WQ0034806_Residual Annual Report 2021_20220218

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0034806
Applicant/Permittee Coastal Farms and Residuals,LLC
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office Wilmington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Martin Mabe
Email Address* Phone Number*
[e-mail] 3363121396
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0034806
Has Current Existing permit number
Applicant/Permittee Address* 8155 Malpass Corner Road,Currie,NC 28435
Facility Name* Coastal Farms and Residuals Class B Residuals Program
Please provide comments/notes on your current submittal below.
Coastal Farms and Residuals,LLC-2021 Class B Annual Report(WQ0034806)
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
Coastal Farms-2021 Annual Report WO0034806.pdf 38.49MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature
CP rz W
Submission Date 2/18/2022

2021 ANNUAL REPORT
LAND APPLICATION PROGRAM
COASTAL FARMS AND RESIDUALS, LLC
PERMIT #WQ0034806
Prepared For:
Coastal Farms and Residuals,LLC
8155 Malpass Corner Road
Currie,North Carolina 28435
Compiled By:
Willcox&Mabe Soil Solutions,PLLC
7231B Summerfield Road
Summerfield,North Carolina 27358
February 2022

4
�r 1,
willcox&rnabe
SOIL SOLUTIONS
February 18,2022
NCDEQ-DWR Non-Discharge Compliance Unit
512 North Salisbury Street
9th Floor Office#942X
Raleigh,North Carolina 27604
Attention: Non-Discharge Compliance Unit
Reference: 2021 LAND APPLICATION ANNUAL REPORT
Coastal Farms and Residuals,LLC
Permit No. WQ0034806
WMSS Project No. 15-19 Ph:01
Non-Discharge Compliance Unit:
Willcox&Mabe Soil Solutions,PLLC(WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Coastal Farms and
Residuals,LLC. WMSS compiled this report using data gathered during the compliance
year by Coastal Farms and Residuals, LLC. This data includes: 1)certification form, 2)
residuals analyses and pathogen/vector data, 3)application summaries and field loading
rate reports,4)soil analyses.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact Coastal Farms and Residuals,LLC or WMSS for further
assistance.
Sincerely,
Willcox&Mabe Soil Solutions,PLLC
Martin Mabe
NC Land Application/Residuals Operator
#22753
Enclosures
5hared\WMSS Projects1201 511 5-1 9 Coastal Residuals12021 Annual Report12021 ANNUAL REPORT-COASTAL FARMS.doc
Willcox&Mabe Soil Solutions,PLLC 17231 B Summerfield Road!Summerfreld,NC 27358/Rob 336.339.9128 or Marlin
336.312.1396!www.willcoxmabesoil,com

TABLE OF CONTENTS
SECTION NO. TITLE
I Certification Form
II Residuals Analyses &Pathogen/Vector Attraction Data
III 2021 Application Summary and Field Loading Rate Reports
IV Soil Analysis

CERTIFICATION FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0034806 County: Pender Year: 2021
Facility Name(as shown on permit): Coastal Farms and Residuals, LLC
Land Application Operator: Mr. Wesley Wooten Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
El Yes 0 No -If No,skip Part A,and Part B and proceed to Part C. Also,If residuals were
generated but not land applied,please attach an explanation on how the residuals were handled.
Part A-Residuals Application Summary:
Total number of application fields in the permit:1 12
Total number of fields utilized for land application during the year: 7
Total amount of dry tons applied during the year for all application sites:I 861.87
Total number of acres utilized for land application during the year: 407.7
Part B -Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below)issued by the Division of Water Quality. p Yes ❑ No
If no please, provide a written description why the facility was not compliant,the dates,and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least
6.0 or the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)
copies of laboratory results are attached.
4) Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are
5) All other monitoring was performed in accordance with the permit and reported during the year as required and
three(3)copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a)or the Pollutant
Loading Rates in 15A NCAC 02T.1105(b)(applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40
CFR Part 503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with(applicable to 40 CFR
Part 503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or,in the case of a deviation,
prior authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations
are attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals,as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application ofresiduals.
Part C- Certification:
"I certify, under penalty of law,that the above information is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Mr. Wesley W000ten, President 1/25/2022
Permittee Name and Title(type or print) Signature of Pe ittee Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T .1102(26)
DENR FORM ACF (12/2006)

RESIDUAL ANALYSES
TCLP ANALYSES IF REQUIRED
AND PATHOGEN AND VECTOR ATTRACTION REDUCTION

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding laboratory analysis.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number WQ0034806 Laboratory 1)Environmental Chemist,Inc.
Facility Name Coastal Residuals 2)
NPDES# See Below 3)
WWTP Name See Below 2021 DATA
RESIDUAL ANALYSIS DATA
NPOES# W00030775 NC0023256 W00005790 NC0002305 WQ0034367 W00037287 W00005849 W00013200 W00029955 WQ0000795
WWTP Name Avendale Carolina Beach Oak Island WWTP Lear Corporation NW Regional WRF Pluris Hampstead North Topsail _ SE Brunswick Summerhouse Surf City WWTP
Composited/Grab 12/27/21 11/05/21 _ 08/02/21 _ 04/22/21 03/25/21 03/08/21 01/20/21 06/03/21 02/10/21 10/28/21
Percent Solids 2.53 1.77 2.07 4.28 3.8 0 3.02 4.07 3.4 0.7 2.14 I
PARAMETERS(mg/kg dry weight)
Arsenic 30.80 _ 30.10 27.40 15.70 26.10 17.70 22.40 25.60 31.60 30.70
Cadmium 30.80 30.10 13.70 10.20 13.00 16.20 11.90 20.70 31.60 30.70
Copper 87.70 291.00 239.00 62.80 335.00 207.00 134.00 249.00 92.70 394.00
Lead 30.80 30.10 13.70 10.20 20.70 16.20 11.90 20.70 31.60 30.70
Mercury 0.64 0.94 1.30 0.390 0.62 0.57 0.41 0.68 2.390 _ 0.75
Molybdenum 30.80 30.10 13.70 10.20 13.00 16.20 11.90 20.70 31.60 30.70
Nickel 30.80 r 30.10 13.70 10.20 13.00 16.20 11.90 20.70 31.60 30.70
Selenium 30.80 30.10 13.70 10.20 13.00 16.20 - 11.90 20.70 31.60 30.70
Zinc 2,070.00 320.00 1,270.00 273.00 875.00 560.00 2,390.00 806.00 1,540.00 3,45000
TKN 77,100.00 73,100.00 20,200.00 39,400.00 36,500.00 70,100.00 38,500.00 62,900.00 57,800.00 53,800.00
Ammonia-Nitrogen 7,340.00 1,950.00 11,900.000 3,980.00 1,190.00 1,790.0D 2.46 4,790.00 1,510.00 1,200.00
_
Nitrate-Nitrogen 4.63 _ 3.44 12.60 2.00 4.21 14.30 _ 15.50 4.20 _ 28.50 20.60
Total Phosphorus 30,900.00 23,900.00 5,310.00 18,000.00 31,000.00 23,000.00 31,800.00 2,270.00 18,200.00 22,400.00
RESIDUAL ANALYSIS DATA
NPDES# W00023261 NC0057703 NC0026611
WfP Name Swansboro The Cape Morehead City -
W
Composited 1 Grab 03/24/21 12/10/21 03/18/21
Percent Solids 2.74 2.14 16.6
PARAMETERS(mg/kg dry weight)
Arsenic 36.40 44.10 10.50 t
Cadmium _ 18.20 44.10 3.68
Copper 228.00 166.00 741.00
Lead 18.20 44.10 15,40
Mercury 0.61 0.90 0.82 - -
Molybdenum 18.20 44.10 4.64
Nickel 18.20 44.10 11.50 -
Selenium 18.20 44.10 6.69
Zinc 3,720.00 4,060.00 904.00
TKN 56,000,00 73,900.00 61,700.00
Ammonia-Nitrogen 4,090,00 2,780.00 0.602 - -
Nitrate-Nitrogen 90.60 3.95 2.16
Total Phosphorus 22,400.00 30,200.00 32,500.00 -
X N/A due to number of sources
(SIGNATURE OF PREPARER) DATE
I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
1

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 27,2021
Avendale WWTP Permit No.WQ0030775
2.53 %Solids
6.6 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 7.710 77,100.000 154.200
Phosphorus 3.090 30,900.000 61.800
Potassium 0.644 6,440.000 12.880
PAN(injected)* 2.827 28,272.630 56.545
PAN(surface)* 2.460 24,602.630 49.205
Ammonia Nitrogen 0.734 7,340.000 14.680
Calcium 1.890 18,900.000 37.800
Calcium Carbonate Eq. --- --- ---
Magnesium --- 3,420.000 6.840
Sodium --- 4,310.000 8.620
Sulfur --- --- ---
Nitrate N/Nitrite N --- 4.630 0.009
Barium --- --- --- SAR
Chloride --- --- --- 1.20
Iron --- --- --- Ceiling Concen.
Aluminum --- 8,850.00 17.700 (Mg/Kg)
Arsenic --- 30.80 0.062 75
Cadmium --- 30.80 0.062 85
Chromium --- 30.800 0.062 --
Copper --- 87.70 0.175 4,300
Lead --- 30.80 0.062 840
Mercury --- 0.640 0.001 57
Molybdenum --- 30.80 0.062 75
Nickel --- 30.80 0.062 420
Selenium --- 30.80 0.062 100
Zinc --- 2,070.00 4.140 7,500
Environmental Chemists# 2021-22770
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are Iisted as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS,LLC
WQ0034806
Avendale WWTP
tat 1111'1 g
12/27/21 74,075 4.8697
12/27/21 68,670 4.8368
12/27/21 66,946 4.8257
12/27/21 101,266 5.0055
12/27/21 106,195 5.0261
12/27/21 75,118 4.8757
12/27/21 68,966 4.8386
Total 34.2781
Average 4.8969
Geometric Mean 100118A63.iii Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B -Alternative 1 Pathogen Reduction
requirement.

Environmental Chemists, Inc.
envirachen 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
s Nlf J� -'sp:i. 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
a s;_ x 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Lewis Farms& Liquid Waste, INC. Date of Report: Jan 17, 2022
8155 Malpass Corner Road Customer PO#:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2021-22770
Project ID: Aqua-Sludge Il►1 ile
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56937 Site:Aqua-Sludge 12/27/2021 7:32 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids(%) SM 2540 B 2.16% 12/27/2021
Fecal Density SM 9221C E-2014 74075 MPN/g 12/27/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56938 Site: 1 12/27/2021 7:33 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 2,33% 12/27/2021
Fecal Density SM 9221C E-2014 68670 MPN/g 12/27/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56939 Site: 2 12/27/2021 7:34 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2,39% 12/27/2021
Fecal Density SM 9221C E-2014 66946 MPN/g 12/27/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56940 Site: 3 12/27/2021 7:35 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.37% 12/27/2021
Fecal Density SM 9221C E-2014 101266 MPN/g 12/27/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56941 Site:4 12/27/2021 7:36 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.26% 12/27/2021
Fecal Density SM 9221C E-2014 106195 MPN/g 12/27/2021
Report 4:: 2021-22770
Page 1 of 3

Environmental Chemists, Inca
'..1.eitviro.6hent.:ti 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
r Y.51'sm- 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
r ":514,''k ' 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info rr environmentalchemists.com
Lewis Farms& Liquid Waste, INC. Date of Report: Jan 17. 2022
8155 Malpass Corner Road Customer PO#:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2021-22770
Project ID: Aqua-Sludge laike+^a4-1 C.
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-56942 Site: 5 12/27/2021 7:37 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 2,13% 12/27/2021
Fecal Density SM 9221C E-2014 75118 MPN/g 12/27/2021
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
21-56943 Site: 6 12/27/2021 7:38 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 2-32% 12/27/2021
Fecal Density SM 9221C E-2014 68966 MPNIg 12/27/2021
Repoli ff.: 2021-22770
Page 2 of 3

:r y� ,s, , , Environmental Chemists, Inc.
,1erivlroctle 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
y, 710 Bowsertawn Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
x !� = ' 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoiyenvironmentalchemists.com
Lewis Farms& Liquid Waste, INC. Date of Report: Jan 24, 2022
8155 Malpass Corner Road Customer PO#:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2021-22770 Project ID: Aqua-Sludge IeLe ` le_
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
21-56944 Site: Sludge 12/27/2021 7:30 AM Solid/Sludge Client
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200.7,Rev.4.4,1994 8850 mg/kg 01/04/2022
Arsenic EPA 200.7.Rev.4.4,1994 <30.8 mg/kg 01/04/2022
Cadmium EPA 200.7,Rev.4,4,1994 <30.8 mg/kg 01/04/2022
Calcium EPA 200.7,Rev.4.4,1994 18900 mg/kg 01/04/2022
Chromium EPA 200.7,Rev 4.4,1994 <30.8 mg/kg 01/04/2022
Copper EPA 200.7,Rev.4 4,1994 87.7 mg/kg 01/04/2022
Lead EPA 200.7,Rev.4.4,1994 <30,8 mg/kg 01/04/2022
Magnesium EPA 200 7,Rev.4.4,1994 3420 mg/kg 01/04/2022
Molybdenum EPA 200.7,Rev.4.4,1994 <30.8 mg/kg 01/04/2022
Nickel EPA 200.7,Rev.4.4,1994 <30.8 mg/kg 01/04/2022
Potassium EPA 200.7,Rev.4.4,1994 6440 mg/kg 01/04/2022
Selenium EPA 200.7,Rev.4.4.1994 <30.8 mg/kg 01/04/2022
Sodium EPA 200.7,Rev.4.4,1994 4310 mg/kg 01/04/2022
Zinc EPA 200.7,Rev.4.4,1994 2070 mg/kg 01/04/2022
Nitrate+Nitrite-Nitrogen EPA 353.2 4.63 mg/kg 12/28/2021
Total Solids (%) SM 2540 B 2.53% 12/27/2021
Ammonia Nitrogen SM 4500 NN3 C-2011 7340 mg/kg 12/28/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011 77100 mg/kg 12/28/2021
Total Phosphorous SM 4500 P(F-H)-2011 30900 mg/kg 12/30/2021
pH SW e46 Method 9045D 6.60 units 01/14/2022
Result estimated, Analyzed out of 15 minutes hold time.
Mercury SW-B48 7471 8 <0.640 mg/kg 01/05/2022
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report it. 2021.22770
Page 3 of 3

ENVIRONMENTAL CHEMISTS, INC OFFICEindmil Way
2 3'IFAX910-392-44245
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Lewis Farms& Liquid Waste PROJECT NAME: 4e40 Sl REPORT NO: 2. 1 —22 77 O
ADDRESS: CONTACT NAME: Wesley Wooten PO NO:
REPORT TO: Martin Mabe/Mahe-Wilcox _PHONE/FAX:
COPY TO: email:
Sampled By: IE..:s e.✓aw+5 SAMPLE TYPE: I=Influent, E=Effluent,W=Well,ST=Stream,SO=Soil, SL=Sludge,Other:
Collection y PRESERVATION
Sample Identification a s o o 5 (7 c = = m
c ° Cs in c a t m z 'o $ o w ANALYSIS REQUESTED
Date Time _ Temp U " 3 2 x S z c
/1-44Af 1"'= c P
Sludge G G Siv941-1 X Full T Nutrients/Metals
pi_ C P
I „ G G 5 4937 X Fecal Density/%TS
4"-- C P "—
2 G G 83i X Fecal Density/%TS
4 }' C P
3 G G SLa 439 X Fecal Density/%TS
4 s Ca9'4C o
X Fecal Density/%TS
C P
5 G G 54 X Fecal Density/%TS
6 X Fecal Density/%TS
}sr C P
7 G G tJ(CA 43
X Fecal Density/%TS
Transfer Relinquished By: Date/Time Received By: DateiTime
I.
2.
Temperature when Received: Accepted: Re'ected: Resample Re nested:
Delivered By: Received By: ../—r Date: / t 1- tr I Time: /J-It-
Comments: TURNAROUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: Coastal Farms and Residuals,LLC WQ Permit Number: WQ0034806
WWTP Name: Avendafe WWTP NPDES Number: WQ0030775
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) 0 Alt B(Alk Treatment)❑ Alt. C(Prior Testing)❑
AIt.D(No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ ,
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying, ❑ Heat Treatment ❑ Thermophilie ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ ' _
Class B: lAIt.(1)Fecal Density p Alt. (2)Process to Significantly Reduce Pathojens ❑
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ I Air Drying ❑ Composting ❑ Aerobic Digestion 0
P 1= g
Anaero
bic Digestion ❑ �_ : .:<:::•. ..; ::
If applicable to alternative performed (Class A or Class B)complete the following monitoring data:
Number p Analytical
Parameter Allowable Level Pathogen Density Excee- FrequenY cy Sample Te h-
in Sludge Minimum Geo.Mean Maximum Units deuces of Anal sisType nirnie
2 x'lobo the MPN`' 66,946 78,863 106,195 MPN/g 0 Annual Grab SM922ICE
6th power
per gram of CPU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
weight) •
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T.1107)-Please indicate alternative performed:
Alt.l (VS reduction) ❑ Alt.2(40-day bench) ❑ •Alt. 3(30-day bench) ❑ Alt.4(Spec.O,uptake) ❑
Alt. 5(I4-Day Aerobic) ❑ Alt.6(Alk. Stabilization ❑_Alt 7 (Drying-Stable) ❑ Alt.8(Drying-Unstable) ❑
Alt.9(Injection) p Alt. I0(Incorporation) 11 No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT(please check the appropriate statement)
C7 "1 certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
❑ "I certify,under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 1SA NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kirklyn Fields,ORC Wesley Wooten,President
Preparer Name and Title(type or print) Land Applier Name and Title(if applicable)(type or print)
hUift./ — /24712 2/7/22 , 1/24/22
Signature ofdireparer* Date Signature of L d Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
DENR FORM PVRF 02T(12/2006)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: November 5,2021
Carolina Beach WWTP Permit No.NC0023256
1.77 %Solids
6.9 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 7.310 73,100.000 146.200
Phosphorus 2.390 23,900.000 47.800
Potassium 0.553 5,530.000 11.060
PAN(injected)* 2.330 23,298.440 46.597
PAN(surface)* 2.232 22,323.440 44.647
Ammonia Nitrogen 0.I95 _ 1,950.000 3.900
Calcium 1.570 15,700.000 3 I.400_
Calcium Carbonate Eq. --- _- -_-
_
Magnesium --- 3,670.000 7.340
Sodium --- 6,380.000 12.760
Sulfur --- --- ---
Nitrate N/Nitrite N --- 3.440 0.007
Barium ___ ___
--- SAR
Chloride --- --- --- 1.58
Iron --- --- --- Ceiling Concen.
Aluminum --- _ 30,800.00 61.600 (Mg/Kg)
Arsenic --- 30.10 0.060 I 75
Cadmium --- 30.10 0.060 85
Chromium --- 30.I00 0.060 --
Copper --- 291.00 _ 0.582 4,300
Lead --- 30.10 _ 0.060 840
Mercury --- 0.944 0.002 57
Molybdenum _ --- 30.10 0.060 75
Nickel _ 30.10 0.060 420
Selenium --- 30.10 0.060 100
Zinc --- 320.00 0.640 7,500
Environmental Chemists# 2021-19655
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits arc listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Carolina Beach WWTP
11/05/21 72,581 4.8608
I1/05/21 66,327 4.8217
11/05/21 62,500 4.7959
11/05/21 32,985 _ 4.5183
11/05/21 41,579 4.6189
11/05/21 78,314 4.8938
11/05/21 45,403 4.6571
Total 33.1665
Average 4.7381
Geometric Mean Fecal Coliform MPN I gram
Geometric Mean of Less than 2,000,000 meets Class B -Alternative 1 Pathogen Reduction
requirement.

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Environmental
� Chemists, Inc.teliViii010110111:0
v �f4 a,,
6602 Windmill Way,Wilmington,NC 28405 . 910.392.0223 Lab • 910 392 4424 Fax
' +ram '- r' 4•r` 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
4{a,ti �� * , �Y'sr � iSMi
'` {emu., ,?.s ` _ 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Town of Carolina Beach Date of Report: Nov 24, 2021
1121 North Lake Park Blvd Customer PO#:
Carolina Beach NC 28428 Customer ID: 08100295
Attention: Bill Raymond Report#: 2021-19655
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-49167 Site: Sludge 11/5/2021 8:00 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Chlordane (TCLP) SW 846 8081 B <0.02 mg/L 11/11/2021
Endrin (TCLP) SW-846 8081 B <0.0005 mg/L 11/11/2021
Heptachlor(TCLP) SW-846 8081 B <0.0005 mg/L 11/11/2021
Heptachlor epoxide (TCLP) SW-846 8081 s <0.0005 mg/L 11/11/2021
Lindane (TCLP) SW-846 8081 B <0.0005 mg/L 11/11/2021
Methoxychlor(TCLP) SW 846 8081 B <0.0005 mg/L 11/11/2021
Toxaphene (TCLP) SW-846 8081 B <0.05mg/L 11/11/2021
2,4,5-TP (TCLP) SW-846 8151 A <0.003 mg/L 11/10/2021
2,4-D (TCLP) SW-846 8151 A <0.003 mg/L 11/10/2021
1,4-Dichforobenzene (TCLP) SW-846 8270 E <0.050 mg/L 11/11/2021
2,4,5-Trichlorophenol (TCLP) SW-846 8270 E <0.050 mg/L 11/11/2021
2,4,6-Trichlorophenol (TCLP) SW-846 8270 E <0.050 mg/L 11/11/2021
2,4-Dinitrotoluene(TCLP) SW-846 8270 E <0.050 mg/L 11/11/2021
Cresol (TCLP) SW-846 8270 E 0.097 mg/L 11/11/2021
Hexachloro-1,3-butadiene (TCLP) SW-846 8270 E <0.050 mg/L 11/11/2021
Hexachlorobenzene (TCLP) SW-846 8270 E <0.050 mg/L 11/11/2021
Hexachloroethane (TCLP) SW-846 8270 E <0.050 mg/L 11/11/2021
m + p-Cresol (TCLP) SW-846 6270E 0.097 mg/L 11/11/2021
Nitrobenzene (TCLP) SW-846 8270 E <0.050 mg/L 11/11/2021
o-Cresol (TCLP) SW-846 8270 E <0.050 mg/L 11/11/2021
Pentachiorophenol (TCLP) SW-6468270E <0.250mg/L 11/11/2021
Pyridine (TCLP) SW-846 8270 E <0.050 mg/L 11/11/2021
1,1-Dichloroethylene (TCLP) SW-846 Method 8260D <0.01 mg/L 11/13/2021
1,2-Dichloroethane (TCLP) SW-046 Method 8260D <0.01 mg/L 11/13/2021
Benzene(TCLP) SW846 Method 8260D <0.01 mg/L 11/13/2021
Carbon Tetrachloride (TCLP) SW-846 Method 8280D <0.01 mg/L 11/13/2021
Report#:: 2021-19655

Environmental Chemists, Inc.
1_.,Einvirochewi L, 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab ° 910.392.4424 Fax
t ,� -=•". 710 Bowsertown Road,Manteo,NC 27954 • 252,473.5702 Lab/Fax
:. F 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info@ environmentalchemists.corn
Town of Carolina Beach Date of Report: Nov 24, 2021
1121 North Lake Park Blvd Customer PO#:
Carolina Beach NC 28428 Customer ID: 08100295
Attention: Bill Raymond Report#: 2021-19655
Project ID: Sludge
Chlorobenzene (TCLP) SW-846 Method 8260D <0,01 mg/L 11/13/2021
Chloroform (TCLP) SW-846 Method 8260D <0.01 mg/L 11/13/2021
Methyl ethyl ketone (TCLP) SW-846 Method 82800 <0.05 mg/L 11/13/2021
Tetrachloroethylene(TCLP) SW-846 Method 8260D <0.01 rng/L 11/13/2021
Trichloroethylene (TCLP) SW-846 Method 8260D <0,01 mg/L 11/13/2021
Vinyl Chloride (TCLP) SW-846 Method 8260D <0.01 mg/L 11/13/2021
RCI
Cyanide SM 4500 CN D 3.84 mg/kg 11/15/2021
Sulfide SM 4500 S D 1.74 mg/kg 11/22/2021
Ignitability SW 846 method 1010 >200 of 11/12/2021
pH SW 846 Method 9045D 6.90 units 11/08/2021
Result estimated. Analyzed out of 15 minutes hold time.
Sludge Residuals
Arsenic EPA 200.7 <30.1 mg/kg 11/18/2021
Cadmium EPA 200.7 <30.1 mg/kg 11/18/2021
Calcium CPA 200.7 15700 mg/kg 11/18/2021
Capper EPA 200.7 291 mg/kg 11/18/2021
Lead EPA 200.7 <30.1 mg/kg 11/18/2021
Magnesium EPA 200,7 3670 mg/kg 11/18/2021
Molybdenum EPA 200.7 <30.1 mg/kg 11/18/2021
Nickel EPA 200.7 <30.1 mg/kg 11/18/2021
Potassium EPA 200.7 5530 mg/kg 11/18/2021
Selenium EPA 200.7 <30.1 mg/kg 11/18/2021
Sodium EPA 200.7 6380 mg/kg 11/18/2021
Zinc EPA 200.7 320 mg/kg 11/18/2021
Aluminum EPA 200.7,Rev.4.4.1994 30800 mg/kg 11/18/2021
Chromium EPA 200.7,Rev.4.4,1994 <30.1 mg/kg 11/18/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 3.44 mg/kg 11/08/2021
Total Solids (%) SM 2540 t3 1.77% 11/05/2021
Ammonia Nitrogen SM 4500 NH3 C-2011 1950 mg/kg 11/08/2021
Report tr.: 2021.19555

Environmental Chemists, Inc.
.�erivirocher�' 6602 Windmill Way,Wilmington,NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax
"^~ �r� 4 r cs' 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
. :,:rr ' i.:t e C 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Town of Carolina Beach Date of Report: Nov 24, 2021
1121 North Lake Park Blvd Customer PO#:
Carolina Beach NC 28428 Customer ID: 08100295
Attention: Bill Raymond Report#: 2021-19655
Project ID: Sludge
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011 73100 mg/kg 11/08/2021
Total Phosphorus SM 4500 P F-2011 23900 mg/kg 11/12/2021
Mercury SW-946 7471 B <0.944 mg/kg 11/18/2021
TCLP Metals
Arsenic EPA 200.7,Rev.4.4,1994 <1.0 mg/L 11/16/2021
Barium EPA 200.7,Rev.4.4,1994 <1.0 mg/L 11/16/2021
Cadmium EPA200.7,Rev.4.4,1994 <1.0mg/L 11/16/2021
Chromium EPA200.7,Rev.4.4,1994 <1.0mg/L 11/16/2021
Lead EPA 200.7,Rev.4.4,1994 <1.0 mg/L 11/16/2021
Selenium EPA 200.7,Rev.4.4,1994 <1.0 mg/L 11/16/2021
Silver EPA 200.7,Rev.4.4,1994 <1.0 mg/L 11/16/2021
Mercury EPA 245.1 <0.0002 mg/L 11/12/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-49168 Site: Sludge 11/5/2021 8:05 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 1.86% 11/05/2021
Fecal Density SM 9221C E-2014 72581 MPN/g 11/05/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-49169 Site: Sludge 11/5/2021 8:06 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) sM 2540 a 1.96% 11/05/2021
Fecal Density SM 9221C E-2014 66327 MPNIg 11/05/2021
Lab ID Sample ID: Collect DateITime Matrix Sampled by
21-49170 Site:Sludge 11/5/2021 8:07 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1,92% 11/05/2021
Fecal Density SM 9221C E-2014 62500 MPN/g 11/05/2021
Report#:: 2021-19655 ,

v Environmental Chemists, Inc.
A. envirochent ,,, 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
i •,.,, - " #y v tS, 710 Bowsertown Road,Manteo,NC 27954 • 252 473 5702 Lab/Fax
r�sr F a., £ 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Town of Carolina Beach Date of Report: Nov 24, 2021
1121 North Lake Park Blvd Customer PO#:
Carolina Beach NC 28428 Customer ID: 08100295
Attention: Bill Raymond Report#: 2021-19655
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-49171 Site: Sludge 11/5/2021 8:08 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 6 1.91 % 11/05/2021
Fecal Density SM 9221C E-2014 32985 MPN/g 11/05/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-49172 Site: Sludge 11/5/2021 8:09 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.90% 11/05/2021
Fecal Density SM 9221C E-2014 41579 MPN/g 11105/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-49173 Site: Sludge 11/5/2021 8:10 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 FI 1.66% 1110512021
Fecal Density SM 9221C E-2014 78314 MPN/g 11105I2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-49174 Site: Sludge 11/5/2021 8:11 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2541:1 8 1.74% 11/05/2021
Fecal Density SM 9221C E-2014 45403 MPN/g 11105/2021
Comment: Sludge residual reported on a dry weight basis.
Reviewed by: '7 , {.e(t `,,
7
Report#;; 2021-19655

Environmental Chemist, Inc., Wilmington, NC Lab#94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:t ra K-Q BEA{ -�ln)f`J Dater t 5 02-� Rq tPJ�
� Report Number: 02, � — I �P
Receipt of sample: ECHEM Pickup 0 Client Delivery`]
❑ YES ❑ NO ,r4 UPS ❑ FedEx 0 Other 0
N/A 1. Were custody seals present on the cooler?
❑ YES 0 NO A. N/A 2. if custody seals were
Original temperature upon receiptresent p � were they intact/unbroken?
5 °C Corrected temperature upon receipt 'C
How temperature taken: 0 Temperature Blank k Against Bottles
iR Gun iD:Thomas Traceable 5/N 192511657 1R Gun Correction Factor°C: 0.0
❑ YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
K` YES 0 NO 4. Were proper custody procedures (relinquished/received)followed?
qYES 0 NO 5. Were sample ID's listed on the COC?
YES 0 NO 6. Were samples iD`s listed on sample containers?
YES 0 NO 7. Were collection date and time listed on the COC?
YES 0 NO 8. Were tests to be performed listed on the COC?
YES 0 NO 9. Did samples arrive in proper containers for each test?
YES ❑ NO 10. Did samples arrive in good condition for each test?
''E3 0 NC/ 11. vas adequate saniple volume available?'
YES ❑ NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH >12?
0 YES ❑ NO 15. Were sulfide samples received at a pH>9?
❑ YES 0 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2504 HNO3 MCI NaOH
Time of preservation: if more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

eri ENVIRONMENTAL CHEMASTS, INC OFI Windmill 103 202 Wilmington,NC
2a
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Lewis Farms & Liquid Waste PROJECT NAME: zZ40 dew t GJi...!Y REPORT NO: 2...L' — I t'to s-� ~
ADDRESS: CONTACT NAME: Wesley Wooten PO NO:
REPORT TO: Martin Mabe/Mabe-Wilcox PHONE/FAX:
COPY TO: email:
Sampled By: Lcy•Je...jSAMPLE TYPE: I=Influent, E=Effluent, W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection w i. a, a PRESERVATION
Sample identification E . , c� ` _j o m
r- E tD c ° r E m g z --1 ii o 0 o w ANALYSIS REQUESTED
Date Time Temp �' a " S z °z z _ _ o
h/ �! Y n� C P
Sludge G G X Full TCLP, RCI, Nutrients/Metals
r C P
1 G G X Fecal Density/%TS
' PI C P _
2 G G _ X Fecal Density/%TS
fag. _ C P -
3 G G X Fecal Density/%TS
9t C P
4
G G X Fecal Density)%TS
as C q P
5 G G X Fecal Density/%TS
"t C P
6
G G X Fecal Density/%TS
2-- C P
7 G G _ X Fecal Density/%TS
Transfer Relinquished By: Date/Time Received By: Date/Time
1.
2.
Temperature when Received: Accepted: !------- Rejects Resample Re a d:
Delivered By: Received By: %/5 -�,�� Date: /r 4-1 Time: j�`1-
Comments: TU NAROUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals,LLC WQ Permit Number: WQ0034806
WWTP Name: Carolina Beach WWTP NPDES Number: NC0023256
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A(tithe/temp) ❑ Alt B (Alit Treatment)❑ Alt. C(Prior Testing)❑
AIt.D(No Prior Test) ❑ Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thertnophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ _ .
•
Class B: Alt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens 0 '
If applicable to alternative performed (Class B only) indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen Density Number of Analytical
Parameter > Excee- Frequency Sample Tech-
in Sludge Minimum Geo. Mean Maximum Units tiences of Analysis Type
moue
2 x 10 to the MPN 32,985 54,711 78,314 MPN/g 0 Annual Grab SM922 iCE
6th power
per gram of
Fecal Coliform total solids CPU
000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
colilcnn) weight)
Vector Attraction Reduction (15A NCAC 02T.1107)- Please indicate alternative performed:
Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4(Spec. 0,uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alit. Stabilization ❑ Air 7(Drying- Stable) ❑ Alt_8(Drying-Unstable) ❑
•Alt. 9(Injection) 0 Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT(please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
0 "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
William Raymond, CIRC: Wesley Wooten, President
Preparer Name and Title (type or print) Land Applier Name and Title(if applicable)(type or print)
_._fzlL.._ �_ 7 . i 1129J21
Signature f repave : Date Signature of La Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1 102(26)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: August 2,2021
Oak Island WWTP Permit No.WQ0005790
2.07 %Solids
8.41 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
, (%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 2.020 20,200.000 40.400
Phosphorus 0.531 5,310.000 10.620
Potassium _ 0.246 _ 2,460.000 4.920
PAN(injected)* 1.440 14,402.600 28.805
PAN(surface)* 0.845 8,452.600 16.905
Ammonia Nitrogen 1.190 11,900.000 _ 23.800
Calcium 4.380 43,800.000 87.600_
Calcium Carbonate Eq. - -__ ---
Magnesium --- _ 2,660.000 5.320
Sodium --- 2,610.000 5.220
Sulfur -__ ___
Nitrate N/Nitrite N --- 12.600 0.025
Barium --- --- --- SAR
Chloride --- --- -__ 0.47
Iron --- _ --- --- Ceiling Concen.
Aluminum --- 3,790.00 7.580 (Mg/Kg)
Arsenic _ --- 27.40 0.055 75
Cadmium --- 13.70 0.027 85
Chromium --- 17.300 0.035 ---
Copper --- _ 239,00 0.478 4,300
Lead --- 13.70 0.027 840
Mercury - 1.30 0.003 57
Molybdenum --- 13.70 0.027 75
Nickel --- 13.70 0.027 420
Selenium --- 13.70 0.027 100
Zinc --- 1,270.00 2.540 7,500
Environmental Chemists ti 2021-12892
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS,LLC
WQ0034806
Oak Island WWTP
......... ....
08/02/21 6,763 3.8301
08/02/21 5,671 3.7537
08/02/21 20,000 4.3010
08/02/21 8,375 _ 3.9230
08/02/21 _ 5,979 3.7766
08/02/21 4,620 _ 3.6646
08/02/21 4,818 3.6829
Total 26.9320
Average 3.8474
Geometric Mean 7f € Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction
requirement.

