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Home My WebLink AboutNCG060407_Amazon Services Monitoring_20220210NCDEQ Division of Energy, Mineral and Land Resources Stormwater Discharge Monitoring Report (DIYIR) Form for NCG060000 Food and Kindred Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30days of receiving sampling results. Mail the original, signed hard copyof the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG06 0407 Person Collecting Samples: John Haffner kA Facility Name: Amazon.com Services LLC -RDU 1 Laboratory Name: Eutofins TestAmedca Facility County: Wake I Laboratory Cert. No.: 269 °°'a0F Discharge during this period: 0 Yes 0 No /ifno, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceeds If so, which Tier (I, II, or III)? °m g r� A copy of this DMR has been uploaded electronically via https://edocs.deg.nc.gov/Forms/SW-DMR 3' x❑ Yes []No Date Uploaded: B AnalyticatMonitoring Requirements for Outfatts with Industriat Activities —Benchmarks in (Red) Parameter Code Parameter Outfaµ 001 OutfaR 002 Outfalt Outfall Outfaff N/A Receiving Stream Class C, NSW C, NSW N/A Date Sample Collected MM/DD/YYYY 12/8/2021 12/8/2021 46529 24-Hour Rainfall in inches 0.62 - 0.62 C0530 TSSin mg/L (100or50•) 12 12 00400 PH in standard units (6.0-9.0 FW, 6.8-8.5 SW) 8.04 8.25 Fecal Coliform per 100 ml of 31616 freshwater (if required) (1000) N/A N/A 61211 Enterococci per 100 ml of saltwater N/A N/A (if required) (500 Chemical Oxygen Demand in mg/L 00340 (120) 110 S Additional parameters for outfalls in drainage areas that use>55 gallons per month of new hydraulic oil on average NCOIL Estimated New Motor/Hydraulic oil N/A N/A Usage in gal/month 00552 Non -Polar Oil & Grease in mg/L (15) 1 N/A I N/A " Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 5o mg/L. All other water classifications have a benchmark of 100 mg/L FW (Freshwater) SW (Saltwater) Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my Inquiry of the person or persons who manage the system, or those persons directly responsible forgathering the information, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including ibi tes and imprisonment for knowing violations." / 1 Signature of Permittee or Delegated Authorized Individual Date boese@amazon.com Email Address Phone Number urofins I 0 Environment Testing America ANALYTICAL REPORT' Eurofins TestAmerica, Savannah o� n 5102 LaRoche Avenue Pop G Savannah, GA 31404°mom �C1 Tel: (912)354-7858 {� Laboratory Job ID: 680-208586-1 4? Client Project/Site: Storm Water - Amazon Warehoses RDU1 For: ERM-West 1920 Main Street Suite 300 Irvine, California 92614 Attn: Doug J Wade Rox�.c. �S1uros Authorized for release by: 1212812021 8:20:10 AM Roxanne Cisneros, Senior Project Manager (615)301-5761 roxanne.cisneros@Eurofinset.com The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Definitions/Glossary Client: ERM-West Job ID: 680-208586-1 Project/Site: Storm Water -Amazon Warehouses RDIJ1 Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. a Listed under the " o" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) oil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis ofthe sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DOD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Lever (Dioxin) MPN Most Probable Number MOIL Method Quentitation Limit NC Not Calculated NO Not Detected at the reporting limit(or MOIL or EDL if shown) NEG Negative/Absent POS Positive/Present PQL Practical Quantitabon Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins TestAmerica, Savannah Page 2 of 13 12/28/2021 Sample Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses RDU1 Job rD: 680-208586-1 Lab Sampte tD Ment Sampte M Mawx Cbttected Received, 680-208586-1 RDU1_Sample_Point 01_20211208 Water 12/08/21 09:00 12/09/21 11:00 680 208'586-2 RfU1_Sempie Point 02_20241208 Water 12/08/2-108.20 12109/21 MOO Page 3 of 13 Eurofins TestAmerica,@�1 Case Narrative Client: ERM-West ProjectlSite: Storm Water -Amazon Warehouses RDU1 Job ID: 680-208686-1 Laboratory: Eurofins TestAmerica, Savannah Narrative Job ID:680-208586-1 141 Job Narrative 680-208586-1 Comments No additional comments. Receipt The samples were received on 12/W2021 11:00 AM. Unless otherwise noted below, the samples arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 2.30 