WQ0034513_Residual Annual Report 2021_20220216

I
Non-Discharge Branch Upload/Submittal Form
NORTH CAROLINA
EnWron.M&IQualfty
Version 2-Revised June 23.2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0034513
Applicant/Permittee Brunswick County
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes OO No
Regional Office Wilmington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Rob Willcox
Email Address* Phone Number*
[e-mail] 3363399128
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0034513
Has Current Existing permit number
Applicant/Permittee Address* Post Office Box 249;Bolivia,N.C.28422
Facility Name* Brunswick County Class B Residuals Program
Please provide comments/notes on your current submittal below.
Brunswick County-2021 Land Application of Class B Residuals Annual Report-Permit No.
WQ0034513
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
2021 CLASS B ANNUAL REPORT-WQ0034513-Brunswick
35.84MB
County.pdf
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature

Submission Date 2/16/2022

2021 ANNUAL REPORT
BRUNSWICK COUNTY PUBLIC UTILITIES
RESIDUALS LAND APPLICATION PROGRAM
NON-DISCHARGE PERMIT #WQ0034513
Prepared For:
Brunswick County
Public Utilities
Post Office Box 249
Bolivia,North Carolina 28422
Compiled By:
Willcox&Mabe Soil Solutions, PLLC
7231 B Summerfield Road
Summerfield,North Carolina 27358
February 2022

Willcox&mate
SOIL SOLUTIONS
February 16, 2022
N.C. Depailment of Environmental Quality
Division of Water Resources—Information Processing Unit
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
Attention: Information Processing Unit
Reference: 2021 LAND APPLICATION ANNUAL REPORT
Brunswick County Public Utilities
Non-Discharge Permit No. WQ0034513
WMSS Project No. 15-04 Phase: 16
Non-Discharge Branch:
Willcox&Mabe Soil Solutions,PLLC (WMSS)is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Brunswick County
Public Utilities (Brunswick County). WMSS compiled this report using data gathered
during the compliance year by Brunswick County and BioGreen Services,Inc. This data
includes: 1) land application certification forms,2) annual residual sampling summary
forms, 3)annual pathogen and vector attraction reduction forms,4)annual field summary
forms and metals field loading summary forms, 5)lab sheets, and 6) soil analysis reports.
Brunswick County land applied a total of 84.0 dry tons of biosolids under Permit No.
WQ0034513 during the 2021 calendar year(West Brunswick Regional WWTP-62.45 dry
tons, and Ocean Isle Beach WWTP-21.55 dry tons.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact Mr. Donald Dixon,Deputy Director of Wastewater Operations
with Brunswick County at(910)253-2485 or Rob Willcox with WMSS for further
assistance.
Sincerely,
Willcox &Mabe Soil Solutions,PLLC
Ade_ 4/4/-44r77-
Martin Mabe Rob Willcox,L.S.S.
Agronomist/Partner Soil Scientist/Partner
Enclosures
Shared\WMSS Projects\2015\15-04 Brunswick County\Phase 16-2021 Annual Report\Class B\2021 CLASS B ANNUAL REPORT-Brunswick
County.doc
Willcox&Mabe Soil Solutions,PLLC/7231 B Summerfield Road/Summerfield,NC 27358/Rob 336.339.9128 or
Martin 336.312.1396/www.willcoxmabesoil.com

Brunswick County Public Utilities
Post Office Box 249
Bolivia, North Carolina 28422
RESIDUALS LAND APPLICATION PROGRAM
CLASS B RESIDUALS
PERMIT NO. WQ0034513
OCEAN ISLE BEACH WWTP
PERMIT NO. WQ0006085
WEST BRUNSWICK REGIONAL WWTP
NON-DISCHARGE PERMIT NO. WQ0023693
Mr. Donald Dixon, Deputy Director of Wastewater Operations
Brunswick County Public Utilities
Post Office Box 249
Bolivia, North Carolina 28422
[phone]
2021 Ocean Isle Beach WWTP Dry Tons - 21.55
2021 West Brunswick Regional WWTP Dry Tons - 62.45
Total Dry Tons - 84.0
2021 Ocean Isle Beach WWTP Dry Metric Tons - 19.55
2021 West Brunswick Regional WWTP Dry Metric Tons - 56.64
Total Dry Metric Tons - 76.19

TABLE OF CONTENTS
SECTION NO. TITLE
I Annual Land Application Certification Forms
(Form ACF)
II Annual Residual Sampling Summary Forms
(Form RSSF)
III Annual Pathogen and Vector Attraction Reduction Forms
(503 Rules)
(Form PVRF 503)
IV Annual Land Application Field Summary Forms and Annual
Metals Field Loading Summary Forms
(Form FSF and MFLSF)
V Lab Sheets
VI Soil Analysis Reports

SECTION I
ANNUAL LAND APPLICATION CERTIFICATION FORMS
(Form ACF)

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0034513 County: Brunswick Year: 2021
Facility Name(as shown on permit): Brunswick County
Land Application Operator: Bio-Green Services,Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
1 Yes❑ No -If No,skip Part A,and Part B and proceed to Part C. Also, If residuals were
generated but not land applied,please attach an explanation on how the residuals were handled.
Part A-Residuals Application Summary: West Brunswick Regional WWTP
Total number of application fields in the permit: 31
Total number of fields utilized for land application during the year: 4
Total amount of dry tons applied during the year for all application sites: 62.45
Total number of acres utilizes for land application during the year: 36.9
Part B-Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below)issued by the Division of Water Resources. 0 Yes ❑ No
If no please,provide a written description why the facility was not compliant,the dates,and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)copies of
laboratory results are attached.
4) Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1105(a)or the Pollutant Loading
Rates in 15A NCAC 02T.1105(b)(applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with(applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C-Certification:
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate,
and complete.I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Donald B. Dixon-Deputy Director7f'Z-i Z,
Permittee Name and Title(type or print) Signature of Permittee ' Date
Signature of Preparer* West Brunswick WWTP / •'Date Signatu of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T .1102(26) DENR FORM ACF(12/2006)

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0034513 County: Brunswick Year: 2021
Facility Name(as shown on permit): Brunswick County
Land Application Operator: Bio-Green Services,Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
Yes No - If No,skip Part A,and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A-Residuals Application Summary: Ocean Isle Beach WWTP
Total number of application fields in the permit: 31
Total number of fields utilized for land application during the year: 1
Total amount of dry tons applied during the year for all application sites: 21.55
Total number of acres utilizes for land application during the year: 12.0
Part B-Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below)issued by the Division of Water Resources. 0 Yes ❑ No
If no please,provide a written description why the facility was not compliant,the dates,and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)copies of
laboratory results are attached.
4) Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1105(a)or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b)(applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with(applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C- Certification:
"I certify, under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate,
and complete. I am aware that there are significant penalties for submitting false information,including the possibility
of fines and imprisonment for knowing violations."
Donald B. Dixon-Deputy Director
Permittee Name and Title(type or print) Signature of Permittee at
a
Signature of Preparer* Ocean Isle Beach WWTP Date Signat re of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r)and 15A NCAC 02T.1102(26) DENR FORM ACF(12/2006)

SECTION II
ANNUAL RESIDUAL SAMPLING SUMMARY FORMS
(Form RSSF)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF-B
WQ Permit Number: WQ0034513 Laboratory: 1) Environmental Chemists, Inc.
Facility Name: Brunswick County 2)
Residual Source WQ#or WQ0023693 3)
NPDES#: 4)
WWTP Name: West Brunswick Regional WWTP 5)
Residual Analysis Data
Conc. Sample or Composite Date
Parameter Limit
(mg/kg) (mg/kg)a 03/11/21
Percent Solids(%) NA 2.88
Arsenic 75 17.4
Cadmium 85 17.4
Chromium NA 62.5
Copper 4,300 628
Lead 840 21.1
Mercury 57 1.62
Molybdenum 75 17.4
Nickel 420 27.6
Selenium 100 17.4
Zinc 7,500 5,210
Total Phosphorus NA 53,400
TKN NA 58,900
Ammonia-Nitrogen NA 19,600
Nitrate and Nitrite NA 172
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties
for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer* 1 /Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0034513 Laboratory: 1) Environmental Chemists, Inc.
Facility Name: Brunswick County 2)
Residual Source WQ0023693 3)
NPDES#or WQ#: 4)
WWTP Name: West Brunswick Regional WWTP 5)
Residual Analysis Data
Sample or Composite Date
Parameter
(mg/kg) 03/11/21
Aluminum 32,000
Calcium 31,600
Magnesium 4,970
pH 6.20
Potassium 6,910
Sodium 3,580
SAR 0.84
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer* % ,DDate
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26) DENR FORM RSSF B (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF-B
WQ Permit Number: WQ0034513 Laboratory: 1) Environmental Chemists, Inc.
Facility Name: Brunswick County 2)
Residual Source WQ#or WQ0006085 3)
NPDES#: 4)
WWTP Name: Ocean Isle Beach WWTP 5)
Residual Analysis Data
Conc. Sample or Composite Date
Parameter Limit
(mg/kg) (mg/kg)a 0]/06/21
Percent Solids(%) NA 1.42
Arsenic 75 23.5
Cadmium 85 23.5
Chromium NA 23.5
Copper 4,300 173
Lead 840 23.5
Mercury 57 1.10
Molybdenum 75 23.5
Nickel 420 23.5
Selenium 100 23.5
Zinc 7,500 492
Total Phosphorus NA 15,300
TKN NA 35,100
Ammonia-Nitrogen NA 774
Nitrate and Nitrite NA 5.96
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties
for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2Z
Signature of Preparer* / ;Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0034513 Laboratory: 1) Environmental Chemists, Inc.
Facility Name: Brunswick County 2)
Residual Source WQ0006085 3)
NPDES#or WQ#: 4)
WWTP Name: Ocean Isle Beach WWTP 5)
Residual Analysis Data
Sample or Composite Date
Parameter
(mg/kg) 01/06/21
Aluminum 2,990
Calcium 9,930
Magnesium 4,850
pH 6.41
Potassium 6,720
Sodium 7,680
SAR 1.88
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
S.' 3 �ZZ
Signature of Preparer* , Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26)
DENR FORM RSSF- B (12/2006)