Z=\ r' �rf �,�++.}. Environmental Chemists, Inca
Y1 -: orien7 6602 Windmill Way,Wilmington,NC 28905 • 910.392.0223 Lab • 910.392.4424 Fax
7:4-:i , w;`mi,,"•:* ¢s- - �' iid 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
... 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoaenvironmentalchemists.corn
Lewis Farms & Liquid Waste, INC. Date of Report: Aug 20, 2021
8155 Malpass Corner Road Customer PO#:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2021-12892
Project ID: Oak Island
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-32255 Site: Sludge 8/2/2021 7:30 AM Solid/Sludge Wesley Wooten
Test Method Results Date Analyzed
Chlordane (TCLP) SW 846 Method 8061B/3510 <0.02 mg/L 08/09/2021
Endrin (TCLP) SW 846 Method 8081 B/3510 <0.0005 mg/L 08/09/2021
Heptachlor(TCLP) SW 846 Method B0B1B/3510 <0.0005 mg/L 08/09/2021
Heptachlor epoxide (TCLP) SW 846 Method 8081 B/3510 <0.0005 mg/L 08/09/2021
Lindane(TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 08/09/2021
Methoxychlor(TCLP) SW 846 Method 80B1 B/3510 <0.0005 mg/L 08/09/2021
Toxaphene(TCLP) SW 846 Method 8081B/3510 <0.05 mg/L 08/09/2021
1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0,050 mg/L 08/06/2021
2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021
2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021
2,4-Dinitrotoluene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021
Cresol (TCLP) sW 846 method 8270/3510 <0.050 mg/L 08/06/2021
Hexachloro-1,3-butadiene (TCLP) SW 646 method 8270/3510 <0.050 mg/L 08/06/2021
Hexachlorobenzene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021
Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021
m + p-Cresol(TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021
Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021
o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021
Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 08/06/2021
Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 08/06/2021
2,4,5-TP (TCLP) SW846 Method 8151A <0.003 mg/L 08/10/2021
2,4-D(TCLP) 5W846 Method 8151A <0.003 mg/L 08/10/2021
1,1-Dichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 08/05/2021
1,2-Dichioroethane (TCLP) SW846 Method 8260/5030 <0.01 mg/L 08/05/2021
Benzene(TCLP) SW846 Method 8260/5030 <0.01 mg/L 08/05/2021
Carbon Tetrachloride(TCLP) SW846 Method 626015030 <0.01 mg/L 08/05/2021
Report*: 2021-12892
•
Page 1 of 4

` 1,^ _w-- Environmental. Chemists, Ines
G "'�"r 4i r a 1
" ' 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
.- i b cat S .Y f hf-++R+ 5 :.•r
4r,?. . _.#�,` ,,ice' a�' . . 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
>''%� }`q'tj.' F ISMS
��:::.�_ 255 A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
environmentalchemists,com
Lewis Farms & Liquid Waste,INC. Date of Report Aug 20, 2021
8155 Malpass Corner Road Customer PO#:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2021-12892
Project ID: Oak Island
Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 08/05/2021
Chloroform (TCLP) SW846 Method 8260/5030 <0,01 mg/L 08/05/2021
Methyl ethyl ketone (TCLP) SW846 Method 826D/5030 <0.05 mg/L 08/05/2021
Tetrachloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 08/05/2021
Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 08/05/2021
Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 08/05/2021
RCI
Cyanide SM 4500 CN D <1 mg/kg 08/03/2021
Sulfide sM 4500 s o 11.8 mg/kg 08/09/2021 '
Ignitability SW 846 method 1010 >190°F 08/05/2021
Sludge Residuals
Aluminum EPA 200.7 3790 mg/kg 08/03/2021
Arsenic EPA 200.7 <27.4 mg/kg 08/09/2021
Cadmium EPA 200.7 <13.7 mg/kg 08/03/2021
Calcium EPA 200.7 43800 mg/kg 08/03/2021
Chromium EPA 200.7 17.3 mg/kg 08/03/2021
Copper EPA 200,7
239 mg/kg 08/03/2021
Lead EPA 200.7 <13.7 mg/kg 08/03/2021
Magnesium EPA 200.7 2660 mg/kg 08/03/2021
Molybdenum EPA 200.7 <13.7 mg/kg 08/03/2021
Nickel EPA 200.7 <13.7 mg/kg 08/03/2021
Potassium EPA 200.7 2460 mg/kg 08/03/2021
Selenium EPA 200.7 <13.7 mg/kg 08/03/2021
Sodium EPA 200.7 2610mg/kg 08/03/2021
Zinc EPA 200.7 1270 mg/kg 08/03/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 12.6 mg/kg 08/05/2021
Total Solids (%) SM 2540 a 2,07% 08/02/2021
pH SM 4500 H B 8.41 units 08/05/2021
Result estimated. Analyzed out of 15 minutes hold time.
Ammonia Nitrogen SM 4500 NH3 C 11900 mg/kg 08/05/2021
Report f,' 2021-12892
Page2of4

F v y Environmental Chemists, Inca
b , -i s•,
;t: en. IrQ� e a 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
ems. ,, ��,�y, ; :,_#}. �,� . 710 8owsertown Road,Manteo,NC 27954 252.473.5702 Lab/Fax
��s: 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infol environmentaichemists.com
Lewis Farms & Liquid Waste, INC. Date of Report: Aug 20, 2021
8155 Malpass Corner Road Customer PO#:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2021-12892
Project ID: Oak Island
Total Kjeldahl Nitrogen (TKN) SM 4500 Org 8 20200 mg/kg 08/05/2021
Total Phosphorus SM4500 P F 5310 mg/kg 08/09/2021
Mercury 5WB4B 7471 B 1.30 mg/kg 08/06/2021
TCLP Metals
Arsenic EPA 200.7 <1.0 mg/L 08/09/2021
Barium EPA 200.7 <1.0 mg/L 08/09/2021
Cadmium EPA 200.7 <1.0 mg/L 08/09/2021
Chromium EPA200.7 <1.0mg/L 08/09/2021
Lead EPA200.7 <1,0 mg/L 08/09/2021
Selenium EPA 200.7 <1.0 mg/L 08/09/2021
Silver EPA 200.7 <1.0 mg/L 08/09/2021
Mercury EPA 245.1 <0.0002 mg/L 08/06/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-32256 Site: 1 8/2/2021 7:35 AM Solid/Sludge Wesley Wooten
Test Method Results Date Analyzed
Total Solids(%) SM 2540 B 1.39% 08/02/2021
Fecal Density SM 9221C E-2014 6763 MPN/g 08/02/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-32257 Site:2 8/2/2021 7:36 AM Solid/Sludge Wesley Wooten
Test Method Results Date Analyzed
Total Solids(%) SM 2540 B 1,94% 08/02/2021
Fecal Density SM 9221C E-2014 5671 MPN/g 08/02/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-32258 Site:3 8/2/2021 7:37 AM Solid/Sludge Wesley Wooten
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 1.75% 08/02/2021
Fecal Density SM 9221C E-2014 20000 MPN/g 08/02/2021
Report#:: 2021-12892
. Page 3 0(4

`% o , Environmental Chemists, Inc.
4
iiik- Ylviiii IiE', 6602 Windmill Way,Wilmington,
",;�,;, �,��,'x,. ca• . ,� �g: Y g ,NC 28405 910.392.0223 Lab + 9�Q.392.4�24 Fax
•'� -: 'T'i,�W. ".c. - 710 8owsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
.,�, <? 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Lewis Farms & Liquid Waste, INC. Date of Report: Aug 20, 2021
8155 Malpass Corner Road Customer PO#:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2021-12892
Project ID: Oak Island
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-32259 Site:4 8/2/2021 7:38 AM Solid/Sludge Wesley Wooten
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.03% 08/02/2021
Fecal Density SM 9221C E-2014 8375 MPN/g 08/02/2021
Lab ID Sample 1D: Collect Date/Time Matrix Sampled by
21-32260 Site:5 8/2/2021 7:39 AM Solid/Sludge Wesley Wooten
Test Method Results Date Analyzed
Total Solids(%) SM 2540 B 1.84% 08/02/2021
Fecal Density SM 9221C E-2014 5979 MPN/g 08/02/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-32261 Site:6 8/2/2021 7:40 AM Solid/Sludge Wesley Wooten
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 1,71 % 08/02/2021
Fecal Density SM 9221C E-2014
4620 MPN/g 08/02/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-32262 Site: 7 8/2/2021 7:41 AM Solid/Sludge Wesley Wooten
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.64% 08/02/2021
Fecal Density sM 9221C E-2014 4818 MPN/g 08/0212021
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: 4 ,D 0.*il
•
Report#:: 2021-12592
Page 4of4

Environmental Chemist, inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client ES F-PAZAA S Date: 8/ /c3Ri Report Number: —
Receipt of sample: ECHEM Pickup 0 Client Delivery 0 UPS 0
CI YES ❑ NO FedEx 0 Other 0
N/A 1. Were custody seals present on the cooler?
❑ YES 0 ND R N/A 2. if custody seals were present, were theyintact/unbroken?temperature upon receipt 5 °C r cn receioken?
.
Corrected temperature upon receipt °C
How temperature taken: 0 Temperature Blank ,i Against Bottles
IR Gun ID: Thomas Traceable 5/N 192511657 iR Gun Correction Factor°C: 0.0
❑ YES 0 NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
2 YES 0 NO 4. Were proper custody procedures(relinquished/received)followed?
II YES 0 NO 5. Were sample ID's listed on the COC?
Ii YES 0 NO 6. Were samples tD's fisted on sample containers?
11 YES 0 NO 7. Were collection date and time listed on the COC?
'■ YES 0 NO 8. Were tests to be performed listed on the COC?
Ii YES 0 NO 9. Did samples arrive in proper containers for each test?
iw YES 0 NO 10. Did samples arrive in good condition for each test?
■• YES 0 NO 11. Was adequate sample volume available?'
cst YES 0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH>12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH >9?
0 YES 0 NO 16. Were NH3/TKN/phenol received at a chlorine residual of<0.5 m/L.
z {x
0 YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
0 YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
• Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding(circle one): H2SO4 HNO3 HCi NaOH
Time of preservation: If more than one preservative is needed, notate in comments below _
Note:Notify customer service immediately for incorrectly preserved samples Obtain a new sample or
notify the state lab if directed to analyzed by the customer, Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

. ENVIRONMENTAL CHEMISTS INC 6602 Windmill Way Wilmington,NC 28405
7 OFFICE:910-392-0223 FAX [phone]
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS: DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Lewis Farms &Liquid Waste PROJECT NAME: 7:..- a J4e r-1/,,4 REPORT NO: 4,_02,-/ — /2.-1'4 L
ADDRESS: -CONTACT NAME: Wesley Wooten PO NO:
REPORT TO: Martin Mabe/Mahe-Wilcox PHONE/FAX:
COPY TO: email:
Sampled By: eissr._ Waal.-- SAMPLE TYPE: I=Influent,E=Effluent,W=Well, ST=Stream,SO=Soil,SL=Sludge,Other:
•
Collection 2, - �, a PRESERVATION
Sample Identification Q o 'e 5 o W
a ~ Co a d r E m g `t d o $ o o ANALYSIS REQUESTED
to Time Temp u 0 z z = z Z z
-
C P
Sludge G G 4LL� X Full TCLP, RCI, Nutrients/Metals
71-3r C P -
1 G G ' 5` X Fecal Density/%TS
2
4. le C P
G G X Fecal Density/%TS
*,t C P eq
3 G G X Fecal Density/%TS
1 \ �-le C P
4 G G S X Fecal Density/%TS
t 1..39 C P 05
G G X Fecal Density/%TS
'P.: C P ( -
6 G G X Fecal Density)%TS
��/ C P 0/7 -
' G G X Fecal Density/%TS
Transfer Relinquished By: Date/Time Received By: Date/Time
1.
2. _
Temperature when Rec ived: Accepted: / Rejected: Resample Re ted: -
•
Delivered By: l s/� A Received By: lTh��--- Date: 1f c t Time: "I}'�4
Comm ents:
T AROUND:
•
` y 1 2',Lt _, 43...id o �4-4"-- ��I

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM f021' Ruts)
Facility Name: Coastal I:oats and Result_ak,1.LC WO Permit ;Nu relict: \'.,.. t;t-•:
11'11"i'P Nome: Oak island 1VWTP °I'l)i:ti�vrrrh�r. t
Monitoring Period: From I'lr2021 To 12 31 0t_ 't _ -
I'athogen Reduction(iSA NCAC 02T.1106)- Please indicate level:chief ed and allern rti%c ptr f„rrtic(I:
Class A: Alt. A i trine`tern1') :J Alt B(Alk Ireatincntt0 Alt (''Pi i.: Ic.11I) I Jt
Alta)(No Prier Test) ❑ I I'rc:cc.:s to ruittfer Red:,_ ['. •i;+r .,:u 2 J ,
If applicable to alternative perforated((lase A cads)indic•are"Process to Further Rtduce l'.ttha_+ci1.'-:
Compost El1 Heat Drviii YI - Heat Ire-,tnrent ❑ Ilunno•ftrltc iJ
Beta Ray D Gamma Rav _l Pasteurization Li
Class B: All. (1)Fecal Density (rJ Alt_ (2)Process to!*nrticantly'Reduce 1'jt]t;a cils
If applicable to alternatit c performed(Class II only)indicate-Process to Si+nilic:tatty Reduce Patho,i.as-:
Lint,Stabilization ❑ Air Diving 0 1 ('ornpostiny 0 Aerobic I)1.-e-ttco:: 0
1
Anaerobic Digestion ❑
If applicable io alternative perforated (Class A or Class B)complete tire following.monitarini,data:
All Lt ael Patho Ctl Eli Density -Ntit t er++r •1
Parameter — - 1=\ccc- ,hrc. .t s_nrrl�
an Sludge Minis un-Geo. Mean Maximum l nits 0t Ail1t.•,1. r)[,_
2 t 10 to the It1'V
ttlh power I
p=r_earn of
Fecal Collforrn total solids CFI?
1000 mina per gun 'of tetsF solid (dry .),(110 7.03S 20.000 \MPN+�, to Annual t ir.il+ s:q,"'tt i
weight)
Saiman:lta b.Lteria 3 hIP\per 4 guano
on lieu of Taal total solid idn
colrlornrl wetolri1
Vector A Attraction Reduction i1SA NCAC )2T.1'07)- Please indicate alternative performed:
Alt.I (VS rcducrloal LiIAli.2(4t-day bench) ] Al(.3(30-day bench) 0 Alt 4'Siv; t7i,u;•:.r',et ;_1-
Alt.5(14-Day Aerobic) D Ali h(Alt: Stabilization U Alt 1(Drying-Stable) A Alt `(1 try lne l'n:,,.thlc t J
AE( 9(Injection) [1 Alt I tlncorpt'ratiolil 0- No teeter attraction ream tloa;lirm BLit..:etc 11.1 f"inc.! J
CERTIFICATION STATEAIE,NT(please check the appropriate statement)
!] "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.l 10o and the
vector attraction reduction requirement in 15A NCAC 021'.1107 have been nmet.-
J "I certify. under penalty of law,Mal the pathogen requirements in 15A NC.AC 02T.i l06 and the
vector attraction reduction requirement in 15A NCAC 02•f.1107 hare nor heel] met." (Plr.'1.e"1,,
if you check this statement attach an oplanation wiry you have not met one or both of the
requirements.)
"This determination 11;1s been made under lily direction and supervision in accordance with the s}sietii
designed to ensure (lint qualified personnel properly gather and evaluate the information used to deternnne
that the pathogen and vector attraction reduction requirements have been reei. I 3111 :mate that there are
significant [lenailies far raise certification including line:ltltl itstllt'iti011mei11.
Kenny Von Voigt,ORC' -, \Ye-do WAooten, Pi esident
Preparer Name and'-tie '-A-n'6Cpc i - -°� Lind :111pht'r Name and Talc(if.y:l,l'ic ihle)(tt pi.-or Nuns
.: c3:7"- -, -._.4....-------; ://\
S-7,ll.tture of Preparer' Date tit nature of I .rnt pplier l i r'applic.,hlc l Date
'Prepaid is defined in 40 CFR Parr 503 9(r)and 1SA bil'At '1' I l02 t2(+r
DENR FORM 1'VI.i U. (l2 €F.';)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 22,2021
Lear Corporation WWTP Permit No.WQ0005849
4.28 %Solids
6.71 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
-
Nitrogen(TKN) 3.940 39,400.000 78.800
Phosphorus 1.800 18,000.000 36.000
Potassium 0.320 3,200.000 6.400
PAN(injected)* 1.461 14,608.000 29.216
PAN(surface)* -
1.262 12,618.000 25.236
Ammonia Nitrogen 0.398 3,980.000 7.960
Calcium 1.080 10,800.000 21.600
Calcium Carbonate Eq. --- --- __-
Magnesium --- 2,230.000 4.460
Sodium _ --- _ 2,080.000 4.160
Sulfur --- --- ---
Nitrate N/Nitrite N --- 2.000 0.004
Barium --- --- --- SAR
Chloride --- --- --- 0.98
Iron --- --- --- Ceiling Concen.
Aluminum --- 57,800.00 115.600 (Mg/Kg)
Arsenic --- 1 5.70_ 0.031 75
Cadmium --- 10.20 0.020 85
Chromium --- 10.200 --- --
Copper --- - 62.80 0.126 4,300
Lead --- 10.20 0.020 840
Mercury --- _ 0.39 0.001 57
Molybdenum --- 10.20 0.020 75
Nickel --- 10.20 0.020 420
Selenium _ --- 10.20 _ 0.020_ 100
Zinc --- 273.00 0.546 7,500
Environmental Chemists#2021-06585
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits arc listed as detection limits
for calculation purposes.

' nx
d-mom Environmental Chemists, Inc®
`., ° 0 2 0 9 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
.4i`' • -, ,I :Y ',`. 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
or,'' ' LI 5- -- �`� 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info@environmentalchemis ts.com
Guilford East Date of Report: May 25, 2021
1754 NC HY 903
W Customer PO#:
Kenansville NC 28349 Customer ID: 11030018
Attention: George Yankay Report#: 2021-06585
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-16413 Site: sludge 4/22/2021 3:00 PM Solid/Sludge lewis farms
Test Method Results Date Analyzed
Chlordane (TCLP) SW 846 Method 8081813510 <0.02 mg/L 04/30/2021
Endrin (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 04/30/2021
Heptachlor(TCLP) SW 846 Method 60818/3510 <0.0005 mg/L 04/30/2021
Heptachlor epoxide (TCLP) SW 846 Method 808113/3510 <0.0005 mg/L 04/30/2021
Lindane(TCLP) SW 846 Method 808113/3510 <0.0005 mg/L 04/30/2021
Methoxychlor(TCLP) SW 846 Method 8081B/3510 <0,0005 mg/L 04/30/2021
Toxaphene(TCLP) SW 846 Method 8081 B/3510 <0.02 mg/L 04/30/2021
1,4-Dichlorobenzene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/04/2021
2,4,5-Trichlorophenol (TCLP) 5W 846 method 8270/3510 <0.050 mg/L 05/04/2021
2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/04/2021
2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/04/2021
Cresol(TCLP) SW 846 method 8270/3510 0.716 mg/L 05/04/2021
Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/04/2021
Hexachlorobenzene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/04/2021
Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/04/2021
m + p-Cresol (TCLP) SW 848 method 8270/3510 0.716 mg/L 05/04/2021
Nitrobenzene(TCLP) 51N646 method 8270/3510 <0.050 mg/L 05/04/2021
o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/04/2021
Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 05/04/2021
Pyridine(TCLP) SW 846 method 8270/3510 <0.050 rnglL 05/04/2021
pH SW 846 Method 90450 6.71 units 05/05/2021
Result estimated. Analyzed out of 15 minutes hold time.
2,4,5-TP (TCLP) SW846 Method B151A <0.003 rng/L 05/03/2021
2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 05/03/2021
1,1-Dichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 04/30/2021
1,2-Dichloroethane (TCLP) SW846 Method 8260/5030 <0.01 mg/L 04/30/2021
Report#:: 2021-06585
Page 1 of 3

14
-iwis',0.FAtioff� y,r� r 5 EnvironmentalChemists, Inc.
Y cieh t ` 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
r`T,l'"�: i .� 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
.r`; A '`5- 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Guilford East Date of Report: May 25, 2021
1754 NC HWY 903 Customer PO#:
Kenansville NC 28349 Customer ID: 11030018
Attention: George Yankay Report#: 2021-06585
Project ID: Sludge
Benzene (TCLP) SW846 Method 826015030 <0.01 mg/L 04/30/2021
Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 04/30/2021
Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 04/30/2021
Chloroform (TCLP) SW846 Method 6260/5030 • <0.01 mg/L 04/30/2021
Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 0.06 mg/L 04/30/2021
Tetrachloroethylene(TCLP) SW846 Method 8250/5030 <0.01 mg/L 04/30/2021
Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 04/30/2021
Vinyl Chloride (TCLP) SW846 Method 6260/5030 <0,01 mg/L 04/30/2021
RCI
Cyanide SM 4500 CN D 8.64 mg/kg 9 g 04/26/2021
Sulfide SM 4500 S[) 19.0 mg/kg 04/27/2021
Ignitability SW 846 method 1010 >190°F 05/25/2021
Sludge Residuals
PAN Calculation 12600 mg/kg 05/06/2021
Used 30%Mineralization Rate.
Aluminum EPA 200.7 57800 mg/kg 04/28/2021
Arsenic EPA 200.7 15.7 mg/kg 04/28/2021
Cadmium EPA 200.7 <10.2 mg/kg 04/28/2021
Calcium EPA 200.7 10800 mg/kg 04/2B/2021
Chromium EPA200.7 <10.2mg/kg 04/28/2021
Copper EPA 200.7 62.8 mg/kg 04/28/2021
Lead EPA zaaa <10.2 mg/kg 04/28/2021
Magnesium EPA 200.7 2230 mg/kg 04/28/2021
Molybdenum EPA 200.7 <10.2 mg/kg 04/28/2021
Nickel EPA 200.7 <10.2 mg/kg 04/28/2021
Potassium EPA 200 7 3200 mg/kg 04/28/2021
Selenium EPA 200 7 <10.2 mg/kg 04/28/2021
Sodium EPA 200.7 2080 mg/kg 04/28/2021
Zinc EPA 200.7 273 mg/kg 04/28/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 2.00 mg/kg 04/28/2021
Report#.: 2021-06585
Page 2 or 3

Env ro menta . Chenaists, Lae
envirachem 3 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Mante°,NC 27954 • 252.473.5702 Lab/Fax
�, 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Guilford East Date of Report: May 25, 2021
1754 NC HWY 903 Customer PO#:
Kenansville NC 28349 Customer ID: 11030018
Attention: George Yankay Report#: 2021-06585
Project ID: Sludge
Total Solids(%) SM 2540 a 4.28% 04/26/2021
Ammonia Nitrogen SM 4500 NH3 C 3980 mg/kg 04/23/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Org 8 39400 mg/kg 04/23/2021
Total Phosphorus SM 4500 P F 18000 mg/kg 05/04/2021
Mercury SW846 74715 <0.390 mg/kg 05/03/2021
TCLP Metals
Arsenic EPA 200.7 <1.0 mg/L 04/30/2021
Barium EPA 200.7 <1.0 mg/L 04/30/2021
Cadmium EPA 200.7 <1.0mg/L 04/30/2021
Chromium EPA 200,7 <1.0mg/L 04/30/2021
Lead EPA 200.7 <1.0 mg/L 04/30/2021
Selenium EPA200.7 <1.0mg/L 05/04/2021
Silver EPA 200.7 <1.0 mg/L 04/30/2021
Mercury EPA245.1 <0.0002mg/L 05/03/2021
Comment: Sludge resisuals reported on a dry weight basis.
Reviewed by: Nat,6041. ONOQi
Report#:; 2021-06565
Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client LUOMI L. r. 4ST" Date: `11cc23 /DR/ Report Number: Q f ---C. j8 S
Receipt of sample: ECHEM Pickup 0 Client Delivery [UPS❑ FedEx 0 Other 0
❑ YES I 0 NO N/A 1. Were custody seals pres nt on the cooler?
❑ YES ❑ NO i N/A 2. if custody seals were present, were theyintact/unbroken?
Original temperature upon receipt ..S °C f oken.
Corrected temperature upon receipt "C
How temperature taken: ❑ Temperature Blank Or Against Bottles
iR Gun iD:Thomas Traceable S/N 192511657 IR Gun Correction Factor°C: 0.0
0 YES 0 NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
L+ YES 0 NO 4. Were proper custody procedures(relinquished/received)followed?
ill YES 0 NO 5. Were sample ID's listed on the COC?
III YES 0 NO 6. Were samples ID's listed on sample containers?
n YES ❑ NO 7. Were collection date and time listed on the COC?
IN YES 0 NO 8. Were tests to be performed listed on the COC?
if YES 0 NO 9. Did samples arrive in proper containers for each test?
II YES ❑ NO 10. Did samples arrive in good condition for each test?
■i YES 0 NO 11. Was adequate sample volume available?'
f� YES 0 NO 12. Were samples received within proper holding time for requested tests?
0 YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES ❑ NO 14. Were cyanide samples received at a pH>12?
❑ YES 0 NO 15. Were sulfide samples received at a pH>9?
❑ YES 0 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES El NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES El NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation; (Must be completed for any samples) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding(circle one): H2504 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

EinVizachem ENVIRONMENTAL CHEMISTS INC�+ 6602 Windmill Way Wilmington, NC 28405
DLS CERTIFICATION#37729 info@envir nmenta chem sFFICE: 91G-392-0223 FAX ts.O om� 424
Client: C.,..IA �,I
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME: _al t REPORT N0: L/ �7
CONTACT NAME:
REPORT TO: Po No;
COPY TO: PHONE/FAX:
Sampled B : _ _ 5-_- .--~ ,_ email:
SAMPLE TYPE; =influent, E_Effluent, W=Weft,5T=
4Collection Stream, So
_ -Soil, SL=Sludge, Other:
Sample Identification CL ` D 4 PRESERVATION
L'1 r 0 tY
N J
al
m a o o a E a m n 0 upa
.11 Time Temp m " a g z z z z z F tii o ANALYSIS REQUESTED
Q�aI Sb� C P
C p
G G
C p %�i.P
G G A. ,i.mimmiii
C ? j
G G
C P
G G
C p
G G
C p
MMIIIIIIIIIIIIIIIIIIIIIII
G G
C p
G G
rarlcE_
t TransRInIArION: Samples for Ammonia,7KN,Cyanide,Phenol and Bacteria must be dechlorinaled 0.5
Transfer i pornor less)in the field at the time of collection. See reverse for Instructions
Relinquished By:
I. Date/Time
2.
Received By:
Date/Time
Temperature when Received °C;
)elivered By: Accepted;
Rejected: Resampl R
=omments: Received By: quested:
Date: 'i L
Time:
TUR A OUND:

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
LEAR CORPORATION WWTP
03/2'4/21 297 2.4728
03/24/21 I,698 3.2299
03/24/21 _ 2,661 3.4250
03/24/2I 292 2.4654
03/24/21 683 2.8344
03/24/21 304 2.4829
03/24/21 1,399 3.1458
Total 20.0562
Average 2.8652
Geometric Mean ' 3 = `a_ Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

} 7 : � Environmental Chemists, Inca
1 5 1�} L
m, '> fru W -5o , ) 6602 Windmill Way,Wilmington,NC 28405 ° 910.392.0223 Labe 910 392.4424 Fax
L. Y f`"' ..'t r 710 8owsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
F!f 1 f Ham• ISM'.
'L ..� �,:,,,�__..- -- 255-A Wilrnington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info cr environmentalchemists.corn
Guilford East Date of Report: Mar 31, 2021
1754 NC HWY 903 Customer PO#:
Kenansville NC 28349 Customer ID: 11030018
Attention: George Yankay Report#: 2021-04687
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12044 Site: Sample 1 3/24/2021 10:30 AM Solid/Sludge Dale Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 8 6.75% 03/27/2021
Fecal Density SM 9221C EMPN 24 hr 503 297 MPN/g 03/24/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12045 Site: Sample 2 3/24/2021 10:45 AM Solid/Sludge Dale Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 8 6.48%
03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 1698 MPN/g 03/24/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12046 Site: Sample 3 3/24/2021 11:00 AM Solid/Sludge Dale Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 6.39%
03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 2661 MPN/g 03/24/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12047 Site: Sample 4 3/24/2021 11:15 AM Solid/Sludge Dale Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 6.85% 03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 292 MPN/g 03/24/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12048 Site: Sample 5 3/24/2021 11:30 AM Solid/Sludge Dale Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 6.59% 03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 683 MPN/g 03/24/2021
•
Report#:. 2021.04897
p O,lp t of 7

{�` � ` Environmental Chemists, Inc.
� � 3 X�a r -. 3 6602 Windmill Way,Wilmington,NC 28405 * 910 392.0223 Lab • 910.392.4424 Fax
1,7 . 710 Bowsertown Road,Manteo,NC 27954 0 252.473.5702 Lab/Fax
' 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info@environmentalchemis ts.com
Guilford East Date of Report: Mar 31, 2021
1754 NC HWY 903 Customer PO#:
Kenansville NC 28349 Customer ID: 11030018
Attention: George Yankay Report#: 2021-04887
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12049 Site: Sample 6 3/24/2021 11:45 AM Solid/Sludge Dale Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 6.58% 03/27/2021
Fecal Density SM92210EMPN 24hr503 304 MPN/g 03/24/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12050 Site: Sample 7 3/24/2021 12:00 PM Solid/Sludge Dale Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 6.58% 0312712021
Fecal Density SM 9221C E MPN 24 hr 503 1399 MPN/g 03/24/2021
Comment: Results reported on a dry weight basis.
Reviewed by: U` `
Report#:: 2021-04887
Panes 9nf9

Environmental Chemist, Inc., Wilmington, NC Lab#94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:/��u 1 L-001? 0 sxsr Date:3 Lf el?) Report Number: C:?) ----0 `f es
Receipt of sample: ECHEM Pickup, Client Delivery ❑ [UPS 0 FedEx ❑ Other 0
❑ YES 0 NO X' N/A 1. Were custody seals present on the cooler?
❑ YES 0 NO R N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt J,$ °C Corrected temperature upon receipt °C
How temperature taken: 0 Temperature Blank '' Against Bottles
IR Gun ID:Thomas Traceable S/N 192511657 IR Gun Correction Factor°C: 0.0
❑ YES '❑ NO 3. If temperature of cooler exceeded 6°C,was Project Mgr./QA notified?
YES ❑ NO 4. Were proper custody procedures (relinquished/received)followed?
YES ❑ NO 5. Were sample ID's listed on the COC?
YES ❑ NO 6. Were samples ID's listed on sample containers?
YES 0 NO 7. Were collection date and time listed on the COC?
YES 0 NO 8. Were tests to be performed listed on the COC?
YES ❑ NO 9. Did samples arrive in proper containers for each test?
YES ❑ NO 10. Did samples arrive in good condition for each test?
YES 0 NO _ 11. Was adequate sample volume available?'
YES 0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES ❑ NO 14. Were cyanide samples received at a pH>12?
❑ YES 0 NO 15. Were sulfide samples received at a pH>9?
❑ YES ❑ NO 16. Were NH3/TI(N/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding(circle one): H2504 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

nili ENVIRONMENTAL CHEMISTS I N C 6602 Windmill Way Wilmington, NC 28405
OFFICE:910-392-0223 FAX [phone]
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 info@environmentalchemists,corn
COLLECTION AND CHAIN OF CUSTODY
Client: Guilford East PROJECT NAME: Sludge REPORT NO: 2 1 _C(4 ss-1
ADDRESS: CONTACT NAME: PO NO:
REPORT TO: George Yankay PHONE/FAX:
COPY TO: email:
Sampled By:`br, le Sb I n 5o,N _ SAMPLE TYPE: 1 =Influent, E=Effluent, W=Well,ST=Stream,SO=Soil, SL=Sludge, Other:
Collection PRESERVATION
Sample Identification E III
I7.3 15 2 " o P ° m
y I- of to o a m E m m i H $ zo o ANALYSIS REQUESTED
lDate Time Temp " z x = z o
Sample# 1 3rZ1(Z i /03o SL C P
G G f X Fecal Density; T5%
Sample#2 31 zy 6-1 ie y Si_ C P
G G ZaLIS X Fecal Density; TS%
Sample#3 3(z�ll L{ Hoc SL C P
G G rZp`}rP X Fecal Density; TS% .
Sample#4 e4(a( ///5--_ SL C P
G G �204) X Fecal Density; TS%
Sample#5 3� 124 //3o SL C P
I G G \Z°` X Fecal Density; TS%
Sample#6 4z.y i! //yam 5L C P
G G � Q X Fecal Density; TS%
Sample#7 -412( . /Zo0 SL C P
G G � X Fecal Density; TS%
C P
G G
C _ P
G G
Transfer Relinquished By: Date/Time Received By: Date/Time
P
Temperature when Received °C: I. p Accepted: Rejected: Resample equ sted:
Delivered By: s - Received By: Date: 3Y Time: 3 .",,5- /a
Comments: TURNAROUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTIONFORM(02T Rules)
Facility Warne;. Coastal Farms.and Residuals,LLC WQ'Permit Number: *Q0034806 _
WWII*Name: Lear'Corporation.WWTP NPDES Number: N0002305
Monitoring Period: From 1/1./2021 'To 1213i/2021
Pathogen Reduction.(1SA N.CAC'02T.1106).-Please.indicatelevel achieved.and•alternafive'performed;
Class-A: Alt.A.(tiixie/`tenip) 0 Alt B.(Alk Treatment),❑ I Alt.C•(Prior Testing)iJ
Alt D.(No Prior Test) Li I .....Process to Further-Reduce-Pathogengs:❑
If applicable to alternative performed(Class A Daly)indicate`Process to FurtherReduce Pathogeins":
Cornp.ost ....,❑ Heat Drying El ` Heat Treatment 0 Theriophilic •.❑ I
Ray •
B eta ❑ . Gamma. r.. : >:>:= 1;;-.;z-::._s :...ti��;< :.� 0 .. Pasteurization ❑ .,....:. . ` r %�
` Class.B: 'Alt.(1)•Fecal Density p I Alt.(2)Process to Significantly ReducePathogens 0: .
Itapplic'able.to alternative.performed(pass.only)indicate-"Process.to Signifieantly.RetlucePatltogeas":
Lune Stabilization . 0 I: Air Drying, Ef I Composting. El [Aerobic Digestion 0.
:Sf ::>�;{.� :=.;t;;i•[�;!r?s::':fizz,-:xr:"rj-r:;:>::;?:;.-YnXc?:z:ta:i�,5\:.?�:•1-+:r:t;:r-r•+r+•:`•
Ana.eroblcDigestion ❑ :r_:c: k�r,.. ;::,_;�o:�;v:r ah:--ari-;:F:.yxtim•_;:ccs; :R s-:.�:`•. :<=:•>u:::r.; 1}4y.5 :tr"•_`SIN
b �:•::.. n::::_.::.fv.:.•r:r...:.v}5.u-:5._v...-:•r:�::.,:v:r..:::..--..v..r.hb:}::.>�:-..7r:.t-r5n_'t:-}Y,r...r.::.
+:.s•r.4•.a
If:applicable.to:alternative performed (Class A or Class.B)complete the followingJnomitoring.data: . -
AitowableLevel Pathogen :l%lumberof• Analytical
p1etep. g Density Frequency Sample •
in Sludge J✓xcee- ofAn Tech
g. Mini num Geo.Mean Maximum Units rien�ec alysis Type. •mane
2x 10 to the MP--Y
6th power .
per gram of . • .
Fecal Coliform total solids CFU
l O00 mpn per gram •
of total solid (dty 292 733 2,661 MPN/g. :0 • Annual Grab: $Nl92210E
weight)
Salrnonella bacteria 3'MPN per 4 grams -
(in lieu•offecal total solid(thy
coliform) weight) __ _
.Vector Attractioti.Reduction:(15A NCAC 02T.110.7)-Please indicate alternative'performed:
Altai (VS reduction) ❑ Alt.,2.(40,day bench) El Alt.3'(30-day bench) ❑ Alt:4•(Spec.O,uptake) • .0'
Alt.5(14-Day Aerobic) 0 Alt.6(AIL Stabilization p 'Alt 7(Drying-Stable) ❑ Alt..8(Drying-Unstable) 0
Alt g(Infection) p Alt.10(Incorporation) p No Vector at-II-action reduction alternatives were performed 0
CERTIFICATION STATEMENT(plea se check the appropriate.statement)
"Iertify,under penalty.of law,that the pathogen requirements'in 15A NCAC 02T.1106•and the
vector-..attraction reduction re'quiremnent:in t:SA NCAC•OZT.1107 have been met."
❑ :"I certify.,under penalty of law,:that the pathogen requirements.in 15A.NCAC.02T.1106'and the
vector a tti-action reduction.requirement in-15A NCAC 02T•1107 have:not been met."' (Please_note!
ifyou eheck this statement attach.an.explanation why you have:not met oneor both.of the
requireinenfs:)
"T'his determination has.been made under my direction and supervision in accordance with the system
designed,to ensure that:qualified personnel properly gather and evaluate the information used to determine
that'the pathogen and,vector attraction reduction requirements have been.met. I am aware that there are
significant-penalties for false certification including fine:and_imprisonment."
George•-Yarkay,ORC Wesley Wooten,'President
Pre al-eet Name ai d Title type or print) Land ApplierNartie and Title(if applicable)(type or'pririt)
_ �� . � / JJ//
r �i✓ 8123/21
Signature f P.. r* Date Signa
- P o t>xre of Lan Applrer if applicable) Date:
*Prepazer is . • ed'in40.CFR Pzrt 503.9(r)and I5ANCAC 2T.1102(26)
DENR FORM PVRF 02T(12/2006)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 25,2021
Northwest Regional WRF Permit No.WQ0034367
3.80 %Solids
6.88 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 3.650 36,500.000 73.000
Phosphorus 3.100 31,000.000 62.000_
Potassium 0.231 _ 2,310.000 4.620
PAN(inlected)* 1.179 11,787.210 23.574
PAN(surface)* 1.I19 11,192.210 22.384
Ammonia Nitrogen _ 0.119 1,190.000 2.380
Calcium 1.290 12,900.000 25.800
Calcium Carbonate Eq. _ --- --- ---
Magnesium --- 1,280.000 2.560_
Sodium --- 2,980.000 5.960
Sulfur --- --- ---
Nitrate N/Nitrite N -- 4.210 0.008 _
Barium -- --- --- SAR
Chloride --- --- --- 1.30
Iron --- --- -- Ceiling Concen.
Aluminum --- 38,200.00 76.400 (Mg/Kg) ,
Arsenic --- 26.10 0.052 75
Cadmium --- 13.00 0.026 85
Chromium --- 26.400 ---
Copper --- 335.00 0.670 4,300
Lead --- 20.70 0.041 840
Mercury --- 0.617 0.001 57
Molybdenum --- 13.00 0.026 75
Nickel --- 13.00 0.026 420
Selenium 13.00 0.026 100
Zinc 875.00 1.750 7,500
Environmental Chemists# 2021-04952
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits arc listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS,LLC
WQ0034806
Northwest Regional WRF
a e ` ;a ecal Co1i
03/25/21 I,324 3.1219
03/25/21 _ 3,824 3.5825
03/25/21 12,685 4.1033
03/25/21 4,900 3.6902
03/25/21 4,957 3.6952
03/25/21 3,595 3.5557
03/25/21 5,432 3.7350
Total 25.483 8
Average 3.6405
Geometric Mean 4 371 Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B -Alternative 1 Pathogen Reduction
requirement.

