WQ0033677_Groundwater Monitoring Report November 2021_20211214

GW-59A COMPLIANCE REPORT FORM Permit # Wk Qo314 77
(Suhmil Z-111 mmrit"hel period with GlY-59famor)
I
Enter date monitoring results were due. - ) WIII this monitoring report (GIN-59 and GW-59A)
YES
NO
be submitted after the established due the ?
2
Was any required info' motion missing on the GW-59 report fin ms?
YES
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification numb,r(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identifiwtioa plate, area overgrown, etc.)? Ifthe answer is "Yes'{ contact the Regional Ofce for guidance.
q
Are any monitored constituents equal to or above the established standards?
YES
NO
lithe answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concenbution(s)
exceeding standards in the space provided below.-
5
For the constituents Identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES" list in the space provided below, each well with constituents) exceeding
standards, concantration(s) reported, and sample collection data for each occurrence (for the last two years).
6
Are the monitoring wells listed in section 6 located al gr beyond the review boundary?
YES
NO
If the answer Is "YES", a groundwater qualityprob/em may be occurring. CONTACT THE REGIONAL
OFFICE /MMEDIA TELY FOR GUIDANCE. Iftheansweris"NO", monitoring wells maybe improperly
located; contact the Regional Office.
7
Is the permiHee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
lithe answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 71s "NO", contact the Regional Office within 90 dayI tl n may be
required to determine the impact the waste disposal system /s having at the review and compliance
boundaries surrognding this facility Failure to up so read s0gect the a "ttto a Notice of Violation,
lines. andrornenaltles.
g
The person completing this portion (GIN-59A) of the monitoring reportshould sign below and submit this
form with G W-59 forms for requ/red walls to the address provided at the top of the current GIN--59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report GIN-59A) is true andcomplete to the best of my knowledge.
Signatureo ermlftee(or Authonzed Agent) paw
GW-59A 12/8/2993

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wircnircCH LRBS.Inc.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms-Hatchery-MW#3 COLLECTIONDATE,
11/10/2021
PERMIT #: COLLECTION TIME:
13:15
ADDRESS: Case Farms Hatchery RECEIVED DATE:
11/10/2021
RECEIVED TIME:
15:15
REPORTFIT
101019n01
ANALYSIS
ANALYSIS
RESULTS
UNITS
DATE
ANALYST
TDS
101
mg/L
11/16/21
Conductivity
133
umhos/cm
11/11/21
Th
NH3
'U
mgll-
11/12/21
jrg
Chloride
11B
mg/L
11/190
Metals
pace
NO3-N
1.60
nnyL
11/15121
leg
TKN
1.40
mg/L
11/151TI
jdg
T. Nitrogen
3.00
mglL
11/15/21
Ida
T. Phosphorus
<0.16
mg/L
11/12/21
jog
LOG ID: 2111-217 REPORTED BY: NC CERTIFIED LAB # 50
S
Tony Gragg, Lab Supervisor

aceAnalj tical
www.pasileEe.ppm
ANALYTICAL RESULTS
Pace Analytical Servlees, LLC ,
1377 South Para Drive
KsreereVils, NO 27204
(704)977 Goal
Protect CASEFARMS
Pace Phu of NO.: 92672192
Sample: MW3METALS
La610: 9237219200E
C01lected: 11/1012113:15
Received: 1111112110:35 Matdx: Water
Parameters
Results units
RBPOrt Limit DF
Prepared
Analyzed CAS No. Qual
200.7 MET Me
Analytical Method: EPA 200.7Rev 4.41994 Preparation Method:EPA200.7Rev4.41%4
Pars Analyllcal SOMces-Asheville
Arsenic
ND "IL
0.010 1
1111812104:26
1111=114A8 7440.30-2 80
Dapper
ND m9IL
0.0060 1
11/182104:26
111182114:48 744050.8
Potioslum
ND m911-
- 5.0 1
11110104:28
1111"108:34 7440A9-7
Sadlum
8.3 mglL
5.0 1
11118210428
111192110:27 7440-23-5
Zinc
NO mgli-
0.010 1
11/18/2104:26
1111812114:48 7440-805
REPORT OF LABORATORY ANALYSIS
This repent shall not be unpmtluced, except In full,
Data: 11122120210488 PM without the Who, coherent of Pace Anelylloel Souvres,LLC.
Page 11 of34

