WQ0009477_Residual Annual Report 2021_20220216

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Non-Discharge Branch Upload/Submittal Form
NORTH CAROLINA
Environment N Qmilelr
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0009477
Applicant/Permittee Cascades Tissue Group-North Carolina,A Division of Cascades Holding US,Inc.
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes 7 No
Regional Office Fayetteville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Karen V.Bellamy
Email Address* Phone Number*
[e-mail] 19109958292
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0009477
Has Current Existing permit number
Applicant/Permittee Address* 805 Midway Rd Rockingham,NC 28379
Facility Name* Cascades Tissue Group Class A Residuals Program
Please provide comments/notes on your current submittal below.
Please Contact Karen Bellamy 910-995-8292 or 910-895-4033 Ext 74280 if there are any
questions.
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
Cascades Tissue Group North Carolina Land Application
14.62MB
Annual Report WQ0009477 02162022.pdf
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature

Submission Date 2/16/2022

OIL Cascades Tissue Group—North Carekina
A Division of Cascades Holding US Inc.
805 Midway Road, P.O. Box 578, rbackinghem, NC 28380 USA
Cascades Phone: [phone] Fax: [phone]
www,casc 0 coni ' Info cascades.com
Date: Jan 31 ,2022
To: State of North Carolina Department of Environment and Natural Resources
Division of Water Quality
Aquifer Protection Section
Land Application Unit
512 N Salisbury St,
Raleigh, North Carolina 27604
1-919-807-6300
From: Karen Bellamy-CRC and Preparer of 2021 Annual Report
Cascades Tissue Group-North Carolina, a division of Cascades Holding US Inc.
805 Midway Road
Rockingham, NC 28379
1-910-895-4033 EXT 74280
1- 10-89 -1877 Fax
Karen BellarnvAascades,com
Permit # WQ0009477
Subject: Land Application Annual Report Cover Letter
Forms Included:
Cover Letter and Compliance inspection Letter from DEQ
Annual Land Application Certification Form DENR Form ACF
August 11,2021 Non-Discharge Permit W00009477 Compliance Inspection Report
Elwood Black PH D Letter on Field Application
Elwood Black PH D Pan Calculation for Cascades Biosolids
Excel Spreadsheets on Farmers, Field #, Address, Rain Data, Crops, If K Soil, % Solids: Acres: Wet Tons,
Dry Tons, Dry tons per Acre, Long and Latitudes
DENR Form DMDF and Additional Supplemental
DENR Form RSSF
DENR Form RF-B
Lab Results
T LP, Ignitability, Reactivity: & Corrosivity
DENR Form PVRF 2T
Letter on Vector Reduction
Page 1 of 2

Subject: Land Applrcatron Annual Report Cover Letter,
Cascades has 1 ORC and 2 Backup CRC. Karen Bellamy ORC and ( Corey Wyand & Jacob Groth as
Backup).VVe have more employee who completed training and still needs to pass the final exarri
Field Inspections where conducted, equipment calibration, PM work on equipment and ORC and backup
ORC performed required inspections for the year.
Corey 1Nyanq, and Karen Bellamy attended Rural Water Association Training in 2021 for our Continuing
Education Contact Hours. Jacob Groth took the exam and passed in 2021.
Dr. Elwood Black continues to work closely with our land application Program.
Advanced Residuals had No incidents in 2021 .
2021- Challenging year with Covid and difficulty getting parts for equipment, .
Cascades has received the New Permit for 2021.
Cascades and Advanced Residuals has worked hard to make sure we have a good program that is
Environmentally Friendly and also benefits the farmers. We have gotten a lot of positive feedback from
farmers. Duke Goodwin is the Project Manager for Advanced Residuals project at Cascades. Mr. Goodwin
has been a farmer for several years and also has worked at the City of Rockingham VV4VTP, so he is very
familiar with regulations, Duke Goodwin also received his certification for Land Application rn 2016 . Mr.
Goodwin arso received his continuing Ed hours for 2021,
Pathogen and Vector Reduction aren't required on by our Permit. Several of the heavy metals have also
been removed from our permit. since levels have been extremely low for over 10 years.
We also have testing performed by Department of Agronomics, so the farmers can have access to
information.

