WQ0031314_Residual Annual Report 2021_20220217

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Non-Discharge Branch Upload/Submittal Form
NORTH CAROLINA
Environment N Qmilelr
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0031314
Applicant/Permittee Winston-Salem/Forsyth County Utilities Commission
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes OO No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* William C Brewer
Email Address* Phone Number*
[e-mail] 3363977727
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0031314
Has Current Existing permit number
Applicant/Permittee Address* 101 N.Main Street,Winston-Salem,NC 27101
Facility Name* Winston-Salem/Forsyth County Utilities Commission Class A Residuals
Program
Please provide comments/notes on your current submittal below.
This submittal is the WSFC Utilities Land Application Report for the 2021 calendar year for
Class A Residuals.The WSFC Utilities Commission owns and operates three water treatment
facilities(P.W.Swann WTP,R.W.Neilson WTP and R.A.Thomas WTP).The R.W.Neilson
and R.A.Thomas WTP's are permitted as generating facilties under the P.W.Swann Plant's
Land Application Permit.
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
2021 City of Winston-Salem Permit WQ0031314 Residuals
27.36MB
Annual Report 021621.pdf
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617

Signature
WiLLjAAIG sr -
Submission Date 2/17/2022

Winston-54km/Forsyth County
i ,
utilities
Water•Wastr■aser•sad Waste
Administration,P.O.Box 2511,Winston-Salem,NC 27102
0:336-727-8000, F:336-727-8432,wsfcutilities.org
Date February 11, 2022
North Carolina Division of Environmental Quality
Aquifer Protection-Land Application Section
1636 Mail Service Center
Raleigh, NC 27699-1636
Dear Sir or Madam,
Attached is our 2021 Residuals Land Application Annual Report and supporting documentation for the
City of Winston-Salem's Swann, Thomas and Neilson Water Treatment Plants for permit WQ0031314.
Swann Water Treatment Plant
The Swann Water Treatment Plant operated in compliance with all parameters of its permit during the
2021 calendar year. The Swann WTP operates one equalization basin and two residuals lagoons that
produces a Class A Residual,which is 503 exempt. Residuals generated by filter washes flow through an
equalization basin,whereas solids removed from the plant's sedimentation basins flow by gravity directly
to the residuals lagoon in service. The lagoons are operated such that one lagoon accepts residuals while
the other lagoon is cleaned or in reserve. During the 2021 calendar year,the Swann WTP contracted with
Synagro Central,LLC to land apply 64.8 dry tons of residuals to farmland in Yadkin County. Listed
below are documents associated with this land application event.
Section 1
• DEQ Form DMSDF -Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form
• DEQ Form RSSF -Annual Residual Sampling Summary Form
• DEQ Form RSSF B -Annual Residual Sampling Summary Form
Section 2
• DEQ Form MFLSF -Annual Metals Field Loading Summary Form
• DEQ Form FSF-Annual Land Application Field Summary Form
Section 3
• Lab data sheets from Pace Analytical(nutrient metal analysis data sheets)
• Lab data sheets from Summit Environmental Technologies,Inc. (TCLP,reactivity, ignitability,
and cyanide)
• Copies of our SAR/PAN calculations
Section 4
• Maps of the residuals disposal sites
Section 5
• Field soil sampling results
City Council:Mayor Allen Joines;Denise D.Adams,Mayor Pro Tempore,North Ward;Barbara Hanes Burke,Northeast Ward;Robert C.Clark,West Ward;
John C.Larson,South Ward;Jeff Macintosh,Northwest Ward;Kevin Mundy,Southwest Ward;Annette Scippio,East Ward;James Taylor,Jr.,Southeast Ward;
City Manager:Lee D.Garrity
County Commissioners:David R.Plyler,Chair;Don Martin,Vice Chair;Fleming El-Amin;Ted Kaplan;Richard V.Linville;Tanya McDaniel;Gloria D.Whisenhunt;
Call 311 or 335-727-8000 County Manager:Dudley Watts,Jr.
Winston-Salem/Forsyth County Utility Commission:Randall S.Tuttle,Chair;L.Wesley Curtis,Jr.,Vice Chair;Harold E.Day;Tom Griffin;Yvonne H.Hines;
cityfinkcityotws.org Duane Long;Hugh W.Jernigan;Chris Parker;Charles Wilson;Allan Younger

Thomas Water Treatment Plant
The Thomas Water Treatment Plant operated in compliance with all parameters of its permit during the
2021 calendar year. During the 2021 calendar year,no residuals were hauled from the Thomas WTP.
Neilson Water Treatment Plant
The Neilson Plant operated in compliance with all parameters of its permit during the 2021 calendar year.
The Neilson Water Treatment Plant operates three residuals lagoons and produces a Class A Residual,
which is 503 exempt. Solids from the sedimentation basins flow directly to the residual lagoon in service.
The lagoons are in a rotation so one is in service,one is drying and one is empty and ready to be placed
into service. During the 2021 calendar year EMA Resources,Inc.removed and applied 1,647.48 dry tons
of residuals on land owned by Frank Small. Based on the soil results,approximately 173 tons of lime
were applied.Listed below are documents associated with this land application event.
Section 1
• DEQ Form DMSDF-Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form
• DEQ Form DMSDF(Supp)-Class A Annual Distribution and Marketing/Surface Disposal
Certification and Summary Form(Supplemental Information)
• DEQ Form RSSF-Annual Residual Sampling Summary Form
• DEQ Form RSSF B-Annual Residual Sampling Summary Form
Section 2
• DEQ Form MFLSF-Annual Metals Field Loading Summary Form
• DEQ Form FSF-Annual Land Application Field Summary Form
Section 3
• Lab data sheets from Waypoint(nutrient metal analysis data sheets)
• Lab data sheets from Waypoint(TCLP,reactivity,ignitability,and cyanide)
• Copies of our SAR/PAN calculations
Section 4
• Maps of the residuals disposal sites
Section 5
• Field soil sampling results
If you have any questions or require additional information regarding our 2021 Annual Report,please call
Bill Brewer, Water Treatment Superintendent,at(336)397-7727.
S' erely,
Courtney L. Dr v William C. Brewer
Permittee: Preparer of Annual Report:
Courtney L.Driver William C.Brewer
Director of Utilities Water Treatment Superintendent
Utilities Administration Swarm Water Treatment Plant
P.O.Box 2511 2800 River Ridge Road
Winston-Salem,NC 27102 Pfafftown,NC 27040
2

Winston-Salem/Forsyth County Utilities
WQ0031314
2021 Residuals Land Application Report
P.W. Swann Water Treatment Plant
TABLE OF CONTENTS
Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form
• DEQ Form RSSF -Annual Residual Sampling Summary Form
• DEQ Form RSSF B-Annual Residual Sampling Summary Form
Section 2
• DEQ Form MFLSF -Annual Metals Field Loading Summary Form
• DEQ Form FSF -Annual Land Application Field Summary Form
Section 3
• Lab data sheets from Pace Analytical, LLC (nutrient, nutrient metal sampling data and chain of
custody's)
• Lab data sheets from Summit Environmental Technologies, INC (TCLP, Reactivity, Ignitability
Analysis for this Permit Cycle)
• Copies of our SAR/PAN calculations
Section 4
• Maps of the residuals disposal sites
Section 5
• Field soil sampling results
• Agricultural Lime Application Logs

Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface
Disposal Certification and Summary Form
• DEQ Form RSSF - Annual Residual Sampling Summary Form
• DEQ Form RSSF B - Annual Residual Sampling Summary Form

CLASS A ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT#: WQ00031314 FACILITY NAME: Winston Salem-Swann WTP
PHONE: [phone] COUNTY: Forsyth OPERATOR: City of Winston Salem
FACILITY TYPE(please check one): ❑ Surface Disposal(complete Part A(Source(s)and "Residual In"Volume only)and Part C)
El Distribution and Marketing(complete Parts A,B,and C)
Was the facility in operation during the past calendar year? Yes El No ❑ —* If No skip parts A,B,C and certify form below
Part A*: Part B*:
Volume(dry tons) Recipient Information
Sources(s)(include NPDES#if
Month applicable) Amendment/ Residual In Product Out Name(s) Volume(dry tons) Intended use(s)
Bulking Agent
January Swann WTP 0 64.8 64.8 Greg Voyger 64.8 Pasture
February
March
April
May
June
July
August
September
October
November
December
Total from FORM DMSDF(sup) 0 0 0 0
Totals: Annual(dry tons): 0 64.8 64.8 64.8
Amendment(s)used: Bulking Agent(s)used:
* If more space is required,attach additional information sheets(FORM DMSDF(supp)): Total Number of Form DMSDF(Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit El Yes
(including but not limited to items 1-3 below)issued by the Division of Water Resources: ❑ No > If No,Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three(3)copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or,in the case of a deviation,prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate and complete.I am aware that there are significant
penalti s or submitting fal ormation,including the possibility of fines and imprisonment for knowing violations."
a ) a G✓ ol/940L2,
Signature of Permittee Date Signature of Preparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
DENR FORM DMSDF(12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed.The parameters can be reported in FORM RSSF-B
WQ Permit Number: WQ0031314 Laboratory:
Facility Name: WINSTON-SALEM,NC PACE ANALYTICAL
Residual Source WQ#or
NPDES#: NC0079821
WWTP Name: PW SWANN WTP
Residual Analysis Data
Product Type WPL
Sample or Composite Date 01/12/21
Parameter(mg/kg dry weight) Ceiling Conc.
Limit
Percent Solids(%) NA 5.57
Arsenic 75 7.8
Cadmium 85 <1
Copper 4300 68
Chromium NA 52
Lead 840 26
Mercury 57 <0.34
Molybdenum 75 <8.1
Nickel 420 32
Selenium 100 6.6
Zinc 7500 260
Total Phosphorus NA 2900
TKN NA 9700
Ammonia-Nitrogen NA 1300
Nitrate and Nitrite NA 12
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable.Reference the individual permit for metals limits.
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted.I am aware that there are significant penalties for submitting false information,including the
possibility of fines and imprisonment for knowing violations."
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15 A NCAC 2T.1102(26) DENR FORM RSSF(12/2006)
Printed:1/6/2022 9:58:00 AM For:2055 04

ANNUAL RESIDUAL SAMPLING SUMMARY FORM -B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0031314 Laboratory:
Facility Name: WINSTON-SALEM,NC PACE ANALYTICAL
Residual Source
NPDES#or WQ#: NC0079821
WWTP Name: PW SWANN WTP
Residual Analysis Data
Product Type WPL
Sample or Composite Date 01/12/21
Parameters(mg/kg dry weight)
Aluminium 150000
Calcium 2100
Magnesium 2700
pH(s.u.) 6.40
Potassium 2000
Sodium <510
PAN <4022
SAR(Ratio) 0.4074
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted.I am aware that there are significant penalties for submitting false information,including the
possibility of fines and imprisonment for knowing violations."
7/9/1 Z.-
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15 A NCAC 2T.1102(26)
Printed:1/6/2022 9:59:09 AM For:2055 04 DENR FORM RSSF-B(12/2006)

Section 2
• DEQ Form MFLSF - Annual Metals Field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form

ANNUAL LAND APPLICATION FIELD SUMETARY FOF1I sec 1
HUM'9.a.%1F. '.'I13TONSALEki,NC IN PERFaT F:Inalialliul PIEibil IWG'r'K {IF•IU+01. mu nun 11.5
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Pried:tr J 2 DEW FIRM FER(1 l

ANNUAL METALS Fl E l.D LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Farm to be submitted in Annual Report
Facility Name: Winston-Salem. NC 'fetal Dr) Tons Applied(Annual): 41.76
Permit g: WQ003I314 Cation F.cehange Capacity{nun 503 only):
Operator: Greg Vuyger Owner: Greg Voyger Predominant Soil Series:~ Tomlin
Acres Used: 11.5 Acres Permitted: 11.5 Site#: SIC YK O0X47 Field #: 1I0K47 0001
Residual Analysis Data (IIeavv Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample Or L_J .1_2 t 3 5 J 6 7 7.1 9 -t o} 1 t '12
Corn-
perfit�
Dole I/l2,21
sit Solids 5.57
Arsenic 7.8 - -
Cadmium 1 -Copper 68
Chromium 52
Lead 26
Mercury 0.34 -
Mulyb-
denum R-1
Nickel 32
Selenium 6.6
Zinc 260
Total
Phis- 2900
phuruK
Annual Heavy Metal Field Loadings(Calculated in Ibstacre):
Total 1I 2; 1-3 - s} 7 S1 J io 1, +2
❑T/Ac. a
App.
Event 3.63
Arsenic 0.057 0.000 0.000 t1.001) 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.100 0,057
•C'ddrntum 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 U.)00 0.007
Copper 0.494 0.000 0.000 0.000 0.000 0.0111 0.000 0,000 0.000 0.000 0.000 0.:100 0494
C'hronvwtt 0.378 0.000 (1.(100 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0300 0.378
Lead 0.1119 0.00(1 0.000 0.000 0,000 0.000 0.000 0000 0.000 0,000 0.000 0.000 0.189
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0000 0.0)00 0.002
Moiyb- 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0_000 0.000 w 0.000 0.000 0.000 0.059
denur _
Nickel 0.232 0.000 0-000 0.00t1 0.000 0.000 (1.((X] 0.000 0.0(X} 0.000 0100(1 0,000 - 0.232
~Selenium 0.048 0.000 11.000 0.000 0,00(1 0.000 0.000 0.000 0.000 r (1.000 0.000 0,000 0.048
zinc 1.888 0.000 0.000 0.004 0,000 0.000 0.000 0.000 0.000 0.00(1 0.000 0.000 1.888
Total
Phos- 21.060 0.000 0,000 0.000 0_000 (1.0011 0.000 0.000 0.0011 0.000 0.000 0.000 21.060
pharus
•
"I certify,under penalty of law. that this document was prepared under niy direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the Information submitted.
I urn aware that there are significant penalties for submitting false information,including the possibility of fines and
imprison cnt for knowing violations".
(/( VVz )
Signature of Land Applies D:irr
DENR FORM MFLSF (1212006)

ANNUAL LANE/APPLICATION ["IELD SUMMARY FORM Page 1
FACILITY NAME 141NSTUN-5ALEM NC OCI PERMIT 0 WOCK313IS FIEMO.NI- -COUT .04O3• ACRES i nL17F.A:11-0
LAND OWNER:G7EG VOYGER ANNWIL DRY TONS APPLIED 2111 MTV 0 MC YK OOxai ACRES PERIATTED 110
OPERATOR-GREG VC:IGEN PREDOMINANT SOL 5E111ES.TCIULIN CATION EXCIW,GE CAPAC1I (Na11'.o31.
CROP 1 ICE FESCUE 1-1AY IFSP41 CROP 1 MAX PAN Tar CAtP;Yh11.IE CROP 2 MAX,PAN
RESUXLIA1 SaJRCE151 'sbe MI 31 bottom of raped
CHYor15 tCI) SU - I- - - -- Name o'Cacp Typo
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Chair or a Wet Torra;W) % R9#1rlra3l flr Y4et �WI7�i M[ A
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V2712021 3r-20Q-00 IG) 6.520 0.75$ 10SPVlMR 1XxsT 111(2. SUR 0.5 040 0 70E00 1300X 12.'13 6.311 FSIy •
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law 2114 Tola1 15.1149 O.oeo
AS CO I Cu CR P13 h O �_M f SE + IN P Lima Appr�od
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C.rrnulalrvc mar ra*pp*: Q.Od] Q,aot T 0.285 11.21) I 0.100 QOQT 4A31 Q TSI I Dane Loot T
1
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-
redenlC.P.L.Ritaslaeral"" 38.13 • 34.2 1,33GA 2Gr.9 j 1&0 I 375.0 R0 f moo I I
IMSPIIfsWPL a WINSTON-SALEM,NC AN SWAHA WV LIQUID -
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Rntatl: 1 ted2022 oFJ1R FoRy FSF Oti20001

ANNUAL METALS FIELD LOADING SUMMARY FORM'
Attach this form to the corresponding Field loading Summary Form to be submitted in Annual Report
Facility Name: Winston-Salem,NC Total Dry Tons Applied(Annenl): 23.04
l tirmir #: WQ0031314 Crtlon Exchange Capacity(non sill only':
Operator: _ Greg Voyger Owner: Greg Vayncr Predominant Soil Series: Tomlin
Acres Used: I I Acres Permitted: 11 Site#: NC YK 00X47 Reid 0: 5'k 00X47 0003
Residual Analysis Data heavy Metals and Total Phosphorus use mg/kg. 'la Solids use Raw Percent#):
Sanrplr ire_ t_ 3 4 s j fi • S 9 110 t T 1Z j
Cues•
rustic
Elate 1r1121
n�Solids 5.57
r
Arsenic 7.8
Cadmium I
Copper 08
Chrmmiun\ 32
Lemd 76
t
N1crrury 0.34
Mulyla• 8.1
denum
Nickel 32
Selenium 6.6
Zinc 260
TOIJI
Phos- 2900
pht>'ni.
Annual Heavy Nletal Field Loadings(Calculated in lbs/acre):
Total 1 , - 2 1 4 a Si 101 1= 12
13T/Ac..
Aprn
Event 2.09
Arsenic 0.033 0.000 0.0011 0 000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0000 0.033
Cadmium 0.004 0.000 0.0110 0(000 0.000 0,000 0.000 0.000 (1.000 0.000 0.000 0.000 0.004
Copper 0.285 0.0100 0.000 0.000 0.000 0,000 0 000 0.000 0.0011 0.000 0,000 0,000 0.285
Chromium 0.218 0.000 01.000 0.000 0.000 0.000 0.000 0.0110 0.000 0.000 0.000 0.000 0.218
Lead O.109 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.109
Mercury 0.001 0,000 0.000 0.000 0.000 0.0011 0.000 0.000 0.000 0.000 0.000 0.000 0.001 '
�ialy#r 0.034 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.034
doom
Nickel 0.134 0.000 0.000 0.000 0,000 I1,0(J0 0.0iX1 0.000 0.000 0.000 0.000 0.000 0,134
Selenium 0.028 0.000 0.000 0.000 0,000 0.000 0.000 0.0IHI 0.000 0.000 0000 0.000 0.028
Zinc 1.089 0.000 0.000 0.000 0.000 0.000 0.0(]0 0.000 0.000 0,00(1 0000 0.000 1.089
Total
Phos- 12.145 0.0(0 0.000 0.000 0.1100 0.000 0.000 0.000 0.000 0.000 I 0 000 0,000 12.145
plturus
"I certify,ender penalty of law,that this document was prepared under my direction or super►'ision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties fur submitting false information,including the possibility of fines and
imprisonnfeirt for know violations".
Jet/X iffr //tRies)...
Signature of Land Applier Date
OENR FORM 1AFl.SF(12/2006)

Section 3
• Lab data sheets from Pace Analytical Services, LLC (nutrient, nutrient metal
sampling data and chain of custody's)
• Lab data sheets from Summit Environmental Technologies, INC (TCLP,
Reactivity, Ignitability Analysis for this Permit Cycle)
• Copies of our SAR/PAN calculations

0
Pace Analytical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Winston WTP
Lot Number:WA14017
Date Completed:01/29/2021
02/01/2021 10:24 AM
Approved and released by:
Project Manager II: Lucas Odom
MILB
Q PCCR�c��
'ye )
ANSI NatonalAccredltatlon Board
ACCREDITEDORA1O,
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Synagro
Lot Number: WA14017
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Metals by ICP
Due to the matrix and low percent solids, the initial sample amount used for sample -001 was 3X more
than the standard procedure. The LOQ has been adjusted accordingly.
TKN
The method blank for analytical batch 80781 contained the analyte: Total Kjeldahl Nitrogen (TKN) greater
than the acceptance criteria. The associated samples, contained detections for this analyte at
concentrations greater than 10X the value found in the method blank; therefore sample results are not
impacted. The data has been reported.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2of7

Client:Synagro Laboratory ID:WA14017-001
Description:Winston WTP Matrix:Solid
Date Sampled:01/12/2021 1000 % Solids: 5.57 01/14/2021 2255
Date Received:01/14/2021
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (% Solids)SM 2540G 1 01/14/2021 2255 SRB 79511
1 350.1 (Ammonia-N )350.1 2 01/19/2021 1339 DRD 79842
1 (Nitrate-N )9056A 1 01/19/2021 1315 AMR 79937
1 (Nitrite-N )9056A 1 01/19/2021 1315 AMR 79944
2 (Phosphorus)365.1 5 01/27/2021 1129 DMA 01/26/2021 1924 80750
1 (Soil pH meas)9045D 1 01/14/2021 1815 AAB 79516
1 351.4 (TKN)351.2 1 01/26/2021 1512 DMA 01/21/2021 1755 80265
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
% Solids SM 2540G 5.57 % 1
Ammonia-N (gas diffusion) 350.1 1300 36 19 mg/kg 1
Nitrate-N (soluble) 9056A 12 9.0 1.8 mg/kg 1
Nitrite-N (soluble) 9056A ND 3.6 1.8 mg/kg 1
Phosphorus 7723-14-0 365.1 2900 450 90 mg/kg 2
Soil pH measured in water @ 17.9° C 9045D 6.4 su 1
TKN 351.2 9700 450 450 mg/kg 1
CVAA
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/21/2021 1238 JAB2 01/20/2021 1110 79538
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Mercury 7439-97-6 7471B ND 1.4 0.34 mg/kg 1
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/20/2021 0846 KSH2 01/19/2021 0905 79720
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Aluminum 7429-90-5 6010D 150000 320 120 mg/kg 1
Arsenic 7440-38-2 6010D 7.8 J 12 4.1 mg/kg 1
Cadmium 7440-43-9 6010D ND 4.1 1.0 mg/kg 1
Calcium 7440-70-2 6010D 2100 J 4100 510 mg/kg 1
Chromium 7440-47-3 6010D 52 8.1 2.0 mg/kg 1
Copper 7440-50-8 6010D 68 8.1 3.7 mg/kg 1
Iron 7439-89-6 6010D 46000 81 37 mg/kg 1
Lead 7439-92-1 6010D 26 8.1 3.7 mg/kg 1
Magnesium 7439-95-4 6010D 2700 J 4100 510 mg/kg 1
Manganese 7439-96-5 6010D 1300 12 4.8 mg/kg 1
Molybdenum 7439-98-7 6010D ND 32 8.1 mg/kg 1
Nickel 7440-02-0 6010D 32 32 8.5 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:WA14017-001
Description:Winston WTP Matrix:Solid
Date Sampled:01/12/2021 1000 % Solids: 5.57 01/14/2021 2255
Date Received:01/14/2021
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 01/20/2021 0846 KSH2 01/19/2021 0905 79720
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Potassium 7440-09-7 6010D 2000 J 4100 510 mg/kg 1
Selenium 7782-49-2 6010D 6.6 J 16 6.6 mg/kg 1
Sodium 7440-23-5 6010D ND 4100 510 mg/kg 1
Zinc 7440-66-6 6010D 260 41 10 mg/kg 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range DL=Detection Limit
ND=Not detected at or above the DL N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% J=Estimated result<LOQ and>DL
H=Out of holding time W=Reported on wet weight basis
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 7