ONWASA Laboratory
, 228 Georgetown Road
Jacksonville NC 28540
• NWASA [phone]
April 26, 2021
Mark Young
Northwest RWRF
189 Mills Field Rd.
Richlands, NC 28574
RE: NW Solids
Enclosed are the results of analyses for samples received by our laboratory on 3/25/2021. If you
have any questions concerning this report, please feel free to contact me.
Sincerely,
h ' 4 Ma
Todd A. Roberts For Mark Young
Northwest ORC

t
ONWASA
Northwest RWRF Project: NW Solids
189 Mills Field Rd. Project Number: Reported:
Richlands,NC 28574 Project Manager: Mark Young 04/26/2021 12:09
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: NW Fecal#1 N211304-01(WW) 03/25/2021 09:43
Digester Sludge
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed initials Method
Fecal Density 1324 MPN/g 03/25/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 3.4 % 03/27/2021 SM 2540 G
Sample: NW Fecal# 2 N211304-02(WW) 03/25/2021 09:45
Digestor Sludge
I
Reporting Date Analyst
Analyte Result Quaf Limit Units Analyzed Initials Method
Fecal Density 3824 MPN/g 03/25/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 3.4 % 03/27/2021 SM 2590 G
Sample: NW Fecal #3 N211304-03(WW) 03/25/2021 09:46
Digestor Sludge
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 12685 MPN/g 03/25/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 3.39 % 03/27/2021 SM 2540 G
Sample: NW Fecal#4 N211304-04(WW) 03/25/2021 09:47
Digestor Sludge
Reporting Date Analyst
— Analyte Result Qual Unit Units Analyzed Initials Method
Fecal Density 4900 MPN/g 03/25/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 3.47 % 03/27/2021 SM 2540 G
Sample: NW Fecal#5 N211304-05(WW) 03/25/2021 09:48
Digestor Sludge
Reporting Date Analyst
Analyte Result Qua! Limit Units Analyzed Initials Method
Fecal Density 4957 MPN/g 03/25/2021 SM 9221C E MAN
24hr 503
Total Solids(%) 3.43 rya 03/27/2021 SM 2540 G
The cnnten&of this report apply to the samples)analyzed to accordance with the chain of custody document
No duplication of this report allowed except in its entirety. Page 2 of 8

ONWASA
Northwest RWRF Project: NW Solids
189 Mills Field Rd. Project Number: Reported:
Richlands,NC 28574 Project Manager: Mark Young 04/26/2021 12:09
Sample Results
(Continued)
Data Analyzed by:Environmental Chemists,Inc.
Sample: NW Fecal#6 N211304-06(WW) 03/25/2021 09:49
Digestor Sludge
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 3595 MPN/g 03/25/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 3.06 % 03/27/2021 SM 2510 G
Sample: NW Fecal#7 N211304-07(WW) 03/25/2021 09:50
Digestor Sludge
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 5432 MPN/g 03/25/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 3.13 % 03/27/2021 SM 2510 G
The contents of this report apply to the samples)analyzed In accordance with the chain of custody document.
Noduplrcatlonofth.(s report Isallowed,emeltiniientirely Page 3 of 8

c
ONWASA
Northwest RWRF Project: NW Solids
189 Mills Feld Rd. Project Number: Reported:
Richlands,NC 28574 Project Manager: Mark Young 04/26/2021 12:09
Sample Results
(Continued)
Data Analyzed by:Environmental Chemists,Inc.
Sample: NW Digester N211304-08 (SL) 03/25/2021 09:42
Digestor Sludge
Reporting bate Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Aluminum 38200 mg/Kg 03/29/2021 EPA 200.7
Ammonia-N 1190 mg/Kg 03/31/2021 SM 4500 NH3 C
Arsenic < mg/Kg 03/31/2021 EPA 200.7
Calcium 12900 mg/Kg 03/29/2021 EPA 200.7
Cadmium < mg/Kg 93/29/2021 EPA 200.7
Cyanide 6.19 0.025 mg/Kg 03/29/2021 EPA 335.4
Chromium 26.4 mg/Kg 03/29/2021 EPA 200.7
Copper 335 mg/Kg 03/29/2021 EPA 200.7
Mercury c0.0002 0.0002 mg/L 04/13/2021 EPA 245.1
Mercury 0.617 mg/Kg 03/30/2021 SW846 7471B
Ign€tability < °F 04'05/2021 EPA 1030
Potassium -.
2310 mg/Kg 03/29/2021 EPA 200.7
Magnesium 128o mg/Kg 03/29/2021 EPA 2007
Molybdenum < -- --
mg/Kg 03/29/2021 EPA 200.7
Sodium 2980 mg/Kg 03/29/2021 EPA 200.7
Nickel <
mg/Kg 03/29/2021 EPA 200.7
Nitrate+Nitrite-Nitrogen 4.21 mg/Kg 03/30/2021 EPA 353.2
Lead 20.7
mg/Kg 03/29/2021 EPA 200.7
. PH 6.88 pH Units 03/30/2021 SM 4500 H B
PH 6.88 pH Units 03/30/2021 SW846 9045D
Selenium < mg/Kg 03/29/2021 EPA 200.7
Sulfide 2.96 mg/Kg 03/30/2021 SM 4500 S D
Chlordane <0.02 0.02 mg/L 04/08/2021 SW846 808113/3510
Endrin <0.0005 0.0005 mg/L 04/08/2021 SW846 8081B/3510
Heptachlor <0.0005 0.0005 mg/L 04/08/2021 SW846 80818/3510
Heptachlor epoxide <0.0005 0.0005 mg/L 04/08/2021 SW846 8081B/3510
Undane <0.0005 0.0005 mg/L 04/08/2021 SW846 8081B/3510
Methoxydilor <0.05 0.05 mg/L 04/08/2021 SW846 8081B/3510
Toxephene <0.05 0.055 mg/L 04/0_8/2021 5W846 80818/3510
1,4-D€chlorobenzene <0.05 0.05 mg/L 04/07/2021 SW846 8270/3510
2,4,5-Trichlorophenol <0.05 0.05 mg/L 04/07/2021 SW846 8270/3510
2,4,6-Trichorophenol <0.05 0.05 mg/L 04/07/2021 SW846 8270/3510
2,4-Dinitotoluene <0.05 0.05 mg/L 04/07/2021 SW8468270/3510
Cresol <0.05 0.05 mg/L 04/07/2021 SW846 8270/3510
Hexachloro-1,3-butadlene <0.05 0.05 mg/L 04/07/2021 SW846 8270/3510
Hexachlombenzene <0.05 0.05 mg/L 04/07/2021 SW846 8270/3510
Hexachlomethane <0.05 0.05 mg/L 04/07/2021 SW846 8270/3510
M+P Cresol <0.05 0.05 mg/L 04/07/2021 SW846 8270/3510
Nitrobenzene <0.05 0.05 mg/L 04/07/2021 SW846 8270/3510
0-0resol <0.05 0.05 mg/L 04/07/2021 SW846 8270/3510
Pentachlorophenol <0.25 0.25 mg/f- 04/07/2021 SW846 8270/3510
Pyridine <0.05 0.05 mg/L 04/07/2021 SW846 8270/3510
2,4,5-TP <0.003 0.003 mg/L 04/12/2021 SW846 8151A
2,4-0 <0.003 0.003 mg/L 04/12/2021 SW846 8151A
The contents of this report apply to the sarnple(s)analyzed in accvm nce with the chain of custody document.
No duplication af this reportts allowed,except in its entirety. gage 4 of 8

to
ONWASA
Northwest RWRF Project: NW Solids
189 Mills Field Rd. Project Number: Reported:
Richlands,NC 28574 Project Manager: Mark Young 04/26/2021 12:09
Sample Results
(Continued)
Data Analyzed by:Environmental Chemists,Inc.
Sample: NW Digestor (Continued) N211304-08(SL) 03/25/2021 09:42
Digestor Sludge
Reporting Date Analyst
—Analyse Result Qual Limit Units Analyzed Initials Method
1,1-Dirhloroethylene <0,01 0.01 mg/L 04/06/2021 SW846 8260 5030
1,2-Dichloroethane <0.01 0.01 mg/L 04/06/2021 5W846 8260/S030
Benzene <0.01 0.01 mg/L 04/06/202.1 SW846 8260/5030
Carbon Tetrachloride <0.01 0,01 mg/L 04/06/2021 SW846 8260/5030
Chlarobenzene <0.01 0.01 mg/L 04/06/2021 SW846.8260/5030
Chloroform <0.01 0.01 mg/L 01/06/2021 SW846 8260/5030
Methyl ethyl ketone <0.05 0.05 mg/L 01/06/2021 SW846 8260/5080
Tetrachloroethylene <0.01 0.01 mg/L 01/06/2021 SW846 8260/5030
Trichloraethyrene <0.01 0.01 mg/L 04/06/2021 5W8468260/5030
Vinyl Chloride <0.01 0,01 mg/L 04/06/2021 SW846 8260/5030
Arsenic <1 1 mg/L 0.4/12/.2021 EPA 200.7
Barium <1 1 mg/L 04/12/2021 EPA 200.7
Cadmium <1 1 mg/L 04/12/2021 EPA 200.7
Chromium <1 1 mg/L 04/12/2021 EPA 200.7
Lead <1 1 mg/L 04/12/2021 EPA 200.7
Selenium <1 1 mg/L 04/12/2021 EPA 200.7
Silver <1 1 mg/L 04/12/2021 EPA 200.7
Total Njeldahl Nitrogen 36500 mg/Kg 03/30/2021 EPA 351.2
Phosphorus,total S ludge 31000 mg/Kg 04/07/2021 5M 4500 P E
Total Solids(%) 3.0 % 03/27/2021 SM 2540 G
Zinc 875 mg/Kg 03/29/2021 EPA 200.7
The contents of elks report apply to thesample(s)analyzed in acxvrdance with the chain ofcvstndy document
No duplication of this report is allowed,except In Rs entirely. Page 5 of 8

ONWASA
Northwest RWRF Project: NW Solids
189 Mills Field Rd. Project Number: Reported:
Richlands,NC 28574 Project Manager: Mark Young 04/26/2021 12:09
Notes and Definitions
Item Definition
Dry Sample results reported on a dry weight basis.
ND Analyte NOT DETECTED at or above the reporting limit.
The contents of this report apply to the sample(s)analyzed/n accordance with the drain of austodydocument
No dupl cation of this report is allowed,except lb Its entirety. Page 6 of 8

L a t-4 ENVIRONMENTAL CHEMISTS, INC 6602 OFFICE
:1m0 l Way
2 Wilmington,
1 - ..: . -� NCDCNR: CERTIFICATION
Analytical Consulting Chemists DWQ CERT CATION#94 NCDHHS: DLS CERTIFICATION#37729 [e-mail]_
COLLECTION AND CHAIN OF CUSTODY
Client: Onslow Water& Sewer Authority(ONWASA) PROJECT NAME: Northwest Regional WRF REPORT NO:
ADDRESS: 228 Georgetown Rd CONTACT NAME: Mark Young PO NO:
Jacksonville, NC 28540 REPORT TO: [e-mail] PHONE/FAX: [phone]
COPY TO: Martin a_WILLCOXMABESOIL.COM email: [e-mail]
• Sampled By: � —L Q'�Q n SAMPLE TYPE: I=Influent, E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge, Other:
Collection a .0 a a = J o PRESERVATION
Sample Identification f a a o` g a` o `co m w g 2
in E o a z 5 j = a v m p o o = ANALYSIS REQUESTED
Date Time Temp u " 0 z z _ = x .- o
3/25/21 Dttz. C © —
Digester /�D SL © G X _ Annual TCLP w/RIC, Nutrient& Metals
3/25/21 of y3 c
Digester- Fecal 1 j r f SL © G
X Fecal Density
3/25/21 _ OLIt{r C
Digester- Fecal 2 /11• SL n G X Fecal Density
3/25/21 09#4 ` C
Digester- Fecal 3 / /`D SL G X Fecal Density
3/25/21 0(7 / /60 C
Digester- Fecal 4 II II SL 0 G X Fecal Density
3/25/21 09c/ l,/� C
Digester- Fecal 5 7 SL C) G _ X Fecal Density
3/25/21 Q cm _ /f le C MD
Fecal 6 7�� SL OG G X Fecal Density
3/25/21 Q?6" f /,, C
Digester Fecal 7 ! �`� SL
- , G� G X Fecal Density
Transfer _ Relinquished By: Date/Time Received By: Date/Time
1. AP.__ `YduYla 4z5/2-I ✓9
2.
Temperature when Received: Accepted: Rejected: Resample Requested: _
Delivered By: Received By: Date: Time:
Comments:
TURNAROUND:

. : -°"it,f- � EnvironmentalChemists, Inc.
G1'Li , . ...,,,,,
6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab o 910.392.4424 Fax
4`+W4 '`:0•,- 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab Fax
`lam_',....; '---', 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS inforrienvironmentalchemists.corn
Onslow Water&Sewer Authority Date of Report: Apr 22, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Mark Young Report#: 2021-04952
Project ID: Northwest Reg. WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12236 Site:001 3/25/2021 9:43 AM Solid/Sludge Mark Young
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 3.40% 03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 1324 MPNIg 03/25/2021
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
21-12237 Site: 002 3/25/2021 9:45 AM Solid/Sludge Mark Young
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 3.40% 03/27/2021
Fecal Density SM 9221C E MPN 24hr503 3824 MPN/g 03/25/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12238 Site:003 3/25/2021 9:46 AM Solid/Sludge Mark Young
Test Method Results Date Analyzed
Total Solids(%) SM 2540 G 3.39% 03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 12685 MPN/g 03/25/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12239 Site:004 3/25/2021 9:47 AM Solid/Sludge Mark Young
Test Method Results Date Analyzed
Total Solids(%) SM 2540 G 3.47% 03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 4900 MPN/g 03/25/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12240 Site:005 3/25/2021 9:48 AM Solid/Sludge Mark Young
Test Method Results Date Analyzed
Total Solids(%) SM 2540 G 3.43% 03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 4957 MPN/g 03/25/2021
Report#:: 2021.04952 Page t of 5

r . 5' iF'^_ ' � E ti Environmental Chemists, Inc.
envlttoene. - 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
'" "' _' 710 8owsertovvn Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
,j'lit .S1 255-A Wilmington Highway,Jacksonville,NC 28540 ■ 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoCrtenvironmentaIchemists.com
Onslow Water& Sewer Authority Date of Report: Apr 22, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Mark Young Report#: 2021-04952
Project ID: Northwest Reg. WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12241 Site:006 3/25/2021 9:49 AM Solid/Sludge Mark Young
Test Method Results Date Analyzed
Total Solids(%) SM 2540 G 3.06% 03/27/2021
Fecal Density SM 9221C E MPN 24 hr503 3595 MPN/g 03/25/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12242 Site:007 3/25/2021 9:50 AM Solid/Sludge Mark Young
Test Method Results Date Analyzed
Total Solids(%) SM 2540 c 3.13% 03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 5432 MPN/g 03/25/2021
Report#:: 2021-04952
Page 2 or 5

�- -,.q ..-N Environmental Chemists,
�.44'., '7 '' _ Inc.
,_ : 6602 Windmill Way,.Wilmington,NC 28405 e 910.392.0223 Labe 910.392.4424 Fax
''•�'{l-�y4f�-f'~f t • y .' : u o Lab/Fax
Bowsertown Rd,Manteo,NC 27954 • 252.473.5702 Lab Fax
_ kt
. -,.— ;'- 255-A Wilmington Highway,Jacksonville,NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS iinfo@environ men ta Leh emists.corn
Onslow Water& Sewer Authority Date of Report: Apr 22, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 05100092
Attention: Mark Young Report#: 2021-04952
Project ID: Northwest Reg. WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-12243 Site: Sludge 3/25/2021 9:42 AM Solid/Sludge Mark Young
Test Method Results Date Analyzed
Chlordane (TCLP) SW 846 Method 8061B/3510 <0.02 mg/L 04/08/2021
End rin (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 04/08/2021
Heptachlor(TCLP) SW 846 Method 8061B/3510 <0.0005 mg/L 04/08/2021
Heptachlor epoxide (TCLP) SW 845 Method 80818/3510 <0.0005 mg/L 04/08/2021
Lindane (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 04/08/2021
Methoxychlor(TCLP) SW 846 Method 8081S/3510 <0.0005 mg/L 04/08/2021
Toxaphene(TCLP) SW 846 Method 6081B/3510 <0.05 mg/L 04/08/2021
1,4-Dichforobenzene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2021
2,4,5-Trichlorophenof(TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2021
2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2021
2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2021
Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2021
Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2021
Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2021
Hexachloroethane(TCLP) SW 846 method 8270/3510 <0,050 mg/L 04/07/2021
m + p-Cresol(TCLP) sW 846 method 8270/3510 <0.050 mg/L 04/07/2021
Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2021
o-Cresol(TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2021
Pentachlorophenof(TCLP) SW 846 method 8270/3510 <0.250 mg/L 04/07/2021
Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 04/07/2021
2,4,5-TP (TCLP) SWB46 Method 6151A <0.003 mg/L 04/12/2021
2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 04/12/2021
1,1-Dichforoethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 04/06/2021
1,2-Dichloroethane(TCLP) 5W846 Method 8260/5030 <0.01 mg/L 04/06/2021
Benzene(TCLP) SW846 Method 8260/5030 <4.01 mg/L 04/06/2021
Carbon Tetrachloride(TCLP) SW846 Method 8280/5030 <0.01 mg/L 04/06/2021
Report#:: 2021-04952
Page 3 of 5

,a Environmental Chemists, Inc.
.. $,
r l r� t 6602 Windmill Way,Wilmington,NC 28405 0 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Goad,Manteo,NC 27954 Y 252.473.5702 Lab/Fax
;;"_} 255-A Wilmington Highway,Jacksonville,NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Onslow Water&Sewer Authority Date of Report: Apr 22, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Mark Young Report#: 2021-04952
Project ID: Northwest Reg. WRF
Chlorobenzene(TCLP) SW846 Method 8260/5030 <0.01 mg/L 04/06/2021
Chloroform (TCLP) SW846 Method 826D/5030 <0.01 mg/L 04/06/2021
Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 04/06/2021
Tetrachloroethylene(TCLP) SW846 Method 8260/5030 <0.01 mg/L 04/06/2021
Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 04/06/2021
Vinyl Chloride(TCLP) 5W646 Method 8260/5030 <0.01 mg/L 04/06/2021
RCI
Cyanide SM 4500 CN 0 6.19 mg/kg 03/29/2021
Sulfide SM 4500 S o 2.96 mg/kg 03/30/2021
Ignitability SW 846 method 1010 >180 OF 04/05/2021
Sludge Residuals
Aluminum EPA 200.7 38200 mg/kg 03/29/2021
Arsenic EPA 200.7 <26.1 mg/kg 03/31/2021
Cadmium EPA 200.7 <13.0mg/kg 03/29/2021
Calcium EPA 200.7 12900 mg/kg 03/29/2021
Chromium EPA 200.7 26.4 mg/kg 03/29/2021
Copper EPA 200.7 335 mg/kg
03/29/2021
Lead EPA 200.7 20.7 mg/kg 03/29/2021
Magnesium EPA 200.7 1280 mg/kg 03/29/2021
Molybdenum EPA 200.7 <13.0 mg/kg 03/29/2021
Nickel EPA 200.7 <13.0 mg/kg 03/29/2021
Potassium EPA 200.7 2310 mg/kg 03/29/2021
Selenium EPA 200.7 <13.0 mg/kg 03/29/2021
Sodium EPA 200.7 2980 mg/kg 03/29/2021
Zinc EPA 200.7 875 mg/kg 03/29/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 4.21 mg/kg 03/30/2021
Total Solids (%) SM 2540 B 3.80% 03/27/2021
pH SM 4500 H B 6.88 units 03/30/2021
Ammonia Nitrogen SM 4500 NH3 C 1 190 mg/kg 03/31/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 36500 mg/kg 03/30/2021
Report OP: 2021-04952 Page 4 of 5

7 it i.,, Environmental Chemists, Inc.
: : ' ,0,7' 6602 Windmill Way,Wilmington,NC 28405 0 910.392.0223 Lab • 910.392.4424 Fax
i"?'-�ti ' =�a.', -:: - :: V4?. ;- 710 Bowsertown Road,Mantea,NC 27954 • 252.473.5702 Lab/Fax
e ; kr;s 255-A Wilmington Highway,Jacksonville,NC 28540 0 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infofgwenvironmentaichemists.corn
Onslow Water& Sewer Authority Date of Report: Apr 22, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Mark Young Report#: 2021-04952
Project ID: Northwest Reg. WRF
Total Phosphorus SM 4500 P F 31000 mg/kg 04/07/2021
Mercury SW046 74718 0.6170 mg/kg 03/3D/2021
TCLP Metals
Arsenic EPA 200.7 <1.0 mg/L 04/12/2021
Barium EPA z00.7 <1.0 mg/L 04/12/2021
Cadmium EPA 200.7 <1.0 mg/L 04/12/2021
Chromium EPA200.7 <1.0 mg/L 04/12/2021
Lead EPA 200.7 <1.0 mg/L 04/12/2021
Selenium EPA 200.7 <1.0 mg/L 04/12/2021
Silver EPA 200.7 <1.0 mg/L 04/12/2021
Mercury EPA 245.1 <0.0002 mg/L 04/13/2021
Comment: Sludge residual results, except pH, reported on a dry weight basis. pH reported on an as received
basis. 8151 LCS/LCSDIMS Recoveries low.is
Reviewed by: t k[ lA.,O, 064 ,
Report#.: 2021-04952
Page 5 of 5

Environmental Chemist, Inc., Wilmington, NC Lab#94
6602 Windmill 4
Wilmington, NC 28'
9/0.392.02
l Sample Receipt Checklist
V
Cfiant. 4 O( 1AJiS4- Res 3125\21
{?ate: Report Number: 21 -4°152-
Receipt of sample: ECHEM Pickup Client Delivery 0 1uPs 0 FedEk❑ Other❑
YES to NO N/A 11. Were custody seals present on the cooler?
❑ YES ❑ NO N/A 12. If custody seals were present, were theyintact/unbroken?
Original temperature upon receipt 4 9 oC - _/unbro°..n.
or ected tern pareture upon receipt =C
Hose temperature taken: 0 Temperature Blank
Against Bottles
fR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor°C: 0.0
►' YES 1❑ NO 1 3. If temperature of cooler exceeded 6rC was Project Mar. notified?
21 YES ❑ NO 4. Were Mgr./QA notifi_o? 1
1 proper custody procedures (relinquished/received) followed? 1
Pl YES 1❑ NO 1 5. Were sample 1D's listed on the COC?
R. YES 10 NO 1 6. Were samples 1D's fisted on sample containers?
0 YES 10 NO 1 7. Were collection date and time fisted on the COC?
'TI YES 1❑ NO I
E. Were tests to be performed listed on the COC?
YES 1❑ NO 9. Did samples arrive in proper containers for each test?
Pa. YES ❑ NO 10. Did samples arrive in good condition for each test?
YES 0 NO 11. Was adequate sample volume available?'
Xl YES 10 NO 12. Were samples received within proper hofdin5 time for requested tests?
0 YES 10 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 10 NO 14. Were cyanide samples received at a pH>12?
❑ YES 10 NO 15. Were sulfide samples received at a pH>9?
❑ YES 10 NO J15. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L. :
❑ YES 0 NO �
17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
0 YES 0 NO 118. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volai fes are pH checked at time of analysis and recorded on the benchsheet.
k Bacteria sennp'es are checked for Chlorine 2tt time of analysis and recorded on the benthsheet.
:Sairrple Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Samples) were received incorrectly preserved and were adjusted accordingly
. by adding (circle one): H2S0, HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
_:No.:yCLi ?.,m2.ie--,ice im . :{a_e y r4rii:orre:t;I Pei_'i✓edsa !es.Obtain a re::s_mp'a 0r
notify the stEe tab I"th e_ted to ana'yzed by the Customer.WhO V125 notified,date and t:,me:
Volatiles Sample(s) were received with headspace
COMMENTS:
ti
DOC. QA.002 Rev 1

6602
a�A I} ENVIRONMENTAL CHEMISTS, INC OFFICE 910ill Way 2-0223 AX91n,N2-4424
OFFICE:910-392.0223 FAX [phone]
Analytical R Consulting Chemists NCDENR: DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Onslow Water&Sewer Authority (ONWASA) PROJECT NAME: Northwest Regional WRF REPORT NO: L --kaI52
ADDRESS: 228 Georgetown Rd CONTACT NAME: Mark Young PO NO:
Jacksonville, NC 28540 REPORT TO: [e-mail] PHONE/FAX: [phone]
COPY TO: [e-mail] email: [e-mail]
Sampled By: / 441 L e (7-, 4-1 'i"; SAMPLE TYPE: I=Influent, E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge, Other:
Collection w PRESERVATION
Sample Identification a ., Ti a 5 W e w
m
H i- a ° ca `o a s E °° 5 z u 4 2 o a ANALYSIS REQUESTED
Date Time Temp u " z x = y = x I= o
3/25/21
C
Digester / a9 SL © G 1-2.2g3 X Annual TCLP w/RIC, Nutrient&Metals
3/25/21 eny1 C CI-3)
.Digester-Fecal 1 Hi SL �G G - 12230 X Fecal Density
3/25/21 c/45' C
Digester-Fecal 2 /'in— SL 1. G 1-2/31
X Fecal Density
3/25/21 o91/. C
Digester- Fecal 3 f d SL O I"L23 S
X Fecal Density
3/25/21 0 gieri /10 C ® _ 1 Z235
Digester-Fecal 4 Is SL a) G X Fecal Density
3/25/21 0(30 f-/& C
Lfp
Digester- Fecal 5 T 7`� SL © GZ X Fecal Density
3/25/21 Oq�9 /T le C 1
Digester- Fecal 6 SL © G Z2�
X Fecal Density
3/25/21 09.0-
/,, c
Digester- Fecal 7 ��'`� SL [G) , �G 1 Z2�? _ X Fecal Density
Transfer Relinquished By: DatelTime l ceived B�� Y Datefl'im
1. 4 3/2s/zJ ,as/9 (Y\J ‘ x� 6 ! j 1
2. `` �� z
Temperature w r Re e , `1•I Accepted: eject d: Resample Requested:
Delivered By: 4- Received B : • c o-Y����.�
V Y Date: ZS Zl
Time: t l
Comments: TURNAR UND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name; Coastal Farms and Residuals,LLC WQ Permit Number: WQ0034806
WWTP Name: Northwest Regional WRF NPDES Number: WQ0034367
Monitoring Period: From I/1/2021 To 12/3I/2021
Pathogen Reduction (15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A: I Alt. A(time/temp) ❑ I Alt B(Alk Treatment)El I Alt. C(Prior Testing)❑
A1t.D(No Prior Test) 0 I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment El Thermophilic ❑
Beta Ray ❑ Gamma Ray 0 Pasteurization ❑
Class B: IAIt.(1)Fecal Density ..
❑ Alt. (2)Process to Significantly Reduce Pathogens ❑ —I
If applicable to alternative performed(Class B only)indicate"Process to Significantly-Reduce Pathogens":
Lime Stabilization ❑ Air Drying 0 1 Composting ❑ 'Aerobic Digestion Eli D
Anaerobic g
estio
n
applicableIf
to alternative performed (Class A or Class B)complete the following monitoring data:
Allowable Level Pathogen DensityNumberot Analytical
Parameter gExcee- Frequency Sample
Tech-
in Sludge Minimum Geo.Mean Maximum Units denCeS of Analysis Type ninue
2x10tothe niRue
6thpower MPN 1,324 4,371 12,685 MPN/g 0 Annual Grab SM9221C)r
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T.1107)-Please indicate alternative performed:
Alt.l (VS reduction) ❑ Alt.2(40-day bench) ❑ Alt.3(30-day bench) ❑ Alt.4(Spec. 0,uptake) El
Alt.5(14-Day Aerobic) ❑ Alt.6(Alk.Stabilization ❑ Alt 7(Drying-Stable) ❑ Alt.8(Drying-Unstable) ❑
Alt. 9(Injection) El JAlt. 10(Incorporation) El No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT(please check the appropriate statement)
0 "I certify,under penalty of law,that the pathogen requirements in I5A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
❑ "I certify,under penalty of law,that the pathogen requirements in I5A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mark Young, ORC Wesley Wooten, President
Preparer Name and Title(type or print) Land Applier Name and Title(if applicable)(type or print)
72 ( ' 7� 1/18/22 , 4/27/21
Signature of Preparer* Date Signature of La Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
DENR FORM PVRF 02T(12/2006) '

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 8,2021
Pluris Hampstead WWTF Permit No.WQ0037287
3.02 %Solids
6.22 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) _ 7.010 70,100.000 I, 140.200
Phosphorus 2.300 23,000.000 46.000
Potassium 0.639 6,390.000 12.780
PAN(injected)* 2.230 22,297.300 44.595
PAN(surface)* 2.140 21,402.300 _ 42.805
Ammonia Nitrogen 0.I79 1,790.000 3.580
Calcium 1.580 15,800.000 31.600
Calcium Carbonate Eq. --- --- ---
Magnesium --- 3,090.000 6.180
Sodium --- 3,440.000 6.880
Sulfur --- --- ---
Nitrate N/Nitrite N --- 14.300 0.029
Barium --- --- --- SAR i
Chloride --- --- --- 1.14
Iron --- --- --- Ceiling Concen.
Aluminum --- 16,600.00 33.200 (Mg/Kg)
Arsenic --- 17.70 0.035 75
Cadmium --- 16.20 0.032 85
Chromium --- 32.500 0.065 —
Copper --- 207.00 0.414 _ 4,300
Lead --- 16.20 0.032 840
Mercury --- 0.57 0.001 57
Molybdenum --- 16.20 0.032 75
Nickel --- 16.20 0.032 420
Selenium --- 16.20 0.032 100
Zinc --- 560.00 1.120 7,500
Environmental Chemists ii 2021-03856
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Pluris Hampstead WWTF
11111101!0*Iililli11110041P0)10*Ii l_ = '
03/0.8/.21 I,526 3.1836
_ 03/08/21 667 2.8241
03/08/21 1,360 3.1335
03/08/21 531 2.7251
03/08/21 5,630 3.7505
03/08/21 616 2.7896
03/08/21 667 2.8241
Total 21.2305
Average 3.0329
Geometric Mean Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

4.
,4w Environmental Chemists, Inc®
. ej1vnirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392 0223 Lab • 910 392.4424 Fax
"� }' = 4 ,: `1, r -. 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
.r'z. :a.,;-`aw t'� ssu 255 A Wilmington Highway,Jacksonville,NC 28540 • 410.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(u'environmenialchemists.com
Pluris LLC. Date of Report: Mar 22, 2021
P. 0. Box 856 Customer P4#:
Sneads Ferry . NC 28460 Customer ID: 09110001
Attention: Randy Hoffer Report#: 2021-03856
Project ID: Hampstead Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-09396 Site: 001 3/8/2021 10:50 AM Solid/Sludge Kris King
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 2,95% 03/10/2021
Fecal Density SM 9221 C E MPN 24 hr 503 1526 MPN/g 03/08/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-09397 Site: 002 3/8/2021 10:50 AM Solid/Sludge Kris King
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.00% 03/10/2021
Fecal Density SM 9221 C E MPN 24 hr 503 667 MPN/g 03/08/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-09398 Site: 003 3/8/2021 10:50 AM Solid/Sludge Kris King
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.31 % 03/10/2021
Fecal Density SM 9221C E MPN 24 hr 503 1360 MPN/g 03/08/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-09399 Site: 004 3/8/2021 10:50 AM Solid/Sludge Kris King
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 3.39% 03/10/2021
Fecal Density SM 9221C E MPN 24 hr 503 <531 MPN/g 03/08/2021
Lab ID Sample ID: Collect Date/ime Matrix Sampled by
21-09400 Site: 005 3/8/2021 10:50 AM Solid/Sludge Kris King
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.02% 03/10/2021
Fecal Density SM 9221C E MPN 24 hr 503 5630 MPN/g 03/08/2021
•
Reonrt 5' 7n91-rmaca

�. � Environmental Chemists, Inca
r ol)- ,�rochern 6602 Windmill Way,Wilmin ton NC 28405 • 910.392.0223910.392.4424 Fax
Y g Lab •
`t , a r 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
�zt, Est :5.217-' 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS into(a'.environmentalcl1emists.com
Pluris LLC. Date of Report: Mar 22, 2021
P. O. Box 856 Customer PO#:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Randy Hoffer Report#: 2021-03856
Project ID: Hampstead Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-09401 Site: 006 3/8/2021 10:50 AM Solid/Sludge Kris King
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.25% 03/10/2021
Fecal Density SM 9221C E MPN 24 hr 503 616 MPN/g 03/08/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-09402 Site:007 3/8/2021 10:50 AM Solid/Sludge Kris King
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 3,00% 03/10/2021
Fecal Density SM 9221C E MPN 24 hr 503 667 MPN/g 03/08/2021
Reoart it:- 7021.03n56

� 'i 1, � ".. Environmental Chemists, Inc.
t�nVlr O�llem 6602 Windmill Way,Wilmington,NC 28405 • 910.392,0223 Lab • 910.392.4424 Fax
z5 � - 710 Bowsertown Road,Man teo,NC 27954 • 252.473.5702 Lab/Fax
% 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info@.'environmentaichemists.com
Pluris LLC. Date of Report: Mar 22, 2021
P. O. Box 856 Customer PO#:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Randy Hoffer Report#: 2021-03856
Project ID: Hampstead Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-09403 Site: Sludge 3/8/2021 10:50 AM Solid/Sludge Kris King
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200.7 16600 mg/kg 03/11/2021
Arsenic EPA 200.7 17.7 mg/kg 03/11/2021
Cadmium EPA 200.7 <16.2mg/kg 03/11/2021
Calcium EPA 200.7 15800 mg/kg 03/16/2021
Chromium EPA200.7 32.5mg/kg 03/11/2021
Copper EPA 200.7 207 mg/kg 03/11/2021
Lead EPA 200.7 <16.2 mg/kg 03/11/2021
Magnesium EPA 200.7 3090 mg/kg 03/11/2021
Molybdenum EPA 200.7 <16.2 mg/kg 03/16/2021
Nickel EPA 200,7 <16.2 mg/kg 03/11/2021
Potassium EPA 200.7 6390 mg/kg 03/16/2021
Selenium EPA 200.7 <16.2 mg/kg 03/18/2021
Sodium EPA 200.7 3440 mg/kg 03/16/2021
Zinc EPA 200,7 560 mg/kg 03/11/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 14.3 mg/kg 03/15/2021
Total Solids (%) SM 2540 B 3.02% 03/10/2021
pH SM 4500 H B 6.22 units 03/10/2021
Ammonia Nitrogen SM 4500 NH3 C 1790 mg/kg 03/11/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Or9 B 70100 mg/kg 03/11/2021
Total Phosphorus SM 4500 P F 23000 mg/kg 03/15/2021
Mercury SW046 7471B <0.570 mg/kg 03/12/2021
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: V\OLA.A10 \OV /1_,
Reanrt it 9f171.n'{R5fi

