mn-I
Mn-AI
Cu-I Na
ESP 1 CEC BS (%) HM (%)
Soil Class
21
8933290W
348
28
8
69
5 6
2 2
47
959
959
44
36
635
0 2
2 9 8
78
1 31
Ain
22
8933300W
471
25
7
65
5 5
2.4
53
1321
1321
47
38
972
0 2
2 9 0
73
2 89
Min
23
8933310W
486
19
7
77
5 4
1.4
50
1321
1321
41
35
945
0 1
2 9 1
85
0 83
Mn
Explanation of Symbols - % (percent) -I Index), Sod um (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations' Ac (Acidity), CEC (Cation Exchange Capacity). BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (Ibs/A)
Sample ID
21
22
Crop
SOYBEANS
SOYBEANS
Lime N
Tons/Acre Nitrogen
0 9
11
P205 K20
Phosphate Potash
80
90
Mg
Megneslum
S
Sulfur
B
Boron
Zn
Zinc
Mn
Mange nese
Cu
Copper
See Note
3
3
23
SOYBEANS
0.7
100
3
Explanation of Symbols - lbs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This document may be reproduced only n its sorely Wain Agnculural Latcratanes has no control over the manner in which samples are taken, therefore analysis is based solely on the sample as received Laboratory hatihiy is limited to the lee assessed on the referenced sample

\,
WATERS 14 BICULTURAL•
LABOR Of4IE�SNC :"'k
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- I Phone [phone]
riI11LT) "O-VIA 'O-).t'014..
i(/ all S c. e,rii tom"
HARVEYS-BEULAVILLE [60126] Grower TRIPLE S FARMS Page 4
Farm: TRIPLE S FARM / FIELD 3A
1060 S NC 41 & 111 LID: D2FF3586188 Target pH: 6
BEULAVILLE, NC 28518 .,, .,., Test Method: Mehlich III Received: 12/14/2021 Processed: 12/16/2021
Sample ID Lab ID
24 8933320W
P4
K4
Mg (%)
Ca (%)
pHw
Ac
S4
Zn4
Zn-AI Mn-I
Mn-AI
Cu-I Na
ESP CEC BS (%) HM (%)
Soil Class
352
25
7
68
5 4
1.6
48
899
899 56
44
570
0.2
2 7.0
77
0.90
Min
25 8933330W
498
25
7
73
5 8
2.0
44
1342
1342 56
44
782
0 2
2 10.6
81
0.58
Min
26 ' 8933340W
461
33
8
74
5.7
2.2
56
1512
1512 59
45
735
0 2
2 13.5
84
1.05
Mn
27 8933350W
504
29
8
79
5 7
1.4
67
1534
1534 59
45
850
0 2
2 11.9
88
0.66
Min
28 8933360W
535
23
6
80
5 7
1.4
61
1386
1386 50
40
865
0.2
2 107
87
0 81
Min
Explanation of Symbols - % (percent), -I Index), Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity) BS (Base Saturat on), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
mill,mca.e i:- �r"mot w __y NCDA Soil Fertility Recommendations (Ibs A)
Sample ID
24
Crop
"SOYBEANS
Lime N
TonstAcrs NItro9.n
08
05
P205 K20
PhD.phete Potash
90
90
Mg
Mapneslum
S
Sulfur
B
Boron
Zn
Zinc
Mn
Manila nose
Cu
Copp.,
See Note
3
3
25
SOYBEANS
26
SOYBEANS
07
70
3
27
SOYBEANS
05
80
3
28
SOYBEANS
05
90
3
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This dcmmenl may be reprodixed only n ih enorery Waters AgrcwLral Labcralcnes has no control CV EN the manner m which samples are 0kn, therefore, analysts is bused solely on the sample as recaved Laboratory liiabdty is limited to the lee assessed on Se referenced sample

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- I Phone [phone]
"/ 17 Lill -eel:1 1 y. Li;
1,,(Lt'l1. sote,tice."
HARVEYS-BEULAVILLE [60126] Grower. TRIPLE S FARMS Page 5
Farm: TRIPLE S FARM / FIELD 38
1060 S NC 41 8111 LID: D2FF3586189 Target pH: 6
BEULAVILLE, NC 28518 Test Method: Mehlich III Received: 12/14/2021 Processed: 12/16/2021
Sample ID Lab ID
P-I
325
K-1
43
Mg (%)
12
Ca (%)
70
pHw
6 1
Ac
1.6
S-I
50
Zri-I
660
Zn-AI Mnd
660 31
Mn-AI
27
Cu-1
402
Na
0.1
ESP CEC
1 10 2
BS (%)
84
HM (%)
2 65
Soil Class
Min
29 8933370W
30 8933380W
321
54
15
69
6 2
1.0
41
584
584 41
32
350
0.1
1 8 0
88
1.56
Min
31 8933390W
339
42
14
75
6 0
0.8
49
652
652 38
33
398
0.1
2 9 5
92
1 23
Min
Explanation of Symbols - % (percent), -I Index), Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations. Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (Ibs/A)
Sample ID
29
30
Crop
SOYBEANS
SOYBEANS
Lime N
TonalAcr. Nitrogen
P2O5 K2O
Phou spFub Potash
50
40
Mg
M.9ruslum
S
Sulfur
B
Boron
Zn
Zinc
— .-
Mn
Mange nese
Cu
Copper
See Note
3
3
31
SOYBEANS
60
3
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWO Laboratory Certification Number 635
This document may be reproduced only n its entirety Waters Agncutural Lahcratones has no control over t'e mercer in which samples are mien, therekre anatyvs is based sorely co the sample as received Laboratory fiabity is hinted to the fee assessed on the referenced sample