a Pace Anelytloel Sarulcus, LLC
ace Analytical 1377SculhPork Pg.
www.p9wlehvcom
Ker,..Alle, NC 27284
(]04)8]]A881
ANALYTICAL RESULTS
Project CASEFARMS
Pace Project Ns.: 02572192
Gondola; MW3VOCS Lab ID: 92572182003 Collected: 11/10/2113:15 Received: 11/11/211035 Matrix: Water
Parameters Result. Unite Report Limit OF Prepared Analyzed CAS No. Quel
624 Volatile Organics
A,olydocl Method: EPA 024,1
Pace Analytical Se itae-Charlotte
Benzene
NO
of/L
1.0
1
111122114:36
71.43.2
BromodlWoromathane
NO
unlL
2.0
1
11112121 14:36
75.27-4
Bmmoform
NO
uglL
2.0
1
11/12/21 14:36
76.26-2
Bromomethane
NO
ugh-
2.0
1
1111212114:36
74.8342
Carbon tetrachloride
NO
ug/L
2.0
1
11/120 14:36
56-23-6
Chlambenzene
NO
ug/L
2.0
1
11/122114:36
108.90.7
Chiamethan.
NO
ug1l.
2,0
1
MUM 14:36
75-00-3
Chlorofoml
NO
ug/L
2.0
1
1111212114:36
07-66-3
Chloromethane
NO
uqd-
2.0
1
11/1212114:36
74-873
Dibromochloromethens
NO
uglL
2.0
1
it/12/2114:36
12A48-1
1,2-01Morob.nzene
NO
un/L
2.0
1
111122114:30
95-50-1
43-D1chlwob,g.ne
NO
ug/L
2.0
1
1111=11416
541-73-1
1,4-Dichiorobanzene
NO
Tilt.
2,0
1
11112/211T36
10040-7
1,1-D1ch1oroelhane
NO
ug/L
2.0
1
1111212114:36
7534-3
1,2D1c1-glmoethene
NO
ugrL
2,0
1
11112M 14:38
ig7-0B-2
1,1-DI.N.,eeihene
NO
uglL
2.0
1
11/12/21 14:30
75354
ci.-1,2-Dichl... too.
NO
ugrL
2.0
1
1111212114:36
166.W2
tran.-1,2-Dlchlom.thene
ND
ug1L
2.0
1
11/122114:36
166-60-5
1,2-Dichloropropene
NO
ug/L
2.0
1
III= 1436
78-ST-5
Ge-1,8-Olchbropropene
NO
ugh-
2.0
1
1111212114:36
10081-013
tran9-1,3-Dlchlmoprapene
ND
wilt.
2.0
1
11/12/21 14:30
10001-02-6
Ethylbenzane
NO
unit.
10
1
1111212114:35
100-01-4
Methylene Chloride
NO
uglL
2.0
1
11/122114:36
76-09.2
1,1,22-Tetrachloroathane
NO
ug1L
2,0
1
11/12121 14:30
79-34
Te rouldomethene
NO
uglL
2.0
1
11/122114:36
1274&4
Toluene
NO
ug(L
1.0
1
1111221 14:36
108-Sti
1,1,1-Tdchlomethone
NO
Tiff.
2.0
1
11/12121 14:36
71.55-6
1,1,2-Trichioroothare
NO
ug/L
2.0
1
11/1221 14:36
79.00-5
Tdchlor.elhene
NO
ugh-
2.0
1
11/122114:36
79-01-6
1'rlchloro0uoromethane
NO
ug1L
2.0
1
11A212114:36
75-69.4
Vinyl chloride
NO
uglL
2,0
1
11/12121 14:38
7504
Surrogates
4-Bremo6uorobenzene(S)
09
%
70-130
1
111122114:36
480-00-4
Toluene d8(S)
107
%
70-130
1
1111212114:3e
2037-6-5
1,2-Dlchioroethane d4(8)
98
%
70-13D
1
11112/2114:36
17060-07-0
REPORT OF LABORATORY ANALYSIS
This re podshol not be retooduced, axes,[In full,
Dale', 1 11221202104:98 PM rvlihout the wrSlen consent of Paco Anelyllcei SBMeae,LLC.
Page 8 of 34