SECTION HI
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS
(503 RULES)
(Form PVRF 503)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Brunswick County WQ Permit Number: WQ0034468
WWTP Name: West Brunswick Regional WWTP NPDES Number: WQ0023693
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (40 CFR 503.32) -Please indicate level achieved and alternative performed:
Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 Li
Alternative 4 Li Alternative 5 ❑ Alternative 6 ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alternative 1 0 Alternative 2 0
If applicable to alternative performed(Class B only)indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0 Air Drying❑ Composting ❑ Aerobic Digestion
Anaerobic Digestion ❑ I
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Patho en DensityNumber of
Parameter g Frequency Sample Analytical
Excee-
in Sludge Minimum Geo. Mean Maximum Units dences of Analysis Type Tech-pique
2 x 10 to the MPN
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (40 CFR 503.33)-Please indicate option performed:
Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt.4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization Q Alt 7(Drying-Stable) ❑ Alt. 8 (Drying-Unstable)
Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed Li
CERTIFICATION STATEMENT (please check the appropriate statement)
c0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
'❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this
statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Ray Gambill, President- BioGreen
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signatu e of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Brunswick County WQ Permit Number: WQ0034513
WWTP Name: Ocean Isle WWTP NPDES Number: WQ0006085
Monitoring Period: From 1/1/2021 To 12/31/2021
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑
Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Therrnophilic
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alternative 1 ❑ Alternative 2 O
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization Z] Air Drying❑ Composting ❑ Aerobic Digestion Li
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level in Pathogen Density Number of Frequency Sample Analytical
Parameter Excee-
Sludge Minimum Geo. Mean Maximum Units dences of Analysis Type Tech-nique
2 x 10 to the MPN
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (40 CFR 503.33) -Please indicate option performed:
Alt.1 (VS reduction) ❑ Alt. 2(40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4(Spec.02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6(Alk. Stabilization 0 Alt 7 (Drying- Stable) ❑ Alt. 8 (Drying- Unstable) ❑
Alt. 9(Injection) ❑ Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law,that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this
statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Ray Gambill- President(BioGreen)
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signa ure of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102(26)
DENR FORM PVRF 503 (12/2006)