WATERS tiiCUI.URAL'•
R�!Cff1ES,•1� Ni
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364W. Park Drive l Warsaw, NC 28398- l Phone [phone]
„If'3tl-wct:;t,lt,..t
,(IL(i1 SGLe.t.t. crr
,? HARVEYS-BEULAVILLE [60126] Grower. TRIPLE S FARMS Page 6
Farm: TRIPLE S FARM / FIELD 4
1060 S NC 41 8111 UD: D2FF3586197 Target pH: 6
BEULAVILLE, NC 28518 Test Method: Mehlich III Received: 12/14/2021 Processed: 12/16/2021
Sample ID Lab ID P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-I
Zn-AI Mn-I
Mn-AI
Cu-I Na
ESP CEC BS (%) HM (%)
Soil Class
' 32 893340OW
336
74
13
64
5 6
1 6
55
620
620 41
35
365
0.1
2 8.4
81
1.53
Mn
33 893341OW
385
49
9
50
51
2 6
43
629
629 , 50
40
312
0.1
1 7.1
63
1.76
Min
Explanation of Symbols - % (percent), -I Index), Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (Ibs/A)
Sample ID
32
33
Crop
SOYBEANS
SOYBEANS
Lime N
TomIAcre Nitrogen
0 6
1.6
P205 K20
Phosphate Potash
20
40
Mg
Megraslum
S
Sulfur
B
Boron
Zn
Zinc
Mn
Menge nese
Cu
Copper
See Note
3
3
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
The document may be reproduced only n its entirety Waters AgncvtuM Latcralones Sus no ant of over be manner in -xhch samples are taken, therefcre analysis is based solely m the sample as received Latcratcry tiatdity is limited to Me lee assessed on Se referenced mimic

Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive I Warsaw, NC 28398- I Phone [phone]
'11;Lp "0\'Llt (5;-QT1.lttlL...
WLt11 Sete. ice r
HARVEYS BEULAV1LLE [60126] Grower. TRIPLE S FARMS Page 7
Farm: TRIPLE S ARM / FIELD 5
1060 S NC 41 8111 LID: D2FF3586191 Target pH: 6
BEULAVILLE, NC 28518 Test Method: Mehrch III Received: 12/14/2021 Processed: 12/16/2021
Sample ID Lab ID P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-1
Zn-AI I Mn-I
Mn-AI
Cu-I Na
ESP CEC BS (%) HM (%)
Soil Class
34 893342OW
409
62
9
54
5 3
2.8
51
658
658 50
40
420
0 1
2 8 3
66
1.35
Min
35 893343OW
507
62
8
67
5.2
2.0
45
1199
1199 56
44
490
0.1
2 I 9.3
78
2 08
Min
36 893344OW
569
75
8
70
5.4
2.0
45
1184
1184 53
42
638
0 1
1 10 6
81
1 30
Mtn
37 893345OW
528
49
7
59
5 4
3.0
50
1012
1012 47
38
688
0 1
1 9 5
69
0 80
Min
38 893346OW
442
28
6
65
5 6
2.4
54
836
836 44
36
528
0.1
1 9 0
73
0 80
Min
Explanation of Symbols - % (percent), -I (Index), Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations. Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter). ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (IbslA)
Sample ID
34
35
Crop
.r ''SOYBEANS
Lime N
TOroIACl1 Nitrogen
P205 K20
Phan ghat. Potash
Mg
Map mature
S
golfer
B
Boron
Zn
Zino
Mn
Menge nose
Cu
Co ppsr
See Note
.. 3
3
1 5
1.1
30 __
- -- 30
SOYBEANS
36
SOYBEANS
1.0
20
3
37
SOYBEANS
1.5
40
3
38
SOYBEANS
1.0
80
3
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWD Laboratory Certification Number 635
Tres dcc ment maybe reproduced only n its entirety Waters ArncuLral Latcratxries has re cored over Te marrer in which samples are 2Wen therefore. analysts is based sclely m the sample as received Labcramry Sabi n limited to the fee assessed on the referenced sample

: WATER9'A RICL1L,1URAL
•'•. LA80• �es-IE3rx1NC: s'/
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364W. Park Drive 1 Warsaw, NC 28398- I Phone [phone]
"111tr)lcif '(%l 1,.
l(iLti1 5c e.i t e r
HARVEYS-BEULAVILLE (60126]
1060 S NC 41 8111
BEULAVILLE, NC 28518
Sample ID Lab ID
44 I8933520W
P-I
Grower. TRIPLE
Farm: TRIPLE
LID: D2FF3586196
Test Method: Mehlich
S FARMS
S FARM / FIELD
III
Page 8
6
Target pH: 6
Received: 12/14/2021 Processed: 12/16/2021
K-I
Mg (%)
' Ca (%)
pHw
Ac
S-I
Zn-I
'i': Mn-I Mn-Al
Cu-1 Na
ESP CEC BS (%) HM (%)
Soil Class
93
73
11
45
4.8
2.8
43
185
185 31
29
135
0.1
2 73
62
2.27
Min
45 8933530W
70
61
9
27
4.5
3.4
38
138
138 I 41
35
120
0.1
2 5 8
41
1.18
Min
Explanation of Symbols - 96 (percent), -I Index) Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations Ac (Acidity) CEC (Cation Exchange Capacity), BS (Base Saturation). HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (Ibs/A)
Sample ID
44
45
Crop
SOYBEANS
Lime N
Ton,tAere Nitrogen
1 9
24
P205 K20
Phosphate Potash
Mg
Megnesfum
S
Sulfur
B
Bonn
Zn
Zinc
Mn
Menge nese
Cu
Copper
-
See Note
3
20
30
SOYBEANS
Explanation of Symbols - lbs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
Ths document may be reproduced only n ,ts comely Waters Agnnrtural Laboratories has no coned ever the marrcr m which samylcs arc taken therefore analysis is based solely on the sample as received Laboratory natal,/ is limited to the fee assessed on the referenced sample