Analytical Cnviromnental Services, Inc
Date! 22-Nov-21
Client:
Pace Analytical Services, Inc.
Client Smaple ID:
MW3
Project Name:
92572192
Caullatlon Date!
11110120211: MOOPM
Lab ID:
21111l
Matrix:
Agueona
Anniyaes
Reporting
Result Qaai Units DntablD
Marble
Date AoalYzed Analyst
Limit
Factor
Formaldehyde by SW8315A
Formaldehyde HRL 50 H tell. 326094 1 11/19/202122:00 DS
pvulllen: • Mlu«xae<damv1roloo omvmitoww el
IIPL Dolow,kelioth
N H<IdNg tlmtt(«VrcOmvtbn v<vnvlyeie yv«tleJ
N Aoalylo n<t NeLAC awlifmd
D A,wlybd<t<eled III heacm<Inledmethedblavk
> nNolar lrycn ltwullvWue
B Celimvt<d (seen nbov<gimntilefimu<ng<)
S aVlke 2<mvery ouplbe llMN dire to m<Irie
Nnrt au<e<eo �mreoaea
P NlvlyuA in tM1e lvb rvFleM1 6ndevt<Iian Lam lM m<IM1OA
a Lcvv olo. aowlt oaw
s mJmaud value Jaeclvl b<t<w 6epmina elmit page 28 of 34
oe en,e Ja

aceAnalyilcal e
www.pecsk s.
ANALYTICAL RESULTS
Pace Analytical Services, LLC
1377 South Perk Drive
Kernomvkle, NC 27284
(704f977 W81
ProJeol: CASE FARMS
Pace Project No.: 02572192
Be.,[.; MW3
Lab ID: 925M102001 Collected:
11/10013:15
Pauli 11/1112110:35 Matrix: Water
Poramclam
Results Whs Report Limit DP
Prepared Analyzed CAS No, Qual
2540C Total Dissolved Solid.
Analytical Method: SM 2540C.2015
Pace Analytical Services -Asheville
Total Dissolved Solid.
101 "ki
25.0 1
11/16/211021
4500 Chloride
Analytical Method: SM 4500-0I-E-2011
Pace Analytical Services -Asheville
Chloride
11.5 mg/L
1.0 1
11/10210735 18887-00-0
5310B TOC
Analy JwI Method: SM 531OB-2014
Pace AnelNlcel Services -Asheville
Total Organic Carbon
ND mg/L
1.0 1
11/182f 04:04 7440-44-0
REPORT OF LABORATORY ANALYSIS
Thin repodahall not be repmducw, , ekcapt T lull,
Data: 11122=2104:38 PM "bls the written wrxwtbf Pew Aw11U.l Services,LLC. Page 4 of 34

mjvrxRircCH LANSINc.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms-Hatchery-MW#4 COLLECTIONDATE.
11/10/2021
PERMIT#: COLLECTION TIME,
14:15
ADDRESS: Case Farms Hatchery RECEIVEDDATE..
11/10/2021
RECEIVED TIME:
15:15
REPORTED:
121912021
ANALYSIS
RESULTS
UNITS
DATE
ANALYST
FANALYSIS
104
mg/L
11/160
y
731
umhos/wn
17/1121
7h
<1.0
mg/L
11/12/21
],a
11.6
mgli.
11/19/21
pace
NO3-N
1.60
mglL
11/15121
leg
TKN
<1.0
mg/L
11/15/21
Jog
T. Nitrogen
1.60
mg/L
11/15/21
Jdg
T. Phosphorus
<0.16
mg/L
11/12/21
Jdg
LOG ID: 2111-218 REPORTED BY: NC CERTIFIED LAB # 50
l
Tony Gragg, Lab Supervisor

