WQ0002712_Residual Annual Report 2021_20220221

Non -Discharge Branch Upload/Submittal Form
NORTH CAROLINA
EnvironmentalQuul1ty
Version 2 - Revised June 23, 2020
Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?*
Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0002712
Applicant/Permittee City of Lincolnton
Email Notifications
Does this need review by the hydrogeologist? * 0 Yes OO No
Regional Office
CO Reviewer
Admin Reviewer
Mooresville

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name*
Lysa Finnerty
Email Address*
[e-mail]
Project Information
Application/Document Type *
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
14105376150
O Modification - Minor
O Renewal
O GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Permit Number:*
Applicant/Permittee Address *
Facility Name*
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
WQ0002712
Has Current Existing permit number
435 Williams Court, Ste 100, Baltimore, MD 21220
City of Lincolnton Class B Residuals Program
Please provide comments/notes on your current submittal below.
2021 Annual Report for City of Lincolnton, NC
High -Rate Infiltration
Reclaimed Water
Residuals
Other
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Lincolnton NC 2021 Annual Report FINAL.pdf 23.02MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
lyaa„ff./0u0
Submission Date 2/21/2022

435 Williams Court, Suite 100
Baltimore, MD 21220
wwwsynagro.com
SYNAGRO
FEBRUARY 21, 2022
NCDEQ
Division of Water Resourcs
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2021 Annual Report for Permit No. WQ0002712
Dear NCDEQ:
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Lincolnton, NC.
If you have any questions or need additional information, please do not hesitate to contact
Robert Pearson at [phone] or Alex Fox at [phone].
Sincerely,
De't ic& Sfiiva't 25
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Robert Pearson, City of Lincolnton
Alex Fox, Synagro
YOUR PARTNER FORA CLEANER, GREENER WORLD

CITY OF LINCOLNTON, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0002712
2021 ANNUAL REPORT

City of Lincolnton, NC
Residuals Land Application Program
2021 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00002712 County Lincoln Year 2021
Facility Name (as shown on permit) City of Lineolntou WWTP and WTP NPDES No. NC(1025496 Sr 0085588
Land Application Operator Synagro Phonic# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please enact: an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 33
TomI number of fields utilized for land application during the year: >s
Total amount of dry tons applied during the year for all application sites: 636,82
Total number of acres utilized for land application during the year: 250-00
Part B—Annual Compliance Statement:
Facility was compliant during calendar year 2021 with all conditions ofthc land application permit (including but sot limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
if no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
S. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Awtual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results arc attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specked m the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. AU monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations arc
attached to include appropriate actions and remediations.
1 1. Vegetative cover was maintained and proper crop management was perfomicd on each site receiving residuals, as specified
in the permit
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified Olathe permit were maintained during each application of residuals.
Part C — Certification:
"1 certify, under penalty of law, that the above information is, to the best of m
am aware that there are significant penalties for submitting false informed
;mowing violations."
Robert Pearson, Water Services Director
Pemtitteg44ame and or print)
owledge and
tiding the p
Signature ofP
true, accurate, and complete. 1
ty of fines and imprisonment for
2'2---
Date`— !L
2/9/2022
Signature of Preparer' i %% Date Signa. . d A. cr Date
(if different from Permittee) !/ (if different from ' crmittce and Preparer)
"Preparer is defined in 40 CFR Part 503.9(r) and l5A NCAC 02T .1102 (26) DENR FORM ACV (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2021 - 6/24/2021
LINCOLNTON, NC
LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
January 2021 446,400.00 G 104.06 D 94.38
March 2021 483,600.00 G 112.73 D 102.24
April 2021 799,800.00 G 151.08 D 137.03
May 2021 440,200.00 G 83.15 D 75.42
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/3/2022 10:00:19 AM
2,170,000.00 G 451.02 D
409.08

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 6/29/2021 - 8/20/2021
LINCOLNTON, NC
LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
June 2021 297,600.00 G 56.22 D 50.99
July 2021 477,400.00 G 55.74 D 50.56
TOTAL 775,000.00 G 111.96 D 101.55
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/3/2022 10:09:43 AM

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 10/14/2021 - 12/3/2021
LINCOLNTON, NC
LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
October 2021 297,600.00 G 34.75 D 31.52
TOTAL 297,600.00 G 34.75 D 31.52
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/3/2022 10:11:49 AM

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 12/28/2021 - 12/31/2021
LINCOLNTON, NC
LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT DRY METRIC TONS
December 2021 223,200.00 G 39.09 D 35.46
TOTAL 223,200.00 G 39.09 D 35.46
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/3/2022 10:13:22 AM

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Piease note that your permit may contain additional parameters to be analyzed. The parameters can be reported In FORM RSSF - B
WQ Permit Number: WQ0002712 Laboratory:
Facltity Name: LINCOLNTON, NC PACE ANALYTICAL
Residual Source WQ 8 or
NPDES#: NC0025496
WWTP Name: L0NCOLNTON WWTP
Residual Analysis Data
Product Type
LIQ LIQ LIQ LIQ
Sample or Composite Date 01/04/21 04/06/21 07/06/21 11/02/21
Parameter (mg/kg dry weight) Ceiling Conc.
Limit
Percent Solids (%) NA 5.59 4.53 2.80 4.20
Arsenic 75 6.8 4.5 3.8 4,7
Cadmium B5 0.44 <0.43 <0.74 0.77
Capper 4300 220 230 180 280
Chromium NA 56 41 29 110
Lead 840 12 8.3 5 15
Mercury 57 <0.33 <0.39 <0.68 <0.46
Molybdenum 75 6.6 <3.4 <5.9 5.5
Nickel 420 12 8.2 <6.2 12
Selenium 100 4.1 <2.8 <4.8 3.8
Zinc 7500 250 130 87 270
Total Phosphorus NA 11000 14000 7200 16000
TKN NA 48000 34000 17000 42000
Ammonia -Nitrogen NA 11000 12000 1300 18000
Nitrate and Nitrite NA 79.7 60.3 2108 48.5
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision In accordance with a system designed to assure that qualified
personnel property gathered end evaluated the Information submitted. I am aware that there are significant penalties for submitting false Information, including the
ppsgibl)lty dikes and Imprisonment for knowing violations,"
Signature of Preparer
2-9-2022
Delo
'Preparer is defined in 40 CFR Part 503.9(r} and 15 A NCAC 2T.1102(26} DENR FORM RSSF (12/2006)
Printed: 2/2/2622 5:07:04 PM For: 2161 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM ROOF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed,
WQ Permit Number:
Facility Name:
Residual Source
NPDES 8 or WON:
WWTP Name:
WQ0002712
LINCOLNTON, NC
NC0025496
LINCOLNTON WWTP
Residual Analysis Data
Laboratory:
PACE ANALYTICAL
Product Type
Sample or Composite Date
Parameters (mglkg dry weight)
Aluminium
Calcium
Magnesium
pH (s.u.)
Potassium
Sodium
PAN
SAR (Ratio)
LIQ LIQ LIQ LIQ
01/04/21 04/06121 07)06/21 11/02/21
9700 11000 8800 12000
8600 5400 3800 8900
4500 2700 1509 2900
7.30 6.80 5.80 7.30
2500 4000 1900 3000
740 1200 2200 1000
12980 10460 5898 13849
0.3792 0.7059 1.2754 0.4809
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false Information, Inciuding the
rissibility of fines and imprisonment for knowing violations."
oO'
Signature of Proparer'
'Preparer Is defined In 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
2-9-2022
Date
Printed: 2/2/25225:08:08 PM For: 2161 01 DENR FORM RSSF-R (12/2006)

PaceAnalytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Adam Brigman
Project Name: Lincolnton VWVTP
Lot Number:WA05054
Date Completed:01/28/2021
01/28/2021 1:10 PM
Approved and released by:
Project Manager II: Lucas Odom
A413
ANSI National Accreditation Board
ACCREDITED
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653
NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: WA05054
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to low % solids the initial amount of sample -001 was 3 times the standard procedure amount per
PM's request. The LOQ has been adjusted accordingly.
TKN
Sample -001 was run at reduced volume due to sample sludge matrix. LOW has been adjusted
accordingly.
The method blank for analytical batch 80782 contained the analyte Total Kjeldahl Nitrogen (TKN) greater
than the acceptance criteria. The associated sample, WA05054-001, contained detections for this analyte
at concentrations greater than 10X the value found in the method blank; therefore sample results are not
impacted. The data has been reported.
Pace Analytical Services, LLC (formerly ShealyEnvironmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2of7

Client:Synagro
Description: Lincolnton WWTP
Date Sampled:01/04/2021 0950
Date Received:01/05/2021
Laboratory ID:WA05054-001
Matrix: Solid
% Solids: 5.59 01/07/2021 0115
Inorganic non-metals
Run Prep Method
1
1 350.1
1
1
1
1
3 351.4
Analytical Method
(% Solids) SM 2540G
(Ammonia - N ) 350.1
(Nitrate - N ) 9056A
(Nitrite - N ) 9056A
(Phosphorus) 365.1
(Soil pH meas) 9045D
(TKN) 351.2
Dilution
1
25
5
1
25
1
2
Analysis Date Analyst
01/07/2021 0115 MOM
01/08/2021 1022 DRD
01/08/2021 2005 AMR
01/08/2021 1225 AMR
01/08/2021 1116 DMA
01/07/2021 2330 AAB
01/26/2021 1700 DMA
Prep Date Batch
78694
78739
79020
79022
01/07/2021 1936 78800
78814
01/22/2021 1642 80429
Parameter
CAS
Number
Analytical
Method
Result Q LOQ
DL
Units Run
Solids
Ammonia - N (gas diffusion)
Nitrate - N (soluble)
Nitrite - N (soluble)
Phosphorus
Soil pH measured in water @ 19.4 ° C
TKN
7723-14-0
SM 2540G
350.1
9056A
9056A
365.1
9045D
351.2
CVAA
5.59
11000
75
4.7
11000
7.3
48000
450
45
3.6
2200
900
230
9.0
1.8
450
900
1
mg/kg 1
mg/kg 1
mg/kg 1
mg/kg 1
su 1
mg/kg 3
Run Prep Method
1 7471B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
7471B 1 01/07/2021 1004 JAB2 01/07/2021 0400 78580
Parameter
CAS
Number
Analytical
Method
Result Q LOQ
DL
Units Run
Mercury
7439-97-6 7471 B
ICP-AES
ND 1.4
0.33
mg/kg 1
Run Prep Method
1 3050B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
6010D 1 01/08/2021 1653 KSH2 01/08/2021 0311 78587
Parameter
CAS
Number
Analytical
Method
Result Q LOQ
DL
Units Run
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
7429-90-5
7440-38-2
7440-43-9
7440-70-2
7440-47-3
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-98-7
7440-02-0
6010D 9700 120 44 mg/kg 1
6010D 6.8 4.4 1.5 mg/kg 1
6010D 0.44 J 1.5 0.37 mg/kg 1
6010D 8600 1500 180 mg/kg 1
6010D 56 2.9 0.73 mg/kg 1
6010D 220 2.9 1.3 mg/kg 1
6010D 12000 29 13 mg/kg 1
6010D 12 2.9 1.3 mg/kg 1
6010D 4500 1500 180 mg/kg 1
6010D 220 4.4 1.7 mg/kg 1
6010D 6.6 J 12 2.9 mg/kg 1
6010D 12 12 3.1 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank
N = Recovery is out of criteria
W = Reported on wet weight basis
E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
DL = Detection Limit
J = Estimated result < LOQ and > DL
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of7

Client:Synagro Laboratory ID:WA05054-001
Description: Lincolnton WWTP Matrix: Solid
Date Sampled:01/04/2021 0950 % Solids: 5.59 01/07/2021 0115
Date Received:01/05/2021
ICP-AES
Run Prep Method
1 3050B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
6010D 1 01/08/2021 1653 KSH2 01/08/2021 0311 78587
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Potassium
Selenium
Sodium
Zinc
7440-09-7 6010D 2500 1500 180 mg/kg 1
7782-49-2 6010D 4.1 J 5.8 2.4 mg/kg 1
7440-23-5 6010D 740 J 1500 180 mg/kg 1
7440-66-6 6010D 250 15 3.6 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank
N = Recovery is out of criteria
W = Reported on wet weight basis
E = Quantitation of compound exceeded the calibration range DL = Detection Limit
P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4of7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

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Client: Oyu,#c,ur7
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ATo
❑ No
I Yes ❑N
'nY.es
ri Yes
❑ Yes
D Nu
LI No
u..
❑ No
LI' No
IN. ?�NA
E RfiNA
J No DNA
No
JA
9. WP an l lv.ir.tion date & time l iakal cn all sample containers?
JCL, Did s;II ceatairtcr Iahel iidhrm,tior. (la date, lirr,c) 1.1.V4212. with the CDC?
I. Were It GIs -,a be ?el formed listed on tt e COC?
12. Did all sarnples arrive iA prup4r containers for each test an(Por iu i,00d cundr.:c
(unbroken, lids. on, etc.)?
13. Was aclequulc somplo valance a4aiiahlr?
14. Were all samples rece.i e4 Yitlr n [ he holdi,q tltne or 48 _lours, w])ich.tym- U rmm first?
15. Wereane sump[cscantainvrsanissing,'ex.c4ss ('circleafe) ...airripir--9 Not listed or. COC?
16. Fur 'OA and RSK-175 samples, were 'illbrAMS present -,:pea-SI2s:" {'/i"ur 6mm in diameter)
trr arry of [he VOA vials?
[7- Were All LIkO'mctalslnutrientsamples receivni at pH if<2?
18, Were; tiIJ cyanide samplrs received at a pH > 12 and sulfide samples Mrrived at a J�:I `-• ?2
19- 'We ill app T-LTKN?r:yaaidephertot625, l r61:4.3 {ti. 0.5111.8.01.) ra,? Iras ti.ee 0I-
rtr¢:r11r9I chlorine?
❑ Y.-~5 ❑ No NA
• Yes LJ NO�
Sarup Preaervatlnu
20, Wire client remarkafrcquexts (i.e- requesi.d dilutions, N[S1+ SD designation ,
curivct:p traineri1nd from the cOC into the comnleir[ seoli0:i in UMS7
21- Was [lie cuotc number listed. oil the' container lal-x 1? ] ..es,"Quote # NA
(.dust 'a' competed rar 8113' arfrplc(s) intorrettly preserved or wilt; hcacspace.)
Sample(s) NA s received incnn-porly p:-ese,'Mei[ an;1 wrGre adjusted accordingly
in sample ter iviog with Nd arte.: 1i2$04, HIS O3, 13C:1, NaOH using SR Ir `tA
lime ofpreScrauu on NA . I` more Lila° 1-ma [14;Y:re alive L need Ed, please twt Ja lc 40rnrnonts below,
5arrrple(0 r- - were received with bubbles >6 mn- in disone'er-
Sarirlrs(a) N.A we:nc rarsfivod witty TRC x 0.5 nsg?!, {]''+:-.19 is w) and were
adjt.Lskti according[y in sample receiYing with sodiutn thins iIFatc (Na2SeOs) With Shealy ID: NA
SR baruusle labels applied by; hdFJi Date.: 0ll73.' 0c:
•
Ca rn rncnts:
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Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
Sample Date Report Range Ratio
2161-01-LIQ-NC LINCOLNTON, NC WWTP ANAEROB. DIGESTED 1/4/2021 1/1/2021 - 3/31/2021 0.3792
LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (740 x 5.5900) = 100 = 41.366
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (8600 x 5.5900) = 100 = 480.74
Mg mg/I = (mg mg/kg x % Solids) = 100 = (4500 x 5.5900) = 100 = 251.55
Na meq = Na mg/I = Molec.Wgt.Na = 41.366 = 23 = 1.79852
Ca meq = Ca mg/I = Molec.Wgt.Ca = 480.74 = 20 = 24.037
Mg meq = Mg mg/I = Molec.Wgt.Mg = 251.55 = 12 = 20.9625
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.79852 = SgrRoot[0.5(24.037+20.9625)] = 0.379164

PaceAnalytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Lincolnton
Lot Number:WD06050
Date Completed:04/15/2021
04/16/2021 9:16 AM
Approved and released by:
Project Manager II: Lucas Odom
A413
ANSI National Accreditation Board
ACCREDITED
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 16

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653
NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: WD06050
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix, the initial sample amount used for the following sample deviated from the standard
procedure 3: WD06050-001. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The following sample was diluted due to the nature of the sample matrix: WD06050-001. The LOQ has
been elevated to reflect the dilution.
Geometric Mean
54,087
Pace Analytical Services, LLC (formerly ShealyEnvironmetal Services, Inc.)
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Page 2 of 16

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: WD06050
Sample Number Sample ID
Matrix Date Sampled Date Received
001 Lincolnton Solid 04/06/2021 1045 04/06/2021
002 L 1-7 Solid 04/06/2021 1045 04/06/2021
003 L 1-7 Solid 04/06/2021 1045 04/06/2021
004 L 1-7 Solid 04/06/2021 1045 04/06/2021
005 L 1-7 Solid 04/06/2021 1045 04/06/2021
006 L 1-7 Solid 04/06/2021 1045 04/06/2021
007 L 1-7 Solid 04/06/2021 1045 04/06/2021
008 L 1-7 Solid 04/06/2021 1045 04/06/2021
(8 samples)
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Page 3 of 16

Inorganic non-metals
Client: Synagro
Description: Lincolnton
Date Sampled:04/06/2021 1045
Date Received:04/06/2021
Laboratory ID: WD06050-001
Matrix: Solid
% Solids: 4.53 04/06/2021 2311
Run Prep Method
1 350.1
1
1
1
1
1 351.4
Analytical Method
(Ammonia - N) 350.1
(Nitrate - N ) 9056A
(Nitrite - N ) 9056A
(Phosphorus) 365.1
(Soil pH meas) 9045D
(TKN) 351.2
Dilution
25
5
1
25
1
2
Analysis Date Analyst
04/07/20211206 KFE
04/08/2021 1249 AMR
04/08/2021 1017 AMR
04/12/2021 1614 DMA
04/07/20211915 NBW
04/09/20211731 MSG
Batch
88135
88521
88522
04/10/2021 1429 88601
88303
04/07/2021 1700 88277
Prep Date
Parameter
CAS Analytical
Number Method Result Q LOQ
DL
Units Run
Ammonia - N (gas diffusion)
Nitrate - N (soluble)
Nitrite - N (soluble)
Phosphorus
Soil pH measured in water @ 21.5 ° C
TKN
7723-14-0
350.1
9056A
9056A
365.1
9045D
351.2
12000
51
9.3
14000
6.8
34000
550
J 55
4.4
2800
290
11
2.2
550
1100 1100
mg/kg 1
mg/kg 1
mg/kg 1
mg/kg 1
su 1
mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
W = Reported on wet weight basis
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
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Page 4 of 16

CVAA
Client: Synagro Laboratory ID: WD06050-001
Description: Lincolnton Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 4.53 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method
1 7471B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
7471B 1 04/09/2021 1821 CMS2 04/09/2021 1308 88366
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Mercury
7439-97-6
7471B ND 1.6 0.39 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5of16

ICP-AES
Client:Synagro Laboratory ID:WD06050-001
Description: Lincolnton Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 4.53 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method
1 3050B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
6010D 1 04/08/2021 1402 JMH 04/07/2021 1012 88194
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
7429-90-5 6010D 11000 140 51 mg/kg 1
7440-38-2 6010D 4.5 J 5.1 1.7 mg/kg 1
7440-43-9 6010D ND 1.7 0.43 mg/kg 1
7440-70-2 6010D 5400 1700 210 mg/kg 1
7440-47-3 6010D 41 3.4 0.85 mg/kg 1
7440-50-8 6010D 230 3.4 1.5 mg/kg 1
7439-89-6 6010D 10000 34 15 mg/kg 1
7439-92-1 6010D 8.3 3.4 1.5 mg/kg 1
7439-95-4 6010D 2700 1700 210 mg/kg 1
7439-96-5 6010D 360 5.1 2.0 mg/kg 1
7439-98-7 6010D ND 14 3.4 mg/kg 1
7440-02-0 6010D 8.2 J 14 3.6 mg/kg 1
7440-09-7 6010D 4000 B 1700 210 mg/kg 1
7782-49-2 6010D ND 6.8 2.8 mg/kg 1
7440-23-5 6010D 1200 J 1700 210 mg/kg 1
7440-66-6 6010D 130 17 4.2 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 6 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-002
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.62 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 38123 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
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Page 7 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-003
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.23 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <44928 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 8 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-004
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.71 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 36877 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
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Page 9 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-005
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 3.09 04/08/2021 0019
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 64763 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 10 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-006
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.25 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 88774 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-007
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.88 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 104315 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
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Page 12 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-008
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.80 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 35747 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
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Page 13 of 16