WAfERs , i,
L'A ORAAAAAA"''''111111pgtE3;iNC.
�1l
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364W. Park Drive) Warsaw, NC 28398-) Phone [phone]
rrl1;i111YTVi.1l1f C7i-(}1t'th .
lilt 11 Sc.te-rice,"
HARVEYS-BEULAVILLE [60126] Grower. TRIPLES FARMS Page 9
Farm: TRIPLE S FARM / FIELD 7
1060 S NC 41 & 111 LID: D2FF3586195 Target pH: 6
BEULAVILLE, NC 28518 \- Test Method: Mehfich III Received: 12/14/2021 Processed: 12/16/2021
Sample ID Lab ID _ P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-1
Zn-I
Zn-AI Mn-I
Mn-AI
Cu-I Na
ESP CEC BS (%) HM (%)
Soil Class
14 893322OW
264
58
10
45
4 9
3 0
71
502
502 38
33
325
0 2
2 7.3
59
1.21
Min
15 893323OW
307
51
10
49
4 8
2 2
64
444
444 38
33
295
0 2
3 6.1
64
1.98
Min
16 i 893324OW
171
58
11
41
51
2.4
76
261
261 28
27
188
0 2
3 5.7
58
2 30
Min
17 i 893325OW
180
52
10
33
4 8
4.8
63
318
397 28
34
185
0 2
2 7.4
46
3 52
M-0
18 I8933260W
216
34
10
38
4.8
3.6
73
374
467 25
33
242
0.3
5 7.2
50
4.05
M-0
19 893327OW
230
32
11
45
49
1.6
86
334
334 22
23
272
0.3
7 4.0
60
2.20
Mn
20 893328OW
217 45
11
41
4 7
2.8
59
278
278 28
27
175
0.2
3 6.2
55
2 76
Min
Explanation of Symbols - % (percent), -I Index), Sod um (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations Ac (Acid ty), CEC (Cation Exchange Capacity), BS (Base Saturation) HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (Ibs A)
Sample ID
14
15
Crop
'SOYBEANS
SOYBEANS
Lime N
Ton!Aere Nitrogen
19
1.5
P205 K20
Phosphate Potash
30
40
Mg
Magnesium
S
Sulfur
B
Boron
Zn
Zinc
Mn
Mene.nea.
Cu
Copper
—
See Note
3
3
16
SOYBEANS
1.4
30
3
17
SOYBEANS
1.9
40
3
18
SOYBEANS
1.4
70
3
19
20
SOYBEANS
SOYBEANS
1.0
1.9
80
50
- _ 10
3
Explanation of Symbols - Ibs)A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWQ Laboratory Certification Number 635
This dccument may be reproduced only nits enhrery Waters xgncutural Latcratcres has no coned over 7e manner in ahidl samples are taken. therefore. anaiysts is tared scIdy en pre sample as received. Lataratery H&J rr is limited to the tee assessed an the relererced sample

;�� 7S?
• WATERS RICULTURAL'><
o Cir57
2.104.
i0L':
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364W. Park Drive l Warsaw, NC 28398- l Phone [phone]
�rll;if7:'/?L'LI•L�F t7F.C.YW 1...
1,,(1uh. Se. e,elce,
HARVEYS-BEULAVILLE [60126] Grower. TRIPLE S FARMS Page 10
Farm: TRIPLE S FARM / FIELD 8
1060 S NC 41 8 111 LID: D2FF3586192 Target pH: 6
BEULAVILLE, NC 28518 Test Method: Mehlich III Received: 12/14/2021 Processed: 12/16/2021
Sample ID Lab ID
46 8933540W
P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-I
Zn-1
Zn-AI I Mn-I
Mn-AI
Cu-I Na
ESP CEC BS (%) HM (%)
Soil Class
330
175
14
52
6 5
1.0
32
536
536 91
57
518
0 1
2 5 5
82
0.77
Min
47 8933550W
374
197
16
64
66
0.2
27
692
692 125
76
655
0.1
2 5.8
97
0.54
Min
48 8933560W
371
182
15
66
67
04
27
694
694 109
65
720
0.1
2 6.7
94
0.82
Min
49 8933570W
328
213
13
60
6 7
0.8
30
570
570 78
46
615
01
2 6 9
88
0.77
Min
50 8933580W
372
245
13
58
6 8
0.6
33
586
586 106
61
612
0 1
2 6 3
90
1.69
Min
51 8933590W
222
231
17
58
63
0.8
36
405
405 75
50
470
0.1
2 7.7
90
1.32
Min
Explanation of Symbols - % (percent), -I Index): Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
kA NCDA Soil Fertility Recommendations(lbs/A)
Sample ID
46
47
Crop
SOYBEANS
Lime N
Tons/Acre Nitrogen
P205 K20
Phosphele Potash
Mg
Magneilum
S
Sulfur
B
Boron
Zn
Zinc
Mn
Menge nese
Cu
Copper
See Note
3
3
SOYBEANS
48
SOYBEANS
3
49
SOYBEANS
3
50
SOYBEANS
3
51
SOYBEANS
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronom c D vision
DWD Laboratory Certification Number 635
Ths document may be reprx'tced aniy'n,ts anbrery Waters Arcuate' Laboratories has no control over tl:e manner in whch samcles are taken therefore analysis s based solely m 1e sample as renewed Labcratcq haLifty is hintedto the fee assessed an the referenced sample

1•' \ JJ
( WATER
S
-
�yRIIICUL4URAL
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364W. Park Drive Warsaw, NC 28398- l Phone [phone]
"Iiit. 1;..O \.'LP1 f'17F2T1t1LZL..
ltFtth cc '
HARVEYS-BEULAVILLE [60126] Grower. TRIPLE S FARMS
Farm: TRIPLE S FARM / FIELD 9
1060 S NC 41 & 111 LID: D2FF3586193
BEULAVILLE, NC 28518 Test Method: Mehlich III
Page
Target pH: 6
Received: 12/14/2021 Processed: 12/16/2021
Sample ID
39
Lab ID
8933470W
P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S-1
Zn-I
Zn-AI
Mn-I
Mn-AI
Cu-I Na
ESP CEC BS (%) HM (%)
Soil Class
382
71
10
71
5.6
1.4
55
649
649
44
36
395
0 1
2 9 4
85
0 92
Min
40
8933480W
344
40
10
77
5.9
0.6
35
590
590
72
53
382
0 1
2 6 4
91
0.78
Min
41
8933490W
347
58
11
69
5 8
1.6
42
596
596
56
44
418
0.1
2 9 2
83
0.88
Min
42
8933500W
281
83
12
70
5 7
1.4
45
500
500
41
35
385
0 2
2 9 9
86
1.57
Min
43
! 8933510W
258
56
11
71
5 6
1.0
36
432
432
41
35
310
0 1
2 i 7.2
86
0.95
Min
Explanation of Symbols - % (percent), -I Index); Sodium (Na) and CEC reported in meq/100cm3 (milli -equivalent per 100 cubic centimeters)
Abbreviations Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
NCDA Soil Fertility Recommendations (Ibs/A) -
Sample ID
39
40
Crop
SOYBEANS
SOYBEANS
Lime N
TonsIAcn Nitrogen
06
03
P205 K20
Phosphate Potash
20
60
Mg
Magnesium
S
Sulfur
B
Bonn
Zn
Zinc
_
Mn
Manganese
Cu
Capper
See Note
3
3
41
SOYBEANS
04
30
3
42
SOYBEANS
0.5
3
43
SOYBEANS
04
40
3
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronam c Division
DWQ Laboratory Certification Number 635
lints document may be ,n rodieed Orly n do enhrety Waters Agcutural Labcratores has no contrd over be mannerwhich samples are taken, therefore analysts is based solely on rie sample as receved Laboratory liabdlty ts limited to the fee assessed on the referenced sample.