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit*: WQ0009477 County: Richmond Year: 202€
Facility Name (as shown on permit): Cascades Tissue Group-North Carolina, a division of Cascades I!o€ding LIS
Inc.
[.and Application Operator: Karen V. Bellamy Phone: [phone] Ext 74280
an
application of residuals as allowed by the permit occurred during the past calendar year?
Yes 0 No - If Igo, skip Part A, and Part B and proceed to Part C. Also, EC residuals were
generated but not hand applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
_ Total number of application fields in the permit:
Total number of fie€ds utilized for land application during the year:
Total amount of dry tons applied during the year for all application itcs= 21492.60796
—
Total number of acres utilizes for land application during the year:
Part B- Annual Compiance Statement:
Facility was compliant during calendar year 2021_ with all conditions of the land applic ion permit
(including but not limited to items I-13 below)issued by the Division of Water Quality. Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates,and explain corrective action
taken.
I) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)copies of
laboratory results are attached.
4) Annual TCLP analysis (if required)was performed and three (3)copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached_
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .] 105(a) or the Pollutant Loading
Rates in 1A NCAC 02T.€ 1 05(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CPR Part 503
regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T.11 1 1 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
€0) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
€2) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
€3) All buffer requirements as specified on the permit were maintained during each app€€cation of residuals.
Part C-Certification:
"I certify, under penalty of law,that the above information is, to the best of my knowledge and belief, true,accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of lines and imprisonment for knowing violations."
Karen V. Bellamy Environmental Manager _
Per it-tee Name and Title (type or print) Signature of Permittee Date
f Duke G �n
* Dte
77,
g store of Preparer � Dale Signature of Land Applier
(if different from Permittee) (if different from Pennittee and Preparer)
'" Preparer is defined in 40 CFR Part 503,9(r) and I SA NCAC O2T.1102 (26) DENR FORM ACF (1212006)

Itfti
ROY COOPEF
Couemar �
ELIZABETH S.BFSER ,
secretary h„c„
S.DANIEL SMITH Norm cAROLINA
Ofrerrnr Environmental Q er y
August 11, 2021
Karen V. Bellamy
Cascades Tissue Group - North Carolina A Division of Cascades Holding US Inc,
PO Box 578
Rockingham, NC 8380-0578
SUBJECT: Compliance Inspection Report
Cascades Tissue Group DCAR
Nora-discharge Permit No, WQ0009477
Richmond County
Dear Permit-tee:
The North Carolina Division of Water Resources conducted an inspection of the Cascades Tissue Group
DCAR on 8/1O/20Z1. This inspection was conducted to verify that the facility is operating in compliance
with the conditions and limitations specified in Non-discharge Permit No. WQ0009477. The findings and
comments noted during this inspection are provided in the enclosed copy of the inspection report
entitled "Compliance Inspection Report".
If you should have any questions, please do not hesitate to contact Tony Honeycutt with the Water
Quality Regional Operations Section in the Fayetteville Regional Office at 910-433-3300 or via email at
[e-mail].
Sincerely,
ocu.rpned hy:rf
D1,
Sr9rFr'a�3OE}�d2$,
1. Trent Allen, Regional Supervisor
Water Quality Regional Operations Section
Fayetteville Regional Office
Division of Water Resources, NCDEQ
ATTACHMENTS
Cc: Karen Bellamy - ORC
WQS Fayetteville Regional Office— (TM)
NON- 1SCHARGE Compliance Laserfiche File
7rnrih t:rapru Ofwrtrrr,ir AfErnImaruniAltyrogly L Un,FnnN Wait-Rrwurc..
F.,rtw.1k R.. tg9Flkr 14M.cr rt01.4,�ru.rufrrur„Fk,rswihir.dn.IOW!

Compliance Inspection Report
Permit:W00009477 Effective: 01101121 Expiration_ 11/30/26 Owner; Cascades Tissue Group• North Carolina A
Division of cascades Holding US Inc
SOC: Effective; Expiration; Facility: Cascades Tissue Group DCAR
County: Richmond 805 Midway Rd
Regient Fayetteville
Rockingham NC 283794101
Contact Person;Karen V Bellamy Tin: CRC(201i designasion form) Phone!910-895.4033 Ext-2280
Directions to Facility:
Travel US Hwy.74 is US Hwy- 1 intersection- Follow US Hwy. 1 interchange. Turn west onto Midway Road, The plant is
approximately two miles from this turn
System Classifications! LA.
Primary ORC: Karen V 6ellerny Certification: 19197 Phone:[phone]
Secondary ORC(s):
On-Site Representatives};
Related Parrnits:
Inspection Date: 08110l2021 p1:30PM Exit Time: 03:30PM
Primary Inspector:Tony VV Honeycutt pn, onr, s Phone; 910-433-3339
Secondary hispectnr(s); 4axosgroa,cr4c2..
ocouslgrea by:
8/12/2021
Reason for Inspection; Routine 5.isx303hU1C429. Inspection Type: Compliance Evaluation
Permit Inspection Type: Distribution of Residues Solids{503 Exempt)
Facility Status: Compliant 0 Not Compliant
Question Areas:
• Miscellaneous Questions Record Keeping
(See attachment summary)
Page 1 of 3