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910•392.0223
Client:—PU.IR.6
Date Report Number:0I — 038SIcy
Receipt of sample: ECHEM Picku. -011
Client Delivery❑ UPS 0 FedEx 0 Other
❑ YES 0 NO E N/A 1. Were custody seals present on the cooler?
0 YES ❑ NO ii N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt r2. 9 °C
How temperature taken: 0 Temperature Blank Corrected temperature upon receipt °C
les
IR Gun ID: Thomas Traceable 5/N 192511657 Against
!R Gun Correction Factor°°C:C: 0.0
ME❑ YES 0 NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
M❑ NO 4. Were proper custody procedures(relinquished/received) followed?
►! YES I NO 5. Were sample ID's listed on the COC?
NI YES ❑ NO 6. Were samples ID's listed on sample containers?
81. YES 0 NO 7. Were collection date and time listed on the COC?
Nl YES 0 NO 8. Were tests to be performed listed on the COC?
. YES ❑ NO 9. Did samples arrive in proper containers for each test?
YES 0 NO 10. Did samples arrive in good condition for each test?
NMi`N; 0 NO 11. Was adequate sample volume available?'
0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2?
❑ YES 0 NO 14. Were cyanide samples received at a pH>12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH>9?
•
❑ YES 0 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrect!
Sample(s) y preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCf
Time of preservation: NaOH
If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Vofatiles Samples) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

dmill Way
ton, NC
( 40 r '_4! ENVIRONMENTAL CHEMISTS, OFF!En 10 3 2 0223I FAX [phone]
NCDENR: DWQ CERTIFICATION#94 NCDHHS: DLS CERTIFICATION#37729 [e-mail]
Analytical&Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
Client: Pluris USA-Hampstead Facility PROJECT NAME: Hampstead WWTP1WQ0037287 REPORT NO: r
ADDRESS: PO Box 856 CONTACT NAME: Randy Hoffer PO NO: it. O
mcb-T,2 1
Hampstead, NC 28460 REPORT TO: rf coo p),,r, Lis,t,e i PHONE/FAX:
COPY TO: )6K 1,„, p l"`- c U54, Care email: [e-mail]
Sampled By: ,r. - SAMPLE TYPE: I =Influent, E =Effluent, W=Well, ST=Stream, SO=Soil, SL =Sludge, Other:
ollection ' _ PRESERVATION
d c� N .0 C S.7 C _1 W -'
Sample Identification E a `o 2 o `o at g ? .., o 3 0 o W ANALYSIS REQUESTED
+n F o C9 o a U E 1 i O s N z z r F
Date _ Time Temp U " Z z °_
C P
PPI 001 Eff(2/week) G G X BOD,TSS
C P
-
PP! 001 Eff(2/week) _ G G X Total P,Total N(calc), NH3
C P
PP! 001 Eff(2/wee _
G G X Fecal Coliform (grab)
C P
PPI 001 (March, July, Nov) G G X TDS, Chloride (Triannuals)
/cc,k -#5�43 3-?a..\ Joe /7..21) C 9 0 / _ / l�►`r5
1�cv,s��/C 6 #7 - CD G � ._ .
C P
PPI 002 (2/month) _ G G 1. q( X > fo
T N(calc), NH3
C P . q9
`PPI 002 (2/month) G _ G q Cl, r ,� X
[l /r
/ -,e..f`5 3-$—aA /D isa l u I C I,,.�` /f/✓/Y�c.+5 QL Ik
C P
PPI 002 (March, July, Nov) G G X TDS, Chloride (triannuals)
C P
G G
BOD Limit: 10 mglL(monthly), Fecal Coilform limit: 14 colonies/100 ml (geometric average/month), NH3-4 me/L i it-4 mg/L. P limit:2 mg/L.TSS-15 rng1L
Transfer Relinquished By: Date/Time eceived By: DatefTime
ici Q_ [
2. / D q
e °C -C ` Accepted: acted: Resample a uested:
Temperature p r1
Delivered By Received By: Date: Time: ca
Comments: TU NA OUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals,LLC WQ Permit Number: WQ0034806
WWTP Name: Pluris Hampstead WWTF NPDES Number: WQ0037287
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106)-Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ - Alt B (Alk Treatment)❑ 1 Alt. C (Prior Testing)❑
Alt.D(No Prior Test) ❑ Process to Further Reduce Pathogengs ❑
If applicable to alternative performed(Class A only)indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying 0 Heat Treatment ❑ Thennophilic ❑
Beta Ray 0 Gamma Ray 0 Pasteurization 0
Class B: lAit. (1)Fecal Density a Alt. (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion CI
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B)complete the following monitoring data:
-Numbcrot Analytical
Parameter Allowable Level Pathogen Density Frequency Sample
Tech-
in Sludge densExcee- of AnalysisType 8 Minimum Geo. Mean Maximum Units deuces yp niatie
2 x 10 to the MPN 531 1,079 5,630 MPN/g 0 Annual Grab SM92210E
6th power
per gram of -
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T.1107)-Please indicate alternative performed:
Alt.1 (VS reduction) 0 Alt.2 (40-day bench) ❑ Alt. 3.(30-day bench) ❑ Alt.4(Spec.O.uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6(Alk. Stabilization ❑ Alt 7(Drying-Stable) ❑ Alt. 8 (Drying-Unstable) ❑
Alt. 9 (Injection) 11:1 ,Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
E1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
0 "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in I5A NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kris King, O ( Wesley Wooten, President
Preparer Name and Titl type or print) Land Applier Name and Title(if applicable)(type or print)
At al .., 3/22/21
Sign ure of P arer* Si nature of La Applier(if applicable)
g pp pp ) Datc
*Preparer is defined in 40 CFR Part 503.9(r)and I5A NCAC 2T .1102(26)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 20,2021
North Topsail WWTF Permit No.WQ0005849
4.07 %Solids
6.78 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) _ (Mg/Kg x 0.002)
Nitrogen(TKN) 3.850 38,500.000 77.000
Phosphorus 3.180 31,800.000 63.600
Potassium 0.391 3,910.000 7.820
PAN(injected)* 1.157 11,567.222 23.I34
PAN(surface)* 1.157 11,565.992 _ 23.132
Ammonia Nitrogen 0.000 2.460 0.005
Calcium 2.110 21,100.000 42.200
Calcium Carbonate Eq. --- --- --
Magnesium --- 2,360.000 4.720
Sodium --- 3,240.000 6.480
Sulfur ___ ___
Nitrate N/Nitrite N --- 15.500 0.031
Barium --- -- --- SAR
Chloride --- --- --- 1.14
Iron --- --- --- Ceiling Concen.
Aluminum --- 32,400.00_ 64.800 (Mg/Kg)
Arsenic _ --- 22.40 0.045 75
Cadmium --- 11.90 0.024 _ 85
Chromium --- 31.400 --- --
Copper --- 134.00 0.268 4,300
Lead --- 11.90 0.024 840
Mercury --- 0.41 0.001 57
Molybdenum --- 11.90 _ 0.024 75
Nickel --- 11.90 0.024 420
Selenium --- 11.90 0.024 100
Zinc --- 2,390.00 4.780 7,500
1
Environmental Chemists# 2021-01017
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits arc listed as detection Iimits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Pluris North Topsail WWTP
€;Date€ € €Fecal Co if€aim 11• ill
01/20/21 2,942 _ 3.4686
01/20/21 _ 1,166 3.0667
01/20/21 1,194 3.0770
01/20/21 469 2.6712
01/20/21 3,476 3.5411
01/20/21 1,197 3.0781 _
01/20/21 3,386 3.5297
Total 22.4324
Average 1 3.2046
Geometric Mean 642 Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

-' , , Environmental Chemists, Inc.
! J1 evzrachenrn°- 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
'4 rya `;s,x i `, ," 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
`1', ' f�i�'-', ::: • s esra 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Pluris LLC. Date of Report: Feb 05, 2021
P. O. Box 856 Customer PO#:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Randy Hoffer Report#: 2021-01017
Project ID: North Topsail
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-02468 Site: Sludge 1/20/2021 8:45 AM Solid/Sludge Client
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200.7 32400 mg/kg 01/29/2021
Arsenic EPA 200.7 • 22.4 mg/kg 01/29/2021
Cadmium EPA 200.7 <11.9 mg/kg 01/29/2021
Calcium EPA 200.7 21100 mg/kg 01/29/2021
Chromium EPA 200.7 31.4 mg/kg 01/29/2021
Copper EPA 200.7
134 mg/kg 01/29/2021
Lead EPA 200.7 <11.9 mg/kg 01/29/2021
Magnesium EPA200.7 2360mg/kg 01/29/2021
Molybdenum EPA 200.7 <11.9 mg/kg 01/29/2021
Nickel EPA 200.7 <11.9 mg/kg 01/29/2021
Potassium EPA 200.7 3910 mg/kg 01/29/2021
Selenium EPA 200.7 <11.9 mg/kg 01/29/2021
Sodium EPA 200.7 3240 mg/kg 01/29/2021
Zinc EPA200.7 2390mg/kg 01/29/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 15.5 mg/kg 01/26/2021
Total Solids (%) SM 2540 B 4.07% 01/21/2021
pH SM 4500 H B 6.78 units 01/25/2021
Ammonia Nitrogen SM 4500 NH3 c <2.46 mg/kg 01/22/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 org B 38500 mg/kg 01/22/2021
Total Phosphorus SM 4500 P F 31800 mg/kg 01/29/2021
Mercury SW8467471B <0.410 mg/kg 01/25/2021
Report#:: 2021-01017
OMITS]1 n!'I

•
am t kwYr r}4 s )r,
Environmental Chemists, Inc.o {it S ' a r:s:=, , ,_
k envirocheniw 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab ° 910.392.4424 Fax
r r' `{'3 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab Fax
"* 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoia environmentalchemists.com
Pluris LLC. Date of Report: Feb 05, 2021
P. O. Box 856 Customer PO#:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Randy Hoffer Report#: 2021-01017
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-02469 Site: 001 1/20/2021 8:47 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.74% 01/21/2021
Fecal Density SM 9221C E MPN 24 hr 503 2942 MPN/g 01/20/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-02470 Site: 002 1/20/2021 8:50 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.86% 01/21/2021
Fecal Density SM 9221C E MPN 24 hr 503 1166 M PN/g 01/20/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-02471 Site: 003 1/20/2021 8:52 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) 5M 2540 8 3,77% 01/21/2021
Fecal Density 5M 9221C E MPN 24 hr 503 1194 MPN/g 01/20/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-02472 Site: 004 1/20/2021 8:54 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) 5M25406 4.27% 01/21/2021
Fecal Density SM 9221C E MPN 24 hr 503 469 MPN/g 01/20/2021
Lab ID Sample ID: Collect Date/ime Matrix Sampled by
21-02473 Site:005 1/20/2021 8:56 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.74% 01/21/2021
Fecal Density SM 9221C E MPN 24 hr 503 3476 MPN/g 01/20/2021
Report#: 2021-01017

f � Environmental Chemists, Inc.tiiiti'ri�r�irocchemlhq ' 6602 Windmill Way, Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
��;� , � ,� �� � ,--, 710 Bowsertown Road,Manheo,NC 27954 ' 252,473.5702 Lab/Fax�' *� ° li" $M` 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Pluris LLC, Date of Report: Feb 05, 2021
P. O. Box 856 Customer PO #:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Randy Hoffer Report#: 2021-01017
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-02474 Site: 006 1/20/2021 8:58 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.76% 01/21/2021
Fecal Density SM 9221C E MPN 24 hr 503 1197 MPN/g 01/20/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-02475 Site: 007 1/20/2021 8:59 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.84% 01/21/2021
Fecal Density SM 9221C E MPN 24 hr 503 3386 MPN/g 01/20/2021
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: la4,,,cQ,9a! OWp;;01
Report#.: 2021.01017 Pace 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab#94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
-� 1 ' Y�4,t` Sample Receipt Checklist
I�LJ
Client: 5 Date: JZO/ a./ Report Number:' I 01 0 11
Receipt of sample: ECHEM Pickup ❑ Client Delivery q1 1UPS ❑ FedEx 0 Other El
❑ YES ❑ NO N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt , t °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank IX
Against Bottles
IR Gun ID: Thomas Traceable 5/N 192511657 IR Gun Correction Factor°C: 0.0
❑ YES El NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
►% YES 0 NO 4. Were proper custody procedures (relinquished/received) followed?
>," YES 0 NO 5. Were sample iD's listed on the COC?
l YES El NO 6. Were samples lD's listed on sample containers?
•'N YES ❑ NO 7. Were collection date and time listed on the COC?
1i' YES 0 NO 8. Were tests to be performed listed on the COC?
YES 0 NO 9. Did samples arrive in proper containers for each test?
EV YES El NO 10. Did samples arrive in good condition for each test?
l!' YES ❑ NO 11. Was adequate sample volume available?'
r YES ❑ NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES El NO 14. Were cyanide samples received at a pH>12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH>9?
❑ YES 0 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet,
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2504 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s) _were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

• ENVIRONMENTAL CHEMISTS, INC 06Q2 Windmill Way Wilmington,NC21 5
Analytical&Consulting ChemistsNCDENR: DWQ CERTERICATION#94 NCDHHS:DLS CERTIFICA'i10N#37729 OFFICE:99Q-392-0223 FAX 910-3B2�4Z4
COLLECTION AND CHAIN OF CUSTODY
CLIEhiT:_Pluris x`
PROJECT NAME: ,. „ � REPORT NO: ! — Oi 0 /
ADDRESS: CONTACT NAME: - r��'> PO NO:
REPORT TO: PHONE/FAX:
COPY TO: E-MAIL;
Sampled By: SAMPLE TYPE: I =influent, E=Effluent,W=Well,�-, ST=Stream, SO=Soil, SL=Sludge, Other:
Collection 2 _
Sample Identification E E o E. T t n m PRESERVATION
t' E is e ° ° S ; m -' 8 s 2 u°ri ANALYSIS REQUESTED
Date Time Temp rn U U ' L./ 2 2 = o
es_ �u . 1 /-.�-z/ �-y$-- C P -
1-Za-zl F-,Y7 C P
7ec�; / G G clYV9
T 1 -� a_ /-2 z1 k.' -0_ C P 3
f1 G G 4910
7'— °C /-2c-Z/ S'! -CZ. C P - -
/� G G o?�1 t
7 '1 Sr J-2�-v(- �:5 t:s C P °���a
7C/4
G G Y73
4- ' 4 1-24)-2f 5-, C P
G G a`�t1-7�j
(�PC 7 1-?a-71 8S7'-'. ' C P -
/�/ G G t-[ 77
a
l zzf _ g of C P 0 t — i . . .
- 15/&-e
' (01'1 ' (1g,r4-
NOTICE-0 45 '' 0:1
l:CHLORINA7laN: Samples for monla,TKN, yanlde,Phenol and erla must be dechlorinated(0.2 ppm or l )In the field at the time of collection. See reverse for Instructions
Transfer linquished By: Date/Time Received BY Datemme
1.
2.
Temperature when Received: o: ' 1 Accepted: ✓
p Rejected: Date:Resampfr3 IReq lasted:
,(ko.,A)b Received By:/ � l
Delivered By: e f 0-D
Comments: �- Time:
TURN OUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: Lewis Farms and Liquid Waste,Inc. WQ Permit Number: WQ0000455
WWTP Name: Pluris North Topsail _ NPDES Number: WQ0005849
Monitoring Period: From 1/1/2021 12/31/2021 •
Pathogen Reduction(15A NCAC 02T.1106)-Please indicate level achieved and alternative performed: :
Class A: ' Alt.A(time/temp) 0 I Alt B (Alit Treatment)❑ 1 Alt.C(Prior Testing)❑ i
AIt.Di
(No Prior Test) ❑ Process to Further Reduce I'athogengs ❑
If applicable to alternative performed(Class A only)Indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying 0 Heat Treatment ❑ Thennophilic 0
Beta Ray Cl Gamma Ray ❑ Pasteurization ❑ MEERMSERM
Class B: lAlt.(I)Fecal Density El I Alt.(2)Process to Significantly Reduce Pathogens ❑.. f
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
•
Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑
Anaerobic _ : s::: P g g
Digestion :,•> >:�.: •:ton ❑
If applicable to alternative performed(Class'A or Class B)complete the following monitoring data:
Allowable Level Pathogen DensityP Number of Analytical •
Parameter Tech-
in Sludge g Excee- l reguency Sample g Minimum Geo.Mean Maximum Units drnces of Analysis Type _ n;aue
2 0 to le MPN 469 1,602 3,476 MPN/g 0 Annual Grab 5M92210E 6th
power _
per gram of CFU
Fecal Coliform total solids
I000 mpn per gram
of total solid (dry
weight) 7.
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T.1107)-Please indicate alternative performed:
_Alt,1(VS reduction) ❑ Alt.2(40-day bench) ❑ Alt.3 (30-day bench) El Alt.4(Spec.0,uptake) ❑
Alt.5(14-Day Aerobic) ❑ Alt.6(Alk.Stabilization ❑ Alt 7(Drying-Stable) ❑ AIt.8(Drying-Unstable) ❑
Alt.9(Injection) 0 Alt. 10(Incorporation) El_No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT(please check the appropriate statement)
0 "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Randy Hoffer,ORC Wesley Wooten,President
Preparer Name and Title ty e or print) Land AppIier Name and Title(if applicable)(type or print)
) /17 - 1 t�/•✓/�' Il17/21
�t i
ature of r ,, to Signature ofLand Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
l]ENR FORM PVRF 02T(12/2006)

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: June 3,2021
Southeast Brunswick Sanitary District WWTP Permit No.WQ0013200
3.40 %Solids
6.54 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x-10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 6.290 62,900.000 125.800
Phosphorus 0.227 2,270.000 4.540
Potassium 0.524 5,240.000 10.480
PAN(injected)* 2.223 22,227.200 44.454
PAN(surface)* 1.983 19,832.200 39.664
Ammonia Nitrogen 0.479 4,790.000 9.580
Calcium 2.590 25,900.000 51.800
Calcium Carbonate Eq. --- --. ---
Magnesium --- 4,180.000 8.360
Sodium --- 2,160.000 4.320
Sulfur --- --- ---
Nitrate N/Nitrite N --- 4.200 0.008
Barium --- SAR
Chloride _ --- --- --- 0.60
Iron --- --- --- Ceiling Concen.
Aluminum --- 20,600.00 41.200 (Mg/Kg)
Arsenic --- 25.60 0.051 75
Cadmium --- 20.70 0.04I 85
Chromium --- 35.600 --- --
Copper --- 249.00 0.498 4,300
Lead --- 20.70 0.041 840
Mercury --- 0.676 0.001 57
Molybdenum --- 20.70 _ 0.041 75 _
Nickel - --- 20.70 0.041 420
Selenium --- 20.70 0,041 100
Zinc --- 806.00 1.612 7,500
Environmental Chemists# 2021-08981
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Ratc)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

t ,s . ;� Environmental Chemists, Inc
fir t .1 : � ,� .
, ):erivingon -me 6602 Windmill Way,Wilmington,NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
r,'vncs `'f 710 Bowsertown Road,Manteo,NC 27954 . 252.473.5702 Lab/Fax
z =te , ' y „s„ rtr �' 255-A Wilmington Highway,Jacksonville,NC 28540 . 910.347.5843 Lab/Fax
39 7...q
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Envirolink, Inc. Date of Report: Jul 01, 2021
PO Box 670 Customer PO#:
Bailey NC 27807 Customer ID: 16040014
Attention: Report#: 2021-08981
Project ID: SE Brunswick Sanitary
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-22380 Site: Sludge 6/3/2021 1:00 PM Solid/Sludge Client
Test Method Results Date Analyzed
Total Organic Carbon (TOC) 9060 302000 mg/kg 06/15/2021
PAN Calculation 19800 mg/kg 06/17/2021
Used 30%Mineralization Rate
Chlordane(TCLP) SW 846 Method BOB16/3510 <0.02 mg/L 06/09/2021
Endrin (TCLP) SW 646 Method 8081B/3510 <0.0005 mg/L 06/09/2021
Heptachlor(TCLP) SW 646 Method 8081S/3510 <0.0005 mg/L 06/09/2021
Heptachlor epoxide (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 06/09/2021
Lindane (TCLP) SW 846 Method 80 81 813 5 1 0 <0.0005 mg/L 06/09/2021
Methoxychlor(TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 06/09/2021
Toxaphene(TCLP) SW 846 Method 8081B/3510 <0.05 mg/L 06/09/2021
1,4-Dichlorobenzene(TCLP) SW B46 method 8270/3510 <0.050 mg/L 06/11/2021
2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/11/2021
2,4,6-Trichlorophenol(TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/11/2021
2,4-Dinitrotoluene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/11/2021
Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/11/2021
Hexachioro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/11/2021
Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/11/2021
Hexachioroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/11/2021
m +p-Cresol (TCLP) SW 846 method 8270/3510 <0,050 mg/L 06/11/2021
Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 06/11/2021
o-Cresol (TCLP) SW 846 method B270/3510 <0.050 mg/L 06/11/2021
Pentachlorophenol(TCLP) SW 846 method 8270/3510 <0.250 mg/L 06/11/2021
Pyridine (TCLP) 5W 848 method 8270/3510 <0.050 mg/L 06/11/2021
pH SW 846 Method 9045D 6.54 units 06/30/2021
Result estimated. Analyzed out of 15 minutes hold time.
2,4,5-TP(TCLP) SW846 Method 8151A <0.003 mg/L 06/10/2021
2,4-D (TCLP) 5W846 Method 8151A <0.003 mg/L 06/10/2021
Report#:: 20 21-08 9 8 1 Page 1 of 3

r .4 , Environmental Chemists, Inc.
F'," envirocheII:- . 6602 Windmill Way,Wilmington,NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
�' _ '.�-P `- r sm
710 Bowsertown Road,Manteo,NC 27954 . 252.473.5702 Lab/Fax
255 A Wilmington Highway,Jacksonville,NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info@ environmentalchemists.com
Envirolink, Inc. Date of Report: Jul 01, 2021
PO Box 670 Customer PO#:
Bailey NC 27807 Customer ID: 16040014
Attention: Report#: 2021-08981
Project ID: SE Brunswick Sanitary
1,1-Dichloroethylene (TCLP) SW846 Method 8280/5030 <0.01 mg/L 0610912021
1,2-Dichloroethane(TCLP) SW846 Method 8260/5030 <0.01 mg/L 06/09/2021
Benzene(TCLP) SW846 Method 826015030 <0.01 mg/L 06/09/2021
Carbon Tetrachloride(TCLP) 5W846 Method 8260/5030 <0.01 mg/L 06/09/2021
Chlorobenzene(TCLP) SW846 Method 8260/5030 <0.01 mg/L 06/09/2021
Chloroform (TCLP) 5W846 Method 0260/5030 <0.01 mg/L 06/09/2021
Methyl ethyl ketone(TCLP) SW846 Method 8260/5030 <0.05 mg/L 06/09/2021
Tetrachloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 06/09/2021
Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 06/09/2021
Vinyl Chloride(TCLP) SW846 Method 0260/5030 <0.01 mg/L 06/09/2021
RCI
Cyanide SM 4500 CN 0 5.49 mg/kg 06/08/2021
Sulfide SM 4500 s o 6.20 mg/kg 06/08/2021
Ignitability SW 846 method 1010 >195'F 06/18/2021
Sludge Residuals
Aluminum EPA 200.7 20600 mg/kg 06/09/2021
Arsenic EPA 200.7 25.6 mg/kg 06/09/2021
Cadmium EPA 200.7 <20.7 mg/kg 06/09/2021
Calcium EPA 200.7 25900 mg/kg 06/09/2021
Chromium EPA 200.7 35.6 mg/kg 06/09/2021
Copper EPA 200.7 249 mg/kg 06/09/2021
Lead EPA 200.7 <20.7 mg/kg 06/09/2021
Magnesium EPA 200.7 4180 mg/kg 06/09/2021
Molybdenum EPA 200.7 <20.7 mg/kg 06/09/2021
Nickel EPA 200.7 <20.7 mg/kg 06/09/2021
Potassium EPA 200.7 5240 mg/kg 06/09/2021
Selenium EPA 200.7 <20,7 mg/kg 06/09/2021
Sodium EPA 200.7 2160 mg/kg 06/09/2021
Zinc EPA 200.7 806 mg/kg 06/09/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 4.20 mg/kg 06/1012021
Report#:: 2021-08901
Page 2 of 3

r' .r k Environmental C emists, Inc..,' ' . Ag ,
..
e iaeh
` �0 3 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
V�sa 4 "' � rrri; 710 Bowsertown Road,Manteo,NC 27954 . 252.473.5702 Lab/Fax
' '` ;;r;. a.,ti 255-A Wilmington Highway,Jacksonville,NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(aenvironmentalchemists.cool
Envirolink, Inc. Date of Report: Jul 01, 2021
PO Box 670 Customer PO#:
Bailey NC 27807 Customer ID: 16040014
Attention: Report#: 2021-08981
Project ID: SE Brunswick Sanitary
Total Solids(%) SM 2540 B 3.40°/n 0 611 412 0 2 1
Ammonia Nitrogen SM 4500 NH3 C 4790 mg/kg 06/04/2021
Total Kjeldah! Nitrogen (TKN) SM 4500 Org B 62900 mg/kg 06/04/2021
Total Phosphorus SM 4500 P r 2270 mg/kg 06/10/2021
Mercury SW846 74710 0.6760 mg/kg 06/09/2021
TCLP Metals
Arsenic EPA 200.7 <1.0 mg/L 06/15/2021
Barium EPA 200.7 <1.0 mg/L 06/15/2021
Cadmium EPA 200.7 <1.0 mg/L 06/15/2021
Chromium EPA 200,7 <1.0 mglL 06/15/2021
Lead EPA 200.7 <1.0 mg/L 06/15/2021
Selenium EPA 200.7 <1.0 mg/L 06/15/2021
Silver EPA 200.7 <1.0 mg/L 06/15/2021
Mercury EPA 245.1 <0.0002 mg/L 06/09/2021
Comment: Results reported on a dry weight basis.
Reviewed by: `7, d ,d_r,-.-L -,,t____d,
Report#:: 2021-06901
Page 3 of 3

Analytical Environmental Services, Inc Date: I8-Jun-21
Client: Environmental Chemists,Inc. Client Sample ID: 21-22380
Project Name: 21-22380 Collection Dale: 6/3/2021 1:00:00 PM
Lab ID: 2106C29-001 Matrix:
Soil
Analyses Result Reporting Dilution
Limit Qual Units BatchlD Date Analyzed Analyst
Factor
Total Organic Carbon in Soil SW9060 (SW9060 Modified)
Total Organic Carbon(TOC) 302000 998 m8/1c8•dry 316981 I 06/15/2021 10.04 GK
Qualinen: • Value exceeds maximum conumtnant lead
E Eswnased(value above qu nurauon range)
BELL Below reporting brill{ S Spike Recovery ausende hmtu due to manse
H Holding limes for preparation or analysts exceeded
Narr Sec case narrative
N Ana lyre not NCLAC certified F Analyzed in the lab which is a devsauon nom the method
B Analyze detected In the associated method blank
c Less than Resell value
Grimmz. than Result value
1 Estimated value detected below Reporting Lima
Page 4 of 7

Environmental Chemist, Inc., Wilmington, NC Lab#94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: 3e. �{�bt-c.Dk ( (-5- Date: � 3 l21 Report Number: --GjCj CD I
Receipt of sample: CHEM Pickup V Client Delivery !LIPS 0 FedEx El Other 0
❑ YES ❑ NO N/A 1. Were custody seals present on the cooler?
❑ YES 0 NO N/A . If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: 0 Temperature Blank X Against Bottles
IR Gun ID:Thomas Traceable S/N 192511657 1R Gun Correction Factor°C: 0.0
)I'4 YES ❑ NO 3. if temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
►4 YES 0 NO 4. Were proper custody procedures(relinquished/received) followed?
V. YES 0 NO 5. Were sample ID's listed on the COC?
YES ❑ NO 6. Were samples ID's listed on sample containers?
YES 0 NO 7, Were collection date and time listed on the COC?
►~ YES ❑ NO 8. Were tests to be performed listed on the COC?
r YES 0 NO 9, Did samples arrive in proper containers for each test?
k.. YES 0 NO 10. Did samples arrive in good condition for each test?
r YES ❑ NO 11. Was adequate sample volume available?'
P+ YES 0 NO 12. Were samples received within proper holding time for requested tests?
YES ❑ NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH >12?
YES 0 NO 15. Were sulfide samples received at a pH>9?
OK YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/E? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/I_?
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Vofatiles are pH checked at time of analysis and recorded on the benchsheet. )
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
i Sample(s) _ were received incorrectly preserved and were adjusted accordingly
by adding(circle one): 1-12504 HNO3 NCI NaOH
Time of preservation: if more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s)_ _ were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

envizochem. ENVIRONMENTAL CHEMISTS I N C 6602 Windmill Way Wilmington,NC 2E40$
OFFICE:910-392-0223 FAX [phone]
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 info Oenvironmentalchemists.com
COLLECTION AND CHAIN OF CUSTODY
Client: 6 k jr,f4,_bu: 541%),-KjiDi PROJECT NAME: REPORT NO:
ADDRESS: CONTACT NAME: PO NO: ,{,- b V
REPORT TO: PHONE/FAX:
COPY TO: email:
Sampled By: SAMPLE TYPE:I=Influent,E=Effluent,W=Weil,ST=Stream,SO=Soil,SL=Sludge,
OMotion ' a s Other:
... ;o ., o Q PRESERVATION
Sample Identification a a 8 E 1 o o a co m w
E a t� o le,- s E z 3 on o o w ANALYSIS REQUESTED
Date Time Temp 0 e " 'z 2 z o
j'WP *DWG- i 6 ' }3�� j L C CPJ 3
c- �cLA -rk,� s
C P
G G _ � �� cS,��S
C P
G G
C P
G G
_ C P I
G G
C P
G G
C P
G G
C p
I I G G
i _
Transfer Relinquished By: DatetTme
Received By: Datenme
1.
2. r
Temperature when Received: p26 � Accepted: e ec ,
Resample u t
Delivered By: Received By: Date: Time:
Comments: TURNAROUND:

COASTAL FARMS AND RESIDUALS,LLC
WQ0034806
Southeast Brunswick Sanitary District WWTF
_ 11/15/21 174,194 5.2410
11/15/21 104,478 5.0190
11/15/21 169,812 5.2300
11/15/21 155,173 5.1908
11/15/21 165,645 5.2192
11/15/21 _ 112,904 5.0527
11/15/21 113,269 5.0541
Total 36.0068 1
Average 5.1438
Geometric Mean !iiiiigIng0iin Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B -Alternative 1 Pathogen Reduction
requirement.

:6 Environmental Chemists, Inc.
je virOehn a $ 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
�p fi sM, 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
"`~ 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Envirolink, Inc. Date of Report: Nov 18, 2021
PO Box 670 Customer PO#:
Bailey NC 27807 Customer ID: 16040014
Attention: Report#: 2021-20213
Project ID: SE Brunswick Sanitary
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-50655 Site: 1 11/15/2021 7:30 AM Solid/Sludge lewis farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 3.10% 11/16/2021
Fecal Density SM 9221C E-2014 174194 MPN/g 11/15/2021
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
21-50656 Site: 2 11/15/2021 7:32 AM Solid/Sludge lewis farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 3,35% 11/16/2021
Fecal Density SM 9221C E-2014 104478MPN/g 11/15/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-50657 Site:3 11/15/2021 7:34 AM Solid/Sludge lewis farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 3.18% 11/16/2021
Fecal Density SM 9221C E-2014 169812 MPN/g 11/15/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-50658 Site:4 11/15/2021 7:36 AM Solid/Sludge lewis farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.48% 11/16/2021
Fecal Density SM 9221C E-2014 155173 MPN/g 11/15/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-50659 Site: 5 11/15/2021 7:38 AM Solid/Sludge lewis farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 3,26% 11/16/2021
Fecal Density SM 9221C E-2014 165645 MPN/g 11/15/2021
Report#:: 2021-20 21 3
Page 1°€2

1 µ�,5 Environmental Chemists, Inc.
a r t
st'
envlroGh ie i 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910 392.4424 Fax
a �4, ' ''fir 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
` '`• 1' •':10.-* 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5643 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Envirolink, Inc. Date of Report: Nov 18, 2021
PO Box 670 Customer PO#:
Bailey NC 27807 Customer ID: 16040014
Attention: Report#: 2021-20213
Project ID: SE Brunswick Sanitary
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-50660 Site:6 11/15/2021 7:40 AM Solid/Sludge lewis farms
Test Method Results Date Analyzed
Total Solids(%) SM 2540 s 3.10% 11/16/2021
Fecal Density SM 9221C E-2014 112904 MPN/g 11/15/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-50661 Site: 7 11/15/2021 7:42 AM Solid/Sludge lewis farms
Test Method Results Date Analyzed
Total Solids(%) SM2540a 3,09% 11/16/2021
Fecal Density SM 9221C E-2014 113269 MPN/g 11/15/2021
Comment: Results reported on a dry weight basis.
Reviewed by: ,66
Report fir: 2021-20213
Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab#94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: NUl lz-C] LAIC- _ Date1 15 0Z.1 Report Number:_ 02,1 -�0 9
Receipt of sample: ECHEM Pickup 0 Client Deliveryl' 1UPS 0 FedEx 0 Other 0
❑ YES ❑ NO ,( N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO k N/A 2. If custody seals were present, were
they intact/unbroken?
Original temperature upon receipt__, . °C Corrected temperature upon receipt C
How temperature taken: ❑ Temperature Blank lT Against Bottles
IR Gun ID:Thomas Traceable 5/N 192511657 fR Gun Correction Factor°C:0.0
❑ YES 0 NO 3. If temperature of cooler exceeded 6°C,was Project Mgr./QA notified?
R4 YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed?
iy YES 0 NO 5. Were sample ID's listed on the COC?
YES 0 NO 6. Were samples ID's fisted on sample containers?
YES ❑ NO 7. Were collection date and time listed on the COC?
YES ❑ NO 8. Were tests to be performed listed on the COC?
YES 0 NO 9. Did samples arrive in proper containers for each test?
YES ❑ NO 10. Did samples arrive in good condition for each test?
tit YES 0 NO 11. Was adequate sample volume available?'
YES ❑ NO 12. Were samples received within proper holding time for requested tests?
❑ YES El NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH>12?
r
❑ YES ❑ NO 15. Were sulfide samples received at a pH>9?
❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
0 YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Samples) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2504 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

e tiVirt  0 ENVIRONMENTAL CHEMISTS, INC 6602Wiind9 it 20223ilmingon,NC284 FAX 5
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: Lewis Farms &Liquid Waste PROJECT NAME: SSC Or,..•1, .j L� c.ii 1/ REPORT NO: Jit2 / - ZoL/-T
ADDRESS: CONTACT NAME: Wesley Wooten PO NO:
REPORT TO: Martin Mabe/Mahe-Wilcox PHONE/FAX:
COPY TO: email:
Sampled By:_ (s a-s horl5 SAMPLE TYPE: I=Influent, E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge, Other:
Collection -
a r a _ m PRESERVATION
Sample Identification °. co a ` " •E � o 111 ,
C h E 8 t7 a s r E a z u g n o o r6 ANALYSIS REQUESTED
Date Time Temp u u " `' z z = 2 = x i- o
/r/ 0 _ C _ P _ -
Sludge G G / X Full TCLP, RCI, Nutrients/Metals
1 44: C P _ f1L14
G G X Fecal Density/%TS
2
4-54 _ C P _ S�L4 - -
G G _ X Fecal Density/%TS
3 )4 - C P 5.1:(�
G G X Fecal Density/%TS
4-ii C P
sl
4 G G �'� X Fecal Density!°/aTS
.5 G G ('6 X Fecal Density)%TS
''ra. C P
6 i G G Pt" - X Fecal Density/%TS
4.vt.
C P
7 G G ���� X Fecal Density/%T5
Transfer Relinquished By: Date/Time Received By: Date/Time
1.
2. s
Temperature when Received: r Accepted: Rejected: Resarnple sted:
Delivered By: Received By: (/�`,�(/7 Date: 'r Ls& Time: ref
Comments: TU NAROUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals,LLC WQ Permit Number: WQ0034806
WWTP Name: Southeast Brunswick Sanitary District WWTP NPDES Number: WQ0013200
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A: Alt. A (timeltemp) ❑ f Alt B (AIk Treatment)❑ Alt.C(Prior Testing)❑
AIt.D(No Prior Test) ❑ 1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ IIeat Treatment ❑ Thennophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alt.(1)Fecal Density El Alt.(2)Process to Significantly Reduce Pathogens 0
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization 0 I Air Drying ❑ j Composting ❑ 'Aerobic Digestion ❑
Anaerobic Digestion ❑ :-
If applicable to alternative performed (Class A or Class B)complete the following monitoring data:
Allowable Level Pathogen en DensityNumber of Analytical
Parameter Excee- Frequency Sample Tech
in Sludge Minimum Geo.Mean Maximum Units dcnccs of Analysis Type ninuc
2 x 10 to the MPN 104,478 139,263 174,194 MPN/g 0 Annual Grab SM922ICE
6th power
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
conform) weight)
Vector Attraction Reduction (15A NCAC 02T.1107)-Please indicate alternative performed:
Alt.1 (VS reduction) ❑ Alt.2(40-day bench) 0 Alt.3 (30-day bench) ❑ ,Alt.4(Spec.O,uptake) 0
Alt.5 (14-Day Aerobic) ❑ Alt.6(Alk.Stabilization ❑ Alt 7(Drying-Stable) ❑ Alt.8(Drying-Unstable) CI
Alt.9(Injection) p Alt. 10(Incorporation) [l No vector attraction reduction alternatives were perfornied ❑
CERTIFICATION STATEMENT(please check the appropriate statement)
0 "I certify,under penalty of law,that the pathogen requirements in 15A NCAC OZT.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. 1 am aware that there are
significant penalties for false certification including fine and imprisonment."
Stephanie Moore,ORC Wesley Wooten,President
Preparer Name and Title(type or print) Land Applier Name and Title(if applicable)(type or print)
1/19122
Signature of Preparer* Date Signature of La Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
DENR FORM PVRF 02T(1212006)

COASTAL FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 10,2021
Summerhouse Permit No.WQ0029945
0.70 %Solids
6.84 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 5.780 57,800.000 115.600
Phosphorus 1.820 18,200.000 36.400
Potassium 0.154 1,540.000 3.080
PAN(infected)* 1.843 18,425.500 _ 36.851
PAN(surface)* 1.767 17,670.500 _ 35.341
Ammonia Nitrogen 0.151 1,510.000 3.020
Calcium 3.400 34,000.000 68.000_
Calcium Carbonate Eq. --- --- ---
Magnesium --- 3,290.000 6.580
Sodium --- 9,170.000 18.340
Sulfur --- --- ---
Nitrate N/Nitrite N --- 28.500 0 057
Barium --- --- --- SAR
Chloride --- --- --- _ 1.92
Iron - --- --- Ceiling Concen.
Aluminum --- 1,670.00 3.340 (Mg/Kg)
Arsenic --- 31.60 _ 0.063 75
Cadmium --- _ 31.60 0.063 85
Chromium --- 31.600 --- —
Copper --- _ 92.70 0.185 4,300
Lead -- 31.60 0.063 840 _
Mercury --- 2.39 0.005 57
Molybdenum --- 31.60 0.063 _ 75
Nickel --- _ 31.60 0.063 420
Selenium --- 31.60 0.063 _ 100
Zinc --- 1,540.00 3.080 7,500
Environmental Chemists# 2021-02309
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection Iimits arc listed as detection limits
for calculation purposes.