C. General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Eurofins TestAmerica, Savannah Page 4 of 13 12/28/2021 Client Sample Results Client: ERM-West Job ID: 680-208586-1 Project/Site: Storm Water -Amazon Warehouses RDU1 Client Sample ID: RDU1_Sample_Point_01_20211208 Lab Sample ID: 680-208586-1 Date Collected: 12JO8121 09:00 Matrix: Water Date Received: 12/09/21 11:00 General Chemistry Analyte Result Qualifier RL &ML Unit D Prepared Analyzed Oil Fac Chemical Oxygen Demand 110 10 5.0 mglL 12/20121 20:01 1 Total Suspended Solids 12 2.5 2.5 mg/L 12/15121 14A7 1 Eurofins TestAmerica, Savannah Page 5 of 13 12/28/2021 Client Sample Results Client: ERM-West Job ID: 680-208586-1 Project/Site: Storm Water -Amazon Warehouses RDU1 Client Sample ID: RDU1_Sample_Point_02_20211208 Lab Sample ID: 680-208586-2 Date Collected: 12108121 08:20 Matrix: Water Date Received: 12109121 11:00 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DLL Faa Chemical Oxygen Demand <5.0 10 5.0 mg/L 12/2o/21 13:03 1 LTotal Suspended Solids 12 25 25 mglL 1211521 14:47 1 Eurofins TestAmerica, Savannah Page 6 of 13 12/28/2021 QC Sample ReGults Client: ERM-West Project/Site: Storm Water - Amazon Warehouses RDU1 Method: 5220D-2011 - Chemical Oxygen Demand r Lab Sample ID: MB 680-69987713 Matrix: Water Analysis Batch: 699877 Analyte Chemical. Oxygen Demand Lab Sample ID: LCS 680-699877/4 Matrix: Water Analysis Batch: 699877 Analyte Chemical Oxygen Demand Lab Sample ID: MB 680-69994013 Matrix: Water Analysis Batch: 699940 MB MB Result Qualifier RL MDL Unit <5.0 10. 5.0. mg& Spike LCS LCS Added Result Qualifier 50.0 47.0 Job ID:680-208586-1 Client Sample ID: Method Blank Prep Type: TOtalINA D Prepared Analyzed oil Fac 1,2120/21 t3:03 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA %Rec. Unit D %Rec Limits mg/L 94 90-110 Client Sample ID: Method Blank Prep Type: Total/NA MB MB Analyte Result Qualifier RL MOIL Unit D Prepared Analyzed Oil Fac Chemical Oxygen Demand <5.0 10 5.0 mg/L 12/20121 20:01 1 Lab Sample ID: LCS 680-699940/4 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 699940 Spiko LCS LCS %Rac. Analyte Added Result Qualifier Unit D %Rec Limits chemicaloxygen.Dsmand 50,0 49,0� mgl.L 98. 9G_110 Method: SM 2540D - Solids, Total Suspended (TSS) Lab Sample ID: MB 680-699056/1 Matrix: Water Analysis Batch: 699056 Analyte -Total Suspended Solids Lab Sample ID: LCS 680-699056/2 Matrix: Water Analysis Batch: 699056 Analyte Total Suspended Solids Lab Sample ID: LCSD 680-69906613 Matrix: Water Analysis Batch: 699056 Analyte Total Suspended Solids Client Sample ID: Method Blank Prep Type: Total/NA MB MB Result Qualifier RL MOIL Unit D Prepared Analyzed oil Fac <2.5 2.5 2.5 mg—L 12M5121 14:47 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Added Result Q"Hfler Unit D %Rec Limits 951 828 mg/L 87 80 -120 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA Spike LCSD LCSD Added Result Qualifier Unit 951 848 mo_/L T,Rec. RPD D %Rec Limits RPD Limit 89 80-120 2 25 Eurofins TestAmerica, Savannah Page 7 of 13 12/28/2021 QC Association Summary Client: ERM-West Job ID: 680-208586-1 Project/Site: Storm Water -Amazon Warehouses RDU1 General Chemistry Analysis Batch: 699066 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-208586-1 RDU1_Sample_Point_01_20211208 TotaVNA Water SM 2540D 6W-208586-2 RDUt_Sampte_Point_02 20211208 TOtaVNA Water SM 2540D MB 680-699056/1 Method Blank Total/NA Water SM 2540D LCS 680-699056/2 Lab Control Sample TotaltNA Water SM 2540D LCSD 680-69905613 Analysis Batch: 699877 Lab Control Sample Dup Total/NA Water SM 2540D Lab Sample to Client Sample ID Prep Type Matrix Method Prep Batch 680-208586-2 RDU1_Sample_Point 02_20211208 TotaVNA Water 522OD-2011 MB 680-69987713 Method Blank TotaVNA Water 52200.2011 LCS 680-699877/4 Lab Control Sample TotaVNA Water 622OD-2011 Analysis Batch: 699940 Lab Sample to Client Sample to Prep Type Matrix Method Prep Batch 680-208586-1 RDUt_Sample_Point 01_20211208 Total/NA Water 522OD-2011 MB 680-69994013 Method Blank ToteVNA Water 5220D-2011 LCS 680-699940/4 Lab Control Sample TotaVNA Water 522OD-2011 Eurofins TestAmerica, Savannah Page 8 of 13 12/28/2021 Lab Chronicle Client: ERM-West Project/Site: Storm Water -Amazon Warehouses RDU1 Client Sample ID: RDU1_Sample_Point_01_20211208 Date Collected: 12108/21 09:00 Date Received: 