\ i 7 1,
WATERS FICyI.# ,r-
LAaOR og IES.1NC.
Soil Analysis Report - NCDA Index
Waters Agricultural Laboratories, Inc
364 W. Park Drive 1 Warsaw, NC 28398- 1 Phone [phone]
"113LT):-Cry IA1 - L71-all'V..
1,tfa1i'-SL%(E Lice'
HARVEYS-BEULAVILLE [60126] Grower: TRIPLE S FARMS Page 12
Farm: TRIPLE S FARM / NEW GROUND
1060 S NC 41 & 111 LID: D2FF3586194 Target pH: 6
BEULAVILLE, NC 28518 Test Method: Mehlich III Received: 12/14/2021 Processed: 12/16/2021
Sample ID Lab ID
P-I
K-I
Mg (%)
Ca (%)
pHw
Ac
S4
Zn4
Zn-AI Mn-I
Mn-AI
Cu-1 Na
ESP CEC BS (%)
HM (%)
Soil Class
52 8933600W
57
37
6
26
4 3
3.8
39
160
160 34
30
148
0 1
2 5 9
35
1.89
Min
Explanation of Symbols - % (percent -I (Index), Sodium (Na) and CEC reported in meq/100cm3 (milli•equivalent per 100 cubic centimeters)
Abbreviations: Ac (Acidity), CEC (Cation Exchange Capacity), BS (Base Saturation), HM (Humic Matter), ESP (Exchangeable Sodium Percentage)
r„a±
NCDA Soil Fertility Recommendations (Ibs/A)
Jt-:xrs.. s -:...
--e
Sample ID
52
:.47,A:msjtw�t.P;.w;,
Crop
SOYBEANS
Lime
Tons/Aare
— — 28
N
Nitrogen
P205
Phosphate
K20
Potash
70
Mg
Mapmadam
25
Sulfur
S____
—
B
Boron
Zn
Zinc
Mn
Manganese
Cu . I
Capper -
—
See Note
3
Explanation of Symbols - Ibs/A (pounds per acre)
Fertilizer recommendations are based on the philosophy and recommendations of the NCDA Agronomic Division
DWCI Laboratory Certification Number 635
ibis document may be re!radtced only n .6 enorery Wa'ers aynculural Labcralcnes has no control over to manner in which samples are then. therefore analysis is based sddy m the sample as recnxed Laboratory liadtly is limited ro to fee assessed on the referenced sample

2021 APPLICATION SUMMARY TABLE

TRIPLE S FARMS
LAND APPLICATION PROGRAM
PERMIT NO. WQ0030998
2021 APPLICATION SUMMARY ALL SOURCES
armer:::':.
Tract
/Site
::::::
:Field:::Acres
::::.
Date
Spread
::.:Dry:Ttitis:::
Gallons
;:::{:Acre::;
Dry;Tous.:::;::::;::=:=
Crop
Source .....:;
.
:'•::PA14::
::(lbs/ac)::
Eric Smith
1
1
34.2
Mar-21
24,000.00
0.04
1.28
Bermudagrass
Southwest Plantation
243.58
Mar-21
528,000.00
1.16
39.63
Bermudagrass
Wallace WWTP
281,686.47
0.57
19.38
Bermudagrass
Clayton Little Creek WRF
Mar-2I
80,000.00
0.12
4.10
Bermudagrass
Beulaville WWTP
Apr-2I
246,000.00
0.81
27.80
Bermudagrass
Wallace WWTP
Jul-21
353,500.00
0.73
25.06
Bermudagrass
Clayton Little Creek WRF
Aug-21
180,000.00
0.46
15.69
Bermudagrass
Wallace WWTP
Oct-21
355,080.00
0.85
29.17
Bermudagrass
Clayton Little Creek WRF
Oct-2l
12,000.00
0.02
0.64
Wheat
Southwest Plantation
47.10
Nov-21
228,080.00
0.55
18.74
Wheat
Clayton Little Creek WRF
Nov-21
66,000.00
0.09
2.97
Wheat
Kenansville WWTP .
Nov-21
80,000.00
0.12
4.10
Wheat
Beulaville WWTP
2
8.48
Jan-21
90,260.03
0.73
6.21
Wheat
Clayton Little Creek WRF
48.75
Mar-21
35,000.00
0.43
3.60
Bermudagrass
Warsaw WWTP
152.68
Apr-2I
138,000.00
1.84
15.59
Bermudagrass
Wallace WWTP
Sep-2I
48,000.00
0.49
4.18
Bermudagrass
Wallace WWTP
Sep-21
96,000.00
0.80
6.81
Bermudagrass
Clayton Little Creek WRF
4
4.14
Jan-2I
111,257.87
1.85
7.66
Fescue
Clayton Little Creek WRF
169.27
Mar-21
29,758.27
0.49
2.05
Fescue
Clayton Little Creek WRF
Sep-21
20,000.00
0.50
2.06
Fescue
Warsaw WWTP
5
11.2
Jan-21
185,362.67
1.14
12.75
Fescue
Clayton Little Creek WRF
174.62
Feb-21
127,835.02
0.79
8.80
Fescue
Clayton Little Creek WRF
Jun-21
78,120.00
0.56
6.29
Fescue
Clayton Little Creek WRF
Sep-2I
55,000.00
0.51
5.66
Fescue
Warsaw WWTP
7
14.5
Feb-2I
150,849.53
0.72
10.38
Wheat
Clayton Little Creek WRF
47.64
Jun-21
12,000.00
0.07
0.97
Bermudagrass
Clayton Little Creek WRF
201.14
Jun-21
234,000.00
1.82
26.44
Bermudagrass
Wallace WWTP
Aug-2I
198,000.00
1.19
17.26
Bermudagrass
Wallace WWTP
Oct-2I
288,000.00
2.24
32.55
Bermudagrass
Wallace WWTP
9
8.93
Mar-21
30,023.93
0.23
2.07
Fescue
Clayton Little Creek WRF
178.73
May-21
12,000.00
0.11
0.97
Fescue
Clayton Little Creek WRF
May-21
80,000.00
0.46
4.10
Fescue
Beulaville WWTP
Jun-21
198,000.00
2.51
22.38
Fescue
Wallace WWTP
Sep-2I
72,000.00
0.57
5.10
Fescue
Clayton Little Creek WRF
Oct-21
24,000.00
0.22
1.97
Fescue
Clayton Little Creek WRF
3A
13.7
Mar-2I
57,000.00
0.43
5.87
Bermudagrass
Warsaw WWTP
147.78
Apr-21
126,000.00
1.04
14.24
Bermudagrass
Wallace WWTP
May-21
12,000.00
0.05
0.64
Bermudagrass
Southwest Plantation
Jun-2I
36,000.00
0.21
2.90
Bermudagrass
Clayton Little Creek WRF
Jul-21
197,880.00
1.02
14.03
Bermudagrass
Clayton Little Creek WRF
Aug-2I
60,000.00
0.38
5.23
Bermudagrass
Wallace WWTP
Nov-21
108,050.00
0.65
8.88
Wheat
Clayton Little Creek WRF
47.08
3B
7.27
Jan-21
142,258.49
1.35
9.79
Fescue
Clayton Little Creek WRF
177.70
Jun-2I
158,000.00
2.24
16.27
Fescue
Warsaw WWTP
Sep-21
75,000.00
1.06
7.72
Fescue
Warsaw WWTP
Total Felds and Acres 8 102.45
Total
Town of Beulaville
Town of Clayton Little Creek WRF
Town of Kenansville
Southwest Plantation
Town of Wallace
Town of Warsaw
Gallons
Dry Tons
Metric
Tons
Permit Limit Dry Tons
5,720,002.28
479.97
436.34
NA
240,000.00
12.31
11.19
38
2,722,002.28
199.94
181.77
300
66,000.00
2.97
2.70
38
48,000.00
2.56
2.33
5
2,244,000.00
220.99
200.90
330
400,000.00
41.20
37.45
38
Branch Residuals Soils, LLC Confidential
2/14/2022
Page 1