® Pece Artalytic0l Services, LLC
ace (7
Analytical 1377 South Park Ddve
Kemers0,
annapathis.'an NC2]2a4
(]04)B]]-0891
ANALYTICAL RESULTS
Prefect: CASE FARMS
Pace Pmfect No.: 92672192
Semple: MW4 METALS Let, ID: 9072192009 Colleaa.& 111101 /2114:15 Received: 11/11/2110:35 Matdx: Water
Paremetere Results What Report Limit DF Prepared Analyzed CAS No, Dual
200.7 MET ICP
Analytical Method: EPA200.7Rev 4.41904 Pmpamtion Method: EPA 200.7 Rev 4A 1994
Pace Analytical SeMces -Asheville
Arsenic
ND m911-
0,010
1
11/10104:26
11/19p2108:60
744030-2
Copper
ND mg)L
0,0060
1
111182104.26
11110121013:60
744MO.8
Potassium
ND mgli-
6.0
1
111181210425
11H8/2108:60
7440-09-7
Sodium
8.2 mg/L
5.0
1
11/18/21 04:26
11119?21 08:50
7440-23-5
Zinc
ND mglL
0.010
1
11118121 04:26
11/19121 0B:50
7440-66-6
REPORT OF LABORATORY ANALYSIS
ThIS report slmll not b0 rep ndnced. except In MI,
Date: 11122/202104:38 PM wldcut the ontan.oll.motf Pere Analytical Park., ILLQ. Page 12 of 34

Pace Analytical Services, LLC
aceAnaljftal ® 1377 South Perk OrWo
wwnpad1hsa4m Kemarevllle, NO 27264
(704)e77-0901
ANALYTICAL RESULTS
Prefed: CASE FARMS
Pace Project No.: 92672192
Sample: MW4V005 WOO: 92572192000 Collected: 11/1012114:15 Received: 1111112110:35 Metrlx: Water
Parameters Recalls Unlls Report Llmh OF Prepared Analynd CAS No, Oual
624 Volatile Organics
Anilylicol Method: EPA 624.1
Pace Analy9cal Services - Challelte
Belrsene
NO
ugly-
1.0
1
11/122114:64
71-43.2
Bromodichlomme llam.
NO
ug/L
2.0
1
11/1212114:64
7&27.4
Bromofa m
NO
ago,
2,0
1
11/12121 14:64
76.25Q
Bromomethane
NO
ugiL
2.0
1
1111212114:54
74.83-9
Carbon tatredrlorldo
NO
ugiL
2.0
1
11/122114S4
5e-235
Chlorobenzene
NO
ugiL
2,0
1
11/12/21 14:54
108-90.7
Chloroethane
ND
u911.
2.0
1
111122114:54
75-00-3
Chloroform
NO
ug/L
2.0
1
11/12/21 14.54
67-66-3
ChloromeNane
NO
ug/L
2.0
1
11/12/2114:54
74-873
Dibromoohloromelhene
NO
ug/L
2.0
1
1V122114:54
124-46-1
12-Dichlarobenzene
NO
ug/L
2.0
1
11/122114:54
95-50-1
1,3-Dlchlorobenzene
NO
ug/L
2.0
1
111122114:64
541.73-1
1,4-0Ichlarobenzene
NO
u91L
2.0
1
1111212114:64
105484
1,1-Olchlcroethane
NO
ug/L
2.0
1
11/12/21 14:54
75-34-3
1,2-Dichioroetheno
NO
ugly-
2.0
1
11/12/21 14:64
107-06-2
1,1-DIW4oroethene
NO
ug/L
2,0
1
1111MI 14:54
76.364
cls-1,2-Dlchlomethene
NO
ugiL
2.0
1
111120 14:54
156-59.2
Irens-1,2-Dichloroethen,
ND
ugiL
2.0
1
11/1221 14:54
156-60-5
1,2A1chloropropaum
NO
ug/L
2.0
1
11112114:64
78-875
ds-1,3-Dlchlompropene
NO
ugiL
2.0
1
1111221 14:54
10061-01-5
trens-0,&Olchloropropene
NO
ugiL
2.0
1
fi/122114:64
10061-02-6
Ethylbenzene
NO
ugiL
1.0
1
11/122114:64
100414
Methylena Chloride
NO
ugiL
2.0
1
11/12/2114:64
75-09-2
1,122-Tefrachloroethane
NO
ag/L
2.0
1
11/12/21 14:54
7934.6
Tetrachlomothane
NO
ug/L
20
1
111122114:64
127-18.4
Toluene
NO
ugly-
1,0
1
11112/21 14:54
108.88-3
1,1,1-Tridlloroethane
NO
ug/L
2.0
1
11/12121 14:64
71.566
1,1,2-Trichloroethane
NO
ug/L
2.0
1
11/12121 14:54
70-OM
T&N,andathene
NO
ugiL
2.0
1
1111212114:54
7 01.8
Trichloro0uommelhane
NO
ug/L
2.0
1
11/12/21 14:64
76-694
Vlayl chlodtla
NO
ugh-
2.0
1
11/12211464
75-01-4
Surrogates
4-Bromolluorobenzene(S)
95
%
70-130
1
11/12/21 14.64
460-00.4
Toluene-b8(S)
107
%
70-13D
1
11/12/2114:54
2037-265
1,2-Dichlaroethene-44(S)
90
%
70-130
1
1111221 14:54
17060-07-0
REPORT OF LABORATORY ANALYSIS
Thls repot shell not be reproduced. can In lull,
Date: 11/2212021 04:38 PM wltbcut the When consent of Pace Analytcal SeMms, LLC,
Page 9 of 34