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 16

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PACE ANALYTICAL SERVICES, LLC
Samples Re•-' Cbeckfl5t15RC)(1161E1I011RC.75J
Issufrtg rarity_ Pare ENV - WC.1
Sample ' Iceipt Checklist (SRC)
CFent: SYf ACRO Corticr In. ..ed I] Mate: JkC N1piv2C21
Means of receipt: O
Ton:a NC
�jYes! 11 Nu
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Pace. • ;lien' ■ UPS . Fedri • O he,;
. Were custcxly scaIs 7 - on the coyIcy'
+' ],IA 2, If custod sea15 were p ent were they intact and unbroken'?
I.a:4; WI] &fl
Revls d.9J29j
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Chlorine Skin 1 1 rvA Te;tctl by;
rigrn j temperature upon receipt "'Derived (C - teneperd[urc upor. receipt
1.4 ft.4 0c NA ° ' NA NA h• /NA Pc
h+Ic[I.Od: J f'eml;erat{ue Eluuik gain! Bottles Gun IL]:
Melhcd of c lrint: ❑ Wet ice ❑ .cc Packs 1 Dry foe • Nona
3. it (ern€,rrattue of any c ,0er exceeded 6.'C, wt,s Project Kinney!: uIifl J
PM was Notified t by: p[rine 1 email; face -to -fake (circle nn45).
No fiNI4 4. Is the commercial caur 's packing aRp artnehcd to this form?
94401id Snap -Cup ID; 21-443
IR Gun C:orrevtiois Fu ttor: a
S. Wc-cpro+e. custody p rucc1ures (°+elir;quis]tedfrectived) followed?
6- Vr'cre sample 11Ds listed dr. ttc COC?
Yes Olio 1. Wore sample ILls listed do all sample containers?
Yes 'No &- Was colleci inn date & t ii :istedo t orzC OC;?
9. Was cotied.ien date. l* 01iated on af: ample containers?
Yes i 4o JD. laid all cor-lair]er label riIforn]attcbl (iJA, c te, rime) a�r -ee wi[]t ;ttc COC?
Ycs _ No I I, Were tests 1 n l e perfoi µtik3.t listed on the COC?
Simple PteseryatIan
Samples) MA
12. laid ail samples arrive in the proper containers for cash test and/or iti weld condition
(a.nbrgken, lisis on, eto,)? y
1
l 3, Was adequate. sartiplo N hurie awailable? —
-4. Were a[: samples rouei e;1 within Yx !ye holding Cline ar4 ( boats, wL] hcvcr comes first?
15- Were any sfmpk i csont: 1ers n_issinfiexc s (circle 0n0) sain Icy Not listed on COC?
]6. Fa. VOA and 11S1C-17f 6ar-5ple_s, were bubbles 1]reseni.>"pea-size ('l"or 6rram in (11w/teter)
in any ut. is VOA vizIs?
17, Were all DRO.!]netalslnatrient saynp:cs received at a pH of 2?
[ - Were all cyanide samprns received at x pl I y 12 and Sulfdc samples received „i. p1.1 >
19. Were all applicable Nl TKNfcytnide/ cnu1 S7G 63 0Sirrvji) samples free o
1'35[dual e1I Corrine?
20- Were client remarks/ra tic9ts (i.e reyucsted thins, NISIMSD deei I1ations, ete,.,)
correctly transcribed from 11'4 COC Lino Inc cernmea]t section in Ltiv25?
21- Wass I.he 911ote ai umber 11od on tt;e Oontainer Iabc1? [f y'e Quote 4 'r+3
(Must be completed far any s.rilptc(s) iru urrcct:y prese!r- ed or with he dspaoe,)
in aaatnple ra'eivirig with NA
Time or preservetion r A
Sample(4)
IrL or circle one: H2
9?
j 5.1.T,972 received incorrectly p]o er d auc were adjusted do rdin3ly
]-11 OS, LIC1, NsOi-i u$.ing SR h. N.A.
. ErnaorD than one p struat�ve is neeadcd, please Date ]u ccrninenia be[gk ,
a_riptes(s) N
adjusted accordin Iy ir. sample receiving w'ih sodium
SR iaureate Jahelsapp]led by: n'a2
Corn]t]ents;
were receivers with bubbksfi rrtri in diameter.4vrr. rCCeived Deis#] TRC. -r�,5 ang/i. (1ffil9 is rtv j and were
osul ta;tc 'azS2O3) whit Shealy ID: A•
04.+65iaa l
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at 1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 16

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
Sample Date Report Range Ratio
2161-01-LIQ-NC LINCOLNTON, NC WWTP ANAEROB. DIGESTED 4/6/2021 4/1/2021 - 6/30/2021 0.7059
LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (1200 x 4.5300) = 100 = 54.36
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (5400 x 4.5300) = 100 = 244.62
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2700 x 4.5300) = 100 = 122.31
Na meq = Na mg/I = Molec.Wgt.Na = 54.36 = 23 = 2.36348
Ca meq = Ca mg/I = Molec.Wgt.Ca = 244.62 = 20 = 12.231
Mg meq = Mg mg/I = Molec.Wgt.Mg = 122.31 = 12 = 10.1925
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.36348 = SgrRoot[0.5(12.231+10.1925)] = 0.705854

PaceAnalytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Lincolnton
Lot Number:WG06038
Date Completed:07/16/2021
Project Manager:Lucas Odom
07/16/2021 5:10 PM
Approved and released by:
Project Manager II: Kathy E. Smith
A413
ANSI National Accreditation Board
ACCREDITED
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 16

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653
NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: WG06038
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 16

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: WG06038
Sample Number Sample ID
Matrix Date Sampled Date Received
001 Lincolnton Solid 07/06/20210945 07/06/2021
002 L 1 Solid 07/06/2021 0950 07/06/2021
003 L 2 Solid 07/06/2021 0950 07/06/2021
004 L 3 Solid 07/06/2021 0950 07/06/2021
005 L 4 Solid 07/06/2021 0950 07/06/2021
006 L 5 Solid 07/06/2021 0950 07/06/2021
007 L 6 Solid 07/06/2021 0950 07/06/2021
008 L 7 Solid 07/06/2021 0950 07/06/2021
(8 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of16

Inorganic non-metals
Client: Synagro
Description: Lincolnton
Date Sampled:07/06/2021 0945
Date Received:07/06/2021
Laboratory ID: WG06038-001
Matrix: Solid
% Solids: 2.80 07/07/2021 0008
Run Prep Method
1 350.1
1
1
1
1
1 351.4
Analytical Method
(Ammonia - N) 350.1
(Nitrate - N ) 9056A
(Nitrite - N ) 9056A
(Phosphorus) 365.1
(Soil pH meas) 9045D
(TKN) 351.2
Dilution Analysis Date Analyst Prep Date Batch
1 07/07/20211157 KFE 97967
1 07/14/2021 1043 AMR 98964
1 07/14/2021 1043 AMR 98966
5 07/08/2021 1357 DMA 07/07/2021 1615 98126
1 07/11/20211753 NBW 98501
1 07/09/2021 1227 DMA 07/07/2021 1535 98116
Parameter
CAS Analytical
Number Method
Result Q LOQ
DL
Units Run
Ammonia - N (gas diffusion)
Nitrate - N (soluble)
Nitrite - N (soluble)
Phosphorus
Soil pH measured in water @ 22.4 ° C
TKN
7723-14-0
350.1
9056A
9056A
365.1
9045D
351.2
1300 36
2100 18
8.0 7.2
7200 S 890
5.8
17000 S 1800
19
3.6
3.6
180
890
mg/kg 1
mg/kg 1
mg/kg 1
mg/kg 1
su 1
mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
W = Reported on wet weight basis
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 4 of 16

CVAA
Client: Synagro Laboratory ID: WG06038-001
Description: Lincolnton Matrix: Solid
Date Sampled:07/06/2021 0945 % Solids: 2.80 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method
1 7471B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
7471B 1 07/15/2021 1453 CMS2 07/14/2021 1532 98385
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Mercury
7439-97-6
7471B ND 2.8 0.68 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5of16

ICP-AES
Client: Synagro Laboratory ID: WG06038-001
Description: Lincolnton Matrix: Solid
Date Sampled:07/06/2021 0945 % Solids: 2.80 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method
1 3050B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
6010D 1 07/08/2021 1116 JMH 07/08/2021 0122 98017
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
7429-90-5 6010D 8800 240 89 mg/kg 1
7440-38-2 6010D 3.8 J 8.9 3.0 mg/kg 1
7440-43-9 6010D ND 3.0 0.74 mg/kg 1
7440-70-2 6010D 3800 3000 370 mg/kg 1
7440-47-3 6010D 29 5.9 1.5 mg/kg 1
7440-50-8 6010D 180 5.9 2.7 mg/kg 1
7439-89-6 6010D 6500 59 27 mg/kg 1
7439-92-1 6010D 5.0 J 5.9 2.7 mg/kg 1
7439-95-4 6010D 1500 J 3000 370 mg/kg 1
7439-96-5 6010D 230 8.9 3.5 mg/kg 1
7439-98-7 6010D ND 24 5.9 mg/kg 1
7440-02-0 6010D ND 24 6.2 mg/kg 1
7440-09-7 6010D 1900 J 3000 370 mg/kg 1
7782-49-2 6010D ND 12 4.8 mg/kg 1
7440-23-5 6010D 2200 J 3000 370 mg/kg 1
7440-66-6 6010D 87 30 7.4 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-002
Description: L 1 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 1.37 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 438597 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-003
Description: L 2 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 1.30 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 615195 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-004
Description: L 3 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 2.70 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 259269 * 20
col/g 1
Footnote(s): *Fecal Coliform (MF) - results estimated
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank
N = Recovery is out of criteria
W = Reported on wet weight basis
E = Quantitation of compound exceeded the calibration range DL = Detection Limit
P = The RPD between two GC columns exceeds 40%
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-005
Description: L 4 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 2.05 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 146384 * 20
col/g 1
Footnote(s): *Fecal Coliform (MF) - results estimated
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank
N = Recovery is out of criteria
W = Reported on wet weight basis
E = Quantitation of compound exceeded the calibration range DL = Detection Limit
P = The RPD between two GC columns exceeds 40%
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-006
Description: L 5 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 2.41 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 83108 * 20
col/g 1
Footnote(s): *Fecal Coliform (MF) - results estimated
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank
N = Recovery is out of criteria
W = Reported on wet weight basis
E = Quantitation of compound exceeded the calibration range DL = Detection Limit
P = The RPD between two GC columns exceeds 40%
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-007
Description: L 6 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 1.22 07/08/2021 0145
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 3161366 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-008
Description: L 7 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 1.62 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 5141111 * 20
col/g 1
Footnote(s): *Fecal Coliform (MF) - duplicates outside 25% RPD
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank
N = Recovery is out of criteria
W = Reported on wet weight basis
E = Quantitation of compound exceeded the calibration range DL = Detection Limit
P = The RPD between two GC columns exceeds 40%
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 16

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 16

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PACE ANALYTICAL SERVICES, LLC
SRr plcs Receipt cherkILst ( r cI IMiGb16G151 Reui;ed;9/29/2020
[ssul i Authorty_ Pace ENV -VI/COL Page 1 of 1
Sample Receipt Checklist (SRC)
COo.cr 1 IS.Metc3 h}Id Le: JS[ + 07.+frtr t7t l Lot 4; welf,6C38
Meant o>rreceip[; d �CIit ul [1PS t FeclFx Q Other:
Yc ' N 1. Wurc rtrs'odu seals present on the ceolcr?
Yet; . No !9 NA • if C i t i • seals �.se ,resen 1, were they intact and u nl_r alien?
pH Strip ID, N" Cislnrinr. Striwn r vrtr
p ID; Tested by:
O gi.uaJtemperatureupnrireetiptlDerived (Carr+ecirtI)tcmpelarit-cupoe;reozipr %SolidSJ,p-Cup ID: 21-i123
2 r /2.1 ac NA INA oc NA fNA <'C Mk 1Nfl DC
Method: FITemperature Blank r'i,s einst Bottles 1J Gun I! ; 5
Method of coolant: P w0[ ]ce LJ ice Pucks ❑ Dry Ice 0 NDri
El No A 3- Irtemperulurc atany c oieu ex L-uetled 6-0°C, was Projour l�vianagct Notilier]?
RNA ]'M was Nod Fled one l email i Fie -to -face (i irci w one.),
C••-' �Y� Ph
I� ` eo LI Nc Q NA 4. Is no eummu-dal anurirr'^ packing slip artathieJ to it ILA
Yes
1 Yes
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Yes r] No
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5. Were proper custody prpCcdkres (ran qu ishedirceei Riad) followed
6. Were sa_'npie IDa listed on the COC?
7. Were sample IDs listed on ,e11 ample centa[ncrt?
S- Wa., aatiectior. date. , time fisted on the CC)C?
9- Wus callectictt date $ time listed on all semplc soar i1i ?
10- Did all e:un [miner [abol mfarrnutFon (ID, d#tc, them) u with the COC?
[ I . Were te;l5 to be p fonned listed on the COCY
12, old a]1 samp[ts arrive in the :roper containers for each. cat an -?or in good Onidilion
(unbroken, lids an,.e,c)7
LI N I5-'Note a,iY xartrles containers e-rssingWeacess (circle one) sample. Nut listed on CDC?
❑ No d , 16. Fcr VOA and RSK-] 75 samples., weN bubbles present :x"pca.ize" (V°'Qr 6]t1n in diameter)
eei any of the VOA yids?
❑?' d NA i7. Were all DRO/mculls/nutrient snmp14sreceivdatapHofC2?
Jo NA II Were Al cvanida earn Its received at a pE ! > 12 and s;u! [ids sam ples recaved at a e H > 9?
❑
l , lk'erc Il applicubie HaITX.Nicyani p enoliG S.I,',pS.3 ( 0-S;n L)samp_ur Jreti or No lY.�l t'esicual ehlprim'?
No LINA 20. Were Client re,rierksfrcgLasls (i.e. requested dilutions. MS MSD designations, eic.,,)
correctlytrAnscrilaed from the COC into [hc aorattte:ttsectinn in LAMS?
❑ Yes
Yet;
No
I:;. W S adequate sample volume. aveilahla'?
1 . 1'fere ail sarr,ples rrxrivad xithin i!3 IJ,c JJaldin limo at 43 hours, wtikchcnr corn LIS first?
21, was the quo1c number ]fate/ on. [lee Lnntainer IibcI? ff es, { uoce tar,
Saniplo P enervation (Must be compeer f r uny sampele..(s) utaorrictty preserved o r tiv i tl-. h cadspatc.)
Samples) NA were received incorrectly preAe:nved ariel ware adjusimi accord,inglw
in sultnpie receiving with NA _in)s otcircle i'ne.; H2304, HNU3, HCI, NaOH using SR g NA
Tim[ of> a ervulion N^ . ifmore tFi - one •ativeisneeded,please min ir_ theournments below.
� PLe(s)
nplc s) were received with TRC - 0. mrL+[,(If ir.
[9 i rr ) and w-e
adjusted uuu,rdirigly in samp]r rocs;wii_g with sod film thiosulfatc (Na,£2O.) wi�llSacab. Tr)- r�i1'1
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were reecitied with b ibbl,6 ram in diameter.
SR. l7rL-code Iabc[s applied by: -5410
CCirttments:
Dom. 07A0(}+1J2.J
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 16

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
Sample Date Report Range Ratio
2161-01-LIQ-NC LINCOLNTON, NC WWTP ANAEROB. DIGESTED 7/6/2021 7/1/2021 - 10/31/2021 1.2754
LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (2200 x 2.8000) = 100 = 61.6
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (3800 x 2.8000) = 100 = 106.4
Mg mg/I = (mg mg/kg x % Solids) = 100 = (1500 x 2.8000) = 100 = 42
Na meq = Na mg/I = Molec.Wgt.Na = 61.6 = 23 = 2.67826
Ca meq = Ca mg/I = Molec.Wgt.Ca = 106.4 = 20 = 5.32
Mg meq = Mg mg/I = Molec.Wgt.Mg = 42 = 12 = 3.5
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.67826 = SgrRoot[0.5(5.32+3.5)] = 1.27536

PaceAnalytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Lincolnton
Lot Number:WK02050
Date Completed:11/21/2021
11/22/2021 11:20 AM
Approved and released by:
Project Manager II: Lucas Odom
A413
ANSI National Accreditation Board
ACCREDITED
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 16

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653
NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: WK02050
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, the following sample has an initial weight that is 3x greater than standard
procedure: WK02050-001. The LOQ has been changed to reflect the additional mass.
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Page 2 of 16

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: WK02050
Sample Number Sample ID
Matrix Date Sampled Date Received
001 Lincolnton Solid 11/02/2021 0915 11/02/2021
002 L-1-7 Solid 11/02/2021 0915 11/02/2021
003 L-1-7 Solid 11/02/2021 0915 11/02/2021
004 L-1-7 Solid 11/02/2021 0915 11/02/2021
005 L-1-7 Solid 11/02/2021 0915 11/02/2021
006 L-1-7 Solid 11/02/2021 0915 11/02/2021
007 L-1-7 Solid 11/02/2021 0915 11/02/2021
008 L-1-7 Solid 11/02/2021 0915 11/02/2021
(8 samples)
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Page 3 of 16

Inorganic non-metals
Client: Synagro
Description: Lincolnton
Date Sampled:11/02/2021 0915
Date Received:11/02/2021
Laboratory ID: WK02050-001
Matrix: Solid
% Solids: 4.20 11/03/2021 0152
Run Prep Method
1 350.1
1
1
1
1
1 351.4
Analytical Method
(Ammonia - N) 350.1
(Nitrate - N ) 9056A
(Nitrite - N ) 9056A
(Phosphorus) 365.1
(Soil pH meas) 9045D
(TKN) 351.2
Dilution
25
1
1
25
1
2
Analysis Date Analyst
11/20/20212008 DRD
11/10/2021 1053 AMR
11/10/2021 1053 AMR
11/04/20211717 DMA
11/07/20211728 NBW
11/05/20211227 DMA
Batch
22997
22147
22153
11/04/2021 1019 21253
21588
11/04/2021 1312 21269
Prep Date
Parameter
CAS Analytical
Number Method
Result Q LOQ
DL
Units Run
Ammonia - N (gas diffusion)
Nitrate - N (soluble)
Nitrite - N (soluble)
Phosphorus
Soil pH measured in water @ 20.8 ° C
TKN
7723-14-0
350.1
9056A
9056A
365.1
9045D
351.2
18000
43
5.5
16000
7.3
42000
600
12
4.8
3000
310
2.4
2.4
600
S 2400 1200
mg/kg 1
mg/kg 1
mg/kg 1
mg/kg 1
su 1
mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
W = Reported on wet weight basis
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
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Page 4 of 16

CVAA
Client: Synagro Laboratory ID: WK02050-001
Description: Lincolnton Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 4.20 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method
1 7471B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
7471B 1 11/16/2021 1644 JAB2 11/15/2021 1536 22152
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Mercury
7439-97-6
7471B ND 1.9 0.46 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5of16

ICP-AES
Client: Synagro Laboratory ID: WK02050-001
Description: Lincolnton Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 4.20 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method
1 3050B
2 3050B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
6010D 1 11/04/2021 1339 JMH 11/04/2021 0126 21089
6010D 1 11/05/2021 1752 KSH2 11/04/2021 0126 21089
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
7429-90-5 6010D 12000 150 58 mg/kg 1
7440-38-2 6010D 4.7 J 5.8 1.9 mg/kg 1
7440-43-9 6010D 0.77 J 1.9 0.49 mg/kg 1
7440-70-2 6010D 8900 1900 240 mg/kg 1
7440-47-3 6010D 110 3.9 0.97 mg/kg 1
7440-50-8 6010D 280 3.9 1.7 mg/kg 1
7439-89-6 6010D 11000 39 18 mg/kg 1
7439-92-1 6010D 15 3.9 1.7 mg/kg 1
7439-95-4 6010D 2900 1900 240 mg/kg 1
7439-96-5 6010D 260 5.8 2.3 mg/kg 1
7439-98-7 6010D 5.5 J 15 3.9 mg/kg 1
7440-02-0 6010D 12 J 15 4.1 mg/kg 1
7440-09-7 6010D 3000 1900 240 mg/kg 2
7782-49-2 6010D 3.8 J 7.7 3.1 mg/kg 1
7440-23-5 6010D 1000 J 1900 240 mg/kg 1
7440-66-6 6010D 270 19 4.8 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-002
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 6.94 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <15553 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-003
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 5.68 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <14402 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-004
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 7.18 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <17595 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-005
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 6.80 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <13927 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-006
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 7.56 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <14704 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-007
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 6.31 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <13219 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 12 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-008
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 6.43 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <15860 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
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Page 13 of 16

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 16

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PACE ANALYTICAL SERVICES, LLC
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Samples Receipt Cheddist (SRCI IMEMISC-15)
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SR Esxrcode labels applied lr}' -IF.. Date: ] 1(17Z202]
Cumin `ILts:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 16

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
Sample Date Report Range Ratio
2161-01-LIQ-NC LINCOLNTON, NC WWTP ANAEROB. DIGESTED
LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (1000 x 4.2000) = 100 = 42
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (8900 x 4.2000) = 100 = 373.8
Mg mg/I = (mg mg/kg x % Solids) = 100 = (2900 x 4.2000) = 100 = 121.8
Na meq = Na mg/I = Molec.Wgt.Na = 42 = 23 = 1.82609
Ca meq = Ca mg/I = Molec.Wgt.Ca = 373.8 = 20 = 18.69
Mg meq = Mgmg/I=Molec.Wgt.Mg=121.8=12=10.15
11/2/2021 11 /1 /2021 -
12/31 /2021
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.82609 = SgrRoot[0.5(18.69+10.15)] = 0.480882
0.4809

SECTION 3

FACILITY NAME LINCOLNTON, NC
LAND OWNER: MIKE DAVIS
OPERATOR: MIKE DAVIS
CROP 1 NAME SOYBEANS (SB)
RESIDUAL SOURCE(S):' See list at bottom of report
Gallons (G)
or Cubic Yards (Y)
Date or or Wet Tons (W)
Month
5/26/2021
5/27/2021
May-21
86,800.00
142,600.00
229,400.00
UOM
(G)
(G)
(G)
Solids
4.530
4.530
Dry Tons/Ac
0.911
1.497
Total 2.408
Annual lbs/acre Applied
[Cumulative Ibs/acre Applied
Permit PAN Limit (Ibs/acre)
Federal C.P.L.R. (lbs/acre)'*"
AS
0.022
0.085
LIL = LINCOLNTON, NC W WTP ANAEROB, DIGESTED LIQUID
"l certify, under penalty of law,
aware that there are significant
0.000
SB
5B
ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
WQ PERMIT 5: W00002712
ANNUAL DRY TONS APPLIED: 43.33
PREDOMINANT SOIL SERIES: CECIL
CROP 1 MAX. PAN: 185
Residual
Source
LIL
LIL
D CU
0.002
0.015
0
1.812
Site
Cand,
Dry, Wel,
Moist
DRY
DRY
CR
Precip
Past 24 Hrs.
Inches
"0-K112"
"0-41/2"
P
Application
Method'
SUR
SUR
HG
Volati-
lization
Rate**
0.5
0.5
MO
FIELD#: NC-CA-00046.0-0010- ACRES UTILIZED: 18.0
SITE #: NC CA 00048 ACRES PERMITTED: 18.0
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 NAME: CROP 2 MAX, PAN:
Mineral-
ization
Rate***
0.20
0.20
NI
TKN
mg/kg
34,000.00
34,000.00
0
0.335
0.040
D.078
0.002
0.004
SE
Ammonia
Nitrogen
mg/kg
2,000.00
2,000.00
Nitrate
and Nitrite
mg/kg
PAN Applied
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
ZN
60.30
60.30
19.068
31,325
Total 50.
P
67.446
ris document wa epared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
Ise information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER
NR = Not Reported or Not Required
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Printed: 2/2/2022
DATE
Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
C.P.L.R.: Cumulative Pollutant Loading Rale
See Site pH & Lime Application Records Section of Report
DENR FORM FSF (12/2006)
Amount