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PACE ANALYTICAL SERVICES, LLC
Samples Receipt checklist(SRC (rlE0O}$C-is) Hevised,9f2W2020
.../.2e-Araiyrizat issuirrg Author Ity:Pace ENV-WOOL Pogo 1of 1
Sample Receipt Checklist (SRC)
Client; sl'n0.°f3 Coolor lnh ected byldat:: ESL r 1-'1"2Q21 Lot#: VL'A]461T
Means c+f reacipt: Paco. Irlient 0 1.112S IIII Fed ( III Other_ �` _
O d No l-Wen v.istody seals present on the cooler? _-
Yes I No' NA 2-If custoriv seals were. oc
prnt,w they ey intact 2.nd unbroken?
'pH Strip la. 14r' Chlorine Strip[il• ''' Tesierl by Nn -
.s rig[i]a,I temperas urr npcu i eoe i pt/Derived(Corrected)t:rnperaturf upon receipt %So]idd Snap-Cup 1D: 23475
.2.3 r F,3 0C 1...r1 rr,'.t aC NA ...NA °c NA f NA of I
Nictho :JTtrnperr.R7re Blank Osigainst Bottles IR Gun ID: 5 IR Cron Correction.?actor: 3 °C.
Method ofmoolant: ❑ Wctlee. ❑.1cePacks 0 Do?Tee. ❑ None ..
'e. ❑ Jo`I � A��' Tr rein ran—of�rnv'mole_ exceeded G.0°C,was Project Manager-Nulified?
© PM was Notiiirid hy_phone i ernai:/face U0-f1ce(circle one),
, 't'c No INA 4. ]s the commercial rier's acting.clip attached to this form?
ii=1 Yet ❑N(' 5- Were proper custody procedures(rclinauisht 1/received)foll.wecn
Yos 11 No 6. Were sarnpie IDs Iiskd uu the COC4-
d Yost No _ 7- Were sample]Ds listed on all sample c `?
an[ainers
DI Yes' L No 8- Was collprtion ristl e&time listed an;hC COC?
rii Yev LiNo 9. Vfaf col Iuki n date&time Iiste d on all sample contamus?
Q Yes. ❑No _ ]0,Did all container label infvrmatiun(ID,dace,time)agree with the COO?
-- DNo '11. 'Were tests I()be leer formed IisEcd on the COG?
❑No 12.Did all samples arrive in the proper containers for nacb test aridfar in good condition
(unbroken,lids on,ale.)? - - -
1 Yes uNn lS- Was adcnrrate sample volume tivsilab°e? _
Ea Yrs ❑No 14. Wra;all samples received within V!Lira holdin time or48.hours,whichever comes first?
'r-1Yes *` No _ 15.Watoony samples contain ers.missirr +excess(circle onejancles Nor litiled SW COG"'
16,For VGA and RSK-175 sarnples,vrero bl]bblei present bra-eiai'('or(own in[Hameln-)
❑Y CS ❑No IZINA irl any of the VOA vinla?
Yes IT No MNA 17. Were all DR-O/metalsinutricp:sarnpats received at a pH of<2? l
'Yes L No [TNA la.Were all cyanide Sam les received at E pFi> 12 and sulfide semp]es received ar a Pr] 0?
19, Were all applical:le1411; I(N cyan kl +pllenoL0625.1i 08,3 ('- 05rr11T]samples freeo�
71 .c, LJ No El NA residual chlorine?
i -�.20, Were client remarks,'requests(i-e-requeverl dintiona,MgilvISD designations,etc...)
❑ - J `' �NA correctly anscr[bcd from the COC into the cnmrnent sectian in L1MW?
ID Yes! ©No 121, Wos else quote nurnber lislerl ur i1 o Woutut :? II Yes,{ uatc rr -
— r
Sample Preservation (Nina be completed for any samples)utcartw.tly prewerved o1'19111 heudspace-)
Saniple(s) '* were:•eceived in:orrcctly prescrved and were adjusted accordiri ly I.
in sample receiving with 1" mL of circle one: 1i2S01.I-IND3, RC],HaOI-[ u ing.SR 6 NR
Tura of preseiv i.ion_^ , If more luau one preservative is nested,pIca pals in the cumm,ani.a relrrnu-
smp[e(s) N _ware re.eived with bubbles>6 rpm in diameter', .I
Satrtpke( _ we.a received with TRC>0.3 utgJL(If iM l9 is rro)and were
adjuaced nnroordidgly:n sample rEcciviig w[h sodium thiasul ante(NaIS,243)v+iiit Shealy ID:N' .
SR},>rrorx]e[abets applied by: m13(1.1Cl Oats; 0ll]4.+1n1
Comments:
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2055-04-WPL-NC WINSTON-SALEM, NC PW SWANN WTP LIQUID 1/12/2021 1/1/2021 -3/31/2021 0.4074
Na mg/I = (Na mg/kg x% Solids)+ 100= (510 x 5.5700)+ 100=28.407
Ca mg/I = (Ca mg/kg x% Solids)+ 100= (2100 x 5.5700)+ 100= 116.97
Mg mg/I = (mg mg/kg x%Solids)+ 100 = (2700 x 5.5700)+ 100= 150.39
Na meq = Na mg/I+Molec.Wgt.Na=28.407+23= 1.23509
Ca meq =Ca mg/I+Molec.Wgt.Ca= 116.97+20=5.8485
Mg meq = Mg mg/I+ Molec.Wgt.Mg = 150.39+ 12 = 12.5325
SAR= Na meq+SgrRoot[0.5 x(Ca meq + Mg meq)] = 1.23509+SgrRoot[0.5(5.8485+12.5325)] = 0.407407

S
a i' Summit Environmental Technologies,Inc.
EIrg 3310 Win St.
MUM ENVIRONMENTAL TECHNOLOCIES,INC Cuyahoga Falls,Ohio 44223
rralyt�cal L9boralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com
December 18, 2020
Alex Fox
Synagro
284 Boger Rd.
Mocksville,NC 27028
TEL: [phone]
FAX: [phone]
RE: Winston WTP
Dear Alex Fox: Order No.: 20120299
Summit Environmental Technologies, Inc. received 1 sample(s) on 12/4/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results,please feel free to call the
laboratory.
Sincerely,
)77.4-#641‘14
1...v10.147921
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls,Ohio 44223
Arkansas 88-0735,California 2943,Colorado,Connecticut PH-0108,Florida NELAC E87688,Idaho OH00923,Illinois 200061,Indiana C-OH-13,Kansas
E-10347,Kentucky(Underground Storage Tank)3,Kentucky 90146,Maryland 339,Michigan 9988,Minnesota 1780279,Nevada OH009232020-1,New
Hampshire 2996,New Jersey OH006,New York 11777,North Carolina 39705 and 631,North Dakota R-201,Ohio DW,Ohio VAP CL0052,Oklahoma
2019-155,Oregon OH200001, Pennsylvania 011,Rhode Island LA000317,South Carolina 92016001,Texas T104704466-19-16,Utah OH009232020-12,
Virginia VELAP 10381,West Virginia 9957C
Page 1 of 34

5 M�'� Summit Environmental Technologies,Inc. Case Narrative
mu 331 Ohio Wm St.
AnalENVIRONMENTAL calLaoraioriNO LOGI ,INC. Cuyahoga Falls, 44223 WO#: 20120299rrafyt�caf iaboralorlas TEL:[phone] FAX. [phone]
Website:http://www.settek.com Date: 12/18/2020
CLIENT: Synagro
Project: Winston WTP
WorkOrder Narrative:
20120299: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report,Applicable Accreditation Information, Chain-of-Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or"wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Notes:
4OPPM SVOC-MSTRS(8270): 8270 CCV exhibits high recovery for Pyridine. Associated samples are
N.D. for this analyte.
LCS-46757 SVOC-BNA TCLP(8270): Possible high bias for Pyridine due to high recovery in CCV.
Original
Page 2 of 34

•
17 S
Mm iT Summit Environmental Technologies,In Qualifiers and Acronyms
331 i Wm 5 `C
Arralytiica @N1 L orator iN❑cOG{ S.INC Cuyahoga Falls,Ohio 442 WO#: 20120299rral}'t�caf iaboralorlas TEL:[phone] FAX. [phone]E
Website:http://www.settek.co Date: 12/18/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25%difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low(-)or high(+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low(-)or high(+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low(-)or high(+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low(-)or high(+).
S The spike result was outside of accepted recovery limits.
Z Deviation;A deviation from the method was performed;Please refer to the Case Narrative for
additional information
Acronyms
ND Not Detected RL Reporting Limit
QC Quality Control MDL Method Detection Limit
MB Method Blank LOD Level of Detection
LCS Laboratory Control Sample LOQ Level of Quantitation
LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS Quality Control Sample CRQL Contract Required Quantitation Limit
DUP Duplicate PL Permit Limit
MS Matrix Spike RegLv1 Regulatory Limit
MSD Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD Relative Percent Different MinCL Minimum Compound Limit
ICV Initial Calibration Verification RA Reanalysis
ICB Initial Calibration Blank RE Reextraction
CCV Continuing Calibration Verification TIC Tentatively Identified Compound
CCB Continuing Calibration Blank RT Retention Time
RLC Reporting Limit Check CF Calibration Factor
DF Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 34

S t�' Summit Environmental Technologies,Inc. Workorder
3310 Win St.
1.7 ENVIRONMENTAL TECHNQI. oiEs,iric, Cuyahoga Falls,Ohio 44223 Sample Summary
4rralyt�cai iaboralorlas TEL:[phone] FAX [phone] WO#: 20120299
Website:http://www.settek.com 18-Dec-20
CLIENT: Synagro
Project: Winston WTP
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
20120299-001 Winston WTP 12/2/2020 11:15:00 AM 12/4/2020 10:55:00 AM Sludge
Page 4 of 34

Summit Environmental Technologies,Inc. DATES REPORT
rg SUMMIT
MN 33hi Win St.
Artal O cat La oratorL iNO LOi,I S,INC Cuyahoga Falls, Ohio 44223 WO#: 20120299
4rra�yt�cai iaboralorlas TEL:[phone] FAX:[phone]
Website:http://www.settekcom 18-Dec-20
Client: Synagro
Project: Winston WTP
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
20120299-001A Winston WTP 12/2/2020 11:15:00 AM Sludge Ignitability of Solids(SW-846: 1030) 12/10/2020 5:30:16 PM
pH(SW9045D) 12/7/2020 12:13:39 PM
Reactive Cyanide(9014/7.3.3.2)-Solid 12/13/2020 12:46:00 PM
Reactive Sulfide(9034)/7.3.4.2 12/13/2020 12:46:00 PM
TCLP Herbicides by EPA 8321B 12/16/2020 6:47:00 PM
TCLP Mercury Analysis(SW1311/74712/9/2020 10:26:06 AM 12/10/2020 9:40:00 AM 12/10/2020 3:05:00 PM
TCLP Metals Analysis(SW 1311/6010:12/9/2020 10:26:06 AM 12/9/2020 10:45:00 AM 12/9/2020 6:23:41 PM
TCLP Pesticides Analysis(SW1311/8(12/9/2020 10:26:06 AM 12/9/2020 12:25:00 PM 12/12/2020 1:03:00 AM
TCLP Pesticides Analysis(SW1311/8(12/9/2020 10:26:06 AM 12/9/2020 12:25:00 PM 12/12/2020 1:03:00 AM
TCLP Semi-Volatiles Analysis 12/9/2020 10:26:06 AM 12/9/2020 12:25:00 PM 12/9/2020 10:30:00 PM
(SW1311/8270)
TCLP Volatiles Analysis 12/9/2020 6:08:00 PM
Original
Page 5 of 34

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECliMOL-OGIES,IFtC Cuyahoga Falls, Ohio44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WO#: 20120299
Website:http://www.settek.com Date Reported: 12/18/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/2/2020 11:15:00 AM
Lab ID: 20120299-001A
Project: Winston WTP
Client Sample ID Winston WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: ERA
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND 0.00200 mg/L 1 12/10/2020 3:05:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW6010D SW3010A Analyst: EAM
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 12/9/2020 6:23:41 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 12/9/2020 6:23:41 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 12/9/2020 6:23:41 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 12/9/2020 6:23:41 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 12/9/2020 6:23:41 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 12/9/2020 6:23:41 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 12/9/2020 6:23:41 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8270 SW3510C Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.200 mg/L 2 12/9/2020 10:30:00 PM
2,4,5-Trichlorophenol ND 0.500 mg/L 2 12/9/2020 10:30:00 PM
2,4,6-Trichlorophenol ND 0.500 mg/L 2 12/9/2020 10:30:00 PM
2,4-Dinitrotoluene ND 0.100 mg/L 2 12/9/2020 10:30:00 PM
Cresols,Total ND 10.0 mg/L 2 12/9/2020 10:30:00 PM
Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 12/9/2020 10:30:00 PM
Hexachlorobenzene ND 0.100 mg/L 2 12/9/2020 10:30:00 PM
Hexachloroethane ND 0.200 mg/L 2 12/9/2020 10:30:00 PM
Nitrobenzene ND 0.200 mg/L 2 12/9/2020 10:30:00 PM
Pentachlorophenol ND 0.500 mg/L 2 12/9/2020 10:30:00 PM
Pyridine ND 0.500 QC+ mg/L 2 12/9/2020 10:30:00 PM
Surr:2-Fluorophenol 41.2 10-157 %Rec 2 12/9/2020 10:30:00 PM
Surr: Phenol-d6 46.8 10-169 %Rec 2 12/9/2020 10:30:00 PM
Surr: Nitrobenzene-d5 46.2 32.1 -130 %Rec 2 12/9/2020 10:30:00 PM
Surr:2,4,6-Tribromophenol 58.6 45.4-166 %Rec 2 12/9/2020 10:30:00 PM
Surr:2-Fluorobiphenyl 57.6 35.7-130 %Rec 2 12/9/2020 10:30:00 PM
Surr: p-Terphenyl-d14 116 74.7-145 %Rec 2 12/9/2020 10:30:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 6 of 34

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECliMOL-OGIES,IFtC Cuyahoga Falls, Ohio44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WO#: 20120299
Website:http://www.settek.com Date Reported: 12/18/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/2/2020 11:15:00 AM
Lab ID: 20120299-001A
Project: Winston WTP
Client Sample ID Winston WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: CSS
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane,total ND 0.0250 mg/L 1 12/12/2020 1:03:00 AM
Toxaphene ND 0.0500 mg/L 1 12/12/2020 1:03:00 AM
Endrin ND 0.00250 mg/L 1 12/12/2020 1:03:00 AM
gamma-BHC ND 0.00250 mg/L 1 12/12/2020 1:03:00 AM
Heptachlor ND 0.00250 mg/L 1 12/12/2020 1:03:00 AM
Heptachlor epoxide ND 0.00250 mg/L 1 12/12/2020 1:03:00 AM
Methoxychlor ND 0.00250 mg/L 1 12/12/2020 1:03:00 AM
Surr:TCMX 73.1 10-119 %Rec 1 12/12/2020 1:03:00 AM
Surr: DCB 71.3 10-119 %Rec 1 12/12/2020 1:03:00 AM
TCLP HERBICIDES BY EPA 8321B SW8321A Analyst: TM
2,4-D ND 0.500 mg/L 50 12/16/2020 6:47:00 PM
2,4,5-TP ND 0.500 mg/L 50 12/16/2020 6:47:00 PM
Surr:2,4-Dichlorophenylacetic aci 83.2 70-130 %Rec 50 12/16/2020 6:47:00 PM
TCLP METALS,VOC, BNA, PEST, HERB-SOLID SW8260 SW1311M Analyst: SLV
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.250 mg/L 50 12/9/2020 6:08:00 PM
1,2-Dichloroethane ND 0.250 mg/L 50 12/9/2020 6:08:00 PM
MEK ND 5.00 mg/L 50 12/9/2020 6:08:00 PM
Benzene ND 0.250 mg/L 50 12/9/2020 6:08:00 PM
Carbon tetrachloride ND 0.250 mg/L 50 12/9/2020 6:08:00 PM
Chlorobenzene ND 2.50 mg/L 50 12/9/2020 6:08:00 PM
Chloroform ND 0.250 mg/L 50 12/9/2020 6:08:00 PM
Tetrachloroethene ND 0.250 mg/L 50 12/9/2020 6:08:00 PM
Trichloroethene ND 0.250 mg/L 50 12/9/2020 6:08:00 PM
Vinyl chloride ND 0.100 mg/L 50 12/9/2020 6:08:00 PM
Surr:4-Bromofluorobenzene 90.5 70-130 %Rec 50 12/9/2020 6:08:00 PM
Surr: Dibromofluoromethane 98.8 70-130 %Rec 50 12/9/2020 6:08:00 PM
Surr:Toluene-d8 98.9 70-130 %Rec 50 12/9/2020 6:08:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 7 of 34

S
it• Summit Environmental Technologies,Inc.3310 Win St. Analytical Report
INiM itrgENVIRONMENTAL TECliMOL-OGIES.IFtC Cuyahoga Falls, Ohio44223 (base report)
�afyt�caf iaboralorfas TEL:[phone] FAX [phone] WO#: 20120299
Website:http://www.settek.com Date Reported: 12/18/2020
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/2/2020 11:15:00 AM
Lab ID: 20120299-001A
Project: Winston WTP
Client Sample ID Winston WTP
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9014 Analyst: MS
REACTIVE CYANIDE(9014/7.3.3.2)-SOLID
Cyanide, Reactive ND 0.490 mg/Kg 1 12/13/2020 12:46:00 PM
IGNITABILITY OF SOLIDS(SW-846: 1030) SW1030 Analyst: CXS
Ignitability nonflammable mm/sec 1 12/10/2020 5:30:16 PM
RCI SW9045D Analyst: WK
PH (SW9045D)
pH 7.2 s.u.@20.0C 1 12/7/2020 12:13:39 PM
RCI SW9034 Analyst: MS
REACTIVE SULFIDE(9034)/7.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 12/13/2020 12:46:00 PM
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected P Second column confirmation exceeds
PL Permit Limit R RPD outside accepted recovery limits Original
RL Reporting Detection Limit U Samples with CalcVal<MDL
Page 8 of 34

�� SUMMIT
Summit Environmental Technologies,Inc. Accreditation Program
1.. 3310 Win St. Anal teS Report
ENVIRONMENTAL TECHNOLOGIES,INC
Cuyahoga Falls,Ohio 44223 Y Y
rral}'t�caf iaboralorlas TEL:[phone] FAX [phone] WO#: 20120299
Website:http://www.settek.com 18-Dec-20
Client: Synagro State: NW
Project: Winston WTP Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
20120299-001A Sludge Ignitability of Solids(SW-846: 1030) Ignitability A
Sludge pH(SW9045D) Hydrogen Ion(pH) A
Sludge Reactive Cyanide(9014/7.3.3.2)-Solid Cyanide,Reactive N
Sludge Reactive Sulfide(9034)/7.3.4.2 Sulfide,Reactive N
Sludge TCLP Herbicides by EPA 8321B 2,4,5-TP A
Sludge TCLP Herbicides by EPA 8321B 2,4-D A
Sludge TCLP Mercury Analysis(SW1311/7470) Mercury A
Sludge TCLP Metals Analysis(SW1311/6010) Arsenic A
Sludge TCLP Metals Analysis(SW1311/6010) Barium A
Sludge TCLP Metals Analysis(SW1311/6010) Cadmium A
Sludge TCLP Metals Analysis(SW1311/6010) Chromium A
Sludge TCLP Metals Analysis(SW1311/6010) Lead A
Sludge TCLP Metals Analysis(SW1311/6010) Selenium A
Sludge TCLP Metals Analysis(SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis(SW1311/8081) Chlordane,total A
Sludge TCLP Pesticides Analysis(SW1311/8081) Endrin A
Sludge TCLP Pesticides Analysis(SW1311/8081) gamma-BHC A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Heptachlor epoxide A
Sludge TCLP Pesticides Analysis(SW1311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis(SW1311/8081) Toxaphene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 1,4-Dichlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,5-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4,6-Trichlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Cresols,Total A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Hexachloroethane A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Nitrobenzene A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi-Volatiles Analysis(SW1311/8270) Pyridine A
Key Key
NC WW SCM A Accredited NC WW SCM N Not Accredited
Original#1
Page 9 of 34