permit: WQ4009477 Owner-Facdllty;Cascadaa 1i$ u9 raL -North Carolina ADiviJion of CascatlaS A:Ming US irbO
inapeclian Date: QB11 Q12021 Inspection Type:Compliance Evaluallon Reason for VCslt, Routine
Inspection Summary:
Cascades produces a class "A"material.
The facility records were up to date and ava iIablr for review.
Ms. Bellamy goes ahovo and beyond in her record keeping and management of the Cascades land application program,
No additional Items noted.
Page 2 of 3

Perm It; W03109477 Owner-Facklity_Cascades Tssue Group-Narlh Carolina A Division of cascades Holding US I no
Iris practi am Date: 0$J10.+2021 Inapoction Type;Compliance L'-waluailon Reason Far Visit: Rouiire
hp& Yea No NA HE
Distribution and Marketing ❑
Land Application U
Record Keeping Yes No NA Ng
Is GW monitoring being conducted, if required? ❑ ❑• ❑
Are GW sarrtptes from all rvIlArs sampled For all required parameters? ❑ ❑ U ❑
Are there any OW quality violations? ❑ ❑ ■ ❑
is GW-59A certification form completed for facility? ❑ ❑ • ❑
Is a copy of current perrnil on-site? e ❑ ❑ ❑
Are current metals and nutrient analysis available? NEED
Are nutrient and metal loading calculating most limiting parameters? MOOD
TCLP analysis? • ❑ ❑ ❑
b. SSFA{Standard Soil Fertility Analysts}? • ❑ ❑ ❑
Are PAN balances being maintained? • ❑ ❑ ❑
Are PAN balances within permit limits? U ❑ ❑ ❑
Has lend application equipment been calibrated? ❑ ❑ ❑
Are there pH records For alkaline stabilization? ❑ ❑ � ❑
Are there pH records for the land application site? ❑ ❑ E ❑
Are nutrienUcrop removal practices in place? 1111171171171
Do lab sheets support data reported on Residual Analysis Summary? e ❑ ❑ ❑
Are hauling records available? II ❑ ❑ ❑
Are hauling records maintained and up-to-date? ❑ ❑ ❑
#Has permittee been free of public complaints in test 12 months? ❑ ❑ ❑
Has application occurred during Seasonal Restriction window? ❑ ❑ • ❑
Comment:
Page 3of3

January 31. 2O22
Cascades Tissue Group
PO Box 578
Rockingham, NC 28380
Attention: Karen Bellamy
Dear Mv15 Bellamy;
From Jan 1,2021 thru December 31, 2021. Biosolids was distributed only to agricultural land. No
Farm field received Biosolids in a continuous year-to-year application as defined by the North
Carolina Department of Environmental Quality respective to permit W00009477-
These 5tatement5 are based on information reported by Advanced Residuals Management.
Sincerely:
Elwood Black, Ph.D.-Soils

Date 1/27/2022
subject: PAN calculation
The Plant Available Nitrogen (PAN) calculation is widely used to estimate the N that will he available to a crop from the biosolids. The carbon to
nitrogen ratio in biosolids is commonly less than 20:1 and net mineralization of N from the biosolids occurs.The mineralizations refers to the
transformation of organic N to inorganic N which is in a plant available form. For materials with a C:N of less than 20:1 the PAN provides a good
estimate of the N that may be available to the plant.
However for materials like the Cascades soil additive , which have a C:N greater than 3O:1,the PAN calculation is not appropriate. Instead of
mineralization, N immobilization occurs_ For crop production, immobilization is a loss of plant available N. Asa result farmers need to apply
additional N to offset the N that will be immobilized as the soil microorganisms assimilate the fiber.
The FAN should be O.
Elwood slack, Ph.D. -Soils
Cascades -ATTENTION: Ce courriel provient de 1'exterieur de ('organisation_ Ne pas'diver sur les liens et ne pas ouvrir 1es pieces jointes sauf si
vows reconnaissez I'expediteur et que vous etes sur que le contenu est legitime_
Cascades - CAUTION: This email is from outside the organization_ Do not click on links or open attachments unless you recognize the sender and
you are sure the content is safe_