FACILITY NAME: LINCOLNTON, NC
LAND OWNER: CHUCK WATERS
OPERATOR: CHUCK WATERS
CROP 1 NAME FESCUE HAY (FSH)
RESIDUAL SOURCE(S): • See list et bottom of report
Gallons (G)
or Cubic Yards (Y)
Date or or Wet Tons (W)
Month Amount UOM Solids Dry Tons/Ac
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
W Q PERMIT #: W 00002712
ANNUAL DRY TONS APPLIED: 66.28
PREDOMINANT SOIL SERIES: LLOYD
CROP 1 MAX. PAN: 216
5/3D/2021 55,800.00
Jun-21 55,800.00
(G)
(G)
4.530 0,252
7/1/2021 161,200.00 (G) 2.800 0.450
7/6/2021 179,800.00 (G) 2.800 0.502
7/7/2021 136,400.00 (G) 2.800 0.381
Jul-21 477,400.00 (G)
FIELD#: NC-LT-00019-0-0001- ACRES UTILIZED: 41,5
SITE #: NC LT 00019 ACRES PERMITTED: 41,8
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 NAME: CROP 2 MAX, PAN:
Site
Cond. Precip Volall- Mineral -
Residual Dry, Wet, Past 24 Hrs. Application Itzation ization
Source Moist Inches Method* Rate*' Rate"**
LIL DRY "0-<1/2" SUR 0.5 0.20
Page:1
TKN
mg/kg
4,000.00
LIL DRY "0-<1/2" SUR 0.5 0.20
LIL DRY '0-<1/2" SUR 0.5 0.20
LIL DRY "3-<1/2' SUR 0.5 0,20
Total 1.585
AS
Annual Ibs/acre Applied 0.012
CD CU CR
0.002 0.596 ( 0.098
Cumulative Ibs/acre Applied 0.229 0.081
[Permit PAN Limit (Ib
[Federal C.P.L.R. (Ibs/acre)**** 36.6 34.
LIL = LINCOLNTON, NC W WTP ANAEROB. DIGESTED LIQUID
"I certify, under penalty of law, that t
aware that (here are significant penal
16.772
17,000.00
17,000.00
17,000.00
Name of Crop Type
Ammonia Nitrate PAN Applied Receiving Residual
Nitrogen and Nitrite (Ibs/acre) Application
mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
2,000.00 60.30 5.276 FSH
,300.00 2,108.00 5.312 FSH
,300.00 2,105.00 5.924 FSH
,300,00 2,108,00 4.494 FSH
0.018 0.002 0.017
0.497 I 1.076
Total 21.006 0.000
26.253
216
e Applied
ument was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted, Tam
submi'ia'TSyr information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER
NR = Not Reported or Not Required
Application Method: SUR • Surface, INJ - Injection, SURIN - Incorporation
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Printed: 2/2/2022
DATE
Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
C.P.L.R.: Cumulative Pollutant Loading Rate
See Site pH d Lime Application Records Section of Report
DENR FORM FSF (12/2006)

FACILITY NAME: LINCOLNTON, NC
LAND OWNER: CHUCK WATERS
OPERATOR: CHUCK WATERS
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): • See list et bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT it: WQ0002712 FIELD#: NC-LT-00019-0-0002-
ANNUAL DRY TONS APPLIED:44.51 SITE #: NC LT 00019
PREDOMINANT SOIL SERIES: LLOYD
CROP 1 MAX. PAN: 216
CROP 2 NAME:
Date or
Month
4/1 212021
4/13/2021
4/14/2021
Apr•21
Gallons (G)
or Cubic Yards (Y)
or Wet Tons (W)
Amount
6,200.00
204,600.00
24,800.00
235,600.00
UOM
(G)
(G)
(G)
(G)
Solids
4.530
4.530
4.530
Annual Iles/
cre Applied
Dry Tons/Ac
0.092
3.043
0.369
Residual
Source
LIL
LIL
Total 3.504
'Cumulative Ibslacre Applied 0.
'Permit PAN Limit (Ibs/acre)
Site
Cond.
ry, Wet,
Moist
DRY
DRY
DRY
CR
Precip
Past 24 Hrs.
Inches
"0-<1/2"
"0-<112"
PB
Application
Method'
SUR
SUR
SUR
HG
Volati-
zalion
Rate""
TKN
mg/kg
0llneral-
ization
Rate""
0.20
0,20
0.20
Page: 1
ACRES UTILIZED: 12.7
ACRES PERMITTED: 12.7
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Name of Crop Type
Ammonia Nitrate PAN Applied Receiving Residual
Nitrogen and Nitrite (Ibslacre) Application
mg/kg mglkg Crop 1 �.. � Crop 1 Cray
34,000,00 12,000.00 60.30 1.929
34,000.00 12,000.00 60.30 63.66E
34,000.00 12,000.00 60.30 7.717
2 0.003 1.612 0.287 0.058 0.003 0.024 0.057 0.020
'Federal C.P.L.R. (Ibslacre)""" 36.6
LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID
"I certify, under penalty of law, that tf, s document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information. submitted, I am
Tata
98.121
73.312 0.000
FSH
FSH
FSH
Applied
b5/Ac
aware that there are significant penal
br su alse infomlatiou, including the possibility of Ones and imprisonment for knowing violations."
7'4". Z
SIGNATURE OF LAND APPLIER
NR = Not Reported or Not Required
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Printed: 2/2/2022
DATE
Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerob
C.P.L.R.: Cumulative Pollutant Loading Rate
See Site pH & Lime Application Records Section of Report
y digested-0.3, Raw Sludge-0.4
DENR FORM FSF (12/2006)

FACILITY NAME: LINCOLNTON, NC
LAND OWNER: CHUCK WATERS
OPERATOR: CHUCK WATERS
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): • See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: W00002712 FIELD#: NC-LT-00019-0-0003-
ANNUAL DRY TONS APPLIED: 44.51 SITE #: NC LT 00019
PREDOMINANT SOIL SERIES: RIVERVIEW LOAM
CROP 1 MAX, PAN: 198 CROP 2 NAME:
Gallons (G)
or Cubic Yards (Y)
Date or or Wet Tons (W)
Month Amount UOM Solids Dry Tons/Ac
6/29/2021
6/33/2021
Jun-21
124,000.00
111,600.00
235,000.00
Annual Ibs/acre Applied
umulative Ibs/acre Applied
Permit PAN Limit (Ibs/acre)
(G)
(G)
(G)
4.530
4.530
1.775
Cond.
Residual Dry, Wet,
Source Moist
LIL
1.597 LIL
Total 3.372
LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID
DRY
DRY
Precip
Past 24 Hrs
Inches
"0-<1/2"
"0-<112"
Application
Method*
SUR
SUR
Volati-
lization
Rate*"
0.5
Mineral-
ization
Rate***
0.20
0.20
TKN
mg/kg
34,000.00
34,000,00
ACRES UTILIZED: 13.2
ACRES PERMITTED: 13.2
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Name of Crop Type
Ammonia Nitrate PAN Applied Receiving Residual
Nitrogen and Nitrite (Ibs/acre) Application
mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
12,000.00 60.30 37,124 FSH
12,000.00 60.30 33.412 FSH
Total 70.536 0.000
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I a
aware that there are significant penelti or submtttin also information, including the possibility of fines and imprisonment for knowing violations,"
2
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required "' Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C,P.L,R.: Cumulative Pollutant Loading Rate
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ****" See Site pH 8 Lime Application Records Section of Report
Printed: 2/2/2022
DENR FORM FSF (12/2006)

FACILITY NAME: LINCOLNTON, NC
LAND OWNER: ANGELA UNDERFELT
OPERATOR: ANGELA LINGERFELT
CROP 1 NAME: WHEAT (WH)
RESIDUAL SOURCE(S): • See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT#: WOD002712
ANNUAL DRY TONS APPLIED: 27.46
PREDOMINANT SOIL SERIES: CECIL
CROP 1 MAX. PAN: 115
FIELD#: NC-LT-00036-0-0003-
SITE #: NC LT 00035
CROP 2 NAME:
ACRES UTILIZED: 8.6
ACRES PERMITTED: 8.6
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX, PAN:
Page: 1
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volali-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
Iization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount.
UOM
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate"'
mg/kg
mg/kg
mg/kg
Crop 1
Crop 2
Grop 1
Crop 2
1/2D/2021
12,400.00
(G)
5.590
D.
LIL
DRY
"0.41/2"
SUR
0.5
0.20
45,000,00
11,000,00
79,7D
8.725
WH
1/21/2021
49,600.00
(G)
5.590
1.344
LIL
DRY
"0-41/2"
SUR
0.5
0.20
48,000.00
11,000.00
79.70
34.900
WH
1/22/2021
55,500.00
(G)
5.590
1.512
LIL
DRY
"0-n1/2"
SUR
0.5
0.20
48,000.00
11,000.00
79.70
39.263
WH
Jan•21
117,800.00
(G)
Total 3.192
ulative Ibs/acre Applied
Permit PAN Limit (Ibs/acre) 1st Crop(•
'Federal C.P.L.R. (Ibs/acre)**** 35.6
LIL = LINCOLNTON, NC W WTP ANAEROB, DIGESTED LIQUID
89.0
Total
02,B813 0.000
"I certify, under penalty of law, tho this document was prepared under my direction or supervision in accordance with o system designed to assure that quaffed personnel properly gathered and evaluated the information submitted. I am
aware that there arc significant pese information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER
NR = Not Reported or Not Required
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation
Volatilization Rate: Surface 0.5, Injection/Incorporation 1,0
Printed: 2/2/2022
DATE
Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically dlgested-0
C.P.L.R. : Cumulative Pollutant Loading Rate
See Site pH & Lime Application Records Section of Report
Raw Sludge-0.4
DENR FORM FSF (12/2006)

FACILITY NAME: LINCOLNTON, NC
LAND OWNER: ANGELA LEATHERMAN
OPERATOR: ANGELA LINGERFELT
CROP 1 NAME: CORN SILAGE (CSI)
RESIDUAL SOURCE(5):See list at bottom of report
Gallons (G)
or Cubic Yards (Y)
Dale or or Wel Tons (W)
Month Amount UOO
/21/2021 111,600.00 (G)
/22/2021 117,800.00 (G)
Jan-21 229,400.00 (G)
Annual lbs/acre Applied
Cumulative Ibslacre Applied
Solids
5.590
5.590
Dry Tons/Ac
1.927
2.034
Total 3.96
ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
WQ PERMIT #: WQD002712 FIELD#: NC-LT-00036-0-0005-
ANNUAL DRY TONS APPLIED: 53.47 SITE #: NC LT 00036
PREDOMINANT SOIL SERIES: CECIL
CROP 1 MAX. PAN: 238
Residual
Source
LIL
Cond.
Dry, Wet
Moist
DRY
DRY
Precip
Past 24 Hrs.
Inches
Application
Method*
Volati-
zation
Rate**
ACRES UTILIZED: 13.5
ACRES PERMITTED: 13.5
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 NAME: CROP 2 MAX. PAN:
Mineral-
zation
Rate""
Name of Crop Type
Ammonia Nitrate PAN Applied Receiving Residual
TKN Nitrogen and Nitrite (Ibslacre) Application
mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
0-<1/2
"0-<1/2"
SUR
SUR
0.5
0.5
0.20
0.20
48,000.00 11,000.00 79.70 50,023 CS
48,000.00 11,000.00 79.70 52.802 CSI
Total 102.825 0.000
Permit PAN Limit (lbs/acre
p[
'Federal C.P.L.R. (Ibslacre)
LIL = LINCOLNTON, NC WWTP ANAEROB. DIGESTED LIQUID
238
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that gratified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penAtfs for subm' false information, including the possibility of fines and imprisonment for knowing violations"
SIGNATURE OF LAND APPLIER
NR = Not Reported or Not Required
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Printed: 2/2/2022
2-k-zz
DATE
Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
C.P.L.R. : Cumulative Pollutant Loading Rate
See Site pH & Lime Application Records Section of Report
DENR FORM FSF (12/2006)

FACILITY NAME: LINCOLNTON, NC
LAND OWNER: RANDY LEATHERMAN
OPERATOR; RANDY LEATHERMAN
CROP 1 NAME: SOYBEANS (SB)
RESIDUAL SOURCE(S):' See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT#; W00002712 FIELD#: NC-LT-00047-0-0002-
ANNUAL DRY TONS APPLIED: 39.82 SITE #; NC LT 00047
PREDOMINANT SOIL SERIES; CECIL
CROP 1 MAX, PAN: 185
Gallons (G)
or Cubic Yards (Y)
Date or or Wet Tons(W)
Month Amount UOI
Solid
5/25/2021
5/26/2021
May-21
136,400.00
74,400.00
210,800.00
(G)
(G)
(G)
Annual lbs/acre Applie
Cumulalve lbs/acre Applied
Permit PAN Limit (lbs/acre)
Federal C.P.L.R.(lbs/acre)
LIL = LINCOLNTON, NC W
4.530
4,530
Tote
Dry TonslAc
0,748
0.408
56
AS ( CD
0.010 <0.001
36.6
TP ANAEROB. DIGESTED LIQUID
Residual
Source
LIL
LIL
0.532
Site
Cond. Precip
Dry, Wet, Past 24 Hrs
Moist Inches
DRY "0-<1/2„
DRY "0-<1/2"
Application
Volali-
Ilzation
Rate"
CROP 2 NAME;
camera/
ization
Ratee'
TKN
mg/kg
SUR
SUR
0.5
0.5
0,20
0.20
34,000.00
34,000.00
Page: 1
ACRES UTILIZED; 34.5
ACRES PERMITTED: 34.5
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Name of Crop Type
Ammonia Nitrate PAN Applied Receiving Residual
Nitrogen and Nllrite (lbs/acre) Application
mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
12,000.00 60.30 15.643 SB
12,000.00 60.39 6.532 SB
0.095
D.019
0.057
<0.001
O
0.008
NI
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qua
aware that there are significant per lfes for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER
NR = Not Reported or Not Required
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Printed: 2/2/2022
SE
0.006
Total 24.175 0.000
185
Lime Applied
Date
Lbs/Ac
ed personnel properly gathered and evaluated the information submitted. 1 am
DATE
Mineralization Rates: Compost-0.1, Anaeroblcally digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
C.P.L.R.: Cumulative Pollutant Loading Rate
See Site pH & Lime Application Records Section of Report
DENR FORM FSF (12/2006)

FACILITY NAME: LINCOLNTON, NC
LAND OWNER: FLORENCE CRIMAN
OPERATOR: RANDY LEATHERMAN
CROP 1 NAME: CORN SILAGE (CSI)
RESIDUAL SOURCE(S):See list al bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT k: W00002712 FIELDS: NC-LT-00047-0-0004-
SITE Si NC LT 00047
ANNUAL DRY TONS APPLIED: 147.48
PREDOMINANT SOIL SERIES: CECIL
CROP 1 MAX. PAN: 238
Gallons (G) Site
or Cubic Yards (Y) Cond. Precip
Dale or or W el Tons (W) % Residual Dry, Wet, Past 24 Hrs, Application
Month Amount UOM Solids Dry Tons/Ac Source Moist Inches Method'
3/12/2021 74,400.00 (G) 5.590 0.555 ._.._ LIL D' "0-a1/2" SUR
3M 3/2021 217,000.00 (G) 5.590 1.620 LIL D' "0-<1/2" SUR
3/15/2021 192,200.00 (G) 5.590 1.435 LIL D' "0-<1/2" SUR
Mar-21 483,600.00 (G)
10/14/2021 80,600.00 (G) 2.800 0.301 LIL
10/15/2021 148,800.00 (G) 2.800 0,556 LIL
10/18/2021 68,200.00 (G) 2.800 0.255 LIL
Oct-21 297,600,00 (0)
Total
4.722
Annual lbs/acre Applied
AS
0.058
CD
0.005
Cumulative Ibs/acre Applied
Permit PAN Limit (Ibs/acre)
Federal
C.P.L.R. (Ibs/acre)
0.088 ( 0.008 ( 2.
= LINCOLNTON, NC W WTP ANAEROB. DIGESTED LIQUID
DRY
DRY
DRY
"0-<1/2"
"0-<1l2"
SUR
SUR
SUR
0.712 ( 0.142 0.007
Volati-
lization
Rate**
0,5
0.5
0.5
0.5
0.5
0.5
CROP 2 NAME: WHEAT (WH)
neral-
tion
Rate**
0.20
0.20
0.20
0.20
0.20
0.20
TKN
mg/kg
48,000.00
48,000.00
48,000.00
17,000.00
17,000,00
17,000.00
Ammonia
Nitrogen
mg/kg
1,000.00
1,000.00
1,000.00
1,300.00
1,300.00
1,300.00
ACRES UTILIZED: 31.2
ACRES PERMITTED: 31.2
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX, PAN: 50
Nitrate
nd Nitrite
mg/kg
79.70
79.70
79.70
PAN Applied
(Ibs/acre)
Crop 2
Page: 1
Name of Crop Type
Receiving Residual
Application
Crop
Crop 2
2,108.00
2,108.00
2,108.00
Total
4.41
42.047
37.241
93.704 13.125
238
50
CS
CSI
CSI
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
aware that there are significant penult'? 1 submitting fat information, including the possibility of fines and imprisonment for knowing violations."
- ZZ
IGNATURE OF LAND APPLIER
NR = Not Reported or Not Required
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation
Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Printed: 2/2/2022
DATE
Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
C.P.L.R.: Cumulative Pollutant Loading Rate
See Site pH & Lime Application Records Section of Report
DENR FORM FSF (12/2006)
Lbs/Ac

FACILITY NAME: LINCOLNTON, NC
LAND OWNER: SUE GILBERT
OPERATOR: RANDY LEATHERMAN
CROP 1 NAME FESCUE HAY (FSH)
RESIDUAL SOURCE(S):' See list at bottom of report
Gallons (G)
or Cubic Yards (Y)
Date or or Wet Tons (W)
Month Amount
Solids
Tons/Ac
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT 8: W00002712 FIELD/4: NC-LT-00047-0-0005-
ANNUAL DRY TONS APPLIED: 39.09 SITE 0: NC LT D0047
PREDOMINANT SOIL SERIES: CECIL
CROP 1 MAX. PAN: 209 CROP 2 NAME:
Residual
Source
12/28/2021
12/29/2021
Dec-21
124,000.00
99,200.00
223,200.00
(G)
(G)
(G)
4.200
4.200
0.787
0.630
LI
LIL
Site
Cond. Precip
Dry, Wel, Past 24 H
Moist Inches
Application
Method*
Volati-
lization
Rate**
Mineral-
zation
Rate**
TKN
mg/kg
Page: 1
ACRES UTILIZED: 27.6
ACRES PERMITTED: 27.6
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Name of Crop Type
Ammonia Nitrate PAN Applied Receiving Residual
Nitrogen and Nitrite (Ibs/acre) Application
mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
DRY
DRY
0-<1/2
"0,1/2"
SUR
SUR
Total 1.417
nuai Ibs/acre Applied
AS CO CU OR PB
D.013
0.002
0,793
0.043
HG
0.001
0.5
0.5
0.20
0.20
42,000.00
42,000,00
18,000,00
18,000.00
48.50
48.50
21.802
7.44
0
0.016
N
0.034
E
0.011
ZN
0.765
FSH
FSH
Total 39.243 0.000
P
45.340
Cumulative Ibs/acre Applied
Permit PAN Limit Ohs/acre) let Cropi
Federal C.P,L.R, (Ibs/acre)""
0.038
0.005
2.025
0.567 i 0.106
0.004
0.041
0.097 I 0.046
1.933
209
.6
LIL = LINCOLNTON, NC W WTP ANAEROB. DIGESTED LIQUID
ate
Applied
"1 certify, under penalty of law, that ll''s document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the informalou Submitted.
aware that there are significant penal t s�gorssub e infomhation, including the possibility of fines and imprisonment
for knowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation
Volatilization Rate: Surface 0.5, Infection/Incorporation 1.0
Printed: 2/3/2022
tttt
Mineralization Rates: Compost-0.1, Anaerobically digested-0,2, Aerobically digested-0.3, Raw Sludge-0.4
C.P.L.R.: Cumulative Pollutant Loading Rate
See Site pH & Lime Application Records Section of Report
DENR FORM FSF (12/2006)
b
Ac

FACILITY NAME: LINCOLNTON, NC
LAND OWNER: MICHAEL N TERESA WESSON
ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
WO PERMIT #: WQ0002712 FIELD#: NC-LT-00049-0-0001-
ANNUAL DRY TONS APPLIED: 57.09 SITE F: NC LT 00049
OPERATOR: MICHAEL N TERESA WESSON PREDOMINANT SOIL SERIES: CECIL
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): See list al bottom of report
CROP 1 MAX. PAN: 209 CROP 2 NAME:
Date or
Month
1/23/2021
Jan-21
4/8/2021
4/9/2021
Apr-21
Gallons (G)
or Cubic Yards (Y)
or Wet Tons (W)
Amount
UO
Solids
Dry Tons/Ac
Residual
Source
Site
Cond, Precip
Dry, Wet, Past 24 Hrs, Application
Moist Inches Method"
Volati-
I ion
Rate*
99,200.00
99,200.00
155,000.00
24,800.00
179,800.00
(G)
(G)
(G)
(G)
(G)
0
4.
4.530
, .
Annual lbstacte Applied
1.570
1,999
0.318
Total 3.876
AS
0.042
[Permit PAN Limit (lbs/acre) 1st crop)
Federal C.P.L.R. (Ms/ave)""'
LIL = LINCOLNTON, NC WVVTP ANAEROB, DIGESTED LIQUID
CD
0,003
LIL
LIL
DRY
DRY
DRY
CU
.7
R
0,36
"0-< 2"
"D,1/2"
PB
SUR
UR
SUR
0,076 0.00
0.
MO
0.0 6
Mineral- Ammonia
ization TKN Nitrogen
Rate""" mg/kg mg/kg
0,20 49,000.00 11,000.00
ACRES UTILIZED: 14.7
ACRES PERMITTED: 14.7
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Nitrate
and Nitrite
mg/kg
Name of Crop Type
PAN Applied Receiving Residual
(lbs/acre) Application
79.70
Crop 1
40.752
Crop 2
Crop 1
Crop 2
FSH
0.20 1 34,000.00
0.20
34,000.00
12,000.00
12,000.00
60.30
6D.30
41.585
6.654
0 076 0.026
FSH
FSH
Total 88.991 0.000
ZN
.384
99.099
Lime Applied
"1 certify, under penalty of law, that this document was prepared under iny direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penaltiespenaIties,'submittos,joLsenfonriation, including the possibility of tines and imprisonment for }mowing violations."
1-401
SIGNATURE OF LAND APPLIER
NR = Not Reported or Not Required
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation
Volatilization Rale: Surface 0.5, Injection/Incorporation 1.0
Printed: 2/7/2022
72_
DATE
Mineralization Rates: Compost-0.1, Anaerobically dlgested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
C.P.L.R. : Cumulative Pollutant Loading Rate
See Site pH & Lime Application Records Section of Report
DENR FORM ESE (12/2006)