S UMM IT Summit Environmental Technologies,Inc. Accreditation Program
3310 Win St. Anal tes Re ort
EN ENVIRONMENTAL TECHN❑w oes,INC Cuyahoga Falls,Ohio 44223 3' 1�
rral}'0caf iaboralorlas TEL:[phone] FAX [phone] WO#: 20120299
Website:http://www.settek.com 18-Dec-20
Client: Synagro State: NW
Project: Winston WTP Program Name: NC_WW_SCM
Sample ID Matrix Test Name Analyte Status
20120299-OO1A Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
Key Key
NC WW SCM A Accredited NC WW SCM N Not Accredited
Original#1
Page 10 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: 46751
Sample ID: MB-46751 SampType: MBLK TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 121165
Client ID: PBS Batch ID: 46751 TestNo: SW8260 SW1311M Analysis Date: 12/9/2020 SeqNo: 3110032
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,1-Dichloroethene ND 0.250
1,2-Dichloroethane ND 0.250
MEK ND 5.00
Benzene ND 0.250
Carbon tetrachloride ND 0.250
Chlorobenzene ND 2.50
Chloroform ND 0.250
Tetrachloroethene ND 0.250
Trichloroethene ND 0.250
Vinyl chloride ND 0.100
Surr:4-Bromofluorobenzene 2250 2500 89.8 70 130
Surr: Dibromofluoromethane 2510 2500 100 70 130
Surr:Toluene-d8 2460 2500 98.5 70 130
Sample ID: LCS-46751 SampType: LCS TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 121165
Client ID: LCSS Batch ID: 46751 TestNo: SW8260 SW1311M Analysis Date: 12/9/2020 SeqNo: 3110033
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,1-Dichloroethene 0.906 0.250 1.00 0 90.7 64.7 136
1,2-Dichloroethane 0.927 0.250 1.00 0 92.7 70 130
MEK ND 5.00 5.00 0 79.4 55.1 149
Benzene 0.925 0.250 1.00 0 92.5 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 11 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: 46751
Sample ID: LCS-46751 SampType: LCS TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 121165
Client ID: LCSS Batch ID: 46751 TestNo: SW8260 SW1311M Analysis Date: 12/9/2020 SeqNo: 3110033
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Carbon tetrachloride 0.951 0.250 1.00 0 95.1 70 130
Chlorobenzene ND 2.50 1.00 0 90.4 70 130
Chloroform 0.885 0.250 1.00 0 88.4 70 130
Tetrachloroethene 0.877 0.250 1.00 0 87.7 70 134
Trichloroethene 0.918 0.250 1.00 0 91.8 62.8 160
Vinyl chloride 0.856 0.100 1.00 0 85.6 67.1 130
Surr:4-Bromofluorobenzene 2540 2500 102 70 130
Surr: Dibromofluoromethane 2450 2500 98.0 70 130
Surr:Toluene-d8 2480 2500 99.4 70 130
Sample ID: 20120398-001AMS SampType: MS TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 121165
Client ID: BatchQC Batch ID: 46751 TestNo: SW8260 SW1311M Analysis Date: 12/9/2020 SeqNo: 3110043
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,1-Dichloroethene 1.04 0.250 1.00 0 104 13.6 202
1,2-Dichloroethane 1.01 0.250 1.00 0 101 55.7 138
MEK ND 5.00 5.00 0 91.8 65.3 118
Benzene 1.11 0.250 1.00 0.0635 104 49.2 145
Carbon tetrachloride 1.07 0.250 1.00 0 107 26.7 156
Chlorobenzene ND 2.50 1.00 0 102 33.7 159
Chloroform 0.996 0.250 1.00 0 99.6 48.5 145
Tetrachloroethene 0.999 0.250 1.00 0 99.9 19.2 191
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 12 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: 46751
Sample ID: 20120398-001AMS SampType: MS TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 121165
Client ID: BatchQC Batch ID: 46751 TestNo: SW8260 SW1311M Analysis Date: 12/9/2020 SeqNo: 3110043
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Trichloroethene 1.04 0.250 1.00 0 104 38.4 167
Vinyl chloride 0.980 0.100 1.00 0 98.0 27.3 161
Surr:4-Bromofluorobenzene 2550 2500 102 70 130
Surr: Dibromofluoromethane 2520 2500 101 70 130
Surr:Toluene-d8 2540 2500 101 70 130
Sample ID: 20120398-001AMSD SampType: MSD TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 121165
Client ID: BatchQC Batch ID: 46751 TestNo: SW8260 SW1311M Analysis Date: 12/9/2020 SeqNo: 3110051
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,1-Dichloroethene 1.06 0.250 1.00 0 106 13.6 202 1.04 1.48 25
1,2-Dichloroethane 1.00 0.250 1.00 0 100 55.7 138 1.01 0.941 25
MEK ND 5.00 5.00 0 93.8 65.3 130 0 0 25
Benzene 1.10 0.250 1.00 0.0635 104 49.2 145 1.11 0.634 25
Carbon tetrachloride 1.07 0.250 1.00 0 107 26.7 156 1.07 0.280 25
Chlorobenzene ND 2.50 1.00 0 102 33.7 159 0 0 25
Chloroform 1.00 0.250 1.00 0 100 48.5 145 0.996 0.601 25
Tetrachloroethene 0.982 0.250 1.00 0 98.2 19.2 191 0.999 1.77 25
Trichloroethene 1.04 0.250 1.00 0 104 38.4 167 1.04 0.337 25
Vinyl chloride 1.09 0.100 1.00 0 109 27.3 161 0.980 11.0 25
Surr:4-Bromofluorobenzene 2570 2500 103 70 130 0 25
Surr: Dibromofluoromethane 2490 2500 99.5 70 130 0 25
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 13 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
1.7ra 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: 46751
Sample ID: 20120398-001AMSD SampType: MSD TestCode: TCLP-VOC-M Units: mg/L Prep Date: RunNo: 121165
Client ID: BatchQC Batch ID: 46751 TestNo: SW8260 SW1311M Analysis Date: 12/9/2020 SeqNo: 3110051
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Surr:Toluene-d8 2490 2500 99.6 70 130 0 25
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 14 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: 46757
Sample ID: MB-46757 SampType: MBLK TestCode: SVOC-BNA T Units: mg/L Prep Date: 12/9/2020 RunNo: 121173
Client ID: PBS Batch ID: 46757 TestNo: SW8270 SW3510C Analysis Date: 12/9/2020 SeqNo: 3110322
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene ND 0.100
2,4,5-Trichlorophenol ND 0.250
2,4,6-Trichlorophenol ND 0.250
2,4-Dinitrotoluene ND 0.0500
o-Cresol ND 0.250
Cresols,Total ND 5.00
Hexachloro-1,3-butadiene ND 0.0200
Hexachlorobenzene ND 0.0500
Hexachloroethane ND 0.100
Nitrobenzene ND 0.100
Pentachlorophenol ND 0.250
Pyridine ND 0.250 QC+
Surr:2-Fluorophenol 0.736 1.000 73.6 10 130
Surr: Phenol-d6 0.864 1.000 86.4 10 130
Surr: Nitrobenzene-d5 0.814 1.000 81.4 19 130
Surr:2,4,6-Tribromophenol 0.866 1.000 86.6 10 130
Surr:2-Fluorobiphenyl 0.909 1.000 90.9 22 130
Surr: p-Terphenyl-d14 1.18 1.000 118 34 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 15 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
Artai ON M cat Lab ralorf NO LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: 46757
Sample ID: LCS-46757 SampType: LCS TestCode: SVOC-BNA T Units: mg/L Prep Date: 12/9/2020 RunNo: 121173
Client ID: LCSS Batch ID: 46757 TestNo: SW8270 SW3510C Analysis Date: 12/9/2020 SeqNo: 3110323
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene 0.515 0.100 0.8000 0 64.4 36.4 130
2,4,5-Trichlorophenol 0.750 0.250 0.8000 0 93.8 31.7 132
2,4,6-Trichlorophenol 0.708 0.250 0.8000 0 88.5 31.1 133
2,4-Dinitrotoluene 0.768 0.0500 0.8000 0 96.0 43.3 130
o-Cresol 0.612 0.250 0.8000 0 76.5 32.9 130
Cresols,Total ND 5.00 1.600 0 77.8 31.7 130
Hexachloro-1,3-butadiene 0.531 0.0200 0.8000 0 66.4 31.4 130
Hexachlorobenzene 0.787 0.0500 0.8000 0 98.4 43.1 130
Hexachloroethane 0.471 0.100 0.8000 0 58.9 36.5 130
Nitrobenzene 0.560 0.100 0.8000 0 70.0 39.5 130
Pentachlorophenol 0.745 0.250 0.8000 0 93.2 34 130
Pyridine 0.466 0.250 0.8000 0 58.2 10 130 mQC+
Surr:2-Fluorophenol 0.690 1.000 69.0 17.1 130
Surr: Phenol-d6 0.878 1.000 87.8 10 130
Surr: Nitrobenzene-d5 0.758 1.000 75.8 32.6 130
Surr:2,4,6-Tribromophenol 1.02 1.000 102 4.43 130
Surr:2-Fluorobiphenyl 0.884 1.000 88.4 41.8 130
Surr: p-Terphenyl-d14 1.17 1.000 117 36.4 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 16 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: 46757
Sample ID: 20120397-001AMS SampType: MS TestCode: SVOC-BNA T Units: mg/L Prep Date: 12/9/2020 RunNo: 121173
Client ID: BatchQC Batch ID: 46757 TestNo: SW8270 SW3510C Analysis Date: 12/9/2020 SeqNo: 3110324
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene 0.580 0.200 0.8000 0 72.6 33.8 126
2,4,5-Trichlorophenol 0.775 0.500 0.8000 0 96.9 28.7 144
2,4,6-Trichlorophenol 0.716 0.500 0.8000 0 89.4 12.8 153
2,4-Dinitrotoluene 0.703 0.100 0.8000 0 87.9 20.4 155
o-Cresol 0.679 0.500 0.8000 0 84.9 10 148
Cresols,Total ND 10.0 1.600 0 84.6 10 148
Hexachloro-1,3-butadiene 0.577 0.0400 0.8000 0 72.2 29 130
Hexachlorobenzene 0.765 0.100 0.8000 0 95.7 33.7 134
Hexachloroethane 0.529 0.200 0.8000 0 66.2 32.8 132
Nitrobenzene 0.700 0.200 0.8000 0 87.5 20 158
Pentachlorophenol 0.685 0.500 0.8000 0 85.7 10 176
Pyridine ND 0.500 0.8000 0 61.7 10 130 mQC+
Surr:2-Fluorophenol 0.721 1.000 72.1 3.39 130
Surr: Phenol-d6 0.881 1.000 88.1 5 130
Surr: Nitrobenzene-d5 0.783 1.000 78.3 14.5 154
Surr:2,4,6-Tribromophenol 0.946 1.000 94.6 19.5 130
Surr:2-Fluorobiphenyl 0.942 1.000 94.2 34.4 130
Surr: p-Terphenyl-d14 1.07 1.000 107 8.86 156
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 17 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: 46757
Sample ID: 20120397-001AMSD SampType: MSD TestCode: SVOC-BNA T Units: mg/L Prep Date: 12/9/2020 RunNo: 121173
Client ID: BatchQC Batch ID: 46757 TestNo: SW8270 SW3510C Analysis Date: 12/9/2020 SeqNo: 3110325
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
1,4-Dichlorobenzene 0.608 0.200 0.8000 0 76.0 33.8 126 0.5804 4.64 30
2,4,5-Trichlorophenol 0.798 0.500 0.8000 0 99.8 28.7 144 0.7748 3.00 30
2,4,6-Trichlorophenol 0.781 0.500 0.8000 0 97.6 12.8 153 0.7156 8.71 30
2,4-Dinitrotoluene 0.738 0.100 0.8000 0 92.3 20.4 155 0.7032 4.88 30 m
o-Cresol 0.697 0.500 0.8000 0 87.1 10 148 0.6792 2.56 30
Cresols,Total ND 10.0 1.600 0 88.6 10 148 0 0 30
Hexachloro-1,3-butadiene 0.655 0.0400 0.8000 0 81.9 29 130 0.5772 12.7 30
Hexachlorobenzene 0.871 0.100 0.8000 0 109 33.7 134 0.7652 12.9 30
Hexachloroethane 0.556 0.200 0.8000 0 69.6 32.8 132 0.5292 5.01 30
Nitrobenzene 0.790 0.200 0.8000 0 98.8 20 158 0.7000 12.1 30
Pentachlorophenol 0.750 0.500 0.8000 0 93.8 10 176 0.6852 9.03 30
Pyridine 0.555 0.500 0.8000 0 69.4 10 130 0.4936 11.7 30 mQC+
Surr:2-Fluorophenol 0.796 1.000 79.6 3.39 130 0
Surr: Phenol-d6 0.984 1.000 98.4 10 130 0
Surr: Nitrobenzene-d5 0.896 1.000 89.6 14.5 154 0
Surr:2,4,6-Tribromophenol 0.963 1.000 96.3 19.5 130 0
Surr:2-Fluorobiphenyl 1.09 1.000 109 34.4 130 0
Surr: p-Terphenyl-d14 1.24 1.000 124 8.86 156 0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 18 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: 46758
Sample ID: 20120299-001ams SampType: MS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 12/9/2020 RunNo: 121304
Client ID: Winston WTP Batch ID: 46758 TestNo: SW8081 SW3510C Analysis Date: 12/12/2020 SeqNo: 3115479
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Endrin 0.00970 0.000500 0.0100 0 97.0 10 224 m
gamma-BHC 0.00984 0.000500 0.0100 0 98.4 10 192
Heptachlor 0.0114 0.000500 0.0100 0 114 10 197
Heptachlor epoxide 0.0106 0.000500 0.0100 0 106 10 208
Methoxychlor 0.0124 0.000500 0.0100 0 124 10 251
Surr:TCMX 17.5 20.00 87.6 10 157
Surr: DCB 17.1 20.00 85.7 10 194
Sample ID: 20120299-001amsd SampType: MSD TestCode: TCLP-SVOC- Units: mg/L Prep Date: 12/9/2020 RunNo: 121304
Client ID: Winston WTP Batch ID: 46758 TestNo: SW8081 SW3510C Analysis Date: 12/12/2020 SeqNo: 3115480
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Endrin 0.00872 0.000500 0.0100 0 87.2 10 224 0.00970 10.6 30 m
gamma-BHC 0.00823 0.000500 0.0100 0 82.3 10 192 0.00984 17.8 30
Heptachlor 0.00957 0.000500 0.0100 0 95.7 10 197 0.0114 17.7 30
Heptachlor epoxide 0.00900 0.000500 0.0100 0 90.0 10 208 0.0106 16.2 30
Methoxychlor 0.0104 0.000500 0.0100 0 104 10 251 0.0124 17.0 30
Surr:TCMX 14.7 20.00 73.5 10 157 0
Surr: DCB 15.0 20.00 75.0 10 194 0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 19 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: 46758
Sample ID: LCS-46758 SampType: LCS TestCode: TCLP-SVOC- Units: mg/L Prep Date: 12/9/2020 RunNo: 121304
Client ID: LCSS Batch ID: 46758 TestNo: SW8081 SW3510C Analysis Date: 12/12/2020 SeqNo: 3115482
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Endrin 0.0107 0.000500 0.0100 0 107 10 130 m
gamma-BHC 0.00914 0.000500 0.0100 0 91.4 10 130
Heptachlor 0.0105 0.000500 0.0100 0 105 10 130
Heptachlor epoxide 0.00994 0.000500 0.0100 0 99.4 10 130
Methoxychlor 0.0111 0.000500 0.0100 0 111 10 178
Surr:TCMX 16.8 20.00 83.9 10 130
Surr: DCB 20.6 20.00 103 10 130
Sample ID: MB-46758 SampType: MBLK TestCode: TCLP-SVOC- Units: mg/L Prep Date: 12/9/2020 RunNo: 121304
Client ID: PBS Batch ID: 46758 TestNo: SW8081 SW3510C Analysis Date: 12/12/2020 SeqNo: 3115483
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Chlordane,total ND 0.00250
Toxaphene ND 0.00500
Endrin ND 0.000500
gamma-BHC ND 0.000500
Heptachlor ND 0.000500
Heptachlor epoxide ND 0.000500
Methoxychlor ND 0.000500
Surr:TCMX 15.3 20.00 76.7 10 119
Surr: DCB 19.6 20.00 98.1 10 119
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 20 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: 46776
Sample ID: MB-46776 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM Prep Date: 12/10/2020 RunNo: 121216
Client ID: PBS Batch ID: 46776 TestNo: SW7470A SW7470A Analysis Date: 12/10/2020 SeqNo: 3111910
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID: LCS-46776 SampType: LCS TestCode: HG_TCLP(74 Units: PPM Prep Date: 12/10/2020 RunNo: 121216
Client ID: LCSS Batch ID: 46776 TestNo: SW7470A SW7470A Analysis Date: 12/10/2020 SeqNo: 3111911
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury 0.00400 0.00200 0.00400 0 100 80 120
Sample ID: 20120288-001AMS SampType: MS TestCode: HG_TCLP(74 Units: PPM Prep Date: 12/10/2020 RunNo: 121216
Client ID: BatchQC Batch ID: 46776 TestNo: SW7470A SW7470A Analysis Date: 12/10/2020 SeqNo: 3111915
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury 0.00421 0.00200 0.00400 0.000108 103 75 125
Sample ID: 20120288-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 12/10/2020 RunNo: 121216
Client ID: BatchQC Batch ID: 46776 TestNo: SW7470A SW7470A Analysis Date: 12/10/2020 SeqNo: 3111916
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
TCLP Mercury 0.00442 0.00200 0.00400 0.000108 108 75 125 0.00421 4.87 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 21 of 34

U��' Summit Environmental Technologies,Inc. QC SUMMARY REPORT
OM5 T 33hi Win St.
ENVIRONMENTAL rmy' TE ides Oi,I S,INC Cuyahoga Falls, Ohio 44223 WO#: 20120299
4rra�yt�caf iaboralorlas TEL:[phone] FAX:[phone]
Website:http://www.settekcom 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: 46776
Sample ID: 20120288-001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 12/10/2020 RunNo: 121216
Client ID: BatchQC Batch ID: 46776 TestNo: SW7470A SW7470A Analysis Date: 12/10/2020 SeqNo: 3111916
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 22 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
1.7ra 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: R121019
Sample ID: CHECK 7 SampType: LCS TestCode: pH_S(9045D) Units: s.u.@20.2C Prep Date: RunNo: 121019
Client ID: LCSS Batch ID: R121019 TestNo: SW9045D Analysis Date: 12/7/2020 SeqNo: 3105339
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH 7.0 7.0 0 101 90 110
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 23 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: R121019
Sample ID: LCS-R121019 SampType: LCS TestCode: pH_Oil(9045D Units: s.u.@20.1C Prep Date: RunNo: 121019
Client ID: LCSW Batch ID: R121019 TestNo: SW9045D Analysis Date: 12/7/2020 SeqNo: 3104675
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH 7.0 7.0 0 101 90 110
Sample ID: 20120229-001ADUP SampType: DUP TestCode: pH_Oil(9045D Units: s.u.@20.1C Prep Date: RunNo: 121019
Client ID: BatchQC Batch ID: R121019 TestNo: SW9045D Analysis Date: 12/7/2020 SeqNo: 3104677
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
pH 6.7 0 0 6.7 0.1 10
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 24 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,IF1C Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: R121273
Sample ID: LCS-R121273 SampType: LCS TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 121273
Client ID: LCSS Batch ID: R121273 TestNo: SW1030 Analysis Date: 12/10/2020 SeqNo: 3113980
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability 7.94 7.240 0 110 70 130
Sample ID: 20120299-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 121273
Client ID: Winston WTP Batch ID: R121273 TestNo: SW1030 Analysis Date: 12/10/2020 SeqNo: 3113982
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Sample ID: 20120496-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 121273
Client ID: BatchQC Batch ID: R121273 TestNo: SW1030 Analysis Date: 12/10/2020 SeqNo: 3113984
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability <2.2 0 0 20
Sample ID: 20120496-002ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 121273
Client ID: BatchQC Batch ID: R121273 TestNo: SW1030 Analysis Date: 12/10/2020 SeqNo: 3114016
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Ignitability nonflammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 25 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
1.7ra 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,IF1C Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchlD: R121273
Sample ID: 20120496-002ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 121273
Client ID: BatchQC Batch ID: R121273 TestNo: SW1030 Analysis Date: 12/10/2020 SeqNo: 3114016
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 26 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: R121312
Sample ID: Blank SampType: MBLK TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 121312
Client ID: PBW Batch ID: R121312 TestNo: SW9014 Analysis Date: 12/13/2020 SeqNo: 3114988
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive ND 0.485
Sample ID: LCS SampType: LCS TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 121312
Client ID: LCSW Batch ID: R121312 TestNo: SW9014 Analysis Date: 12/13/2020 SeqNo: 3114989
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive 9.51 0.490 10.00 0 95.1 85 115
Sample ID: RLCheck SampType: RLC TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 121312
Client ID: BatchQC Batch ID: R121312 TestNo: SW9014 Analysis Date: 12/13/2020 SeqNo: 3114991
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive 0.543 0.481 0.5000 0 109 65 135
Sample ID: 20120711-007AMS SampType: MS TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 121312
Client ID: BatchQC Batch ID: R121312 TestNo: SW9014 Analysis Date: 12/13/2020 SeqNo: 3115003
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive 9.45 0.490 10.00 0 94.5 75 125
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 27 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,IF1C Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: R121312
Sample ID: 20120711-007AMS SampType: MS TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 121312
Client ID: BatchQC Batch ID: R121312 TestNo: SW9014 Analysis Date: 12/13/2020 SeqNo: 3115003
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sample ID: 20120711-007AMSD SampType: MSD TestCode: Cyanide,Rea Units: mg/L Prep Date: RunNo: 121312
Client ID: BatchQC Batch ID: R121312 TestNo: SW9014 Analysis Date: 12/13/2020 SeqNo: 3115004
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Cyanide, Reactive 9.46 0.481 10.00 0 94.6 75 125 9.446 0.121 10
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 28 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: R121313
Sample ID: MB-R121313 SampType: MBLK TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 121313
Client ID: PBW Batch ID: R121313 TestNo: SW9034 Analysis Date: 12/13/2020 SeqNo: 3115019
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-R121313 SampType: LCS TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 121313
Client ID: LCSW Batch ID: R121313 TestNo: SW9034 Analysis Date: 12/13/2020 SeqNo: 3115020
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive 3130 25.0 3090 0 101 85 115
Sample ID: 20120711-007AMS SampType: MS TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 121313
Client ID: BatchQC Batch ID: R121313 TestNo: SW9034 Analysis Date: 12/13/2020 SeqNo: 3115031
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive 2870 25.0 3090 0 92.9 75 125 W
Sample ID: 20120711-007AMSD SampType: MSD TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 121313
Client ID: BatchQC Batch ID: R121313 TestNo: SW9034 Analysis Date: 12/13/2020 SeqNo: 3115032
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Sulfide, Reactive 2730 25.0 3090 0 88.3 75 125 2870 5.00 30 W
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 29 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
1.7ra 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: R121313
Sample ID: 20120711-007AMSD SampType: MSD TestCode: Sulfide,React Units: mg/L Prep Date: RunNo: 121313
Client ID: BatchQC Batch ID: R121313 TestNo: SW9034 Analysis Date: 12/13/2020 SeqNo: 3115032
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 30 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
III rg 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: R121521
Sample ID: MB SampType: MBLK TestCode: SVOC-Herb_ Units: mg/L Prep Date: RunNo: 121521
Client ID: PBW Batch ID: R121521 TestNo: SW8321A Analysis Date: 12/16/2020 SeqNo: 3123461
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D ND 0.0250
2,4,5-TP ND 0.0100
Surr:2,4-Dichlorophenylacetic acid 0.847 1.000 84.7 70 130
Sample ID: LCS SampType: LCS TestCode: SVOC-Herb_ Units: mg/L Prep Date: RunNo: 121521
Client ID: LCSW Batch ID: R121521 TestNo: SW8321A Analysis Date: 12/16/2020 SeqNo: 3123462
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D 0.339 0.0250 0.3000 0 113 70 130
2,4,5-TP 0.293 0.0100 0.3000 0 97.8 70 130
Surr:2,4-Dichlorophenylacetic acid 2.85 3.000 94.9 70 130
Sample ID: LCS SampType: LCSD TestCode: SVOC-Herb_ Units: mg/L Prep Date: RunNo: 121521
Client ID: LCSS02 Batch ID: R121521 TestNo: SW8321A Analysis Date: 12/16/2020 SeqNo: 3123463
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D 0.324 0.0250 0.3000 0 108 70 130 0.3389 4.46 30
2,4,5-TP 0.280 0.0100 0.3000 0 93.3 70 130 0.2934 4.71 30
Surr:2,4-Dichlorophenylacetic acid 2.71 1.000 271 70 130 0 30 S
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 31 of 34