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CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT th W 0009477 FACILITY NAME: Cascades Tissue Group-North Carolina,a division of Cascades Holding US Inc,
PHONE: 9i0-895-4033 74280 COUNTY: Richmond OPERATOR: Karen V. Bellamy
FACILITY TYPE(please check one): 1)urface Disposal (complete Part A(Source(s)and "Residual In" Volume only)and Part
Distribution and larketing(complete Parts A, B,and )
Was the facility in operation during the past calendar year? Yes No ❑ If No skip parts A, B,t~ and certify form below
Part A*: Part B*:
$ouree5(s) (include NPDES# if Volume(dry tons) Recipient Information
Month Amendment!
applicable) Residual In Product Out Name(s) Volume(dry tons) Intended use(s)
Bulking Agent
January W 0009477 1909, 8385 I909, 8385 See Attached 1909.28385 Agricultural
February WQ0009477 I I854_]4944 1854.14944. 1854.14944 Agricultural
March WQ0009477 1562,84400 1562.84400 1526.84400 Agricultural
April WQ0009477 1924.14212 1924.14212 1924.14212 I Agficultura►l
May WQ0009477 I 949.27706 I 949.27706 1949.27706 Agricultural
June WQ4009477 _1058.77044 1058.77044 - I058,77044 Agricultural
July WQ0009477 1936.32648 1936.32648 1936.32648 Agricultural
August WQ0009477 185 i.09230 185 i.09230 1856,09230 Agricultural
September - - - yQ0049477 2002.70727 2002.70727 2002.70727 At cultural
October WQ0009477 1712,04.552 17[2.04552 I712.04552 Agricultural
November WQ0009477 _ 1866.90096 1866.90096 _ _ 1866.90096 Agricultural
December VQO009477 1860.06852 ]860.0_6852 1860.06852 Agricultural
Total from FORM DMDF(sup) 0 21492.60796 21492, 07{?b 21456.60796
Totals: Annual (dry tons): 0 21492.60796 21492.60796 / 21456.60796
Amendments)used:1 Bulking Ajuenr(s)used:
* If more space is required,attach additional information sheets(FORM DMSDF(supp)): Total Number of Form DMSDF(Supp) 8
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: Li No If No, Explain irs Narrltive
I, All monitoring was done in accordance with the permit and reported for the year as required and three(3)copies of certified laboratory results are attached,
2_ Al] operation and maintenance requirements were compiled with or, in the case of a deviation,prior authorization was received from the Division of Water Quality.
3, No contravention of'Ground Water Quality Standards occurred at a monitoring well,
"l certify, under penalty of law,that the above information is, to the best of my knowledge and belief,true,accurate and complete. I am aware that there are significant
penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
•
era.
Signature of Permitter Date Signature of Prepurer** Date
(if different from Perrnittee)
**Preparer is defined in 40 CFR Part 503.9(r)and I5A NCAC 2T_1 102 (26)
D1-NR FORM DMSDF (i2i2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT#: WQ0009477 FACILITY NAME: Cascades Tissue Group-North Carolina.a division ofC'ascades Holding US Inc.
PHONE: [phone] COUNTY: Richmond OPERATOR; Karen V. BelIerny
FACILITY TYPE (please check one): Drface Disposal(complete Part A- ""Mouth","Source(s)""and "Residual In" columns only)
OF-Distribution and ;4larketing(complete Parts A,and B)
Part A*: I Part B4:
Volume(dry tons) I Recipient Information
Sources(s)(include NI'DIES Of i1 • I
ioo#h applicable) Amendment! Names) Volume(dry I Intended use(s)
Bulking Agent Residual In Product Out tons)
1:,it W 0009477 247.65315 247.65315 John Bridges 247.653 5 ag ,
WQ0009477 20.26745 20,26745 Lacy Cummings 20,26745 ag
WQ0009477 78.86965 78.86965 Superior Crane 78-86965 ag
W 0009477 334.09890 334.09890 Bill Hardin 334.09890 ag
W 0009477 78.27715 78.27715 Wilbur Harris 78.27715 ag
WQ0009477 56.06630 56.06630 James Locklear 56.06.630 ag
WQ0009477 99.96265 99,96265 Rickey Lowery 99,96265 an WQ0009477 _97.90865 �_ 97.90865 Ratlin Matthews 97.90865 ag
WQ0009477 233.68395 233,68595 L8cft Moore Farms I 233.68595 a
WQ0009477 106,48805 106,48805 George Mullen_ ` 106.48805 ag
WQ0009477 49.63570 49-i 3570 John Muller . 49.63570 . ag
Q0009477 327,59720 327,59720 fo, erOxendirte I 327-597203 ag
WQ0009477 17.81845 17.81845 Adrian Purvis 17.81845 an,
v4'Q00.09477 10.19100 10.19100 _ Michael Ross 10,19100 ag
WQ0009477 9.36545 9-.36545 Chris Thomas 9.36545 a
_ V4`Q0009477 21.54330 21,54330 Tommy Williamson 21-54330 a
WQO009477 59.09990 59.09990 Dwayne Wright 59.0999 i ag
WQ0009477 21-01400 21.0I 400 Eric Blalock 21.01400 ; ag
V4Q0009477 19.66705 19.66705 Jamie Caudle _ 19.66705 a
WQ0009477 _ 20.07390 - 20.07390 Franklin Lee 20.07390 I ag
TotaIs: Annual (dry tons): 0 1909.28385 1909.28385 1909,28385
Arnendment(s)used:I Bulldog Agent(s)used:
* If more space is required,attach additional information sheets(FORM FTh4SDF(supp)): Total Number of Form DMSDF(Supp) 8
DENR FORM DMSOF (Supp)(1212006)