FACILITY NAME: LINCOLNTON, NC
LAND OWNER: MICHAEL N TERESA WESSON
OPERATOR: MICHAEL N TERESA WESSON
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): • See list el bottom of report
Gallons (G)
or Cubic Yards (Y)
Date or or We( Tons (W)
Month Amount UO
Solids
Dry Tons/Ac
ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
WQ PERMIT#: W00002712
ANNUAL DRY TONS APPLIED: 72.61
PREDOMINANT SOIL SERIES: CECIL
CROP 1 MAX. PAN: 157
Residual
Source
Site
Cond.
Dry, Wet,
Moist
Precip
Past 24 Hrs.
Inches
FIELD#: NC-LT-00049-0-0002-
SITE #: NC LT 00049
CROP 2 NAME:
ACRES UTILIZED: 34,2
ACRES PERMITTED: 34.2
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Name of Crop Type
Voiall- Mineral- Ammonia Nitrate PAN Applied Receiving Residual
Application lizalion tion TKN Nitrogen and Nitrite (Ibslacre) Application
Method* Rate** Rate*** mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop
SUR 0.5 0.20 34,000.00 12,000.00 60.30 13.612 FSH
4/9/2021
4/10/2021
4/12/2021
Apr-21
117,800.00
124,000.00
142,600.00
384,400.00
(G)
(G)
(G)
(G)
4.530
4.530
4.530
0.651
0.685
0.788
Total 2.124
LIL
LIL
LIL
DRY
DRY
DRY
"D-<112"
0-<1/2"
"0-<112"
SUR 0.5 0.20 34,000.00 12,000.00 60.30 14.329 FSH
SUR 0.5 0.20 34,000.00 12,000.00 60.30 16.478 FSH
Total 44.419 0.000
A
CD
Cu
R
P
HG MO NI SE ZN P Lime Applied
Annual Ibslacre Applied 0.019
0.002
0,977
0.174
0,035
0.002 0.014 0035 0.012 0.552 59.450 Date Lbs/Ac
Cumulative Ibs/acre Applied
0.030
0.003
1.305
0,261
0,051
0.003 1 0,025
Permit PAN Limit (Ibslacre)
.056 0.0
0
Crops 157
Federal C.P.L.R. (Ibs/a
LIL = LINCOLNTON, N
6.6 ( 34.8 1 1,339.0
TP ANAEROB, DIGESTED LIQUID
267,9 ) 15.0 ( ,..... j 375.0 89.0 ( 2,500,0
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Tam
aware that there are significant pen ij6s for sub}1 •
information, including the possibility of fines and imprisonment for knowing violations,"
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required
Application Method: SUR- Surface, INJ - Injection, SURIN - Incorporation
Volatilization Rate: Surface 0.5, Infection/Incorporation 1,0
Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
C.P.L.R. : Cumulative Pollutant Loading Rate
See Site pH 8 Lime Application Records Section of Report
Printed: 2/2/2022 DENR FORM FSF (12/2006)

SECTION 4

it
SU M M 1 Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNO L°CIES, INC Cuyahoga Falls, Ohio 44223
ArralyUcal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://www.settek.com
January 12, 2021
Alex Fox
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: Lincolnton
Dear Alex Fox:
Order No.: 21010091
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/5/2021 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
y77..�t/cRa4--
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP CL0052, Oklahoma
2019-155, Oregon OH200001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 42

it
SU M t 1 T Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNO LOGES, INC. Cuyahoga Falls, Ohio 44223
4rraly0cal Laboralorlas TEL: [phone] FAX. [phone]
Website: http://www.settek.com
Case Narrative
WO#: 21010091
Date: 1/12/2021
CLIENT: Synagro
Project: Lincolnton
WorkOrder Narrative:
21010091: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Original
Page 2 of 42

it
Summit Environmental Technologies, In
3310 Win
EkiwIRONM@Ni'AL TECHN❑LOGiES, INC Cuyahoga Falls, Ohio 442
4rralytiical Laboralorlas TEL: [phone] FAX. [phone]E
Website: http://www.settek.co
Summit
Qualifiers and Acronyms
WO#: 21010091
Date: 1/12/2021
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
QC
MB
LCS
LCSD
QCS
DUP
MS
MSD
RPD
ICV
ICB
CCV
CCB
RLC
DF
Not Detected
Quality Control
Method Blank
Laboratory Control Sample
Laboratory Control Sample Duplicate
Quality Control Sample
Duplicate
Matrix Spike
Matrix Spike Duplicate
Relative Percent Different
Initial Calibration Verification
Initial Calibration Blank
Continuing Calibration Verification
Continuing Calibration Blank
Reporting Limit Check
Dilution Factor
RL
MDL
LOD
LOQ
PQL
CRQL
PL
RegLvl
MCL
MinCL
RA
RE
TIC
RT
CF
RF
Reporting Limit
Method Detection Limit
Level of Detection
Level of Quantitation
Practical Quantitation Limit
Contract Required Quantitation Limit
Permit Limit
Regulatory Limit
Maximum Contamination Limit
Minimum Compound Limit
Reanalysis
Reextraction
Tentatively Identified Compound
Retention Time
Calibration Factor
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 42

it
SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL 'Melilla woiEs, IFIc, Cuyahoga Falls, Ohio 44223
4nalyacal Laboralorfas TEL: [phone] FAX [phone]
Website: http://www.settek.com
Workorder
Sample Summary
WO#: 21010091
12-Jan-21
CLIENT: Synagro
Project: Lincolnton
Lab SamplelD Client Sample ID
21010091-001 Lincolnton
Tag No Date Collected Date Received Matrix
1/4/2021 10:00:00 AM 1/5/2021 10:15:00 AM Sludge
Page 4 of 42

it
SUMMI
ENVIRONMENTAL TECHNOLOGIES, INC
4rralyNcaf Laboratorfas
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: http://www.settekcom
DATES REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
Sample ID
Client Sample ID
Collection Date Matrix
Test Name Leachate Date
Prep Date
Analysis Date
21010091-001A Lincolnton
1/4/2021 10:00:00 AM Sludge Ignitability of Solids (SW-846: 1030)
pH (SW9045D)
Reactive Cyanide (9014/7.3.3.2)-Solid
Reactive Sulfide (9034)/7.3.4.2
TCLP Herbicides by EPA 8321B
TCLP Mercury Analysis (SW1311/7471/6/2021 2:30:00 PM
TCLP Metals Analysis (SW1311/6010:1/6/2021 2:30:00 PM
TCLP Pesticides Analysis (SW1311/8(1/6/2021 2:30:00 PM
TCLP Pesticides Analysis (SW1311/8(1/6/2021 2:30:00 PM
TCLP Semi-Volatiles Analysis 1/6/2021 2:30:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
1/8/2021 8:50:00 AM
1/7/2021 12:30:00 PM
1/8/2021 12:00:00 PM
1/8/2021 12:00:00 PM
1/7/2021 12:15:00 PM
1/6/2021 2:30:00 PM
1/6/2021 2:27:57 PM
1/6/2021 12:50:00 PM
1/7/2021 4:50:00 PM
1/7/2021 4:50:00 PM
1/8/2021 8:45:00 PM
1/8/2021 12:33:00 PM
1/11/2021 12:44:57 PM
1/11/2021 10:20:00 PM
1/11/2021 10:20:00 PM
1/8/2021 1:22:00 AM
1/7/2021 6:25:00 PM
Original
Page 5 of 42

il
5uMMI
ENVIRONMENTAL TECHNOLOGIES, ItlC
4rraly0cal Laboralorfas TEL: [phone] FAX.. [phone]
Website: http://wwi'.settek.com
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Analytical Report
(base report)
WO#: 21010091
Date Reported: 1/12/2021
CLIENT:
Matrix:
Lab ID:
Proj ect:
Synagro
SLUDGE
21010091-001 A
Lincolnton
Client Sample ID Lincolnton
Tag Number:
Collection Date: 1/4/2021 10:00:00 AM
Analyses Result
RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00200 mg/L
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
TCLP Barium(Ba)
TCLP Cadmium(Cd)
TCLP Chromium(Cr)
TCLP Lead(Pb)
TCLP Selenium(Se)
TCLP Silver(Ag)
ND
ND
ND
ND
ND
ND
ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
Cresols, Total
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Surr: 2-Fluorophenol
Surr: Phenol-d6
Surr: Nitrobenzene-d5
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: p-Terphenyl-d14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
70.0
65.4
69.4
88.8
74.8
104
0.500
5.00
0.100
0.200
0.500
0.0500
0.500
SW7470A SW7470A Analyst: ERA
1
SW6010D
mg/L 1
mg/L 1
mg/L 1
mg/L 1
mg/L 1
mg/L 1
mg/L 1
0.200 mg/L
0.500 mg/L
0.500 mg/L
0.100 mg/L
10.0 mg/L
0.0400 mg/L
0.100 mg/L
0.200 mg/L
0.200 mg/L
0.500 mg/L
0.500 mg/L
10 - 157 m %Rec
10 - 169 %Rec
32.1 - 130 %Rec
45.4 - 166 %Rec
35.7 - 130 %Rec
74.7 - 145 %Rec
1/8/2021 12:33:00 PM
SW3010A Analyst: EAM
1/11/2021 12:44:57 PM
1/11/2021 12:44:57 PM
1/11/2021 12:44:57 PM
1/11/2021 12:44:57 PM
1/11/2021 12:44:57 PM
1/11/2021 12:44:57 PM
1/11/2021 12:44:57 PM
SW8270 SW3510C Analyst: SFG
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
2 1/8/2021 1:22:00 AM
Qualifiers:
B
H
MC
ND
PL
RL
Analyte detected in the associated Method Blank
Holding times for preparation or analysis exceeded
Value is below Minimum Compound Limit.
Not Detected
Permit Limit
Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits
U Samples with Ca1cVa1 < MDL
Original
Page 6 of 42

il
5uMMI
ENVIRONMENTAL TECHNOLOGIES, ItlC
4rrafy0caf Laboralorfas TEL: [phone] FAX.. [phone]
Website: http://wni'.settek.com
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Analytical Report
(base report)
WO#: 21010091
Date Reported: 1/12/2021
CLIENT:
Matrix:
Lab ID:
Proj ect:
Synagro
SLUDGE
21010091-001 A
Lincolnton
Client Sample ID Lincolnton
Tag Number:
Collection Date: 1/4/2021 10:00:00 AM
Analyses Result
RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
Toxaphene
Endrin
gamma-BHC
Heptachlor
Heptachlor epoxide
Methoxychlor
Surr: TCMX
Surr: DCB
TCLP HERBICIDES BY EPA 8321B
2,4-D
2,4,5-TP
Surr: 2,4-Dichlorophenylacetic aci
ND
ND
ND
ND
ND
ND
ND
61.3
79.5
ND
ND
106
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
93.6
102
98.3
0.0250
0.0500
0.00250
0.00250
0.00250
0.00250
0.00250
10- 119
10- 119
mg/L 1
mg/L 1
mg/L 1
mg/L 1
mg/L 1
mg/L 1
mg/L 1
%Rec 1
%Rec 1
SW8321A
SW3510C Analyst: CSS
1/11/2021 10:20:00 PM
1/11/2021 10:20:00 PM
1/11/2021 10:20:00 PM
1/11/2021 10:20:00 PM
1/11/2021 10:20:00 PM
1/11/2021 10:20:00 PM
1/11/2021 10:20:00 PM
1/11/2021 10:20:00 PM
1/11/2021 10:20:00 PM
Analyst: JPG
0.500 mg/L 50 1/8/2021 8:45:00 PM
0.500 mg/L 50 1/8/2021 8:45:00 PM
70 - 130 %Rec 50 1/8/2021 8:45:00 PM
0.250
0.250
5.00
0.250
0.250
2.50
0.250
0.250
0.250
0.100
70 - 130
70 - 130
70 - 130
SW8260 SW1311M Analyst: SLV
mg/L 50
mg/L 50
mg/L 50
mg/L 50
mg/L 50
mg/L 50
mg/L 50
mg/L 50
mg/L 50
mg/L 50
%Rec 50
%Rec 50
%Rec 50
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
1/7/2021 6:25:00 PM
Qualifiers:
B
H
MC
ND
PL
RL
Analyte detected in the associated Method Blank
Holding times for preparation or analysis exceeded
Value is below Minimum Compound Limit.
Not Detected
Permit Limit
Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits
U Samples with Ca1cVa1 < MDL
Original
Page 7 of 42

il
5uMMI
ENVIRONMENTAL TECHNOLOGIES, ItlC
4rraly0cal Laboralorfas TEL: [phone] FAX.. [phone]
Website: http://wwi'.settek.com
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
Analytical Report
(base report)
WO#: 21010091
Date Reported: 1/12/2021
CLIENT:
Matrix:
Lab ID:
Proj ect:
Synagro
SLUDGE
21010091-001 A
Lincolnton
Client Sample ID Lincolnton
Tag Number:
Collection Date: 1/4/2021 10:00:00 AM
Analyses
Result RL Qual Units
DF Date Analyzed
RCI
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability
RCI
PH (SW9045D)
pH
RCI
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
nonflammable
7.0
40.0
SW9014
ND 0.495 mg/Kg
SW1030
mm/sec
SW9045D
s.u.@19.8C
SW9034
25.0 mg/Kg
1
1
1
Analyst: MS
1/7/2021 4:50:00 PM
Analyst: SEE
1/6/2021 2:27:57 PM
Analyst: DHC
1/6/2021 12:50:00 PM
Analyst: MS
1 1/7/2021 4:50:00 PM
Qualifiers:
B
H
MC
ND
PL
RL
Analyte detected in the associated Method Blank
Holding times for preparation or analysis exceeded
Value is below Minimum Compound Limit.
Not Detected
Permit Limit
Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits
U Samples with Ca1cVa1 < MDL
Original
Page 8 of 42

it
Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, i Cuyahoga Falls, Ohio 44223
4nalytilcal Laboralorlas TEL: [phone] FAX [phone]
Website: http://www.settek.com
Accreditation Program
Analytes Report
WO#: 21010091
12-Jan-21
Client: Synagro
Project: Lincolnton
State: NW
Program Name: NC_WW_SCM
Sample ID
Matrix
Test Name
Analyte Status
21010091-001 A
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Sludge
Ignitability of Solids (SW-846: 1030)
pH (SW9045D)
Reactive Cyanide (9014/7.3.3.2)-Solid
Reactive Sulfide (9034)/7.3.4.2
TCLP Herbicides by EPA 8321B
TCLP Herbicides by EPA 8321B
TCLP Mercury Analysis (SW1311/7470)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Metals Analysis (SW1311/6010)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Pesticides Analysis (SW1311/8081)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
TCLP Semi-Volatiles Analysis (SW1311/8270)
Ignitability A
Hydrogen Ion (pH) A
Cyanide, Reactive N
Sulfide, Reactive N
2,4,5-TP A
2,4-D A
Mercury A
Arsenic A
Barium A
Cadmium A
Chromium A
Lead A
Selenium A
Silver A
Chlordane, total A
Endrin A
gamma-BHC A
Heptachlor A
Heptachlor epoxide A
Methoxychlor A
Toxaphene A
1,4-Dichlorobenzene A
2,4,5-Trichlorophenol A
2,4,6-Trichlorophenol A
2,4-Dinitrotoluene A
Cresols, Total A
Hexachlorobenzene A
Hexachlorobutadiene A
Hexachloroethane A
Nitrobenzene A
Pentachlorophenol A
Pyridine A
Original #1
Page 9 of 42

it
Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHN❑ LOGIES, INC Cuyahoga Falls, Ohio 44223
4nalytilcal Laboralorlas TEL: [phone] FAX [phone]
Website: http://www.settek.com
Accreditation Program
Analytes Report
WO#: 21010091
12-Jan-21
Client: Synagro
Project: Lincolnton
State: NW
Program Name: NC_WW_SCM
Sample ID
Matrix
Test Name
Analyte Status
21010091-001 A
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
Sludge TCLP Volatiles Analysis
1,1-Dichloroethene
1,2-Dichloroethane
2-Butanone
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
A
A
A
A
A
A
A
A
A
A
Original #1
Page 10 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchID: 47168
Sample ID: LCS-47168
Client ID: LCSS
Analyte
SampType: LCS
TestCode: TCLP-VOC-M Units: mg/L
Batch ID: 47168 TestNo: SW8260 SW1311M
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/7/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122240
SegNo: 3146714
%RPD RPDLimit Qual
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
0.836
0.773
ND
0.893
0.963
ND
0.871
0.960
0.948
0.750
2420
2530
2480
0.250
0.250
5.00
0.250
0.250
2.50
0.250
0.250
0.250
0.100
1.00
1.00
5.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
2500
2500
2500
0 83.6
0 77.3
0 94.7
0 89.3
0 96.3
0 91.0
0 87.1
0 96.0
0 94.8
0 75.0
96.6
101
99.3
64.7
70
55.1
70
70
70
70
70
62.8
67.1
70
70
70
136
130
149
130
130
130
130
134
160
130
130
130
130
Sample ID: MB-47168
Client ID: PBS
Analyte
SampType: MBLK
Batch ID: 47168
Result
TestCode: TCLP-VOC-M Units: mg/L
TestNo: SW8260 SW1311M
PQL
Prep Date: 1/6/2021
Analysis Date: 1/7/2021
SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122240
SegNo: 3146716
%RPD RPDLimit Qual
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
ND
ND
ND
ND
0.250
0.250
5.00
0.250
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 11 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchID: 47168
Sample ID: MB-47168
Client ID: PBS
Analyte
SampType: MBLK TestCode: TCLP-VOC-M Units: mg/L
Batch ID: 47168 TestNo: SW8260 SW1311M
Result PQL SPK value SPK Ref Val
Prep Date: 1/6/2021
Analysis Date: 1/7/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122240
SegNo: 3146716
%RPD RPDLimit Qual
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
ND
ND
ND
ND
ND
ND
2340
2520
2440
0.250
2.50
0.250
0.250
0.250
0.100
2500
2500
2500
93.6
101
97.8
70
70
70
130
130
130
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 12 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchID: 47168
Sample ID: 21010095-001AMS SampType: MS
Client ID: BatchQC Batch ID: 47168
Analyte
TestCode: TCLP-VOC-M Units: mg/L
TestNo: SW8260 SW1311M
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/7/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122240
SegNo: 3146995
%RPD RPDLimit Qual
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
0.884
0.825
ND
0.919
1.02
ND
0.918
0.966
0.978
0.801
2440
2560
2500
0.250
0.250
5.00
0.250
0.250
2.50
0.250
0.250
0.250
0.100
1.00
1.00
5.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
2500
2500
2500
0
0
0
0
0
0
0
0
0
0
88.4
82.5
98.5
91.9
102
94.3
91.8
96.6
97.8
80.1
97.4
102
100
13.6
55.7
65.3
49.2
26.7
33.7
48.5
19.2
38.4
27.3
91.7
75.5
94.1
202
138
118
145
156
159
145
191
167
161
109
118
105
Sample ID: 21010095-001AMSD SampType: MSD
Client ID: BatchQC Batch ID: 47168
Analyte
Result
TestCode: TCLP-VOC-M Units: mg/L
TestNo: SW8260 SW1311M
Prep Date:
Analysis Date: 1/7/2021
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122240
SegNo: 3146996
%RPD RPDLimit Qual
1,1-Dichloroethene
1,2-Dichloroethane
MEK
Benzene
0.901
0.832
ND
0.943
0.250
0.250
5.00
0.250
1.00
1.00
5.00
1.00
0
0
0
0
90.1
83.2
98.0
94.3
13.6
55.7
65.3
49.2
202
138
118
145
0.884
0.825
0
0.919
1.90
0.906
25
25
0 25
2.52 25
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 13 of 42