1210912l 11:00 Job ID: 680-208586-1 Lab Sample ID: 680-208586-1 Matrix: Water Batch Batch Oil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab TotaIINA Analysis 522OD-2011 1 2 mL 2 mL 699940 12120/21 20:01 ALG TAL SAV Instrument ID: SPC7 TotallNA Analysis SM 2540D 1 992 mL 1000 mL 699056 12115f21 14:47 PG TAL SAV LInstrument ID: NOEQUIP Client Sample ID: RDU1_Sample_Point_02_20211208 Date Collected: 12/08/21 08:20 Date Received: 12/09/21 11:00 Lab Sample ID: 680-208586-2 ov° Matrix: Water Batch Batch oil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Analysis 52200-2011 1 2 mL 2mL 6998 77 12120121 13:03 ALG TAL SAV Instrument ID: SPC7 TotaVNA Analysis SM 2540D 1 1000 mL 1000 mL 699056 12/15/21 14,47 PG TAL SAV Instrument ID: NOEQUIP Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 9 of 13 12/28/2021 Accreditation/Certification Summary Client: ERM-West Project/Site: Storm Water -Amazon Warehouses RDU1 Laboratory: Eurofins TestAmerica, Savannah The accreditationslcertifications listed below are applicable to this report. [Authority program IkWm ificatlon Number Expiration Date North Carolina (WW/SW) State 269 12-31-21 .. , __§• M. Eurofns TestAmerica, Savannah Page 10 of 13 12/28/2021 Method Summary Client: ERM-West Job ID: 680-208586-1 Project/Site: Storm Water - Amazon Warehouses RDU1 Method Method Description Protocol Laboratory 5220D-2011 Chemical Oxygen Demand SM TAL SAV SM 2540D Solids, Total Suspended (TSS) SM TAL SAV Protocol References: SM = "Standard Methods For The Examination Of Water And Wastewater' Laboratory References: TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins TestAmerica, Savannah Page 11 of 13 12/28/2021 m 0 m N O Lo Eurofins TestAmerica, Savannah 5102 LaRoche Avenue Savannah GA 31404 Phone 912-354-7858 Fax-912-352-0165 Chain of Custody Record eurofins _ V.LNbn i w Client lnfomlation Samper t Lab PM Canems Roxanne Carder Tra .M No(s Na 240-87337-33335 Crem Comes Doug Wade Phb n !� �- — ✓'1 E4lI roxanne asneros@Eurolinsetcom Suredf Ongm Page page 1 of t dmPeny MSID ERM-West Analysis Requested Jgbx MM" 1920 Main Street Sude 300 Oue Oats Requested g - b w ' o V o m w_ O1 A e o 9 u 15 E a: 9 i'- Preservation Codes A HCL M N vaos) 8 ZAM N Nanaore C Zn AUYae 0 ASNa02 0 NMic APd P Na2Q4S E NaNSO4 0 Na2$03 F McON R Na2S203 0 AmdU4r S N SQ4 N Asmrb¢Abd T TSP DMenhy0rale I ob U Aortpfe K OmTAWr W pH 4-5 L-EOA 2-Mer(speary) Omer ny IMne Ai Requesmtl(day Sete Zip CA 92614 CaayilanCe Prcjaeb 4Yn No Phone 443-812-0046(Tel) PO DRT9 Emaiwor doug vrade@erm cum : fie. -E a ,b E ,� a LL Pmed Nacre. Storm Water • Amazon Warehouses Sde Sample Identification Projw S. 24024260 Sao". Sample Matrix Type (�� Sample (C=comp, o-..rw Sam le Date Time G rab enra.w.w Special InsWctronsMota Preservation Code: X- S 8 N _ it-qa nV-') 1-20 Ll1 08 l 00 Water j(,' Y _ 08 Water v� !II r II IIII IIIIIIIIIIIIIIIIIIIIIIIIIIiIIIII�IIIIIII� Chain of Custody Sam le Disposal(Ateemayn as- saw lfsamplps are retained longer than I Month) �Aetum To Client Daposal By Lab Archive For Months I IIIII� 660-208586 PSesble Haaanl ldentKcadon Non-HazardFlammable �Swn b7ttant Elporsnn 8 M Unfmom MAadiolu ical Deliverable Requested 1 II III N Other (specify) Special InstrucbonslUC Requirements Empty I(it Re inquahed by jDate 71me Method olshlpment Re"uWax! by Dame' 12 L Qom eM 6C R"vad by DalyTms - 2 D {I:Ur Canpany ReGeu by Dame Company Revived by V Oatamme' Cd^WM RalVnuislledbY Dama Company Rebhry by Damn -are, Cmipany Custody Seals Intact o Yes b No Custody Seal No Cmleriampaa¢de(a)ec vm Outer Remedy: n '7 2 ,a Login Sample Receipt Checklist Client: ERM-West .lob Number: 680.,208586.-1 Login Number: 208586 List Number:1 Creator: Padayao, Abigail - Question List Source: Eurofins TestAmerica, Savannah Answer Comment Radioactivity wasn't checked or is </= background as measured by a surrey NIA meter. The cooler's custody seal, if present, is intact. True Sample. custody seals, it present, are, intact True, The cooler or samples do not appear to have been compromised or True tampered mft... Samples were received on ice. True Cooler Temperature is- acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is.the Field. Sampler's. name present on. COC? True. There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A i2 Eurafins TestAmerica, Savannah Page 13 of 13 12/28/2021