COASTAL FARMS & RESIDUALS,LLC
WQ0034806
Summerhouse
1111iiili11040111111!0411000-00iiITIIIIIIIIPCM1111;
02/10/21 10,834 4.0348
02/10/21 14,167 4.1513
02/10/21 2,899 3.4622
02/10/21 2,338 3.3688
02/10/21 12,500 4.0969
02/10/21 8,832 3.9461
02/10/21 2,466 3.3920
Total 26.4521
Average 3.7789
Geometric Mean €' Cr Q 111 Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B -Alternative 1 Pathogen for Reduction
requirement.

A, ONWASA Laboratory
wz. 228 Georgetown Road
Jacksonville NC 28540
KWc .SI- [phone]
March 04, 2021
Kary Herndon
Summer House WRF
Twining Rose Lane
Holly Ridge, NC 28445
RE: Summer House Sludge
Enclosed are the results of analyses for samples received by our laboratory on 2/10/2021. If you
have any questions concerning this report, please feel free to contact me.
Sincerely,
O WA + 1!,
Todd A. Roberts
Lab Administrator

A
ONWASA
Summer House WRF Project: Summer House Sludge
Twining Rose Lane Project Number: Reported:
Holly Ridge,NC 28445 Project Manager: Kary Herndon 03/04/2021 15:01
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: SH Fecal # 1 Q210704-01 (SL) 02/10/202108:18
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 10834 MPN/g 02/10/2021 SM 9221C E MPN
24hr 503
Total Solids(a/o) 0.72 rya 02/11/2021 SM 2540 G
Sample: SH Fecal # 2 Q210704-02(SL) 02/10/2021 08:19
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 14167 MPN/g 02/10/2021 SM 9221C E MPN
24hr 503
Total Solids(0/0) 0.48 % 02/11/2021 SM 2510 G
Sample: SH Fecal # 3 Q210704-03 (SL) 02/10/2021 08:20
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 2899 MPN/g 02/10/2021 SM 9221C E MPN
24hr 503
Total Solids(0/0) 0.69 o/u 02/11/2021 SM 2540 G
Sample: SH Fecal#4 Q210704-04 (SL) 02/10/2021 08:21
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density <2338 MPN/g 02/10/2021 SM 9221C E MPN
24hr 503
Total Solids("/o) 0,77 % 02/11/2021 SM 2540 G
Sample: SH Fecal# 5 Q210704-05 (SL) 02/10/2021 08:22
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 12500 MPN/g 02/10/2021 SM 9221C E MPN
24hr 503
Total Solids(a/o) 1.04 % 02/11/2021 SM 2540 G
The contents of this report apply to the sample(s)analyzed In accordance with the chain of custody document.
. Na duplication of this report 15 allowed,except In it;entirety. .Page 2 of 5

A
ONWASA
Summer House WRF Project: Summer House Sludge
Twining Rose Lane Project Number: Reported:
Holly Ridge,NC 28445 Project Manager: Katy Herndon 03/04/2021 15:01
Sample Results
(Continued)
Data Analyzed by:Environmental Chemists,Inc.
Sample: SH Fecal # 6 Q210704-06(SL) 02/10/2021 08:23
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 8832 MPN/g 02/10/2021 SM 9221C E MPN
24hr 503
Total Solids(A) 0.77 % 02/11/2021 SM 2540 G
Sample: SH Fecal # 7 Q210704-07(SL) 02/10/2021 08:24
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 2466 MPN/g 02/10/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 0.73 % 02/11/2021 SM 2540 G
Sample: SH Digestor Q210704-08 (SL) 02/10/2021 08:15
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Aluminum 1670 mg/Kg 02/18/2021 EPA 200.7
Ammonia-N 1510 mg/Kg 07./11/2021 SM 4500 NH3 C
Arsenic <31.6
- - mg/Kg 02/18/2021 EPA 200.7
Calcium 34000 mg/Kg 02/18/2021 EPA 200.7
Cadmium <31.6 mg/Kg 02/18/2021 EPA 200.7
Chromium <31.6 mg/Kg 02/18/2021 EPA 200.7
Copper 92.7
mg/Kg 02/18/2021 EPA 200.7
Mercury <2.39 mg/Kg 02/12/2021 5W846 7471B
Potassium 1540 mg/Kg 0 18 Z021 EPA 200.7
Magnesium 3290 mg/Kg 02/18/2021 EPA 200.7
Molybdenum <31.6 mg/Kg 02/18/2021 EPA 200.7
Sodium 9170 mg/Kg 02/18/2021 EPA 200.7
Nickel <31.6 mg/Kg 02/18/2021 EPA 240.7
Nitrate+Nitrite-Nitrogen 28.5 mg/Kg 02/18/2021 EPA 353.2
Lead <31.6
mg/Kg 02/18/2021 EPA 200.7
pH 6.84 pH Units 02/23/2021 SM 4500 H 8
Selenium <31.6
m91K9 02/18/2021 EPA 200.7
Total Kjeldahl Nitrogen 57800 mg/Kg 02/11/2021 EPA 351.2
Phosphorus,total Sludge 18200 mg/Kg 02/17/2021 SM 4500 P E
Total Solids(0/0) 0.7 % 02/11/2021 SM 2540 G
zinc 1540 mg/Kg 02/18/2021 EPA 200.7
The content of this report apply to the sample(s)analyzed in accordance with the drain of custody document
No duplicadon of this report is allowed,except In,ts entirety. Page 3 Of 5

ONWASA
Summer House WRF Project: Summer House Sludge
Twining Rose Lane Project Number: Reported:
Holly Ridge,NC 28445 Project Manager: Katy Herndon 03/04/2021 15:01
Notes and Definitions
Item Definition
Dry Sample results reported on a dry weight basis.
ND Analyte NOT DETECTED at or above the reporting limit.
The contents ofdris report apply to the sample(s)analyzed in accordance with the chain of custody document.
No duplication of this report is allowed,except in!ls entirety Page 4 of 5

r n Cq ' it11, iA Environmental Chemists, Inc,
•
a.•, -'- 6602 Windmill Way,Wilmington,NC 28405 910.392.0223 Lab 910.392. 24 Fax
'.t6- 1.4.-'.0 :`s 4,''' _.OPA 710 8owsertown Road,Manta),NC 27954 252.473.5702 Lab/Fax
'"te.. : ; ; • : �;'• 255-A Wilmington Highway,Jacksonville,NC 28540 ° 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(i!environmentalchemists.com
Onslow Water& Sewer Authority Date of Report: Feb 24, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Todd Roberts Report#: 2021-02309
Project ID: Summerhouse
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-05625 Site: Q21o7o4-01 2/10/2021 8:18 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 0.72% 02/11/2021
Fecal Density SM 9221C E MPN 24 hr503 10834 MPN/g 02/10/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-05626 Site: Q210704-02 2/10/2021 8:19 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) 5M 2540 G 0.48% 02/11/2021
Fecal Density SM 9221C E MPN 24 hr503 14167 MPN/g 02/10/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-05627 Site: Q210704-03 2/10/2021 8:20 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 0.69% 02/11/2021
Fecal Density SM 9221C E MPN 24 hr 503 2899 MPN/g 02/10/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-05628 Site: Q210704-04 2/10/2021 8:21 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 25440 G 0_77% 02/11/2021
Fecal Density SM 9221C E MPN 24 hr 503 <2338 MPN/g 02/10/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-05629 Site: Q210704-05 2/10/2021 8:22 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) 5M 2540 G 1.04% 02/11/2021
Fecal Density 5M 9221C E MPN 24 hr 603 12500 MPN/g 02/10/2021

w, Environmental Chemists,9 Inc.
a r l fl ''• ,s 1 6602 Windmill Way,Wilmington,NC 28405 ° 910.392.0223 Lab ° 910.392.4424 Fax
a t `• . :`;.,: �'_Ti'ti' � 710 Bowsertown NC 27954 • 252.473.5702 Lab/Fax
aid" t ,` , :� o n Road,Manteo,
�-"S ' i'7- - 255-A Highway,ton Hi
g g y,Jacksonville,NC 28540 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoa4environmentalchemists.com
Onslow Water& Sewer Authority Date of Report: Feb 24, 2021
228 Georgetown Road Customer PO#:
Jacksonville INC 28540 Customer ID: 08100092
Attention: Todd Roberts Report#: 2021-02309
Project ID: Summerhouse
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-05630 Site: 0210704-06 2/10/2021 8:23 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 0.77% 02/11/2021
Fecal Density SM 9221C E MPN 24 hr 503 8832 MPN/g 02/10/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-05631 Site: Q210704-07 2/10/2021 8:24 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Total Solids (%) SM 2540 G 0.73% 02/11/2021
Fecal Density SM 9221C E MPN 24 hr 503 2466 MPN/g 02/10/2021
-

r
Environmental Chemists, Inc.
i' 6602 Windmill Way,Wilmington,NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
t,e,, �sx ; ,. ,°"'{ht 710 Bowsertown Road,Manteo,NC 27954 r 252.473.5702 Lab/Fax
.sk 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5813 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Onslow Water& Sewer Authority Date of Report: Feb 24, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Todd Roberts Report#: 2021-02309
Project ID: Summerhouse
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-05632 Site: Q210704-08 2/10/2021 8:15 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200.7 1670 mg/kg 02/18/2021
Arsenic EPA 200.7 <31.6 mg/kg 02/18/2021
Cadmium EPA 200.7 <31.6 mg/kg 02/18/2021
Calcium EPA 200.7 34000 mg/kg 02/18/2021
Chromium EPA 200.7 <31.6 mg/kg 02/18/2021
Copper EPA 200.7 92.7 mg/kg 02/18/2021
Lead EPA 200.7 <31.6 mg/kg 02/18/2021
Magnesium EPA 200.7 3290 mg/kg 02/18/2021
Molybdenum EPA 200.7 <31.6 mg/kg 02/18/2021
Nickel EPA 200.7 <31.6 mg/kg 02/18/2021
Potassium EPA 200.7 1540 mg/kg 02/18/2021
Selenium EPA 200.7 <31.6 mg/kg 02/18/2021
Sodium EPA 200.7 9170 mg/kg 02/18/2021
Zinc EPA 200.7 1540 mg/kg 02/18/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 28.5 mg/kg 02/18/2021
Total Solids (%) SM 2540 6 0,70% 02/11/2021
pH SM 4500 H B 6.84 units 02/23/2021
Ammonia Nitrogen SM 4500 NH3 C 1510 mg/kg 02/11/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Org 3 57800 mg/kg 02/11/2021
Total Phosphorus SM 4500 P F 18200 mg/kg 02/17/2021
Mercury SW046 74716 <2.39 mg/kg 02/12/2021
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: '-----,y "e'`6,
Pnnnri H oml nvann

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: A3-toraer IUD IA SQ Date: 2kt C] 21 Report Number: 2 —Z3Q9
Receipt of sample: ECHEM Pickup Client Delivery 0 f uPs 0 FedEx 0 Other 0
❑ YES �❑ NO 10N/A 1. Were custody seats present on the cooler?
❑ YE5 ❑ NO ,1'* N/A 2. If custody seals were present, were they intact unbroken?
/
Original temperature upon receipt 2. 1 °C or ected temperature upon receipt °C
How temperature taken: 0 Temperature Blank Against Bottles
1R Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor°C: 0.0
'ld YES 0 NO 3_ if temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES 0 NO 4. Were proper custody procedures (relinquished/received) followed?
11171 YES 0 NO 5. Were sample ID's fisted on the COC?
rt YES 0 NO 6. Were samples iD's listed on sample containers?
►4 YES 0 NO 7. Were collection date and time listed on the COC?
74 YES 0 NO 8. Were tests to be performed listed on the COC?
51 YES 0 NO 9. Did samples arrive in proper containers for each test?
Pa YES 0 NO 10. Did samples arrive in good condition for each test?
YES 0 NO 11. Was adequate sample volume available?'
x. YES 0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
D YES 0 NO 14. Were cyanide samples received at a pH >12?
❑ YES 0 NO 15. Were sulfide samples received at a pH>9?
0 YES 0 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked far Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2504 HNO3 HO NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified,date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

Onslow Water&Sewer Authority SUBCONTRACT
7 228 Georgetown Road
ONWAJacksonville NC 28540 ORDER
SA
Sending Facility: Subcontracted Laboratory:
Summer House WRF
Twining Rose Lane A 9i < <i
Holly Ridge, NC 28445
Phone: [phone] Environmental Chemists,Inc.
6602 Windmill Way
Wilmington,NC 28405
Project Manager: Todd A. Roberts Phone: [phone] Fax:[phone]
NCDEHR:DWQ CERTIFICATION M 94 NCBHHS€BLS CERTIFICATION A 37729
Work Order: Q210704 Summer House WRF
Sample ID:Q210704-01 SH Fecal#1 SL Sampled: 02/10/2021 08:18 Sampled by:tearvHerndart
I Analysis Due Expires EnviroChem Lab ID I
Fecal Density 02/20/2021 02/10/2021 14:1B C5;62S
I Analysis Due Expires EnviroChem Lab ID I
Total Solids(%) 02/20/2021 02/17/2021 06:18 0 5(11-5
Containers Supplied:
120 Sterile Na2S2O3(A)
Sample ID:Q210704-02 SH Fecal#2 SL Sampled: 02/10/2021 08:19 Sampled by:Karr Herndon
Analysis Due Expires EnviroChem Lab ID 1
Fecal Density 02/20/2021 02/10/2021 14:19 cicb Z6
Analysis Due Expires EnviroChem Lab ID
Total Solids(%) 02/20/2021 02/17/2021 08:19 Ct,6 2 6
Containers supplied:
124 Sterile NaZ$203(A)
Sample ID:Q210704-03 SH Fecal#3 SL Sampled: 02/10/2021 08:20 Sampled by::Nary Herpdon
Analysis Due Expires EnviroChem Lab ID I
Fecal Density 02/20/2021 02/10/2021 14:20 OSb7
I Analysis Due Expires EnviroChem Lab ID
Total Solids(%) 02/20/2021 02/17/2021 08:20 s]5627
Containers Supplied:
120 Sterile Na2S203(A)
Sample ID:Q210704-04 SH Fecal#4 SL Sampled:: 02/10/2021 08:21 Sampled by:J(arvHerndon
Analysis Due Expires EnviroChem Lab ID 1
Fecal Density 02/20/2021 02/10/2021 14:21 a 5 6Z 9
Analysis Due Expires EnviroChem Lab ID
Total Solids(%) 02/20/2021 02/17/2021 08:21 _ U567-Y
Containers Supplied:
120 Sterile Na2S203(A)
Sample ID:Q210704-05 SH Fecal#5 SL Sampled: 02/10/2021 08:22 Sampled by:Katy Herndon
EnviroChem Report No: 2} �23 9
e, , i0,.._
-J A & a O//2�z/ T•'1/ jG—l____ f%"� _—.�. Z.-( -z 0 I :5�
Relinquished By Date Received By Date
Page 1 of 3

.... .
��
4
Onslow Water&Sewer Authority SUBCONTRACT
,—._ 228 Georgetown Road
Jacksonville NC 28540 ORDER
(Continued)
Work Order: Q210704 (Continued) Summer House WRF
Sample ID:Q210704-05 SH Fecal#S SL Sampled: 02/10/2021 08:22 Sampled by:Kary Herndon
LAnalysis Due Expires EnviroChem Lab ID I
Fecal Density 02/20/2021 02/10/2021 14:22 p 5 b4-t I
Analysis Due Expires EnviroChem Lab ID I
Total Solids(%) 02/20/2021 02/17/2021 08:22 0;hcl 1
Containers Supplied:
120 Sterile Na25203(A)
Sample ID:Q210704-06 SH Fecal#6 SL Sampled: 02/10/2021 08:23 Sampled 6y:Pry Herndon
fAnalysts Due Expires EnviroChem Lab ID
Fecal Density 02/20/2021 02/10/2021 14:23 f15630
IAnalysis Due Expires EnviroChem Lab ID
Total Solids(%) 02/20/2021 02/17/2021 08:23 U'bSO
Containers Supplied:
120 Sterile Na25203(A)
Sample ID:Q210704-07 SH Fecal#7 SL Sampled: 02/10/2021 08:24 Sampled by:pry lierndo0
Analysis Due Expires EnviroChom Lab ID f
Fecaf Density 02/20/2021 02/10/2021 14:24 n 5.63 t
Analysis Due Expires EnviroChem Lab ID
Total Solids(%) 02/20/2021 02/17/2021 08:24 OS GS'
Containers Supplied:
120 Sterile Na2S203(A)
Sample ID:Q210704-08 SH Digester Si. Sampled: 02/10/2021 08:15 Sampled by:Kary Herndon
Analysis Due Expires EnviroChem Lab ID f
Cd 200.7 02/20/2021 02/10/2021 08:15 056,37.-
Analysis Due Expires EnviroChem Lab ID
Al 200.7 02/20/2021 02/10/2021 08:15 1I 5r53-
Analysis Due Expires EnviroChem Lab ID
Na 200.7 02/20/2021 02/10/2021 08:15 a C,637..,
Analysis Due Expires EnviroChem Lab ID
As 200.7 02/20/2021 02/10/2021 08:15 6�(33Z
Analysis Due Expires EnviroChem Lab ID
Ni 200.7 02/20/2021 02/10/2021 08:15 _ esS 6 31
Analysis Due Expires EnvlraChem Lab ID
Ca 200.7 02/20/2021 02/10/2021 08:15 0 S632
Analysis Due Expires EnviroChem Lab ID
Mo 200.7 02/20/2021 02/10/2021 08;15 C -52.
Analysis Due Expires EnviroChem Lab ID
Mg 200.7 02/20/2021 02/10/2021 08:15 OSA :7-0
Analysis Due Expires EnviroChem Lab ID
K 200.7 02/20/2021 02/10/2021 08:15 (7 S b 3 L
EnviroChem Report Na: r- \ - 0 \
Tr,/A. 4 Lv7 24/ ,, 9.z z 10-�1 �j
Relinquished By Date �l.`� ��' "
Received By Date
Page 2 of 3

Onslow Water&Sewer Authority SUBCONTRACT
228 Georgetown Road
ON
Jacksonville NC 28540 ORDER WASA (Continued)
Work Order: Q210704 (Continued) Summer House WRF
Sample ID:Q210704-08 SH Digester SL Sampled: 02/10/2021 05:15 Sampled by:Karygerrrdon
Analysis Due Expires EnvlroChem Lab ID r
Hg 5W846 7471E 02/20/2021 02/10/2021 08:15 ()54,32 1
Analysis Due Expires EnviroChem Lab ID
pH 02/20/2021 02/10/2021 08:32 0.5.6 3Z
Analysis Due Expires EnviroChem Lab ID
Total Solids(%) 02/20/2021 02/17/2021 08:15 O. 6 Z
Analysis Due Expires EnviroChem Lab ID
Se 200.7 02/20/2021 02/24/2021 08:15 OS 6s2..
Analysis Due Expires EnviroChem Lab ID
Zn 200.7 02/20/2021 02/24/2021 08:15 05 62,
Analysis Due Expires EnviroChem Lab ID
Ammonia Nitrogen 02/20/2021 03/10/2021 08:15 e 5{02 _
I Analysis Due Expires EnviroChem Lab ID
Total Phosphorus 02/20/2021 03/10/2021 08:15 f7`✓b' 7.
Analysis Due Expires EnviroChem Lab ID
Total K)eldahl Nitrogen(TKN) 02/20/2021 03/10/2021 08:15 0�6s L
I Analysis Due Expires EnvlroChem Lab ID
Nitrate+Nitrite-Nitrogen 02/20/2021 03/10/2021 08:15 656?a�
Analysis Due Expires EnviroChem Lab ID
Pb 200.7 02/20/2021 08/09/2021 08:15 (356 SL
Analysis Due Expires EnvlroChem Lab ID
Cu 200.7 02/20/2021 08/09/2021 08:15 n5637.- _
Analysis Due Expires EnvlroChem Lab ID
Cr 200.7 02/20/2021 08/09/2021 08:15 05632 _
Containers Supplied:
P 1 liter(A) P I liter(a)
EnviroChem Report No: 1 —t-2- t a - t ° c-
Relinquished By Date Received By Date
Page 3 of 3

't�4r3�+.r k En _
irinmental Chemists, Inc. .
r � x
�� v�.�,,". �f e ;f< 6642 Windmill Way,Wilmington,NC 28405 • 914.392.0223 Lab • 910.392.4424 Fax
, _,*!'`'" �x a 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
p.lit, 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5643 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(4•environmentalchemists.com
Onslow Water&Sewer Authority Date of Report: Jul 20, 2021
228 Georgetown Road Customer PO #:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Todd Roberts Report#: 2021-10651
Project ID: Summer House WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-26545 Site: SH Digestor 6/29/2021 7:23 AM Solid/Sludge Kary Herndon
Test Method Results Date Analyzed
Chlordane (TCLP) SW 848 Method 8081 B/3510 <0.02 mg/L 07/09/2021
Endrin (TCLP) SW 846 Method 80818/3510 <0,0005 mg/L 07/09/2021
Heptachlor(TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 07/09/2021
Heptachlor epoxide(TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 07/09/2021
Lindane (TCLP) SW 846 Method 80818/3510 <0.0005 mglL 07/09/2021
Methoxychior(TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 07109/2021
Toxaphene(TCLP) SW 846 Method 13081B/3510 <0.05 mg/L 07/09/2021
1,4-Dichlorobenzene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
2,4,5-Trichlorophenol (TCLP) SW 646 method 8270/3510 <0.050 mg/L 07/08/2021
2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
Cresol(TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
Hexachloro-1,3-butadiene(TCLP) SW B46 method 8270/3510 <0.050 mg/L 07/08/2021
Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
Hexachioroethane(TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
m +p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
o-Cresol (TCLP) SW 046 method 8270/3510 <0.050 mglL 07/08/2021
Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 07/08/2021
Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mglL 07/08/2021
2,4,5-TP (TCLP) 5W846 Method 8151A <0.003 mg/L 07/13/2021
2,4-D (TCLP) SW846 Method 8151A <0,003 mg/L 07/13/2021
1,1-Dichloroetliylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
1,2-Dichioroethane (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
Benzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
Carbon Tetrachloride(TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
Report#:: 2021-10651
Page 1 of 2 .

=�v ` g _ Environmental Chemist Inc.
,,r� Y-,F,6 —14ty 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
" ` , ' 710 8owsertawn Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
' rat -'.sM,
{� '� �.';,`r 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info(ivenvironmentalchemists.com
Onslow Water& Sewer Authority Date of Report: Jul 20, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Todd Roberts Report#: 2021-10651
Project ID: Summer House WRF
Chlorobenzene(TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
Methyl ethyl ketone(TCLP) SW846 Method 8260/5030 <0.05 mg/L 07/02/2021
Tetrachloroethylene (TCLP) 5W846 Method 8260/5030 <0.01 mg/L 07/02/2021
Trichloroethylene (TCLP) 5W846 Method 8260/5030 <0.01 mg/L 07/02/2021
Vinyl Chloride(TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
RCI
Cyanide SM 4500 CN 0 <1 mg/kg 07/07/2021
Reporting limit elevated due to matrix interference.
Sulfide SM 4500 S 0 0.15 mg/kg 07/06/2021
Ignitability SW 846 method 1010 >200°F 07/20/2021
pH SW 846 Method 90450 6.33 units 06/30/2021
Result estimated. Analyzed out of 15 minutes hold time.
TCLP Metals
Arsenic EPA 200.7 <1.0 mg/L 07/09/2021
Barium EPA 200.7 <1.0 mg/L 07/09/2021
Cadmium EPA 200.7 <1.0 mg/L 07/09/2021
Chromium EPA 200.7 <1.0 mg/L 07/09/2021
Lead EPA 200.7 <1.0 mg/L 07/09/2021
Selenium EPA 200.7 <1.0 mg/L 07/09/2021
Silver EPA 200.7 <1.0 mg/L 07/09/2021
Mercury EPA 245.1 <0.0002 mg/L 07/14/2021
Comment: pil
t
Reviewed by; katetdr� VAZPAra,..)
Report#:: 2021-10651
Page2of2

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington NC 28405
910.392.0223
Sample Receipt Checklist
Client: ���� I ii
Date: 129 7-1 Report Number: 2 i --» J 1
Receipt of sample: E HEM Pickup V Client Delivery❑ UPS ❑ FedEx ❑ Other ❑
❑ YES f❑ NO I N/A 1. Were custody seats presentres ent onav the cooler?
❑ YES f JI❑ NOO N/A 2. !f custadyseals were
Original temperature upon receipt �, p ere they intact/unbroken?
p 1 °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank X Against Bottles
IR Gun ID: Thomas Traceable 5/N 192511657 lR Gun Correction Factor'Cr 0.0
YES ❑ NO 3. ff temperature of cooler exceeded 6°C, was Project Mgr,/QA notified?
YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed?
g. YES ❑ NO 5. Were sample ID's listed on the COC?
YES ❑ NO 6. Were samples JD's listed on sample containers?
gi YES ❑ NO 7. Were collection date and time listed on the ?
YES ❑ NO COC.
8. Were tests to be performed listed on the COC?
YES ❑ NO 9. Did samples arrive in proper containers for each test?
l YES 0 NO 10. Did samples arrive in good condition for each test?
vCC i r-i r,n .. ,
;. ) __ •,�.. 1...,.�y..cft.. ,),. .N,L V4iu:IL_(“aiIPWC:
YES 0 NO 12. Were samples received within proper holding time for requested tests?
It
❑ YES ❑ NO 13. Were add preserved samples received at a pH of<2? *
❑ YES ❑ NO 14. Were cyanide samples received at a pH >12?
❑ YES 10 NO 15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO 1b. Were NH3/T KN/Phenol received at a chlorine residual of<0,5 m/L.
❑ YES ❑ NO ? y
17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L? }
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the fie.fd within 15 minutes?
* TJC/Votatiles are H the pchecked at fin«. of analysis and recorded on the benchsheet
"" Bacteria samples checked'p es a -cn=_-,;_d fo CnIarl 1e a: t me or a9a,ys,s and recorded on the b; : :9 tea.
;Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
.Sample(s) were received incorrectly preserved and were adjusted a_cordingiy
by adding (circle one): H.SO.: HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
ND'-=_:,tia,::r:.s'amer s-?^;;_=_ imm�j,rF.:y;o-,-=o;r _tiyDras='•redsan•oes re _ g Oc:a,n a :r s� 5_
-i 7 rye sa: :a If d. to-=_r Tp
c �'-_' of C.,c Cil5:0Me . 4+,ca....as nom,ed o?•e and tIrne: -
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev I

Onslow Water&Sewer Authority SUBCONTRACT
228 Georgetown Road
Jacksonville NC 28540 ORDER
N ASA
Sending Facility: Subcontracted Laboratory:
Summer House WRF
Twining Rose Lane ei ;I +.:,-.±
Holly Ridge, NC 28445
Phone: [phone] Environmental Chemists,Inc.
6602 Windmill Way
Wilmington,NC 28405
Project Manager: Kary Herndon Phone:[phone] Fax: [phone]
NCDENR:DWQ CERTIFICATION k 94 NCONNS:DLS CERTIFICATION X 37129
Work Order: Q212701 Summer House WRF
Sample ID:Q212701-01 SH Dlgestor St Sampled: 06/29/2021 07:23 Sampled by:Kary Herndon
Analysis Due Expires EnviroChem Lab ID J
pH,5W846 07/09/2021 06/29/2021 07:90
f Analysis Due Expires EnviroChem Lab ID I
Sulfide colorlmetric 07/09/2021 07/13/2021 07:23 1
I Analysis Due Expires EnviroChem Lab ID I
Cn-335.4 07/09/2021 07/13/2021 07:23
[Analysis Due Expires EnviroChem Lab ID i
SW 846 Mtd 8270/3510 07/09/2021 07/27/2021 07:23 I
IAnalysis Due Expires
5W 846 80816/3510 EnviroChem Lab ID
07/09/2021 07/27/2021 07:23
I Analysis Due Expires EnviroChem Lab ID r
Ignitability 1030 07/09/2021 07/27/2021 07:23
IAnalysis Due Expires I
Hg 245.1 P EnviroChem Lab ID
07/09/2021 07/27/2021 07:23
Analysis Due Expires
Ex i
TCLP Metals p EnviroChem Lab ID
07/09/2021 12/26/2021 07:23
I Analysis Due Expires p EnviroChem Lab ID
5W846 6260/5030
07/09/2021 12J26J2021 07:23
Analysis Due Expires
5W846 8151A EnviroChem Lab ID
07/09/2021 12/26/2021 07:23
Containers Supplied.'
P 1 liter(A) AG IL(B) AG 11(C) AG 1L(0)
EnviroChem Report No: .� 16"
.---c,a 4, 4,4 othoa, ,,,,
D()
Relinquished By Date ,;, cp\x-i\21l�
R eived By Date
Page 1of1 2 , I. Utz

•
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: Coastal Farms and Residuals,LLC WQ Permit Number: WQ0034806
WWTP Name: Summerhouse WWTP NPDES Number: WQ0029945
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106)-Please indicate level achieved and alternative performed:
Class A: ^ Alt. A(time/temp) ❑ J Alt B (AIk Treatment)❑ Alt. C (Prior Testing)❑
AIt.D(No Prior Test) 0 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophiiic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alt. (1)Fecal Density 0 Alt. (2)Process to Siga.iticantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate"Process to Significantly Reduce Pathogens' :
Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑
•
Anaerobic
zr erobic Digestion'
ron
g l
applicableIf to alternative performed (Class A or'Class B)complete the following monitoring data:,
Allowable Level PathogenDensityNumber of Analytical
Parameter - Excee- Frequency Sample Tech-
in Sludge Minimum Geo. Mean Maximum Units deuces of Analysis Type
ninue
2 x 10 to the MPN 2,338 6,010 14,167 MPN/g 0 Annual Grab SM9221Cfi
6th power
per gram of
Fecal Coliform total solids CFU
1 000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T.1107)-Please indicate alternative performed:
Alt.1 (VS reduction) 0 Alt.2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt.4 (Spec.02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6(Alk. Stabilization 0 Alt 7(Drying-Stable) Cl Alt. 8(Drying-Unstable) ❑
Alt. 9(Injection) 0 Alt. 10 (Incorporation) 0 No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT(please check the appropriate statement)
CI "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
❑ "I certify, under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kary Herndon,ORC Wesley Wooten, President
Preparer Name and Ti le e or_print) Land Applier Name and Title(if applicable)(type or print)
a/ er 3/8/21
rep Date Signature of Lan Applier(if applicable) Date

COASTAL RESIDUALS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: October 28,2021
Surf City WWTP Permit No.WQ0000795
2.14 %Solids
7.00 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 5.380 53,800.000 107.600
Phosphorus 2.240 22,400.000 44.800
Potassium 0.405 4,050.000 8.100
PAN(injected)* 1.700 17,000.600 34.001
PAN(surface)* 1.640 16,400.600 32.801
Ammonia Nitrogen 0.120 1,200.000 2.400
Calcium 0.004 _ 41.400 0.083
Calcium Carbonate Eq. _ --- _ --- --
Magnesium --- 3,530.000 7.060
Sodium --- 8,880.000 17.760
Sulfur --- --- ---
Nitrate N/Nitrite N --- 20.600 0.041
Barium --- --- SAR
Chloride --- --- --- 4.64
Iron --- --- --- Ceiling Con cen.
Aluminum --- 3,340.00 6.680 , (Mg/Kg)
Arsenic --- 30.70 0.061 75
Cadmium --- 30.70 0.061 I. 85 _
Chromium --- 30.700 0.061 -
Copper _ --- 394.00 0.788 4,300
Lead --- 30.70 0.061 840
Mercury --- 0.752 0.002 57
Molybdenum --- 30.70 0.061 75
Nickel --- 30.70 0.061 420
Selenium --- 30.70_ 0.061 100
Zinc --- 3,450.00 6.900 7,500
Environmental Chemists# 202I-19026
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits arc listed as detection limits
for calculation purposes.

LEWIS FARMS
WQ0000455
Surf City WWTP
iato€ 111oiol'�
10/28/21 1,461 3.1647
10/28/21 3,334 3.5230
10/28/21 1,051 3.0216
I0/28/21 1,467 3.1664
10/28/21 1,423 3.1532
10/28/21 2,051 3.3120
10/28/21 1,435 3.1569
Total 22.4977
Average 3.2140
Geometric Mean iiii1111111 Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B -Alternative 1 Pathogen Reduction
requirement.

Environmental Chemists, Inc.
'r` �t, 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
enviroc em.�� y g •
c4Rx ,•5 ���5} 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
---:;•" '" :::, 5,;,;x, z".'€ 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info r@i environmentalchemists.com
Town of Surf City Date of Report: Nov 19, 2021
Post Office Box 2475 Customer PO#:
Surf City NC 28445 Customer ID: 08110024
Attention: Arthur Mark Report#: 2021-19026
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-47626 Site:Sludge 10/28/2021 7:00 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Chlordane (TCLP) SW-846 8081 B <0.02 mg/L 11/05/2021
Endrin (TCLP) SW-848 8081 B <0.0005 mg/L 11/05/2021
Heptachlor(TCLP) SW-846 8081 B <0.0005 mg/L 11/05/2021
Heptachlor epoxide(TCLP) SW-646 8081 B <0.0005 mg/L 11/05/2021
Lindane (TCLP) SW-845 8081 B <0.0005 mglL 11/05/2021
Methoxychior(TCLP) SW-846 0081 B <0.0005 mg/L 11/05/2021
Toxaphene(TCLP) SW-846 8081 B <0.05 mg/L 11/05/2021
2,4,5-TP (TCLP) SW-846 8151 A <0.003 mg/L 11/10/2021
2,4-D(TCLP) SW-846 8151 A <0.003 mg/L 11/10/2021
1,4-Dichlorobenzene (TCLP) SW-8466270E <0.050 mg/L 11/04/2021
2,4,5-Trichlorophenol (TCLP) SW-846 8270E <0.050 mglL 11/04/2021
2,4,5-Trichlorophenol (TCLP) SW-846 8270 E <0.050 mg/L 11/04/2021
2,4-Dinitrotoluene (TCLP) SW-846 8270E <0.050 mglL 11/04/2021
Cresol (TCLP) sw-846 8270 E <0.050 mg/L 11/04/2021
Hexachioro-1,3-butadiene (TCLP) SW-846 8270 E <0.050 mg/L 11/04/2021
Hexachlorobenzene (TCLP) SW-846 8270 E <0.050 mg/L 11/04/2021
Hexachloroethane (TCLP) SW-846 8270E <0.050 mg/L 11/04/2021
m + p-Cresol (TCLP) SW-846 8270E <0.050 mg/L 11/04/2021
Nitrobenzene (TCLP) sW-848 8270 E <0.050 mg/L 11/04/2021
o-Cresol (TCLP) SW-846 8270 E <0.050 mg/L 11/04/2021
Pentachiorophenol (TCLP) SW-846 8270 E <0.250 mglL 11/04/2021
Pyridine (TCLP) SW-846 8270 E <0.050 mg/L 11/04/2021
1,1-Dich loroethylene (TCLP) SW-846 Method 8260D <0.01 mg/L 11/02/2021
1,2-Dichloroethane (TCLP) SW-846 Method 8260D <0.01 mg/L 11/02/2021
Benzene(TCLP) SW-846 Method 6260D <0,01 mg/L 11/02/2021
Carbon Tetrachloride (TCLP) SW-846 Method 8260D <0.01 mg/L 11/02/2021
Report#;: 2021-19026 „---,

�a ,_ Environmental Chemists, Inc.
envlrochem ,.' 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
"G 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
' u; F 1 M, 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347,5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
environmentalchemists.com
Town of Surf City Date of Report: Nov 19, 2021
Post Office Box 2475 Customer PO#:
Surf City NC 28445 Customer ID: 08110024
Attention: Arthur Mark Report#: 2021-19026
Project ID: Sludge
Chlorobenzene (TCLP) SW-846 Method 8260D <0.01 mg/L 11/02/2021
Chloroform (TCLP) SW-846 Method 8260D <0.01 mg/L 11/02/2021
Methyl ethyl ketone (TCLP) SW-846 Method 8260D <0.05 mg/L 11/02/2021
Tetrachloroethylene (TCLP) SW-846 Method 8260D <0.01 mg/L 11/02/2021
Trichloroethylene(TCLP) SW-846 Method 8260D <0.01 mg/L 11/02/2021
Vinyl Chloride(TCLP) SW-846 Method 8260D <0.01 mg/L 11/02/2021
RCI
Cyanide SM 4500 CN D 1.84 mg/kg 11/08/2021
Sulfide SM 4500 S D 0.72 mg/kg 11/09/2021
Ignitability SW 846 method 1010 >195°F 11/02/2021
Sludge Residuals
Arsenic EPA 200.7 <30.7 mg/kg 10/28/2021
Cadmium EPA 200.7 <30.7 mg/kg 10/28/2021
Calcium EPA 200.7 41.4 mg/kg 10/28/2021
Copper EPA 200.7 394 mg/kg 10/28/2021
Lead EPA 200.7 <30.7 mg/kg 10/28/2021
Magnesium EPA 200.7 3530 mg/kg 10/28/2021
Molybdenum EPA 200.7 <30.7 mg/kg 10/28/2021
Nickel EPA 200.7 <30.7 mg/kg 10/28/2021
Potassium EPA 200.7 4050 mg/kg 10/28/2021
Selenium EPA200.7 <30.7 mg/kg 10/28/2021
Sodium EPA 200.7 8880 mg/kg 10/28/2021
Zinc EPA 200.7 3450 mg/kg 10/28/2021
Aluminum EPA 200.7,Rev.4.4,1994 3340 mg/kg 11/03/2021
Chromium EPA 200.7,Rev.4.4,1994 <30.7 mg/kg 10/28/2021
Nitrate+Nitrite-Nitrogen EPA 353,2 20.6 mg/kg 10/29/2021
Total Solids (%) 5M 2540 B 2.14% 10/28/2021
Ammonia Nitrogen SM 4500 NH3 C-2011 1200 mg/kg 10/29/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg 8-2011 53800 mg/kg 10/29/2021
Total Phosphorus SM 4500 P F-2011 22400 mg/kg 11/02/2021
•
Report#:' 2021-19026 .