CLASS A ANNUAL D!STRIDE 11ON AND MARKETING/SCRI A('F DISPOSAL CERTIFICATION AND SUMMAR'i FORM
Supplernentaf Information
N'Q PERMIT0: W.LX J444T7 FACILITY NAME; C'ascadeaTivsuc 4imup-Nupli Carolina,a divisien c.4ff Cascades Holding US Lae
PHONE;910.895-4033 74220 COUNTY!TY! Riebinuud - - .... _.. OPERATOR: Karen V.Aellan3y
FACILITY TYPE{gleam cheek one1: Surface Disposal{coinplcle Part A-"Nloelh","Sourcc(s)"and"Residual Ih"columns only)
X !NMI- m:don and%la Aeai SR{egmplere Parrs A,and IR}
Part A`; ]Surd I4•:
niJme(dry toes) Recipient Information
!Llar4th Sources(s)(include'IPDES Al if F1an�cis! Vatunie IntcnUed aiae(sl
applicable) Amendment/ Bulking Agent Residual In PLoduea oae I dry Lln'S I.
WQ0609477 30.01742 20.0!7y. Eivi'n1) 13aacuio 20.01792 eg
WQ1X09477 74 72832 70.72832 _ Lee i3 • 76 72$32, ag
WQ 6v44 7 20.2300E 20.23008 Jamie Caudle 20.23DD8 ag
WQOLi09477 1130.82/84 13U 82784 l.aty Cinninini p 130.$27$4 ag
W000094 7 311.67264 318..57264 Dalc DcWiin 318.0264
WQo6D9377 30 26460 30.254C0 3u101 I. C..T.n 36.254i10 ag
WQg049477 10.108S0 ]0.108S0 Frank Howcy 10.10880 ag
WQ00[6.i77 - -- 90.79616 9p. mes 79616 � Aarun A 90.79616 ag
WQ465119477 40.26880 10.268S0 Franklin lee 40.26880 ;yI
VON:09477 50-44384 50.64384 Jason Mahe 50.64384
WQ0069477 107.5 00 107 53600 f Iin Allultlunws L07 53600 $g
WQ0407477 200-4 E00 20.18800 Babb}.McCollum 20.48800 qJ
WQ0009477 59.52960 59.52960 Mike McCormick 59.52960 ag
WQ0009d77 59030d10 551.03040 L7kwiRhl MicholI 59-03040 ak
h� R'Q0009777 _ 120.17360 120.47360 Ozsiar Lee Oxcndina I7(P-47360 ;g
WQ4009477 103.19744 106.19744 Rog iOxeodion 108.19714 249
WQ0009497 161.32296 161..324196 ClrarLec l96pe 161..3295 a..
WQ0004477 7S.84032 7834032 Charles Richardson 7&84032 ak
WQ0009477 I 254.191580 254.19680 ThomasSteeke 254.19480 ag
RTLX1064477 ' 10I.969'}2 ]OL.96992 SapercorCrane 10L.% J2 ag
ITatalsr Annual idry tnna) 4 !1 R5-4 11$J.E IRS! i 1Y44 - - 1354 1.1 J44
. 'nrnd'n 't(a)UM!:I Bulking Agrngs I used:
'lfmorc space is n71111ir&i4ia0 ad,zielieffifil iI!1Mn2Linn sheers(FORM DMSDF(supp)J.: Total Nurnbea of Form DMSDF{Sapp} 8