•
5uMMI
ENVIRONMENTAL TECHNOLOGI S.INC
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchID: 47168
Sample ID: 21010095-001AMSD SampType: MSD
Client ID: BatchQC Batch ID: 47168
Analyte
TestCode: TCLP-VOC-M Units: mg/L
TestNo: SW8260 SW1311M
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/7/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122240
SegNo: 3146996
%RPD RPDLimit Qual
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surr: 4-Bromofluorobenzene
Surr: Dibromofluoromethane
Surr: Toluene-d8
1.03
ND
0.924
0.972
0.981
0.808
2420
2570
2500
0.250
2.50
0.250
0.250
0.250
0.100
1.00
1.00
1.00
1.00
1.00
1.00
2500
2500
2500
0
0
0
0
0
0
103
94.4
92.4
97.2
98.1
80.8
96.9
103
99.9
26.7
33.7
48.5
19.2
38.4
27.3
91.7
75.5
94.1
156
159
145
191
167
161
109
118
105
1.02
0
0.918
0.966
0.978
0.801
1.51
0
0.652
0.722
0.306
0.870
0
0
0
25
25
25
25
25
25
25
25
25
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 14 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchID: 47176
Sample ID: MB-47176
Client ID: PBS
Analyte
SampType: MBLK
Batch ID: 47176
TestCode: MtI-TCLP-7(6 Units: mg/L
TestNo: SW6010D SW3010A
Result PQL SPK value SPK Ref Val
Prep Date: 1/7/2021
Analysis Date: 1/11/2021
RunNo: 122314
SegNo: 3148738
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Arsenic(As)
TCLP Barium(Ba)
TCLP Cadmium(Cd)
TCLP Chromium(Cr)
TCLP Lead(Pb)
TCLP Selenium(Se)
TCLP Silver(Ag)
ND
ND
ND
ND
ND
ND
ND
0.500
5.00
0.100
0.200
0.500
0.0500
0.500
Sample ID: LCS-47176
Client ID: LCSS
Analyte
SampType: LCS
Batch ID: 47176
Result
TestCode: MtI-TCLP-7(6 Units: mg/L
TestNo: SW6010D SW3010A
PQL
SPK value SPK Ref Val
Prep Date: 1/7/2021
Analysis Date: 1/11/2021
RunNo: 122314
SegNo: 3148739
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Arsenic(As)
TCLP Barium(Ba)
TCLP Cadmium(Cd)
TCLP Chromium(Cr)
TCLP Lead(Pb)
TCLP Selenium(Se)
TCLP Silver(Ag)
1.92
ND
2.00
2.13
2.08
2.07
2.10
0.500
5.00
0.100
0.200
0.500
0.0500
0.500
2.000
2.000
2.000
2.000
2.000
2.000
2.000
0 96.1
0 105
0 99.9
0 107
0 104
0 104
0 105
80 120
80 120
80 120
80 120
80 120
80 120
80 120
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 15 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchID: 47176
Sample ID: TCLP BLANK 1-7-21 SampType: MBLK
Client ID: PBS Batch ID: 47176
Analyte
TestCode: MtI-TCLP-7(6 Units: mg/L
TestNo: SW6010D SW3010A
Result PQL SPK value SPK Ref Val
Prep Date: 1/7/2021
Analysis Date: 1/11/2021
RunNo: 122314
SeqNo: 3148740
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Barium(Ba)
TCLP Cadmium(Cd)
TCLP Chromium(Cr)
TCLP Lead(Pb)
TCLP Silver(Ag)
ND
ND
ND
ND
ND
5.00
0.100
0.200
0.500
0.500
Sample ID: TCLP BLANK 1-7-21 SampType: MBLK
Client ID: PBS Batch ID: 47176
Analyte
Result
TestCode: MtI-TCLP-7(6 Units: mg/L
TestNo: SW6010D SW3010A
PQL
SPK value SPK Ref Val
Prep Date: 1/7/2021
Analysis Date: 1/11/2021
RunNo: 122314
SegNo: 3148749
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Arsenic(As)
TCLP Selenium(Se)
ND
ND
0.500
0.0500
Sample ID: 21010094-001AMSD SampType: MSD TestCode: MtI-TCLP-7(6 Units: mg/L
Client ID: BatchQC Batch ID: 47176
Analyte
TestNo: SW6010D SW3010A
Result PQL
SPK value SPK Ref Val
Prep Date: 1/7/2021
Analysis Date: 1/11/2021
RunNo: 122314
SegNo: 3149171
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Arsenic(As)
TCLP Barium(Ba)
TCLP Cadmium(Cd)
1.90 0.500 2.000 0
ND 5.00 2.000 0.2512
1.83 0.100 2.000 0.001953
95.2 70
88.4 70
91.3 70
130
130
130
1.895
0
1.862
0.500
0
1.90
20
20
20
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 16 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchID: 47176
Sample ID: 21010094-001AMSD SampType: MSD TestCode: MtI-TCLP-7(6 Units: mg/L
Client ID: BatchQC Batch ID: 47176
Analyte
TestNo: SW6010D SW3010A
Result PQL SPK value SPK Ref Val
Prep Date: 1/7/2021
Analysis Date: 1/11/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122314
SegNo: 3149171
%RPD RPDLimit Qual
TCLP Chromium(Cr)
TCLP Lead(Pb)
TCLP Selenium(Se)
TCLP Silver(Ag)
1.83
1.69
2.21
1.94
0.200
0.500
0.0500
0.500
2.000 0
2.000 0
2.000 0.03034
2.000 0
91.5
84.5
109
97.2
70
70
70
70
130
130
130
130
1.880
1.735
2.177
1.984
2.69
2.62
1.64
2.04
20
20
20
20
Sample ID: 21010094-001AMS SampType: MS
Client ID: BatchQC Batch ID: 47176
Analyte
Result
TestCode: MtI-TCLP-7(6 Units: mg/L
TestNo: SW6010D SW3010A
PQL
Prep Date: 1/7/2021
Analysis Date: 1/11/2021
SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122314
SegNo: 3149236
%RPD RPDLimit Qual
TCLP Arsenic(As)
TCLP Barium(Ba)
TCLP Cadmium(Cd)
TCLP Chromium(Cr)
TCLP Lead(Pb)
TCLP Selenium(Se)
TCLP Silver(Ag)
1.89 0.500 2.000 0 94.7
ND 5.00 2.000 0.2512 90.4
1.86 0.100 2.000 0.001953 93.0
1.88 0.200 2.000 0 94.0
1.74 0.500 2.000 0 86.8
2.18 0.0500 2.000 0.03034 107
1.98 0.500 2.000 0 99.2
70 130
70 130
70 130
70 130
70 130
70 130
70 130
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 17 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: 47177
Sample ID: MB-47177
Client ID: PBS
Analyte
SampType: MBLK TestCode: TCLP-SVOC_ Units: mg/L
Batch ID: 47177 TestNo: SW8270 SW3510C
Result PQL SPK value SPK Ref Val
Prep Date: 1/7/2021
Analysis Date: 1/7/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122260
SegNo: 3147025
%RPD RPDLimit Qual
1,4-Dichlorobenzene
2,4, 5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
o-Cresol
Cresols, Total
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Surr: 2-Fluorophenol
Surr: Phenol-d6
Surr: Nitrobenzene-d5
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: p-Terphenyl-d14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.856
0.775
0.918
1.03
0.832
1.03
0.100
0.250
0.250
0.0500
0.250
5.00
0.0200
0.0500
0.100
0.100
0.250
0.250
1.000
1.000
1.000
1.000
1.000
1.000
85.6
77.5
91.8
103
83.2
103
10
10
19
10
22
34
109
109
120
120
117
116
m
m
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 18 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: 47177
Sample ID: LCS-47177
Client ID: LCSS
Analyte
SampType: LCS
Batch ID: 47177
TestCode: TCLP-SVOC_ Units: mg/L
TestNo: SW8270 SW3510C
Result PQL
Prep Date: 1/7/2021
Analysis Date: 1/7/2021
SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122260
SegNo: 3147026
%RPD RPDLimit Qual
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
o-Cresol
Cresols, Total
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Surr: 2-Fluorophenol
Surr: Phenol-d6
Surr: Nitrobenzene-d5
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: p-Terphenyl-d14
0.670
0.745
0.783
0.829
0.800
ND
0.620
0.764
0.643
0.756
0.850
0.285
0.982
0.911
0.897
1.09
0.945
1.08
0.100
0.250
0.250
0.0500
0.250
5.00
0.0200
0.0500
0.100
0.100
0.250
0.250
0.8000
0.8000
0.8000
0.8000
0.8000
1.600
0.8000
0.8000
0.8000
0.8000
0.8000
0.8000
1.000
1.000
1.000
1.000
1.000
1.000
0
0
0
0
0
0
0
0
0
0
0
0
83.8
93.2
97.8
104
100
98.3
77.4
95.6
80.4
94.5
106
35.6
98.2
91.1
89.7
109
94.5
108
36.4
31.7
31.1
43.3
32.9
31.7
31.4
43.1
36.5
39.5
34
10
17.1
10
32.6
4.43
41.8
36.4
130
132
133
130
130
130
130
130
130
130
130
130
130
130
130
130
130
130
m
m
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 19 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: 47177
Sample ID: 21010089-001AMS SampType: MS
Client ID: BatchQC Batch ID: 47177
Analyte
TestCode: TCLP-SVOC_ Units: mg/L Prep Date: 1/7/2021
TestNo: SW8270 SW3510C Analysis Date: 1/8/2021
Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122338
SegNo: 3149456
%RPD RPDLimit Qual
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
o-Cresol
Cresols, Total
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Surr: 2-Fluorophenol
Surr: Phenol-d6
Surr: Nitrobenzene-d5
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: p-Terphenyl-d14
0.676
0.788
0.805
0.716
0.792
ND
0.649
0.746
0.676
0.759
0.832
ND
0.898
0.914
0.870
1.02
0.860
1.10
0.200
0.500
0.500
0.100
0.500
10.0
0.0400
0.100
0.200
0.200
0.500
0.500
0.8000
0.8000
0.8000
0.8000
0.8000
1.600
0.8000
0.8000
0.8000
0.8000
0.8000
0.8000
1.000
1.000
1.000
1.000
1.000
1.000
0
0
0
0
0
1.030
0
0
0
0
0
0
84.5
98.5
101
89.6
99.0
91.8
81.1
93.2
84.5
94.9
104
16.4
89.8
91.4
87.0
102
86.0
110
15.2
30.6
27.6
58
26.9
27.6
10
54.3
1.92
21
47.4
10
9.77
20.7
13.9
27.3
21.4
54.8
124
152
150
141
132
132
156
142
131
135
134
130
146
130
156
183
153
154
mQMR
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 20 of 42

•
5uMMI
ENVIRONMENTAL TECHNOLOGI S.INC
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: 47177
Sample ID: 21010089-001AMSD SampType: MSD
Client ID: BatchQC Batch ID: 47177
Analyte
TestCode: TCLP-SVOC_ Units: mg/L
TestNo: SW8270 SW3510C
Result PQL SPK value SPK Ref Val
Prep Date: 1/7/2021
Analysis Date: 1/8/2021
RunNo: 122338
SeqNo: 3149457
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
o-Cresol
Cresols, Total
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
Surr: 2-Fluorophenol
Surr: Phenol-d6
Surr: Nitrobenzene-d5
Surr: 2,4,6-Tribromophenol
Surr: 2-Fluorobiphenyl
Surr: p-Terphenyl-d14
0.584 0.200 0.8000 0 73.0 15.2 124 0.6760 14.5 30
0.740 0.500 0.8000 0 92.5 30.6 152 0.7880 6.28 30
0.745 0.500 0.8000 0 93.1 27.6 150 0.8052 7.79 30
0.803 0.100 0.8000 0 100 58 141 0.7164 11.4 30
0.761 0.500 0.8000 0 95.2 26.9 132 0.7924 4.02 30
ND 10.0 1.600 1.030 79.8 27.6 132 0 0 30
0.584 0.0400 0.8000 0 73.0 10 156 0.6488 10.4 30
0.758 0.100 0.8000 0 94.8 54.3 142 0.7456 1.65 30
0.576 0.200 0.8000 0 72.0 1.92 131 0.6760 15.9 30
0.680 0.200 0.8000 0 85.1 21 135 0.7592 10.9 30
0.816 0.500 0.8000 0 102 47.4 134 0.8320 1.89 30
ND 0.500 0.8000 0 29.2 10 130 0 0 30 Rm
0.748 1.000 74.8 9.77 146 0
0.824 1.000 82.4 20.7 130 0
0.832 1.000 83.2 13.9 156 0
1.07 1.000 107 27.3 183 0
0.828 1.000 82.8 21.4 153 0
1.15 1.000 115 54.8 154 0
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 21 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: 47184
Sample ID: MB-47184
Client ID: PBS
Analyte
SampType: MBLK
Batch ID: 47184
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
Result PQL SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/8/2021
RunNo: 122272
SegNo: 3147490
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury
ND
0.00200
Sample ID: LCS-47184
Client ID: LCSS
Analyte
SampType: LCS
Batch ID: 47184
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
Result PQL SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/8/2021
RunNo: 122272
SegNo: 3147491
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury
0.00365
0.00200
0.00400
0
91.2
80
120
Sample ID: 21010094-001AMS SampType: MS
Client ID: BatchQC Batch ID: 47184
Analyte
Result
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL
SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/8/2021
RunNo: 122272
SegNo: 3147498
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury
0.00365
0.00200
0.00400 0.0000160
90.8
75
125
Sample ID: 21010094-001AMSD SampType: MSD
Client ID: BatchQC Batch ID: 47184
Analyte
Result
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL
SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/8/2021
RunNo: 122272
SegNo: 3147499
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury
0.00362
0.00200
0.00400 0.0000160
90.1
75
125
0.00365
0.825
20
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal)
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 22 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: 47184
Sample ID: 21010094-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM
Client ID: BatchQC Batch ID: 47184
Analyte
Result
TestNo: SW7470A SW7470A
PQL SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/8/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122272
SegNo: 3147499
%RPD RPDLimit Qual
Sample ID: TCLP Blankl 1-7-21 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM
Client ID: PBS Batch ID: 47184
Analyte
TestNo: SW7470A SW7470A
Result PQL SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/8/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122272
SegNo: 3147506
%RPD RPDLimit Qual
TCLP Mercury
ND
0.00200
Sample ID: MB2-47184
Client ID: PBS
Analyte
SampType: MBLK
Batch ID: 47184
Result
TestCode: HG_TCLP(74 Units: PPM
TestNo: SW7470A SW7470A
PQL
Prep Date: 1/8/2021
Analysis Date: 1/8/2021
SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122272
SegNo: 3147507
%RPD RPDLimit Qual
TCLP Mercury
ND
0.00200
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal)
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 23 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD:
47205
Sample ID: 21010092-001ams
Client ID: BatchQC
Analyte
SampType: MS
TestCode: TCLP-SVOC- Units: mg/L
Batch ID: 47205 TestNo: SW8081 SW3510C
Result PQL SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/11/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122365
SegNo: 3150630
%RPD RPDLimit Qual
Endrin
Methoxychlor
0.00799
0.000500
0.0100 0.000500
0.0100
0.0100
0
0
79.9
100
10
10
224
251
m
Sample ID: 21010092-001amsd SampType: MSD TestCode: TCLP-SVOC- Units: mg/L
Client ID: BatchQC Batch ID: 47205 TestNo: SW8081 SW3510C
Analyte
Result PQL SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/11/2021
RunNo: 122365
SegNo: 3150631
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Endrin
Methoxychlor
0.00746
0.000500
0.00896 0.000500
0.0100
0.0100
0
0
74.6
89.6
10
10
224
251
0.00799
0.0100
6.93
11.0
30 m
30
Sample ID: LCS-47205
Client ID: LCSS
Analyte
SampType: LCS
Batch ID: 47205
Result
TestCode: TCLP-SVOC- Units: mg/L
TestNo: SW8081 SW3510C
PQL
SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/11/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122365
SegNo: 3150641
%RPD RPDLimit Qual
Endrin
Methoxychlor
0.00659
0.000500
0.00925 0.000500
0.0100
0.0100
0
0
65.9
92.5
10
10
130
178
m
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 24 of 42

•
Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TEC!*10 LOi,1 5, INC Cuyahoga Falls, Ohio 44223
4rraiyticaf Laboratorfas TEL: [phone] FAX: [phone]
Website: http://www.settek.com
5uMMI
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: 47205
Sample ID: MB-47205
Client ID: PBS
Analyte
SampType: MBLK TestCode: TCLP-SVOC- Units: mg/L
Batch ID: 47205 TestNo: SW8081 SW3510C
Result PQL SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/11/2021
RunNo: 122365
SegNo: 3150643
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Endrin
Methoxychlor
ND
ND 0.000500
0.000500
Qualifiers:
B
J
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 25 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: 47205
Sample ID: 21010092-001ams
Client ID: BatchQC
Analyte
SampType: MS
TestCode: TCLP-SVOC- Units: mg/L
Batch ID: 47205 TestNo: SW8081 SW3510C
Result PQL SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/11/2021
RunNo: 122364
SeqNo: 3150607
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
gamma-BHC
Heptachlor
Heptachlor epoxide
Surr: TCMX
Surr: DCB
0.00840
0.00895
0.00964
14.5
17.4
0.000500
0.000500
0.000500
0.0100
0.0100
0.0100
20.00
20.00
0
0
0
84.0
89.5
96.4
72.5
87.0
10
10
10
10
10
192
197
208
157
194
P
P
P
P
P
Sample ID: 21010092-001amsd SampType: MSD
Client ID: BatchQC Batch ID: 47205
Analyte
TestCode: TCLP-SVOC- Units: mg/L
TestNo: SW8081 SW3510C
Result PQL
SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/11/2021
RunNo: 122364
SeqNo: 3150608
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
gamma-BHC
Heptachlor
Heptachlor epoxide
Surr: TCMX
Surr: DCB
0.00769
0.00812
0.00867
13.2
15.6
0.000500
0.000500
0.000500
0.0100
0.0100
0.0100
20.00
20.00
0
0
0
76.9
81.2
86.7
66.0
78.1
10
10
10
10
10
192
197
208
157
194
0.00840
0.00895
0.00964
8.85
9.75
10.7
0
0
30
30
30
P
P
P
P
P
Sample ID: LCS-47205
Client ID: LCSS
Analyte
SampType: LCS
Batch ID: 47205
Result
TestCode: TCLP-SVOC- Units: mg/L
TestNo: SW8081 SW3510C
PQL
SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/11/2021
RunNo: 122364
SeqNo: 3150618
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 26 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: 47205
Sample ID: LCS-47205
Client ID: LCSS
Analyte
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Batch ID: 47205 TestNo: SW8081 SW3510C
Result PQL SPK value SPK Ref Val
Prep Date: 1/8/2021
Analysis Date: 1/11/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122364
SegNo: 3150618
%RPD RPDLimit Qual
gamma-BHC
Heptachlor
Heptachlor epoxide
Surr: TCMX
Surr: DCB
0.00848
0.00899
0.00953
14.2
17.4
0.000500
0.000500
0.000500
0.0100
0.0100
0.0100
20.00
20.00
0
0
0
84.8
89.9
95.3
71.1
87.0
10
10
10
10
10
130
130
130
130
130
Sample ID: MB-47205
Client ID: PBS
Analyte
SampType: MBLK
Batch ID: 47205
Result
TestCode: TCLP-SVOC- Units: mg/L
TestNo: SW8081 SW3510C
PQL
Prep Date: 1/8/2021
Analysis Date: 1/11/2021
SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122364
SegNo: 3150620
%RPD RPDLimit Qual
Chlordane, total
Toxaphene
gamma-BHC
Heptachlor
Heptachlor epoxide
Surr: TCMX
Surr: DCB
ND
ND
ND
ND
ND
13.2
16.7
0.00250
0.00500
0.000500
0.000500
0.000500
20.00
65.9
20.00 83.3
10
10
119
119
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 27 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: R122166
Sample ID: 21010121-001ADUP SampType: DUP
Client ID: BatchQC Batch ID: R122166
Analyte
TestCode: pH_Oil(9045D Units: s.u.@20.2C
TestNo: SW9045D
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/6/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122166
SegNo: 3145092
%RPD RPDLimit Qual
pH
6.2
0
0
6.2
0.5
10
Sample ID: PH 7 CHECK
Client ID: LCSW
Analyte
SampType: LCS
Batch ID: R122166
TestCode: PH_OIL(9045 Units: s.u.@19.3C
TestNo: SW9045D
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/6/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122166
SegNo: 3145095
%RPD RPDLimit Qual
pH
7.0
7.0
0
101
90
110
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal)
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 28 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: R122166
Sample ID: LCS-R122166 SampType: LCS
Client ID: LCSS
Analyte
TestCode: pH_S(9045D) Units: s.u.@20.6C
Batch ID: R122166 TestNo: SW9045D
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/6/2021
RunNo: 122166
SeqNo: 3144997
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH
7.0
7.0
0
100
90
110
Sample ID: 21010089-001ADUP SampType: DUP
Client ID: BatchQC Batch ID: R122166
Analyte
TestCode: pH_S(9045D) Units: s.u.@19.6C
TestNo: SW9045D
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/6/2021
RunNo: 122166
SegNo: 3144999
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH
6.4
0
0
0
0
6.4
0
10
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 29 of 42

•
Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TEC!*10LOcI S,IFtc Cuyahoga Falls, Ohio 44223
4rraiyticaf Laboratorfas TEL: [phone] FAX: [phone]
Website: http://www.settek.com
5uMMI
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: R122166
Sample ID: PH 7 CHECK SampType: LCS
Client ID: LCSW
Analyte
TestCode: PH_NPW(450 Units: s.u.@19.6C
Batch ID: R122166 TestNo: SW9045D
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/6/2021
RunNo: 122166
SegNo: 3145006
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH
7.0
7.0
0
101
98.6
101.4
Qualifiers:
B
J
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal)
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 30 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: R122219
Sample ID: LCS-R122219 SampType: LCS
Client ID: LCSS
Analyte
TestCode: Ignitability_S Units: mm/sec
Batch ID: R122219 TestNo: SW1030
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/6/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122219
SegNo: 3145972
%RPD RPDLimit Qual
Ignitability
6.63
7.240
0
91.6
70
130
Sample ID: 21010089-001ADUP SampType: DUP
Client ID: BatchQC Batch ID: R122219
Analyte
TestCode: Ignitability_S Units: mm/sec
TestNo: SW1030
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/6/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122219
SegNo: 3145974
%RPD RPDLimit Qual
Ignitability
nonflammable
0
0
20
Sample ID: 21010090-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec
Client ID: BatchQC Batch ID: R122219
Analyte
Result
TestNo: SW1030
PQL
Prep Date:
Analysis Date: 1/6/2021
SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122219
SegNo: 3145976
%RPD RPDLimit Qual
Ignitability
nonflammable
0
0
20
Sample ID: 21010091-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec
Client ID: Lincolnton Batch ID: R122219
Analyte
Result
TestNo: SW1030
PQL
Prep Date:
Analysis Date: 1/6/2021
SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122219
SegNo: 3145978
%RPD RPDLimit Qual
Ignitability
nonflammable
0
0
20
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 31 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: R122219
Sample ID: 21010091-001ADUP SampType: DUP
Client ID: Lincolnton Batch ID: R122219
Analyte
Result
TestCode: Ignitability_S Units: min/sec
TestNo: SW1030
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/6/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122219
SegNo: 3145978
%RPD RPDLimit Qual
Sample ID: 21010092-001ADUP SampType: DUP
Client ID: BatchQC Batch ID: R122219
Analyte
TestCode: Ignitability_S Units: mm/sec
TestNo: SW1030
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/6/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122219
SegNo: 3145980
%RPD RPDLimit Qual
Ignitability
nonflammable
0
0
20
Sample ID: 21010093-001ADUP SampType: DUP
Client ID: BatchQC Batch ID: R122219
Analyte
Result
TestCode: Ignitability_S Units: mm/sec
TestNo: SW1030
PQL
Prep Date:
Analysis Date: 1/6/2021
SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122219
SegNo: 3145982
%RPD RPDLimit Qual
Ignitability
nonflammable
0
0
20
Sample ID: 21010094-001ADUP SampType: DUP
Client ID: BatchQC Batch ID: R122219
Analyte
Result
TestCode: Ignitability_S Units: mm/sec
TestNo: SW1030
PQL
Prep Date:
Analysis Date: 1/6/2021
SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122219
SegNo: 3145984
%RPD RPDLimit Qual
Ignitability
nonflammable
0
0
20
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 32 of 42