Environmental Chemists, Inc.
..envlroche ni 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
11 j} Eli r? 'fsrs 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
+=F 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Town of Surf City Date of Report: Nov 19, 2021
Post Office Box 2475 Customer PO#:
Surf City NC 28445 Customer ID: 08110024
Attention: Arthur Mark Report#: 2021-19026
Project ID: Sludge
pH SW B46 Method 90450 7.00 units 11/08/2021
Result estimated. Analyzed out of 15 minutes hold time.
Mercury SW-846 7471 B <0.752 mg/kg 10/28/2021
TCLP Metals
Arsenic EPA200.7,Rev,4.4,1994 <1.0 mg/L 11/08/2021
Barium EPA 200.7,Rev.4.4,1994 <1.0 mg/L 11/08/2021
Cadmium EPA 200.7,Rev.4.4.1994 <1.0 mg/L 11/08/2021
Chromium EPA 200.7,Rev.4.4,1994 <1.0 mg/L 11/08/2021
Lead EPA 200.7,Rev.4.4,1994 <1.0 mg/L 11/08/2021
Selenium EPA 200.7,Rev.4.4,1994 <1.0 mg/L 11/08/2021
Silver EPA200.7,Rev.4.4,1994 <1.0 mg/L 11/08/2021
Mercury EPA 245.1 <0.0002 mg/L 11/05/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-47627 Site: 1 10/28/2021 7:01 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.26% 10/28/2021
Fecal Density SM 9221C E-2014 1461 MPN/g 10/28/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-47628 Site:2 10/28/2021 7:02 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.37% 10/28/2021
Fecal Density 5M 9221C E-2014 3334 MPN/g 10/28/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-47629 Site: 3 10/28/2021 7:03 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.19% 10/28/2021
Fecal Density SM 9221C E-2014 1051 MPN/g 10/28/2021
Report#:: 2021-19026 • .
Pan!.3 Of 4

Environmental Chemists, Inc.
t. envlroche m y' 6602 Windmill Way,Wilmington,NC 28405 • 910 392.0223 Lab • 910.392.4424 Fax
�. " E, - =-, 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
M, 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
� by S f 5 •...
ANALYTICAL&CONSULTING CHEMISTS info@cnvironmentalchemists,com
Town of Surf City Date of Report: Nov 19, 2021
Post Office Box 2475 Customer PO#:
Surf City NC 28445 Customer ID: 08110024
Attention. Arthur Mark Report#: 2021-19026
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-47630 Site: 4 10/28/2021 7:04 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.25% 10/28/2021
Fecal Density SM 9221C E-2014 1467 MPN/g 10/28/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-47631 Site: 5 10/28/2021 7:05 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.18% 10/28/2021
Fecal Density SM 9221C E-2014 1423 MPN/g 10/28/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-47632 Site: 6 10/28/2021 7:06 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 254013 2.39% 10/28/2021
Fecal Density SM 9221C E-2014 2051 MPN/g 10/28/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-47633 Site: 7 10/28/2021 7:07 AM Solid/Sludge Lewis Farms
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.30% 10/28/2021
Fecal Density SM 9221C E•2014 1435 MPN/g 10/28/2021
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: t -A-a-fig
Report#:: 2021-19026

Environmental Chemist, Inc., Wilmington, NC Lab 1194
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:V, IS /1/451-A-12-F ` Date/D on �i Report Number: r
Receipt of sample: ECHEM Pickup ❑ Client Delivery [UPS ❑ FedEx 0 Other ❑
❑ YES ❑ NO N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO N/A 2. If seals were
custody present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank lIZ Against Bottles
IR Gun ID:Thomas Traceable 5/N 192511657 IR Gun Correction Factor°C:0.0
❑ YES ❑ NO 3. If temperature of cooler exceeded 6°C,was Project Mgr./QA notified?
' YES 0 NO 4. Were proper custody procedures (relinquished/received)followed?
YES 0 NO 5. Were sample ID's listed on the COC?
EX YES ❑ NO 6. Were samples ID's listed on sample containers?
YES ❑ NO 7. Were collection date and time listed on the COC?
YES 0 NO 8. Were tests to be performed listed on the COC?
YES ❑ NO 9. Did samples arrive in proper containers for each test?
YES ❑ NO 10. Did samples arrive in good condition for each test?
'ES ❑ NO 11. Was adequate sample volume available?'
I YES 0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH >12?
0 YES 0 NO 15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 rn/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s) - were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

.A:"va',,Z:1:::=: ! ll Way
ENVIRONMENTAL CHEMISTS, INC OFFICE'"s O'392-02231FAX91Q392-44246
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDI•IHS:DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
•Client: Lewis Farms & Liquid Waste PROJECT NAME: ce../% C:ic REPORT NO: 2..a t- / - "o 2
ADDRESS: CONTACT NAME: Wesley Wooten PO NO:
REPORT TO: Martin MabelMabe-Wilcox PHONE/FAX:
COPY TO: email:
Sampled By: L<<.,'" 14✓.- S SAMPLE TYPE: I=Influent, E=Effluent,W=Well,ST=Stream, SO=Soil,SL=Sludge,Other:
Collection - PRESERVATION
Sample Identification E o. c 2 `� g m
cn r- c ° ca o a .� E m a z r) o 0 o 0 ANALYSIS REQUESTED
Date Time Temp c� u " " z z = i z o
l-t+lbr C P
Sludge G G 604.1, X Full TCLP, RCI, Nutrients/Metals
e...i C P
1 G G 140-- X Fecal Density/%TS
r C P
2 +y G G 14- X Fecal Density/%TS
C P
3 G G - M O X Fecal Density/%TS
4 � -
G G VLP
X Fecal Density/%TS
'',r C P
5 G G IWO X Fecal Density/%TS
C P
6 a� G GLOC X Fecal Density/%TS
7 053
G G
X Fecal Density)%TS
Transfer Relinquished By: Date/Time Received By: Date/Time
1.
2. —
Temperature when Received: .S Accepted: Rejected: Resample R u ted:
Delivered By: ( (A i.y. -. Received By: J (1 Date: t �/ Time: �'�
Comments T N ROUND:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: Coastal Farms and Residuals,LLC WQ Permit Number:_ WQ0034806
WWTP Name: Surf City WWTP NPDES Number: WQ0000795
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A: Alt.A(time/temp) ❑ Alt B (Alk Treatment)❑ , Alt. C (Prior Testing)❑
Alt.D(No Prior Test) ❑ Process to Further Reduce Pathogengs ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray 0 Gamma Ray 0 Pasteurization ❑ ..................................................
Class B: (Alt. (1)Fecal Density p 1 Alt. (2)Process to Significantly Reduce Pathogens ❑.. .,
If applicable to alternative performed (Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ I Air Drying 0 Composting 0 Aerobic Digestion 0
Anaer
obic
Digestion
ton
If applicable to alternative performed (Class A or Class B)complete the following monitoring data:
Allowable Level Pathogen DensityNumber of Analytical
Parameter Sludge gExcee- Frequency Sample Tech-
ing Minimum Geo. Mean Maximum Units dences of Analysis Type niotie
2 x 10 to the MPN 1,051 1,637 3,334 MPN/g 0 Annual Grab 3M922ICE
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
conform) weight)
Vector Attraction Reduction (1SA NCAC 02T .1107)-Please indicate alternative performed:
Alt.I (VS reduction) 0 Alt.2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt.4 (Spec.0:uptake) ❑
Alt.5 (14-Day Aerobic) El Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying-Stable) ❑ Alt. 8(Drying-Unstable) ❑
Alt. 9(Injection) p Alt. 10(Incorporation) a_No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT(please check the appropriate statement)
0 "I certify,under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
0 "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
.significant penalties for false certification including fine and imprisonment."
Zachary Butler,ORC Wesley Wooten,President
Preparer Name and Title(type or print) Land Applier Name and Title(if applicable)(type or print)
9 � 11/29/21
� 11/29/21
Sig/tire ature of P parer* Date Signature
gn tune of Land Ap ter(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102 (26)

COASTAL FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 24,2021
Swansboro Permit No.WQ0034806
2.74 %Solids
7.36 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) _ 5.600 56,000.000 112.000
Phosphorus 2.240 22,400.000 44.800
Potassium 0.304 3,040.000 6.080
PAN(injected)* 1,975 19,753.600 _ 39.507
PAN(surface)* 1.771 17,708.600 35.417
Ammonia Nitrogen 0.409 4,090.000 8.180
Calcium 3.210 32,100.000 64.200
Calcium Carbonate Eq. --- --- ___
-
Magnesium --- _ 1,670.000 3.340
Sodium --- 3,160.000 - 6.320
Sulfur --_ --- ---
Nitrate N/Nitrite N --- 90.600 0.181
Barium --- --- --- SAR
Chloride --- _ --- --- _ 3.81
Iron --- --- --- Ceiling Concen.
Aluminum --- 3,370.00 6.740 (Mg/Kg)
Arsenic --- 36.40 0.073 75
Cadmium --- 18.20 0.036 _ 85
Chromium --- 18.200 --- _-
Copper --- 228.00 0.456 4,300
Lead --- 18.20 0.036 840
Mercury _ --- 0.608 0.001 57
Molybdenum --- 18.20 _ 0.036_ 75
Nickel --- 18.20 0.036 420
Selenium --- 18.20 0.036_ 100
Zinc --- 3,720.00 7.440 7,500
Environmental Chemists# 2021-04853
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Swansboro WRF
..............:...affix ; .....;:_,,:Ptg:::::_:;:::;:
03/24/21 87,592 4.9425
03/24/21 62,500 4.7959
03/24/21 85,715 4.9331
03/24/21 48,690 4.6874
03/24/21 80,000 4.9031
03/24/21 16,313 4.2125
03/24/21 47,971 4.6810
Total 33.1554
Average 4.7365
Geometric Mean Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B -Alternative 1 Pathogen Reduction
requirement.

".q ONWASA Laboratory
228 Georgetown Road
Jacksonville NC 28540
.1 [phone]
April 26, 2021
Mark Young
Swansboro WRF
199 Williams Road
Swansboro, NC 28584
RE: Swan Solids
Enclosed are the results of analyses for samples received by our laboratory on 3/24/2021. If you
have any questions concerning this report, please feel free to contact me.
Sincerely,
,/, l
Todd A. Roberts For Randal Riggs
Swansboro Operator

ONWASA
Swansboro WRF Project: Swan Solids
199 Williams Road Project Number: Reported:
Swansboro,NC 28584 Project Manager: Mark Young 04/26/2021 11:17
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: Swan Fecal#1 5211305-01(WW)
Reporting Date Analyst
Analyte Result Qual Umit Units Analyzed Initials Method
Fecal Density 87582 MPN/g 03/27/2021 SM 9221C E MPN
24hr 503
Total Solids Vic) 2.74 % 03/24/2021 SM 2540 G
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: Swan Fecal#2 S211305-02(WW)
Reporting Date Analyst
Analyte Result Qual Umit Units Analyzed Initials Method
Fecal Density 62500 MPN/9 03/27/2021 SM 9221C E MPN
24hr 503
Total Solids(oh) 2.72 % 03/24/2021 SM 2540 G
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: Swan Fecal#3 5211305-03(WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 85715 MPN/g 03/27/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 2.8 % 03/24/2021 SM 2540 G
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: Swan Fecal#4 S211305-04(WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
The contents of this report apply to Ore sample(s)analyzed hr accordance with the chain of custody document
No duplication of this report is allowed,except In its entirety. Page 2 of 6

4.5
ONWASA
Swansboro WRF Project: Swan Solids
199 Williams Road Project Number: Reported:
Swansboro,NC 28584 Project Manager: Mark Young 04/26/2021 11:17
Sample Results
(Continued)
Data Analyzed by:Environmental Chemists,Inc.
Sample: Swan Fecal #4 (Continued) S211305-04(WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 48690 MPN/g 03/27/2021 SM 9221C E MPN
24hr503
Total Solids(%) 2.67 % 03/24/2021 SM 2540 G
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: Swan Fecal#5 S211305-05(WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 80000 MPN/9 03/27/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 2.75 °f° 03/24/2021 SM 2540 G
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: Swan Fecal#6 S211305-06 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 16313 MPN/9 03/27/2021 SM 9221C E MPN
24hr 503
Total Solids Pk) 2.62 °f° 03/24/2021 SM 2540 G
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: Swan Fecal#7 S211305-07(WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
The contents of this report apply to the samples)analyzed In acmrdance with the chain of custody document
No duplkadon of this report Is allowed,except In its entirety. Page 3 of 6

A
ONWASA
Swansboro WRF Project: Swan Solids
199 Williams Road Project Number: Reported:
Swansboro,NC 28584 Project Manager: Mark Young 04/26/2021 11:17
Sample Results
(Continued)
Data Analyzed by: Environmental Chemists,Inc.
Sample: Swan Fecal#7 (Continued) S211305-07(WW)
Reporting Date Analyst
Analyte Result Qual Umit Units Analyzed Initials Method
•
Fecal Density 47971 MPN/g 03/27/2021 SM 9221C E MPN
24hr 503
Total Solids(0/0) 2.71 % 03/24/2021 SM 2540 G
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: Swansboro Digestor S211305-08(SL)
001
I
Reporting Date Analyst
Analyte Result Qual Umit Units Analyzed Initials Method
Aluminum 3370 mg/Kg 03/29/2021 EPA 200.7
Ammonia-N 4090 mg/Kg 03/25/2021 SM 4500 NH3 C
Arsenic
mg/Kg 03/29/2021 EPA 200.7
Calcium 32100 mg/Kg 03/29/2021 EPA 200.7
Cadmium
< mg/Kg 03/29/2021
Chromium EPA 200.7
mg/Kg 03/29/2021 EPA 200.7
Copper 228 mg/Kg 03/29/2021 EPA 200.7
Mercury < mg/Kg 03/30/2021 SW846 7471E
Potassium 3040 mg/Kg 03/29/2021 EPA 200.7
Magnesium 1670 mg/Kg 03/29/2021 EPA 200.7
Molybdenum
mg/Kg 03/29/20. EPA 200.7
Sodium 3160 mg/Kg 03/29/2021 EPA 200.7
Nickel
mg/Kg 03/29/2021 EPA 200.7
Nitrate+Nitrite-Nitrogen 90.6 mg/Kg 03/29/2021 EPA 353.2
Lead < mg/Kg 03/29/2021 EPA 200.7
PH 7.36 pH Units 03/25/2021 SM 4500 H B
Selenium < mg/Kg 03/29/2021 EPA 200.7
Total Kjeldahl Nitrogen 56000 mg/Kg 03/29/2021 EPA 351.2
Phosphorus,total Sludge 22400 mg/Kg 04/02/2021 SM 4500 P E
Total Solids(%) 2.74 % 03/27/2021 SM 2540 G
Zinc 3720 mg/Kg 03/29/2021 EPA 200.7
The contents ofthIs report apply to the sample(s)analyzed In accordance with the drain of custody document
No duplication of this report is allowed,except in its entirety. Page 4 of 6

6602
l Way
lu!� >y�taYsn> 40? ENVIRONMENTAL- CHEMISTS, INC OFFICE 9 0�3 2022'IFAX910,NC
3924a245
NCDENR:DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 [e-mail]
Analytical&Consulting Chemists °�
i
COLLECTION AND CHAIN OF CUSTODY
Client: Onslow Water& Sewer Authority(ONWASA) PROJECT NAME: Swansboro WRF REPORT NO:
ADDRESS: 228 Georgetown Rd CONTACT NAME: Mark Young PO NO:
Jacksonville, NC 28540 REPORT TO: [e-mail] PHONE/FAX: [phone]
COPY TO: [e-mail] email: myoungeonwasa.com _
Sampled By: L-ta.;0 £/JG2s L SAMPLE TYPE:I=Influent, E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection v PRESERVATION
• a " C Jq m -
Sample Identification £ o .ta — E m a
o p o w ANALYSIS REQUESTED
N u " " z _N Date Time Temp v 3/24/21 0 y/5 ix 7 C Q
Digester SL (G) G X Annual Sludge Analysis/Nutrient&Metal
3/24/21 (3 to/ f'f C CD
Digester- Fecal 1 G i- SL n G _ X Fecal Density
3/24/21 .( qi 2 . 1 (/ / C (P)
Digester- Fecal 2 _ SL CGS G X Fecal Density
3/24/21 if k' f V (1 C C)Digester- Fecal 3 ( D f SL 0 G X Fecal Density
3/24/21 .0 q It/ CD
/
Digester- Fecal 4 _ SL - GG _G _ X Fecal Density
3/24/21 -(1' y.d f r y C C P)
Digester- Fecal 5 ! SL () G X Fecal Density
3/24/21 J'(. -f j a r cED
Digester- Fecal 6 f SL © G X Fecal Density
3/24/21 b -- i i /
� C --
Digester- Fecal 7 I `� SL CO) G X Fecal Density
Transfer Relinquished By: Date/Time Received By: Date/Time
1. (.rz•g (rrat\ 3-z,/-zl PR03
2.
Temperature when Received: Accepted: Rejected: Resample Requested:
Delivered By: Received By: Date: Time:
Comments: TURNAROUND:

�,Y � ` � , 1 e c Environmental Chemists, Inc®
{ r„ fi,.r .+�rx,-r1 ,
t e l 1, 1 '�,�w It 6602 Windmill Way,Wilmington,NC 28405 0 910.392 0223 Lab P 910.392.4424 Fax
`' ;';',Ai„ ;-t-t: ",;r ;, 5's 710 Bowsertown Road,lvlanteo,NC 27954 4 252.473.5702 Lab/Fax
• +-''e ,,;4;fir; Y=` :r- t-,
.�r 255-A Wilmington Highway,Jacksonville,NC 28540 * 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Onslow Water&Sewer Authority Date of Report: Apr 06, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Mark Young Report#: 2021-04853
Project ID: Swansboro WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11956 Site: Digester 3/24/2021 9:15 AM Solid/Sludge Craig Green
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200.7 3370 mg/kg 03/29/2021
Arsenic EPA 200.7 <36.4 mg/kg 03/31/2021
Cadmium EPA 200.7 <18.2 mg/kg 03/29/2021
Calcium EPA 200.7 32100 mg/kg 03/29/2021
Chromium EPA 200.7 <18.2 mg/kg 03/29/2021
Copper EPA 200.7 228 mg/kg 03/29/2021
Lead EPA 200.7 <18.2 mg/kg 03/29/2021
Magnesium EPA 200.7 1670 mg/kg 03/29/2021
Molybdenum EPA 200.7 <18.2 mg/kg 03/29/2021
Nickel EPA 200.7 <18.2 mg/kg 03/29/2021
Potassium EPA 200.7 3040 mg/kg 03/29/2021
Selenium EPA 200.7 <18.2 mg/kg 03/29/2021
Sodium EPA 200.7 3160 mg/kg 03/29/2021
Zinc EPA 200.7 3720 mg/kg 03/29/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 90.6 mg/kg 03/29/2021
Total Solids (%) SM 2540 B 2.74% 03/27/2021
pH SM 4500 H B 7.36 units 03/25/2021
Ammonia Nitrogen SM 4500 NH3 C 4090 mg/kg 03/25/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 56000 mg/kg 03/29/2021
Total Phosphorus SM 4500 P F 22400 mg/kg 04/02/2021
Mercury Sw848 747,E <0.608 mg/kg 03/30/2021
Report ffr, 2021-04853
Page 1 of 3

�,T �, ,„�a Environmental Chemists, Inc.
A iR O* ,n rtf7rA yES�1
°31 k. ;3„we 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 9/0.392.4424 Fax
" '% ! ' 710 Bowsertown Rod,Manteo,NC 27954 • 252.473.5702 Lab/Fax
li:-_ � '..; - sM' 255-A Wilmington Highway,Jacksonville,NC 28540 a 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Onslow Water& Sewer Authority Date of Report: Apr 06, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Mark Young Report#: 2021-04853
Project ID: Swansboro WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11958 Site: Dilution#1 3/24/2021 9:16 AM Solid/Sludge Craig Green
Test Method Results Date Analyzed
Total Solids(%) SM 2540 B 2.74% 03/27/2021
Fecal Density SM 9221C EMPN 24 hr 503 87592 MPNIg 03/24/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11959 Site: Dilution#2 3/24/2021 9:17 AM Solid/Sludge Craig Green
Test Method Results Date Analyzed
Total Solids (%) SM 2540 8 2.72% 03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 62500 MPN/g 03/24/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11960 Site: Dilution#3 3/24/2021 9:18 AM Solid/Sludge Craig Green
Test Method Results Date Analyzed
Total Solids(%) SM 2540 B 2.8D% 03/27/2021
Fecal Density SM 9221C EMPN 24 hr 503 85715 MPN/g 03/24/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11961 Site: Dilution#4 3/24/2021 9:19 AM Solid/Sludge Craig Green
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2,67% 03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 48690 MPN/g 03/24/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11962 Site: Dilution#5 3/24/2021 9:20 AM Solid/Sludge Craig Green
Test Method Results Date Analyzed
Total Solids(%) SM 2540 8 2.75% 03/27/2021
Fecal Density SM 9221C E MPN 24 hr 503 80000 MPN/g 03/24/2021
Report 9:: 2021-04853
Page 2of3

Environmental Chemists, Inc.
en.virochee 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab Y 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
sr 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS inforthenvi roamer'talchemists.corn
Onslow Water&Sewer Authority Date of Report: Apr 06, 2021
228 Georgetown Road Customer PO #:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Mark Young Report#: 2021-04853
Project ID: Swansboro WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11963 Site: Dilution#6 3/24/2021 9:21 AM Solid/Sludge Craig Green
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 2.82% 03/27/2021
Fecal Density 5M 9221 C E MPN 24 hr 503 16313 MPN/g 03/24/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11964 Site: Dilution#7 3/24/2021 9:22 AM Solid/Sludge Craig Green
Test Method Results Date Analyzed
Total Solids(%) SM 2540 a 2.71% 03/27/2021
Fecal Density SM 9221C E MPH 24 hr 503 47971 MPN/g 03/24/2021
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: PCLitk,0 0Nok
Report#: 2021-04853
Page 3 of 3

Environmental Chemist, inc., Wilmington, NC Lab#94 6602 Windmill Way
Wilmington,NC 28405
910.392.0223
Sample Receipt Checklist
Client: 01\1L01)-1 MUTT-. Date:
3 a,��11 7 oR) Report Number: 02] —0(-(8S 3
Receipt of sample: ECHEM Pickui Client Delivery❑ 'UPS 0 FedEx 0 Other ❑
❑ YES f❑ NO N/A JJ1..Were custody seals present on the cooler?
❑ YES Cl NO R N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt_R. °C Corrected temperature upon receipt °C
How temperature taken: 0 Temperature Blank 1, '' Against Bottles
IR Gun ID:Thomas Traceable S/N 192511657 IR Gun Correction Factor°C:0.0
❑ YES ❑ NO 3. If temperature of cooler exceeded 6°C,was Project Mgr./QA notified?
YES 0 NO 4. Were proper custody procedures(relinquished/received)followed?
❑ YES ❑ NO 5. Were sample ID's listed on the COC?
❑ YES 0 NO 6. Were samples ID's listed on sample containers?
_ YES ❑ NO 7. Were collection date and time listed on the COC?
YES ❑ NO 8. Were tests to be performed listed on the COC?
YES 0 NO 9. Did samples arrive in proper containers for each test?
YES ❑ NO 10. Did samples arrive in good condition for each test?
YES 0 NO _ 11. Was adequate sample volume available?'
YES 0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES ,❑ NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH>12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH>9? •
❑ YES ❑ NO 16. Were NF13/TKN/Phenol received at a chlorine residual of<O.5 m/L?**
0 YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) )
Sample(s) _ were received incorrectly preserved and were adjusted accordingly
by adding(circle one): H2504 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC.QA.002 Rev 1

h �r ENVIRONMENTAL CHEMISTS, 6602 Windmill Way Wilmington,NC 28405
3 OFFICE:910-392-0223 FAX 910�92-4424
Analytical$Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS: DLS CERTIFICATION#37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
•Client: Onslow Water&Sewer Authority(ONWASA) PROJECT NAME: Swansboro WRF
REPORT NO: c>2/— oq S-S 3
ADDRESS: 228 Georgetown Rd CONTACT NAME: Mark Young PO NO:
Jacksonville, NC 28540 REPORT TO: [e-mail] PHONE/FAX: [phone]
COPY TO: Martin [e-mail] email: [e-mail]
Sampled By: (mot, ;U q rj-/' 2 t SAMPLE TYPE: I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,Si_=Sludge,Other:
Collection
m 2 a a PRESERVATION
Sample identificationA 6 w
4a pr.,
� �� �
E ° r o a°, 5 E m 1 z u 8 o 0 o 5 ANALYSIS REQUESTED
Date Time Temp 0 u V n 2 °_ _ _ = z o
3/24/21 Yf/j I X 7 c
Digester SL © G )!q5.7 X Annual Sludge Analysis/Nutrient& Metal
•
3/24/21 (a(//b p? ) C CD
Digester- Fecal 1 G SL QG G irM X Fecal Density
3/24/21 IN/7 J�J 0. c ®-
Digester-Fecal 2 ! i, SL CD G 11 9S X Fecal Density
3/24/21 kyle [f q c Grp
-
Digester-Fecal 3 SL CD G Li °)(OD X Fecal Density
3/24/21 -V /q 191 C C�
Digester-Fecal 4 SL Q _G 119(e i X Fecal Density
3/24/21 e q { 5 C P�
Digester-Fecal 5 f SL - CG) G i 19(el-- X Fecal Density
3/24/21 01)-f _ )p (� C 'CDDigester-Fecal 6 l f ! SL C.c.) G 119(03 X Fecal Density
3/24/21 b 0 2-vt )q I G _
Digester-Fecal 7 f� SL CO G , fIti(pV X Fecal Density
Transfer Relinquished By: Date/Time Re`slued B
1. C�rst,� �rre�n 3-L i / $ 30 y` Date/Time
A.:.)14a.” ) I.2:31-
z.
Temperature we
n R d: y Acce ted:
�" � ' P cted: Resampl�e� equ ted:
Delivered By: ey Received B .
Comments:
Y' Date. t{ Time:
TURNAROUND:

, m 0 �� Environmental Chemists, Inc.
enirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab e 910.392.4424 Fax
vip, ,'i � - 7I0 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
:...,,,,�,��s 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS inforkenvironmentalchemists.com
Onslow Water&Sewer Authority Date of Report: Jul 21, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Todd Roberts Report#: 2021-10653
Project ID: Swansboro WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-26548 Site: Digester 6/29/2021 6:30 AM Solid/Sludge Randal Riggs
Test Method Results Date Analyzed
Chlordane(TCLP) SW 846 Method 8081 B/3510 <0.02 mg/L 07/09/2021
Endrin (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 07/09/2021
Heptachlor(TCLP) 5W 846 Method 8081B/3510 <0.0005 mg/L 07/09/2021
Heptachlor epoxide (TCLP) SW 846 Method 808113/3510 <0.0005 mg/L 07/09/2021
Lindane (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 07/09/2021
Methoxychlor(TCLP) SW 046 Method 8081B/3510 <0.0005 mg/L 07/09/2021
Toxaphene (TCLP) SW 846 Method 8 081 8/3 5 1 0 <0.05 mg/L 07/09/2021
1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0,050 mg/L 07/08/2021
2,4,5-Trichiorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
2,4,6-Trichiorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
2,4-Dinitrotoluene (TCLP) . SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
Cresol(TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 • <0.050 mg/L 07/08/2021
Hexachlorobenzene (TCLP) SW 046 method 0270/3510 <0.050 mg/L 07/08/2021
Hexachloroethane(TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
o-Cresol (TCLP) 5W 646 method B270/3510 <0.050 mg/L 07/08/2021
Pentachlorophenol(TCLP) 5W 848 method 827013510 <0.250 mg/L 07/0B/2021
Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 07/08/2021
2,4,5-TP (TCLP) SW846 Method B151A <0.003 mg/L 07/13/2021
2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 07/13/2021
1,1-Dichloroetliylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
1,2-Dichloroethane (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
Benzene (TCLP) SW848 Method 8260/5030 <0.01 mg/L 07/02/2021
Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
Report*: 2021-10653
Page 1 of 2

y ° � Y � Environmental Chemists, Inc.
kr: rtv� ochEriit,- 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
,]" ` ' '' -- , :, F' 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
M "" ' `SM' 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info!a•environmentalchemists.com
Onslow Water& Sewer Authority Date of Report: Jul 21, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Todd Roberts Report#: 2021-10653
Project ID: Swansboro WRF
Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 07/02/2021
Tetrachloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 07/02/2021
RCI
Cyanide SM 4500 CN D 2.05 mg/kg 07/07/2021
Sulfide SM 4500 s o 22.8 mg/kg 07/06/2021
lgnitability SW 846 method 1010 >195°F 07/20/2021
pH SW 846 Method 804so 7.53 units 06/30/2021
Result estimated. Analyzed out of 15 minutes hold time.
TCLP Metals
Arsenic EPA 200.7 <1.0 mg/L 07/09/2021
Barium EPA 200.7 <1.0 mg/L 07/09/2021
Cadmium EPA 200.7 <1,0mg/L 07/09/2021
Chromium EPA 200.7 <1.0 mg/L 07/09/2021
Lead EPA200.7 <1.0 mg/L 07/09/2021
Selenium EPA z0o.7 <1.0mg/L 07/09/2021
Silver EPA 200.7 <1.0 mg/L 07/09/2021
Mercury EPA 245.1 <0.0002 mg/L 07/14/2021,
Comment: t
Reviewed by: �Q 6
Report#:: 2021-10653
. Page 2 or 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilrnineto n, NC 28405
910.392.0223
Sample Receipt Checklist
Client: OK.MR-S Date: l frd 2 Z� !! 2
1 J Report Plumber: �� " ! �[p�J
Receipt of sample: ECHEM Pickup Client Delivery❑ !UPS 0 FedEx 0 Other 0
0 YES 10 NO mi. N/A 1, Were custody seals present on the cooler? I
❑ YES f❑ No ri N/A 2. 1F custody seals were present ? it
Original temperature upon receipt -2 •1 " � were the y intact/unbroken?C Corrected temperature upon receipt 'C
How temperature taken: 0 Temperature Blank
Against Bottles
IR Gun ID: Thomas Traceable 5/N 192511657 IR Gun Correction Factor °C: 0.0
J 4 YES 0 NO 3. if temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
3R1' YES 0 NO 4. Were proper custody procedures (relinquished/received) followed?
R. YES 0 NO 5. Were sample ID's listed on the COC?
I YES 0 NO 6. Were samples ID's listed on sample containers?
?f YES 0 NO 7. Were collection date and time listed on the COC?
YES ❑ NO 8. Were tests to be performed listed on the COC?
YES 0 NO 9. Did samples arrive in proper containers for each test?
:! YES ❑ NO 10. Did samples arrive in good condition for each test?
vrr r-t .,r,
!• I — r -- ..'. _, ....,�y.....,.. ...1,.it.,i._ ruiuiliC 0,0411pulC:
JiE Yk5 0 NO 12. Were samples received within proper holding time For requested tests? I
b Y E 5 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH>9?
❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? ."
❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES r❑ NO 18. Were orthophosphate samples filtered in the Field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchshaet
''` Bane;is -samples a`e check?d for Crilorrne at time or analysis and recorded or the be. :,'iih2et.
Sample Preservation; (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) _ were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H SO_ HNO; HCl NaOH
Time of preservation: if more than one preservative is needed, notate in comments below
.*1ot_:ti3:i ., f i,�car ._.:,.
Y. i:J^'-ter 5?^J�:?r!']rT'=�jd t''y .�i, r2i2"12d 537U:i O^:a.n 2 n?: ?"i
q:.ti y t 'e i__.e ..•.'ieb l;d rec to ai eized by the c.15:aTe- V,r. v.4s no nr,ad Oa'?ana turn?: .-2
Volatiles Sample(s) were received with headspace .
COMMENTS: w
DOC. QA.002 Rev 1

t:
Onslow Water&Sewer Authority SUBCONTRAC
T
� .--,__:� 228 Georgetown Road
ONWA�,,A Jacksonville NC 28540 ORDER
Sending Facility: Subcontracted Laboratory:
5wansboro WWTF
228 Georgetown Road 1 r�,.4 : .1
Jacksonville, NC 28540
Phone:[phone] Environmental Chemists, Inc.
6602 Windmill Way
Wilmington, NC 28905
Project Manager: Randal Riggs Phone:[phone] Fax: [phone]
NCOENR:OW9 CERTIFICATION 5 94 NCOHNS:0L5 CERTIFICATION C 37779
Work Order: S212701 Swansboro WRF
Sample ID:5212701-01 Swansboro Digester 001 St Sampled: 06/29/2021 06:30 Sampled by:fandal Riggs
Analysis Due Expires EnviraChem Lab ID
pH,5W846 07/09/2021 06/29/2021 06:47
Analysis Due Expires EnviroChem Lab ID
Sulfide colorimetric 07/09/2021 07/13/2021 06:30
Analysis Due Expires EnviroChem Lab ID
Cn-335.4 07/09/2021 07/I3/2021 06130
Analysis DUG Expires EnviroChem Lab ID
SW 846 Mtd 8270/3510 07/09/2021 07/27/2021 06:30
Analysis Due Expires EnviroChem Lab ID
SW 846 808111/3510 07/09/2021 07/27/2021 06:30
Analysis Due Expires EnviroChem Lab ID
Ignitabillty 1030 07/09/2021 07/27/2021 06:30
Analysis Due Expires EnviroChem Lab ID
Hg 245.1 07/09/2021 07/27/2021 06:30
Analysis Due Expires EnviraChem Lab ID
TCLP Metals 07/09/2021 12/26/2021 06:30
Analysis Due Expires EnviroChem Lab ID
5W846 8260/5030 07/09/2021 12/26/2021 06:30
Analysis Due Expires EnviraChem Lab ID
5W896 8151A 07/09/2021 12/26/2021 06:30
Containers Supplied;
AG IL(A) AG IL(B) AG 1L(C) IL Plastic(0)
EnviroChem Report No: 2_t - r Off' 3
.-----ii4114 , 411jc
Relinquished By Z 2v /r�/� /10z,--
t -2 Z1
Date eived By bate
Page 1 or I •

COASTAL FARMS AND RESIDUALS,LLC
WQ0034806
Swansboro WRF
12/02/.21 86,891 4.9390
12/02/21 28I,346 5.4492
12/02/21 109,375 5.0389
12/02/21 116,667 5.0669
12/02/21 165,645 5.2192
12/02/21 144,386 5.1595
12/02/21 168,225 5.2259
Total 36.0987
Average 5.1570
Geometric Mean Fecal Coliform MPN 1 gram
Geometric Mean of Less than 2,000,000 meets Class B -Alternative 1 Pathogen Reduction
requirement.