CLASS A ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT#: WQ0009473 FACILITY NAME: Cascades T'issue Cruup-North.(arulinai. a dil Sion of(-$scadc-6 Holding kJS Inc.
PHONE; 9W-895403 74230 00UNT}:: Richmond OPERATOR; Karen V. Bellamy
FACILITY'TYPE/please c heck une): Surface Disposal(complete PaartA-"Month","Sourttl(sr and"Residual le"en1umes only)
X !hod butinn and M3rlicling icnrnp]etc Parts A. B)
Par!A4; Part B":
Volume{dry tans) -- Recipient Information
monthSourees(s)(include NP11I;S it if
hlame(s) Volume(dry Jntcnded usc(y)
applicable) Amendment( Bulking Agent Residual In Product Out tons)
Mar WQ0009477 440.44824 440.44824 InnQ Ranch J 440 44824_- a
WQ)[ 9477 54.70464 54.70464 John Brides , 54-70464 ug
W00009477 48-43368 48.43368 Franklin Byrd 48.43368 a;
WQ0009477 88.27488 88,27488 Chris Dewitt 88.27488 ag
W'Q0009477 105.98616 105-98616 Franklin Lee 105-98616 ag
W Q0009477 58 9396$ 58.93968 Ly'avan Lowery 58.93968 a .
W Q0009477 82.24)56 82.24056 L&R Moore Fars 82.24056
W00009477 144.71352 144.71352 Omar Lee Oxcndiie 144.71352 a4
WQ0009477 26{].82216 260.82211'i Rilgo-Oxendinc 2( 122]6 8g
WQ0009477 29-97168 29.97168 Chris Pope 29.97168 ag
WQI]0(9477 9.46560 9.46560 Mithaet Russ 9.46560 ag
WQ0009477 40.14720 4(i.t4720 Ronald Strickland 40,14720 a
WQ0009477 9.90216 9.90216 Chris Thomas 9.90216 ag
rVQ0009477 .178.59384 178,59384 Rill Webb 178.59384 ag
I` V�Q00943F 10.2000 I.0.20000 .I°mnt 4'illiamsun 10.20000 ao 11111111111
AGMIIM
lh`Q0009417 223.45 223.45 Lannie Allen 223-45 ag
W Q0009477 13.6.83424 136.83424 Kevin Saucom 136.$3424 a
WQ[WJt. 477 107.31268 107.31268 Franklin Byrd 107.31268 ag
W00009477 42.62772 42.62772 Robert Byrd 42.62772 aag
WQ0009477 31.04756 31.04756 Jamie Caud476 ag
isle 31-0� ..
- WQ0009473 _ - 1i 'i730Q 65.Q73{]-0 Ra}Collura 65.D73. -5ti11 ag iiiiii
Totals: Annual(dry toms): 0 2 I 69.18920 2169.18920 2169.18920 -
-
,Ametidmcnlls)usod;I _ Bulking Agent(s)used:
.*lfmare space is required,attach additional information shIoots(FORM I)M SDP(Sapp)): Total Number of Form DMSDF(Supp) 8