MM Summit Environmental Technologies,Inc. QC SUMMARY REPORT
1.7ra 5 U IT 331 Ohio Win St.
ENVIRONMENTAL rmy' Tlorfes LOi,I S,INC Cuyahoga Falls, 44223 WO#: 20120299
4�a/yt�caf iaboralorfas TEL:[phone] FAX[phone]
Website:http://www.settek.com 18-Dec-20
Client: Synagro
Project: Winston WTP BatchID: R121521
Sample ID: 20120773-001AMS SampType: MS TestCode: SVOC-Herb_ Units: mg/L Prep Date: RunNo: 121521
Client ID: BatchQC Batch ID: R121521 TestNo: SW8321A Analysis Date: 12/16/2020 SeqNo: 3123465
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D 15.9 1.25 15.00 0.5200 102 70 130 H
2,4,5-TP 13.0 0.500 15.00 0 87.0 70 130 H
Surr:2,4-Dichlorophenylacetic acid 126 150.0 41.6 70 130 SH
Sample ID: 20120773-001AMS SampType: MSD TestCode: SVOC-Herb_ Units: mg/L Prep Date: RunNo: 121521
Client ID: BatchQC Batch ID: R121521 TestNo: SW8321A Analysis Date: 12/16/2020 SeqNo: 3123466
Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual
2,4-D 16.0 1.25 15.00 0.5200 103 70 130 15.88 0.784 30 H
2,4,5-TP 13.1 0.500 15.00 0 87.6 70 130 13.05 0.726 30 H
Surr:2,4-Dichlorophenylacetic acid 127 50.00 126 70 130 0 30 H
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or ana15
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 32 of 34

2C-t1ACOC SJ& Rev s; Teo[-flnt Date IO011J17014
��T P Analysis Request/Chain of Custody os
r l of
£14V1F1 ON AA a 147A L TECHPICLOGIR S.INC- SET Fer Sualmil riranmrnu[ h���n'''o}}}laeia,lne.ssennly
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SynagTO Winston VVTP a 1 Analytical Parameters and Methods Requested
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Alex Fox 12/02120 1:15 UPS
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swoon valume provided to run QC?pp S n NO Cooky'!y 1. ENO
R riled it Ruiumll Time Carrier I riv[d Temp.' Other Coo Miner:
by: ■ Rush R ue9[t'J. UxySsl
'+� r � i r r E I t l t�'1 r a Mum hr�ippra+rd U4 Lab AIan.KSr ( J l` 4 lee Present' ES ONO�w1ELTFD
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w

;74700,1summIT Summit Environmental Techn3310ologiesW,in Inc.St.
II a
ENVIRONMENTAL TEC„NOLOGaS,INC Cuyahoga Falls, Ohio 44223 Sample Log-In Check List
ArrafyOcaf Laborator/as TEL:[phone] FAX. [phone]
Website:http:/Aiww.settek.com
Client Name: SYN-NC-27028 Work Order Number: 20120299 RcptNo: 1
Logged by: Jacqueline Rasile 12/4/2020 10:55:00 AM
Completed By: Jacqueline Rasile 12/6/2020 3:47:22 PM
Reviewed By: Jennifer Woolf 12/7/2020 2:04:11 PM (...710‘7*.?1' M''oaL011,--
Chain of Custody
1. Is Chain of Custody complete? Yes ❑ No ❑d Not Present ❑
2. How was the sample delivered? Fed Ex
Log In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0°C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s)in proper container(s)? Yes ❑d No ❑
8. Sufficient sample volume for indicated test(s)? Yes ❑d No ❑
g. Are samples(except VOA and ONG)properly preserved? Yes ❑d No ❑
10.Was preservative added to bottles? Yes ❑ No ❑d NA ❑
it. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials V
12.Were any sample containers received broken? Yes ❑ No ❑d
13. Does paperwork match bottle labels? Yes ❑d No ❑
(Note discrepancies on chain of custody)
14.Are matrices correctly identified on Chain of Custody? Yes ❑d No ❑
15. Is it clear what analyses were requested? Yes ❑d No ❑
16. Were all holding times able to be met? Yes ❑d No ❑
(If no, notify customer for authorization.)
Special Handling(if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑d No ❑ NA ❑
Person Notified: 'Alex Fox Date:II-- 12/7/2020
By Whom: !Jennifer Woolf Via: 0 eMail ❑ Phone ❑ Fax ❑ In Person
Regarding: sample date listed as 9/22/20. time as 10/15/20
Client Instructions: livas sampled on 12/2/20 and time collected be 11:15 shipped at 1:00
18.Additional remarks:
sample date incorrect
Cooler Information
Cooler No Temp°C Condition Seal Intact Seal No Seal Date Signed By
1 0.7 Good Not Present
Page 34 of 34

SAR and PAN Verifications for 2021
Dry Tons 64.8
Gallons Hauled 279,000
%Solids = 5.570
mg/kg mg/I meq
Sodium 510 28.407 1.2351
Calcium 2100 116.970 5.8485
Magnesium 2700 150.390 12.5325
Sodium Adsorbtion Ratio= 0.4074
SAR= Na meq/sq rt((Ca meq + Mg meq)/2)
Mineralization Rate 0.4
TKN 9700
Ammonia-Nitrogen 1300
Nitrate+ Nitrite 12
Plant Available Nitrogen = 4022
PAN = (Min Rate * (TKN - NH4)) + (0.5 * NH4) + Nitrate+ Nitrite

Section 4
• Maps of the residuals disposal sites

Soil Map—Yadkin County, North Carolina
a
541300 541400 541500 541030 541700 541800 541900 542000 542100 542200 542300 542400
36°4'14"N - 36°4'14"N
§ a..
r StB\
(\GuE
g A g- TnB2
\ TnD2
ToD3\
•
\ PfB GuE §
CrA ' TmB 0
TmE
§ GuE —i ToE3l
0
TnB2
--)
ir-- TnD2
Il " P
, • 1 ,
i
TmB 0
TnB2•, 4.
4 t0co _
ToE3 I, . F.
Oct] Gawp may'moil Pa walk! ail t lhilo walla° •.
8
36°3'48"N .i....-.. 1. - 36°3'48"N
541300 541400 541500 541600 541700 541800 541900 542000 542100 542200 542300 542400
Map Scale:1:5,470 if printed on A landscape(11"x 8.5")sheet.
Meters
$ A
0 y0 100 200 300 $
0 250 y00 1000 1y00
Mapprojedion:Web Mercator Coner000rdinates:WGS84 Edge tics:UTM Zone 17N WGS84
USDA Natural Resources Web Soil Survey 2/7/2022
Conservation Service National Cooperative Soil Survey Page 1 of 3

Soil Map—Yadkin County, North Carolina
MAP LEGEND MAP INFORMATION
Area of Interest(AOI) Spoil Area The soil surveys that comprise your AOI were mapped at
n Area of Interest(AOI) StonySot 1:15,800.
p
Soilsel Very Stony Spot Warning:Soil Map may not be valid at this scale.
El Soil Map Unit Polygons
Wet Spot Enlargement of maps beyond the scale of mapping can cause
Soil Map Unit Lines misunderstanding of the detail of mapping and accuracy of soil
Other line placement.The maps do not show the small areas of
• Soil Map Unit Points contrasting soils that could have been shown at a more detailed
Special Line Features
Special Point Features scale.
Blowout Water Features
Streams and Canals Please rely on the bar scale on each map sheet for map
031 Borrow Pit measurements.
Transportation
Clay Spot _ Rails Source of Map: Natural Resources Conservation Service
Closed Depression Web Soil Survey URL:
., Interstate Highways Coordinate System: Web Mercator(EPSG:3857)
Gravel Pit US Routes
Maps from the Web Soil Survey are based on the Web Mercator
Gravelly Spot Major Roads projection,which preserves direction and shape but distorts
distance and area.A projection that preserves area,such as the
▪ Landfill Local Roads Albers equal-area conic projection,should be used if more
A. Lava Flow accurate calculations of distance or area are required.
Background
Marsh or swamp rika Aerial Photography This product is generated from the USDA-NRCS certified data as
of the version date(s)listed below.
• Mine or Quarry
Soil Survey Area: Yadkin County, North Carolina
Miscellaneous Water Survey Area Data: Version 25,Jan 21,2022
▪ Perennial Water Soil map units are labeled(as space allows)for map scales
Rock Outcrop 1:50,000 or larger.
Saline Spot Date(s)aerial images were photographed: May 18,2019—May
21,2019
Sandy Spot
° The orthophoto or other base map on which the soil lines were
Severely Eroded Spot compiled and digitized probably differs from the background
imagery displayed on these maps.As a result,some minor
• Sinkhole shifting of map unit boundaries may be evident.
Slide or Slip
o Sodic Spot
USDA Natural Resources Web Soil Survey 2/7/2022
Conservation Service National Cooperative Soil Survey Page 2 of 3

Soil Map—Yadkin County, North Carolina
Map Unit Legend
Map Unit Symbol Map Unit Name Acres in AOI Percent of AOI
CrA Codorus loam,0 to 2 percent 20.1 18.7%
slopes,occasionally flooded
GuE Gullied land-Fairview complex, 0.9 0.8%
10 to 25 percent slopes
PfB Pfafftown fine sandy loam,0 to 1.8 1.6%
6 percent slopes,rarely
flooded
StB Starr loam,0 to 6 percent 0.0 0.0%
slopes,rarely flooded
TmB Tomlin loam,2 to 6 percent 30.1 28.0%
slopes
TmC Tomlin loam,6 to 10 percent 5.5 5.1%
slopes
TmE Tomlin loam, 15 to 25 percent 3.0 2.8%
slopes
TnB2 Tomlin sandy clay loam,2 to 6 29.3 27.3%
percent slopes, moderately
eroded
TnD2 Tomlin sandy clay loam, 10 to 1.3 1.2%
15 percent slopes,
moderately eroded
ToD3 Tomlin clay loam, 10 to 15 6.4 5.9%
percent slopes,severely
eroded
ToE3 Tomlin clay loam, 15 to 25 9.2 8.5%
percent slopes,severely
eroded
Totals for Area of Interest 107.4 100.0%
USDA Natural Resources Web Soil Survey 2/7/2022
Conservation Service National Cooperative Soil Survey Page 3 of 3

Section 5
• Field soil sampling results
• Agricultural Lime Application Logs

Page 1 of 1
•
Report No: 21-046-0552
Account No: 12259 ay JA I L .
7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Advisor: Synagro/Columbus NC Client:Winston WTP Farm:YK-X47
Mary Brewer Greg Voyger
284 Boger Rd
Mocksville NC 27028 Date Received:02/15/2021
Date of Report:02/16/2021
Lab No Field ID Sample ID Soil Class HM% WA' pH Ac P-I K-I S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I CEC BS% Ca% Mg% ESP Na
I00487 1 MIN 2.0 7.0 0.0 52 24 33 869 523 0 423 423 215 8.1 101 80 18 0.8 0.1
Crop Recommendations: Rec Uom Lime(t/acre) N P205 K20 S Mn Zn Cu B Mg Last Crop
1-Mix Grass Hay lb/acre 0.0 160 30 250 9 0 0 0 0 0
00489 2 MIN 2.2 6.8 0.3 21 141 25 488 298 0 280 280 115 8.6 97 72 17 0.6 0
Crop Recommendations: Rec Uom Lime(t/acre) N P2O5 K20 S Mn Zn Cu B Mg Last Crop
1-Mix Grass Hay lb/acre 0.0 160 55 0 10 0 0 0 0 0
Comment:
Test result units=CEC and Na in meq/100cm3;NO3 N in mg/dm3;W/V in g/cm3
North Carolina Division of Water Quality Certification#257,Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines,Analysis prepared by:Waypoint Analytical Virginia,Inc.

Agricultural Lime Application Log
Year: 2021
Project: Winston
Field Soil Lime Requirement Tons/Acre Date Applied
(state-county-site-field) pH (from soil analysis) Applied(CCE Eq.)
YK-X47-1 7.0 0.0T/Ac.
YK-X47-2 6.8 0.0T/Ac.
*Lime will be applied when conditions improve.

Winston-Salem/Forsyth County Utilities
WQ0031314
2021 Residuals Land Application Report
R.W. Neilson Water Treatment Plant
TABLE OF CONTENTS
Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface Disposal Certification
and Summary Form
• DEQ Form DMSDF(Supp) - Class A Annual Distribution and Marketing/Surface Disposal
Certification and Summary Form (Supplemental Information)
• DEQ Form RSSF -Annual Residual Sampling Summary Form
• DEQ Form RSSF B-Annual Residual Sampling Summary Form
Section 2
• DEQ Form MFLSF -Annual Metals Field Loading Summary Form
• DEQ Form FSF -Annual Land Application Field Summary Form
Section 3
• Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and chain of custody's)
• Lab data sheets from Waypoint for this permit cycle (TCLP, Corrosivity, Ignitability and Cyanide)
• Copies of our SAR/PAN calculations
Section 4
• Maps of the residuals disposal sites
Section 5
• Field soil sampling results

Section 1
• DEQ Form DMSDF - Class A Annual Distribution and Marketing/Surface
Disposal Certification and Summary Form
• DEQ Form DMSDF(Supp) - Class A Annual Distribution and
Marketing/Surface Disposal Certification and Summary Form (Supplemental
Information)
• DEQ Form RSSF - Annual Residual Sampling Summary Form
• DEQ Form RSSF B - Annual Residual Sampling Summary Form

CLASS A ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT#: WQ0031314 FACILITY NAME: Winston Salem-Neilson Water Treatment Plant
PHONE: COUNTY: Forsyth OPERATOR: City of Winston Salem
FACILITY TYPE(please check one): ❑ Surface Disposal(complete Part A(Source(s)and"Residual In"Volume only)and Part C)
0 Distribution and Marketing(complete Parts A,B,and C)
Was the facility in operation during the past calendar year? Yes 21 No ❑ -► If No skip parts A,B,C and certify form below
Part A*: Part B*:
Volume(dry tons) Recipient Information
Month Sources(s)(include NPDES#if Amendment/
applicable) Bulking Agent Residual In Product Out Name(s) Volume(dry tons) Intended use(s)
January
February
March
April
May
June
July
August
September
October
November
December
Total from FORM DMSDF(sup) 0 1647.48 1647.48 1647.48
Totals: I Annual(dry tons): 0 1647.48 1647.48 1647.48
Amendment(s)used:I Bulking Agent(s)used:
*If more space is required,attach additional information sheets(FORM DMSDF(supp)): Total Number of Form DMSDF(Supp) 1
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit El Yes
(including but not limited to items 1-3 below)issued by the Division of Water Quality: ❑ No ► If No,Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three(3)copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or,in the case of a deviation,prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate and complete.I am aware that there are significant
penalties for submitting false in ation,including the possibility of fines and imprisonment for knowing violations."
07//1/ 004 a-3-ao aa.
Signature of Permittee Date Signature r6f'P eparer** Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
DENR FORM DMSDF(12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT#: WQ0031314 FACILITY NAME: Winston Salem-Neilson Water Treatment Plant
PHONE: COUNTY: Forsyth OPERATOR: City of Winston Salem
FACILITY TYPE(please check one): ❑ Surface Disposal(complete Part A- "Month", "Source(s)" and "Residual In" columns only)
.J Distribution and Marketing(complete Parts A,and B)
Part A*: Part B*:
Volume(dry tons) Recipient Information
Month Sources(s)(include NPDES#if Volume(dry
applicable) Amendment/ Name(s) Intended use(s)
Bulking Agent Residual In Product Out tons)
January Neilson WTP-NC0086011 1647.48 1647.48 Frank Small 1647.48 soil amendment
Totals: Annual(dry tons): 0 1647.48 1647.48 1647.48
Amendment(s)used: Bulking Agent(s)used:
* If more space is required,attach additional information sheets(FORM DMSDF(supp)): Total Number of Form DMSDF(Supp) 1
DENR FORM DMSDF(Supp) (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF-B
WQ Permit Number: WQ0031314 Laboratory: 1) Waypoint Analytical
Facility Name: Winston Salem/Forsyth County Utilities Commission 2)
Residual Source WQ#or NC0086011 3)
NPDES#: 4)
WWTP Name: Neilson Water Treatment Plant 5)
Residual Analysis Data
Conc. Sample or Composite Date
Parameter Limit 1/12/21 1/12/21 1/12/21 1/12/21 January
(mg/kg) (mg/kg)a #1 #2 #3 #4 Average
Percent Solids(%) NA 34.8 40.3 35 37.2 36.8
Arsenic 75 7.5 6.2 6.97 6.83 7
Cadmium 85 0.931 0.695 0.654 0.581 1
Copper 4,300 38.5 34.7 34.9 34.1 36
Chromium NA 59.5 46.7 49.7 44.9 50
Lead 840 26.2 22.4 24.1 22.5 24
Mercury 57 0.0862 0.0685 0.0723 0.0855 0
Molybdenum 75 0.712 0.59 0.585 0.645 1
Nickel 420 29 21.6 24.2 21.5 24
Selenium 100 0.919 0.794 0.914 0.86 1
Zinc 7,500 112 90.8 99.4 90.6 98
Total Phosphorus NA 1710 1500 1530 1460 1550
TKN NA 2620 2850 2830 2350 2663
Ammonia-Nitrogen NA 368 400 349 419 384
Nitrate and Nitrite NA 23.1 21.8 30 17.4 23
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
k-- � a- 3- aoaa__
Signature of parer* Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
DENR FORM RSSF(12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0031314 Laboratory: 1) Waypoint Analytical
Facility Name: Winston Salem/Forsyth County Utilities Commission 2)
Residual Source NC0086011 3)
NPDES#or WQ#: 4)
WWTP Name: Neilson Water Treatment Plant 5)
Residual Analysis Data
Sample or Composite Date
Parameter 1/12/21 1/12/21 1/12/21 1/12/21 January
(mg/kg) #1 #2 #3 #4 Average
Aluminum 111000 95000 101000 92200 99800
Calcium 928 784 726 761 799.75
Magnesium 6180 3420 4910 3760 4567.5
pH 5.9 5.9 5.8 5.8 5.85
Potassium 5690 3230 4460 3440 4205
Sodium 164 131 147 131 143.25
PAN 1108 1202 1197 999 1126
SAR 0.25 0.28 0.25 0.26
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2- 3- avaa
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102(26)
DENR FORM RSSF- B (12/2006)

Section 2
• DEQ Form MFLSF - Annual Metals Field Loading Summary Form
• DEQ Form FSF - Annual Land Application Field Summary Form

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Winston Salem -Neilson WTP Total Dry Tons Applied(Annual): 1647.48
Permit#: WQ0031314 Cation Exchange Capacity(non 503 only): 0
Operator: Frank Small Owner: Frank Small Predominant Soil Series:
Acres Used: 173 Acres Permitted: 173 Site#: DA10 Field#: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 2 3 4 5 6 I 7 8 9 10 11 12
Com- January
posite Average
Date
%Solids 36.8
Arsenic 6.9
Cadmium 0.7
Copper 35.6
Chromium 50.2
Lead 23.8
Mercury 0.08
Molyb- 0.6
denum
Nickel 24.1
Selenium 0.9
Zinc 98.2
Total
Phos- 1550
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 3- 4 5 6 7 8 9 10 11 12 y
DT/Ac./
App.
Event 9.52
Arsenic 0.131 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.131
Cadmium 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013
Copper 0.678 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.678
Chromium 0.956 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.956
Lead 0.453 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.453
Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011
denum
Nickel 0.459 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.459
Selenium 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017
Zinc 1.870 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.870
Total
Phos- 29.521 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 29.521
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
Zfd
1/26/2022
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Winston Salem-Neilson WTP WQ Permit#: WQ0031314 Field#: 1 Acres Utilized: 173
Land Owner: Frank Small Annual Dry Tons Applied: 1647.48 Site#: DA10 Acres Permitted: 173
Operator: Frank Small Predominant Soil Series: 0 Cation Exchange Capacity(non 503):
Crop 1 Name: Corn Crop 1 Max.PAN: 198 Crop 2 Name: Crop 2 Max.PAN:
Volume applied Volume Residual Sources Soil Precip. r- o Z a Nitrate Name of Crop Type
a, (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 ,� �. w ��, TKN o and P b Aa peied Receiving Residual
ro Liquid Solids Acre Pert.,Animal (Dry' Hrs. a . �' Nitrite ( ) Application
Q Wet, * o * �
Cu.Yds Gallons (DryTons/Ac) Waste,etc) inches o
Moist) o' mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
1/18/21 1096 36.8 1.963 Neilson WTP Dry <.5" S 0.5 0.4 2662.5 384 23.1 4.424 NA Corn
1/19/21 1313 36.8 2.352 Neilson WTP Dry <.5" S 0.5 0.4 2662.5 384 23.1 5.299 NA Corn
1/20/21 1275 36.8 2.284 Neilson WTP Dry <.5" S 0.5 0.4 2662.5 384 23.1 5.146 NA Corn
1/21/21 969 36.8 1.736 Neilson WTP Dry <.5" S 0.5 0.4 2662.5 384 23.1 3.911 NA Corn
1/22/21 459 36.8 0.822 Neilson WTP Dry <.5" S 0.5 0.4 2662.5 384 23.1 1.853 NA Corn
1/23/21 204 36.8 0.365 Neilson WTP Dry <.5" S 0.5 0.4 2662.5 384 23.1 0.823 NA Corn
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 5316 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 21.456 0.000 Lime Applied
Annual lbs/acre 0.131 0.013 0.678 0.956 0.453 0.002 0.011 0.459 0.017 1.870 29.521 Date lbs/ac
Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0
Current Cumulative lbs/ac 0.131 0.013 0.678 0.956 0.453 0.002 0.011 0.459 0.017 1.870
Permitted C.P.L.R.**** 36 34 1338 267 15 374 89 2498
Permit PAN Limit 1 st/2nd Crop 198
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method:S-Surface,IN-Injection,INC-Incorporation
1/26/2022 **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.:Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

Section 3
• Lab data sheets from Waypoint (nutrient, nutrient metal sampling data and
chain of custody's)
• Lab data sheets from Waypoint for this permit cycle (TCLP, Corrosivity,
Ignitability and Cyanide)
• Copies of our SAR/PAN calculations

w°
Waypoint,, 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
1/21/2021
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 21-013-0048
Client Project Description: Winston Salem
Winston Salem, NC
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s)on 1/13/2021 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
COro LC6-Q.' ) Q
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
hit
Page 1 of 14

w•
\4fIaypo i nt... 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN:Waypoint Analytical, LLC., Memphis,TN
State Program Lab ID Expiration Date
Alabama State Program 40750 02/28/2021
Arkansas State Program 88-0650 02/07/2021
California State Program 2904 06/30/2021
Florida State Program-NELAP E871157 06/30/2021
Georgia State Program C044 02/18/2023
Georgia State Program 04015 06/30/2021
Illinois State Program-NELAP 200078 10/10/2021
Kentucky State Program 80215 06/30/2021
Kentucky State Program KY90047 12/31/2021
Louisiana State Program-NELAP LA037 12/31/2021
Louisiana State Program-NELAP 04015 06/30/2021
Mississippi State Program MS 02/11/2023
North Carolina State Program 415 12/31/2021
Oklahoma State Program 9311 08/31/2021
Pennsylvania State Program-NELAP 68-03195 05/31/2021
South Carolina State Program 84002 06/30/2021
South Carolina State Program 84002 06/30/2021
Tennessee State Program 02027 02/11/2023
Tennessee A2LA ISO 17025:2017 4313.01 10/31/2021
Texas State Program-NELAP T104704180 09/30/2021
Virginia State Program 00106 06/30/2021
Virginia State Program-NELAP 460181 09/14/2021
Page 1 of 1 00001/21-013-0048
Page 2 of 14