Analytical Environmental Services, Inc
Datt: 22,Nnv-21
Cnenh
Pace Analytical Services,Inc.
Client 8nmple lD:
MW4
Project Name:
92572192
Collection Data;
I1/10/20212:15:00 PM
Lab ID:
211INS1-002
Matrix:
Aqueoas
Renornnu
Dlhninn
Formaldehyde by S W8315A
Formaldehyde Dn
eunlmeee: �
vmnee.ewa: mnxbvnmw�lmminnnlevel
ORL nelaxrtpJXlup llmil
N
Hultling lime[Wepmpueullon o, vnolyAv waeaN
N
Alwlylellol NI1LAC«nlaetl
n
Amlylo tlalxled In lha ovaooiohd moNod blollk
>
OreouMau.11 value
Imil Qual units natcelD Factor Dote Analyztd Analyst
50 H ug/L 326094 1 11/191202122:11 DS
e MMOMO tvoluo ebN qunnliblionm So
a Slike AeeoveryouttWe llmik ave x mMli.
Nnrt $W EoeOnmmlivu
r Andyml in Ne lobwhl,h hndeulollon s.,hemelLad
c IFulllu�Rprnll wino
I e,amel«Lellxseleolenbanwawenmsumu Pe9e 29 of 34

mowrmirrm LRBS.Inc
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 26630
[phone]
SAMPLE: Case Farms-Hatchery-MW#5 COLLECTIONDATE..
11/10/2021
PERMIT #: COLLECTION TIME:
13:45
ADDRESS: Case Farms Hatchery RECEIVED DATE:
11/10/2021
RECEIVED TIME:
15:15
REPORTED.:
12/9/2021
ANALYSIS
ANALYSIS
RESULTS
UNITS
DATE
ANALYST
TDS
106
mg/L
11/16121
Conductivity
133
umhos/cm
11/1121
Th
NH3
<1.0
mg/L
11112121
Jrg
Chloride
11.9
mg/L
11/1921
Metals
pace
NO3-N
1.50
mg/L
11115/21
lag
TKN
1.10
mg/L
11/15/21
Jog
T. Nitrogen
2.60
mg1L
11/15/21
jdg
T. Phosphorus
c0.16
mg/L
11/1221
Jdg
LOG ID: 2111-219 REPORTED BY: NC CERTIFIED LAB It 50
Tony Gragg, Lab Supervisor