CLASS A ANNUAL L}IS-I`RIBcrIoN AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
R'Q PERMIT N: WQ H 9477 FACILITY NAME: C tadrs Tissue axarrp•Ncvlh{'analma,a disiginu ofCasimeh:§Wading(:$Lnc
PHONE:[phone] COUNTY: Riclouut t OPERATOR: lC.3re!n V.Sellir y'
FAC'iLllY TYPE[please thtelt one} Surface Ikxleusal(Enairdele Pert A-^SSarstie",":io•erulx)"and"Residue'In"columns nnlsy
X Distribution and Miaowing Eeoiaplm Paris A,surd 8} _
Fur!A•: Far I IP
•
I1 ul u me,J Ions.) Recipient Enformaiinn
Souretgs)(lnelude N PAES Al ill' 'a no[s} Vo hone{iJr
Mouth Intended use(s)
1 SIppticehle) Amendmaltt: Bulking Agent I Residual In ProductOnL tam)
A rHC"ontiantimmilipd W'L 000'1477 L3_?_.15+]33_ 132_]643Z ChrisDeWrLt 1r2.16Ac12 4W00004471 --- -75 1 152 75.13152 Jeremy Efrid 75.13 J S2 ,
WQ30041477 47.gg0110 47.48040 Ltsrtr Hine€ a7.48(40 a5
WQ01305.1.77 291.65E+36 271.64656 han lii Lu '_9 1.66656 a5
4i'Q0 J 1477 632.03669 62_2.133634 Bill Web'!" 622 0:3614 ny
W00404477 L25,3-537 l28.34532 Shaun Morgan 128.34532 e,;,
W Q0009477 2097346 20.97596 Litany l'4pliu - 20_97596 4
1LQ0409.I77 21.61144 21.69144 LAM AIkl 21.691.44 41l'Q0409#77 144.50103 14-4.50E03 Mark Allen 144.50103 ag
'11,0-i 9437 176.0/316 1 376.01116 Etue(}Rasrth 376.0]316 sly
WQ11409477 72.39222 72.39222 Emmett Nadi 72.39322
WQI*00177 33.58452 93.58152. Danny Poplin 93.58452 ag
WQ0004177 123.752LS I23.75288 Jury Roan , 121.752d8 ag
W Q9004177 1.48.0146 34408316 Wayne Saunders 346.98346 ag
WQ0004177 63.606St 63466.51 - DyineSarider 63.40651 se
W04039477 1;9.44-46I I29.I4441 Qkn Troia 1.29.04461 aqs
1k'Q0L149177 51.55101. r 51.55101 Bilk Webb SLS3101 4
W Q0044477 7,0!.829a; 309.80443 Chad Whitley 100.80943 ale
_ WQ0u49477 214.7i4679 214.3-4659 Rankin)Byrd 214.3-4679 aT
. wrjoi fl9477
rulaiSt I Annual lily! Edna): 0 3267.07.10 3267.0740 3_267.4 7460
L. hmundinent()uteri I ]3ulkiny Aprnl{s1 used:
-I I inure spate sa seyuire&atiath addrhooal ntforrnasion shads(FORM 1MSDF(aim.' Tara[Number of lono DMSDF(Supp) 8

CLASS A ANNUAL DISTRIBUT/ON AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Suppkolenl1t Informalion
WII)PERMIT 1: WQ4999-77 FACILITY NAME Cascades Thane GruupNurrhOa:alum.a alit isinaffazevfes Hulling USlrr.
PHONE:910-F454033 741:6( COUNTY; Ri Iiii Opd OPIE.Fi-i-11514. Y48rE V.6811Esnp
FA{.,,-t'r t"I'YPl:(pleaat cheek ars*. Surfuet 6eispassl;eompleee Pali A A.-MEW,"Source(sr"sad"Residing Ln^arduous;anLt'}
X Disarshu[ion and!darkelinie(tampbe[e Parts A.Nod 8!
Parr A': E^arr kr
Warne Or),ians} 3irripiern luferaa[ioc
i4rarC61441{melyde NPBE8 I If Valuie(Jr..
111um1h rtailuclapplicable/ ,Loendmenlf Ela igg.4geee Residual la Ftia srs(s1 sons i In-ended use's)
Jame WQ11ID 477 45.96138 4496I3a 1 Anson CauntyAiGui 45 le!38 ag
WQ4009477 156.01696/L5601698 Blue Q Ranch 15661658 28
wQplow77 2A5.43i 18 2.1?.5.41.!l I9 T}{er.Edxards 20641410 allWQi1009477 85.42474 8542476 MarkCiaddy 85.42476 alit
184Q01103477 124.68636 EIS 4$G77h C/wlecCG46c 12i.1:447Z
WQ9079477 -
I491121 S !49 36218 Leff Lase Id9.S 16 48
WQPx19477 I I L6 31926 1136.1 I926 Emmei Marsh. 1 Ib.II 35t6 43
WQg034777 4!o3u4# 41.33946 Lynn&MIA llrumlrs 41 7,3946 21F__,
WQ41:19477 /487708 24.87713F Glenn Tradar 2487Tp11 ao
WQC0;/9477 3249400 D3.l l:I3 Wane Saunders 32 4%44
411QCON1477 5045868 9045216E Tlrg4d0l3 Ft 1•miier in4.5.968 srk
-
WQ41O09477� a3$IM 835[64 DuaneSuiier II151a4 rig
WQ0209477 /664856 to 44856 Michael Gaskins" Ib.6485h au
d Ir VlQr1fr0917J 41.72415 41.72056 Eric$11 #, 91'7J[ES$ ea173.4404
�4TJ !4!#774b PM 3774>a J'finny EUry 14$ 7746 2x 414.#4652
_ W 0000.77 71 S74114 71 53414 Michael Q¢skins 71 57414 ag 39.3E035
984004 23 ff. Racer Gae 79. 404 IV4¢d149#T+ 42.6
F riWQ307
u'Q4#7't 6d7682 fi660582
205.7395p 285.33964 Charing 11as
Robert 1101 60.685112
205 73960 ag
al I li.[9 79
7.03772_ I '0040#11 11206998 I L2069518 _ Emmelt Marsh 112.06998 aK
u•fiiil .7 112.52884 322 53864 K-.n kWin 323.52813 au
WQ00094n 4012171 74001n0 -
2 L.Cnu.s. kls]selmrd 4008202 ag
- WQ449P#77 - --- 7#.12t}74 73 12474 7hoQ.ssPoe 73.12074 38
WQ0o09477 I11.68542 L III 68542 LackPraien !]].68542 ag MUM
balm .4•11111•11 idry E01:1 ! 6 7,4*p1sop 24.ffi I1104 MI6.11101
AsieraLiR (s)used I RulkigAgenttslused
[f mere-space- is reysired.snarls addciunal information sleets;FORM DM3L31 WW1 raial\umker of Farm Ll}.3SDFF(Srrpp]1 8