2021 APPLICATION CONDITION SUMMARIES

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2021
Beulaville WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 1.23
Residual Report No.: BL 2021-14538
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/12/21
1
80,000.0
Dry
Warm,Clear
0.00
Total Gallons
80,000.0

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2021
Beulaville WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 1.23
Residual Report No.: BL 2021-14538
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/8/21
1
80,000.0
Dry
Warm,Clear
0.00
Total Gallons
80,000.0

Town of Beulaville
Beulaville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2021
Beulaville WWTP
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Surface
Field: 9
Percent Solids: 1.23
Residual Report No.: BL 2021-14538
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/31/21
9
40,000.0
Dry
Warm,Clear
0.00
6/1/21
9
40,000.0
Dry
Warm,Clear
0.00
Total Gallons
80,000.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 1.65
Residual Report No.: C 1-21-013-0004
Crop: Bennudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/8/21
1
30,191.4
Dry
Cool,Clear
0.00
3/10/21
1
30,047.7
Dry
Warm,Clear
0.00
3/11/21
1
11,377.4
Dry
Warm,Clear
0.00
3/15/21
1
24,020.0
Moist
cool,Cloudy
T
3/22/21
1
41,950.0
Dry
Cool,Clear
0.00
3/23/21
1
48,050.0
Dry
Cool,Clear
0.00
3/24/21
1
48,050.0
Dry
Warm,Cloudy
0.19
3/25/21
1
48,000.0
Dry
Warm,Cloudy
T
::::Total:Gallons:::::::::::::::::::::::::::::::::: 281,68:6.5

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer:
Eric Smith
Acres:
8.48
Site/Tract:
1
Application Method: Injected
Field:
2
Percent Solids:
1.65
Residual Report No.:
C 1-21-013-0004
Crop:
Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/18/21
2
30,253.0
Dry
Cool,Clear
0.00
1/19/21
2
30,034.5
Dry
Cool,Clear
0.00
1/20/21
2
29,972.5
Dry
Cool,Clear
0.00
;26. .

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
I st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 7.27
Site/Tract: 1
Application Method: Injected
Field: 3B
Percent Solids: 1.65
Residual Report No.: C 1-21-013-0004
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/13/21
3B
29,913.8
Moist
Cool,Clear
0.00
1/26/21
3B
16,053.0
Moist
Cool,Cloudy
0.42
2/2/21
3B
16,042.5
Dry
Cool,Clear
0.00
2/3/21
3B
30,691.3
Dry
Cool,Clear
0.00
2/8/21
3B
29,802.9
Dry
Cool,Clear
0.00
2/9/21
3B
19,755.0
Dry
Cool,Clear
0.00
11 Total qallons
2,258.5

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 4.14
Site/Tract: 1
Application Method: Injected
Field: 4
Percent Solids: 1.65
Residual Report No.: C 1-21-013-0004
Crop: Fescue
iii
..:.:.:.:...:.:.:.:.:.:.:.......................................................................................................................... .
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/15/21
4
16,753.0
Dry
Cool,Cloudy
0.32
1/21/21
4
30,039.4
Dry
Cool,Cloudy
T
1/26/21
4
9,029.5
Moist
Cool,Cloudy
0.42
2/1/21
4
25,811.1
Moist
Cool,Cloudy
0.04
2/10/21
4
29,624.9
Dry
Cool,Clear
0.00
• .. •Total:Gallons: i .........
.:::::::::. • . •::::;:::::1 :42 ...:9

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
lst Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres:
4.14
Site/Tract:
1
Application Method: Injected
Field:
4
Percent Solids:
1.65
Residual Report No.:
C 1-21-013-0004
Crop:
Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/5/21
4
29,758.3
Dry
Cool,Clear
0.00
otal Gallons:.:.....:
29758:3

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 11.2
Site/Tract: 1
Application Method: Injected
Field: 5
Percent Solids: 1.65
Residual Report No.: C 1-21-013-0004
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
1/11/21
5
11,482.1
Dry
cool,cloudy
0.03
1/12/21
5
21,593.0
Dry
Cool,Cloudy
0.23
1/15/21
5
13,333.4
Dry
Cool,Cloudy
0.32
1/22/21
5
30,100.6
Moist
Cool,Clear
0.00
1/26/21
5
4,950.4
Moist
Cool,Cloudy
0.42
1/29/21
5
20,133.6
Moist
Cool,Clear
0.00
2/2/21
5
13,453.3
Dry
Cool,Clear
0.00
2/4/21
5
30,176.2
Dry
Cool,Cloudy
T
2/5/21
5
29,868.8
Moist
Cool,Cloudy
0.22
2/9/21
5
10,271.2
Dry
Cool,Clear
0.00
::Total:Gallon::::::.:.:.::::::::::::::::::::::::::::::::1 .362:7.