®
Pace Analytical Senlcae, LLC
aceAnalytica!
1377 800h Perk Orlve
www.peealebe.wm
ae,nereNlle. NO 27284
(704)977-058f
ANALYTICAL RESULTS
Project: CASE FARMS
Pace Pmfed No.'. 925721 M
Semple: MW5 METALS
Lab 10: 92572192010 Colleclad: 11/102113:46
Received: 11/11M 1035 Matrix: Wale,
Parameters
Reaclts Units Report Limit DF
Prepared
Analyratl CAS No. Duel
200.7 MET HOP
Analytical Method; EPA200.7 Rev 4.41094 Preparation Method: EPA200.7 Rev 4.41994
PaceAn rlylical Selvicss-Asheville
Arsenic
NO mglL 0.010 1
1111812104:20
11118/21 15 01 7440-3&2
Copper
NO mglL 0.0050 1
11/182104:26
IV182116:01 7440-60.8
Potassium
ND mg/L 5.0 1
11/18/21 04:20
11/18/21 15:01 7440-09-7
Sodium
8.9 WIL 5.0 1
11/182104:26
11/162116:01 7440-235
Zinc
ND mg/L 0.010 1
11/1812104:25
1111812115:01 7440-80-6
REPORT OF LABORATORYANALYSIS
The report shell net be mpmduced, except In full,
Dabs: 11 t2M02104:38 PM waOopRhe wnaen consent of Pace AnaW.1 SeMcae,LLC. Page 13 of 34

Para Anelyllaal eeMcae, LLC
aceAnalytical a 1377 somh Pe,a rove
waM'.peoeNbrom, Kernersvllle, NC 27284
[phone]
ANALYTICAL RESULTS
Projeoh CASE FARMS
Pace Project No.: 925721P2
Semple: MW5VOCS Lab 11925721B2007 Collectetl', 11/10/2113:45 Recelvad: 71/71/211036 Matrix: Water
Perorate. Results Units Report Limit OF Prepared Analyzed CAS No, qual
624 Volatile Organics
Analydool Method: EPA 024.1
Pace Analytical Senleae-Charlotte
Benzene
NO
ug/L
1.0
1
11/12121 15:12
71.43-2
Bromodichlommethana
NO
u91L
2.0
1
11/122116:12
76-274
Bromoform
NO
ugf-
2.0
1
111122115:12
75-25.2
Bromomethans
ND
ui
2.0
1
111122115:12
7483-9
Carbon tetrachloride
NO
ug1L
2.0
1
11/1221 15:12
66-23-5
Chlorobatlzene
NO
ug/L
2.0
1
111120 16:12
108-90-7
Chloroethane
ND
ug l-
2,0
1
11/1212116:12
76-005
Chloroform
NO
u0/L
2.0
1
11/12/21 16:12
67-66-3
Chlommethane
ND
ugA.
2.0
1
111122115:12
74-874
Dlbromochlcromathane
NO
ug1L
2.0
1
11/122116:12
1244E.1
1Z01chiorobenzene
NO
ugh-
2.0
1
11/12/21 11512
95-50.1
1,3-Dichlembenzene
NO
ui
2.0
1
111122116:12
641-73.1
1,40chlombanzene
NO
uglL
2.0
1
11/122115:12
101
1,1-Dlchlorcethane
NO
ug/L
2.0
1
11/1221 15:12
764VI3
1,2-Dlchlomethans
NO
ug1L
2.0
1
11/1201 15:12
107-06.2
1,1-Dichloroethene
NO
ug1L
2.0
1
11/12121 15:12
75-36-4
cia-1,2-Dlchlorcathene
ND
staff.
2.0
1
11/12/21 15:12
166.59-2
imne-1,2-Dlchlommin.ne
NO
u01L
2,0
1
11112M 15:12
168-60-6
1,2-DIchlcropropene
NO
uglL
2.0
1
111120 15:12
7&8i
cis-1,3-Dlchleroproperbs
NO
ui
2.0
1
111122115:12
10061-01.5
Imns1,3-Olchloropropene
NO
ug4
2,0
1
111122115:12
10061-02.8
Ethylbenzene
ND
ug/L
1.0
1
11/12/21 15:12
100-414
Methylene Chloride
ND
ug/L
2.0
1
111IT2115:12
75.09.2
1,1,2,2-Tetrachicmatheme
NO
ug1L
2.0
1
111120 16',12
79.34.E
Te6achloroelhene
NO
ugd-
2.0
1
11/12121 15A2
127-18.4
Talons
NO
ug/L
1.0
1
11/12/21 15:1Z
108.88-3
1,1,14dd1monathane
NO
ug(L
2.0
1
1111212116:12
71-56A
1,1,2-Tdchioleethana
ND
ug1IL
2.0
1
11/12/21 16:12
70-005
Tdchlonoethene
NO
ug/L
2.0
1
111122116:12
7B-01.6
Tdchloro0uoromelhane
NO
ug/L
2.0
1
11M22115:12
76.6g-0
Vinyl chlodde
NO
ug1L
2.0
1
11/122115:12
75-01-4
Sid"g. es
4-Bihnu luombenzene(B)
99
%
70.130
1
1111221 15:12
460.004
Toluene-de(8)
110
%
70-130
1
1111221 1512
2037.2E-5
1,2-Dichlomethane-d4(S)
93
%
70-130
1
11/1212115:12
17060.07.0
REPORT OF LABORATORY ANALYSIS
This open shall not be reproduceb, except in mq
Dale: 111221202104:38 PM without the wtllom content of Pace AnahlIctl Services,Mo.
Page 10 of 34