•
Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TEC!*10 LOi,1 5, INC Cuyahoga Falls, Ohio 44223
4rratyticaf Laboratorfas TEL: [phone] FAX: [phone]
Website: http://www.settek.com
5uMMI
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: R122219
Sample ID: 21010095-001ADUP
Client ID: BatchQC
Analyte
SampType: DUP
Batch ID: R122219
Result
TestCode: Ignitability_S Units: mm/sec
TestNo: SW1030
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/6/2021
RunNo: 122219
SegNo: 3145986
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability
nonflammable
0
0
20
Qualifiers:
B
J
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 33 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: R122266
Sample ID: MB-R122266
Client ID: PBW
Analyte
SampType: MBLK
Batch ID: R122266
TestCode: Sulfide,React Units: mg/L
TestNo: SW9034
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/7/2021
RunNo: 122266
SeqNo: 3147220
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive
ND
25.0
Sample ID: LCS-R122266
Client ID: LCSW
Analyte
SampType: LCS
Batch ID: R122266
Result
TestCode: Sulfide,React Units: mg/L
TestNo: SW9034
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/7/2021
RunNo: 122266
SeqNo: 3147221
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive
2880
25.0
3010
0
95.7
85
115
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 34 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: R122266
Sample ID: 21010091-001AMS SampType: MS
Client ID: Lincolnton Batch ID: R122266
Analyte
TestCode: Sulfide,React Units: mg/Kg
TestNo: SW9034
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/7/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122266
SegNo: 3147244
%RPD RPDLimit Qual
Sulfide, Reactive
2980
25.0
3010
40.00
97.7
80
120
Sample ID: 21010091-001AMSD SampType: MSD TestCode: Sulfide,React Units: mg/Kg
Client ID: Lincolnton Batch ID: R122266
Analyte
TestNo: SW9034
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/7/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122266
SegNo: 3147245
%RPD RPDLimit Qual
Sulfide, Reactive
2940
25.0
3010
40.00
96.3
80
120
2980
1.35
30
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 35 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: R122270
Sample ID: Blank
Client ID: PBW
Analyte
SampType: MBLK
Batch ID: R122270
TestCode: Cyanide,Rea Units: mg/L
TestNo: SW9014
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/7/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122270
SegNo: 3147429
%RPD RPDLimit Qual
Cyanide, Reactive
ND
0.495
Sample ID: LCS
Client ID: LCSW
Analyte
SampType: LCS
Batch ID: R122270
TestCode: Cyanide,Rea Units: mg/L
TestNo: SW9014
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/7/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122270
SegNo: 3147430
%RPD RPDLimit Qual
Cyanide, Reactive
9.46
0.495
10.00
0
94.6
85
115
Sample ID: RLCheck
Client ID: BatchQC
Analyte
SampType: RLC
Batch ID: R122270
Result
TestCode: Cyanide,Rea Units: mg/L
TestNo: SW9014
PQL
Prep Date:
Analysis Date: 1/7/2021
SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122270
SegNo: 3147432
%RPD RPDLimit Qual
Cyanide, Reactive
ND
0.485
0.5000
0
77.2
65
135
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 36 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchlD: R122270
Sample ID: 21010091-001AMS SampType: MS
Client ID: Lincolnton Batch ID: R122270
Analyte
TestCode: Cyanide,Rea Units: mg/Kg
TestNo: SW9014
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/7/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122270
SegNo: 3147444
%RPD RPDLimit Qual
Cyanide, Reactive
9.63
0.490
10.00
0
96.3
75
125
Sample ID: 21010091-001AMSD SampType: MSD TestCode: Cyanide,Rea Units: mg/Kg
Client ID: Lincolnton Batch ID: R122270
Analyte
TestNo: SW9014
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/7/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122270
SegNo: 3147445
%RPD RPDLimit Qual
Cyanide, Reactive
9.49
0.485
10.00
0
94.9
75
125
9.628
1.39
10
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 37 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchID: R122312
Sample ID: MB
Client ID: PBS
Analyte
SampType: MBLK
Batch ID: R122312
TestCode: TCLP-SVOC- Units: mg/L
TestNo: SW8321A
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/8/2021
RunNo: 122312
SegNo: 3148878
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D
2,4,5-TP
Surr: 2,4-Dichlorophenylacetic acid
ND
ND
1.03
0.0100
0.0100
1.000
103
70
130
Sample ID: LCS
Client ID: LCSS
Analyte
SampType: LCS
Batch ID: R122312
Result
TestCode: TCLP-SVOC- Units: mg/L
TestNo: SW8321A
PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/8/2021
RunNo: 122312
SegNo: 3148879
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D
2,4,5-TP
Surr: 2,4-Dichlorophenylacetic acid
0.357
0.304
3.01
0.0100
0.0100
0.3000
0.3000
3.000
0
0
119 60.5 141
102 68.3 144
100 70 130
Sample ID: LCSD
Client ID: LCSSO2
Analyte
SampType: LCSD
Batch ID: R122312
Result
TestCode: TCLP-SVOC- Units: mg/L
TestNo: SW8321A
PQL
SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/8/2021
RunNo: 122312
SegNo: 3148880
%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D
2,4,5-TP
Surr: 2,4-Dichlorophenylacetic acid
0.287
0.249
2.44
0.0100
0.0100
0.3000
0.3000
3.000
0
0
95.6
82.9
81.5
60.5
68.3
70
141
144
130
0.3571
0.3045
21.8
20.2
0
30
30
0
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 38 of 42

•
5uMMI
EHMIROhl MENtALTEC„NOL4 1 S.IF#C
4rra/yOcaf Laboralorfes TEL: [phone] FAX [phone]
Website: http://www.settek.com
SummitEnvironmentalTechnologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
QC SUMMARY REPORT
WO#: 21010091
12-Jan-21
Client:
Project:
Synagro
Lincolnton
BatchID: R122312
Sample ID: 21010089-001AMS SampType: MS
Client ID: BatchQC Batch ID: R122312
Analyte
TestCode: TCLP-SVOC- Units: mg/L
TestNo: SW8321A
Result PQL SPK value SPK Ref Val
Prep Date:
Analysis Date: 1/8/2021
%REC LowLimit HighLimit RPD Ref Val
RunNo: 122312
SegNo: 3148881
%RPD RPDLimit Qual
2,4-D
2,4,5-TP
Surr: 2,4-Dichlorophenylacetic acid
16.9
14.4
143
0.500
0.500
15.00
15.00
150.0
0
0
112 60.5 141
96.2 68.3 144
95.0 70 130
Sample ID: 21010089-001AMSD SampType: MSD TestCode: TCLP-SVOC- Units: mg/L
Client ID: BatchQC Batch ID: R122312
Analyte
Result
TestNo: SW8321A
Prep Date:
Analysis Date: 1/8/2021
PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val
RunNo: 122312
SegNo: 3148882
%RPD RPDLimit Qual
2,4-D
2,4,5-TP
Surr: 2,4-Dichlorophenylacetic acid
17.9
15.4
151
0.500
0.500
15.00
15.00
150.0
0
0
119
102
101
60.5
68.3
70
141
144
130
16.87
14.43
5.67
6.28
0
30
30
0
Qualifiers: B
ND
R
Analyte detected in the associated Method Blank
Analyte detected below quantitation limits
Not Detected
RPD outside accepted recovery limits
E
M
P
RL
Value above quantitation range
Manual Integration used to determine area response
Second column confirmation exceeds
Reporting Detection Limit
H
MC
PL
S
Holding times for preparation or anal}
Value is below Minimum Compound
Permit Limit
Spike Recovery outside accepted reco
Original
Page 39 of 42

-171° 017 abed
DC-QAODC336 R. Ai
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Analysis Request / Chain of Custody r.s...chgl
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Page 1 of 2

115/2021 Summt Environmental Technologies Mail - Re° Send data from MFP12072737 0110512021 12:24
SUMMIT
_r.R:e7IKr„r5;rv:i.cG[1ii
4,1.1,1110:•1trr
Re: Send data from MFP12072737 01105/2021 12:24
1 message
Jennifer Woolf [e-mail],
Alex Fox <afox©a synagro.com> Tue, Jan 5, 2021 at 1:01 PM
To: Jennifer Woolf ‹jwoolffa settek.com>
They are all innNC and yes that's part of Tclip.
Thanks,
Alex Fox
TSS Western NC
336-103-8681
afoxca synagro.corn
On Jan 5, 2021, at 12:39 PM, Jennifer Woolf <jwoolfci settek.com> wrote:
Could you resend them with the state included in the Project Address box? Also, cculd you indicate that
the Pest/Herb are TCLP also.
thanks'
jen
N
Jennifer Woolf
Project Manager c\l
JWoolft@settek,com cy
3310 Win St. a_
Cuyahoga Falls, Ohio 44223
Summit Environmental Technologies, Inc.
TEL: [phone]
FAX: [phone]
http:f /www, s ette k . co m
PLEASE NOTE; This email, including any attachments, may include privileged and/or confidential
that may only be reviewed by the intended recipient. Any distribution or use of this
communication by anyone other than the intended recipient is strictly prohibited and may be
unlawful. if this email has been received in error, please notify the sender immediately by
replying to this message and delete the contents of this email from your files.
Please let us know how we are doing by participating in an online survey at
https://www.surveymonkey.corniri5BC3DYM.
On Tue, Jan 5, 2021 at 12:31 PM Alex Fox safox a+~"tsynagro.com> wrote:
Here am the COC.
You can take Will, Marshall and Melvin of the list they no longer work for Synagro
Thanks,
Alex Fax
TSS Western NC
336-703-8681
afoxrsynagro.com
https:f1mail.googlie.camrmalvu/o?ifca79f59241 &view=ptasearch=elApermthid=thread-%3418Baosa831827375652%7Cmsg-f°k3A166B0747515158,.. 1/2
Page 41 of 42

it
SUMMI T Summit Environmental Technologies, Inc.
3310 Win St.
MORON MENTAL TECHNOLOGa S, INC Cuyahoga Falls, Ohio 44223
Arrafyacaf Laboratorlas TEL: [phone] FAX. [phone]
Website: http://www.settek.com
Sample Log -In Check List
Client Name: SYN-NC-27028
Work Order Number: 21010091
RcptNo: 1
Logged by: Jesseca E. Westfall 1/5/2021 10:15:00 AM
Completed By: Jesseca E. Westfall 1/5/2021 4:19:02 PM
Reviewed By: Jennifer Woolf 1/5/2021 4:30:44 PM
Chain of Custody
1. Is Chain of Custody complete?
2. How was the sample delivered?
Loci In
3. Coolers are present?
Yes ❑d
FedEx
Yes ❑d
4. Shipping container/cooler in good condition? Yes d❑
Custody seals intact on shipping container/cooler? Yes ❑
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d
6. Were all samples received at a temperature of >0° C to 6.0°C
No ❑ Not Present ❑
No ❑ NA ❑
No ❑
No ❑
No ❑
Yes ❑d No ❑
7. Sample(s) in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
g. Are samples (except VOA and ONG) properly preserved? Yes ❑d No ❑
10. Was preservative added to bottles? Yes ❑ No ❑d
Not Present V
NA ❑
NA ❑
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials V
12. Were any sample containers received broken? Yes ❑ No ❑d
13. Does paperwork match bottle labels? Yes ❑d No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody? Yes ❑d No
15. Is it clear what analyses were requested? Yes ❑d No
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes ❑d No
Yes ❑
No ❑
NA V
Person Notified:
By Whom:
Regarding:
Client Instructions:
Date: J
Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
18. Additional remarks:
COC emailed
Cooler Information
Cooler No
Temp °C
Condition
Seal Intact
Seal No
Seal Date
Signed By
1
3.6
Good
Not Present
Page 42 of 42

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lincolnton WWTP WQ Permit Number: WQ 0016247
WWTP Name: Lihcolnton WW TP NPDES Number: NC 0025496
Monitoring Period: From 01/01/21 To 03/31/2021
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T,1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt, 4/D (No Prior Test)
Alt. 5/Process to Further Reduce Pathogens - Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Therrnophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaerobic Digestion
Air Drying
Composting
Aerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitorinf data:
Parameter
Allowable Level in Sludge
Pathogen Density
Minimum Geo. Mean Maximum Units
No. of
Excee-
dences
Frequency
of
Analysis
Sample
Type
Analytical
Technique
Fecal
Coliform
2x10 to the 6th
power per gram
of total solids
MPN
CFU
1
MPN/g
15181
17067
19636
CFU/g
0
Quarterly
Grab
9222D
SM
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
bacteria (in
lieu of fecal
coliform)
3 MPN per 4 grams total
solids (dry weight)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction) X
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt. 2
(40-day bench)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench)
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T,1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an
_A explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Donald Burkey Jr. WWTP Superintendent
itoberbikeassm kktilitinQipectu
P parer Name and Titl (type or print)
Signature of Prepar r*
2-9-2022
Land Applier Name and Title (if applicable) (type or print)
Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

PaceAnalytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Lincolnton
Lot Number:WC03084
Date Completed:03/15/2021
03/15/2021 4:26 PM
Approved and released by:
Project Manager II: Lucas Odom
A413
ANSI National Accreditation Board
ACCREDITED
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 13

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653
NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: WC03084
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly ShealyEnvironmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 13

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: WC03084
Sample Number Sample ID
Matrix Date Sampled Date Received
001 Fecals Solid 03/03/2021 0930 03/03/2021
002 Fecals Solid 03/03/2021 0930 03/03/2021
003 Fecals Solid 03/03/2021 0930 03/03/2021
004 Fecals Solid 03/03/2021 0930 03/03/2021
005 Fecals Solid 03/03/2021 0930 03/03/2021
006 Fecals Solid 03/03/2021 0930 03/03/2021
007 Fecals Solid 03/03/2021 0930 03/03/2021
(7 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 13

Inorganic non-metals
Client: Synagro Laboratory ID: WC03084-001
Description: Fecals Matrix: Solid
Date Sampled:03/03/2021 0930 % Solids: 5.59 03/04/2021 0033
Date Received:03/03/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 03/04/2021 2131 GDC 03/03/2021 2140
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <17885 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 13

Inorganic non-metals
Client: Synagro Laboratory ID: WC03084-002
Description: Fecals Matrix: Solid
Date Sampled:03/03/2021 0930 % Solids: 6.59 03/04/2021 0033
Date Received:03/03/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 03/04/2021 2131 GDC 03/03/2021 2140
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <15181 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5of13

Inorganic non-metals
Client: Synagro Laboratory ID: WC03084-003
Description: Fecals Matrix: Solid
Date Sampled:03/03/2021 0930 % Solids: 5.40 03/04/2021 0033
Date Received:03/03/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 03/04/2021 2131 GDC 03/03/2021 2140
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <18509 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 13

Inorganic non-metals
Client: Synagro Laboratory ID: WC03084-004
Description: Fecals Matrix: Solid
Date Sampled:03/03/2021 0930 % Solids: 5.09 03/04/2021 0033
Date Received:03/03/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 03/04/2021 2131 GDC 03/03/2021 2140
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <19636 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 13

Inorganic non-metals
Client: Synagro Laboratory ID: WC03084-005
Description: Fecals Matrix: Solid
Date Sampled:03/03/2021 0930 % Solids: 6.51 03/04/2021 0033
Date Received:03/03/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 03/04/2021 2131 GDC 03/03/2021 2140
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <15349 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 13

Inorganic non-metals
Client: Synagro Laboratory ID: WC03084-006
Description: Fecals Matrix: Solid
Date Sampled:03/03/2021 0930 % Solids: 5.71 03/04/2021 0033
Date Received:03/03/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 03/04/2021 2131 GDC 03/03/2021 2140
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <17515 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 13

Inorganic non-metals
Client: Synagro Laboratory ID: WC03084-007
Description: Fecals Matrix: Solid
Date Sampled:03/03/2021 0930 % Solids: 6.29 03/04/2021 0033
Date Received:03/03/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 03/04/2021 2131 GDC 03/03/2021 2140
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <15899 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 13

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 13

PACE ANALYTICAL SERVICES, LLC
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Chaim .of Custody Record
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 13

PACE ANALYTICAL SERVICES, LLC
Client: 8ynagrna
pli St-ip ID: NA Chlorine Strip ID: NA
Original ter erature upon receipt i Derived (Corrected) 5entpe_ature upon rzccipt
2.$ j .g ac NA j N . oC NP, "No".. ac NA +NA
Jv aiod �J]Ternperatare Blank OA soinse Bottle; TR. Caen LD: 6
Tedlod of corol:Lo : Q Wet Ice 0 Ica Packs ❑ Dray Ice ❑ Noon
❑Y:s
Yes
Yes
Yes
�No
DNu
EINn
No
S: mpl es Receipt Checklist. (SRC} (mum 3sc-i.9I
Issuinc Authn.ri Ly_ Pace ENV-'u5�COL
Sample Receipt C"het;1dist (SRC)
C oMer lr_spec[e1 by /t.at., IRG2 6 klt1J,J21
Lot *I: WCO34 3
tlevIsexh9,r29j2Q20
Page L of 1
Clint UPS rmtirx 71 °thee!
I. Wert custody seals present on the cooler?
2. If a '_Istxad); Nulls p: es ear, were thy° intact and I niaroltcn7
Tested by: NA
6Solid Snapu>p 1D
LIB Gun Ccrrec'ion Factor e
204175
aC
1711.4A 3_ If t tllper al tot: of any cooler excooded 6.IrC, was; Project manager NotuTpd7
Fh I was Notified by: phzne f Thai] i face -to -Cued {e lock: rn,n),
IZIT1A 4. Is tFc ci mnieiral packingl3p atiachcrf to this fortre
ryes
® Yes
No
0 No
Yee I; lea
Yes. No
EJYes ❑Nu.
Yes-11Na
Yes ❑ No
y,QYes (JNo
El Yes r]No
Yes, LI No
Yusl
❑ 5fcs
❑ hlo
5. Were proper custody procecures (relinquishe ra eciv .) followed?
6: Were sartit:1c la listed on the CQC7
7: Were stanpL TI7& Jilted
on all 9e;nple cn€3tainera?
>3: Was collection date & time [istcd on the COC?
9.
Was craIlcction date & _irn0.[isLed on al[ maniple. containers?
16_ Did al[ c01i ainer label inFormadon (ID; AV title) awe with the COC?
11. We o tests to be performed listed an the C'?
12. Ca [d all s.et rplcs arrive in the proper cnnr&r.ers for each test and/or in good oored:tion
(unbroken, [icis on, ctcr
I;#_ Was adequate awn* volume mailable?
❑d N?k
14. Were ail samples received with]] V, the holklirtg tune or 4S hours, wriichin-er comes First?
15. Were any lam pies containers in issing/exetS,s (oi rcic one}Lan ples Not listed on .0 0C?
16. For 'VOA tuad #R.1:iK-175 samples, were bubbles present :"}:aa-si e- Cit"or6rrm bi diameter)
ill any of the VOA Vials?
DNA
O NA
® 1\ A
El Yes
Q Yes
❑ No
.J No
NA
1! 7_ }krerC a1[ DROin ieleilinutrient sar71pTe xc received at a }RH ref < 27
T$, Were al[ cya_rii1c samples received et a pH 12 aral sulfide sarriples received to a .I Ill', 9?
19_ Wcru ail. applicable NI-13 exain[d4Jphs nabr6 5.1i .3 (< oim fL) sarnp*G5 free or
residual chlorine?
20. Ware client terlarksirequets (L . requcgted tli lu ians, U.'/MS") elmi:gnatirma,
oorr+cct[y transcribed from tiro COC into the comment section in LAI' ?
21. Was the uote number listal on the container ittlx17 If arcs, ()Lititz rl
Sam.* k'reser Lion (Must he completed for any santpio(e) incorrectly preserved or with Fi Lpaue.)
3ampI t) a' were reuu [veil incorrectly preserved and were adjusted accordingly
' in sample receiving with NA mL &ci.rcle ono; 1-25O4, HNO3, HC], NaOH usng SR NA
T°r_se of preservatitui NA _ IFMoroi elan 4r pJ-eservativc is needed., piCazu note in : le com:nctits below_
Sampler) NAwere received wit bubbles.> i rnm in diameter_
anr:p]as(s) NA were received with TRC _} 0.5 Inrefir (1f till 9 is Ito) arid Wcrc
adjusted accordingly tr_ sample receiving with FA 1ki ii thiosuifate (N+Tta2S]O;) with Shealy ID:
SR larrrcodc labels applied by; JI('*
Commeni8:
onto: cill'3a021
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 13

Technician
quarter year ° e__
SM 2540 B-2011, 2540 D -2011
NC0025496
All weighings are done in grams
MiSfik.CAINir-:1.Pateagnir' 'A"'''S*Vg? VIVA 400i • - •
tobtor, to, --
Time Collected
Date Collected
Date / Time In
Date / Time Out
Total Wet Wgt
Wet Sludge Wgt
(103-105°C) Dried
Wgt
Dry Solids Wgt
% Solids
AVG % Solids •
Time In/Out
(103-105°C) Dried
Wgt
550°C Wt
Volatile Solids Wgt
% Volatile Solids
AVG
% Volatile Solids
% TS DAF =
% TS Sludge =
/4/62 ci 7
7 ao
/113W
0 -2 0
% Total Solids =
% Volatile Solids =
% Reduction =
u'r 3 7
0 '12-r
r). 0 ?fj
a_3
% VS DAF =
Y
% VS Sludge =
c,. J...4.-Z;4L ,6, 8
Dry Solids Wgt
Wet Solids Wgt
(Volatile Solids Wgt)
Dried Solids Wgt
(VS DAF - VS Sludge)
VS DAF - (VS DAF)(VS Sludge)
X 100
X 100
X 100

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lincolnton WWTP WQ Permit Number: WQ 0016247
WWTP Name: Lincolnton WWTP NPDES Number: NC 0025496
Monitoring Period: From 04/01/21 To 06/30/2021
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (A1k Treatment) Alt, 3/C (Prior Testing)
Alt. 4/D (No Prior Test) AIt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (C ass A or Class B) complete the following monitorinii data:
Parameter
Allowable Level in Sludge
Pathogen Density
Minimum ' Geo. Mean Maximum Units
No. of
Excee-
dences
Frequency
of
Analysis
Sample
Type
Analytical
Technique
Fecal
Coliform
2x10 to the 0
power per gram
of total solids
MPN
CFU
MPN/g
35,747
54,087
104,315
CFU/g
0
Quarterly
Grab
9222D
SM
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
bacteria (in
lieu of fecal
coliform)
3 MPN per 4 grams total
solids (dry weight)
Vector Attraction Reduction (40 CFR503.33/1SA NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction) X
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/A1t. 2
(40-day bench)
Option/Alt, 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench)
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
No vector attraction reduction alternatives were performed
"2 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met,"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1 106 and the vector attraction
reduction requirement in 40 CFRS03.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met, I am aware that there are significant penalties for false certification including fine and imprisonment."
Donald Burkey Jr. WVVTP Superintendent
xRuberkBeaxaox uttittautivaxx
Pita rer Nam Band � if e( type or print) Land Applier Name and Title (if applicable) (type or print)
2-9-2022
Signature of Preparer* Date Signature of Land Applier (if applicable) Date

PaceAnalytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Lincolnton
Lot Number:WD06050
Date Completed:04/15/2021
04/16/2021 9:16 AM
Approved and released by:
Project Manager II: Lucas Odom
A413
ANSI National Accreditation Board
ACCREDITED
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 16

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653
NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: WD06050
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix, the initial sample amount used for the following sample deviated from the standard
procedure 3: WD06050-001. The LOQ has been adjusted accordingly.
Inorganic Non -Metals
The following sample was diluted due to the nature of the sample matrix: WD06050-001. The LOQ has
been elevated to reflect the dilution.
Geometric Mean
54,087
Pace Analytical Services, LLC (formerly ShealyEnvironmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 16

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: WD06050
Sample Number Sample ID
Matrix Date Sampled Date Received
001 Lincolnton Solid 04/06/2021 1045 04/06/2021
002 L 1-7 Solid 04/06/2021 1045 04/06/2021
003 L 1-7 Solid 04/06/2021 1045 04/06/2021
004 L 1-7 Solid 04/06/2021 1045 04/06/2021
005 L 1-7 Solid 04/06/2021 1045 04/06/2021
006 L 1-7 Solid 04/06/2021 1045 04/06/2021
007 L 1-7 Solid 04/06/2021 1045 04/06/2021
008 L 1-7 Solid 04/06/2021 1045 04/06/2021
(8 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 16