\ Iaypo I nt.. 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-013-0048
Client Project Description: Winston Salem
Winston Salem, NC
Lab No Client Sample ID Matrix Date Collected Date Received
85356 Neilson WTP#1 Solids 01/12/2021 10:00 01/13/2021
85357 Neilson WTP#2 Solids 01/12/2021 10:15 01/13/2021
85358 Neilson WTP#3 Solids 01/12/2021 10:30 01/13/2021
85359 Neilson WTP#4 Solids 01/12/2021 10:45 01/13/2021
Page 3 of 14

o
Waypoi nt. 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Client: EMA Resources Inc CASE NARRATIVE
Project: Winston Salem
Lab Report Number: 21-013-0048
Date: 1/21/2021
Metals Analysis Method 6010D
Sample 85492
Analyte:Aluminum
QC Batch No: L531894
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L531894
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L531894
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L531894
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Manganese
QC Batch No: L532349
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L531894
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L531894
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: L531894
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 14

wWaypaint.., 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Winston Salem
Mr. Brent Collins Report Date: 01/21/2021
755 Yadkinville Rd Information : Winston Salem, NC Received : 01/13/2021
Mocksville, NC 27028 UOmLa&.�0J-X-Q--
Report Number:21-013-0048 REPORT OF ANALYSIS Danyale Love
Project Manager
Lab No : 85356 Matrix: Solids
Sample ID: Neilson WTP#1 Sampled: 1/12/2021 10:00
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Moisture 65.2 °A) 0.010 0.010 1 01/13/21 16:16 FMM SW-DRYWT
Ammonia Nitrogen 368 mg/Kg-dry 71.8 71.8 1 01/20/21 15:00 JPJ 4500NH3C-2011
Nitrate+Nitrite-N 23.1 mg/Kg-dry 14.4 14.4 1 01/19/21 14:27 ZBD 4500NO3F-2011
Organic N 2250 mg/Kg-dry 145.7 293.1 1 01/18/21 16:19 CALCULATION
pH 5.9 s.u. 1 01/20/21 15:36 CxC 9045D
Total Solids 34.8 % 0.010 0.010 1 01/13/21 16:16 FMM 2540G-2011
Total Volatile Solids 20.5 % 0.010 0.010 1 01/13/21 16:16 FMM 2540G-2011
Total Kjeldahl Nitrogen 2620 mg/Kg-dry 293 1 01/18/21 16:19 CLP 4500NORGD-2011
Phosphorus 1710 mg/Kg-dry 7.93 14.4 1 01/19/21 07:02 TJS 6010D
Aluminum 111000 mg/Kg-dry 66.4 71.8 5 01/20/21 19:39 TJS 6010D
Arsenic 7.50 mg/Kg-dry 0.689 1.44 1 01/19/21 07:02 TJS 6010D
Cadmium 0.931 mg/Kg-dry 0.0574 0.287 1 01/19/21 07:02 TJS 6010D
Calcium 928 mg/Kg-dry 111 144 1 01/19/21 07:02 TJS 6010D
Chromium 59.5 mg/Kg-dry 0.678 0.718 1 01/19/21 07:02 TJS 6010D
Copper 38.5 mg/Kg-dry 0.891 1.44 1 01/20/21 19:33 TJS 6010D
Iron 56300 mg/Kg-dry 122 144 5 01/20/21 19:39 TJS 6010D
Lead 26.2 mg/Kg-dry 0.517 0.862 1 01/20/21 19:33 TJS 6010D
Magnesium 6180 mg/Kg-dry 7.41 14.4 1 01/19/21 07:02 TJS 6010D
Manganese 523 mg/Kg-dry 0.933 1.44 1 01/19/21 07:02 JADS 6010D
Mercury 0.0862 mg/Kg-dry 0.00954 0.0434 1 01/14/21 11:41 DDB 7471A
Molybdenum 0.7123 mg/Kg-dry 0.387 0.718 1 01/19/21 07:02 TJS 6010D
Nickel 29.0 mg/Kg-dry 0.344 0.718 1 01/19/21 07:02 TJS 6010D
Potassium 5690 mg/Kg-dry 88.8 144 5 01/20/21 19:39 TJS 6010D
Qualifiers/ DF Dilution Factor J Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 5 of 14

Iwo
\Aaypo i nt.. 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytcal.com
46245
EMA Resources Inc Project Winston Salem
Mr. Brent Collins Report Date: 01/21/2021
755 Yadkinville Rd Information : Winston Salem, NC Received :01/13/2021
Mocksville, NC 27028 00Pn10-Q 0-3-Xa-
Report Number:21-013-0048 REPORT OF ANALYSIS Danyale Love
Project Manager
Lab No: 85356 Matrix: Solids
Sample ID :Neilson WTP#1 Sampled: 1/12/2021 10:00
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Selenium <0.919 mg/Kg-dry 0.919 1.44 1 01/19/21 07:02 TJS 6010D
Sodium 164 mg/Kg-dry 37.4 71.8 1 01/19/21 07:02 TJS 6010D
Zinc 112 mg/Kg-dry 2.33 3.59 1 01/19/21 07:02 TJS 6010D
Sulfur 1570 mg/Kg-dry 14.9 28.7 1 01/19/21 07:02 TJS 6010D
Sodium Absorption Ratio 0.25 Ratio 0.01 0.01 1 01/19/21 07:02 CALCULATION
Qualifiers/ DF Dilution Factor J Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 6 of 14

1/12/21 #1
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 164 57.072 23 2.481391
Calcium 928 322.944 20 16.1472
Magnesium 6180 2150.64 12 179.22
Percent Solids 34.8 Na+
SAR =
/2(Ca2+ +Mg2-�-)
SAR 0.25 V

w
Waypoint.. 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Winston Salem
Mr. Brent Collins Report Date: 01/21/2021
755 Yadkinville Rd Information : Winston Salem,NC Received :01/13/2021
Mocksville, NC 27028 00^Lo6Q-�Q1,3'D"
Report Number:21-013-0048 REPORT OF ANALYSIS Danyale Love
Project Manager
Lab No: 85357 Matrix: Solids
Sample ID: Neilson WTP#2 Sampled: 1/12/2021 10:15
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Moisture 59.7 % 0.010 0.010 1 01/13/21 16:16 FMM SW-DRYWT
Ammonia Nitrogen 400 mg/Kg-dry 62.0 62.0 1 01/20/21 15:00 JPJ 4500NH3C-2011
Nitrate+Nitrite-N 21.8 mg/Kg-dry 11.4 11.4 1 01/19/21 14:28 ZBD 4500NO3F-2011
Organic N 2454 mg/Kg-dry 123.1 248.1 1 01/18/21 16:22 CALCULATION
pH 5.9 s.u. 1 01/20/21 15:36 CxC 9045D
Total Solids 40.3 % 0.010 0.010 1 01/13/21 16:16 FMM 2540G-2011
Total Volatile Solids 17.9 % 0.010 0.010 1 01/13/21 16:16 FMM 2540G-2011
Total Kjeldahl Nitrogen 2850 mg/Kg-dry 248 1 01/18/21 16:22 CLP 4500NORGD-2011
Phosphorus 1500 mg/Kg-dry 6.85 12.4 1 01/19/21 07:08 TJS 6010D
Aluminum 95000 mg/Kg-dry 57.3 62.0 5 01/20/21 19:49 TJS 6010D
Arsenic 6.20 mg/Kg-dry 0.595 1.24 1 01/19/21 07:08 TJS 6010D
Cadmium 0.695 mg/Kg-dry 0.0496 0.248 1 01/19/21 07:08 TJS 6010D
Calcium 784 mg/Kg-dry 96.0 124 1 01/19/21 07:08 TJS 6010D
Chromium 46.7 mg/Kg-dry 0.585 0.620 1 01/19/21 07:08 TJS 6010D
Copper 34.7 mg/Kg-dry 0.769 1.24 1 01/20/21 19:44 TJS 6010D
Iron 45900 mg/Kg-dry 106 124 5 01/20/21 19:49 TJS 6010D
Lead 22.4 mg/Kg-dry 0.446 0.744 1 01/20/21 19:44 TJS 6010D
Magnesium 3420 mg/Kg-dry 6.40 12.4 1 01/19/21 07:08 TJS 6010D
Manganese 417 mg/Kg-dry 0.806 1.24 1 01/19/21 07:08 JADS 6010D
Mercury 0.0685 mg/Kg-dry 0.00836 0.0380 1 01/14/21 11:42 DDB 7471A
Molybdenum 0.590] mg/Kg-dry 0.334 0.620 1 01/19/21 07:08 TJS 6010D
Nickel 21.6 mg/Kg-dry 0.297 0.620 1 01/19/21 07:08 TJS 6010D
Potassium 3230 mg/Kg-dry 76.7 124 5 01/20/21 19:49 TJS 6010D
Qualifiers/ DF Dilution Factor J Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 7 of 14

w
\Vaypo i nt.. 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Winston Salem
Mr. Brent Collins Report Date : 01/21/2021
755 Yadkinville Rd Information : Winston Salem, NC Received : 01/13/2021
Mocksville, NC 27028 Uom� 9,Q. 0-3-)-Q-
Report Number:21-013-0048 REPORT OF ANALYSIS Danyale Love
Project Manager
Lab No : 85357 Matrix: Solids
Sample ID: Neilson WTP#2 Sampled: 1/12/2021 10:15
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Selenium <0.794 mg/Kg-dry 0.794 1.24 1 01/19/21 07:08 TJS 6010D
Sodium 131 mg/Kg-dry 32.3 62.0 1 01/19/21 07:08 TJS 6010D
Zinc 90.8 mg/Kg-dry 2.01 3.10 1 01/19/21 07:08 TJS 6010D
Sulfur 1500 mg/Kg-dry 12.9 24.8 1 01/19/21 07:08 TJS 6010D
Sodium Absorption Ratio 0.28 Ratio 0.01 0.01 1 01/19/21 07:08 CALCULATION
Qualifiers/ DF Dilution Factor J Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 8 of 14

1/12/21 #2
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 131 52.793 23 2.295348
Calcium 784 315.952 20 15.7976
Magnesium 3420 1378.26 12 114.855
Percent Solids 40.3 Naj
SAR =
(Ca24 -i-Mg2+)
SAR 0.28

W
Waypoi nt... 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Winston Salem
Mr. Brent Collins Report Date: 01/21/2021
755 Yadkinville Rd Information : Winston Salem,NC Received :01/13/2021
Mocksville, NC 27028 0 Gitl ,66Q- ())-A)--
Report Number:21-013-0048 REPORT OF ANALYSIS Danyale Love
Project Manager
Lab No: 85358 Matrix: Solids
Sample ID: Neilson WTP#3 Sampled: 1/12/2021 10:30
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Moisture 65.0 % 0.010 0.010 1 01/13/21 16:16 FMM SW-DRYWT
Ammonia Nitrogen 349 mg/Kg-dry 71.4 71.4 1 01/20/21 15:00 JPJ 4500NH3C-2011
Nitrate+Nitrite-N 30.0 mg/Kg-dry 14.3 14.3 1 01/19/21 14:28 ZBD 4500NO3F-2011
Organic N 2486 mg/Kg-dry 71.43 71.43 1 01/18/21 16:23 CALCULATION
pH 5.8 s.u. 1 01/20/21 15:36 CxC 9045D
Total Solids 35.0 % 0.010 0.010 1 01/13/21 16:16 FMM 2540G-2011
Total Volatile Solids 19.9 % 0.010 0.010 1 01/13/21 16:16 FMM 2540G-2011
Total Kjeldahl Nitrogen 2830 mg/Kg-dry 143 1 01/18/21 16:23 CLP 4500NORGD-2011
Phosphorus 1530 mg/Kg-dry 7.89 14.3 1 01/19/21 07:13 TJS 6010D
Aluminum 101000 mg/Kg-dry 66.0 71.4 5 01/20/21 19:59 TJS 6010D
Arsenic 6.97 mg/Kg-dry 0.685 1.43 1 01/19/21 07:13 TJS 6010D
Cadmium 0.654 mg/Kg-dry 0.0571 0.286 1 01/19/21 07:13 TJS 6010D
Calcium 726 mg/Kg-dry iii 143 1 01/19/21 07:13 TJS 6010D
Chromium 49.7 mg/Kg-dry 0.674 0.714 1 01/19/21 07:13 TJS 6010D
Copper 34.9 mg/Kg-dry 0.886 1.43 1 01/20/21 19:54 TJS 6010D
Iron 48000 mg/Kg-dry 122 143 5 01/20/21 19:59 TJS 6010D
Lead 24.1 mg/Kg-dry 0.514 0.857 1 01/20/21 19:54 TJS 6010D
Magnesium 4910 mg/Kg-dry 7.37 14.3 1 01/19/21 07:13 TJS 6010D
Manganese 469 mg/Kg-dry 0.928 1.43 1 01/19/21 07:13 JADS 6010D
Mercury 0.0723 mg/Kg-dry 0.00868 0.0394 1 01/14/21 11:43 DDB 7471A
Molybdenum 0.5853 mg/Kg-dry 0.385 0.714 1 01/19/21 07:13 TJS 6010D
Nickel 24.2 mg/Kg-dry 0.342 0.714 1 01/19/21 07:13 TJS 6010D
Potassium 4460 mg/Kg-dry 883 143 5 01/20/21 19:59 TJS 6010D
Qualifiers/ DF Dilution Factor 3 Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 9 of 14

,W0
Waypoi nt... 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Winston Salem
Mr. Brent Collins Report Date: 01/21/2021
755 Yadkinville Rd Information : Winston Salem,NC Received :01/13/2021
Mocksville, NC 27028 U OPEN Lo4QC Q)- -
Danyale Love
Report Number:21-013-0048 REPORT OF ANALYSIS Project Manager
Lab No: 85358 Matrix: Solids
Sample ID : Neilson WTP#3 Sampled: 1/12/2021 10:30
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Selenium <0.914 mg/Kg-dry 0.914 1.43 1 01/19/21 07:13 TJS 6010D
Sodium 147 mg/Kg-dry 37.1 71.4 1 01/19/21 07:13 TJS 6010D
Zinc 99.4 mg/Kg-dry 2.31 3.57 1 01/19/21 07:13 TJS 6010D
Sulfur 1510 mg/Kg-dry 14.8 28.6 1 01/19/21 07:13 TJS 6010D
Sodium Absorption Ratio 0.25 Ratio 0.01 0.01 1 01/19/21 07:13 CALCULATION
Qualifiers/ DF Dilution Factor J Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 10 of 14

1/12/21 #3
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 147 51.45 23 2.236957
Calcium 726 254.1 20 12.705
Magnesium 4910 1718.5 12 143.2083
Percent Solids 35 Na
SAR =
(Ca21 + Mg2+
SAR 0.25

w
Waypoint.. 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Winston Salem
Mr. Brent Collins Report Date : 01/21/2021
755 Yadkinville Rd Information : Winston Salem, NC Received : 01/13/2021
Mocksville, NC 27028 0 ^on 1
Danyale Love
Report Number:21-013-0048 REPORT OF ANALYSIS Project Manager
Lab No: 85359 Matrix: Solids
Sample ID : Neilson WTP#4 Sampled: 1/12/2021 10:45
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Moisture 62.8 % 0.010 0.010 1 01/13/21 16:16 FMM SW-DRYWT
Ammonia Nitrogen 419 mg/Kg-dry 67.2 67.2 1 01/20/21 15:00 JPJ 4500NH3C-2011
Nitrate+Nitrite-N 17.4 mg/Kg-dry 12.3 12.3 1 01/19/21 14:30 ZBD 4500NO3F-2011
Organic N 1930 mg/Kg-dry 134.1 271.5 1 01/18/21 16:24 CALCULATION
pH 5.8 s.u. 1 01/20/21 15:36 CxC 9045D
Total Solids 37.2 % 0.010 0.010 1 01/13/21 16:16 FMM 2540G-2011
Total Volatile Solids 19.7 % 0.010 0.010 1 01/13/21 16:16 FMM 2540G-2011
Total Kjeldahl Nitrogen 2350 mg/Kg-dry 272 1 01/18/21 16:24 CLP 4500NORGD-2011
Phosphorus 1460 mg/Kg-dry 7.42 13.4 1 01/19/21 07:18 TJS 6010D
Aluminum 92200 mg/Kg-dry 62.1 67.2 5 01/20/21 20:09 TJS 6010D
Arsenic 6.83 mg/Kg-dry 0.645 1.34 1 01/19/21 07:18 TJS 6010D
Cadmium 0.581 mg/Kg-dry 0.0537 0.269 1 01/19/21 07:18 TJS 6010D
Calcium 761 mg/Kg-dry 104 134 1 01/19/21 07:18 TJS 6010D
Chromium 44.9 mg/Kg-dry 0.634 0.672 1 01/19/21 07:18 TJS 6010D
Copper 34.1 mg/Kg-dry 0.833 1.34 1 01/20/21 20:04 TJS 6010D
Iron 43500 mg/Kg-dry 115 134 5 01/20/21 20:09 TJS 6010D
Lead 22.5 mg/Kg-dry 0.483 0.806 1 01/20/21 20:04 TJS 6010D
Magnesium 3760 mg/Kg-dry 6.94 13.4 1 01/19/21 07:18 TJS 6010D
Manganese 435 mg/Kg-dry 0.873 1.34 1 01/19/21 07:18 JADS 6010D
Mercury 0.0855 mg/Kg-dry 0.00854 0.0387 1 01/14/21 11:45 DDB 7471A
Molybdenum 0.6453 mg/Kg-dry 0.362 0.672 1 01/19/21 07:18 TJS 6010D
Nickel 21.5 mg/Kg-dry 0.322 0.672 1 01/19/21 07:18 TJS 6010D
Potassium 3440 mg/Kg-dry 83.1 134 5 01/20/21 20:09 TJS 6010D
Qualifiers/ DF Dilution Factor J Estimated value
Definitions L Limit Exceeded MQL Method Quantitation Limit
Page 11 of 14

vo
Waypoint. 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Winston Salem
Mr. Brent Collins Report Date: 01/21/2021
755 Yadkinville Rd Information : Winston Salem,NC Received :01/13/2021
Mocksville, NC 27028 0 Orn,64Q)-)--Cl-
Report Number:21-013-0048 REPORT OF ANALYSIS Danyale Love
Project Manager
Lab No: 85359 Matrix: Solids
Sample ID: Neilson WTP#4 Sampled: 1/12/2021 10:45
Test Results Units MDL MQL DF Date/Time By Analytical
Analyzed Method
Selenium <0.860 mg/Kg-dry 0.860 1.34 1 01/19/21 07:18 TJS 6010D
Sodium 131 mg/Kg-dry 34.9 67.2 1 01/19/21 07:18 TJS 6010D
Zinc 90.6 mg/Kg-dry 2.18 3.36 1 01/19/21 07:18 TJS 6010D
Sulfur 1510 mg/Kg-dry 13.9 26.9 1 01/19/21 07:18 TJS 6010D
Sodium Absorption Ratio 0.26 Ratio 0.01 0.01 1 01/19/21 07:18 CALCULATION
Qualifiers/ DF Dilution Factor J Estimated value
Definitions
Page 12 of 14

1/12/21 #4
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 131 48.732 23 2.118783
Calcium 761 283.092 20 14.1546
Magnesium 3760 1398.72 12 116.56
Percent Solids 37.2 Na+
SAR =
V z(Ca24 +Mgt+
SAR 0.26

Waypoi nt., 2790 Whitten Road,Memphis,TN 38133
Main 901.213.2400°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:46245
Customer Name: EMA Resources Inc
Report Number: 21-013-0048
Shipping Method
• Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: °4#102
Shipping container/cooler uncompromised? • Yes 0 No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No • Not Present
Custody seals intact on sample bottles? 0 Yes 0 No • Not Present
Chain of Custody(COC) present? • Yes 0 No
COC agrees with sample label(s)? • Yes 0 No
COC properly completed Yes 0 No
Samples in proper containers? • Yes 0 No
Sample containers intact? Yes 0 No
Sufficient sample volume for indicated test(s)? • Yes 0 No
All samples received within holding time? • Yes 0 No
Cooler temperature in compliance? Yes 0 No
Cooler/Samples arrived at the laboratory on ice. Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No • N/A
Water-VOA vials free of headspace 0 Yes 0 No • N/A
Trip Blanks received with VOAs 0 Yes 0 No • N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No N/A
High concentration container(48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol-14 d) r- Low conc pre-weighed vials (Sod Bis-14 d)
Special precautions or instructions included? 0 Yes • No
Comments:
Signature: KristinaA. McAdams Date &Time: 01/13/2021 09:20:07
Page 13 of 14

Client name/Address Client ProjaxManager/contact Ming Information For Laboratory Use Only
EMA Resources Inc Brent Collins Account#46245
755 Yadkinville Rd
Mocksviile,NC 27028
Project Description ProjeWsiteLocation(City/state) RUSH-AdtlonaIctwges apply M of Shipment Matrix
Key
-c/� C — Special Detection iimK(s) Fed Ex Hups QUSPs ww-Wastewater GW-Groundwater
iu r�J S?DA-sik.CE 04At Results Needed 0 Courier Client Drop Off Dw-Drinking Water S-soil/Sad O-Oil
P-Product M-Misc
Other
Project Number Project Manager Ptm>a<#
Project Manager Email Purchase Order Number Ste/Facility ID It
336-399-3646 [e-mail]
'�° - 03 z U) - A Cool<10C Na2S203(Micro OW
'� ��6. a ^> z e-CI o v Z3 B trtolGec
• C a a r C3 CE tq py�
ANALYTICAL `era' ° tID D rn 0 None Required
2790 Whitten Road U s` _� W Fe MOH p*fcln
c i U co Q -.'�.. F t ptic2
Memphis,TN 38133 Unless noted,all containers V (15 1 > r
[phone] per Table II of 40 CFR Part . x .0 '- 0 ^ /�/•,J� H tome j ic2
136. 1 a 2 h- 2 l— Q. V I too(c 6C NA2S2O3
Date Time Sample Identification z 2 o
Rego; Anaiysk/Preservative Comments/Notes
011/04 Ib:bDA /1iCIr_sent o(,�)j`P A e, l.s M M=s a Metals:ALAs,Ca,Cd,Cr,Cu,Fe,Pb
(ill ( 10=15Rrk A/i i o.., GJT7 .P, I 0-
{ r ►/' Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
j/44I to:1t.w.. IYtrZC,S:"1 r? ..3 I & / / V i ✓ t7
" IMA 16:44,ft AfEt.co,,i 43 IP-- I / is 6.- ' / / 17 1 V Lf . /
21-013-0048
iriitirrr 111r1r11r ,
EMA Resou Inc 09 19.46
Winston Sarceslem
For Laboratory Use Only
Sam try(Name-Print) Client Remarks/Cononents
Ice O stody Lab comments
rN /N / If
a/ rf Sludge Samples - Report Dry Weight
Y Time Received by:(SIGNATURE) Date Tine
1 i
OrP1.41t110 Temp Ref .(SIGNATURE) to Time Received by:(SIGNATURE) Date Time
ti
it (. , L I 1 Relinquished by:(SIGNATURE) Date Tune i by,(SIGNATURE) Date Time