SECTION IV
ANNUAL LAND APPLICATON FIELD SUMMARY FORMS
ANNUAL METALS LOADING SUMMARY FORMS
(Form FSF and MFLSF)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Brunswick County Permit#: WQ0034513 Annual Dry Tons Applied: 18.74
Owner: Richard Clemmons Operator: Richard Clemmons Predominant Soil Series: Goldsboro-GoA
Site#: NC-BR-RC Field #: 1 Acres Utilized: 10.60 Acres Permitted: 10.60
�. c Specify % Site Inches Appli- Vola- Miner- Ammo- Must Select
Residual Cond. Ni-trate *
° u Cu.Yd. Totals Dry Tons Per Precip. cation tili ali- nia Crop 1 or Crop
o Solid Sources Dry, TKN and PAN 1 PAN 2 2 *
Q _ Report Per Acre s Acre (Summarize) Wet Past 24 Meth- zation zation Ni- Nitrite
in Gal.
Moist Hrs. od* Rate** Rate trogen Crop 1 Crop 2
0 0.0000 0.000 0.000 1
0 0.0000 0.000 0.000 2
Mar-21 156,000 14,717 2.88 1.7675 West Brunswick WWTP D <0.5" S 0.50 0.30 58,900 19,600 172 76.927 ####### Corn 3
0 0.0000 0.000 0.000 4
0 0.0000 0.000 0.000 5
0 0.0000 0.000 0.000 6
0 0.0000 0.000 0.000 7
0 0.0000 0.000 0.000 8
0 0.0000 0.000 0.000 9
0 0.0000 0.000 0.000 10
0 0.0000 0.000 0.000 11
0 0.0000 0.000 0.000 12
TOTALS: 14,717 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied
Annual lbs/acre 0.0615 0.0615 0.2209 2.2200 0.0746 0.0057 0.0615 0.0976 0.0615 18.4174 188.769 76.927 0.000 Date lbs/ac
Current Cumulative lbs/ac 0.4035 0.4035 6.3029 2.6050 0.5566 0.0167 0.467 0.6036 0.7405 36.3354 :::::::::::::::::::::::::
Prior Years Cumulative lbs/ac 0.3420 0.3420 6.0820 0.3850 0.4820 0.0110 0.405 0.5060 0.6790 17.9180 ::: ::::: ::::::::::::::::::::::::
Permitted C. P. L. R.*** 36 34 1,338 267 15 374 89 2498
Permit
e it PAN Limit 1 st/2n d Crop
]35
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
A-e3/ (JS-10‘44.e4s. Z/e77-7 *Application Method: S-Surface,IN-Injection,INC -Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface-0.5,Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form.The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations.ie.FSF row#1 to MFLSF column#1.
DENR FORM FSF(5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Brunswick County Total Dry Tons Applied(Annual): 18.74
Permit#: WQ0034513 Predominant Soil Series: Goldsboro-GoA
Operator: Richard Clemmons Owner: Richard Clemmons
Acres Used: 10.60 Acres Permitted: 10.60 Site#: NC-BR-RC Field#: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample ' z 41 41 s 8 io ii Uzi
or Corn-
03/11/21
posite
Date
%Solids 2.88
Arsenic 17.4
Cadmium 17.4
Chromium 62.5
Copper 628
Lead 21.1
Mercury 1.62
Molyb- 17.4
denum
Nickel 27.6
Selenium 17.4
Zinc 5,210
Total
Phos- 53,400
phorus
Annual Heavy Metal Field Loadings(Calculated in lbs/acre):
a 1 z 3J 4J 5 6.1 11 .8i 1:91 ?o_ iJ 12_
° H sv
1.7675
Arsenic 0.0000 0.0000 0.0615 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0615
Cadmium 0.0000 0.0000 0.0615 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0615
Chromium 0.0000 0.0000 0.2209 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.2209
Copper 0.0000 0.0000 2.2200 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 2.2200
Lead 0.0000 0.0000 0.0746 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0746
Mercury 0.0000 0.0000 0.0057 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0057
Molyb 0.0000 0.0000 0.0615 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0615
denum
Nickel 0.0000 0.0000 0.0976 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0976
Selenium 0.0000 0.0000 0.0615 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0615
Zinc 0.0000 0.0000 18.4174 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 18.417
Total
Phos- 0.0000 0.0000 188.769 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 188.769
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
s ZZ
Signatur Land Applier ate
*See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM FSF(5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Brunswick County Permit#: WQ0034513 Annual Dry Tons Applied: 18.74
Owner: Richard Clemmons Operator: Richard Clemmons Predominant Soil Series: Onslow-On
Site#: NC-BR-RC Field #: 4 Acres Utilized: 11.60 Acres Permitted: 11.60
Specifyl Site Inches Appli- Vola- Miner- Ammo- Must Select
o Totals Cond. Ni-trate *
�, Cu.Yd. % Dry Tons Residual Sources Precip. cation tili- ali- nia- Crop 1 or Crop
TKN and PAN 1 PAN 2
Q Report Acre Solids Per Acre (Summarize) We Past 24 Meth- zation zation Ni- 2
*
- Hrs. od* Rate** Rate trogen Nitrite Crop1 Crop2
in Gal. Moist
0 0.0000 0.000 0.000 1
0 0.0000 0.000 0.000 2
0 0.0000 0.000 0.000 3
0 0.0000 0.000 0.000 4
0 0.0000 0.000 0.000 5
0 0.0000 0.000 0.000 6
0 0.0000 0.000 0.000 7
0 0.0000 0.000 0.000 8
0 0.0000 0.000 0.000 9
0 0.0000 0.000 0.000 10
0 0.0000 0.000 0.000 11
Dec-21 156,000 13,448 2.88 1.6151 West Brunswick WWTP D <0.5" S 0.50 0.30 58,900 19,600 172 70.295 ####### Rye 12
TOTALS: 13,448 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied _
Annual lbs/acre 0.0562 0.0562 0.2019 2.0286 0.0682 0.0052 0.0562 0.0892 0.0562 16.8293 172.493 70.295 0.000 Date lbs/ac
Current Cumulative lbs/ac 0.2872 0.3232 2.5049 2.3596 0.3522 0.0172 0.334 0.3902 0.5962 23.6633 :::
Prior Years Cumulative lbs/ac 0.2310 0.2670 2.3030 0.3310 0.2840 0.0120 0.278 0.3010 0.5400 6.8340
Permitted C. P. L. R.*** 36 34 1,338 267 15 374 89 2,498
Pe
rmit PAN Limit lst/2nd
Crop
10
6
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
P-...r / ,...14.0...r.Ati7_
� Date 2 *Application Method: S- Surface,IN-Injection,INC-Incorporation
Signature of Land Applier **Volatilization Rate: Surface-0.5,Iniection/Incorporation- 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form.The FSF and MFLSF are mathematically linked so this information needs to be entered into the same
numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations.ie.FSF row#1 to MFLSF column#1.
DENR FORM FSF(5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Brunswick County Total Dry Tons Applied(Annual): 18.74
Permit#: WQ0034513 Predominant Soil Series: Onslow-On
Operator: Richard Clemmons Owner: Richard Clemmons
Acres Used: 11.60 Acres Permitted: 11.60 Site#: NC-BR-RC Field#: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample ?) 2 3 41 6 6 7 e1 s 10 I Itj iz
or Com-
posite 03/11/21
Date
%Solids 2.88
Arsenic 17.4
Cadmium 17.4
Chromium 62.5
Copper 628
Lead 21.1
Mercury 1.62
Molyb-
denum 17.4
Nickel 27.6
Selenium 17.4
Zinc 5,210
Total
Phos-
p 53,400
horus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
-C o - 2 i _3 4] _51 6 7j 9 rig] i 12.1
arrri -
d
r.
w
° 1.6151
Arsenic 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0562 0.0562
Cadmium 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0562 0.0562
Chromium 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.2019 0.2019
Copper 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 2.0286 2.0286
Lead 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0682 0.0682
Mercury 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0052 0.0052
Molyb 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0562 0.0562
denum
Nickel 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0892 0.0892
Selenium 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0562 0.0562
Zinc 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 16.8293 16.8293
Total
Phos- 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 172.493 172.493
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
r/2 Z
Signatur Land Applier Date
*See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM FSF(5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Brunswick County Permit#: WQ0034513 Annual Dry Tons Applied: 8.59
Owner: Richard Clemmons Operator: Richard Clemmons Predominant Soil Series: Goldsboro-GoA
Site#: NC-BR-RC Field#: 6 Acres Utilized: 4.50 Acres Permitted: 4.50
Specify Site Must Select
*
�, Gal. Inches Appli- Vola- Miner- Ammo-o Y Totals Cond. Ni-trate Crop 1 or Cro
, o 9 Cu.Yd. Per % Dry Tons Residual Sources Precip. cation tili- ali- nia- p p *
Q Report Dry TKN and PAN 1 PAN 2
�,
_ Totals Acre Solids Per Acre (Summarize) Wet Past 24 Meth- zation zation Ni- Nitrite 2 **
: in Gal.
Moist Hrs. od* Rate** Rate trogen Crop 1 Crop 2
0 0.0000 0.000 0.000 1
0 0.0000 0.000 0.000 2
0 0.0000 0.000 0.000 3
0 0.0000 0.000 0.000 4
0 0.0000 0.000 0.000 5
0 0.0000 0.000 0.000 6
0 0.0000 0.000 0.000 7
Aug-21 71,500 15,889 2.88 1.9082 West Brunswick WWTP D <0.5" S 0.50 0.30 58,900 19,600 172 83.052 ####### Coastal 8
0 0.0000 0.000 0.000 9
0 0.0000 0.000 0.000 10
0 0.0000 0.000 0.000 11
0 0.0000 0.000 0.000 12
TOTALS: 15,889 :: ::::::::: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied
Annual lbs/acre 0.0664 0.0664 0.2385 2.3967 0.0805 0.0062 0.0664 0.1053 0.0664 19.8834 203.796 83.052 0.000 Date lbs/ac
Current Cumulative lbs/ac 0.4089 0.4265 7.6947 3.5574 0.6131 0.0312 0.498 0.7339 0.5262 46.0127 :::::::::::::::::.::: ::::
Prior Years Cumulative lbs/ac 0.3425 0.3601 7.4562 1.1607 0.5325 0.0250 0.432 0.6285 0.4598 26.1293
Permitted C. P. L. R.*** 36 34 1,338 267 15 374 89 2,498
Permit PAN
Limit 1 st/2nd Crop 9
,. 29
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
6-A-e•st.e
2/$/ *Application Method: S- Surface,IN-Injection,INC-Incorporation
ignature of Land Applier Datee **Volatilization Rate: Surface-0.5,Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form.The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations.ie.FSF row#1 to MFLSF column#1.
DENR FORM FSF(5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Brunswick County Total Dry Tons Applied(Annual): 8.59
Permit#: WQ0034513 Predominant Soil Series: Goldsboro-GoA
Operator: Richard Clemmons Owner: Richard Clemmons
Acres Used: 4.50 Acres Permitted: 4.50 Site#: NC-BR-RC Field#: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample 1 ? 3! a eii s J s sj 19_1 ILI 12
or Com-
posite 03/11/21
Date
%Solids 2.88
Arsenic 17.4
Cadmium 17.4
Chromium 62.5
Copper 628
Lead 21.1
Mercury 1.62
Molyb-
denum 17.4
Nickel 27.6
Selenium 17.4
Zinc 5,210
Total
Phos- 53,400
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
11 _3...1 _4J .`'. .91 10 11 1.2
C17
° 1.9082
Arsenic 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0664 0.0000 0.0000 0.0000 0.0000 0.0664
Cadmium 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0664 0.0000 0.0000 0.0000 0.0000 0.0664
Chromium 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.2385 0.0000 0.0000 0.0000 0.0000 0.2385
Copper 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 2.3967 0.0000 0.0000 0.0000 0.0000 2.3967
Lead 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0805 0.0000 0.0000 0.0000 0.0000 0.0805
Mercury 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0062 0.0000 0.0000 0.0000 0.0000 0.0062
Molyb 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0664 0.0000 0.0000 0.0000 0.0000 0.0664
denum
Nickel 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.1053 0.0000 0.0000 0.0000 0.0000 0.1053
Selenium 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0664 0.0000 0.0000 0.0000 0.0000 0.0664
Zinc 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 19.8834 0.0000 0.0000 0.0000 0.0000 19.883
Total
Phos- 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 203.796 0.0000 0.0000 0.0000 0.0000 203.796
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature and Applier� pp Date
*See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM FSF(5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Brunswick County Permit#: WQ0034513 Annual Dry Tons Applied: 16.39
Owner: Joyce Brown Operator: Harvey Bell Predominant Soil Series: Goldsboro-GoA
Site#: NC-BR-HB Field #: 1 Acres Utilized: 10.20 Acres Permitted: 10.20
Specify Site Inches A h Vola- Miner- Ammo- Must Select
i.. L. Gal. o Cond. pP Ni-trate
a' °.:a Cu.Yd. Totals /c Dry Tons Residual Sources Precip. cation tili- ali- nia_ Crop 1 or Crop
rt o Per Solid D TKN and PAN 1 PAN 2
Q *
Toport ls Acre s Per Acre (Summarize) We Past 24 Meth- zation zation Ni- 2
- Hrs. od* Rate** Rate trogen Nitrite Crop1 Crop2
in Gal. Moist
0 0.0000 0.000 0.000 1
0 0.0000 0.000 0.000 2
0 0.0000 0.000 0.000 3
0 0.0000 0.000 0.000 4
0 0.0000 0.000 0.000 5
0 0.0000 0.000 0.000 6
Jul-21 136,500 13,382 2.88 1.6072 West Brunswick WWTP D <0.5" S 0.50 0.30 58,900 19,600 172 69.95 ####### Coastal 7
0 0.0000 0.000 0.000 8
0 0.0000 0.000 0.000 9
0 0.0000 0.000 0.000 10
0 0.0000 0.000 0.000 11
0 0.0000 0.000 0.000 12
TOTALS: 13,382 : :::::::::: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied
Annual lbs/acre 0.0559 0.0559 0.2009 2.0186 0.0678 0.0052 0.0559 0.0887 0.0559 16.7470 171.649 69.950 0.000 Date lbs/ac
Current Cumulative lbs/ac 0.5491 0.4333 12.4953 3.0381 0.7122 0.0419 0.579 0.6771 0.5766 43.5226 ::::::::::::::::::::::::
Prior Years Cumulative lbs/ac 0.4932 0.3773 12.2944 1.0195 0.6444 0.0367 0.523 0.5884 0.5207 26.7756
Permitted C. P. L. R.*** 36 34 1,338 267 15 374 89 2,498
Permit PAN Limit 1 st/2nd Crop
... .. . . ........... ...
29
9
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
ag-r/ .Le.0.4 /9." Z7/ 7a Z- *Application Method: S-Surface,IN-Injection,INC -Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface-0.5,Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form.The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations.ie.FSF row#1 to MFLSF column#1.
DENR FORM FSF(5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Brunswick County Total Dry Tons Applied(Annual): 16.39
Permit#: WQ0034513 Predominant Soil Series: Goldsboro-GoA
Operator: Harvey Bell Owner: Joyce Brown
Acres Used: 10.20 Acres Permitted: 10.20 Site#: NC-BR-HB Field#: 1
Residual Analysis Data(Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample 1 2' 3 4 5I 6 7 - a' 9 10 11 12_�
or Com-
posite 03/11/21
Date
%Solids 2.88
Arsenic 17.4
Cadmium 17.4
Chromium 62.5
Copper 628
Lead 21.1
Mercury 1.62
Molyb-
denum 17.4
Nickel 27.6
Selenium 17.4
Zinc 5,210
Total
Phos- 53,400
phorus
Annual Heavy Metal Field Loadings(Calculated in lbs/acre):
o 1 ? 31 4.I 5 :61 -711 8? 9I i l 111 12_
CD
m
w �
5 1.6072
Arsenic 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0559 0.0000 0.0000 0.0000 0.0000 0.0000 0.0559
Cadmium 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0559 0.0000 0.0000 0.0000 0.0000 0.0000 0.0559
Chromiun- 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.2009 0.0000 0.0000 0.0000 0.0000 0.0000 0.2009
Copper 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 2.0186 0.0000 0.0000 0.0000 0.0000 0.0000 2.0186
Lead 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0678 0.0000 0.0000 0.0000 0.0000 0.0000 0.0678
Mercury 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0052 0.0000 0.0000 0.0000 0.0000 0.0000 0.0052
Molyb 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0559 0.0000 0.0000 0.0000 0.0000 0.0000 0.0559
denum
Nickel 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0887 0.0000 0.0000 0.0000 0.0000 0.0000 0.0887
Selenium 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0559 0.0000 0.0000 0.0000 0.0000 0.0000 0.0559
Zinc 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 16.7470 0.0000 0.0000 0.0000 0.0000 0.0000 16.7470
Total
Phos- 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 171.649 0.0000 0.0000 0.0000 0.0000 0.0000 171.649
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted.I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature 6f and Applier Date
*See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM FSF(5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Brunswick County Permit#: WQ0034513 Annual Dry Tons Applied: 21.55
Owner: Pearly Vereen Operator: Pearly Vereen Predominant Soil Series: Lynchburg-Ly
Site#: NC-BR-PV Field #: 2 Acres Utilized: 12.0 Acres Permitted: 12.0
�J SpecifyCll Site Inches Appli- Vola- Miner- Ammo- Must Select
*
o ,� Totals Cond. Ni-trate Crop 1 or Crop
a D Cu.Yd. % Dry Tons Residual Sources Precip. cation tili- ali- nia- p P *
Per TKN and PAN 1 PAN 2
Q ± _ Report
Acre Solids Per Acre (Summarize) Wet,, Past 24 Meth- zation zation Ni- 2 *
To
Nitrite *
in Gal.
Moist Hrs. od* Rate** Rate trogen Crop 1 Crop 2
0 0.0000 0.000 0.000 1
0 0.0000 0.000 0.000 2
0 0.0000 0.000 0.000 3
Apr-21 364,000 30,333 1.42 1.7962 Ocean Isle Beach WWTP G/D <0.5" S 0.50 0.30 35,100 774 6.0 38.405 ####### Coastal 4
0 0.0000 0.000 0.000 5
0 0.0000 0.000 0.000 6
0 0.0000 0.000 0.000 7
0 0.0000 0.000 0.000 8
0 0.0000 0.000 0.000 9
0 0.0000 0.000 0.000 10
0 0.0000 0.000 0.000 11
0 0.0000 0.000 0.000 12
TOTALS: 30,333 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied
Annual lbs/acre 0.0844 0.0844 0.0844 0.6215 0.0844 0.0040 0.0844 0.0844 0.0844 1.7675 54.964 38.405 0.000 Date lbs/ac
Current Cumulative lbs/ac 0.1623 0.1706 0.2486 0.8373 0.2486 0.0090 0.164 0.2156 0.2156 2.5780
Prior Years Cumulative lbs/ac 0.0778 0.0861 0.1641 0.2158 0.1641 0.0050 0.080 0.1311 0.1311 0.8105
Permitted C. P. L. R.*** 36 34 1,338 267 15 374 89 2,498
Pe
rmit PAN Limit 1st/2nd Crop
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
,::2 ' 4.0-scre... 77/07Z'Z *Application Method: S- Surface,IN-Injection, INC- Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface- 0.5,Injection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form.The FSF and MFLSF are mathematically linked so this information needs to be entered into the same
numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations.ie.FSF row#1 to MFLSF column#1.
DENR FORM FSF(5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Brunswick County Total Dry Tons Applied(Annual): 21.55
Permit#: WQ0034513 Predominant Soil Series: Lynchburg-Ly
Operator: Pearly Vereen Owner: Pearly Vereen
Acres Used: 12.00 Acres Permitted: 12.00 Site#: NC-BR-PV Field#: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample 3 41, 5 81 10 11- 12
or Com-
01/06/21
posite
Date
%Solids 1.42
Arsenic 23.5
Cadmium 23.5
Chromium 23.5
Copper 173
Lead 23.5
Mercury 1.1
Molyb-
denum 23.5
Nickel 23.5
Selenium 23.5
Zinc 492
Total
Phos- 15,300
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 11
4 1 ..7.1 6 1 J 10' 11 121
< d
H
5.
o 1.7962
Arsenic 0.0000 0.0000 0.0000 0.0844 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0844
Cadmium 0.0000 0.0000 0.0000 0.0844 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0844
Chromium 0.0000 0.0000 0.0000 0.0844 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0844
Copper 0.0000 0.0000 0.0000 0.6215 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.6215
Lead 0.0000 0.0000 0.0000 0.0844 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0844
Mercury 0.0000 0.0000 0.0000 0.0040 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0040
Molyb 0.0000 0.0000 0.0000 0.0844 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0844
denum
Nickel 0.0000 0.0000 0.0000 0.0844 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0844
Selenium 0.0000 0.0000 0.0000 0.0844 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0844
Zinc 0.0000 0.0000 0.0000 1.7675 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 1.7675
Total
Phos- 0.0000 0.0000 0.0000 54.964 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 54.964
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
*See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM FSF(5/2003)