Inorganic non-metals
Client: Synagro
Description: Lincolnton
Date Sampled:04/06/2021 1045
Date Received:04/06/2021
Laboratory ID: WD06050-001
Matrix: Solid
% Solids: 4.53 04/06/2021 2311
Run Prep Method
1 350.1
1
1
1
1
1 351.4
Analytical Method
(Ammonia - N) 350.1
(Nitrate - N ) 9056A
(Nitrite - N ) 9056A
(Phosphorus) 365.1
(Soil pH meas) 9045D
(TKN) 351.2
Dilution
25
5
1
25
1
2
Analysis Date Analyst
04/07/20211206 KFE
04/08/2021 1249 AMR
04/08/2021 1017 AMR
04/12/2021 1614 DMA
04/07/20211915 NBW
04/09/20211731 MSG
Batch
88135
88521
88522
04/10/2021 1429 88601
88303
04/07/2021 1700 88277
Prep Date
Parameter
CAS Analytical
Number Method Result Q LOQ
DL
Units Run
Ammonia - N (gas diffusion)
Nitrate - N (soluble)
Nitrite - N (soluble)
Phosphorus
Soil pH measured in water @ 21.5 ° C
TKN
7723-14-0
350.1
9056A
9056A
365.1
9045D
351.2
12000
51
9.3
14000
6.8
34000
550
J 55
4.4
2800
290
11
2.2
550
1100 1100
mg/kg 1
mg/kg 1
mg/kg 1
mg/kg 1
su 1
mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
W = Reported on wet weight basis
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 16

CVAA
Client: Synagro Laboratory ID: WD06050-001
Description: Lincolnton Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 4.53 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method
1 7471B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
7471B 1 04/09/2021 1821 CMS2 04/09/2021 1308 88366
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Mercury
7439-97-6
7471B ND 1.6 0.39 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5of16

ICP-AES
Client:Synagro Laboratory ID:WD06050-001
Description: Lincolnton Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 4.53 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method
1 3050B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
6010D 1 04/08/2021 1402 JMH 04/07/2021 1012 88194
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
7429-90-5 6010D 11000 140 51 mg/kg 1
7440-38-2 6010D 4.5 J 5.1 1.7 mg/kg 1
7440-43-9 6010D ND 1.7 0.43 mg/kg 1
7440-70-2 6010D 5400 1700 210 mg/kg 1
7440-47-3 6010D 41 3.4 0.85 mg/kg 1
7440-50-8 6010D 230 3.4 1.5 mg/kg 1
7439-89-6 6010D 10000 34 15 mg/kg 1
7439-92-1 6010D 8.3 3.4 1.5 mg/kg 1
7439-95-4 6010D 2700 1700 210 mg/kg 1
7439-96-5 6010D 360 5.1 2.0 mg/kg 1
7439-98-7 6010D ND 14 3.4 mg/kg 1
7440-02-0 6010D 8.2 J 14 3.6 mg/kg 1
7440-09-7 6010D 4000 B 1700 210 mg/kg 1
7782-49-2 6010D ND 6.8 2.8 mg/kg 1
7440-23-5 6010D 1200 J 1700 210 mg/kg 1
7440-66-6 6010D 130 17 4.2 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-002
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.62 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 38123 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-003
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.23 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <44928 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-004
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.71 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 36877 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-005
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 3.09 04/08/2021 0019
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 64763 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-006
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.25 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 88774 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-007
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.88 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 104315 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WD06050-008
Description: L 1-7 Matrix: Solid
Date Sampled:04/06/2021 1045 % Solids: 2.80 04/06/2021 2311
Date Received:04/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 04/07/2021 2012 MOM 04/06/2021 2007
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 35747 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 16

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 16

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ace.4r2Ofical
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Moms of receipt: 1 Nee.
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S. Were sample 113s Iisteel, r- .he COC?
4. Is the commercial tzsLtr
7.
101Cre sample ILIs listed do all sa niplc containers?
col]eci1nn date Se t
9. \VW Cotie,ziim date
l0. Did al[cut=lau]er label
I, Were tests 10 be perfd
12. Did a[i rartrpl+ s arrive
(tinbrcakcn, lids on, etc.)?
Fine listed of t11;. COC?
F e listed on ni: triple container
riForniation ([D, r ate, runt) ag ee wiCh ;etc COC.?
listed €tri the COC?
the proper rontai itas For each test aadfor its l4od Condit[ rfi
13. Was mkt oath sarttp]a
14, Were a[i samples mod
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 16

technician
SM 2540 B-2011, 2540 0 -2011 NC0025496 All weighings are done in grams
rr)
Time Collected
Date Collected
Date / Time In
Date / Time Out
Total Wet Wgt
Dish
Wet Sludge Wgt
(103-105°C) Dried
Wgt
Dish
Dry Solids Wgt
% Solids
AVG % Solids
Time In/Out
(103-105°C) Dried
Wgt
411
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Volatile Solids Wgt
% Volatile Solids
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% Volatile Solids
% TS DAF =
t 1
%TS Sludge=
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% Volatile Solids
% Reduction =
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X 100
X 100
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of .L.imolnton WWTP WQ Permit Number: WQ 0016247
WWTP Name: Lincolnton WWTP NPDES Number: NC 0025496
Monitoring Period: From 07/01/21 To 09/30/2021
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1 /A (time/temp) Alt. 2B (A1k Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thennophitic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaerobic Digestion
Air Drying
Composting Aerobic Digestion
If applicable to alternative performed (C ass A or Class B) complete the followine monitorin! data:
Parameter
I Allowable Level in Sludge
Pathogen Density
Minimum Geo. Mean Maximum Units
No. of
Excee-
dences
Frequency
of
Analysis
Sample
Type
Analytical
Technique
Fecal
Coliform
2x10 to the 6'"
power per gram
of total solids
MPN
CFU
MPN/g
CFU/g
1000 MPN per gram of
total solids (dry weight)
16,552
238,992
3,161,366
MPN/g
2
Quarterly
Grab
9222DSM
Salmonella
bacteria (in
lieu of fecal
coliform)
3 MPN per 4 grams total
solids (dry weight)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/AIt. 1
(VS reduction) X
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt. 2
(40-day bench)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench)
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying — Unstable)
No vector attraction reduction alternatives were performed
"1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment"
Donald 8urkey Jr. WWI? Superintendent
>IVIRINXI4WIRM Ut11iftx912'gciti4
>7rarerName and Title ( type or print) Land Applier Name and Title (if applicable) (type or print)
ILO—V.)4
Signature of Pre ararr
g P
2-9-2022
Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Date

PaceAnalytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Lincolnton
Lot Number:WG06038
Date Completed:07/16/2021
Project Manager:Lucas Odom
07/16/2021 5:10 PM
Approved and released by:
Project Manager II: Kathy E. Smith
A413
ANSI National Accreditation Board
ACCREDITED
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 16

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653
NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: WG06038
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 16

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: WG06038
Sample Number Sample ID
Matrix Date Sampled Date Received
001 Lincolnton Solid 07/06/20210945 07/06/2021
002 L 1 Solid 07/06/2021 0950 07/06/2021
003 L 2 Solid 07/06/2021 0950 07/06/2021
004 L 3 Solid 07/06/2021 0950 07/06/2021
005 L 4 Solid 07/06/2021 0950 07/06/2021
006 L 5 Solid 07/06/2021 0950 07/06/2021
007 L 6 Solid 07/06/2021 0950 07/06/2021
008 L 7 Solid 07/06/2021 0950 07/06/2021
(8 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3of16

Inorganic non-metals
Client: Synagro
Description: Lincolnton
Date Sampled:07/06/2021 0945
Date Received:07/06/2021
Laboratory ID: WG06038-001
Matrix: Solid
% Solids: 2.80 07/07/2021 0008
Run Prep Method
1 350.1
1
1
1
1
1 351.4
Analytical Method
(Ammonia - N) 350.1
(Nitrate - N ) 9056A
(Nitrite - N ) 9056A
(Phosphorus) 365.1
(Soil pH meas) 9045D
(TKN) 351.2
Dilution Analysis Date Analyst Prep Date Batch
1 07/07/20211157 KFE 97967
1 07/14/2021 1043 AMR 98964
1 07/14/2021 1043 AMR 98966
5 07/08/2021 1357 DMA 07/07/2021 1615 98126
1 07/11/20211753 NBW 98501
1 07/09/2021 1227 DMA 07/07/2021 1535 98116
Parameter
CAS Analytical
Number Method
Result Q LOQ
DL
Units Run
Ammonia - N (gas diffusion)
Nitrate - N (soluble)
Nitrite - N (soluble)
Phosphorus
Soil pH measured in water @ 22.4 ° C
TKN
7723-14-0
350.1
9056A
9056A
365.1
9045D
351.2
1300 36
2100 18
8.0 7.2
7200 S 890
5.8
17000 S 1800
19
3.6
3.6
180
890
mg/kg 1
mg/kg 1
mg/kg 1
mg/kg 1
su 1
mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
W = Reported on wet weight basis
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 16

CVAA
Client: Synagro Laboratory ID: WG06038-001
Description: Lincolnton Matrix: Solid
Date Sampled:07/06/2021 0945 % Solids: 2.80 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method
1 7471B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
7471B 1 07/15/2021 1453 CMS2 07/14/2021 1532 98385
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Mercury
7439-97-6
7471B ND 2.8 0.68 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5of16

ICP-AES
Client: Synagro Laboratory ID: WG06038-001
Description: Lincolnton Matrix: Solid
Date Sampled:07/06/2021 0945 % Solids: 2.80 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method
1 3050B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
6010D 1 07/08/2021 1116 JMH 07/08/2021 0122 98017
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
7429-90-5 6010D 8800 240 89 mg/kg 1
7440-38-2 6010D 3.8 J 8.9 3.0 mg/kg 1
7440-43-9 6010D ND 3.0 0.74 mg/kg 1
7440-70-2 6010D 3800 3000 370 mg/kg 1
7440-47-3 6010D 29 5.9 1.5 mg/kg 1
7440-50-8 6010D 180 5.9 2.7 mg/kg 1
7439-89-6 6010D 6500 59 27 mg/kg 1
7439-92-1 6010D 5.0 J 5.9 2.7 mg/kg 1
7439-95-4 6010D 1500 J 3000 370 mg/kg 1
7439-96-5 6010D 230 8.9 3.5 mg/kg 1
7439-98-7 6010D ND 24 5.9 mg/kg 1
7440-02-0 6010D ND 24 6.2 mg/kg 1
7440-09-7 6010D 1900 J 3000 370 mg/kg 1
7782-49-2 6010D ND 12 4.8 mg/kg 1
7440-23-5 6010D 2200 J 3000 370 mg/kg 1
7440-66-6 6010D 87 30 7.4 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-002
Description: L 1 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 1.37 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 438597 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-003
Description: L 2 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 1.30 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 615195 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-004
Description: L 3 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 2.70 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 259269 * 20
col/g 1
Footnote(s): *Fecal Coliform (MF) - results estimated
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank
N = Recovery is out of criteria
W = Reported on wet weight basis
E = Quantitation of compound exceeded the calibration range DL = Detection Limit
P = The RPD between two GC columns exceeds 40%
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-005
Description: L 4 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 2.05 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 146384 * 20
col/g 1
Footnote(s): *Fecal Coliform (MF) - results estimated
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank
N = Recovery is out of criteria
W = Reported on wet weight basis
E = Quantitation of compound exceeded the calibration range DL = Detection Limit
P = The RPD between two GC columns exceeds 40%
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-006
Description: L 5 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 2.41 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 83108 * 20
col/g 1
Footnote(s): *Fecal Coliform (MF) - results estimated
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank
N = Recovery is out of criteria
W = Reported on wet weight basis
E = Quantitation of compound exceeded the calibration range DL = Detection Limit
P = The RPD between two GC columns exceeds 40%
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-007
Description: L 6 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 1.22 07/08/2021 0145
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 3161366 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WG06038-008
Description: L 7 Matrix: Solid
Date Sampled:07/06/2021 0950 % Solids: 1.62 07/07/2021 0008
Date Received:07/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 07/07/2021 2153 NBW 07/06/2021 2232
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 5141111 * 20
col/g 1
Footnote(s): *Fecal Coliform (MF) - duplicates outside 25% RPD
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank
N = Recovery is out of criteria
W = Reported on wet weight basis
E = Quantitation of compound exceeded the calibration range DL = Detection Limit
P = The RPD between two GC columns exceeds 40%
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 16

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 16

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PACE ANALYTICAL SERVICES, LLC
t Jient:: SYNACke4
Means,ofreceip[; ✓
Lit
LI■IStl I itall Ltd
Samples Receipt Medium(SRC' IM1 JU1 - 5)
rssui i A.uthar•ty_Pace t 1V-INCCL
Simple Receipt Checklist (SR
coo:cr i35. 'too by/tie: JSV a+ p7.+{PFn'2t' 1
Pace E:P5
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▪ J ▪ t custi lv soak weir resent, were th • in act a un:
pH Strip ID: N" Chlorine drip ID; NA
rrgival temperature upno receipt 1 Deo ived ( ecled) temperature upon, remipr
2.1 j2.i ac NA oc t�lli 1N4 <' 11A 1 NA oc
Meths : f'1'emperuture Blank ra"..lainst Bottle& fRGw, I�j _ iRciu
Method of cor,Lana: Wot lee ❑ Ica Pak e;
L� Dry Ice 0 Non
Revised:S/29/20 0
Page 1 of 1
Lot 4; }'(ii:6C38
0 Yes
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3_ if temperature Dram+ ceder CkcueiJe t 6_0° , was Pruj
?NI was Notified by; phone? t inst;I1 race -to -face (eircl
4. Is tho buiumcruia1 courier's packing slip attached to dr-
5. Were proper custody proCekres (relinqu isheel'nxei4
6. Were ample IDa listed on the COC?
7. Were sample IDs lisped on a1l wimple containers?
8_ WR.r. ooCiectior. dare & erne, listed cm the C.[)C?
9. Was collection date it time listed rrh a]] apmplc con ih
10. Did all c.un[uiner EakeI infarrnut ,n (ID, date, flick) ul,
11 _ Were tleols to be rid -formed ned listed on fire COC'?
12. Did all sanip[ s arrive in the ;5'0per containers for eat
(unbroken, lids on, a n_ 1
den?
eated by: x t
%Solid Snap -Cup JD: 21-1423
Correcti0r. Pac:ur: 0
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Sample Preservation
•Sarrrplefs) a.x
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Time of preservation M
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tear and?or in good condition
I.;. Was [tclegnatc sample volume. available'?
114. 1'fere all Sam 10s rrxr ived within IA 11,n baldin: time o
15_ Wcrc any, xarKiles containers 1yi5singWexcess (circle nor
16. For VOA and R.SK-]75 samples, weNbuhitlespresent
in any ofthc VOA vials,
NA i 7, Were all DROlmstatsfnutdelnt samples receiiipd at a p
l8. Were all cyanide samples received at a p[ [ > 12 and su!
Werev11 ]wi- /1"rCNryanicep enoli025.]/
nesiGtral chlorine?
20. Were client reirtarksfrcgcesls (Le, requested dilutions,
co:reedy transcribed from the COC into the c i:untuent secti
21, Wa$ the ;coke. nu .: ". od , t the container tubcl? If
([tit ust be ,:cahkp]etel for any sarnple.(s) incorrectly presermecl o
arts pies) NA
tiamplox s) M. were received with. 'MC 1
adjusted accordingly in sample receiving with gadilim thiosuIIitc (Na2£2O3) with Saca
were received incorrectly pre
nnL tat circle one; H2SO4, HNU3, HCI, NaOFI using
. if mare tar one p, esea-vative is needed, please not
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 16

technician
NC0025496
uuarter / Year 3 /d
9z_ D z- 1
-2011, 2540 D -2011
All weighings are done in grams
1 }� �Itd-17►�� Y ~ tF
1 h+ ���M�lye
...X
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Time Collected
° 6
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/// 0
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7-24-24
2_zfai
7"2-/ ` 2 1
Date /Time In
)- / Z / / )3 6
Date / Time Out
()_ ZZ - 21 / ®6 60
Total Wet Wgt
/Q ®J` !I
)5 2--z6
1v2 `/, 335 15-
/
,
Dish
l( if ci763
S, 01/�
(r 62_22--
Wet Sludge Wgt
9 7 z 6
59,
6, C 2-3/
2 / 90‘3
(103-105°C) Dried
Wgt
_. /
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(( _
ff! )370
5-0 J r.l 7
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% Total Solids =
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Wet Solids Wgt
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X 100
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X 100

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Lincolnton WWII) WQ Permit Number: WQ 0016247
WWTP Name: Lincolnton WWTP NPDESNumber: NC 0025496
Monitoring Period: From 10/01/21 To 12/31/21
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp)
Alt. 4/D (No Prior Test)
Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying . Heat Treatment Therinophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the followine monitoring data:
Air Drying Composting _T Aerobic Digestion
Parameter
Allowable Level in Sludge
Pathogen Density
Minimum Geo. Mean Maximum Units
No. of
Excee-
dences
Frequency
of
Analysis
Sample
Type
Analytical
Technique
Fecal
Coliform
2x10to the 6th
power per gram
of total solids
MPN
CFU
MPN/g
13,219
14,979
17,595
CFU/g
0
Quarterly
Grab
9222D
SM
1000 MPN per gram of
total solids (dry weight)
MPN/g
Salmonella
bacteria (in
lieu of fecal
coliform)
3 MPN per 4 grams total
solids (diy weight)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt, 1
(VS reduction) X
Option/Alt. 5
{14-Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt. 2
(40-day bench)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3
(30-day bench)
Option/Alt. 7
(Drying — Stable)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying —Unstable) _
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCACO2T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Donald Burkey Jr. WWTP Superintendent
>RobarocRagiaon: liitiat!t�(Mt=
rerName end title type or print)
3ignatnre of Preparer
Land Applier Name and Title {if applicable) (type or print)
2-9-2022
Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T,1102 (26)
Date

PaceAnalytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Lincolnton
Lot Number:WK02050
Date Completed:11/21/2021
11/22/2021 11:20 AM
Approved and released by:
Project Manager II: Lucas Odom
A413
ANSI National Accreditation Board
ACCREDITED
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 16

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653
NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: WK02050
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the low percent solids, the following sample has an initial weight that is 3x greater than standard
procedure: WK02050-001. The LOQ has been changed to reflect the additional mass.
Pace Analytical Services, LLC (formerly ShealyEnvironmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 16

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Synagro
Lot Number: WK02050
Sample Number Sample ID
Matrix Date Sampled Date Received
001 Lincolnton Solid 11/02/2021 0915 11/02/2021
002 L-1-7 Solid 11/02/2021 0915 11/02/2021
003 L-1-7 Solid 11/02/2021 0915 11/02/2021
004 L-1-7 Solid 11/02/2021 0915 11/02/2021
005 L-1-7 Solid 11/02/2021 0915 11/02/2021
006 L-1-7 Solid 11/02/2021 0915 11/02/2021
007 L-1-7 Solid 11/02/2021 0915 11/02/2021
008 L-1-7 Solid 11/02/2021 0915 11/02/2021
(8 samples)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 16

Inorganic non-metals
Client: Synagro
Description: Lincolnton
Date Sampled:11/02/2021 0915
Date Received:11/02/2021
Laboratory ID: WK02050-001
Matrix: Solid
% Solids: 4.20 11/03/2021 0152
Run Prep Method
1 350.1
1
1
1
1
1 351.4
Analytical Method
(Ammonia - N) 350.1
(Nitrate - N ) 9056A
(Nitrite - N ) 9056A
(Phosphorus) 365.1
(Soil pH meas) 9045D
(TKN) 351.2
Dilution
25
1
1
25
1
2
Analysis Date Analyst
11/20/20212008 DRD
11/10/2021 1053 AMR
11/10/2021 1053 AMR
11/04/20211717 DMA
11/07/20211728 NBW
11/05/20211227 DMA
Batch
22997
22147
22153
11/04/2021 1019 21253
21588
11/04/2021 1312 21269
Prep Date
Parameter
CAS Analytical
Number Method
Result Q LOQ
DL
Units Run
Ammonia - N (gas diffusion)
Nitrate - N (soluble)
Nitrite - N (soluble)
Phosphorus
Soil pH measured in water @ 20.8 ° C
TKN
7723-14-0
350.1
9056A
9056A
365.1
9045D
351.2
18000
43
5.5
16000
7.3
42000
600
12
4.8
3000
310
2.4
2.4
600
S 2400 1200
mg/kg 1
mg/kg 1
mg/kg 1
mg/kg 1
su 1
mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
W = Reported on wet weight basis
J = Estimated result < LOQ and > DL
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 16

CVAA
Client: Synagro Laboratory ID: WK02050-001
Description: Lincolnton Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 4.20 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method
1 7471B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
7471B 1 11/16/2021 1644 JAB2 11/15/2021 1536 22152
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Mercury
7439-97-6
7471B ND 1.9 0.46 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5of16

ICP-AES
Client: Synagro Laboratory ID: WK02050-001
Description: Lincolnton Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 4.20 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method
1 3050B
2 3050B
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
6010D 1 11/04/2021 1339 JMH 11/04/2021 0126 21089
6010D 1 11/05/2021 1752 KSH2 11/04/2021 0126 21089
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
7429-90-5 6010D 12000 150 58 mg/kg 1
7440-38-2 6010D 4.7 J 5.8 1.9 mg/kg 1
7440-43-9 6010D 0.77 J 1.9 0.49 mg/kg 1
7440-70-2 6010D 8900 1900 240 mg/kg 1
7440-47-3 6010D 110 3.9 0.97 mg/kg 1
7440-50-8 6010D 280 3.9 1.7 mg/kg 1
7439-89-6 6010D 11000 39 18 mg/kg 1
7439-92-1 6010D 15 3.9 1.7 mg/kg 1
7439-95-4 6010D 2900 1900 240 mg/kg 1
7439-96-5 6010D 260 5.8 2.3 mg/kg 1
7439-98-7 6010D 5.5 J 15 3.9 mg/kg 1
7440-02-0 6010D 12 J 15 4.1 mg/kg 1
7440-09-7 6010D 3000 1900 240 mg/kg 2
7782-49-2 6010D 3.8 J 7.7 3.1 mg/kg 1
7440-23-5 6010D 1000 J 1900 240 mg/kg 1
7440-66-6 6010D 270 19 4.8 mg/kg 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-002
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 6.94 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <15553 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-003
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 5.68 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <14402 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-004
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 7.18 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <17595 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-005
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 6.80 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <13927 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-006
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 7.56 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <14704 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-007
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 6.31 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <13219 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 16

Inorganic non-metals
Client: Synagro Laboratory ID: WK02050-008
Description: L-1-7 Matrix: Solid
Date Sampled:11/02/2021 0915 % Solids: 6.43 11/03/2021 0152
Date Received: 11/02/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 11/03/2021 2305 NBW 11/02/2021 1923
Parameter
CAS Analytical
Number Method Result Q LOQ DL Units Run
Fecal Coliform-MF
SM 9222 D-2006 <15860 20
col/g 1
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
H = Out of holding time
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
W = Reported on wet weight basis
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 16

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 16

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PACE ANALYTICAL SERVICES, LLC