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 11.2
Site/Tract: 1
Application Method: Surface
Field: 5
Percent Solids: 1.65
Residual Report No.: C 1-21-013-0004
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/11/21
5
33,467.5
Dry
Cool,Cloudy
0.45
2/12/21
5
31,947.0
Moist
Cool,cloudy
0.10
2/22/21
5
30,390.1
Dry
Cool,Cloudy
0.29
2/23/21
5
32,030.5
Moist
Cool,Clear
0.00
. i .. ThatGallon:::.:.:.:.:.:::::.......:.:::;::::::::12• 835:0'

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 14.5
Site/Tract: 1
Application Method: Injected
Field: 7
Percent Solids: 1.65
Residual Report No.: C. 1-21-013-0004
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
2/24/21
7
30,331.3
Dry
Warm,Clear
0.00
2/25/21
7
30,099.1
Dry
Warm,Clear
0.00
2/26/21
7
30,175.8
Dry
Cool,Cloudy
0.04
3/1/21
7
30,625.0
Moist
Warrn,Cloudy
0.08
3/2/21
7
29,618.3
Dry
Cool,Clear
0.00
: : iital i Gilliiiii ::.::i:i::•::
:. : • • • •.. • •••••••
::. 5%8493

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
1st Quarter
Clayton Little Creek WRF
Farmer: Eric Smith
Acres:
8.93
Site/Tract:
1
Application Method: Injected
Field:
9
Percent Solids:
1.65
Residual Report No.:
C 1-21-013-0004
Crop:
Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/3/21
9
30,023.9
Dry
(bol,Cloudy
T
:::. Total :Gallons:" >. .
30;023.9

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
2nd Quarter 2021
Clayton Little Creek WRF
Farmer: Eric Smith
Acres:
13.73
Site/Tract: 1
Application Method: Injected
Field: 3A
Percent Solids:
1.93
Residual Report No.: C 2-21-144-0002
Crop:
Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/28/21
3A
36,000.0
Dry
Warm,Cloudy
0.07
:•:-:•:•:•:•....:•:•:•:•:-.
.400.10

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
2nd Quarter 2021
Clayton Little Creek WRF
Farmer:
Eric Smith
Acres:
11.2
Site/Tract:
1
Application Method: Injected
Field:
5
Percent Solids:
1.93
Residual Report No.:
C 2-21-144-0002
Crop:
Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/29/21
5
36,000.0
Dry
Warm,Cloudy
0.14
6/30/21
5
42,120.0
Dry
Hot,Clear
0.00
TotaLGallons.:.

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
2nd Quarter 2021
Clayton Little Creek WRF
Farmer: Eric Smith
Acres:
14.5
Site/Tract:
1
Application Method: Injected
Field:
7
Percent Solids:
1.93
Residual Report No.:
C 2-21-144-0002
Crop:
Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/18/21
7
12,000.0
Dry
Hot,Clear
0.00

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
2nd Quarter 2021
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 8.93
Site/Tract:
1
Application Method: Injected
Field:
9
Percent Solids: 1.93
Residual Report No.:
C 2-21-144-0002
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/27/21
9
12,000.0
Dry
Hot,Clear
0.00
.•.•.•.•.•.•. .
:;000A

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter 2021
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 1.7
Residual Report No.: C 3-21-207-0004
Crop: Bermudagrass
l'':•:.:•:':•::iiiil!il:
iililiiii iiiiiiiiiiiiiiiiii.„ :iiiilili!iiiliiiliiiii.iiiiliiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiigiiiiiiiiiiiiiiiiiii
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/6/21
1
36,000.0
Dry
Hot,Clear
0.00
7/7/21
1
54,000.0
Dry
Hot,Cloudy
0.30
7/14/21
1
30,000.0
Dry
Hot clrar
0.00
7/15/21
1
30,000.0
Dry
Hot,Cloudy
0.02
7/16/21
1
30,000.0
Dry
Hot,Clear
0.00
8/10/21
1
18,000.0
Dry
Hot,Clear
0.00
8/11/21
1
12,000.0
Dry
Hot,Clear
0.00
8/12/21
1
24,000.0
Dry
Hot,Clear
0.00
8/13/21
1
18,000.0
Dry
Hot,Clear
0.00
8/17/21
1
24,000.0
Moist
Warm,Cloudy
0.21
8/18/21
1
24,000.0
Moist
Hot,Cloudy
0.02
8/20/21
1
24,000.0
Moist
Hot,Cloudy
T
8/23/21
1
17,500.0
Dry
Hot,Clear
0.00
8/25/21
1
12,000.0
Dry
Hot,cioud)
0.05
iii]ii . :3.041:qj. ................... .:H • ...... • ......
.1353,5O0.O

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter 2021
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Injected
Field: 2
Percent Solids: 1.7
Residual Report No.: C 3-21-207-0004
Crop: Bermudagrass
!miim
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/2/21
2
42,000.0
Moist
Warm,Clear
0.00
9/7/21
2
12,000.0
Moist
Hot,Clear
0.00
9/8/21
2
18,000.0
Dry
Hot,Cloudy
0.01
9/9/21
2
12,000.0
Dry
Warm,Cloudy
0.23
9/10/21
2
12,000.0
Moist
Warm,Clear
0.00
::96.iflOILO

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter 2021
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 13.73
Site/Tract: 1
Application Method: Injected
Field: 3A
Percent Solids: 1.7
Residual Report No.: C 3-21-207-0004
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/1/21
3A
4,000.0
Dry
Hot,Cloudy
0.08
7/1/21
3A
32,000.0
Dry
Hot,Cloudy
0.08
8/30/21
3A
35,980.0
Dry
Hot,Clear
0.00
8/31/21
3A
5,990.0
Dry
Hot,Clear
0.00
9/13/21
3A
35,900.0
Dry
Hot,Clear
0.00
9/14/21
3A
6,010.0
Dry
Hot,Clear
0.00
9/15/21
3A
24,000.0
Dry
Hot,Clear
0.00
9/16/21
3A
42,000.0
Dry
Warm,Clear
0.00
9/17/21
3A
2,000.0
Dry
Warm,Clear
0.00
9/17/21
3A
10,000.0
Dry
Warm,Clear
0.00
:::':Total Gallons :: >:.:::.:.:.:.::::.>.::;:_:
::197,880.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
3rd Quarter 2021
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Injected
Field: 9
Percent Solids: 1.7
Residual Report No.: C 3-21-207-0004
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/20/21
9
18,000.0
Dry
Warm,Cloudy
T
9/21/21
9
6,000.0
Moist
Warm,Cloudy
0.03
9/27/21
9
30,000.0
Dry
Warm,Clear
0.00
9/28/21
9
18,000.0
Dry
Warm,Clear
0.00
Tiital:GAIIOIT '.::' ' :::.:.:
:::::::::ii: * :::::
::::i. : 2;000.0.