SECTION V
LAB SHEETS

BRUNSWICK COUNTY
LAND APPLICATION PROGRAM
BIOSOLIDS ANALYSIS
Residual Type: Wastewater Treatment Plant(Class B)
Date Sampled: March 11,2021
West Brunswick Regional WWTP Permit No.WQ0034513
Mineralization Rate 0.30 2.88 %Solids Class B
6.20 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 5.890 58,900.000 117.800
Phosphorus 5.340 53,400.000 106.800
Potassium 0.691 6,910.000 13.820
PAN(injected)* 3.156 31,562.000 63.124
PAN(surface)* 2.176 21,762.000 43.524
Ammonia Nitrogen 1.960 19,600.000 39.200
Calcium 3.160 31,600.000 63.200
Calcium Carbonate Eq. --- ___ ---
Magnesium --- 4,970.000 9.940
Sodium --- 3,580.000 7.160
Sulfur -__ ___
Nitrate N/Nitrite N --- 172.000 0.344
Barium --- --- --- SAR
Chloride --- --- --- 0.84
Iron --- --- --- Ceiling Concen.
Aluminum --- 32,000.00 64.000 (Mg/Kg)
Arsenic --- 17.40 0.035 75
Cadmium --- 17.40 0.035 85
Chromium --- 62.50 0.125 ---
Copper --- 628.00 1.256 4,300
Lead --- 21.10 0.042 840
Mercury --- 1.620 0.003 57
Molybdenum --- 17.40 0.035 75
Nickel --- 27.60 0.055 420
Selenium --- 17.40 0.035 100
Zinc --- 5,210.00 10.420 7,500
Env irochem: 2021-04199
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
M 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities Date of Report: Feb 10, 2021
Post Office Box 249 Customer PO#:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report#: 2021-00290
Project ID: WBR WWTP Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-00716 Site: Sludge 1/6/2021 8:15 AM Solid/Sludge Jeffrey Masi
Test Method Results Date Analyzed
Chlordane (TCLP) SW 846 Method 80818/3510 <0.02 mg/L 01/19/2021
Endrin (TCLP) SW 846 Method 808113/3510 <0.0005 mg/L 01/19/2021
Heptachlor(TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 01/19/2021
Heptachlor epoxide(TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 01/19/2021
Lindane (TCLP) SW 846 Method 80818/3510 <0.0005 mg/L 01/19/2021
Methoxychlor (TCLP) SW 846 Method 8 08 113/3 51 0 <0.0005 mg/L 01/19/2021
Toxaphene (TCLP) SW 846 Method 80 81 8/351 0 <0.05 mg/L 01/19/2021
1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
2,4-Dinitrotoluene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Cresol (TC LP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Hexachlorobenzene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Pentachlorophenol (TCLP) SW 846 method 8270;3510 <0.250 mg/L 01/20/2021
Pyridine(TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
2,4,5-TP (TCLP) SW846 Method 8151A <0.003 mg/L 01/20/2021
2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 01/20/2021
1,1-Dichloroethyiene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
1,2-Dichloroethane (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Benzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Carbon Tetrachloride(TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Report#:: 2021-00290 Page 1 of 4

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
Sn+
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities Date of Report: Feb 10, 2021
Post Office Box 249 Customer PO#:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report#: 2021-00290
Project ID: WBR WWTP Sludge
Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Methyl ethyl ketone(TCLP) SW846 Method 8260/5030 <0.05 mg/L 01/14/2021
Tetrachloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Trichloroethylene(TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Vinyl Chloride(TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
RCI
Cyanide SM 4500 CN D 3.20 mg/kg 01/08/2021
Sulfide SM 4500 S D 0.08 mg/kg 01/11/2021
Ignitability SW 846 method 1010 >170°F 01/19/2021
dge Residuals
Alum • EPA 200.7 31300 mg/kg 01/12/ •
Arsenic EPA 200.7 21.5 mg/kg 0 /2021
Cadmium EPA 2007 <10.0 mg/kg 01/12/2021
Calcium EPA 200.7 32000 m /k•
g 01/12/2021
Chromium EPA 200.7 79.6 • kg 01/12/2021
Copper PA 200.7 . 1 mg/kg 01/12/2021
Lead EPA ' 25.5mg/kg 01/12/2021
Magnesium EPA 200.7 , 5010 mg/kg 01/12/2021
Molybdenum EPA 200.7 •
11.5 mg/kg 01/12/2021
Nickel EPA 200.7 27.7 mg/kg 01/12/2021
Potassium EPA 200.7 , ' 4270 mg/kg 01/12/2021
Selenium EPA 200.7 9.56 mg/kg 01/12/2021
Sodium ' '•Q.7 2980 mg/kg 01/12/2021
Zinc EPA 200.7 :.. I mg/kg 01/12/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 94.2 `_ . • 01/13/2021
Total Solids (%) SM 2540 B 4.83% 01/07/2021
pH SM 4500 H B 8.18 units 0 1/15/2021
Ammo." itrogen SM 4500 NH3 C 36400 mg/kg 0 021
Kjeldahl Nitrogen (TKN) SM 4500 Org 6 69900 mg/kg 01/11/21
Report# 2021-00290 Page 2 0f 4

Environmental Chemists, Inc,
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
sm
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities Date of Report: Feb 10, 2021
Post Office Box 249 Customer PO#:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report#: 2021-00290
Project ID: WBR WWTP Sludge
Total Phosphorus " ' g g 01/18/2021
ilimPIIII SW846 74718 . , •
TCLP Metals
Arsenic EPA 200.7 <1 mg/L 01/25/2021
Barium EPA 200.7 <1 mg/L 01/25/2021
Cadmium EPA200.7 <1 mg/L 01/25/2021
Chromium EPA 200.7 <1 mg/L 01/25/2021
Lead EPA 200.7 <1.0 mg/L 01/27/2021
Selenium EPA 200.7 <1 mg/L 01/25/2021
Silver EPA 200.7 <1 mg/L 01/25/2021
Mercury EPA 245.1 <0.0002 mg/L 01/25/2021
L. - 0 Sample ID: Collect Date/Time Matrix Sampled by
21-0071 Site:#1 1/6/2021 10:23 AM Solid/Sludge Jeffrey Masi
Test Method Results , "ate Analyzed
Total Solids (%) SM 2540 B 4.71.• ' ' 01/07/2021
Fecal Density SM 9221C E MPN 24 hr 503 ' ' 83 MPN/g 01/06/2021
Lab ID Sample ID: Collect Date/Time 'rix Sampled by
21-00720 Site:#2 - 2021 10: ' i,. Solid/Sludge Jeffrey Masi
Test Method Results Date Analyzed
Total Solids (%) SM 2540 8 4.88% 01/07/2021
Fecal Density SM 9 , MPN 24 hr 503 <369 MPN/g 01/06/2021
Lab ID Sample ID: Collect Date/Time Matrix` , Sampled by
21-00721 Site:#3 1/6/2021 10:25 AM Solid/Sludge .; -ffrey Masi
Test Method Results . -, Date Analyzed
Total S• " (%) SM 2540 B 4.90% I ' 2021
- Density SM 9221C E MPN 24 hr 503 <368 MPN/g 01/06/20
Report#' 2021.00290 Page 3 of 4