7eAnaIica/® ANALYTICAL REPORT
National Center for Testing&Innovation January 2 5, 2 0 21 Cp
2
Tc
Lssl
EMA Resources
4
Sample Delivery Group: L1306180 Cn
Samples Received: 01/14/2021 s
Sr
Project Number:
Description: Sludge Winston Salem 6Qc
7
GI
Report To: Mr. Brent Collins
755 Yadkinville Road -Al
Mocksville, NC 27028
9
Sc
Entire Report Reviewed By: me Ca/A__
Justin Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values.This test report shall not be
reproduced,except in full,without written approval of the laboratory.Where applicable,sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068.Where sampling conducted by the customer,results relate to the accuracy of the information provided,
and as the samples are received.
4
f
, ;it,tiimi 40o
1.41)4e: . ...,:ileilillillisb-- .'
a
Pace Analytical National
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.co'ht
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 1 of 20

TABLE OF CONTENTS ONE LAB.NATIONWIDE. 10
Cp:Cover Page -
Tc:Table of Contents 2 L CIJ
Ss:Sample Summary 3 2Tc
Cn:Case Narrative 4
3
Sr:Sample Results 5 Ss
NEILSON WTP L1306180-01 5 4
Qc:Quality Control Summary 7 Cn
Wet Chemistry by Method 9012 B 7 5Sr
Wet Chemistry by Method 9034-9030B 8
6
Wet Chemistry by Method 9045D 9 Qc
Wet Chemistry by Method D93/1010A 10
GI
Mercury by Method 7470A 11
Metals(ICP)by Method 6010D 12AI
Volatile Organic Compounds(GC/MS)by Method 8260D 13
9
Chlorinated Acid Herbicides(GC) by Method 8151A 14 Sc
Pesticides(GC)by Method 8081B 15
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 16
GI:Glossary of Terms 18
Al:Accreditations& Locations 19
Sc:Sample Chain of Custody 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/21 16:23 2 of 20

SAMPLE SUMMARY ONE LAB.NATIONWIDE. 1111
Collected by Collected date/time Received date/time
NEILSON WTP L1306180-01 Waste Roy Whittaker 01/13/2109:00 01/14/2109:00
Cp
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 2TC
Preparation by Method 1311 WG1608546 1 01/20/2110:37 01/20/2110:37 IDW Mt.Juliet,TN
Preparation by Method 1311 WG1608795 1 01/20/2115:01 01/20/2115:01 IDW Mt.Juliet,TN
Wet Chemistry by Method 9012 B WG1608874 1 01/20/21 21:32 01/21/2115:45 JER Mt.Juliet,TN Ss
Wet Chemistry by Method 9034-9030B WG1608678 1 01/20/21 21:00 01/20/21 21:00 LDT Mt.Juliet,TN
Wet Chemistry by Method 9045D WG1607108 1 01/19/2116:48 01/20/2100:57 WOS Mt.Juliet,TN 4Cn
Wet Chemistry by Method D93/1010A WG1608937 1 01/21/21 03:59 01/21/2103:59 CAT Mt.Juliet,TN
Mercury by Method 7470A WG1609335 1 01/21/2111:52 01/21/2115:14 BMF Mt.Juliet,TN 5
Metals(ICP)by Method 6010D WG1609356 1 01/21/2112:18 01/21/2114:23 CCE Mt.Juliet,TN Sr
Volatile Organic Compounds(GC/MS)by Method 8260D WG1609535 1 01/21/2117:47 01/21/2117:47 JLB Mt.Juliet,TN
Chlorinated Acid Herbicides(GC)by Method 8151A WG1609799 1 01/22/21 01:29 01/22/2115:18 SSH Mt.Juliet,TN 6
QC
Pesticides(GC)by Method 8081B WG1609775 1 01/23/21 07:04 01/23/2115:00 TAB Mt.Juliet,TN
Semi Volatile Organic Compounds (GC/MS)by Method 8270E WG1610414 1 01/23/2111:25 01/24/21 07:25 AO Mt.Juliet,TN 7
GI
Al
9
SC
l
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 3 of 20

CASE NARRATIVE ONE LAB.NATIONWIDE.
Cp
All sample aliquots were received at the correct temperature, in the proper containers,with the
appropriate preservatives,and within method specified holding times,unless qualified or notated within
the report. Where applicable,all MDL(LOD)and RDL(LOQ)values reported for environmental samples Tc
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative,a non-conformance form 3
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my Ss
knowledge,all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory,and no information or data have been 4
knowingly withheld that would affect the quality of the data. Cn
5
Sr
6
Ati^ Qc
GI
Justin Carr AlJ
Project Manager
Sc
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
•
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 4 of 20

NEILSON WTP SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. 1111 I
Collected date/time: 01/13/21 09:00 L1306180
Preparation by Method 1311
Result Qualifier Prep Batch Cp
Analyte date/time
2
TCLP Extraction - 1/20/202110:37:17 AM WG1608546 Tc
TCLP ZHE Extraction - 1/20/20213:01:01 PM WG1608795
Fluid 1 1/20/202110:37:17 AM WG1608546 3
SS
Initial pH 5.60 1/20/202110:37:17 AM WG1608546
Final pH 4.97 1/20/202110:37:17 AM WG1608546
4
Cn
Wet Chemistry by Method 9012 B
S_
Result Qualifier RDL Dilution Analysis Batch Sr
Analyte mg/kg mg/kg date/time
Reactive Cyanide 0.266 J6 0.250 1 01/21/202115:45 WG1608874 6
Qc
Wet Chemistry by Method 9034-9030B
Result Qualifier RDL Dilution Analysis Batch GI
Analyte mg/kg mg/kg date/time
Reactive Sulfide ND 25.0 1 01/20/2021 21:00 WG1608678 Al
Wet Chemistry by Method 9045D 9Sc
Result Qualifier Dilution Analysis Batch
Analyte su date/time
Corrosivity by pH 6.44 T8 1 01/20/2021 00:57 WG1607108
Sample Narrative:
L1306180-01 WG1607108:6.44 at 20.1C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte Deg.F date/time
Ignitability DNI at 170 1 01/21/2021 03:59 WG1608937
Mercury by Method 7470A
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
Mercury ND 0.0100 0.20 1 01/21/202115:14 WG1609335
Metals (ICP) by Method 6010D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
Arsenic ND 0.100 5 1 01/21/202114:23 WG1609356
Barium 0.485 0.100 100 1 01/21/202114:23 WG1609356
Cadmium ND 0.100 1 1 01/21/202114:23 WG1609356
Chromium ND 0.100 5 1 01/21/202114:23 WG1609356
Lead ND 0.100 5 1 01/21/202114:23 WG1609356
Selenium ND 0.100 1 1 01/21/202114:23 WG1609356
Silver ND 0.100 5 1 01/21/202114:23 WG1609356
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
Benzene ND 0.0500 0.50 1 01/21/202117:47 WG1609535
Carbon tetrachloride ND 0.0500 0.50 1 01/21/202117:47 WG1609535
Chlorobenzene ND 0.0500 100 1 01/21/202117:47 WG1609535
Chloroform ND 0.250 6 1 01/21/202117:47 WG1609535
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 5 of 20

NEILSON WTP SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. SI
Collected date/time: 01/13/21 0 9:0 0 L1306180
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier RDL Limit Dilution Analysis Batch [E1
p
Analyte mg/I mg/I mg/I date/time
1,2-Dichloroethane ND 0.0500 0.50 1 01/21/202117:47 WG1609535 2Tc
1,1-Dichloroethene ND 0.0500 0.70 1 01/21/202117:47 WG1609535
2-Butanone(MEK) ND C3 0.500 200 1 01/21/202117:47 WG1609535 3
Tetrachloroethene ND 0.0500 0.70 1 01/21/202117:47 WG1609535 Ss
Trichloroethene ND 0.0500 0.50 1 01/21/202117:47 WG1609535
Vinyl chloride ND 0.0500 0.20 1 01/21/202117:47 WG1609535 4
Cn
(S)Toluene-d8 98.1 80.0-120 01/21/202117:47 WG1609535
(S)4-Bromolluorobenzene 90.9 770-126 01/21/20211747 WG1609535 5
(S)1,2-Dichloroethane-d4 95.8 70.0-130 01/21/202117..47 WG1609535 Sr
Chlorinated Acid Herbicides (GC) by Method 8151A 6Qc
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time 7GI
2,4,5-TP(Silvex) ND 0.00200 1 1 01/22/202115:18 WG1609799
2,4-0 ND 0.00200 10 1 01/22/202115:18 WG1609799
(S)2,4-Dichloropheny/Acetic Acid 115 14.0-158 01/22/202115:18 WG1609799 Al
Pesticides (GC) by Method 8081B 9Sc
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
Chlordane ND 0.00500 0.03 1 01/23/202115:00 WG1609775
Endrin ND 0.00500 0.02 1 01/23/202115:00 WG1609775 •
Heptachlor ND 0.00500 0.0080 1 01/23/202115:00 WG1609775
Lindane ND 0.00500 0.40 1 01/23/202115:00 WG1609775
Methoxychlor ND 0.00500 10 1 01/23/202115:00 WG1609775
Toxaphene ND 0.0100 0.50 1 01/23/202115:00 WG1609775
(S)Decachlorobipheny/ 69.6 10.0-128 01/23/202115:00 WG1609775
(S)Tetrachloro-m-xylene 79.2 10.0-127 01/23/202115:00 W61609775
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result Qualifier RDL Limit Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
1,4-Dichlorobenzene ND 0.100 7.50 1 01/24/2021 07:25 WG1610414
2,4-Dinitrotoluene ND 0.100 0.13 1 01/24/2021 07:25 WG1610414
Hexachlorobenzene ND 0.100 0.13 1 01/24/2021 07:25 WG1610414
Hexachloro-1,3-butadiene ND 0.100 0.50 1 01/24/2021 07:25 WG1610414
Hexachloroethane ND 0.100 3 1 01/24/2021 07:25 WG1610414
Nitrobenzene ND 0.100 2 1 01/24/2021 07:25 WG1610414
Pyridine ND 0.100 5 1 01/24/2021 07:25 WG1610414
3&4-Methyl Phenol ND 0.100 400 1 01/24/2021 07:25 WG1610414
2-Methylphenol ND 0.100 200 1 01/24/2021 07:25 WG1610414
Pentachlorophenol ND 0.100 100 1 01/24/2021 07:25 WG1610414
2,4,5-Trichlorophenol ND 0.100 400 1 01/24/2021 07:25 WG1610414
2,4,6-Trichlorophenol ND 0.100 2 1 01/24/2021 07:25 WG1610414
(S)2-Fluorophenol 50.0 10.0-120 01/24/202107:25 WG1610414
(S)Phenol-d5 31.1 10.0-120 01/24/202107.25 WG1610414
(S)Nitrobenzene-d5 80.3 10.0-127 01/24/202107:25 WG1610414
(S)2-Fluorobiphenyl 83.1 10.0-130 01/24/202107.25 WG1610414
(S)2,4,6-Tribromophenol 88.5 10.0-155 01/24/202107:25 WG1610414
(S)p-Terphenyl-d14 93.0 10.0-128 01/24/202107:25 WG1610414
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 6 of 20

WG1608874 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Ilk
Wet Chemistry by Method 9012 B L1306180-01
Method Blank (MB)
(MB)R3615005-1 01/21/2115:05 Cp
MB Result MB Qualifier MB MDL MB RDL
2
Analyte mg/kg mg/kg mg/kg Tc
Reactive Cyanide U 0.0390 0.250
SS
Original Sample(OS) • Duplicate(DUP)
4
(OS) •(DUP)R3615005-3 01/21/2115:36 Cn
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP D
Limits RP J Sr
Analyte mg/kg % %
Reactive Cyanide ND 1 0.000 20 6
QC
Original Sample(OS) • Duplicate(DUP) 713
(OS) •(DUP)R3615005-4 01/21/2115:39
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits cAI
Analyte mg/kg % %
Reactive Cyanide ND 1 0.000 20 95C
Laboratory Control Sample(LCS)
(LCS)R3615005-2 01/21/2115:06
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/kg mg/kg % %
Reactive Cyanide 2.50 2.23 89.3 85.0-115
L1305983-01 Original Sample(OS) • Matrix Spike (MS) • Matrix Spike Duplicate(MSD)
(OS)L1305983-01 01/21/2115:40•(MS)R3615005-5 01/21/2115:41-(MSD)R3615005-6 01/21/2115:42
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg % % % % %
Reactive Cyanide 1.67 ND 1.12 0.927 67.0 55.7 1 75.0-125 J6 J6 18.5 20
L1306180-01 Original Sample(OS) • Matrix Spike(MS) • Matrix Spike Duplicate(MSD)
(OS)L1306180-01 01/21/2115:45•(MS)R3615005-7 01/21/2115:48•(MSD)R3615005-8 01/21/2115:50
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg % % % % %
Reactive Cyanide 1.67 0.266 0.994 0.953 43.7 41.3 1 75.0-125 J6 J6 4.17 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 7 of 20

WG1608678 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Wet Chemistry by Method 9034-9030B L1306180-01
Method Blank (MB)
(MB)R3614572-1 01/20/2121:00 Cp
MB Result MB Qualifier MB MDL MB RDL
2
Analyte mg/kg mg/kg mg/kg TC
Reactive Sulfide U 7.63 25.0
3
Ss
Laboratory Control Sample (LCS)
4
(LCS)R3614572-2 01/20/21 21:00 Cn
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/kg mg/kg qo qo s Sr
Reactive Sulfide 100 92.2 92.2 70.0-130
6
QC
7
GI
lAl
9
SC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 8 of 20

WG1607108 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. .O
Wet Chemistry by Method 9045D L1306180-01
Laboratory Control Sample (LCS)
(LCS)R3614171-1 01/20/21 00:57 C�'
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
2
Analyte su su % % Tc
Corrosivity by pH 10.0 10.1 101 99.0-101
3
Sample Narrative: SS
LCS:10.07 at 18.9C
4
Cn
5
Sr
Qc
7
GI
Al
9
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 9 of 20

WG1608937 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. A*
Wet Chemistry by Method D93/1010A L13 0 618 0-01
Laboratory Control Sample(LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS)R3614633-1 01/21/21 03:59•(LCSD)R3614633-2 01/21/21 03:59 Cp
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
2
Analyte Deg.F Deg.F Deg.F % % % % % Tc
Ignitability 126 127 129 101 102 95.6-104 1.57 10
3
SS
4
Cn
5
Sr
e
Qc
7GI
Al
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 10 of 20

WG1609335 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Mercury by Method 7470A L1306180-01
Method Blank (MB)
(MB)R3614996-1 01/21/2114:52
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I Tc.
Mercury U 0.00330 0.0100
3
Ss
Laboratory Control Sample (LCS) 4
(LCS)R3614996-2 01/21/2114:54 Cn
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
5
Analyte mg/I mg/I % % Sr
Mercury 0.0300 0.0296 98.8 80.0-120
QC
7
GI
Al
9
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 11 of 20

WG1609356 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. 4k
Metals (ICP) by Method 6010D L1306180-01
Method Blank (MB)
(MB)R3614934-1 01/21/2113:48 I CFI
MB Result MB Qualifier MB MDL MB RDL
2
Analyte mg/I mg/I mg/I Tc
Arsenic U 0.0333 0.100
Barium U 0.0333 0.100 3SS
Cadmium U 0.0333 0.100
Chromium U 0.0333 0.100
a
Lead U 0.0333 0.100 Cn
Selenium U 0.0333 0.100 -
Silver U 0.0333 0.100 s
Sr
Laboratory Control Sample (LCS) GQc
(LCS)R3614934-2 01/21/2113:50
'Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier GI
Analyte mg/I mg/I % %
Arsenic 10.0 9.60 96.0 80.0-120
Barium 10.0 9.75 97.5 80.0-120
Cadmium 10.0 9.56 95.6 80.0-120
Chromium 10.0 9.75 97.5 80.0-120 Sc
Lead 10.0 9.83 98.3 80.0-120 _1
Selenium 10.0 9.72 97.2 80.0-120
Silver 2.00 1.73 86.5 80.0-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE
EMA Resources L1306180 01/25/2116:23 12 of 20

WG1609535 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1306180-01
Method Blank(MB)
(MB)R3615091-3 01/21/2116:20
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I I-Tc
Benzene U 0.0167 0.0500
Carbon tetrachloride U 0.0167 0.0500 SS
Chlorobenzene U 0.0167 0.0500
Chloroform U 0.0833 0.250
4
1,2-Dichloroethane U 0.0167 0.0500 Cn
1,1-Dichloroethene U 0.0167 0.0500
2-Butanone(MEK) U 0.167 0.500 'Sr
Tetrachloroethene U 0.0167 0.0500
Trichloroethene U 0.0167 0.0500 6
Vinyl chloride U 0.0167 0.0500 Qc
(S)Toluene-d8 99.2 80.0-120
(S)4-Bromofluorobenzene 89.8 77.0-126 -GI
(5)1,2-Dichloroethane-d4 96.1 70.0-130
Laboratory Control Sample(LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS)R3615091-1 01/21/21 09:32•(LCSD)R3615091-2 01/21/2115:58 4Sc
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I % % % % %
Benzene 0.250 0.249 0.229 99.6 91.6 70.0-123 8.37 20
Carbon tetrachloride 0.250 0.246 0.240 98.4 96.0 68.0-126 2.47 20
Chlorobenzene 0.250 0.250 0.232 100 92.8 80.0-121 7.47 20
Chloroform 0.250 0.269 0.255 108 102 73.0-120 5.34 20
1,2-Dichloroethane 0.250 0.258 0.245 103 98.0 70.0-128 5.17 20
1,1-Dichloroethene 0.250 0.278 0.259 111 104 71.0-124 7.08 20
2-Butanone(MEK) 1.25 0.865 0.847 69.2 67.8 44.0-160 2.10 20
Tetrachloroethene 0.250 0.271 0.255 108 102 72.0-132 6.08 20
Trichloroethene 0.250 0.235 0.214 94.0 85.6 78.0-124 9.35 20
Vinyl chloride 0.250 0.269 0.250 108 100 67.0-131 7.32 20
(S)Toluene-d8 96.4 97.7 80.0-120
(S)4-Bromofluorobenzene 91.2 93.6 77.0-126
(S)1,2-Dichloroethane-d4 97.2 98.6 70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE
EMA Resources L1306180 01/25/2116:23 13 of 20

WG1609799 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Chlorinated Acid Herbicides (GC) by Method 8151A L1306180-01
Method Blank (MB)
(MB)R3615526-1 01/22/2113:23
MB Result MB Qualifier MB MDL MB RDL
2
Analyte mg/I mg/I mg/I Tc
2,4-D U 0.000667 0.00200
2,4,5-TP(Silvex) U 0.000667 0.00200 3
(S)2,4-Dichlorophenyl Acetic 92.4 14.0-158 SS
Acid
4
Cn
Laboratory Control Sample(LCS)
(LCS)R3615526-2 01/22/2113:37 Sr
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier 6
Analyte mg/I mg/I % % Qc
2,4-D 0.0500 0.0462 92.4 50.0-120
2,4,5-TP(Silvex) 0.0500 0.0548 110 50.0-125
( 2,4-Dichlorophenyl Acetic 972 14.0-158 G
I
Add
L1305552-01 Original Sample(OS) • Matrix Spike(MS) • Matrix Spike Duplicate(MSD) I -
(OS)L1305552-01 01/22/2113:51•(MS)R3615526-3 01/22/2114:06•(MSD)R3615526-4 01/22/2114:20 Sc 1
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % %
2,4-D 0.0500 ND 0.0376 0.0422 75.2 84.4 1 50.0-120 11.5 20
2,4,5-TP(Silvex) 0.0500 ND 0.0432 0.0457 86.4 91.4 1 50.0-125 5.62 20
(S)Z,4-Dichlorophenyl Acetic 75.8 85.2 14.0-158
Add
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 14 of 20

WG1609775 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. 40
Pesticides (GC) by Method 8081B L1306180-01
Method Blank(MB)
(MB)R3615893-1 01/23/2113:13
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I Tc
Gamma BHC U 0.00167 0.00500
Endrin U 0.00167 0.00500 3SS
Heptachlor U 0.00167 0.00500
Methoxychlor U 0.00167 0.00500
4
Chlordane U 0.00167 0.00500 Cn
Toxaphene U 0.00333 0.0100
(S)Decachlorobiphenyl 72.0 10.0-128 5 Sr
(5)Tetrachloro-m xylene 76.0 10.0-127
6
Qc
Laboratory Control Sample(LCS)
(LCS)R3615893-2 01/23/2113:27
GI
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I mg/I % % Et Al
Gamma BHC 0.0100 0.00847 84.7 55.0-129
Endrin 0.0100 0.00868 86.8 57.0-134 _
Heptachlor 0.0100 0.00812 81.2 27.0-132 eSC
Methoxychlor 0.0100 0.0125 125 54.0-155 P
- (S)Decachlorobiphenyl 56.0 10.0-128
(5)Tetrachloro-m xylene 70.0 10.0-127
Original Sample(OS) • Matrix Spike(MS) • Matrix Spike Duplicate(MSD)
(OS) •(MS)R3615893-3 01/23/2114:07.(MSD)R3615893-4 01/23/2114:20
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I % % % %
Gamma BHC 0.0100 0.00853 0.00907 85.3 90.7 1 14.0-141 6.14 40
Endrin 0.0100 0.00873 0.00945 87.3 94.5 1 10.0-160 7.92 39
Heptachlor 0.0100 0.00824 0.00877 82.4 87.7 1 16.0-136 6.23 40
Methoxychlor 0.0100 0.0136 0.0143 136 143 1 10.0-160 P P 5.02 34
(S)Decachlorobiphenyl 55.5 63.4 10.0-128
(S)Tetrachloro-m-xylene 7L3 76.4 10.0-127
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 15 of 20