Analytical Ei vironmental Services, Inc
Dote: 22-Nmv 21
Client;
Puce Aaalyfical 5ervices, Inc.
Client Semple ID:
MW5
PmJeet Nerni
92572192
Collection Dnto:
11/10/20211:45:00 PM
Leb ID:
211IN81-003
Karl.:
Aqueous
Reoa[thle
❑ilnlinn
Fonnaldebyele by SW8315A
Formaldehyde
Quaid— a
WlneevuNewaMumemw"diddiuvol
HU. odlawrepmlmeliell
H
HoWlu&Ilnvs lur P�eW�^eenonmlyeir eaeatled
m
A dildium NIMADedefud
U
Anvlym demclM In tho onwielod iwlbod blank
>
ammmr@onnemllwbm
11e91.11 Limit
Yen
Ualte
DabehlD
Feeler
Da/OAteelyud
Analyst
on 50
H
eg/6
32609A
1
IVIW202122:22
DS
C GiimorcA (value ebove q�mmllneon mn8e)
e SpsF tacdodry uumide limits doe m mmnK
Nert sewmoumeve
P AunlyeM In Wo laL wM1ieh is a Mviedmo fieeuhe meAmd
Lua dun CemC'um
eulmmw.nwoen:nabanw nepenms l:enl Page 30 of 34

ace Analytical
ANALYTICAL RESULTS
Paco Aaalyllael Sarvluos,LLC
1371 South Pad, Call
Hor llle, NO 27264
(704)e77-0681
Project: CASEFARMS
PeroProject No.: M572192
Semple: all
Lab ID: 02572ID2003 Colleted:
1111012113:45
Received. 11Hi12110:35 Matrix: Water
Padaudane
Reeull. Units Report
Limit
OF
Prepared Analyzed CAS No. Ouel
2540C motel Dlaeolved Solid.
Analytical Method: SM 254OC-2015
Pace Analytical Service. - Ashevllle
Total DSsclved Solids
106 al
26.0
1
1111612110:21
4500 Chloride
Anelyllcal Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
11.9 ral
1,0
1
1111912107:37 16887-00.6
6310B MC
Analytical Method', SM 531OB-2014
Pace Analyllcel Sandal -Aahaville
Total OrOenlc Carbon
NO anal
1.0
1
1111712122: 19 744044-0
REPORT OF LABORATORY ANALYSIS
This heart shell rot be repmdured, except in lull,
Date: 11/22@02104:38 PM atthat the written consent or Pace Analytical Services, LLC.
Page 6 of 34