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
sn+
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347,5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
Brunswick County Public Utilities Date of Report: Feb 10, 2021
Post Office Box 249 Customer PO#:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report#: 2021-00290
Project ID: WBR WWTP Sludge
L• D Sample ID: Collect Date/Time Matrix Sampled by
21-00 • Site:#4 1/6/2021 10:26 AM Solid/Sludge Jeffrey Masi
Test Method Results I ' Analyzed
Total Solids (%) SM 2540 s 4.75% 01/07/2021
Fecal DensitySM 9221C E MPN 24 4 hr 503 <379 g 01/06/2021
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-00723 Site:#5 1/6/2021 10:27 AM Solid/ ,age Jeffrey Masi
Test . od Results Date Analyzed
Total Solids(%) SM 2540 B 4.88% 01/07/2021
Fecal Density SM 9221C E MPN 24 hr <369 MPN/g 01/06/2021
Lab ID Sample ID: Co D.:. -/Time Matrix Sampled by
21-00724 Site:#6 2021 10: ' 'M Solid/Sludge Jeffrey Masi
Test M: •d Results Date Analyzed
Total Solids (%) 2540 B 4.76% 01/07/2021
Fecal Density SM 9221C E MPN 24 hr 503 < .•MPN/g 01/06/2021
Lab ID Sample ID• Collect Date/Time Matrix ' • pled by
21-00725 Site: , 1/6/2021 10:29 AM Solid/Sludge Jeffr- _t asi
Test Method Results . , e Analyzed
Tota '. Ids(%) SM 2540 B 4.60% 01/i . 121
al Density SM 9221C E MPN 24 hr 503 <392 MPN/g 01/06/20
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Report# 2021-00290 Page 4 of 4

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: B Cr Lik- Date:L al Report Number:OZ 1 0019C)
Receipt of sample: ECHEM Pickup Client Delivery 0 UPS 0 FedEx 0 Other 0
❑ YES 1_0 NO N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO l'I
N/A j2. If custody seals were present, were they intact unbroken?
/
i.Original temperature upon receipt 3 °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank i Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor°C: 0.0
tr
❑ YES 0 NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES ❑ NO 4. Were proper custody procedures (relinquished/received)followed?
YES 0 NO 5. Were sample ID's listed on the COC?
l! YES 0 NO 6. Were samples ID's listed on sample containers?
al YES 0 NO 7. Were collection date and time listed on the COC?
EN' YES ❑ NO 8. Were tests to be performed listed on the COC?
tgif YES 0 NO 9. Did samples arrive in proper containers for each test?
Oil YES 0 NO 10. Did samples arrive in good condition for each test?
1Cii YES 0 NO 11. Was adequate sample volume available?'
;?' YES 0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH>12?
❑ YES 0 NO 15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Valatiies are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2504 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Samples) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

COUNTY OF BRUNSWICK ! . , , West Brunswick Regional Laboratory
Public Utilities Department 235 Grey Water Road
Wastewater Treatment Division � Supply, NC 28462
As Phone: [phone] Fax: [phone]
Sample Collection and Chain of Custody d 1 _ aq J
Collected By: Jeffrey Masi
Report No.: 2
Sample Type: I= Influent,E=Effluent,W=Well,ST=Stream,SO=Soil,SL=Sludge Other
Sample Collection Sample Composite Container Chlorine LAB ID ANALYSIS
DATE TIME TEMP Type or GrabPRESERVATION REQUESTED
Identification (Plastic or Glass) mg/L NUMBER NONE HCI I
-
WBR H2SO4 HNO-, THIO OTHER
P
RCI,%Solids,
Sludge 1/6/2021 8:15 SL G ? I metals,nutrients,
X TCLP
P -
fecal density 1/6/2021 10:23 22.5 SL G 7 t
X fecal density
P
fecal density 1/6/2021 10:24 22.5 SL G
X fecal density
P
fecal density 1/6/2021 10:25 22.5 SL G 71 k
X fecal density
P
fecal density 1/6/2021 10:26 22.5 SL G �j
/ X fecal density
P
fecal density 1/6/2021 10:27 22.5 SL G -n-
TZ X fecal density
fecal density 1/6/2021 10:28 22.5 SL G P 7 a -t
i X fecal density _
fecal density 1/6/2021 10:29 22.5 SL G P -7),5"
X ,fecal density
ATTENTION: Samples submitted for analysis for Ammonia,TKN,Cyanide,Phenol and all Bacteriologicais must be dechlonnated to<0.2 ppm at time of collection.
Transfer Relinquished B
�-��� q Y: Date/Time Received By: Date/Time
1 ! ✓�. ..4 t I6 /zi ' %oitO X v �_ i Z
( � t ray°
? r `- ( . (4. Z► /tVr
Temperature when Received: ? •--' Accepted: ./ Rejected:
Resample Required:
Delivered By:._., ,•L-tc.-- .�-
Comments: T

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
n, 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infod environmentalchemists.com
Brunswick County Public Utilities Date of Report: Mar 29, 2021
Post Office Box 249 Customer PO#:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report#: 2021-04199
Project ID: WBR WWTP Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-10335 Site:ATAD#1 3/11/2021 11:00 AM Solid/Sludge Client
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200.7 32000 mg/kg 03/16/2021
Arsenic EPA 200.7 <17.4 mg/kg 03/16/2021
Cadmium EPA 200.7 <17.4 mg/kg 03/16/2021
Calcium EPA200.7 31600mg/kg 03/16/2021
Chromium EPA 200.7 62.5 mg/kg 03/16/2021
Copper EPA 200.7 628 mg/kg 03/16/2021
Lead EPA 200.7 21.1 mg/kg 03/16/2021
Magnesium EPA 200.7 4970 mg/kg 03/16/2021
Molybdenum EPA 200.7 <17.4 mg/kg 03/16/2021
Nickel EPA 200.7 27.6 mg/kg 03/16/2021
Potassium EPA 200.7 6910 mg/kg 03/16/2021
Selenium EPA 200.7 <17.4 mg/kg 03/18/2021
Sodium EPA 200.7 3580 mg/kg 03/16/2021
Zinc EPA200.7 5210mg/kg 03/16/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 172 mg/kg 03/17/2021
Total Solids (%) SM 2540 B 2.88% 03/15/2021
pH SM 4500 H B 6.20 units 03/25/2021
Ammonia Nitrogen SM 4500 NH3 C 19600 mg/kg 03/15/2021
Total Kjeldahl Nitrogen(TKN) SM 4500 Org B 58900 mg/kg 03/12/2021
Total Phosphorus SM 4500 P F 53400 mg/kg 03/24/2021
Mercury SW846 7471 B 1.62 mg/kg 03/22/2021
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: d, --G-,- 17
Report#; 2021-04199 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab#94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: V k. Date:3 /i / Report Number: O2/ --0 Li )9
Receipt of sample: ECHEM PickuX Client Delivery 0 UPS 0 FedEx 0 Other 0
0 YES 0 NO *' N/A 1. Were custody seals present on the cooler?
❑ YES 0 NO _R N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt 5, 5 °C Corrected temperature upon receipt °C
How temperature taken: 0 Temperature Blank 04 Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor°C: 0.0
❑ YES 0 NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES 0 NO 4. Were proper custody procedures(relinquished/received)followed?
YES 0 NO 5. Were sample ID's listed on the COC?
YES 0 NO 6. Were samples ID's listed on sample containers?
YES 0 NO 7. Were collection date and time listed on the COC?
YES 0 NO 8. Were tests to be performed listed on the COC?
YES 0 NO 9. Did samples arrive in proper containers for each test?
YES 0 NO 10. Did samples arrive in good condition for each test?
YES 0 NO 11. Was adequate sample volume available?'
YES 0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH >12?
❑ YES 0 NO 15. Were sulfide samples received at a pH >9?
❑ YES 0 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 NCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC.QA.002 Rev 1

envirochem ENVIRONMENTAL CHEMISTS, INC OFFICE:
6602 Windmill Way Wilmington,NC 28405
Analytical&Consulting Chemists NCDENR:DWQ CERTIFICATION#94 NCDHHS: DLS CERTIFICATION#37729 info@env ronm9entaicheFAX
mists com2-4424
COLLECTION AND CHAIN OF CUSTODY
Client:
_ i t PROJECT NAME:
REPORT NO: ,4 'b
ADDRESS:
CONTACT NAME:
REPORT TO: PO NO:
COPY TO: PHONE/FAX:
Sam•led B : email:
— — -- SAMPLE TYPE: I=Influent, E=Effluent, W=Well, ST=Stream,SO=Soil,SL=Sludge, Other:
Collection . a
CI
Sample Identification a — d PRESERVATION
O ro C C7 C J O 0 W
2. n t7 2Date Time Temp o u a E _ z Q i '� z a T w ki x ANALYSIS REQUESTED
PPP'.
! 33
C p MIIIIIIIIIIIII
G G
jF
C p
G G 11111111111111111
C p
C p
NMI.
G G
P
G G 11111111111.111
C p IIIIIIIIIIIIIII
G G
C p
G G
NOTICE•DECHLORINATION: Samples for Ammonia,TKN,Cyanide,Phenol and Bacteria must be dechlorinated p,S
ppm or less)in the field at the time of collection. See reverse for instructions
Transfer quished By: i
q, Da Time
iv By; ate/Time
2.
Temperature when Received °C f
e
Delivered B Acceptd: Rejected: in
y:____ Efz Resamp a Requested:
Comments: Received By:
Date: Time:
TURN R UND:

BRUNSWICK COUNTY- Permit No. WQ0034513
ALKALINE STABILIZATION OF BIOSOLIDS
Facility Name: West Brunswick -ATAD# 1 Operator: Mike Garrity
Batch Size(gallons): 148,000 Lbs.or Gallons Used: Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date Corr. Corrected Corr. Corrected Corr. Corrected Corr. Corrected Initials
pH Temp C Factor+ pH Time p H Temp C Factor+ pH Time pH Temp C Factor+ pH Time pH Temp C Time
Factor+ pH
3/11/2021 12.00 29.7 0.141 12.14 13:23
3/11/2021 12.00 28.0 0.09 12.09 15:25
3/12/2021 11.50 26.8 0.05 11.55 13:33
C iO CV) N M M M O IN V r C�O- C) �N- O O M C) co 0) N Cl) CO V N. O CO CO CA N Cl)
O O O o r .-. N N N CO CO CO CO V
,t-
r.) C C UO O O O O O O O O O O O O O OO O 6 C d O O O o C C O O 6 O O fn com fn V COcofn COfn COCO COco C oC JlN N C N C C CO 0 0 0 CO C_ L. 37Ou ECG CCCCC C CCC CC
U a s a s a a a a s o_ a 3 a a f ' " f
t f
o
O- O a) co f- co Lo Co N O C) CO f,- CO IS) - CO N .- C) O) 00 N- Co io co N r O
Ei c) co co co co co co co co co N N N N N N N N N N
H

Eitimswick County
Lime Stabilization Ph Test Results
Hattior GREEN&ram Mc,
Sim Source: A TA Q I_. c car 8r,.��usw �lb wrP
Permit j. rJ© ?V /n /s'____ Approximate onx: /5/49Qo
Initial Ph Test
Dare Time -tom •o�4,1 OPenztor M. 14.6ke`,ly
a Temp pA. 7ea
Temperature Corrected Ph -
2 Hour PhTest
", :_U -mil T`Me 15 r / 1,;k ri '
Conected Ph
24 Hour Ph Test
Oate 3-1 a-. fit Time (3: , ? operator ffl;Ike Goat /
Ph _._tr. __ ramp A fo.8 454
t Corrected Pb
a.