WG1610414 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. .*
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1306180-01
Method Blank (MB)
(MB)R3615744-2 01/24/21 06:21 Cp
MB Result MB Qualifier MB MDL MB RDL
2
Analyte mg/I mg/I mg/I Tc
1,4-Dichlorobenzene U 0.0333 0.100
2,4-Dinitrotoluene U 0.0333 0.100 JSS
Hexachlorobenzene U 0.0333 0.100
Hexachloro-1,3-butadiene U 0.0333 0.100
4
Hexachloroethane U 0.0333 0.100 Cn
Nitrobenzene U 0.0333 0.100
Pyridine U 0.0333 0.100 Sr5
2-Methylphenol U 0.0333 0.100
3&4-Methyl Phenol U 0.0333 0.100 6
Pentachlorophenol U 0.0333 0.100 QC
2,4,5-Trichlorophenol U 0.0333 0.100
2,4,6-Trichlorophenol U 0.0333 0.100 lGl
(S)Nitrobenzene-d5 76.9 10.0-127
(5)2-Fluorobiphenyl 79.9 10.0-130
(S)p-Terphenyl-d14 9t4 10.0-128 Al
(S)Phenol-d5 29.6 10.0-120 r
(5)2-Fluorophenol 49.0 10.0-120 9
SC
(S)2,4,6-Tribromophenol 92.0 10.0-155
Laboratory Control Sample(LCS)
(LCS)R3615744-1 01/24/21 05:59
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I mg/I % %
1,4-Dichlorobenzene 0.500 0.393 78.6 18.0-120
2,4-Dinitrotoluene 0.500 0.454 90.8 49.0-124
Hexachlorobenzene 0.500 0.478 95.6 44.0-120
Hexachloro-1,3-butadiene 0.500 0.451 90.2 19.0-120
Hexachloroethane 0.500 0.400 80.0 15.0-120
Nitrobenzene 0.500 0.380 76.0 27.0-120
Pyridine 0.500 0.130 26.0 10.0-120
2-Methylphenol 0.500 0.375 75.0 28.0-120
3&4-Methyl Phenol 0.500 0.383 76.6 31.0-120
Pentachlorophenol 0.500 0.391 78.2 23.0-120
2,4,5-Trichlorophenol 0.500 0.454 90.8 44.0-120
2,4,6-Trichlorophenol 0.500 0.435 87.0 42.0-120
(S)Nitrobenzene-d5 79.2 10.0-127
(S)2-Fluorobiphenyl 81.9 10.0-130
(S)p-Terphenyl-d14 86.7 10.0-128
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE
EMA Resources L1306180 01/25/2116:23 16 of 20

WG1610414 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1306180-01
Laboratory Control Sample (LCS) 1
(LCS)R3615744-1 01/24/21 05:59 Cp
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
2
Analyte mg/I mg/I % % IC
(S)Phenol-d5 30.9 10.0-120
(S)2-Fluorophenol 50.5 10.0-120
(S)2,4,6-Tribromophenol 102 10.0-155 SS
4
Cn
5
Sr
a
Qc
GI
Al
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 17 of 20

GLOSSARY OF TERMS ONE LAB.NATIONWIDE. 4110
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not C P
intended as a comprehensive explanation,and if you have additional questions please contact your project representative.
2
Results Disclaimer-Information that may be provided by the customer,and contained within this report,include Permit Limits,Project Name, Tc
Sample ID,Sample Matrix,Sample Preservation,Field Blanks,Field Spikes,Field Duplicates,On-Site Data,Sampling Collection Dates/Times,and
Sampling Location.Results relate to the accuracy of this information provided,and as the samples are received.
Abbreviations and Definitions 3Ss
MDL Method Detection Limit.
ND Not detected at the Reporting Limit(or MDL where applicable). Cn
RDL Reported Detection Limit.
Rec. Recovery. 5
RPD Relative Percent Difference. Sr
SDG Sample Delivery Group.
Surrogate(Surrogate Standard)-Analytes added to every blank,sample,Laboratory Control Sample/Duplicate and e
(S) Matrix Spike/Duplicate;used to evaluate analytical efficiency by measuring recovery.Surrogates are not expected to be QC
detected in all environmental media.
U Not detected at the Reporting Limit(or MDL where applicable). 6 i
Analyte The name of the particular compound or analysis performed.Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material,the sample preparation volume or weight values differ from the V Al
Dilution standard,or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report,the sample may be diluted for analysis.If a value different than 1 is used in this field,the
result reported has already been corrected for this factor. 9
These are the target%recovery ranges or%difference value that the laboratory has historically determined as normal SC
Limits for the method and analyte being reported.Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD)from a quality control
sample.The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported.If a Qualifier is present,a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result(corrected for any sample specific characteristics)reported for your sample.If there was
no measurable result returned for a specific analyte,the result in this column may state"ND"(Not Detected)or"BDL"
Result (Below Detectable Levels).The information in the results column should always be accompanied by either an MDL
(Method Detection Limit)or RDL(Reporting Detection Limit)that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty Confidence level of 2 sigma.
(Radiochemistry)
A brief discussion about the included sample results,including a discussion of any non-conformances to protocol
Case Narrative(Cn) observed either at sample receipt by the laboratory from the field or during the analytical process.If present,there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary(Qc) analytical methods to assist in evaluating the validity of the results reported for your samples.These analyses are not
being performed on your samples typically,but on laboratory generated material.
This is the document created in the field when your samples were initially collected.This is used to verify the time and
Sample Chain of date of collection,the person collecting the samples,and the analyses that the laboratory is requested to perform.This
Custody(Sc) chain of custody also documents all persons(excluding commercial shippers)that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples.These results are provided
Sample Results(Sr) by sample ID and are separated by the analyses performed on each sample.The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary(Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID,including the dates and
times of preparation and/or analysis.
Qualifier Description
C3 The reported concentration is an estimate.The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
J6 The sample matrix interfered with the ability to make any accurate determination;spike value is low.
P RPD between the primary and confirmatory analysis exceeded 40%.
T8 Sample(s)received past/too close to holding time expiration.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 18 of 20

ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIDE. 110
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location.One phone call,one point of contact,one laboratory.No other lab is as
accessible or prepared to handle your needs throughout the country.Our capacity and capability from our single location laboratory is comparable to the collective totals of the network i
laboratories In our industry.The most significant benefit to our one location design is the design of our laboratory campus.The model is conducive to accelerated productivity,decreasing C p
turn-around time,and preventing cross contamination,thus protecting sample integrity.Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
'Not all certifications held by the laboratory are applicable to the results reported in the attached report.
`Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
Tc
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN, 37122
Alabama 40660 Nebraska NE-OS-15-05 s
SS
Alaska 17-026 Nevada TN000032021-1
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey—NELAP TN002 4 C n
California 2932 New Mexico' TN00003
Colorado _ TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375 5
Sr
Florida E87487 North Carolina' DW21704
Georgia NELAP North Carolina' 41
Georgia' 923 North Dakota R-140 t
QC
Idaho TN00003 Ohio—VAP CL0069
Illinois _200008 _Oklahoma _ _9915 _
Indiana C-TN-01 Oregon TN200002_ GI
Iowa 364 Pennsylvania 68-02979 _
Kansas E-10277 Rhode Island LA000356 _
Kentucky 16 KY900.10 South Carolina 84004002 Al
Kentucky 2 16 _ South Dakota n/a
Louisiana A130792 Tennessee'` 2006
S
Louisiana LA018 Texas T104704245-20-18 SC
Maine TN00003 Texas5 LAB0152
Maryland -324 Utah TN000032021-11
Massachusetts -M-TN003 Vermont VT2006
Michigan 9958 Virginia 110033
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 998093910
Montana CERT0086 Wyoming A2LA
A2LA—ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA—ISO 170255 1461.02 - DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA—Crypto TN00003
Pace Analytical National 1313 Point Mallard Parkway SE Suite B Decatur, AL, 35601
Alabama 40160
ANSI National Accreditation Board L2239
Pace Analytical National 660 Bercut Dr. Ste. C Sacramento, CA, 95811
California 2961 Oregon CA300002
Minnesota 006-999-465 Washington C926
North Dakota R-214
Pace Analytical National 6000 South Eastern Avenue Ste 9A Las Vegas, NV, 89119
Nevada NV009412021-1
Pace Analytical National 1606 E. Brazos Street Suite D Victoria, TX, 77901
Texas T104704328-20-18
'Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity 'Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1306180 01/25/2116:23 19 of 20

Billing lr ormation: Ana vsls orrte ner Pr e hair of ust dy Page ni
EMA Resources
Mr.Brent Collins �.
755 Yadkinville Road Ch r r ii
°
55 Xadklnvllle Road �„�`
Motksville,1�1C 274} 8 � ,.
Mocksv►lle,NC 27028
l
Report to: Email'To;brent�eagins errraresosrcesirs com tt ' fi� asr ano1' '"
,At .` I '1` Im"'"'''Iull'trua7Uz
,Mr.Brent Collins '�� r; vtx sa7ssasa" �'-e,_,r`,
Project-Description:
City/State Please'Circle: e xx:6144584859 °;
Sludge �� ts -� Collected.�� �� PT MT- C �
Phone:33fr711 cant Project Lab Project '�` 7. ���
tlW
E135
wy Table
Cell d by(print): i€Faciity lb P. . 3 r �.
l lecte y igr at ire}. Quote# ew e
iTS t. (Lab MUST Be Notifiedl .m,,
See Day -awe'Day _ , ;� � �r 3
_ Next.Pay :s Day(RodOnly) Date Results Needed Ffu + U$tE tar
trts rnedi X T O Day 10 Day(Rad arty'
-Pa Packed on ice ti____- Y __ �e Day of a,trn� ; Yt
tilt,No ii-
Sample ID
Comp/Grab Matrix" Depth Date Time
Ctrs ;',
Retnark3 Sample a(lab nelvl
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s
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ear 2' .r 3a*
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Matrix:il Remarks:
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6W-Groundwater B-Bioassay srd1AIze
-.—
VAN-WasteWater Flaw Other BCCPPrrea tro 2t
DW-Drinking Water
R
$ti7lS fetti . 3Pla
or-Other ra h 4��
Rel'.,..�cy� Date: lime: „Rece€ved by tSi na re; t r€ `R � ti Ls�ae rwa 3 ' C T 1 c t z
43/al ff4;44Fit.4- ----, , ,i--- ''''=i,k,,''4*.-: '
'Rehm. fished.y:(Signature) De e: Time:. Received€a. 5i attire aCR3 $lar�lk• tlonregt idb gh to f m
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Relinquished by-(Signature) Date: T me: Fie rsrad csr eab g • T€na l lold ',co/tilt-le rfditl
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p
t ra � t i k`r+.. F 9 r:,„,��� w tlCr' �

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g A.L-1 87
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flog

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SA
NAj J 3 j/k� x ,q0.3 = a 9 3 "j/L , 3 0MeglL
6_ 2 S,-1 Moy/j .4163 31 S qs,, �� a_o
61. 30 , a.30 .2.3o
/07",s- is.so ¢icy ,s /3v,6G -4 , -E. b 5
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PA A/
----------
E-79.1 X GeS0 � - (Qs-X Ovo) -I- aI,
t_ _ + a oo 4 8'
q S'o ao 1- `),1 1, 8'
PA a -

3anikctr( goat Ea /tip/ 41 3
2 S- % Sol;clz
SA
G, 7116 x , '�S� = S�/. 1 b = 1 a,7 6
x $ 3 " = / 7I , s 1k_ = ly3 AI /L
at a.ac1
S I- (13 0,
PAN
x ( P30 - 3 Ll 7)3 a, 3 yD + 3�
1196. 9 —

`J aYl\kct�^ o� � So i /�
3 7 a. So 1 dS
SCR
,v4� 13 / y x 0, 372- 2 q 232.Mo1 _ P.3 = 2,/dt,e /L
L� 7 G/ 60/ki 8-3,O?, /L. a0 = l , l 6-Mn/L.
(1374._.. = )3Fg7 JL 1a- = 11b1$ 6 me /L
405-61/./6 ,14114,s: -1/ 6S; 36 ?ios
PA N
a.tI a.4 3 ) - �11 ®, y 19� �- / 7,
om x ),y 31 4, a.O ?,s_ 4 0, 11
PAN = 997

Section 4
• Maps of the residuals disposal sites

-Frank Small Farm a Legend
/7
LY Polygon Measure
- -
Site DA10 Field#01
Klopman Mal Rd— 111
- -
- - - - -- - - --- ----- -- - ------ -- --------- ----- ----
•
,-
, ^
• .
•
_ -
Google Earth
1000 ft
1Z 212' 3cog

Loflin 400-405; 18 (331.32 ac.)
itit* . - - --, . --‘,-- -- . .' .
fir!! Y= ' 44.*
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4I +u y ., AZ..' ,
•
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4. .. i • •109108.107.106.Ti 40 • 1 1 1
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r 317 -�, 04 1 '
* � i •95•96 •97 •98 •99 W0 • 1�
`t 74.
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'.; = fy ..f v- b ate_ •68 1 � , �,sa' ti 4
I,7.t,....,.-7,.:•.....-.-_-i-.'f F ivr-t.:k;;...';-7-.-.','i'-f±-e,A,..-:•Vi-.k,,i---fi--Ii..:,t j.,.i-
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f''^ pp 75 •7 r
.•9.
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Date:Apr 26,2018 I [,Field Boundary
Field Name: Loflin 400-405; 18
Fann Name:2F Farms
Client Name:2F Farms
Total Acres:331.32
Field Boundary Start Location:
Latitude:35.62255293
Longitude:-8(1.09529853
ONOP`.FOCUS

Section 5
• Field soil sampling results

EMA Resources, Inc. EmA Invoice
755 Yadkinville Rd —Resources,Inc. Date Invoice#
Mocksville,NC 27028
1/31/2021 7060
Bill To
City of Winston Salem
PO Box 2511
Winston Salem,NC 27102
Attn:Accounts Payable
P.D. No. Terms Project
Due Upon Receipt
Quantity Description Rate Amount
Hauling Services-Neilson WTP I/18/21 - 1/28/21
5,925 5925 cubic yards L$19.38 19.38 114,826.50
173 Agricultural Lime- 173 tons @$60.35 60.35 10,440.55
Total $125,267.05
Phone [phone] —Fax [phone]
755 Yadkinville Road—Mocksville,NC 27028

SPILL iAN' .UME & 'FERTILIZER .
7682 Hwy. 801 $ • P.O. Box 738
COOLEEM"_ , NC 27014 = .
336-284-2551
NAME DATE
•
/1///) f. C,5014'C 5 ,2[. //Aop j
ADDRESS
PHONE
_ ©C i. V. a . i/C
SOLD BY CASH C.O.D. CHARGE ON ACCT. MDSE.REVD
OTY. . DESCRIPTION AMOUNT '
[. 10- 20 - 20
17 . 17 - 17
14- 14 - 14 •
19- 19. 19 .
• 18 - 9 - 9
•
NITROGEN
lvA;S
/7 9 LIME co 40 7 f Q `3 o oo . ..
IA0t FZL I
TAX 7(00
RECEIVED BY
TOTAL f/0s6 __
3368 THANK YOU
A9 claims and raturned goods MUST Oa accompanied by Ihts hill.
f

KT
r."- + Waters Agoailtural Laboratories.Inc.
I; ' �'^.a- r ! P.O.Box 382 257 Ne+ytan Hwy
3144 vCl. iii 1] b.}IS!S ReH' ..( WAT RSA RIFU'TURAL Camila•GA 31730
25S2 C1iCt1.A BROOK Rf) LABQRIi RIB INC. [phone] FAX[phone]
Tit-1'ON GA '17')4- Grower Code: \\
Grower: 2F Farms Field ID: ��// �` Test Method;Mel)lich!II
Loftin 400 405
Page 7
P K M S /Lab I , ii_ _li:: �. _�
Sample ._ --
p IbS/A lbs/A lbs/A lbs/A Soil Buffer lbs/A fbs/A lbs/A lbs/A lbs/A lbs/A % IbslA megrliog % % ofo
Number ID
pH pH
852150WC 61 535 VII^954 Vti \�i ,(� � K Mg Ca H
I 659 2692 6.3 7.65 37 Al 1.5 It 38.2 VII 199 sal 386 VII 10.6 VII
852151WC 62 368 �'� 798 vli 1073 VII 2809 l 6.02 120.4 �13.5 9.1 20.3 49.9 20.7
2809 6.3 7.55 44 NI 1.7 ii i 279 VII 386 \'ii 438 VII 10.3 vti
852152WC 63 �'li veVII --- L ' 5.6 112 16.1 _ 6.3 27.7 43.E22.3
419 789 I 995 I 3171 61i 6.3 7.65 51 A 1.6 it vti \1i it
862153WC 64 VII � 33.1 342 tt481 �'IIiii 11.0 vil
l 340 704 vi+ 925 c'tt 2389 "H I i 5.159 1039 15.9 6.9 26.1 49.9 17.6
852154WC 1 65 ! � 6.1 7.70 49 NI 1,4 •� 25,7 vi1 219 v11151U vit
l 209 \nt 395 vii 492 VII vit � 9.3 vit 3.95 � 79 13.1 ( 6.9 29.4 45.5 18.3
1463 6.2 7.80 42 m 1.2 A 16.0 Viil 179 viiI586 viii 5.7 vit 3.83 76.6 L 7.8 6.5 26.2 46.8 20.5
852155WC 66 137 It 558 vii l 743 \7i 1727 vit 6.1 7.60 51 A 1.5 III 13.0 VII i97 t11 603 VII 6.1 vill 4.01 80.2 11.3 6.3 27.3 38.1 28.2
8521566WC I 67 I 162 vii 578 VII l 708 vii l 1920 Vu 6 7.70 44 '•t ' vn \71 4.1.4 J f3.5 264 487 \'irl 5.8 vrrl 4.52 90.4 10.9 S.8 27.1 44.1 22.0
852157WC 68 1 174 vii 467 vii 529- vtll 2178 VII 6.3 7.65 35 �I - - 3
852758WC 69 t�i \�t wr 1.4 A f 14.4 V11 248 \1I1506 VII 5.6 vit 5.18 103.6 11.0 � 5.4 20.0 49.3 25.3 359 769 502 I 2701 VII 6.3 7.70 36 +i 1.6 ti 28.4 VII 214 vii 460 vn 8.2 VII 852159WC � 70 82 ^ 319 it 891 Ali I 111 l5.98 119.6 12.2 8.1 17.1 55.2 19.6
2661 6.5 7.65 29 +I 1.6 It 119.8 virl 344 1T11370 vtll 6.0 vial 4.69 93.8 13.6 3.0 27.4 49.0 20.6
ir
Soil Fertility Recommendations (Ibs./Acre) -=Maintenance Recommendation
..I� tv1'- i"_ mil
61 CORN 175 BUSHELS
62 l CORN 175 BUSHELS � I 250 10
I
63 1 CORN 175 BUSHELS I f 250
' 10
64 ( CORN 175 BUSHELS I I -
l l 250 1
I �__..... 1
65 CORN !0 )
665 CORN 175
BUSHELS I 250 I 70 - I 10 I I
175 BUSHELS I l 250 S0 i I 10 I l 5.0 l --`J
67 CORN 175 BUSHELS
68 CORN 175 BUSHELS I 250 4 50 i I L iQ i i 5.0 ---_
69 CORN 175 BUSHELS I 250 250 SU -I 10 r( L
� CORN 1 '^- .{
Comments 175 BUSHELS I _ .__ �_--I 250 J 60 * 80 I I 16 j I _ 1."
15 L13S OF NITROGEN AND 50 1.13S OF PI105PHATE RECOMMENDED AS A STARTER ON A1.I.CORN.FERTILIZER APPLIED AS A STAR'rtig,
SIIGLII.D RE DEDUCTED FRCAI ABOVE.BE SIMI.TiIATSULFUR IS APPLIED IN ORDER TihAT NITROGEN_SIiI.FUR RATIO IS 11AiNTAlNFD.
SC(iGE.STTAKINC;PL.1NT SAMPi US DURING THE GROWING SEASON ADDI'17ONA1.NUTRIENTS MAY HE NEEDED,ESPECIALLY Nr1ROGFEN ANt)POTASSIIJ i
I L=Low M=Medium A=Adequate H=High VH=Very High - C

!C"i' G=j Waters Agricultural Laboratories.Inc.
Soil Analysis Report ' 1'•U Box 332 2S Newton Mvy
3144 UUATE�.}R_ A�RlU�TURAL Cam11a.GA 35730
2552 CI1U1 A BROOKRf) LABORA RE ,S,INC. 326-7216 FAX[phone]
-17P'It)N GA 3179.1- Grower Code:
Grower: 2F FarmsField 10: Loilin 400-405 Test Method:Mehlich III
Page 8
.t P K Mg pH S
Ca B Zn Mn Fe CuGu OM
•
Lab Sample lbs/A lbs/A lbs/A lbs/A Soil Buffer lbs/A lbs/A lbs/A IbsIA tbs/A Ibs/A % IbstA megl100g % % %Number ID pH pH
_ K IVig Ca H
852160WC l- 71~ S2 hi 252 II 803 VII 2611 vii 6.2 7.65 27 a! A I vn vE[
1.424.1 1185 I379 vH 5.2 vH 4.87 97.4 13.0 2.5 25.7 50.2 21.5
852161WC 72 _ 89 A 281 ii 695 vii 2605 vit 6.1 7.60 26 M 1.6 II 1 24.3 \III 156 1111424 vii 5,6 vII 5.29 105.8 13.0 2.8 22.3 50.2 24.7_
852162WC I 73 137 F1 417 vII 526 vII 1929 vIl 6.1 7.70 36 JI 1.5 A 120.7 will 137 vn!1463 vii 5,9 vat 4.76 95.2 9.9 5.4 22.0 48.5 24.1
852163WC 74 292 vII 779 v11 676 vII 2595 v'II 6.2 7.60 44 M 1.8 ii[38.9 viil 22g v7i1464 vii 9,6 VI 5.21 104.2 13.5 7.4 20.9 48.0 23.7
852164WC 75 i 273 Nit! 881 WI 504 vii 2232 vII 6.2 7.65 38 i 1.6 iE; 24.0 vn 281 vII 320 vIl 6.9 v11 5.63 112.6 11.6 9.7 18.1 48.1 24.1 852165WC 76 231 vn) 733 vII 528 v'li l 2500 viI 6.3 7.65 37 XI 1.7 II f 16.9 vII 387 vII 422 will 5.7 vii 5.79 115.8 12.2 l 7.7 18.0 51.3 23.0
852166WC 77 I 337 vii 702 vII 442 v'li 2127 FII 6 7.65 49 sl 1.5 A 28.4 vit 251 vII 379 vs 8.0 vII 5.79 I115.8 10.9 8.3 17.0 49.0 25.8
852167WC 78 256 \'FI 762 "J1 I 531• vII I 2345 v11 6.2 7.50 41 NI 1.7 II 1 23-9 vnI 277 v1I 331 VII6.7 VH 5.6 112 l 13.1 7.5 17.0 44.9 30.6_I
852168WC , 79 228 vII 586 v"l I 614 III l 2370 vl' 6.1 7.65 37 +i 1.6 }1 129.8 v'11 187 11i 437 val 7.8 "II 5.1 102 L^12.0 6.2 21.3 49.2 23.3
L 852169WC 80 i 186 ‘II 451 vii I 1106 ‘'II I 3391 CFI 6.1 7.55 31 a1 1.8 II I 39.5 vrll 122 vII 559 v'iij 9.5 vII, 5.74 114.8 17.3 13.3 26.7 49.1 20.9
Soil Fertility Recommendations (lbs./Acre) '=Maintenance Recommendation
Sample
ID r dls.r„ Ii
71 CORN 175 BUSHELS f 250 80 95 18
I.---- __72._ _..... ..... ... CORN
•
. .
175 BUSHELS 250 55. _... 90 ig ..
73 CORN 175 BUSHELS 250 S0 70 ' 10 I
74 CORN 175 BUSHELS I 250 10 1
75 CORN 175 BUSHELS I 250 •
L� � 10 i _L._ ___I__._-_
76 CORN 175 BUSHELS 250 _ I 10 I
I 77 am 175 BUSHELS 250 L ^-- I 20 I I 1
j-
1------___ 250 175 BUSHELS �- __._ 250 I 10 I I
CORN
7978 CORN 175 BUSHELS '� - } I _ L _
_ _.-_.. �- _.-1�.-.10 J. '
I_� so I �eoRN 17SBUSHELS ' _ r _ ( 1__-_.__.----
- I 250 • 50 14 I II
Comments _. --L---.____..
15 1.BS OF NITROGL••N AND 50 I.I8S OF PIk)SPIIATii R13(•OMMI'NUt n AS A ST\RrtiR(IN All..(OItN.FFItTII_U.Iat AI'PIM 1,AS A STARTHR.
SHOULD HI1 DBDUCfBD,FRUM AROVF.RE SURE TI1AT St II FUR IS APPLIED IN ORDER TIIAT NPTRoGFN-St 9,FUR RATIO IS\MAINTAINED.
St CCIFs'r TAKING PLANT SAMPLES DURING TINE GROWING 5liASON ADD TIONAI-NUTRIENTS MAY HE NGEDI;D,HSPIS IAI.l-Y NITROGEN N AND
PUTASSII 7eI.
L=Low M=Medium A=Adequate H=Nigh VH_Very High ]