ONWASA Laboratory
228 Georgetown Road
—At> Jacksonville NC 28540
ONWASA [phone]
December 13, 2021
Mark Young
Swansboro WRF
199 Williams Road
Swansboro, NC 28584
RE: Swan Solids
Enclosed are the results of analyses for samples received by our laboratory on 12/2/2021. If you
have any questions concerning this report, please feel free to contact me.
Sincerely,
^, 4
Todd A. Roberts For Craig Green
Swansboro Operator

ONWASA
Swansboro WRF Project: Swan Solids
199 Williams Road Project Number: Reported:
Swansboro,NC 28584 Project Manager: Mark Young 12/13/2021 09:00
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: Swan Fecal#1 S214907-01(WW)
Reporting Date Analyst
Analyte Result Qual Umit Units Analyzed Initials Method
Fecal Density 86891 MPN/9 12/06/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 3.28 % 12/02/2021 SM 2510 G
Sample Results
Data Analyzed by: Environmental Chemists,Inc.
Sample: Swan Fecal #2 S214907-02(WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 281346 MPN/g 12/06/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 3.27 % 12/02./202I SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists,Inc.
Sample: Swan Fecal #3 S214907-03(WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 109375 MPN/9 12/06/2021 SM 9221C E MAN
24hr 503
Total Solids(olo) 3.2 % 12/02/2021 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists,Inc.
Sample: Swan Fecal #4 S214907-04(WW)
Reporting Date Analyst
Analyte Result Qual Unit Units Analyzed Initials Method
The contents of this report apply to the sample(s)analyzed in accordance with the drain of custody document.
No duplication of this report is allowed,except In its entirety. Page 2 of 6

6.
ONWASA
Swansboro WRF Project: Swan Solids
199 Williams Road Project Number: Reported:
Swansboro,NC 28584 Project Manager: Mark Young 12/13/2021 09:00
Sample Results
(Continued)
Data Analyzed by: Environmental Chemists,Inc.
Sample: Swan Fecal #4 (Continued) S214907-04(WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 116667 MPN/9 12/06/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 3 % 12/02/202I SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists,Inc.
Sample: Swan Fecal #5 5214907-05 (WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 165647 MPN/9 12/06/2021 SM 9221C E MPN
244 503
Total Solids(%) 3.26 % 12/02/2021 SM 2540 G
Sample Results
Data Analyzed by: Environmental Chemists,Inc.
Sample: Swan Fecal #6 S214907-06(WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed Initials Method
Fecal Density 144386 MPN/9 12/06/2021 SM 9221C E MPN
24hr 503
Total Solids(%) 3.74 % 12/02/2021 5M 2540 G
Sample Results
Data Analyzed by:Environmental Chemists,Inc.
Sample: Swan Fecal #7 S214907-07(WW)
Reporting Date Analyst
Analyte Result Qual Limit Units Analyzed In€tials Method
The contents of this report apply to the sample(s)analyzed in accordance with the chain of custody document.
No duplication of this report Is allowed,except In its entirety. Page 3 of 6

Ta
ONWASA
Swansboro WRF Project: Swan Solids
199 Williams Road Project Number: Reported:
Swansboro,NC 28584 Project Manager: Mark Young 12/13/2021 09:00
Sample Results
(Continued)
Data Analyzed by: Environmental Chemists,Inc.
Sample: Swan Fecal #7 (Continued) S214907-07(WW)
Reporting Date Analyst
Analyse Result Qual Limit Units Analyzed Initials Method
Fecal Density 168225 MPN/g 12/06/2021 SM 9221C E MPN
24hr 503
Total Solids(0/a) 3.21 % 12/02/2021 SM 2540 G
The contents of this report apply to the samples)analyzed in accordance with the chain of custody document.
No duplication ofMisreport Is allowed,except In its entirety. Page 9 of 6

t A s ONWASA Laboratory CHAIN OF CUSTODY 11Il1IlOhII1I 1111 0
228 Georgetown Road Pagc 1 of 1 S 2 1 4 9 0 7
{`' Jacksonville, North Carolina 28540 Phone:[phone] COC Number
Fax:1910}455-5607 Lab Work Order Numbi S214907
Client Name Project Name 'iequested Analyses i-mid Analysis rsequestce rOrn Nrounu
Swansboro WRF Swan SolidsI -
Client Contact Project Number Rush requests subject to additional
Mark Young [none] m
IT charge.
Address Project Description S ' Rush requests subject to lab
199 Williams Road
City -PO Number ru O z M. m approval
Swansboro N c C 4a (1
m
State/Zip Shipped By 2 CZ to ` _. Standard{days)
NC,28584 y O °+ tu 10
Phone/Fax Tracking Number •p Xi up ri n ,' Expedited(days)
910-545-6877/ ,., a ° o 0
Sampler �t ��r/t r r3 Sampler 5i nature) i f m m
ZaChtti, ar ee 'A4i Due Date
/ LL ' 12/12/2021 0:00
Preservation Code
Sample Type Matrix Lontamer
Sample Name or Field ID Sampled Date Sampled Time Code Code Count P::C Sample Comments
Swan Fecal#1 12/2/2021 e ev G WW 1 1 j7t
Swan Fecal#2 12/2/2021 9 f j') G WW 1 1 . 125
Swan Fecal#3 12/2/2021 e fgZ G _ WW 1 1 1?6
Swan Fecal#4 12/2/2021 0 qen G WW 1 1 _ (27
Swan Fecal#5 12/2/2021 0IVy G WW 1 1 i7Q.
-
Swan Fecal#6 _ 12/2/2021 tf_ G WW 1 1 I24f
Swan Fecal#7 12/2/2021 0 g 6 G WW 1 1 - )2•4"
Relinquished By Date/Time I a/�eq r a j Recei ed By Date/Time
_ Zcha tj V#i - l aced ,, F / 1&/4z/ /72z9
Relinquished By Date/Time Received By Date/Time Comments
Relinquished By Date/Time Received By Date/Time
Cooler Numbers and Temperatures /
Default Cooler Receive Temp: / °C pH: Intials: ]77-
Matrix Codes: WW=WW Preserv.Codes: C=0.0008%Na25203
'Indicates Field Tess-Analysis. - --
-- Cant..Codes _P 1205terile_Na252a3

F ` "
t ' Environmental Chemists, Inc.
e viro e i 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910 392.4424 Fax
.. ..; 4-A 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab Fax
0 . Ssti+ 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Onslow Water& Sewer Authority Date of Report: Dec 09, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Craig Green Report#: 2021-21322
Project ID: Swansboro WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53415 Site: Swan Fecal#1 12/2/2021 9:00 AM Solid/Sludge Zachary Dail
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.28% 12/06/2021
Fecal Density SM 9221C E-2014 86891 MPN/g 12/02/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53416 Site: Swan Fecal#2 12/2/2021 9:01 AM Solid/Sludge Zachary Dail
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.27% 12/06/2021
Fecal Density SM 9221C E-2014 281346 MPN/g 12/02/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53417 Site: Swan Fecal#3 12/2/2021 9:02 AM Solid/Sludge Zachary Dail
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.20% 12/06/2021
Fecal Density SM 9221C E-2014 109375 MPNIg 12/02/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53418 Site: Swan Fecal#4 12/2/2021 9:03 AM Solid/Sludge Zachary Dail
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.00% 12/06/2021
Fecal Density SM 9221C E-2014 116667 MPN/g 12/02/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53429 Site: Swan Fecal#5 12/2/2021 9:04 AM Solid/Sludge Zachary Dail
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.26% 12/06/2021
Fecal Density SM 9221C E-2014 165645 MPN/g 12/02/2021
Reoarf 4: 7021-71322

,a� , �}; � � ��*,, Environmental Chemists, Inca
'.-en ir+cheni 6602 Windmill Way Wilmington,NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax
v.•'" d x_ „`� cite'` - 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
., ... ` .: 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Onslow Water&Sewer Authority Date of Report: Dec 09, 2021
228 Georgetown Road Customer PO#:
Jacksonville NC 28540 Customer ID: 08100092
Attention: Craig Green Report#: 2021-21322
Project ID: Swansboro WRF
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53430 Site: Swan Fecal#6 12/2/2021 9:05 AM Solid/Sludge Zachary Dail
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 3.74% 12/06/2021
Fecal Density SM 9221C E-2014 144386 MPN/g 12/02/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-53431 Site: Swan Fecal#7 12/2/2021 9:06 AM Solid/Sludge Zachary Dail
Test Method Results Date Analyzed
Total Solids (%) SM2540B 3.21 % 12/06/2021
Fecal Density SM 9221C E-2014 168225 MPN/g 12/02/2021
Comment: Results reported on a dry weight basis.
Reviewed by: A ,OA
Remit It-- 7roi-71777

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:CU w AW54, Date/ tad GZI
Report Number:_ c�1 --ot!
Receipt of sample: ECI-IEM Pickup Client Delivery❑ jUPS 0 FedEx ❑ Other 0
❑ YES ❑ NO iJf N/A 1. Were custody seals present on the cooler?
❑ YES 0 NO K N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt o?. °C
How temperature taken: ❑ Temperature Blank Correctednst Bottles
temperature upon receipt °C
IR Gun ID:Thomas Traceable 5/N 192511657 IR Gun Correction Factor UC:0.0
❑ YES 0 NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
w YES 0 NO 4. Were proper custody procedures (relinquished/received)followed?
YES ❑ NO 5. Were sample ID's listed on the COC?
417) YES ❑ NO 6. Were samples ID's listed on sample containers?
YES 0 NO 7. Were collection date and time fisted on the COC?
YES ❑ NO 8. Were tests to be performed listed on the COC?
YES 0 NO 9. Did samples arrive in proper containers for each test?
tiYES ❑ NO 10. Did samples arrive in goad condition for each test?
YES 0 NO 11. Was adequate sample volume available?'
►d YES 0 NO 12. Were samples received within proper holding time for requested tests?
0 YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH>12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH>9?
❑ YES 0 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TM/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) _ were received incorrectly
by adding (circle one): H2504 HNO3 Ha Na pl�reserved and were adjusted accordingly
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

Onslow Water&Sewer Authority SUBCONTRACT
228 Georgetown Road
Jacksonville NC 28540 ORDER
N WA S A
01.
Sending Facility: Subcontracted Laboratory: CR1 ~ 1313,
Swansboro WWTF
228 Georgetown Road !
Jacksonville, NC 285.40
Phone: [phone] Environmental Chemists, Inc.
6602 Windmill Way
Wilmington, NC 28405
Project Manager: Craig Green Phone: [phone] Fax: [phone]
HCOENR:DW12 CERTIFICATIONS 94 NCD11H5;DL5 CERTIFICATION b 37729
Work Order: S214907 " Swansboro WRE ``411
Sample ID:S214907-01 Swan Fecal#1 WW Sampled: 12/02/2021 09:00 Sampled by:Zachary Datf 1 �5
Analysis Due Expires EnviroChem Lab ID
Fecal Density 12/12/2021 12/02/2021 15:00
Analysis Due Expires EnviroChem Lab ID
Total Solids(%) 12/12/2021 12/09/2021 09:00
Containers Supplied::
120 Sterile Na2S2O3(A)
Sample ID:S214907-02 Swan Fecal#2 WW Sampled: 12/02/2021 09:01 Sampled by:Zachary call s-8 [ L W
Analysis Due Expires EnviroChem Lab ID
Fecal Density 12/12/2021 12/02/2021 15:01
Analysis Due Expires EnviroChem Lab ID
Total Solids(%) 12/12/2021 12/09/2021 09:0I
Containers Supplied:
120 Sterile Na25203(A)
Sample ID:S214907-03 Swan Fecal#3 WW Sampled: 12/02/2021 09:02 Sampled by:Zachary Gall 5 3 y! 1
Analysis Due Expires EnviroChem Lab ID
Fecal Density 12/12/2021 12/02/2021 15:02
Analysis Due Expires EnviroChem Lab ID
Total Solids(%) 12/12/2021 12/09/2021 09:02
Containers Supplied:
I20 Sterile Na2S203(A)
Sample ID:5214907-04 Swan Fecal#4 WW Sampled: 12/02/2021 09:03 Sampled by:Zachary Dag 5,3 y 8
Analysis Due Expires EnviroChem Lab ID L
Fecal Density 12/12/2021 I2/02/2021 15:03
Analysis Due Expires EnviroChem Lab ID
Total Solids(%) 12/12/2021 12/09/2021 09:03
Containers Supplied;
120 Sterile Na252O3(A)
Sample ID:5214907-05 Swan Fecal#5 WW Sampled: 12/02/2021 09:04 Sampled by:Zachary
EnviroChem Report No:
ern C 4 Ai /2/z/49 //,i
Relinquished By Date Receiv d By Dale
Page 1 of 2 07,

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(02T Rules)
Facility Name: Coastal Farms and Residuals,LLC WQ Permit Number: WQ0034806
WWTP Name: Swansboro WWTP NPDES Number: WQ0023261
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A: Alt. A(time/temp) ❑ Alt B (Alk Treatment)El Alt.C(Prior Testing)❑
AIt.D(No Prior Test) 0 1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thennophilic ❑
Beta Ray 0 Gamma Ray ❑ Pasteurization ❑ _
........
Class B: Alt.(1)Fecal Density p I Alt. (2)Process to Significantly Reduce Pathogens ❑ I
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization El Air Diying ❑ Composting 0 Aerobic Digestion 0
Anaer
obic _Digestion
t scion
g
If applicable to alternative performed (Class A or Class B)complete the following'monitoring data:
Allowable Level Pathogen Densit -Number oil - AnalyncaT
g
Parameter - y Excee- Frequency Sample
in Sludge Minimum Geo.Mean Maximum Units of Analysis Type Teclt
ni
slences rnie
2 O to le MPN 16,313 54,512 87,592 MPN/g 0 Annual Grab SM92210E
6th
power
per gram of
Fecal CoIiform total solids CFU
1000 mpn per gram -
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4.grams
(in lieu of fecal total solid(dry
conform) weight) ,
Vector Attraction Reduction (15A NCAC 02T.1107)-Please indicate alternative performed:
Alt.l (VS reduction) 0 Alt.2(40-day bench) ❑ Alt.3(30-day bench) El Alt.4(Spec.02 uptake) ❑
Alt. 5(14-Day Aerobic) 0 Alt.6(Alk. Stabilization ❑ Alt 7(Drying-Stable) El Alt.8(Drying-Unstable) O.
Alt.9(Injection) El Alt. 10(Incorporation) p No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT(please check the appropriate statement)
0 "I certify, under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
0 "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mark Young,ORC Wesley Wooten,President
Preparer Name and Title(type or print) Land Applier Name and Title(if applicable)(type or print)
7 C.2.i. B 1/1 8/22 4/27/21
Signature of Preparer* Date Signature of La Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
DENR FORM PVRF 02T(1212006)

COASTAL FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: December 10,2021
The Cape Permit No.NC0057703
2.14 %Solids
6.72 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 7.390 73,900.000 147.800
Phosphorus 3.020 30,200.000 60.400
Potassium 0.986 9,860.000 19.720_
PAN(injected)* 2.412 24,119.950 48.240
PAN(surface)* 2.273 22,729.950 45.460
Ammonia Nitrogen 0.278 2,780.000 5.560
Calcium 4.600 46,000.000 92.000
Calcium Carbonate Eq. --- --- --
Magnesium --- 7,340.000 14.680
Sodium --- 6,120.000 12.240
Sulfur ___ --- ---
Nitrate N/Nitrite N _ --- 3.950 0.008_
Barium --_ --- --- SAR
Chloride --- --- _ --- 1.02
Iron --- --- --- Ceiling Concen.
Aluminum --- 2,350.00 4.700_ (Mg/Kg)
Arsenic --- 44.10 0.088 r 75
Cadmium --- _ 44.10 0.088 85
Chromium --- 44.100 ---
Copper --- 166.00 _ 0.332 4,300
Lead --- 44.10 0.088 840
Mercury _ --- 0.902 0.002 57
Molybdenum --- _ 44.10 0.088 75
Nickel --- _ 44.10 0.088 420
Selenium --- 44.10 0.088 100
Zinc --- 4,060.00 8.120 7,500
Environmental Chemists,Inc.# 2021-21935
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits arc listed as detection limits
for calculation purposes.

COASTAL FARMS AND RESIDUALS,LLC
WQ0034806
The Cape WWTP
1H1111111041111101 Fe041 Co i v - 1 =•` 140' 1'€ 1 xrn. L�tg,.
12/10/2.1 111,112 5.0458
12/10/21 _ 23,334 4.3680
12/10/21 84,159 _ 4.9251
12/10/21 92,828 4.9677
12/10/21 35,586 4.5513
12/10/21 50,229 4.7010
12/10/21 51,163 4.7090
Total 33.2677
Average 4.7525
Geometric Mean €11 56 5G1 11 Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B -Alternative 1 Pathogen Reduction
requirement.

" Y f .K;r Environmental Chemists, Inc®
elt .I, �-©_(,° .. ] 6602 Windmill Way,Wilmington,NC 28405 • 9I0.392.0223 Lab ° 910.392.4424 Fax
t i , ,x t<.7.�r'; ✓1 � 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS iafoi�l�?environmentalcliemists.com
Lewis Farms & Liquid Waste, INC, Date of Report: Jan 07, 2022
8155 Malpass Corner Road Customer PO#:
Currie NC 26435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2021-21935
Project ID: AquaNC-The Cape WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-54942 Site: Sludge 12/10/2021 8:30 AM Solid/Sludge Client
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200.7.Rev.4.4,1994 2350 mg/kg 12/22/2021
Arsenic EPA 200.7,Rev.4.4,1994 <44.1 mg/kg 12/22/2021
Cadmium EPA 200.7,Rev.4.4,1994 <44.1 mg/kg 12/22/2021
Calcium EPA 2001,Rev.4 4,1994 46000 mg/kg 12/30/2021
Chromium EPA 200.7,Rev,4.4,1994 <44.1 mg/kg 12/22/2021
Copper EPA 200.7,Rev.4.4,1994 166 mg/kg 12/22/2021
Lead EPA 200.7.Rev.4.4,1994 <44.1 mg/kg 12/22/2021
Magnesium EPA 200.7,Rev.4.4.1994 7340 mg/kg 12/22/2021
Molybdenum EPA 200.7,Rev.4.4,1994 <44.1 mg/kg 12/22/2021
Nickel EPA 200.7,Rev.4.4,1994 <44.1 mg/kg 12/22/2021
Potassium EPA 200.7,Rev,4.4,1994 9860 mg/kg 12/22/2021
Selenium EPA 200.7,Rev.4.4,1994 <44.1 mg/kg 12/22/2021
Sodium EPA 200.7.Rev.4.4,1994 6120 mg/kg 12/22/2021
Zinc EPA 200.7,Rev.4,4,1994 4060 mg/kg 12/22/2021
Nitratei-Nitrite-Nitrogen EPA 353.2 3.95 mg/kg 12/14/2021
Total Solids (%) SM 2540 8 2.14% 12/10/2021
Ammonia Nitrogen SM 4500 NH3 C-2011 2780 mg/kg 12/13/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg a-2011 73900 mg/kg 12/13/2021
Total Phosphorus SM 4500 P F-2011 30200 mg/kg 12/17/2021
pH SW 646 Method 9045D 6.72 units 12/22/2021
Result estimated. Analyzed out of 15 minutes hold time.
Mercury SW-646 7471 B <0.902 mg/kg 12/21/2021
Report f:: 202 1-2 1 935
•
. Page 1 of 3

0:p g� Environmental Chemists, Inc.
,;&,i( 7- .��,.",{'70 fir i- Ei '`.
9?env', 9 it c e 6602 Windmill Way,Wilmington,NC 28405 • 910.392-0223 Lab • 910.392.4424 Fax
�,::,,i. •- 4 - ,. (sue,. 710 Sowsertown Road,Manteo,NC 27954 . 252.4733.5702 Lab/Fax
`; ' '��' '` _- „ a ' 255-A Wilmington Highway, acksonville,NC 28540 . 910.347 5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Lewis Farms & Liquid Waste, INC. Date of Report: Jan 07, 2022
8155 Malpass Corner Road Customer PO#:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2021-21935
Project ID: AquaNC-The Cape WWTP
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-54943 Site: 1 12/10/2021 8:35 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 2-07% 12/10/2021
Fecal Density SM 9221C E-2014 111112 MPN/g
24HR Incubation 9 12/10/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-54944 Site: 2 12/10/2021 8:37 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 8 2.10% 1211012021
Fecal Density SM 9221C E-2014 23334 MPN/g 24HR Incubation 9 12/10/2021
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
21-54945 Site: 3 12/10/2021 8:39 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) 5M 2540 B 2.02% 12/10/2021
Fecal Density SM 9221C E-2014 84159 MPN/g 24HR Incubation 9 12/10/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-54946 Site:4 12/10/2021 8:41 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 s 2,37% 12/10/2021
Fecal Density SM 9221C E-2014 92828 MPN/g 24HR Incubation 9 12/10/2021
Report k:: 2021-21935
Page 2 of 3

: %-,- - Environmental Chemists, Inc.
e u, t .le 6602 Windmill Way,Wilmington,NC 28405 . 910.392.0223 Lab 0 910.392.4424 Fax
~.2:15-.� r=t 4 710 Bowsertown Road,Manteo,NC 27954 . 252.473.5702 Lab/Fax
.:,,i..; .u./, �..- 255 A Wilmington Highway,Jacksonville,NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Lewis Farms & Liquid Waste, INC. Date of Report: Jan 07, 2022
8155 Malpass Corner Road Customer PO#:
Currie NC 28435 Customer ID: 14020008
Attention: Wesley Wooten Report#: 2021-21935
Project ID: AquaNC-The Cape WWTP
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
21-54947 Site: 5 12/10/2021 8:43 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids(%) SM 2540 B 2.22% 12/10/2021
Fecal Density SM 9221C E-2014 35586 MPN/g
24HR Incubation 9 12/10/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-54948 Site: 6 12/10/2021 8:45 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 2,1 g% 1211012021
Fecal Density 5M 9221C E-2014 50229 MPNI Exceeded 24HR Incubation 9 1211012021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-54949 Site: 7 12/10/2021 8:47 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 2.15% 12/10/2021
Fecal Density SM 9221C E-2014 51163 MPNI Exceeded 24HR Incubation 9 1211012021
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: iMAOLL, 0Q1{0A)
Report tk: 2021.21935
Page 3of3

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
`` 1'— Sample Receipt Checklist
Client:Lt-,Kl,l5 C r`t 1 DatZ /l0/ / 9
ReportNumber: �j --c�,� �
Receipt of sample: ECHEM Pickup 0 Client DeliverypI IUPS 0 FedEx 0 Other 0
❑ YES ❑ NO ig N/A 1. Were custody seals present on the cooler?
❑ YES 0 NO K. N/A 2. If custody seals were present, were they
Original temperature upon receipt� °C intact/unbroken?
How temperature taken: 0 Temperature Blank Corrected temperature upon receipt °C
tZ Against Bottles
IR Gun ID:Thomas Traceable 5/N 192511657 IR Gun Correction Factor°C:0.0
❑ YES El NO 3. If temperature of cooler exceeded 6°C,was Project Mgr./QA notified?
R. YES 0 NO 4. Were proper custody procedures(relinquished/received)followed?
YES 0 NO 5. Were sample ID's listed on the COC?
YES 0 NO 6. Were samples ID's listed on sample containers?
YES 0 NO 7. Were collection date and time listed on the COC?
YES 0 NO 8. Were tests to be performed listed on the COC?
YES ❑ NO 9. Did samples arrive in proper containers for each test?
YES El NO 10. Did samples arrive in good condition for each test?
tki YES 0 NO 11. Was adequate sample volume available?'
» YES 0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2?*
❑ YES 0 NO 14. Were cyanide samples received at a pH>12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH>9?
El YES 0 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0,5 rn/I_?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any samples) incorrectly preserved or with headspace)
Sample(s) were received incorrect)
b addin y preserved and were adjusted accordingly
Y g(circle one): H2504 HNO3 HC1 NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s} were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

6602
dmill Way
mington,NC
__ ENVIRONMENTAL CHEMISTS, INC OFFICE:n914-3924z 311FAX[phone]
[e-mail]
DWQ CERTIFICATION#94 NCDHHS:DLS CERTIFICATION#37729 info rrt
Analytical&Consulting Chemists @
COLLECTION AND CHAIN OF CUSTODY
Client: Lewis Farms& Liquid Waste PROJECT NAME: REPORT NO: 2.4 L( — it 9 3.-
ADDRESS: CONTACT NAME: Wesley Wooten PO NO:
REPORT TO: Martin Mabe!Mabe-Wilcox PHONE/FAX:
COPY TO: email:
Sampled By: W6,11 (ALA-- SAMPLE TYPE:I=Influent, E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge,Other:
Collection � PRESERVATION
q m .D J7 C C7 C .J ❑ In I I
Sample Identification �n I `o iz .'a L E m j z u g o 6 o w ANALYSIS REQUESTED
Date Time Temp " r z _ z o
tilt f 2 7� C P
Sludge G G U
5a� X Full TCLP, RCI, utrients/Metals
I3i C P
1 G G 4-
414‘7 X _ Fecal Density/%TS
$s4- C P
G G
P S'1 � X Fecal Density/%TS%s= C
3
G G cqc34(
X Fecal Density/%TS
``, C P -
4 - ' G G `(�41. X Fecal Density/%TS -
C P
5 _ G G 3"t5� X Fecal Density/%TS
4w� C P c,-I�
6 } C P �� A X Fecal Density/%TS
7 6-`M
G _ G X Fecal ❑ensity/%TS
Transfer Relinquished By: DatefTime Received By: Date/Time
1.
2. v ,,----
Temperature when Received: 5 Accepted: Rejected: Resample Requested:
Delivered By: Received By: � � Date: Time: 3 4 ,41—
Comments: TURNAROUND: ( `

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Coastal Farms and Residuals, LLC WQ Permit Number: WQ0034806
WWTP Name: The Cape WWTP NPDES Number: NC0057703
Monitoring Period: Front 1i 1/7f12 1 To 17/31/7f17 i
Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
CIas A: Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment)❑ FAR C (Prior Testing)❑
AIM(Nu Prior Test) ❑ Process to Further Reduce Pathogengs ❑
if applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying U Heat Treatment ❑ Thennophitic ❑ J
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ I
Class B: It. 1 Fecal Densit Alt. 2 Process to Si ihcantiv Reduce Patho ens ❑
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ I Air Drying ❑ Conlpostrng ❑ Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter Allowable Level Pathogen Density fN"ie `Frequency Sample n
Excee- Tech-
in Sludge iGeo. Meanlvlaximurr Units Ap,, of Analysis Type matte
2 z 10 to the MPN 23,334 56,563 111,112 MPN/g 0 Annual Grab ti192210E
6th power
per gram of Fecal Califotm total solids CFU
1000 mpn per gram
aftotai solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams v
(in lieu of fecal total solid(dry
califonn) weight)
Vector Attraction Reduction (15A NCAC 02T.1107)-Please indicate alter ve performed:
Alt.I (VS reduction) ❑ Att.2(40-day bench) ❑ Alt. 3(30-day bench) 0 [Alt. 4(Spec. 0,uptake) Es
Alt.5(14-Day Aerobic) ❑ Alt. 6(Alk Stabilization ❑ Alt 7(Drying-Stable) ❑ [Alt.8(Drying-Unstable) ❑
Alt.9(Injection) tEl Alt. 10(Incorporation) p No vector attraction reduction alternatives v6ere performed ❑
CERTIFICATION STATEMENT(please check the appropriate statement)
El "I certify, under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in I5A NCAC 02T.1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Cole Price, ORC Wesley Wooten,President
Preparer Name and itle(type or print) Land Applier Name and Title(if applicable)(type or print)
2'72 2 1/17/21
Signature of Preparer* Date Signature of Lan ApN1i,,1 kin applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and ISA NCAC 2T .1102(26)
DENR FORM PVRF 02T(12/2006)

COASTAL FARMS
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 18,2021
Morehead City Permit No.NC0026611
16.60 %Solids
6.88 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 6.170 61,700.000 123.400
Phosphorus 3.250 _ 32,500.000 65.000
Potassium 0.458 4,580.000 9.160
PAN(injected)* 1.851 3,869.500 7.739
PAN(surface)* 1.851 3,777.000 7.554
Ammonia Nitrogen 0.000 0.602 0.001
Calcium 3.050 _ 30,500.000 61.000
Calcium Carbonate Eq. --- --- _-
Magnesium 0.366 3,660.000 7.320_
Sodium 0.257 2,570.000 5.140
Sulfur ___ --- ---
Nitrate N/Nitrite N --- 2.160 _ 0.004
Barium --- --- --- _ SAR
Chloride --- --- --- 1.51
Iron ___ --- Ceiling Concen.
Aluminum --- 8,670.00 17.340 (Mg/Kg)
Arsenic --- 10.50 0.021 75
Cadmium --- 3.68 _ 0.007 85
Chromium --- 15.500 --- --
Copper --- 741.00 1.482 4,300
Lead --- 15.40 0.031 840
Mercury --- 0.822 0.002 57
Molybdenum --- 4.64 0.009 75
Nickel --- 11.50 0.023 420
Selenium --- 6.69 0.013 100
Zinc --- 904.00 1.808 7,500
Environmental Chemists,Inc. 2021-04594
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits arc listed as detection limits
For calculation purposes.

COASTAL FARMS AND RESIDUALS, LLC
WQ0034806
Morehead City WWTP
late1 €Fe
perga ' !i` ] €` € °
03/18/21 5,255 3.7206
03/18/21 1,765 3.2467
03/18/21 2,634 3.4206
03/18/21 240 2.3802
03/18/21 5,833 3.7659
03/18/21 12,940 4.1119
03/18/21 1,375 3.1383
Total 23.7843
Average 3.3978
Geometric Mean 4} s €= Fecal Coliform MPN/gram
Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction
requirement.

, ' ` AW,, Environmental Chemists, Inca
„ er1vi.lQ�ch 'rn� . 6602 Windmill Way,Wilmington,NC 28405 a 910.392.0223 Lab • 910.392.4424 Fax
- '' 4T `*r� 0t. =`'S-' ,:r.r. 710 8owsertown Road,Manteo NC 27954 • 252.473.5702 Lab/Fax
rs'�r 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Town Of Morehead City Revised Report: May 14, 2021
706 Arendell Street Original Report Date: Apr 14, 2021
Morehead City NC 26557 Report#: 2021-04594
Attention: Nate Johnson Customer ID: 09020011
Project ID: Sludge
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
21-11319 Site: Sludge 3/18/2021 10:30 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
CCE AOAC 1.005 <1 % 05/05/2021
Chlordane(TCLP) SW 846 Method 8081B13510 <0.02 mg/L 03/29/2021
Endrin (TCLP) SW 846 Method 8081B/3510 <0,0005 mglL 03/29/2021
Heptachlor(TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 03/29/2021
Heptachlor epoxide (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 03/29/2021
Lindene(TCLP) SW 846 Method 80818/3510 <0.0005 mglL 03/29/2021
Methoxychlor(TCLP) SW 846 Method 80816/3510 <0.0005 mgfL 03/29/2021
Toxaphene (TCLP) SW 846 Method 8081B/3510 <0.05 mg/L 03/29/2021
1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/30/2021
2,4,5-Trichlorophenol(TCLP) SW 846 method 8270/3510 <0.050 mglL 03/30/2021
2,4,6-Trichlorophenol(TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/30/2021
2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/30/2021
Cresol (TCLP) SW 846 method 8270/3510 <0.050 mglL 03/30/2021
Hexachloro-1,3-butadiene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/30/2021
Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/30/2021
Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/30/2021
m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/30/2021
Nitrobenzene (TCLP) SW 848 method 8270/3510 <0.050 mg/L 03/30/2021
o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/30/2021
Pentachlorophenol (TCLP) SW 646 method 8270/3510 <0.250 mg/L 03/30/2021
Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 03/30/2021
Paint Filter Test SW 846 Method 9095 A Pass 04/14/2021
2,4,5-TP (TCLP) SW846 Method 8151A <0.003 rng/L 03/28/2021
2,4-D (TCLP) SW846 Method 8151A <0,003 mg/L 03/28/2021
1,1-Dichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2021
1,2-Dichloroethane (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2021
Report#. 2021-04594 Page 1 or 5

zvAi
Y.t,� ,',F'r `N. ,;. � Environmental Chemists, Inca
`,4e•I1irt'§lkrlic 7.e 6602 Windmill Way,Wilmington,NC 28405 • 910-392.0223 Lab • 910.392 4424 Fax
'£-t '• 4'�#2 ,F ' '' C,',r' ` 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
':',; - ' . ,h+ 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoOenvironmentalchemists.com
Town Of Morehead City Revised Report: May 14, 2021
706 Arendell Street Original Report Date: Apr 14, 2021
Morehead City NC 28557 Report#: 2021-04594
Attention: Nate Johnson Customer ID: 09020011
Project ID: Sludge
Benzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2021
Carbon Tetrachloride(TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2021
Chlorobenzene (TCLP) 5W846 Method 8260/5030 <0.01 mg/L 03/25/2021
Chloroform (TCLP) SW846 Method 6260/5030 <0.01 mg/L 03/25/2021
Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 03/25/2021
Tetrachloroethylene(TCLP) 5W646 Method 8260/5030 <0.01 mg/L 03/25/2021
Trichioroethylene(TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2021
Vinyl Chloride(TCLP) SW846 Method 8260/5030 <0.01 mg/L 03/25/2021
RCl
Ignitability EPA 1030 <0.8mm/sec 04/05/2021
Cyanide SM 4500 CN D 2.10 mg/kg 03/25/2021
Sulfide SM 4500 S o 0,50 mg/kg 03/30/2021
Sludge Residuals
Aluminum EPA 200.7 8670 mg/kg 03/22/2021
Arsenic EPA 200.7 10.5 mg/kg 03/22/2021
Cadmium EPA 200,7 <3.68 mg/kg 03/22/2021
Calcium EPA 200.7 30500 mg/kg 03/22/2021
Chromium EPA 200,7 15.5 mg/kg 03/22/2021
Copper EPA 200.7 741 mg/kg 03/22/2021
Lead EPA 200.7 15.4 mg/kg 03/22/2021
Magnesium EPA 200.7 3660 mg/kg 03/22/2021
Molybdenum EPA 200.7 4.64 mg/kg 03/22/2021
Nickel EPA 200.7 11.5 mg/kg 03/22/2021
Potassium EPA 200.7 4580 mg/kg 03/22/2021
Selenium EPA 200.7 6,69mg/kg 03/22/2021
Sodium EPA 200.7 2570 mg/kg 03/22/2021
Zinc EPA 200.7 904 mg/kg 03/22/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 2.16 mg/kg 03/22/2021
Total Solids (%) SM 2540 a 16.6% 03/19/2021
Report/1:: 2021-04594
Page 2 of 5

e, Y-k,•ryi�` Environmental Chemists, Inc.
r
`,' �' ;Y VlY'1OIC;h ', 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4-424 Fax
n� 6 :<3 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
s WS.1 . 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS inforieenvironnlentalchemists.com
Town Of Morehead City Revised Report: May 14, 2021
706 Arendell Street Original Report Date: Apr 14, 2021
Morehead City NC 28557 Report#: 2021-04594
Attention: Nate Johnson Customer ID: 09020011
Project ID: Sludge
Ammonia Nitrogen SM 4500 NH3 C <0.602 mg/kg 03/22/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 61700 mg/kg 03/22/2021
Total Phosphorus SM 4500 P F 32500 mg/kg 03/26/2021
pH SW 846 Method 9045D 6.88 units 04/05/2021
Mercury SW846 7471E 0.8220 mg/kg 03/22/2021
TCLP Metals
Arsenic EPA 200.7 <1.0 mg/L 03/29/2021
Barium EPA 200.7 <1.0 mg/L 03/29/2021
Cadmium EPA 200.7 <1.0 mg/L 03/29/2021
Chromium EPA 200.7 <1.0 mg/L 03/29/2021
Lead EPA 200.7 <1.0 mg/L 03/29/2021
Selenium EPA 200.7 <1.0 mg/L 03/29/2021
Silver EPA 200.7 <1.0 mg/L 03/29/2021
Mercury EPA 245.1 <0.0002mg/L 03/30/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11320 Site: 1 3/18/2021 10:31 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 24.7% 03/19/2021
Fecal Density SM 9221 C E MPN 24 hr 503 5255 MPN/g 03/18/2021
Lab ID Sample ID: Collect DateiTime Matrix Sampled by
21-11321 Site:2 3/18/2021 10:32 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 17.6% 03/19/2021
Fecal Density SM 9221C E MPN 24 hr 503 1765 MPN/g 03/18/2021
Report 4:: 2021-04594
Page 3 of 5

t�5�9'7,�
4; Environmental Chemists, Inc.
° F 0 -f: 6602 Windmill Way,Wilmington,NC 28405 ° 910.392.0223 Lab • 910.392.4424 Fax
,z ,.:'r 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Pax
d��' �;��"`��tS'.+x,��{�Y."mod" SM�
255-A Wilmington Highway,Jacksonville,NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Town Of Morehead City Revised Report: May 14, 2021
706 Arendell Street Original Report Date: Apr 14,2021
Morehead City NC 28557 Report#: 2021-04594
Attention: Nate Johnson Customer ID: 09020011
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11322 Site: 3 3/18/2021 10:33 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) 5M 2540 6 17,5% 03/19/2021
Fecal Density SM 9221C E MPN 24 hr 503 2634 MPN/g 03/18/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11323 Site:4 3/18/2021 10:34 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) sM 2540 a 18.8% 03/19/2021
Fecal Density SM 9221C E MPN 24 hr503 240 MPN/g 03/18/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11324 Site: 5 3/18/2021 10:35 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 18.9% 03/19/2021
Fecal Density SM 9221C E MPN 24 hr 503 5833 MPN/g 03/18/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11325 Site:6 3/18/2021 10:36 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids (%) SM 2540 t3 16,2% 03/19/2021
Fecal Density SM 9221C E MPN 24 hr503 12940 MPN/g 03/18/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-11326 Site: 7 3/18/2021 10:37 AM Solid/Sludge Nate Johnson
Test Method Results Date Analyzed
Total Solids(%) SM 2540 6 16.0% 03/19/2021
Fecal Density SM 9221C E MPN 24 hr 503 1375 MPN/g 03/18/2021
Report#:: 2021.04594
Page 4 of 5