BRUNSWICK COUNTY
ALKALINE STABILIZATION OF BIOSOLIDS
Facility Name: West Brunswick WRF Operator: Michael Garrity
Batch Size(gallons): 95,000 Lbs.or Gallons Used: 10,000 Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date Temp C Corr. Corrected Corr. Corrected Corr. Corrected Corr. Corrected Initials
pHp Time pH Temp C Time pH Temp
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
7/23/2021 12.10 27.1 0.063 12.16 9:50 MG
7/23/2021 12.00 28.4 0.102 12.10 11:52 CC
7/24/2021 11.80 27.3 0.07 11.87 10:00 CC
0 tY CO CO CO CO N N N CO In N O O O O CO0 O N LO CO `- 'CrN N 0 COo CO CDN N
N N N COM M cO
0 V V
N U O O O O O O O O O O O O O O O O O O o O O O O O O O O O O
t/) U) co co Cl) co co Cl) U) U) U) Cl) co co V)
LO 7 7 7 7 7 7 7 7 7 3 7 7 = D 3 3 7 0 7 7 0 0 7 7 0 0 0 7 3
Cl C C C C C C C C cc C C C C
C)
O C) CO N- Co fir) CO N '_ O Cr) CO N- CO Lr) 'C CO N r O 0) CO t` Co In N O
vY CO CO CO CO 00 C"") CO CO CO CO N N N N N N N N N N <— c— v . . . . .

BRUNSWICK COUNTY
ALKALINE STABILIZATION OF BIOSOLIDS
Facility Name: West Brunswick WRF Operator: Michael Garrity
Batch Size(gallons): 71,500 Lbs.or Gallons Used: 7,500 Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH _ Operator
Date Corr. Corrected Corr. Corrected Corr. Corrected Corr. Corrected Initials
pH Temp C Time pH Temp C Time pH Temp C Time pH Temp C Time
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
7/28/2021 12.01 35.7 0.321 12.33 13:40 JC
7/28/2021 12.18 33.6 0.258 12.44 15:50 JC
7/29/2021 12.05 34.6 0.29 12.34 13:50 MG
C L It) N O M M O V 00 IC) N 0) (fl M C) (0 0) N U) Co V t` o CO c0 0) N U)
V . M M M M N N N O O O 0 0 0 o N N N CO CO CO CO V V
O O O O O O O O O O O O O Oin
° O O OU o co)U) N U) Cr) U) 0O w003 00 00O O0B77 77777 777777 CCC CCCCCCCCCCC
a o_ a a a o_ a a a a o_ o_ a o_ o_
U
Q- O O) CO I` I CO ) - CO N — O o) CO I,- CO r.C) d CO N 1— CD CA CO N- C) IC) CO N
Ei 'r CO CO CO CO CO CO CO Cr) CO CO N N N N N N N N N N r- . . o— o— .— N— .—
I—

BRUNSWICK COUNTY
ALKALINE STABILIZATION OF BIOSOLIDS
Facility Name: West Brunswick WRF Operator: Steve Mowrey
Batch Size(gallons): 124,860 Lbs.or Gallons Used: 19,050 lbs Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp C Corr. Corrected Time pH Temp C Corr. Corrected TimepH TempCorr. Corrected Corr. Corrected Initials
Factor+ pH Factor+ pH C Time pH Temp C Time
Factor+ pH Factor+ pH
12/2/2021 10.84 27.3 1:39 10.91 1745 12.12 27.3 0.069 12.19 19:48 12.02 27.9 0.087 12.11 2151 SM
12/3/2021 11.94 27.4 0.07 12.01 1956 SM
L " CO CO e In of ' Cl CO C) CO U)o LV) N C 0 M CO) N N O O M
ViCD
> > > > N7 CO CO N CO VD CO CO V
O 6 O 6 6 O O O 6 O O O O OO oN 6. iN oo 0 0 0 c a a 0 0 0 o O
7 y CO > > > y 3 JVg u N N N N N 7 N 7 N /)
C C C C C C C C C C C C C C C
0 I- a a a a. a_ a_ a. a a a_ a a_ a_ a. a
U
CD CT CO t— CO Cr) *Cr a) N O O) CO t` O Lc) d' M N O 6) CO ti O Lr) d' CO N O
c d' CO CO) CO CO CO) CO CO C') CO C") N N N N N N N N N N '--
I—

BRUNSWICK COUNTY
LAND APPLICATION PROGRAM
BIOSOLIDS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 6,2021
Ocean Isle Beach WWTP Permit No.WQ0034513
Mineralization Rate 0.30 1.42 % Solids
6.41 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 3.510 35,100.000 70.200
Phosphorus 1.530 15,300.000 30.600
Potassium 0.672 6,720.000 13.440
PAN(injected)* 1.108 11,077.760 22.156
PAN(surface)* 1.069 10,690.760 21.382
Ammonia Nitrogen 0.077 774.000 1.548
Calcium 0.993 9,930.000 19.860
Calcium Carbonate Eq. --- --- ---
Magnesium --- 4,850.000 9.700
Sodium --- 7,680.000 15.360
Sulfur --- ---
Nitrate N/Nitrite N --- 5.960 0.012
Barium --- --- --- SAR
Chloride --- --- --- 1.88
Iron --- --- --- Ceiling Concen.
Aluminum --- 2,990.00 5.980 (Mg/Kg)
Arsenic --- 23.50 0.047 75
Cadmium --- 23.50 0.047 85
Chromium --- 23.50 0.047 ---
Copper --- 173.00 0.346 4,300
Lead --- 23.50 0.047 840
Mercury --- 1.100 0.002 57
Molybdenum --- 23.50 0.047 75
Nickel --- 23.50 0.047 420
Selenium --- 23.50 0.047 100
Zinc --- 492.00 0.984 7,500
Envirochem: 2021-00329
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
si' 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infolo environmentalchemists.com
Brunswick County Public Utilities Date of Report: Feb 10, 2021
Post Office Box 249 Customer PO#:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report#: 2021-00329
Project ID: Ocean Isle Beach
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-00800 Site: OIB 1/6/2021 7:57 AM Solid/Sludge Scott Leonard
Test Method Results Date Analyzed
Chlordane (TCLP) SW 846 Method 808113/3510 <0.02 mg/L 01/19/2021
Endrin (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 01/19/2021
Heptachlor(TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 01/19/2021
Heptachlor epoxide(TCLP) SW 846 Method 808113/3510 <0.0005 mg/L 01/19/2021
Lindane (TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 01/19/2021
Methoxychlor(TCLP) SW 846 Method 8081B/3510 <0.0005 mg/L 01/19/2021
Toxaphene (TCLP) SW 846 Method 8081B/3510 <0.05 mg/L 01/19/2021
1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
2,4,5-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
2,4-Dinitrotoluene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Hexachloro-1,3-butadiene(TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 01/20/2021
Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 01/20/2021
2,4,5-TP (TCLP) SW846 Method 8151A <0.003 mg/L 01/20/2021
2,4-D (TCLP) SW846 Method 8151A <0.003 mg/L 01/20/2021
1,1-Dichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
1,2-Dichloroethane (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Benzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Report# 2021-00329 Page 1 of 3.

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infoenvironmentalchemists.com
Brunswick County Public Utilities Date of Report: Feb 10, 2021
Post Office Box 249 Customer PO#:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report#: 2021-00329
Project ID: Ocean Isle Beach
Chlorobenzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Chloroform (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Methyl ethyl ketone (TCLP) SW846 Method 8260/5030 <0.05 mg/L 01/14/2021
Tetrachloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Trichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 01/14/2021
RCI
Cyanide SM 4500 CN D 1.59 mg/kg 01/08/2021
Ignitability SW 846 method 1010 >205°F 01/20/2021
pH SW 846 Method 9045D 6.41 units 01/19/2021
Sludge Residuals
Aluminum EPA 200,7 2990 mg/kg 01/12/2021
Arsenic EPA 200 7 <23.5 mg/kg 01/12/2021
Cadmium EPA 200.7 <23.5 mg/kg 01/12/2021
Calcium EPA 200.7 9930 mg/kg 01/12/2021
Chromium EPA 200.7 <23.5 mg/kg 01/12/2021
Copper EPA 200.7 173 mg/kg 01/12/2021
Lead EPA 200.7 <23.5 mg/kg 01/12/2021
Magnesium EPA 200.7 4850 mg/kg 01/12/2021
Molybdenum EPA 200.7 <23.5 mg/kg 01/12/2021
Nickel EPA 200.7 <23.5 mg/kg 01/12/2021
Potassium EPA 200.7 6720 mg/kg 01/12/2021
Selenium EPA 200.7 <23.5 mg/kg 01/12/2021
Sodium EPA 200.7 7680 mg/kg 01/12/2021
Zinc EPA 200.7 492 mg/kg 01/12/2021
Nitrate+Nitrite-Nitrogen EPA 353.2 5.96 mg/kg 01/13/2021
Total Solids (%) SM 2540 B 1.42
01/07/2021
Ammonia Nitrogen SM 4500 NH3 C 774 mg/kg 01/11/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Org B 35100 mg/kg 01/11/2021
Total Phosphorus SM 4500 P F 15300 mg/kg 01/18/2021
Report#:: 2021-00329 , Page 2 of 3