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
4th Quarter 2021
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 1.97
Residual Report No.: C 4-21-295-0003
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/11/21
1
36,000.0
Dry
Warm,Clear
0.00
10/12/21
1
48,020.0
Dry
Warm,Clear
0.00
10/13/21
1
60,000.0
Dry
Warm,Clear
0.00
10/14/2.1
1
42,020.0
Dry
Warm,Clear
0.00
10/15/21
1
12,010.0
Dry
Warm,Clear
0.00
10/18/21
1
24,030.0
Dry
Warm,Clear
0.00
10/19/21
1
24,000.0
Dry
Warm,Clear
0.00
10/20/21
1
24,000.0
Dry
Warm,Clear
0.00
10/21/21
1
25,000.0
Dry
Warm,Clear
0.00
10/22/21
1
5,990.0
Dry
Warm,Clear
0.00
10/25/21
1
12,000.0
Dry
Warm,Cloudy
0.03
10/26/21
1
12,000.0
Dry
Warm,Clear
0.00
10/28/21
1
30,010.0
Dry
Warm,Cloudy
0.08
••3.55..;08.10

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
4th Quarter 2021
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Injected
Field: 1
Percent Solids: 1.97
Residual Report No.: C 4-21-295-0003
Crop: Wheat
:ii:::iiii:i!i::i:iii!!! !i i:.:ii!i:;i•iii::
!!i0;q:iiil! ::::i:::ii:ii:i::::.,:. iiii:i:::::
iiligiiiiiiiii::111i:iiiil
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/1/21
1
24,000.0
Dry
Warm,Clear
0.00
11/2/21
1
12,000.0
Dry
Warm,Clear
0.00
11/3/21
1
24,000.0
Dry
Cool,Clear
0.00
11/4/21
1
12,000.0
Dry
Cool,Cloudy
0.01
11/5/21
1
12,000.0
Dry
Cool,Clear
0.00
11/23/21
1
35,960.0
Moist
Cool,Clear
0.00
11/24/21
1
24,000.0
Dry
Cool,Clear
0.00
11/29/21
1
42,070.0
Dry
Cool,Clear
0.00
11/30/21
1
18,000.0
Dry
Cool,Clear
0.00
12/1/21
1
12,000.0
Dry
Cool,Clear
0.00
12/2/21
1
12,050.0
Dry
Warm,Clear
0.00
' ?::. '' : ' Toial:Galloiit ' :i :•..:.:*
'' .::..i; ]ii:'-'::::. 8,080'.0

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
4th Quarter 2021
Clayton Little Creek WRF
Farmer: Eric Smith
Acres: 13.73
Site/Tract: 1
Application Method: Injected
Field: 3A
Percent Solids: 1.97
Residual Report No.: C 4-21-295-0003
Crop: Wheat
,.,i::,*•ii . • . " : ii:.0Y! • k. iiiiiiiii!iiiliiiiililiiipiiiiiiii!
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/9/21
3A
18,000.0
Dry
Warm,Clear
0.00
11/10/21
3A
12,000.0
Dry
Warm,Clear
0.00
11/11 /21
3A
12,000.0
Dry
warmaoudy
0.03
11/15/21
3A
12,020.0
Dry
Cool,Clear
0.00
11/16/21
3A
12,010.0
Dry
Cool,Clear
0.00
11/17/21
3A
12,000.0
Dry
Warm,Clear
0.00
11/18/21
3A
6,010.0
Dry
Warm,Clear
0.00
11/22/21
3A
24,010.0
Dry
Cool,Cloudy
0.34
. • . TO.f4M400.1W:1:. ..:::
: ...:,*: ::::: ::::
.i:IIMMQ.

Triple S Farms & Cleaning, Inc
Clayton, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
4th Quarter 2021
Clayton Little Creek WRF
Farmer: Eric Smith
Acres:
8.93
Site/Tract:
1
Application Method: Injected
Field:
9
Percent Solids:
1.97
Residual Report No.:
C 4-21-295-0003
Crop:
Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/1/21
9
24,000.0
Dry
Warm (:: it
0.00
4 000.0

Town of Kenansville
Kenansville, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2021
Kenansville WWTP
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 1.08
Residual Report No.: KV 2021-08913
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/5/21
1
66,000.0
Dry
Cool,Clear
0.00
Total Gallons
66,000.0

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2021
Southwest Plantation
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 1.28
Residual Report No.: SWP 2021 3-21
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/5/21
1
12,000.0
Dry
Cool,Clear
0.00
4/21/21
1
12,000.0
Dry
Warm,Clear
0.00
Total Gallons
24,000.0

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2021
Southwest Plantation
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids: 1.28
Residual Report No.: SWP 2021 3-21
Crop: Wheat
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/26/21
1
12,000.0
Dry
Warm,Clear
0.00
Total Gallons
12,000.0

Triple S Farms
Jacksonville, North Carolina
Triple S Farms
WQ0030998
Annual 2021
Southwest Plantation
Farmer: Eric Smith
Acres: 13.73
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 1.28
Residual Report No.: SWP 2021 3-21
Crop: Bermudagrass
...... . . ...... . . . . .......
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
5/20/21
3A
12,000.0
Dry
Warm,Clear
0.00
.:::Totii :6aliciii:S.. .