Environmental Chemists, Inc®
*17,00Nt u`_r 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax
�a s '`sM. 710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
. ;a.r +a i 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Town Of Morehead City Revised Report: May 14, 2021
706 Arendell Street Original Report Date: Apr 14, 2021
Morehead City NC 28557 Report#: 2021-04594
Attention: Nate Johnson Customer ID: 09020011
Project ID: Sludge
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Revised
to add CCE per client.
Reviewed by: rz..i.CD .natODALLS,LEDI
Report#:, 2021-04594
Page 5of5

Environmental Chemist, Inc., Wilmington, NC Lab#94
6642 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Clientkb 1-QC/1--)1 NM' Date: 3h 3 c l Report Number: / —0 Y5 q kt
Receipt of sample: ECHEM Pickup Client Delivery 0 UPS 0 FedEx 0 Other 0
YES ❑ NOlig-
121N/A 1. Were custody seals present on the cooler?
❑ YES l❑ NO N/A 2. If custody seals were present,were
they intact/unbroken?
Original temperature upon receipt f e °C Corrected temperature upon receipt °C
How temperature taken: 0 Temperature Blank 0 Against Bottles
IR Gun ID:Thomas Traceable S/N 192511657 IR Gun Correction Factor°C:0.0
❑ YES 0 NO 3. if temperature of cooler exceeded 6"C,was Project Mgr./QA notified?
'i YES ❑ NO 4. Were proper custody procedures(relinquished/received)followed?
II YES 0 NO 5. Were sample ID's listed on the COC?
II YES ❑ NO 6. Were samples ID's listed on sample containers?
ra YES ❑ NO 7. Were collection date and time listed on the COC?
is YES ❑ NO 8. Were tests to be performed listed on the COC?
H YES 0 NO 9. Did samples arrive in proper containers for each test?
is YES _ 0 NO 10. Did samples arrive in good condition for each test?
i1 YES 0 NO 11. Was adequate sample volume available?'
►; YES 0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH>12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH>9?
G YES ❑ NO 16. Were NH3/TKN/phenol received at a chlorine residual of<0.5 m/L? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within I5 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(sj incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding(circle one): H2504 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for Incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s) _were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(503 Rules)
Facility Name: Coastal Farms and Residuals,LLC WQ Permit Number: WQ0034806
1 WWTP Name: Town of Morehead City NPDES Number: NC00266i 1
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (40 CFR 503.32) -Please indicate level achieved and alternative performed:
Class A: Alternative I 0 Alternative 2 ❑ Alternative 3 0
Alternative 4 0 Alternative 5 0 Alternative 6 0
If applicable to alternative performed(Class A only)indicate"Process to Farther Reduce Pathogens":
Compost 0 Heat Drying 0 Heat Treatment ❑ Thenxnophilic 0
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: _ Alternative 1 Cl I Alternative 2 ❑
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying❑ Composting 0 !Aerobic Digestion ❑
,Anaerobic Digestion ❑ —
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable LevelL Pathogen DensityNumber of AnaIyucat
Parameter g Excee- Frequency Sample
Tech-
in Sludge Minimum ime
Geo.Mean Maximus-\ Units deuces of Analysis Type T
2 x I0 to the i��te
6th powerMPN 240 2,499 12,940 MPN/g 0 Annual Grab sm 927 ICE
per gram of
Feca[Coliform total solids CFU
t000 mpn per gram t
of total solid (dry '
_ weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliForrn) weight) I
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction) ❑ Alt. 2(40-day bench) ❑ Alt. 3(30-day bench) 0 Alt.4(Spec. 02 uptake)
Alt. 5 (14-Day Aerobic) ❑ Alt. 6(Alk.Stabilization ❑ Alt 7(Drying-Stable) 0 Alt.S(Drying- Unstable) ❑-
Alt. 9(Injection) ❑ Alt. 10(Incorporation) 0 No vector attraction reduction alternatives were performed LI
CERTIFICATION STATEMENT(please check the appropriate statement)
Cl "I certify,under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law,that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including tine and imprisonment."
Chad Sutton, WWTP Superintendent Wesley Wooten, President
Preparer Name and Title
,('type or int) Land Applier Name and Title(if applicabie)(t'pe or print)
1. �� 66% — i/17131
Signature of Preparer* Date Signature of La Applier(if applicable) Date
4'Preparc;r is defined in 40 CFR Part 503.9(r)and I iA NCAC 2T .1102(261

2021 APPLICATION SUMMARY

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-I CPC-2 CB-I CB-2 CFC-1 CFC-2 AS-1 WC-I Total Gallons
NET ACRES 13.90 2I.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40
CROP Com/Wheat Com/Wheat Corn/Wheat Com/Wheat Corn/Wheat Corn/Wheat Corn/Wheat Corn/Wheat Com/Wheat Corn/Wheat Corn/Wheat Bermuda/Rye
Source:
Avondale 96,000
Carolina Beach 630,500 591,500
Oak Island 318,500
Lear Corporation 1,001,000
Northwest Regional 396,500
Pluris Hampstead 643,500
Pluris North Topsail 221,000
R _
Southeast Brunswick SD 416,000
Summerhouse 909,500
Surf City 1,306,500
Swansboro 195,000
The Cape 1,313,500
Total 96,000 318,500 - - 1,001,000 1 416,000 - - 1,501,500 630,500 - 3,575,500 7,539,000
FIELD NO. AW-t AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-1 CB-1 CFC-I CFC-2 AS-1 WC-I Total
NET ACRES 13.90 21.50 16.90 5.90 71.80 55.40 I1.80 11.80 81.90 72.80 70.20 93.40
CROP Corn/Wheat Com/Wheat Corn/Wheat Corn/Wheat Corn/Wheat Corn/Wheat Corn/Wheat Corn/Wheat Coastal/Rye Coastal/Rye Coastal/Rye Bermuda/Rye
Morehead City 283.2 Wet Tons
Total - - - - - - - - - - - 283.2 283.2 I

FIELD APPLICATION SUMMARIES

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Avendale
FIELD NO. AW-I AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-1 CB-2 CRC-1 CFC-2 AS-1 WC-1 Total
NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons
SITE Woolen Wooten Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Farming Sidbury W.Corbett
I
January 12,000
12,000
February -
March 12,000 12,000
April -
May 28,000 28,000
-
June
July 16,000 16,000
August -
September -
October 12,000 v
12,000
- -
November -
December 16,000 '
Total 96,000 - - - - - - - - - - - 96,00J
Soybeans
Corn 56,000 0 0 0 0 0 0 0
Wheal 40,000 0 0 0 0 0 0 0
Rye 0 0 0 0
Bermuda _ 0 0 0 0 96,000

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Town or Carolina Beach WWTP
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-I CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-1 WC-1 Total
NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons
SITE Wooten Wooten Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Fanning Sidbury W.Corbett
January -
February
-
March
April -
May
June 377,000 377,000
July 71,500 71,500
August 97,500 97,500
`September
45,500 45,500
October 260,000 260,000
November 253,500 253,500
December 117,000 117,000
Total - - - - - - - - - 630,500 - 591,500 1,222,000 I
Soybeans
Corn 0 0 0 0 0 0 0 0
Wheat 0 0 0 0 0 0 0 0
Rye I 0 370,500 0 0
Bermuda 0 260,000 0 591,500 1,222,000I

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Town of Oak Island WWTP
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-1 WC-1 Total
NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons
SITE Wooten Wooten Woolen Woolen Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Farming Sidbury W.Corbett
i
January 91,000 91,000
-
February
March
-
-
April
-
May
June
July
-
August 136,500 J 136,500
September
-
October 91,000 91,000
November
-
December
-
Total - 318,500 - - - - - - - - - - 318,500I
Soybeans JJ
Corn 0 136,500 0 0 0 0 0 0
Wheat 0 182,000 0 0 0 0 0 0
Rye 0 0 0 0
Bermuda 0 0 0 0 3I8,500I

Coastal Farms and Residuals,LUC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Lear Corporation WWTP
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 C3-1 CB-2 CFC-1 CFC-2 AS-I WC-1 Total
NET ACRES I3.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons
SITE Wooten Wooten Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Farming Sidbury W.Corbett
January
February
-
March 442,000 442,000
April 559,000
559,000
May
-
June
July
-
August
-
September
-
•
October
-
November
December
Total - 1,001,000 - - - - - - -
1,001,000
Soybeans
Corn 0 0 0 0 1,001,000 0 0 0
Wheat 0 0 0 0 0 0 0 0
—
Rye 0 0 0 0
Bermuda 0 0 0 0 1,001,000 I

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Morehead City WWTF
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-1 WC-1 Total
NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Wet Tons
SITE Wooten Wooten Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Farming Sidbury W.Corbett
-
January
February
March
-
-
April
May 82,6 82.6
June
-
-
July
August
-
September
October
-
November 200.6 200.6
December
-
Total - - I - - - 283.2 283.2I
I
Soybeans
Corn 0 0 0 0 0 0 0 0
Wheat 0 0 0 0 0 0 0 0
Rye 0 0 0 200.6
Bermuda 0 0 0 82.6 r 283.2J

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Northwest Regional WWTF
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-I CPC-2 CB-1 CB-2 CFC-I CFC-2 AS-1 WC-1 Total
NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons
SITE Wooten Wooten Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Farming Sidbury W.Corbett
-
January
-
February
March
-
April
May 84,500 84,500
June 312,000 312,000
July
-
August
September
-
October
-
November
-
December
Total - - - - - - - - - - 396,500 396,500I
I
Soybeans
Corn 0 0 0 0 0 0 0 0
Wheat 0 0 0 0 0 0 D I 0
Rye 0 0 0 0
Bermuda 0 0 0 396,500 396,500 1

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Pluris Hampstead WWTP
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-I CPC-2 CB-1 CB-2 CFC-I CFC-2 AS-1 WC-I Total
NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons
SITE Wooten Wooten Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Farming Sidbury W.Corbett
January 26,000 26,000
February 97,500 97,500
March 52,000 52,000
April 78,000 78,000
May 26,000 26,000
June 39,000 39,000
July 39,000 39,000
August _ 71,500 71,500
September 52,000 52,000
October 26,000 26,000
November 45,500 45,500
December 91,000 91,000
Total - - - - - - - - - - 643,500 643,500
Soybeans
Corn 0 0 0 0 0 0 0 0
Wheat 0 0 0 0 0 0 0 0
Rye 0 0 0 260,000
Bermuda 0 0 0 383,500 643,500

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Pluris-North Topsail WWTF
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-I CB-2 CFC-1 CFC-2 AS-1 WC-1 Total
NET ACRES 13.90 2I.50 16,90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons
SITE Wooten Wooten Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Farming Sidbury W.Corbett
-
January
-
February
March
April
May
-
June
-
July
-
August 78,000 78,000
September 58,500 58,500
October
November 84,500 84,500
December
-
Total - - - - - - - - - - - 221,000 221,000I
Soybeans
Corn 0 0 0 0 0 0 0 0
Wheat 0 0 0 0 0 0 0 0
Rye 0 0 0 84,500
Bermuda 0 0 0 136,500 221,000I

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Southeast Brunswick Sanitary District
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-1 CB-2 CFC-I CFC-2 AS-1 WC-1 Total
NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons
SITE Wooten Wooten Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Farming Sidbury W.Corbett
January
-
February 65,000 65,000
March
_..._.................-..._ 58,500 58,500
-
April
May 65,000 65,000
June 71,500 71,500
July
-
August
September 97,500
97,500
October
-
November 58,500 58,500
December
-
Total 416,000 r
416,000 1
-
-
-
Soybeans 1
Corn 0 0 0 0 0 292,500 0 0
Wheat 0 0 0 0 0 123,500 0 0
Rye 0 0 0 0
Bermuda 0 0 0 0 416,000 I

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Summerhouse
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-1 WC-1 Total
NET ACRES 13.90 21.50 16,90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons
SITE Wooten Woolen Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Fanning Corbett Farming Sidbury W.Corbett
-
January
February 39,000 39,000
March _ 26,000 26,000
April 52,000 52,000
May
June
-
July
-
August _ 78,000 78,000
September 78,000 78,000
October 58,500 58,500
November _ 78,000 78,000
December
Total - - - - - - - - - - - 409,500 409,500I
Soybeans
Corn 0 0 0 0 0 0 0 0
-
Wheat 0 0 0 0 0 0 0 0
Rye 0 0 0 117,000
Bermuda 0 0 0 292,500 409,500I

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Surf City
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-I WC-1 Total
NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 8I.90 72.80 70.20 93.40 Gallons
SITE Wooten Wooten Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Farming Sidbury W.Corbett
January 1 208,000 208,000
-
February
March
175,500 175,500
-
April
May
June 227,500 227,500
July 234,000 J 234,000
August 227,500 227,500
September
-
October
234,004 234,000
November
-
December
-
-
Total - - - - -
- 1,306,500 - - - 1,306,500 I
Soybeans
Corn 0 0 0 0 0 0 0 0
Wheat 0 0 0 0 0 0 0 0
Rye 208,000 0 0 0
Bermuda 1,098,500 0 0 0 1,306,500 I

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: Swansboro
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-I CB-2 CFC-1 CFC-2 AS-I WC-1 Total
NET ACRES I3.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons
SITE Woolen Woolen Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Farming Sidbury W.Corbett
January -
February -
March
April 195,000 195,000
May -
-
June
July -
August -
September -
-
October
-
November
-
December
Total - - - 195,000 - 195,000
Soybeans
Corn 0 0 0 0 0 0 0 0
Wheat 0 0 0 0 0 0 0 0
Rye 0 0 0 0
Bermuda 195,000 0 0 0 195,000I

Coastal Farms and Residuals,LLC
Permit#WQ0034806
2021 Field Application Summary
SOURCE: The Cape
FIELD NO. AW-1 AW-2 AW-3 AW-4 CPC-1 CPC-2 CB-1 CB-2 CFC-1 CFC-2 AS-1 WC-1 Total
NET ACRES 13.90 21.50 16.90 23.40 68.80 55.40 11.80 15.00 81.90 72.80 70.20 93.40 Gallons
SITE Wooten Woolen Wooten Wooten Corbett Packing Corbett Packing Corbett Brothers Corbett Brothers Corbett Farming Corbett Farming Sidbury W.Corbett
January 91,000 91,000
February 117,000 117,000
March 178,500 178,500
April 105,500 I05,500
May 74,500 74,500
June _ 189,000 189,000
July 181,000 181,000
August 97,500 97,500
September 97,500 97,500
October 39,000 39,000
November 130,000 130,000
December 13,000 13,000
-
-
Total - - - - - 1,313,500 1,313,500 I
Soybeans
Corn 0 0 0 0 0 0 0 0
Wheal 0 0 0 0 0 0 0 0
Rye _ 0 0 0 351,000
Bemruda 0 0 0 962,500 1,313,500

FIELD LOADING RATE REPORTS

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Coastal Forms and Rcsidunls WQ Permit N WQ0034806 Field N 1 Acres Utilized: 13.9
Land Owner: Allan Woolen Annual DT's Applied: 10.13 Site M: AW Acres Permitted: 13.9
Operator: Allen Wooten Predominant Soil Series: Norfolk-NIA Cation Exchange Capacity(non 503):
Crop 1 Name: Corn Crop 1 Max.PAN: 131 Crop 2 Name; Wheat Crop 2 Max.PAN: 50
Application Method: S-Surface/I-Injected Volatilization Rate:Surface-0.5/Injected or Incorporated-1.0
-•sf.:• E c dii'lfli:i:Si rY _:i :lii•i .. 7::::�.S1..rt„ i;i4t4hii4 G'ir"
.1t.iCdfS:: I]s,C� :::,
:Ei�ltfE •.... EfaF
RfFCI'.E:E::Ei...
Coh11i' is• ._ . 3
;:N113-�i!i1-143
2021 96,000 6,906 2.53 0.73 AY.adule WWVP my 0.045 0.045 0.128 0.045_0.001 0.045 0.045 0.045 3.017 24.03 17.17 45.03 Corn Wheat 112.36 10.70 0.01
Total 96,000
Annuallhs/acrc 0.045 0.045 0.128 0.045 0.001 0.045 0.045 0.045 3.017 24.03 17.I7 45.03 LimeApp.
Current Cumulative lis/acre 0.33 0.28 13.10 0.41 0.03 0.28 0.39 0.28 17.30 131 50 Permit PAN Limt 1st/2nd Crop Date Lbs/Ac
Prior Years Cumulative lbslacre 0.29 0.23 12.97 0.37 0.03 0.23 0.35 0.23 14.28
Permit'C.P.L.R.*•* 36 34 1,33R 267 15 ate 374 89 2,498
"I certify,under penalty allow,that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted.]am aware that there are
significant penalties for submitting false information,Including the passibility of fines and imprisonment for knowing violations.'
X I/25/22 *Application Method:S-Surface,IN-Injection,!NC-Incorporation
(Signature of Lan Applier) Date **Volatilization Rate:Surface-0.5,Injection/incorporation-1.0
***C.P.L.R.:Cumulative Pollutant Loading Rote
Bold denotes application that was Injected or Incorporated
WMSS,PLLC
DENR FORM FSF(12/2006)Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Cousin!Farms and Residuals WQ Permit* {VQ0034806 Field N 2 Acres Utilized: 21.5
Land Owner Allen Wooten Annual DT's Applied: 27.49 Site 8: AW Acres Permuted: 21.5
Operator: Allen Wooten Predominant Soil Series: Norfolk-NoA Cation Exchange Capacity(non 503):
Crop 1 Name: Corn Crap 1 Max.PAN: 131 Crop 2 Name: Wheat Crop 2 Max.PAN: 50
Application Method: S-Surface/I-Injected Volatilization Rate:Surfnce-0.5/Injected or Incorporated-1.0
.tY:l'.sR.....e.-..€1f0.:010-101 Sect :.>SgQrals.�lllsfte ::•l
:tTllile..
:.-.��-'AEo:aunt°t[C:i i`i tI'SeE iiAc3Fh;ii;:g-:•:�c.: :'-:-'. ",•.f.-..::°::°`:°':°`''°`.....
4 . . .. k l �,..�£dn0 :i�iS::iiiCil: = rt e t;:YG;i i eII E i?j410` i[�Ij ti SCii' i it Sit::I'itili]e Ifillil i i iC`-iiL'fDp3::`•Ehl4';::�r1F13 Fi3ei!73
Uek sl.nd
2021 318,500 14,814 2.07 1.28 tw., Dry 0.070 0.035 0.611 0.035 0.003 0.035 0.035 0.035 3.248 15.78 21.05 13.58 5l.66 30.43 0.03
Total 318.500
Animallbslocre 0.070 0.035 0.611 0.035 0.003 0.035 0.035 0.035 3.248 15.78 21.05 13.58 Lime App.
Current Cumulative Ibslnrro 0.17 0.12 4.55 0.16 0.01 0.12 0.15 0.12 8.02 131 50 Permit PAN Limt 1st/2nd Crop Date Lbs1Ac
Prior Years Cumulative Ibslarre 0.10 0.09 s 3.94 0.13 0.01 0.09 0.I2 0.09 4.77
Permit!C.P.I.,R.••• 36 34 1,338 267 15 n/a 374 89 2,498
"I certify,under penalty of law,that Ibis document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted,1 am aware that there arc
significant penalties for submitting false information,Including the possibility alines and imprisonment for knowing violations."
k lf/'✓it Irz5/22 'Application Method:S-Surface,IN-Injection,INC-Incorporation
(Signs re of L d Applicr) Date ',Volatilization Rate:Surface-0.5In-ectionitnca oration-
, J rP 1.0
••'C.P.L.R.:Cumulative Pollutant Loading Rate
Bold denotes application that was Injected or Incorporated
WMSS,PLLC
DENR FORM FSF(1212006)Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Coastal Farms and Residuals WQ Permit N WQ0034806 Field N 1 Acres Utilized: 68,8
Land Owner:Corbett Package Annual DT's Applied: 178.65 Site N: CPC Acres Permitted: 68.8
Operator: Allen Wooten Predominant Soil Series: Norfolk-NoA Cation Exchange Capacity(nun 503):
Crop 1 Name: Corn Crop I Max.PAN:_ 131 Crop 2 Name: Wheat Crop 2 Max.PAN: 50
Application Method: S-Surface/I-Injected Volatilization Rate:Surrnce-a.S/Injected or Incorporated-1.0
:iiCxPTs:. .a..:D j 1. : C- iil�i=i: f•` _
:>:ivJetdise:rti5
EEhE'''
:::.ro-:..-
rC•..,., r}cra i autdagwrhatm. •Cilrtd ..•tt6.....L'd.�.•Cu:.;:.;7!b:.�Elg,::;:hlo:••-NE:.::•:5E.:y.:;:$u:i: E'a1r5i:1: 1'r(iYi1:. Elp tLR>tile jCrsb�i2 i:i li; I+1 13E:1V2 $
2021 1.001,000 14.549 4.28 2.60 t yn, G/D 0.082 0.053 0.326 0.053 0.002 0.053 0.053 0.053 1.418 75.87 93.48 Com 204.62 20.67 0.01
_ t
Tolol NNNdNNII
Annual lbslncre 0.082 0.053 0.326,0.053 0.002 0.053 0.053,0.053 1.418 75.87 0,00 93.48 , Lime App.,
Current Cumulative lbsloere 0.08 0.05 0.33 0.05 0.00 0.05 0.05 0.05 1A2 I31 50 Permit PAN Limt tstl2nd Crop Date Lbs/Ac
Prior Years Cumulative lbslncre 0.00 0.00 0.00 0.00 0.00 0.0D _0.00 0.00 0.00
Permilt C.P.L.R••• 36 34 4338 267 15 n/a 374 89 2,498
"I ecrlify,under penalty of taw,that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am aware that There are
significant penalties far submitting false information,Including the possibility of fines and imprisonment for knowing violations."
X I/25122 'Application Method:S-Surface,IN-Injection,INC-Incorporation
(Signature of td Applier) Date "Volatilization Rate:Surface-0.5.
. ,Injection/Incorporation-1.0
***C.P.L.R.:Cumulative Pollutant Loading Rale
WMSS,PLLC
DENR FORM FSF(12/2006)Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Coastal Forms and Residuals WQ Permit H W00034806 Field 8 2 Acres Utilized: 55A
Land Owner:Corbett Package Annual DT's Applied: 58.98 Site#: CPC Acres Permitted: 55.4
Operator: Allen Wooten Predominant Soil Series: Norfolk-NoA Cation Exchange Capacity(non 503):
Crop 1 Name: Corn _ Crop I Max.PAN: 131 Crop 2 Name: Wheat Crop 2 Max.PAN: 50
Application Method: S-Surface 11-Injected Volatilization Rate: Sairnce-0.5 laieetedorincorporated-1.0
:;...,.c:-::a•:a-:•:a.�:•��-ql.r.......n...x7,'I'�....-1#Cs�dtl:llEe6 EfS't�=:-"="�:io::::9:?:l::ei:::i:'i.''"'-: '•'.''::;:;:E:E:E:E::::::::::::::::::::::::=:::::':::::c -- • "-••" -: ::: .-..:-.:..•..,-.....::.'....-.." .. .......
..,}...................q 1dafS..IUS/a@}..,.,....-....:-:.;.:.:.:.>:.:.:-:.:o-:.:-.:.:-:::-{VlifhCnls!: �YS(de#:�:�:::::r:::e::•;:::•:•:•: ::•:-:.:-:.:: +":-::;:;:::;
..Ga[aii=:�i'Jl"L'"r!Nii E;E TS'i i'`"'"`.iE:E'OpPj°p°"0ii i':'°'''i.i:i'-':i i:i:'is:.:-.:":::::.''•::.::- .. ...r._.:...;;:•;'--
crif -- uarcosr.,.,..CflpU....kti..-..i tL;;..CU.:.k;:.T.L:. ;;E[�;E i EfVIoEE E:ENi?ii f i$e i iZtYE E` trAM11'IE cT'et1�FE :_EEiEP E:: ra{z?l: Cslili E iT3i]NE;lEt1'fi3:Ej� ��3
2021 416.000 7.509 3,40 I.06 �wrarwn
nnma„rk 0.00 0A55 0.044 0.530 0.044 0.001 0.044 0.044 0.044 1.716 29"69 12.54 4.83 Cam whoa 133.93 10.20 4A1
Total 4[6,000
Anaeml l6s/acre 0.055 0.044 0.530 0.044 0.001 0.044 0.044 0.044 1.716 29.69 12.54 4.83 Lime App.j
Current Cumulative Ibslncre 0.05 0.04 0.53 0.04 0.00 0.04 0.04 0.04 1.72 131 50 Permit PAN Limt Ist/2nd Crop Date Lbs1Ac
Prior Years Cumrslativc Ibslncre 0.00 _0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
Pernritt C.P.L.It.-"" 36 34 1,338 267 15 nla 374 89 2,498
"I certify,under penalty of law,that this document was prepared trader my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am aware that there are
significant penalties for submitting false information,Including the passibility of fines and imprisonment for knowing violations."
X N I/25/22 'Application Method:S-Surface,IN-Injection,INC-Incorporation
(Signature of Lan Applier) Date +
• Valaliliza[ien Rate:Surface-0.5,lnjecliotdbswrporation-1.0
'+'C.P,L,R.:Cumulative Pollutant Loading Rate
WMSS,PLLC
DENR FORM FSF(1212006)Mod.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Coastal Forms and Residuals 3VQ Permit l WQ0034806 Field N 1 Acres Utilized: 81.9
Land Owner:Corbett Farming Annual DT's Applied: 138.87 Site N: CFC Acres Permitted; 81.9
Operator: Allen Wooten_ Predominant Sail Series: Norfolk-NoA Cation Exchange Capacity(non 503):
Crop 1 Name:Coasts!Dermudr Crop I Max.PAN: 299 Crop 2 Name: Rye Crop 2 Max.PAN: 50
Application Method: S-Surface/1-injected Volatilization Rate:Snrfare•0.5/Injected or Ineorpornled-1.0
:i`iifyp `l: iti •i;i is !t?�ciiei "' :s:a•.•.•... ....:........
nj iE"
i&, -Eilliiei E TS! lciii i'
zl
.. _ .... .;E:ESditi!csii�": C.'riiftli:6�gEE cE�`-lfi` itiili: f.h:;:E#IgE ;:hlnE = 3Yiie e:�5�2a 2Ec�72k?F;"Sj!x1AE�i?PXi'e$ =E= :���;:
�.. .. .�. •,e`t 13:i �tiljiil `suji2 1'1243
2021 1.306.500 15,952 2.14 1.42 Surf Ci'Yww P Dry _0.087 0.087 1.122 0.087 0.002 0.087 0.087 0.087 9.823 40.70 7.70 63.78 Cmsul Rcc 153.17 _3.42 0.06
2021 195,000, 2.381 2,74 017 Swambmo G/D 0.020 0.010 0.124 0.010 0.000 0,010 0.010 0.010 2.024 10.75 12.19 cmrnl 30.47 2.23 0.05
Total #N8i8NNit
Annual lbslacre 0.107 0.097 1,246 0.097 0.002 0,097 0.097 0.097 11.847 51.45 7.70 75.96 Lime App.
Current Cumulative Ibslnere 0.11 0.10 1.25 0.10 0.00 0.10 0.10 0.10 11.85 299 50 Permit PAN Limt Ist/2nd Crop Dole Lbs/Ac
Prior'Mears Cmmarntivelbsracre 0-00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
Permfii C.P.LR.^"r 36 34 1,33E 267 IS oho , 374 89 2,498
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am aware that there are
significant penalties for submittingfalse information,Including the possibility of fines and imprisonment for knowing violations."
x / '+� I/25122 *Application Method:S-Surface,IN-Injection,INC-Incorporation
(Signature of id Applier) Dale "Volatilization Rate:Surface-0.5,Injection/Incorporation-1.0
'•'C.P•L.R.:Cumulative Pollutant Loading Rate
WMSS,RUCDENR FORM FSF(1212006)Mod.

ANNUAL LAND APPL1CATMIN FIELD SUMMARY FORM
Facility Name: Coastal Farms and Residuals WQ Permit H 31100034806 Field 8 2 Acres Utilized: 72.8
Land Owner:Corbett Farming Annual DT's Applied: 46.54 Site 8; CFC Acres Permitted: 72.8
Operator: Allen Wooten Predominant Soil Series: Goldsboro-GoA Cation Exchange Capacity(non 503):
Crop I Name:Coastal Bermndr Crop 1 Max,PAN: 299 Crop 2 Name: Rye Crop 2 Max.PAN: 50
Application Method: S-Surface I I-Injected Volatilization Rate:Surface-0.51 Injected ertncarporoted-t.0
:iOR(ii1S:: .a.. :U't d�.-.•1 a...a[- � _.*;sfdn :�Z
i€iiUlixifi3='Ilii:a=:.( 11
i : :S Iil+'s1a
�tii'ciEiEi;i
i1iiiE i 'diei iii t+r::
,..-. .. [ � hx ... [;'dd[ iiyCii---Cil':.9E? :�s:::: :E` .`
... .. 'Pb. .H '(4iui'`r3�i2:i E:ESitE`E xyr€ °ri ri ..-_. ,:.�r .. ... . ,. ... ,..�.. .��:;:} ,r �= �LnR:ii �bpa::'la.lui; �is a�u*a
l3[4 IM1l apC{I
2021 630,500 8,661 1.77_ 0.64 wwTP Dry 0.04 0.04 0.37 0.04 0.00 0.04 0.04 0.04 0A1 17,51 12.28 30.56 Costal R+v 93.46 2.49 0.00
Total 630,500
Annuallbslncre _0.038 0.038 0,372 0.038 0.001 0.038 0.038 0.038 0.409 17,51 12.28 30.56 LimeApp.
Current Cumulative laslncre 0.04 0.04 0.37 0.04 0.00 0.04 0.04 0.04 0.41 299 50 Permit PAN Limt 1stl2nd Crop Date Lbs/Ac
Prior Years Cam/alive Ibslncre 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0,00 0.00
J
PermiC.P.L.R,••• 36 34 1,338 267 I5 n/a 374 89 2,498
lt
t
'I certify,andcr penalty of law,that This document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am aware that there are
significant penalties for submitting false information,Including the possibility of fines and imprisonment for knowing violations."
X , t/f/// I/25/22 'Application Method:S-Surface,IN-Injection,INC-Incorporation
(Signature SI and plier) Date "Volatilization Rate;Surface-0.5 LaIn-ection/lnco oration-1.0
Lo m
'*'C.P.L.R.:Cumulative Pollutant ding Rate
DENR FORM FSF(1 212008)Mod.
WMSS,PLLC

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name: Coastal Farms and Residuals WQ Permit 1 WQ0034806 Field it 1 Acres Utilized: 93.4
Land Owner, Wilber Corbett Annual DT's Applied: 40111 Site WC _ Acres Permitted: 93.4
Operator: Allen Wooten Predominant Soil Series: Autryville-AuB Cation Exchange Capacity(non 503): 4.2
Crop I Name: Bermuda Crop 1 Max.PAN: 196 Crop 2 Name: Rycgrnss Crop 2 Max.PAN: 50
Application Method: S-Surface/1-Infected Volatilization Rate:Surrncc-0.5/Injected or Incorporated-1.0
E;::;SY I>ale �F rtos�s,l % b3 f:::: CSltlylll:i; !i$0i
:::' '::E ::::r �::: :..............: Rl
r,,,. . 11e.a...9 pe;:i:;,hhhQ .,rks.•.,. d,:>.:-CSr:-;•3'fi;.0.fa.3a;::;:I�e.:,.:9ti; :_:Zh:::;;:[?aLlrl:yi:I'11(42 :;::E:R::i::iCr6p }?E i?oaz2 i 7[C[5_i 1!!I]3 3N30 3
Cara{Iaa Beaerf
2021 591,500 6,333 1.77 0.47 ww'rr Dry 0.028 0.028 0.272 0.028 0.001 0.028 0,028 0.028 0.299 21.78 22.34 ['crowds 68.34 1.82 0.00
2021 283.2 3.03 16.60 0.50 Morehead Cy O/D 0.011, 0.004 0.746 0,016 0.001 0.005 0.012 0.007 0,910 1.14 2.76 32.72 Bermuda Rye 6I.11 0.00 0.00
Norrhweu
2021 396,500 4,245 3.80 0.67 aMinuelWRF O/D 0.035,0.017 0.451 0.028 0.001 0.017 0.017 0,017 1.177 15.86 41.71 Bermuda _49.11 1.60 0,01
Mori'Iram:mead
202I 643,500 6,890 _3,02 0.87 �1v-rp Dry 0.031 0.028 0,359 0.028 0.001 0.028 0.028 0.028 0.972 23.06 15.63 39.91 Bar ado Rye 121.64 3.11 0.02
Nor1,-roprail
2021 221,000 2.366 4.07 0.40 WWTF G/D 0.018 0.010 0,108 0.010 0,000 0.010 0.010 0.010 1.920 5.74 3.55 25.54 Bermuda Rye 30.92 0.00 0.01_
2021 405,500 4.384 0.70 0.13 summerhonn G/D 0.008 0.008 0.024 0,008 0.001 0.008 0.008 0.008 0.394 3.37 1.35 4.66 Bermuda Rye 14.79 0,39 0.01
2021 1,313,500 14,063 2.14 1.25 The Cane G/D 0.111 0.111 0.417 0.111 0.002 0.111 0.1I1 0.111 10.190 44.36 16.18 75.80 Banned, Rye 185.48 6.98 0.01
Total 3.575.783
Annuallbslacrc 0.241 0.206 2.376 0.228 0.007 0.207 0.214 0.209 15.862 115.31 39.47 242.68 L[meApp.
Current Cumulative lhslarre 1.34 1.18 34.17 1.80 0.06 1.19 1.55 1.26 115.72 I96 50 Permit PAN Limt lst/2nd Crop Date Lbs/Ac
Prior Year,Cumulative lbs/acre_1.10 0.98 31.80 1.57 0.06 0.98 1.34 1.06 99.86
Permit[C.P.L.R.•++ 36 34 1,338 267 15 n/a 374 89 2,498
"I certify,under penalty of law.that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am aware that there are
significant penalties for submitting false information,Including the possibility of fines and imprisonment for knowing violations."
X 1/25/22 °Application Method:S-Surface,IN-injection,INC-Incorporation
(Signature dF Cand plicr) Date **Volatilization R5te:Surface-0.5,Injection/Incorporation-1.0
r•°C.P.L.R.:Cumulative Pollutant Loading Rate
Bold denotes application that was injected or Incorporated
WMSS.PLLC
DENR FORM F5F(1212006)Mod.

SOIL ANALYSIS REPORTS

Page 1 of 1 >j A_0
Report No: 22-046-1055
Account No: 08361 \llapoint. N 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Advisor: Willcox&Mabe Soil Solutions,PLLC Client:Coastal Farms Farm:
7231 B.Summerfield Rd
Summerfield NC 27358 Date Received:02/15/2022
Date of Report:02/17/2022
Lab No Field 1D Sample ID Soil Class HM% W/V pH Ac P-1 K-I S-! Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-i CEC BS% Ca% Mg% ESP Na I
15710 AW1 MIN 6.4 0.6 77 48 23 25 0 0 100 100 115 6.9 91 76 11 0.9 0.1
15711 AW2 MIN 5.1 0.8 188 25 31 25 0 0 68 68 305 2.1 64 40 16 2.3 0
15712 AW3 MIN 5.2 0.6 183 25 31 31 0 0 68 68 320 1.7 67 44 13 2.3 0
15713 AW4 MIN 6.3 0.7 98 65 31 31 0 0 143 143 145 6.8 89 76 8 0.6 0
15714 WC1 MIN 5.5 0.7 155 28 27 25 0 0 73 73 245 2.9 75 55 13 1.8 0.1
Comment:
Test result units=CEC and Na in meq/100cm3;NO3 N in mg/dm3;WN in g/cm3
North Carolina Division of Water Quality Certification#257,Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines,Analysis prepared by:Waypoinl Analytical Virginia,Inc.