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
sM. 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS infotii:environmentalchemists.corn
Brunswick County Public Utilities Date of Report: Feb 10, 2021
Post Office Box 249 Customer PO#:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report#: 2021-00329
Project ID: Ocean Isle Beach
Mercury SW846 7471E <1.10 mg/kg 01/08/2021
TCLP Metals
Arsenic EPA 200.7 <1.0 mg/L 01/27/2021
Barium EPA 200.7 <1.0 mg/L 01/27/2021
Cadmium EPA 200.7 <1.0mg/L 01/27/2021
Chromium EPA 200.7 <1.0 mg/L 01/27/2021
Lead EPA 200.7 <1.0 mg/L 01/27/2021
Selenium EPA 200.7 <1.0 mg/L 01/27/2021
Silver EPA 200.7 <1.0 mg/L 01/27/2021
Mercury EPA 245.1 <0.0002 mg/L 01/29/2021
Comment: Sludge r iduals reported on a dry weight basis.
Reviewed by: ,d ..�
Report#,: 2021-00329 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab#94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: Be--PLI Date: l /c0 a-f Report Number:OZ 1 0 O, z
Receipt of sample: ECHEM Pickup Q� Client Delivery❑ UPS ❑ Fed Ex ❑ Other 0
❑ YES 1❑ NO N/A (1. Were custody seals present on the cooler?
❑ YES ❑ NO 1i N/A 2. if custody seals were present, were they intact/unbroken?
Original temperature upon receipt �,K1 °C Corrected temperature upon receipt °C
How temperature taken: 0 Temperature Blank Against Bottles
iR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor°C: 0.0
❑ YES 0 NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
hrd YES 0 NO 4. Were proper custody procedures(relinquished/received)followed?
►! YES 0 NO 5. Were sample ID's listed on the COC?
1 YES 0 NO 6. Were samples iD's listed on sample containers?
=+ YES 0 NO 7. Were collection date and time listed on the COC?
YES ❑ NO 8. Were tests to be performed listed on the COC?
bit YES 0 NO 9. Did samples arrive in proper containers for each test?
al YES 0 NO 10. Did samples arrive in good condition for each test?
iaf YES 0 NO 11. Was adequate sample volume available?'
jf '' YES 0 NO 12. Were samples received within proper holding time for requested tests?
❑ YES 0 NO 13. Were acid preserved samples received at a pH of<2? *
❑ YES 0 NO 14. Were cyanide samples received at a pH >12?
❑ YES 0 NO 15. Were sulfide samples received at a pH>9?
❑ YES 0 NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L? **
❑ YES 0 NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 rn/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation; (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding(circle one): H25O4 HNO3 HC( NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:Notify customer service immediately for incorrectly preserved samples.Obtain a new sample or
notify the state lab if directed to analyzed by the customer.Who was notified,date and time:_
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

ENVIRONMENTAL CHEMISTS INC 6602 Windmill Way
tO1? u � :Olt Wilmington,NC 28405
Sample Collection and Chain of Custody Phone: [phone]
���......... R ' ., parr'
Fax [phone]
Clicnt:,�lY�i/tsW%C4C�pi,��.��,c ►(��
Collected .By: ii44 1 Report No: ,-) r ?, - `i
Sample Ty ems: I=Influent, E=Effluent, W=Well, ST=Stream, SO =Soi1,jSL Slud.e I ther:
s
x r z PRESERVATION l
8 ova Collection o „ E
Sample Identification al a ;: 8. o L Y ,o t .. a ?
v� F o o d s E z U CS C _O ANALYSIS REQUESTED
DATE TIME TEMP U U -� v °z = x = 2 O
Ci
-� u---G�.p, rocs
` !1 11r1Gl"a1�
C P
G I I
i
C P 1
I
G
P v E
G I
C P I
i G
C P ;
1
C P
I G G
I G-I 1 G
C P
G G
.SCE L.5Okiirr(t eVli edl @01757 Z . f It. +em , 7 16 , -
Transfer Relinquished B Date/Time
______ Y�9 Received By: Date/Time
L. br4flefrn4tA 1/44• i 0.57( ' '-''' --C,A„,,,,,,---- 1;.---(... - 21 - 1,,,,)5 -‘5 ,
(-4.
'emperature when Received: a-- Accepted: _ Rejected: Resample Requested:
lelivered By: �, - ,--__ _ Received By - Date:_ // - -) , Time: n—

Environmental Chemists, Inc.
envirocheni 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,Manteo,NC 27954 • 252.473.5702 Lab/Fax
M' 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info it environmentalchemists.com
Brunswick County Public Utilities Date of Report: Mar 18, 2021
Post Office Box 249 Customer PO#:
Bolivia NC 28422 Customer ID: 08100011
Attention: Report#: 2021-03683
Project ID: Ocean Isle Beach
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-08973 Site: Sludge 3/4/2021 7:55 AM Solid/Sludge Scott Leonard
Test Method Results Date Analyzed
Sulfide SM 4500 S D 1.06 mg/kg 03/16/2021
Comment: kt ��Reviewed by: �(��
Report#:: 2021-03583 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab#94
6602 Windmill LA,
Wilmington, NC 284
910.392.02
Sample Receipt Checklist
Client!PJCPLA - eaA Date: 3\1* 2-1 Report Number: 21.- 3L 3
Receipt of sample: ECHEM Pickup Client Delivery 0 UPS 0 FedEx❑ Other Q
❑ YES (❑ NO .jn N/A 1. Were custody seals present on the cooler?
❑ YES /0 NO +I N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt ., °C or ected temperature upon receipt -C
How temperature taken: 0 Temperature Blank Against Bottles
JR Gun ID;Thomas Traceable S/N 192511657 IR Gun Correction Factor°C: 0.0
►' YES 10 NO 1 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES 1❑ NO I 4. Were proper custody procedures(relinquished/received) followed?
Ii YES 10 NO 5. Were sample ID's listed on the COC?
YES 10 NO 6. Were samples ID's listed on sample containers?
►U YES ❑ NO 7. Were collection date and time listed on the COC?
'4' YES O NO 8. Were tests to be performed listed on the COC?
91 YES 0 NO 9. Did samples arrive in proper containers for each test?
►2 YES ❑ NO 10. Did samples arrive in good condition for each test?
YES 0 NO 11. Was adequate sample volume available?'
YES ❑ NO 12. Were samples received within proper holding time for requested tests?
O YES 0 NO 13. Were acid preserved samples received at a pH of<2? "`
❑ YES 0 NO 14. Were cyanide samples received at a pH >12?
❑ YES 0 NO 15. Were sulfide samples received at a pH>9?
❑ YES I❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of<0.5 m/L?
❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of<0.5 m/L?
❑ YES 0 NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiies are pH checked at time of anal yss and recorded on the benchshe2t.
'" Bacteria samples aye checked for CHorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding(circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note:✓`o �
::i)✓C'sore'i N'Ce f??'^e�la:2�y' o. o for i c rredly preserved sa^1p'?s Obtain a new Sam(J!e Or
notify the state lab V'directed to ana yzed by the customer.Who was notified,date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

r� Y. ;k ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way
� � c.c9Qt�'1.1 Wilmington,NC 28405
----'/. Sample Collection and Chain of Custody Phone: [phone]
p, u _ Dig t Fax [phone]
Client: f � 1c
Collected Bv: . {— ate Report No: c7 — 0 3 6(-3
Sample Type: I=Influent, E=Effluent, W=Well, ST=Stream, SO=Soil L=Slut her:
x v , _ PRESERVATION
9 m Collection a „ o a
Sample Identification 2 W F�; o I o = Ell z ,, o 6 w o 1 ANALYSIS REQUESTED
DATE TIME TEMP V U° a V °z x E o
0513
6i ,5e.. . i14.3 3-4-42,1 07,55 t(o,3'SL 6) G SO ;d-es
C P
G
C P
CP .,... _ ._...� -------H
G
f f
C P
G
C P ! I}
G G
C P
G G
_ C P
t G G
C P ...._ i
G G !
� 1
pH- 53 .Iv.p ._ ((0, 3a e r'
Transfer Relinquished By: Date/Time :As" alive y,` r Date/Time
JL. P..
fri
t. b.
`emperatur e keceived: -2-‘ Accepted: ejecte Resample Requested:
lelivered By: Received By. ") Date: 314 -2-1 Time: \v-•30

BRUNSWICK COUNTY
ALKALINE STABILIZATION OF BIOSOLIDS
Facility Name: Ocean Isle Beach WWTP -SBR 4 Operator: Scott Leonard
Batch Size(gallons): 280,000 Lbs.or Gallons Used: 7100 lbs. Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date Corr. Corrected Corr. Corrected COrr. Corrected
pH Temp C TimepH TempC Corr. Corrected Initials
Factor+ pH Factor+ pH Time pH Temp C Factor+ pH Time pH Temp C Time
Factor+ pH
4/14/2021 6.80 18.5 -0.2 6.61 914 SL
4/14/2021 12.47 20 -0.15 12.32 1420 SL
4/14/2021 12.18 20.4 -0.14 12.04 1622 SL
4/15/2021 11.72 20.7 -0.13 11.59 1423 SL
N C)) CO CO O I,- `ct CO ' I, 0 CO CO 0) N u)
O o V V co co co co N N N — O O O O O O CON .�- N N N M C) M M v U.
U O O O O O O O O O O O O O O O Ci C) o Oo o C+ o O o 0 06 o O o
In N co U) (n co 4) V) U) )) co to N N y O N (n V) In N N U) N U) (!1 to N N N
7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 CCC O C C J C C C C C C C
C C C C C C C C C C C C
U
Q O 6) Co N- CD Lo Cr Co N r O W co N— CO Lr) 'Ir CO N O 0) CO N- CO II) CO N — O
M C`r) CO C)') CO C`') C") CO M cO N N N N N N N N N
H