mRTER TECH LRBS.Inc
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE: Case Farms-Hatehery COLLECTIONDATE:
11/10/2021
PERMIT A COLLECTION TIME:
14:15
ADDRESS: Case Farms Hatchery RECEIVED DATE:
11/10/2021
RECEIVED TIME:
15:15
REPORTED:
12/9/2021
ANALYSIS
ANALYSIS
EFFLUENT
UNITS
DATE
ANALYST
BOO
596
mg/L
11/11121
jug
TSS
180
mg/L
11/12121
jrg
NH3
3.77
mglL
11/1221
jrg
Fecal Coliform
>2400
/100ml-
11/1021
Th
Conductivity
986
umhoslcm
11/11121
Th
NO3-N
'GA
mglL
11/15/21
lag
TKN
95.00
mg/L
11/1521
jdg
T. Nitrogen
95.00
mpl-
11/15/21
jdg
T. Phosphorus
6.36
mg/L
11/12121
jug
Chloride
65.5
mg1
11/19/21
TDS
590
mgll-
11/16M
LOG ID: 2111-216 REPORTED BY: NC CERTIFIED LAB It 50
Tony Gregg, Lab Supervisor

ace Analytical'
www.paehebaoom
ANALYTICAL RESULTS
Pace Analytical aarvioes, LLC
1377 South Park Drive
Kemencele, NC 27204
[phone]
Project: CASEFARMS
Pace PmJect No.: 92672192
Sample: EFFLUENT
Lab 10: 925721920M Collected: 1111012114:45
Received: 1111MI 10:35 MaUla: Water
Pemmatom
R... Its Unit. Report Limit DF
Prepared Anelyaed CAS No. anal
2640C Total Dissolved Solid.
Analytical Mothad: SM 2540C-2015
Pace Analytical Sercices-Asheville
Total Dissolved Solids
590 mg/L 62.5 1
11/1612110:21
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical P.M.. -Asheville
Chiefs.
65.5 mglL 3.0 3
11/1912107:46 16887-00-6
REPORT OF LABORATORY ANALYSIS
This report shall not be rapradumd, except In full,
Data 11/221202104.38 PM wlihout the wntan ppnsam of Pace Rnelyllcal Sampe,LLC.
Page 7 of 34

5 Pinewood Plaza Drive-P.O.'Box 1056
Granite Falls, NC 26830
Phone [phone] - Fax [phone]
CLIENT: Case Farms Hatchery PHONE NUMBER: 828-438.6900 ext,6975
clo Cindy McGinnis TYPE SAMPLE:
WeManager
No. LOCATIONS:
TT q
SAMPLER NAMB.T05G/
Sam Is
Collection
Information
TYPE
CONTAINERS
Sample Lopation
Faclllt Name
DATE
TIME TEMP,
ANALYSIS REQUIRED
Grab/
. No
Plastic/
Com site
Glass
Effluent
� I Pop
orl(cl)
Grab
8
Plastic
Fecal Collform, Chloride, TDS
BOD-5, TSS, Conductivity
NO3-N,TKN, NH3-N
__ .........
.
Monitoring Well #3
1 t. ...�
+
I ;1�
Q
Grab
1fl
Plastic/
TDS, Chloride, MBAS,
1
Glass
Formaldehyde, Conductivity
As, Cu. K, Zn, Na
NH3-N. NO3-N, T.P., TKN
TOC
VOC(Annual Nov, ant
Monitoring Well#4
fl
�(C"
11
Grab
12
Plastic/
Same As #3
1
Glass
Monitoring Well#5 II
I3;-S,i
Grab tp Plastic/
Glass Same As#3
Relinquished y:
Date:
Time:
Recleved Date:
I�
to l
I5,15
ellnqulehed By:
Date:
Time:
. 1 - 0 ],�7/3
R elved By Date:
PRESERVATION:
WCcol40C
kjH2SO4
()NaOH
UHNO3
flDechlornating Agent
(j Other
ryo
SAMPLE TEMP. @LAB 3,�
Chlorine RosidualLC7_J mill!
NC CERTIFIED LAB # 50