PACE ANALYTICAL SERVICES, LLC
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Samples Receipt Checklist (SRC' 110E0018C-1S)
Issuing AL thority: Race EKV - WCOL
Sample Receipt Checklist (SRC)
Coolor Iris clod ISH I Liale/D21
wie..0.2050
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Yes
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Yes
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MI NA
2. If:custody seals were preset were they intact and unl-proken?
pH Strip
Original
2.1 /2.1
ID: 004
temperature upon
nc NA INA
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Wcl. ICe . Ice PuF.;1,5 0 Dry Ice El 1,0c.c
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PM WW114nli Find by: phone/ email .1 fa.oe-torface (circle one).
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4, Is Ilie etrrirnweial courier's packing slip attached to this forrn"2
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6. Were !-..v_mple II) li,itcd On 1114: COC?
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7. Wert u.'mp le IN listed cio all sample containea?
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9, Was col led. ion dat; it tim. ILEted on all sarr,ple containers?
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11. Wurubs517. to he per:brined lisped on the COC?
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(unhroken, liLs on, Qtc.)?
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15. Were any sainplEi CCii dal ri et luissingiektess (eimit ono) Titrnplos Not listed on COC?
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16. For VOA and RSK-175 FampleN, were Nibbles preserit )."pee -size ('N'or 6rorn in diairetfr)
in any of the VOA vials?
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17. W:sin ere all DROirnei utrlcrit w.m.ples received at a pH of <2?
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reiilu el chlorin...I
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20. Were client remarksirequests (i.e. requested dilutions, 7....ISIMSD detignatiols,
correctly transcribed from the CUC into the comment section in L1MS?
tt NA
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2'). %ix.; the r 'Joie number listed on the container label? If ,es, Quo 4
Sam plc Pretervation (iviust he completed for any sampie(S) incorrectly preserved or with hradSPOcc,)
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NA . If mon.. than one preservative is needed, please note in the tomnients below.
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EECCordingly in sample rocziving wiii sodbm thiosul fate (1%; a2SA) with Slimly la NA
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-I. Date, ]1/1:r2..2021
Conlin .0ms:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 16 of 16

Technician
NC0025496
-2011 2540 D -2011
uuarter Ye -air 7-Asci/
All weighings are done in grams i/
a. r ,....:',,, ,,,:.. , ,,,, P ' ' -;.
4
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% TS DAF =
3
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,'
/6 t j-/
% VS Sludge
% Total Solids
% Volatile Solids =
% Reduction =
Dry Solids Wgt
Wet Solids Wgt
(Volatile Solids Wgt)
Dried Solids Wgt
(VS DAF - VS Sludge)
VS DAF - (VS DAF)(VS Sludge)
X 100
X 100
X 100
I/3

SECTION 6

Agricultural Lime Application Log
Year: 2021
Project:
Lincolnton
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied(CCE Eq.)
Date Applied
LT-36-3
6.1
0.0T/AC
0.0T/AC
LT-36-5
5.8
.5T/AC
.5T/AC
06/02/21
LT-49-1
5.3
1.3T/Ac
1.3T/AC
07/13/21
LT-49-2
5.9
0.0T/AC
0.0T/AC
LT-47-4
5.7
.5T/AC
1T/AC
10/11/21
LT-19-2
6.1
0.0T/AC
0.0T/AC
CA-48-10
5.4
1 T/AC
1T/AC
12/14/21
LT-19-1
6.6
0.0T/AC
0.0T/AC
LT-19-3
6.0
0.0T/AC
0.0T/AC
LT-47-2
5.3
1 T/AC
1 T/AC
12/13/21
LT-47-5
5.8
.5T/AC
* Lime is ordered waiting for Vendor to spread it

SECTION 7

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY22-SL012547
�µ5 i 11L I .t!L
..' r Z , Predictive
i S.. r.
' � Soil Report Mehlich-3 Extraction
"-x.v,it.; .. Links to Helpful Information
Client: Mike Davis
Dansbury Lane
Vale, NC 28168
Sampled County : Catawba
Client ID: 525626
Advisor: Alex Fox
Synagro
284 Boger Rd
Mocksville, NC 27028
Advisor ID: 501947
Sampled: 10/27/2021 Received: 10/29/2021 Completed: 11/17/2021 Farm: CA-48
Sample ID: 1D
Lime History:
Recommendations: Lime
Nutrients (lb/acre)
More
Information
Note: 3
Crop (tons/acre) N P2O5
1 -Corn, grain 1.0 120 - 160 0
2 - 0.0
K2O Mg S Mn Zn
30 0 0 0 0
Cu B
0 0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg%
0.60 1.07 6.7 71 2.0 5.4 204 59 51 15
S-I
49
Soil Class: Mineral
Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-Al
154 109 265 265
Cu-I Na ESP SS -I NO3-N
513 0.1 1
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Tataciw frum fund Co mlb5km

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL012547
Mike Davis Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
Report Abbreviations
Ac exchangeable acidity
B boron
BS% % CEC occupied by basic cations
Ca% % CEC occupied by calcium
CEC cation exchange capacity
Cu-I copper index
ESP exchangeable sodium percent
HM% percent humic matter
K-I potassium index
K20 potash
Mg% % CEC occupied by magnesium
MIN mineral soil class
Mn manganese
Mn-AI1 Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
M-0 mineral -organic soil class
N nitrogen
Na sodium
NO3-N nitrate nitrogen
ORG organic soil class
pH current soil pH
P-I phosphorus index
P205 phosphate
S-I sulfur index
SS -I soluble salt index
W/V weight per volume
Zn-AI zinc availability index
Zn-I zinc index
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely
indicate levels fertility Visit www.ncagr.gov/agronomi/uyrst.htm
available)] of plant nutrients or other measurement.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY22-SL012539
�µ5 i L. .!L
..' r Z , Predictive
i S.. r.
' � Soil Report Mehlich-3 Extraction
"-x.v,it.; .. Links to Helpful Information
Client: Ron Parker
226 Rockdale Rd.
Lawndale, NC 28090
Sampled County : Cleveland
Client ID: 417546
Advisor: Alex Fox
Synagro
284 Boger Rd
Mocksville, NC 27028
Advisor ID: 501947
Sampled: 09/25/2021 Received: 10/29/2021 Completed: 11/17/2021 Farm: C1-2
Sample ID: 3
Lime History:
Recommendations: Lime
Nutrients (lb/acre)
More
Information
Note: 12
Crop (tons/acre) N P2O5
1-Fescue/OGrass/Tim, M 0.0 120-200 0
2 - 0.0
K2O Mg S Mn Zn
0 0 0 0 0
Cu B
0 0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg%
0.36 1.01 6.7 80 1.3 6.0 110 101 55 18
S-I
44
Soil Class: Mineral
Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-Al
198 135 145 145
Cu-I Na ESP SS -I NO3-N
478 0.1 1
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Tataciw frum fund Co mlb5km

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL012539
Ron Parker Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
Report Abbreviations
Ac exchangeable acidity
B boron
BS% % CEC occupied by basic cations
Ca% % CEC occupied by calcium
CEC cation exchange capacity
Cu-I copper index
ESP exchangeable sodium percent
HM% percent humic matter
K-I potassium index
K20 potash
Mg% % CEC occupied by magnesium
MIN mineral soil class
Mn manganese
Mn-AI1 Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
M-0 mineral -organic soil class
N nitrogen
Na sodium
NO3-N nitrate nitrogen
ORG organic soil class
pH current soil pH
P-I phosphorus index
P205 phosphate
S-I sulfur index
SS -I soluble salt index
W/V weight per volume
Zn-AI zinc availability index
Zn-I zinc index
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely
indicate levels fertility Visit www.ncagr.gov/agronomi/uyrst.htm
available)] of plant nutrients or other measurement.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY22-SL000470
�µ5, 14�•: !L
' r " , Predictive
i.S . ' r.
'_ . d II •• =
Soil Report Mehlich-3 Extraction
'w, F.' Links to Helpful Information
Client:
Client ID:
Alex Fox
Synagro
284 Boger Rd
Mocksville, NC 27028
Sampled County :Lincoln
501947
Advisor:
Advisor ID:
Sampled: Received: 07/08/2021 Completed: 07/20/2021 Farm: Lt-19
Sample ID: 1
Lime History:
Recommendations: Lime
Nutrients (lb/acre)
More
Information
Note: 12 Note: $
Crop (tons/acre) N P2O5
1 -Fescue/OGrass/Tim, M 0.0 120-200 0
2 - 0.0
K2O
80
Mg S Mn Zn
0 0 pH$ 0
Cu
0
B
0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg%
0.41 1.10 10.4 92 0.8 6.6 144 28 62 28
S-I
39
Mn-I
1600
Soil Class: Mineral
Mn-AI1 Mn-Al2 Zn-I Zn-Al
968 273 273
Cu-I
266
Na
0.1
ESP
1
SS -I NO3-N
Sample ID: 2A
Lime History:
Recommendations: Lime
Nutrients (lb/acre)
More
Information
Note: 12
Crop (tons/acre) N P2O5
1-Fescue/OGrass/Tim, M 0.0 120-200 0
2 - 0.0
K2O
60
Mg S Mn Zn
0 0 0 0
Cu
0
B
0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg%
0.51 1.05 10.6 87 1.4 6.1 172 38 58 27
S-I
43
Mn-I
1481
Soil Class: Mineral
Mn-AI1 Mn-Al2 Zn-I Zn-AI
904 346 346
Cu-I
335
Na
0.1
ESP
1
SS -I NO3-N
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Tohkiw Trum fund Co mlb5I m

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY22-SL000470
Alex Fox
Page 2 of 3
Sample ID: 2B
Lime History:
Recommendations: Lime
Nutrients (Ib/acre)
More
Information
Note: 12
Crop (tons/acre) N P2O5
1-Fescue/OGrass/Tim, M 0.0 120-200 0
2 - 0.0
K2O
70
Mg S
0 0
Mn Zn
0 0
Cu
0
B
0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg%
0.32 0.98 8.1 84 1.3 5.9 101 32 56 26
S-I
33
Mn-I
495
Soil Class:
Mn-AI1 Mn-Al2
314
Mineral
Zn-I Zn-AI
289 289
Cu-I
329
Na
0.0
ESP
SS -I NO3-N
Sample ID: 3
Lime History:
Recommendations: Lime
Nutrients (Ib/acre)
More
Information
Note: 12
Crop (tons/acre) N P2O5
1-Fescue/OGrass/Tim, M 0.0 120-200 0
2 - 0.0
K2O
10
Mg S
0 0
Mn Zn
0 0
Cu
0
B
0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg%
0.41 1.11 9.6 86 1.3 6.0 192 73 66 17
S-I
51
Mn-I
183
Soil Class:
Mn-AI1 Mn-Al2
127
Mineral
Zn-I Zn-AI
668 668
Cu-I
262
Na
0.1
ESP
1
SS -I NO3-N

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL000470
Alex Fox Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
Report Abbreviations
Ac exchangeable acidity
B boron
BS% % CEC occupied by basic cations
Ca% % CEC occupied by calcium
CEC cation exchange capacity
Cu-1 copper index
ESP exchangeable sodium percent
HM% percent humic matter
K-I potassium index
K20 potash
Mg% % CEC occupied by magnesium
MIN mineral soil class
Mn manganese
Mn-AI1 Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-1 manganese index
M-0 mineral -organic soil class
N nitrogen
Na sodium
NO3-N nitrate nitrogen
ORG organic soil class
pH current soil pH
P-I phosphorus index
P205 phosphate
S-I sulfur index
SS -I soluble salt index
W/V weight per volume
Zn-AI zinc availability index
Zn-I zinc index
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely
indicate levels fertility Visit www.ncagr.gov/agronomi/uyrst.htm
available)] of plant nutrients or other measurement.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY22-SL000476
�µ5i 14�•: !L
..' r " , Predictive
iS . ' r.
$ ���` it �•
_ ,• Soil Report Mehlich-3 Extraction
"ct`
"-x.v, t.; .. Links to Helpful Information
Client: Jeff Lingerfelt
7338 W Hwy 27
Vale, NC 28168
Sampled County : Lincoln
Client ID: 318761
Advisor: Alex Fox
Synagro
284 Boger Rd
Mocksville, NC27028
Advisor ID: 501947
Sampled: Received: 07/08/2021 Completed: 07/20/2021 Farm: Lt-36
Sample ID: 3
Lime History:
Recommendations: Lime
Nutrients (lb/acre)
More
Information
Note: 3
Crop (tons/acre) N P2O5
1 -Small Grain (SG) 0.0 80-100 0
2 - 0.0
K2O Mg S Mn Zn
20 0 0 0 0
Cu B
0 0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg%
0.66 1.00 10.9 89 1.2 6.1 162 66 66 20
S-I
56
Soil Class: Mineral
Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-Al
73 53 298 298
Cu-I Na ESP SS -I NO3-N
261 0.1 1
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Tataciw frum fund Co mlb5I m

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL000476
Jeff Lingerfelt Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
Report Abbreviations
Ac exchangeable acidity
B boron
BS% % CEC occupied by basic cations
Ca% % CEC occupied by calcium
CEC cation exchange capacity
Cu-I copper index
ESP exchangeable sodium percent
HM% percent humic matter
K-I potassium index
K20 potash
Mg% % CEC occupied by magnesium
MIN mineral soil class
Mn manganese
Mn-AI1 Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
M-O mineral -organic soil class
N nitrogen
Na sodium
NO3-N nitrate nitrogen
ORG organic soil class
pH current soil pH
P-I phosphorus index
P205 phosphate
S-I sulfur index
SS -I soluble salt index
W/V weight per volume
Zn-AI zinc availability index
Zn-I zinc index
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely
indicate levels fertility Visit www.ncagr.gov/agronomi/uyrst.htm
available)] of plant nutrients or other measurement.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL031090
�µ5 i L. .!L Client: Alex Fox
..' r " , Predictive Synagro
•'` it' = 284 Boger Rd
; Soil Report Mehlich-3 Extraction Mocksville, NC 27028
-"x'w,,F.;;'. Links to Helpful Information Sampled County : Lincoln
Advisor:
Advisor ID:
Client ID: 501947
Sampled: 03/15/2021 Received: 04/27/2021 Completed: 05/06/2021 Farm: LT-36/ Jeff Lingerfelt
Sample ID: 5
Lime History:
Recommendations: Lime Nutrients (lb/acre)
More
Information
Note: 12
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn
1-Fescue/OGrass/Tim, M 0.3 120-200 10 80 0 0 0 0
2 - 0.0
Cu
0
B
0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-Al
0.60 1.11 5.9 80 1.2 5.8 57 28 55 23 47 197 135 109 109
Cu-I Na
108 0.0
ESP SS -I NO3-N
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Tohkiw frum fund Co mlb5km

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL031090
Alex Fox Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
Report Abbreviations
Ac exchangeable acidity
B boron
BS% % CEC occupied by basic cations
Ca% % CEC occupied by calcium
CEC cation exchange capacity
Cu-I copper index
ESP exchangeable sodium percent
HM% percent humic matter
K-I potassium index
K20 potash
Mg% % CEC occupied by magnesium
MIN mineral soil class
Mn manganese
Mn-AI1 Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-1 manganese index
M-0 mineral -organic soil class
N nitrogen
Na sodium
NO3-N nitrate nitrogen
ORG organic soil class
pH current soil pH
P-I phosphorus index
P205 phosphate
S-I sulfur index
SS -I soluble salt index
W/V weight per volume
Zn-AI zinc availability index
Zn-I zinc index
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely
indicate levels fertility Visit www.ncagr.gov/agronomi/uyrst.htm
available)] of plant nutrients or other measurement.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY22-SL012544
�µ5 i L. .!L
..' r Z , Predictive
iS . ' r.
' Soil Report Mehlich-3 Extraction
"ct`
"-x.v,it.; .. Links to Helpful Information
Client: Randy Leatherman
3322 Dansbury Ln
Vale, NC 28168
Sampled County : Lincoln
Client ID: 502961
Advisor: Alex Fox
Synagro
284 Boger Rd
Mocksville, NC 27028
Advisor ID: 501947
Sampled: 10/27/2021 Received: 10/29/2021 Completed: 11/17/2021 Farm: Lt-47
Sample ID: 2
Lime History:
Recommendations: Lime
Nutrients (lb/acre)
More
Information
Note: 3
Crop (tons/acre) N P2O5
1 -Corn, grain 1.0 120 - 160 0
2 - 0.0
K2O Mg S Mn Zn
80 0 0 0 0
Cu B
0 0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg%
0.66 1.03 5.7 67 1.9 5.3 123 30 49 15
S-I
53
Soil Class: Mineral
Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-Al
106 81 145 145
Cu-I Na ESP SS -I NO3-N
387 0.1 2
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Tataciw Trum fund Co mlb5km

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL012544
Randy Leatherman Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
Report Abbreviations
Ac exchangeable acidity
B boron
BS% % CEC occupied by basic cations
Ca% % CEC occupied by calcium
CEC cation exchange capacity
Cu-I copper index
ESP exchangeable sodium percent
HM% percent humic matter
K-I potassium index
K20 potash
Mg% % CEC occupied by magnesium
MIN mineral soil class
Mn manganese
Mn-AI1 Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
M-0 mineral -organic soil class
N nitrogen
Na sodium
NO3-N nitrate nitrogen
ORG organic soil class
pH current soil pH
P-I phosphorus index
P205 phosphate
S-I sulfur index
SS -I soluble salt index
W/V weight per volume
Zn-AI zinc availability index
Zn-I zinc index
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely
indicate levels fertility Visit www.ncagr.gov/agronomi/uyrst.htm
available)] of plant nutrients or other measurement.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY21-SL031091
�µ5 i L. .!L Client: Alex Fox
..' r " , Predictive Synagro
'`' = 284 Boger Rd
it
; Soil Report Mehlich-3 Extraction Mocksville, NC 27028
-"x'w,,F.;; '. Links to Helpful Information Sampled County : Lincoln
Advisor:
Advisor ID:
Client ID: 501947
Sampled: 04/15/2021 Received: 04/27/2021 Completed: 05/06/2021 Farm: LT-47/ Randy Leatherman
Sample ID: 4
Lime History:
Recommendations: Lime Nutrients (lb/acre)
More
Information
Note: 3
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn
1 -Corn, silage 0.5 180-220 30 100 0 0 0 0
2 - 0.0
Cu
0
B
0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-Al
0.36 1.02 6.5 78 1.4 5.7 56 47 54 20 157 123 91 380 380
Cu-I Na
121 0.0
ESP SS -I NO3-N
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Tohkiw frum fund Co mlb5km

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY21-SL031091
Alex Fox Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
Report Abbreviations
Ac exchangeable acidity
B boron
BS% % CEC occupied by basic cations
Ca% % CEC occupied by calcium
CEC cation exchange capacity
Cu-I copper index
ESP exchangeable sodium percent
HM% percent humic matter
K-I potassium index
K20 potash
Mg% % CEC occupied by magnesium
MIN mineral soil class
Mn manganese
Mn-AI1 Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-1 manganese index
M-0 mineral -organic soil class
N nitrogen
Na sodium
NO3-N nitrate nitrogen
ORG organic soil class
pH current soil pH
P-I phosphorus index
P205 phosphate
S-I sulfur index
SS -I soluble salt index
W/V weight per volume
Zn-AI zinc availability index
Zn-I zinc index
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely
indicate levels fertility Visit www.ncagr.gov/agronomi/uyrst.htm
available)] of plant nutrients or other measurement.

Page 1 of 1
Report No: 21-363-0517
Account No: 12259
Advisor: Synagro/Columbus NC
Mary Brewer
284 Boger Rd
Mocksville NC 27028
Waypoint..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Client: Randy Leatherman Farm: Lt-47
Date Received: 12/29/2021
Date of Report: 12/30/2021
Lab No Field ID
Sample ID Soil Class HM% W/V pH Ac P-I K-I S-I Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-Al Cu-I CEC BS% Ca% Mg% ESP Na
03485 5 MIN 5.8 1.3 129 82 25 94 76 0 255 255 235 6.9 81 55 18 1.2 0.1
Crop Recommendations: Rec Uom Lime (t/acre) N P205 K20 S Mn Zn Cu B Mg Last Crop
1- Fescue Hay lb/acre 0.5 150 0 0 20 0 0 0 0 0
Comment:
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WA/ in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY22-SL000474
�µ5, 14�•: !L
' r " , Predictive
i.S . ' r.
'_ . d II •• =
Soil Report Mehlich-3 Extraction
'w, F.' Links to Helpful Information
Client:
Client ID:
Alex Fox
Synagro
284 Boger Rd
Mocksville, NC 27028
Sampled County :Lincoln
501947
Advisor:
Advisor ID:
Sampled: Received: 07/08/2021 Completed: 07/20/2021 Farm: Lt-49
Sample ID: 1
Lime History:
Recommendations: Lime
Nutrients (lb/acre)
More
Information
Note: 12
Crop (tons/acre) N P2O5
1-Fescue/OGrass/Tim, M 1.3 120-200 70
2 - 0.0
K2O
50
Mg S Mn Zn
0 0 0 0
Cu
0
B
0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg%
1.25 0.96 8.6 72 2.4 5.3 30 43 49 20
S-I
44
Mn-I
64
Soil Class: Mineral
Mn-AI1 Mn-Al2 Zn-I Zn-Al
55 68 68
Cu-I
70
Na
0.1
ESP
1
SS -I NO3-N
Sample ID: 2
Lime History:
Recommendations: Lime
Nutrients (lb/acre)
More
Information
Note: 12
Crop (tons/acre) N P2O5
1-Fescue/OGrass/Tim, M 0.0 120-200 0
2 - 0.0
K2O
30
Mg S Mn Zn
0 0 0 0
Cu
0
B
0
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
HM% W/V CEC BS% Ac pH P-I K-I Ca% Mg%
0.51 1.12 9.6 85 1.4 5.9 175 56 64 19
S-I
46
Mn-I
111
Soil Class: Mineral
Mn-AI1 Mn-Al2 Zn-I Zn-AI
84 406 406
Cu-I
437
Na
0.1
ESP
1
SS -I NO3-N
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Aqriculture
Tohkiw frum fund Co mlb5I m

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY22-SL000474
Alex Fox Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
Report Abbreviations
Ac exchangeable acidity
B boron
BS% % CEC occupied by basic cations
Ca% % CEC occupied by calcium
CEC cation exchange capacity
Cu-1 copper index
ESP exchangeable sodium percent
HM% percent humic matter
K-I potassium index
K20 potash
Mg% % CEC occupied by magnesium
MIN mineral soil class
Mn manganese
Mn-AI1 Mn availability index for crop 1
Mn-Al2 Mn-availability index for crop 2
Mn-1 manganese index
M-0 mineral -organic soil class
N nitrogen
Na sodium
NO3-N nitrate nitrogen
ORG organic soil class
pH current soil pH
P-I phosphorus index
P205 phosphate
S-I sulfur index
SS -I soluble salt index
W/V weight per volume
Zn-AI zinc availability index
Zn-I zinc index
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find
the exact fertilizer grade recommended on the report, visit www.ncagr.qov/agronomi/obpart4.htmsfind information that
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely
indicate levels fertility Visit www.ncagr.gov/agronomi/uyrst.htm
available)] of plant nutrients or other measurement.