SECTION VI
SOIL ANALYSIS REPORTS

Page 1 of 4
Report Number: 21-015-0934 W
Account Number:46646
\1 (an,,ou nt... 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: BIO-GREEN SERVICES INC ANALYTICAL www.waypointanalytical.com
383 POTTS RD "Every acre...Every year."TM Grower: Brunswick Co
ADVANCE NC 27006
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 01/15/2021 Date Of Analysis: 01/18/2021 Date Of Report: 01/18/2021 NC=North Carolina Fertility Index Value
OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0
Sample ID Lab % Soil M3 K MgCa Na Soil H
Field ID Number lbs/A Buffer
Rate Classppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/10og
BGAH1 22336 2.4 90 125 VH 47 VL 111 H 611 M 28 L 5.6 6.80 1.3 5.5
L MIN NC=104 NC=24
BGAH2 22337 2.1 85 88 H 40 VL 106 H 544 M 22 VL 5.6 6.81 1.2 5.0
L MIN NC=73 NC=20
BGAH3 22338 2.4 90 88 H 44 VL 109 H 577 M 26 VL 5.4 6.77 1.6 5.6
L MIN NC=73 NC=23
BGPV1 22339 0.9 67 18 L 5 VL 15 H 75 L 17 H 5.4 6.91 0.2 0.8
VL MIN NC=15 NC=3
BGPV2 22341 I 0.4 57 20 L 5 VL 12 M 64 L 14 H 5.3 6.91 0.2 0.7
VL MIN NC=17 NC=3
Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts
Sample ID
Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS
% % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate
BGAH1 2.2 16.8 55.5 2.2 23.6 27 H 5.3 H 3 VL 347 VH 1.5 M 0.5 L
NC=56 NC=132.5 NC=19 NC=75.0
BGAH2 2.1 17.7 54.4 1.9 24.0 28 H 3.7 H 2 VL 315 VH 1.1 M 0.5 L
NC=58 NC=92.5 NC=13 NC=55.0
BGAH3 2.0 16.2 51.5 2.0 28.6 ' 26 H 4.0 H 2 VL 329 VH 1.1 M 0.5 L
NC=54 NC=100.0 NC=13 NC=55.0
BGPV1 1.6 15.6 46.9 9.2 25.0 19 M 0.5 VL 1 VL 43 H 0.2 VL 0.1 VL
NC=40 NC=12.5 NC=6 NC=10.0
BGPV2 1.8 14.3 45.7 8.7 28.6 20 M 0.6 VL 1 VL 32 H 0.2 VL 0.1 VL
NC=42 NC=15.0 NC=6 NC=10.0
Values on this report represent the plant available nutrients in the Explanation of symbols:%(percent),ppm(parts per million),lbs/A This report applies to sample(s)tested.Samples are retained a
soil.Rating after each value:VL(Very Low),L(Low),M(Medium), (pounds per acre),ms/cm(milli-mhos per centimeter),meq/100g maximum of thirty days after testing.
H(High),VH Ve High).ENR-Estimated Nitrogen Release. (milli-equivalentper 100 grams).Conversions: t (+iaaH/
(Very9 ( q 9 ) ppm x 2=Ibs/A,Soluble Analysis prepared by:WaypointAnalytical Virginia,Inc. by m A
C.E.C.-Cation Exchange Capacity. Salts ms/cm x 640=ppm.
Pauric Mc Groary Ph.D.,CPAg

Page 2 of 4
Report Number: 21-015-0934 W
Account Number:46646 WaypOi nt,» 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: BIO-GREEN SERVICES INC ANALYTICAL www.waypointanalytical.com
383 POTTS RD "Every acre...Every year."TM Grower: Brunswick Co
ADVANCE NC 27006
Date Received: 01/15/2021
Date Of Report: 01/18/2021 SOIL FERTILITY RECOMMENDATIONS
Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron
Sample ID Intended Crop Yield Goal Lime N P205 K2O Mg S Zn Mn Fe Cu B
Field ID bu Tons/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A i lb/A lb/A lb/A
BGAH1
Soybeans 45 0.8 15 0 105 0 0 1.4 4 0 0 0.5
BGAH2
Soybeans 45 0.8 15 30 108 0 0 2.2 4 0 0 0.5
BGAH3
Soybeans 45 1.3 15 30 106 0 0 2.0 4 0 0 0.5
BGPV1
Pasture 3 0.8 50 71 120 25 9 3.0 4 0 0.9 0.5
BGPV2
Pasture 3 0.8 50 67 120 25 8 3.0 4 0 0.9 0.5
Comments:
22339 The sodium rating is high on this sample rather than optimum.
Sample(s): BGPVI,BGPV2 Crop: Pasture
For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer.
For soils low in sulfur, apply 20-40 lbs of sulfur as a sulfate in the spring with the nitrogen.
"The recommendations are based on research data and experience,but NO GUARANTEE or WARRANTY expressed or implied,concerning crop performance is made."
�jglWic �f (,/oay/
Our reports and letters are for the exclusive and confidential use of our clients„and may not be reproduced in whole or part,nor may any reference be made to the o
work,the results,or the company in any advertising,news release,or other public anouncements without obtaining our prior written authorization.Copy right 1977.
Pauric Mc Groary Ph.D.,CPAg

Page 3 of 4
Report Number: 21-015-0934 �O•�
Account Number:46646 Waypoint. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: BIO-GREEN SERVICES INC ANALYTICAL www.waypointanalytical.com
383 POTTS RD "Every acre...Every year",. Grower: Brunswick Co
ADVANCE NC 27006
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 01/15/2021 Date Of Analysis: 01/18/2021 Date Of Report: 01/18/2021 NC=North Carolina Fertility Index Value
OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0
Sample ID Lab % Soil M3 K M Ca Na Soil
Field ID Number lbs/A g Buffer H
Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/100g meq/10og
BGHB1 22342 1.7 78 688 VH 18 VL 32 L 363 L 17 VL 4.8 6.74 1.9 4.1
L MIN NC=573 NC=9
BGHH6 22343 0.6 61 23 L 5 VL 14 M 71 L 15 H 5.2 6.90 0.3 0.8
VL MIN NC= 19 NC=3
BGCG5 22344 2.0 88 49 M 4 VL 17 L 80 VL 16 M 4.5 6.84 0.9 1.5
L MIN NC=41 NC=2
Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts
Sample ID
Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS
% % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate
BGHB1 1.1 6.5 44.3 1.8 46.3 18 M 23.6 VH 7 L 263 VH 4.1 VH 0.4 L
NC=37 NC=590.0 NC=44 NC=205.0
BGHH6 1.6 14.6 44.4 8.2 37.5 19 M 0.7 VL 1 VL 44 H 0.2 VL 0.1 VL
NC=40 NC=17.5 NC=6 NC=10.0
BGCG5 0.7 9.4 26.7 4.6 60.0 41 VH 0.4 VL 1 VL 17 H 0.2 VL 0.1 VL
NC=85 NC=10.0 NC=6 NC=10.0
Values on this report represent the plant available nutrients in the Explanation of symbols:%(percent),ppm(parts per million),lbs/A This report applies to sample(s)tested.Samples are retained a
soil.Rating after each value:VL(Very Low),L(Low),M(Medium), (pounds per acre),ms/cm(milli-mhos per centimeter),meq/100g maximum of thirty days after testing.
H(High),VH Ve High).ENR-Estimated Nitrogen Release. (milli-equivalentper 100 grams).Conversions: r G/aau�
(Very9 ( q 9 ) ppm x 2=Ibs/A,Soluble Analysis prepared by:WaypointAnalytical Virginia,Inc. by: gN/ir (� A
C.E.C.-Cation Exchange Capacity. Salts ms/cm x 640=ppm.
Pauric Mc Groary Ph.D.,CPAg

Page 4 of 4
Report Number: 21-015-0934 0
Account Number:46646 WaiIOi nt.. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: BIO-GREEN SERVICES INC ANALYTICAL www.waypointanalytical.com
383 POTTS RD "Every acre...Every year."TM Grower: Brunswick Co
ADVANCE NC 27006
Date Received: 01/15/2021
Date Of Report: 01/18/2021 SOIL FERTILITY RECOMMENDATIONS
Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron
Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B
Field ID Tons Tons/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A
BGHB1
Pasture 3 1.5 50 0 120 19 10 0 3 0 0 0
BGHH6
Pines 3 0.8 50 61 120 25 9 3.0 4 0 0.9 0.5
BGCG5
Pasture 3 1.0 50 40 120 25 0 3.0 4 0 0.9 0.5
Comments:
Sample(s) : BGCG6,BGCG5 Crop: Pasture
For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer.
For soils low in sulfur, apply 20-40 lbs of sulfur as a sulfate in the spring with the nitrogen.
"The recommendations are based on research data and experience,but NO GUARANTEE or WARRANTY expressed or implied,concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„and may not be reproduced in whole or part,nor may any reference be made to the r m f 6.1p07/
work,the results,or the company in any advertising,news release,or other public anouncements without obtaining our prior written authorization.Copy right 1977.
Pauric Mc Groary Ph.D.,CPAg

Page 1 of 1
Report Number: 22-021-0824 W
Account Number:46646 \9 /a4point,, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: BIO-GREEN SERVICES INC ANALYTICAL www.waypointanalytical.com
383 POTTS RD "Every acre...Every year."ry Grower: Brunswick Co.
ADVANCE NC 27006
Farm: BR
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 01/21/2022 Date Of Analysis: 01/24/2022 Date Of Report: 02/08/2022 NC=North Carolina Fertility Index Value
OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0
Sample ID Lab
Field ID Number % Soil lbs/A M3 K Mg Ca Na Soil
Class
Buffer H
Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/100g meq/100g
BRRC1 20682 7.1 150 1238 VH 59 VL 67 VL 612 VL 18 VL 4.3 6.18 7.5 11.3
RC VH MIN NC=1032 NC=30
BRRC4 20683 6.2 150 1227 VH 54 VL 59 VL 605 L 18 VL 4.4 6.31 6.2 9.9
RC H MIN NC=1022 NC=28
BRRC6 20684 7.5 150 1203 VH 68 L 78 VL 913 L 19 VL 4.6 6.28 6.5 12.0
RC VH MIN NC=1002 NC=35
Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts
Sample ID
Field ID K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS
% % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate
BRRC1 1.3 4.9 27.1 0.7 66.4 29 H 86.8 VH 7 L 403 VH 10.5 VH 0.3 VL
RC NC=60 NC=2170.0 NC=44 NC=525.0
BRRC4 1.4 5.0 30.6 0.8 62.6 27 H 76.8 VH 7 L 405 VH 10.4 VH 0.3 VL
RC NC=56 NC=1920.0 NC=44 NC=520.0
BRRC6 1.5 5.4 38.0 0.7 54.2 29 H 89.2 VH 7 L 391 VH 10.3 VH 0.4 L
RC NC=60 NC=2230.0 NC=44 NC=515.0
Values on this report represent the plant available nutrients in the Explanation of symbols:%(percent),ppm(parts per million),lbs/A This report applies to sample(s)tested.Samples are retained a
soil.Rating after each value:VL(Very Low),L(Low),M(Medium), (pounds per acre),ms/cm(milli-mhos per centimeter),meq/100g maximum of thirty days after testing.
H(High),VH(Very High).ENR-Estimated Nitrogen Release. (milli-equivalent per 100 grams).Conversions:ppm x 2=lbs/A,Soluble by: Tawi‘ pit /.roarU/
C.E.C.-Cation Exchange Capacity. Salts ms/cm x 640=ppm.
Analysis prepared by:Waypoint Analytical Virginia,Inc.
Pauric Mc Groary Ph.D.,CPAg