KT
Waters Agricultural Laboratories.Inc.
Soil Analysis Report I P.O.Box382 A 122(336.7y
3144 WLAB R�I Uk,INC. Camille.GA 31730
2552 C'I1IA.A BROOK}tI) LAB �A kt INC. )229)336-7316 FAX[phone]
TII fON GA ;f 7r1•I- Grower Code:
Grower: 2F Farms Field ID: l.ollin 400-105 Test Method:Mehfich III
Page 9
K Mg Ca pH S B Zn Mn Fe Cu OM CEC B3S: '� +�, , ,.
Lab Sample lbs/A • lbs/A lbs/A lbs/A Soil Buffer lbs/A lbs/A lbs/A lbs/A ibs/A Ibs/A % tbstA meq/100g % % % %
Number ID pH pH
K Mg Ca H
852170WC 81 I 174 vit 576 vII 673 Vn 2499 vrI 6.5 7.75 35 M 1.8 II 31.0 vUJ' 237 vil 489 vll 8.3 vrJ 3
4.73 I94.61 11.8 6. 23.8 -
53.0 17.0
852171WC 82 I 150 It 663 vII 785 VII 2876 "I 6 7.50 43 NI 1.7 II 31.3 \'II 210 \'II 297 vII 8.8 vII 5.65 1113 15.3 5.6 21.4 852172WC I 83 118 A 443 vlt 523 vII 1834 VII 5.6 7.55 50 XI A VII VIl -_ I I 47.0 26.19
852173WC as 36 L 259 tI vn 1.4 � 19.0 142 266 \u 5.0 vII 4,B3 � 96.6 � 10.9 � 52 19.9 41.9. 32.9
533 I 1540 vll 5.3 7.45 47 si 1.2 ,A 1 9.6 II 230 vII 328 VII 3.3 vII 4.5 90 1 10.8 3.1 20.6 35.6 40.7 I
852174WC 85 37 L 189 A 799 vil 1488 vN 6.1 7.65 43 M 1.1 A 6.8 A 203 \'I+304 v11I 2,7 II 3.83 76.6 10.1 2.4 33.0 36.9 27.7 I
852175WC 86 27 L 199 A 1 885 vII 1247 vII 6.1 7.45 34 m 1.0 X1 1 5.7 A 204 vII 366 v Ie
852176WC 87 27 I- 260 rl vll II � 2.4 4.31 86.2 11.5 22 32.2 272 38.4�
1 408 10605.5 7.60 51 A 11 A 1 4.9 \I 290 vtr 314 vu 2.3 II 14.12 182.4 7.9 I 4.2 21.6 33.6 40.6 I
852177WC 88 29 L 303 II I 437.. vII 1467 v11 5.6 7.50 46 M 1.3 A ; 8.1 II O259 \'7I 319 vttl 4.1 vu 4.13 82.6 9.9 I 3.9 18.4 37.1 40.5_I 852178WC f 89 f 27 I- 217 A 417 VLI{ 849 A 5.3 7.55 65 A 11 A 1 4.4 to 257 vII 283 VII - -"`
852179WG 90 I. A VIJ 2.3 II � 3.96 79.2 7.7 I 3.6 22.5 27.4`46.5 I
II 14 203262 709 A 4.8 7.25 66 ,\ 1A NI 1 3.8 AI 136 vII 301 vIII 2.0 If 4.27 85.4 I 9.1 1 29 120 19.4 65.8 I
Sod Fertility Recommendations (Ibs./Acre) =Maintenance Recommendation
�afr.lu
i i Yield Lime ,•
Gypsum v 41 a
81 CORN 175 BUSHELS 250 S0 10
I
.175 BUSHELS 250 I 50 10
83 CORN
175 BUSHELS 250 * 50 70 ' 10
84 CORN 175 BUSHELS 1.2 � 250 105 90 I 10 j 5.0 - -
85 CORN 175 BUSHELS 250 I �-
05 160 10 I 0.1 5.086
CORN 175 BUSHELS I 250 115 -`
150
87 CORN 175 BUSHELS 0.7 - I I I 11 1 0.2 5.0� I I
I I 250 L 115 I ,90 I 10 • I 0.1 l 5.0
88 CORN 175 BUSHELS 0.8 I 250 115 I 80 -L 10 I 5.0
89 CORN 175 BUSHELS 1.0 J 250 115 130 10 I 0.1 5.0 i -
175 BUSHELS 2.0 II_______
� 90 CORN 250 130 145 I �._V
�..__ I 10 0.2 5.0 I
Comments --_ --._ L__-__.L_._----___..
IS LI3S OF NITROGEN AND 50 LIDS OF PIIOSPI!ATE RECOMMENDED AS A STARTER ON ALL CORN.FERTILIZER ILIZ1 R APPLIED AS A STARTER.
SIIOI71.D RE DEDUCTED I)FROM ABOVE.BESIRETILT SI'LFtIR Iti APPLIED IN ORDER THATNITR(KipR-SI:).FIIR kA'rl(IS MAINTAINED.
SUGGEST TARING PLANT SAMPLES DURING SEASON.ADDI'I'IUNAI.xtrren NTl'r&VI'131i NEEDED,ESPECIALLY NITIt)GEN AND
PO'J'ASSILrM.
1 _ L=Low M=Medium A=Adequate H=High VH=Very High _1 c

icr
rc +` W orx Agnculll o P.O.Box 382 ure 257 NovdLeborafanon Hs,wyInc.
Soil Soil Analysis Report WATERS,A RI Li)_TURAL Cxmilla.GA31730
I'fUl.r\BROOK LAB RA, RPg6,INC. Comilla.
FAX
2552C
TtFTON GA 31794-, Grower Code:
•
Grower: 2F Farms •
Field ID: Lorna 400-405 Test Method:Mehlich Ili
Page 10
6
P K
_:. .., M,9 Ca pH S B Zn Mn Fe Cu OM ti CEC �'�. .
Lab Number Sample lbs/A ' ibs/A tbs/A • ibs/A Soil Buffer lbs/A lbs/A lbs/A lbs/A lbs/A lbs/A % IhslA mednoo9 % % % n�
pH pH
K Mg Ca H
852180WC I� 91 I 44 M 263 a 1 851 VII 1599 k1! 5.5 7.55 44 M 1.0 A 8.8 H 178 va1410 va ,�_
852181WC 92 289 4i6 980 II i 3.2 vl1 4.72 94.4 11,5 2.9 30.9 34.8 31.4
I 51 M II f 5 VII 5.4 7.45 36 n'J 1.1 A 6.3 eA 150 va 490 vII 2.6 II 4.71 94.2 9.0 4.1 19.4 27.4 49.1 852182WC 93 187 vn 576 VII I 432 Vii 1723 va 5.8 7.65 37 M 1.4 A 15.7 va 225 Ali 4.9 v 359 vii vN 5 470 .2 VII
852183WC 94 � 134 i3 511 vil 4S3 vn 1590 191 _.______ ___.__ _- 15.04 100.8 9.6 7.7 18.7 44.7 29.0 I
5.8 7.50 46 M 1.3 A 1 11.9 VII 369 va 359
a) va 6 -'- - ' 4.45 89 10.6 6.2 18.3 37.6 37.9 852184WC 95 116 A 437 VII 551 vJ
1490 7,65 46 M _ 1.2 L112.0 VII 359 vi1 387 "II 4,5 vU 4.1 82 9.4 6.0 24.5 39.7 29.8 I
852185WC 96 215 v}1 529 vH 690 VII 2011 va 5.8 7.60 45 M 1.4 A i 18.3 va 229 A1(496 vII VII
852186WC 97 I. li `-`w)1 � 5.4 1 5.01 1100.2 11.8 5.8 24.4 42.7 27.2
28 265 389 998 N 5.8 7,60 31 NI 1.0 A i 5.0 A 213 1111550 VII 2.2 II, 4.04 180.8 7.7 4.4 21.2 32.6 41.8
852187WC 98 25 I- 217 A 244' va I 747 A 5.2 7.40 48 NI 1.0 A 14.7 xi 123 " 1'327 VII 1.8 II
852188WC 99 I L n VII VII - -- 4.38 187.6 8.0 3.5 12.s _ __I
60.3
30 308 I 388 1673 5.6 7.50 70 A 1.1 A 16.6 A 135 vII1368 v1II 2.4 II 4.7 j 94 10.2 3.9 15.9 41.0 39.2
852189WC I 100 i 60 14 450 vaI 439 va 2297 vit 6.2 7.55 40 M, 1.6 n 1 7.1 A 221 VU 384 VII 3.9 vil 4.73 1 94.6 I 11.7 4.9 15.6 48.9 30.6 I
Soil Fertility Recommendations (lbs./Acre) Maintenance Recommendation
Sample - ,.
ID r" i r h., '` w�f Fc Cu
91 CORN 175 BUSHELS 0.8 250 100 90 10 0.2 ] 5.0
92 CORN
175 BUSHELS 1.1 250 90 ]
90
93 CORN 175 BUSHELS I _ 250 • 50 ] 10 0.1 5.0
10
94 CORN 175 BUSHELS 0.5 I_. ____.__. 250 * 50 10
. __.-__-._
5.0
95 CORN 175 BUSHELS ] I I 250 • 50 ] 70 10 I 1 5.0
96 CORN175 BUSHELS ] + 250 10 -.-
97 coati 175 BUSHELS 1 0.4 i 250 115 90 14 0.2 II 5.0 _L
98 CORN _._.L...._... - _
_ 175 BUSHELS T_1.4 i 250 120 130 - ] 10 0.2 ' 5.0i
99 CORN 175 BUSHELS ] 0.8 ' 250 110 80 �- 10 0.1 5.0 �- L
100 I CORN 175 BUSHELS ] I 250 I 80J 70 10 + i 5.0
Comments
IS 1.135 CIF NITROGEN AND SO 1.135 OF PiloSI'II,ITL'RF.0 OMmEN:o D AS A S F.\RTER ON AI.1.CORN,FERTILIZER APPLIED AS A STARTER.
SHOULD 13E DEDIiCrED FRoi l ABOVE HEM IRE THATS111.F1JR IS APPLIEi)iN ORDER TIIAT NITROGEN-SL!i.F!IR RATIO IS MAINT.\NFT)
SUGGEST TAKING PLANT SAMPLES DURING TIIF GROWING SEASON.ADDITIONAL.NUTRIENTS MAY HE NEEDED,FSPk('IAL1.1.NITROGEN AND
IKYI'ASS I t:M.
L=Low M=Medium A=Adequate H=High VH=Very High o

1C'f
p lc+ �q f". 1 Wafers AguaiRurs113bwatoucs.It
3144 SOH Analysis Report I i P.O.Box382 257GA 31730 Hwy
WATERS A RICll��-'TEIRAL CamdW GA 31730
-'.`?3 CI1E)!.A BROOK RB LAB f}A �RI, S,INC. (2Fs)335-7216 FAX[phone]
TIF ON GA 3I794- Grower Code:
Grower: 2F Farms •
Feld ID: Test Method:Mehlich III
•
1..oilin 400-405
Page 11
awn iiii,
P K.. Mg pH
IMp Q t;
E
LabIIIII
Sample lbs/A * ibslA � M k -.
Number ID EbslA lbs/A Soif Buffer !bslA ibslA fbs)A IbsJA lbs/A IbslA % IbstA megnotlg % % % %
pH pH
852190WC 101 u vtr VI K Mg Ca H
53 401 335 1569 ti'rl - --
5.8 7,60 � 42 ^+ 1_1 ^ ( 8.5 11 378 11+340 v+1 5,4 VI! 4.52 90.4 1 9.0 5.7 15.5 43.4 35.4
852191WC 102 63 M 490 111 378 1'11 2010 v11 5.9 7.50 29 MA ; ttan
852192WC 103 at vll --_. 1.4 9.9 165 270 \'I1} 4.1 ti'1+ 4.75 95 1 11.2 5.6 14.0 44.8 35.6
54 333 J 453 1'11 I 1989 v11 6.2 7.70 22 L 1.2 A 6.7 LI 137 VII 342 v11
852193WC 104 --- 44 tit vtt � 3.8 �'++( 4.22 84.4 I 9.7 � 4.4 19.5 51.3 24.8 I
I367 390 vn 1670 �1i 6.4 •� 178 1111275 vIll 5.1 vIIJ 4.09 81.8 9.5 j 5.0 17.2 44,1 33.8
6.1 7.60 38 N 1.2 -•�
852194WC 105 33 L 421 VI1 411 "U' 1601 VII 5.7 7.60 54 �1 1.2 ; ; 6.4 ^ 107 11+259 vn
852195WC 106 M H ( �,11 � I � 3.8 v11 i 2.13 42.6 9.5 5.7 18.1 42.3 33.8 41282380 1244 "71 5.5 7.40 i 35 a1 1.1 A^ 6.1 •)( 410 1111331 vnf 3.5 VIII 4.46 ( 89.2 1 9.9 3.7 16.1 31.6 48.7 I
852196WC 107 ' 59 .1 393 v11 743 111 1592 1111 6 7.60 31 NI 1.1 A v11
852197WC 108 , v1- 8.0 � 469 1493 tnl 4.9 vr1
I 120 551 r 510- vn 1570 vrr + 1 5.041 1102.4 10.8 4.7 19.8 36.5 29.7 I
5.6 7.50 51 A 1.3 A" 11.1 vtl 414 v1i1453 vlt 4.7 vn
852198WC 109 100 ^ 542 vr1 465 v11 v11 i 15.12 (1024 t0$ 6.6 19.8 36.5 372 1
852199WC 10 1 1302 5.8 7.65 53 A 1.4 .A 9.1 11 375 1U'1 471 v111 4_3 vn 14.43 88.6 I 8.7 8.0 7.1'.3 37.5 32.2 1
f 105 A 460 1'FI 369 "d 1048 11 • 5.4 7.45 46 1,1 12 .a . 9.8 11 311 "111370 v11 1
I � 3.8 vn( 4.9 98 ;° 9.1 6.4 16.8 28.6 48.1 I
r Soil Fertility Recommendations (lbs./Acre) =Maintenance Recommendation
Sample
ID C rub •
- �I
101 CORrl I75 BUSHELS 0.4
102 CORN - �.._. 250 90
. .l_ 70 I0 ' 0.1 5.0 ..175 BUSHELS 0.3 250 80
103 I CORN 175 BUSHELS I 250 L 90 - 80 J 23 i SA I
104 CORN 175 BUSHELS
1 I 250 100 70 + 10 1 5.0 I
105 CORN 175 BUSHELS
175 BUSHELS 0.5 + J
1pb CORN I -_250 I I10 ( 70 I
90 s ( 10 I
10 0.1 5.0_
107 ( 1.1 I 250 100 I 5.0 I
i ._.-_ .-lam CORN 175
BUSHELS f i I 250 85 70 I 1 14 0-1 r 5.0 [ 1 I -_ --175 BUSHELS I� 250 50 I '
1 08 CORN 10 i 5.0 ( 1
175 BUSHELS 0.4 I 250 50 ---- ---
-- I 10 5 (
110 CORK! '0 1 175 BUSHELS 1 0.3 ? ( 250 1 50 L I� 10 0.0 i 5.0
Comments _ ' �__
IS LBS OF N1'IROoIiN AND 50 LBS OF P11OSPI IATUE RF.CO IMENUIo;AS A STAR 11O2 ON ALL CORN FERTILIZER APPLIED AS A STARTER.
SIIO1/I.0 Ali D AUC1'EU FROM ABOVE.BE S1IRE Tltxrsu:i.FI:R IS APPI11.0)IN ORDER 171AT NFTROGEN-SULFDR RATIO IS MAINTAINED.
SI'CiGt•S'r TAKING PLA\t SAMPLES DURING TOE GROWING SEASON.Abl)ITIONAI.NUTRIENTS MAY 11F.-NEEDED.ESPECIALLY NITROGEN AND PUTnss111M.
`�� L=Low H=Medium A=Adequate H=Nigh VH=Very High -._..J C

KTT
Waters A.gricullural Laboratories•Inc.
Soil Analysis ReportP.O.335-7216 AX1229)onHwy
3144 WATER ,A R! 1J'TURAL Camilla,GA 31730
7552 CI MLA BROOK RD �qf3 R h, (229) FAX[phone]
TIFTON GA 317g:1- Grower Code:
Grower: 2F Farms Field ID: Loftin 400-405 Test Method:Mehlich III
Page 12
NM' P K Mg Ca `: S B Zn Mn F ., .,QM ' GEC E,a - 3 _.1
Number Lab
Sato
mple lbs/A • lbs/A lbs/A lbs/A Soil Buffer lbs/A lbs/A Ibs/A lbs/A lbs/A lbs/A % Ibs1A meg1100g % % %
pH pH
. K Mg Ca H
852200WC 1 111 88 A 411 VII 515 vH 1171 II 5.5 7.55 49 M 1.1 A L9.8 11 256 v11I 424 v it 3.7 vll 4,13 82.6 9.2 5,7 23.3 31.8 39.1
852201WC � 112 55 Al 239 ^ 884 VII 1326 vi1 7.50 30 �I 1.0 Al4 II 222 v'u 481 vqi 3.6 vli
5,6. I v�-4.96 99.2 11.3 2.7 32.6 29.3 35.4
852202WC 113 36 L 356 vil I 853 vil 1689 vu 5.4 7.50 67 A 1.2 'v 1 7,5 v 247 6)1 335 1a1 vn '
852203WC 114 hi vw� � ' � 4.0 15.07 101.4 12.2 3.7 29.1 34.5 32.7
I 55 414 410 VII 1408 VII 5.2 7.30 53 A 1.3 A 18.9 11 1237 v111372 VII 5,5 1'1i.1 5.67 113.4� 11.4 4.7 15.0 31.0 49.3
852204WC ( 115 I 70 " 457 v'Ii 287 vli j 1304 v71 5.2 7,40 52 A 1.3 A l 8.9 11 90 111 436 V"I 4.2 VII 6.47 129.4 I 9.8 6.0 12.2 331 48.8
I 852205WC I 116 I 56 hi 257 II I 296 VII 1199 II 5.5 7.50 32 3I 1.1 .v ; 8.2 f1 148 "I 457 VII 4,6 vU 4.61 92.2 8.6 3.8 14.4 35.0 46.7
852206WC I 117 23 I• 179 A 376 Vil 1099 11 5.5 7.65 40 AI 1.0 ,v 1 47 >r 159 v'r1 374 vIi `-
852207WC 118 NI VII 2.8 11 4.11 82.2 _7.3 3.1 21.3 37.4 38.1
79 671383. v'II 1463 Vn 5.4 7.40 131 VII 1.3 A 9.2 11 308 v11 189 'I1 i
852208WC 119 H vu vm vn1 I 4.4 v11 4.96 99.2 I 10.9 7.9 14.6 33.5 44.0 I
I 1 148 646 442 1660 5.6 7.55 123 \'!I 1.8 II 121 %At 352 VII 219 VII 6.4 vli 4.79 95.8 I 10.4 7.9 17.7 39.8 34.5
I 852209WC 1 120 120 A 615 vII 378 VII 1637 VII 5.6 7.50 110 VII 1.6 1110.6 "III 325 v11 226 VII 6.1 VII 4.53 90.6 I 10.5 I 7.5 15.1 39.1 38.3
Soil Fertility Recommendations (lbs./Acre) =Maintenance Recommendation
sample
V.C.111 CORN 175 BUSHELS 0.8 250 55 70 10 0.1 5.0 n
CORN 175 BUSHELS
250 90 110 15 0.2 5.0
113 CORN 175 BUSHELS 0.3
114 CORN ( 250 105 70 10 0.0 i 5.0
175 BUSHELS 0.6 I 250 90 70 10 I 5-0
its CORN 175 BUSHELS I 0.5 I 250 70
10 I I 5.0
116 C 13 0.1 5.0
CORN O1w 175 BUSHELS 0.9 l 250 85 90 I I I
117 i ��--
175 BUSHELS 0.6 250 120 170 10 0.2 5.0
`
�^ 118 ( CORN 175 BUSHELS i 0.3 i 250 65 �`_^� � �
5.0
CORN
119 IJ _ !175 BUSHELS } 250 50 - '
_�,__t20 CORN j 5.0
175 BUSHELS I 0.8 { 250 I` 50 I 5.0
�_ � __
Comments --- - _-_ -- I _._ __ _ _.__
15 LDS OF NITROGEN AND S111.135 OF PI IOSPII,VI7 RECOMMENDED AS A STARTER ON Mi.CORN.1TRl11.IZIE APPI.IIO)AS.\S'r. R'IT:R•
SHOULD BE DrIptICIETt FROM ABOVE.BE RIME TIIATSULFUR IS APPLIED IN ORDER'T11ATNITROC;F.N-SI1I.FIIR RATIO IS MAINTAINED.
SUGGEST TARING PLANT SAMPLES DURING TIIE GROWING SEASON.ADI)ITIONAI.NUTRIENTS MAY El'NEEDED,ESPECIALLY NITROGEN AND
PO'I'ASSIUnI.
t L=Low M=MediumA=Adequate H_High VH=very High J c