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
1st Quarter 2021
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Incorporated
Field: 1
Percent Solids: 1.8
Residual Report No.: WL 1-2021-01193
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/8/21
1
108,000.0
Dry
Cool,Clear
0.00
3/9/21
1
144,000.0
Dry
Warm,Clear
0.00
3/10/21
1
138,000.0
Dry
Warm,Clear
0.00
3/11/21
1
138,000.0
Dry
Warm,Clear
0.00
Total Gallons
528,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2021
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Incorporated
Field: 1
Percent Solids: 2.71
Residual Report No.: WL 2-2021-06258
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/21/21
1
54,000.0
Dry
Warm,Clear
0.00
4/22/21
1
66,000.0
Dry
Cool,Clear
0.00
4/23/21
1
90,000.0
Dry
Cool,Clear
0.00
4/28/21
1
36,000.0
Dry
Warm,Clear
0.00
Total Gallons
246,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2021
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Incorporated
Field: 2
Percent Solids: 2.71
Residual Report No.: WL 2-2021-06258
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/28/21
2
72,000.0
Dry
Warm,Clear
0.00
6/25/21
2
66,000.0
Dry
Warm,Cloudy
0.16
Total Gallons
138,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2021
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 13.73
Site/Tract: 1
Application Method: Incorporated
Field: 3A
Percent Solids: 2.71
Residual Report No.: WL 2-2021-06258
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
4/29/21
3A
96,000.0
Dry
Warm,Clear
0.00
4/30/21
3A
30,000.0
Dry
Warm,Clear
0.00
Total Gallons
126,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2021
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 14.5
Site/Tract: 1
Application Method: Incorporated
Field: 7
Percent Solids: 2.71
Residual Report No.: WL 2-2021-06258
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/21/21
7
18,000.0
Moist
Hot,cioudy
0.05
6/23/21
7
96,000.0
Moist
Warm,Clear
0.00
6/24/21
7
120,000.0
Dry
Warm,Clear
0.00
Total Gallons
234,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
2nd Quarter 2021
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 8.93
Site/Tract: 1
Application Method: Incorporated
Field: 9
Percent Solids: 2.71
Residual Report No.: WL 2-2021-06258
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/2/21
9
12,000.0
Dry
war,n,CIoudy
0.38
6/7/21
9
36,000.0
Dry
Warm,Cloudy
0.02
6/14/21
9
78,000.0
Dry
Hot,Cloudy
0.18
6/15/21
9
72,000.0
Dry
Hot,Cloudy
0.03
Total Gallons
198,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2021
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 34.2
Site/Tract: 1
Application Method: Incorporated
Field: 1
Percent Solids: 2.09
Residual Report No.: WL 3-2021-12254
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/11/21
1
36,000.0
Moist
Hot,Clear
0.00
8/12/21
1
24,000.0
Dry
Hot,Clear
0.00
8/13/21
1
30,000.0
Dry
Hot,Clear
0.00
8/16/21
1
30,000.0
Dry
Hot,Cloudy
T
8/17/21
1
12,000.0
Moist
Warm,Cloudy
0.21
8/18/21
1
12,000.0
Moist
Hot,Cloudy
0.02
8/20/21
1
6,000.0
Moist
Hot,Cloudy
T
8/22/21
1
6,000.0
Dry
Hot,Cloudy
0.18
8/23/21
1
24,000.0
Dry
Hot,Clear
0.00
Total Gallons
180,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2021
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Incorporated
Field: 2
Percent Solids: 2.09
Residual Report No.: WL 3-2021-12254
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/1/21
2
30,000.0
Dry
xot,cioudy
T
9/2/22
2
18,000.0
Dry
Warm,Cloudy
0.01
Total Gallons
48,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2021
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 13.73
Site/Tract: 1
Application Method: Incorporated
Field: 3A
Percent Solids: 2.09
Residual Report No.: WL 3-2021-12254
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/30/21
3A
36,000.0
Dry
Hot,Clear
0.00
8/31/21
3A
24,000.0
Dry
Hot,Clear
0.00
Total Gallons
60,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
3rd Quarter 2021
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 14.5
Site/Tract: 1
Application Method: Incorporated
Field: 7
Percent Solids: 2.09
Residual Report No.: WL 3-2021-12254
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
8/24/21
7
66,000.0
Dry
Hot,Clear
0.00
8/25/21
7
78,000.0
Dry
Hot,Cloudy
0.05
8/26/21
7
30,000.0
Dry
Hot,Clear
0.00
8/27/21
7
24,000.0
Dry
Hot,Clear
0.00
Total Gallons
198,000.0

Triple S Farms
Wallace, North Carolina
Triple S Farms
WQ0030998
4th Quarter 2021
Wallace WWTP
Stabilization Method None
Farmer: Eric Smith
Acres: 14.5
Site/Tract: 1
Application Method: Incorporated
Field: 7
Percent Solids: 2.71
Residual Report No.: WL 4-2021-17320
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
10/4/21
7
72,000.0
Dry
Warm,cloudy
0.12
10/5/21
7
84,000.0
Dry
Warm,Clear
0.00
10/6/21
7
90,000.0
Dry
Warm,Clear
0.00
10/7/21
7
42,000.0
Dry
warm,Cloudy
0.07
Total Gallons
288,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2021
Warsaw WWTP
Farmer: Eric Smith
Acres: 8.48
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids: 2.47
Residual Report No.: WR 2021-15014
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/19/21
2
18,000.0
Moist
Cool,Cloudy
0.22
3/22/21
2
17,000.0
Dry
Cool,Clear
0.00
Total Gallons
35,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2021
Warsaw WWTP
Farmer: Eric Smith
Acres: 13.73
Site/Tract: 1
Application Method: Surface
Field: 3A
Percent Solids: 2.47
Residual Report No.: WR 2021-15014
Crop: Bermudagrass
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
3/19/21
3A
30,000.0
Moist
Cool,Cloudy
0.22
3/22/21
3A
27,000.0
Dry
Cool,Clear
0.00
Total Gallons
57,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2021
Warsaw WWTP
Farmer: Eric Smith
Acres: 7.27
Site/Tract: 1
Application Method: Surface
Field: 3B
Percent Solids: 2.47
Residual Report No.: WR 2021-15014
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
6/26/21
3B
18,000.0
Moist
Warm,Cloudy
0.29
6/28/21
3B
48,000.0
Dry
Warm,Cloudy
0.07
6/29/21
3B
48,000.0
Dry
Warm,Cloudy
0.14
6/30/21
3B
44,000.0
Dry
Hot,Clear
0.00
Total Gallons
158,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2021
Warsaw WWTP
Farmer: Eric Smith
Acres: 7.27
Site/Tract: 1
Application Method: Surface
Field: 3B
Percent Solids: 2.47
Residual Report No.: WR 2021-15014
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/15/21
3B
75,000.0
Dry
Hot,Clear
0.00
Total Gallons
75,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2021
Warsaw WWTP
Farmer: Eric Smith
Acres: 4.14
Site/Tract: 1
Application Method: Surface
Field: 4
Percent Solids: 2.47
Residual Report No.: WR 2021-15014
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/14/21
4
20,000.0
Dry
Hot,Clear
0.00
Total Gallons
20,000.0

Town of Warsaw
Warsaw, North Carolina
Triple S Farms & Cleaning, Inc
WQ0030998
Annual 2021
Warsaw WWTP
Farmer: Eric Smith
Acres: 11.2
Site/Tract: 1
Application Method: Surface
Field: 5
Percent Solids: 2.47
Residual Report No.: WR 2021-15014
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
9/14/21
5
55,000.0
Dry
Hot,Clear
0.00
Total Gallons
55,000.0