CLASS A ANNUAL D1 'FRIB[ fION AND\IARKEFIN(;f SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Snp/lcmenia!Information
Illi:12 PF.RMIT It '1x1o9S77 FACI LIT1r'NAME: CaScadcs'i'isane Grourydwx1h Carolina.41 di t iswn of ease w Holding]diog US IIw
PIIOETF.:91( $95463.374381) COUNTN: KitIououd OPFRa<TOI1: Ken V.Ba11em
FACILITY TYPE(pleaile tbe[k wee): Sorfacr Dispose!fcom plete Part A-"Month","Sou me1.5)'.MCI"Residual le"Loki dun only)
X Mirib■liui amJ 3Earkeiing(comrade Ports A..iod 11).
PM A or P»Pe B"i
Volume Or!lens) Recipient Informalipn
MUnbY Seerces(x)(include N PRES A if
— applicahk) Amenclinerei Bulking Agent
JuLv {:onlinucd W"fe'0 47 7022818 70.22S18
WOMINifl 317.9fl O 317.9726.0
13r
Mill= 254.62175
■ 104.141 16
73.110358
4239784
8l.{+4434
▪ ' LsuryGamar 72.25906
.: r Garocr 371.98456 a
wcac9i77
u(wuu4a77
u'1;104309477 F F
u'(7[la[a1477 30.4 4142
WQ00O9477 104'38592 194'38592 Ventie Ritter
14 41009477 323.01477U 32s.08774 wayrn Scuuders
Ve(}1}O04477 I36.21316 I36.2L3I4 Bobby Stung I36.21515 ag
eg
Tomb: Aeattyl{dry■oax): D 2365.U7418 2365.07418 2_lS.O7418
Aioendrmon[(s)used{ Eiulling Agen1(5)upgd.
*I f most awe is regaiftd,math mdditiona3 infomwiion sheets(FORM DMSDF(supp)): Tois3 Number of Irwin 1AA1S])L'ESupp}[ a

CLASS,A ANNUAL.DISTRIBUTION AND MARICETINC!SURFACE DISPOSA1.CERTIFICATION AND SUMMARV FORM
Supplcmcnksl I nfurnlalio-s
wQrER41ITI: WG.Ol 471 FACILITY NA INE: Ourattes tosueCiicup-NuitIit uulrna,a division of Ciisnades Holding 3;-SIpc
PIIONE:$14.105-1033 74180 C:OE:ti1'Y: Richmond CIPLRATOR= --kirerl V.9d'llarny
F'ACIIITY TYPE(please check urte): :'erface Dispusel{complete{'art A•"Maniir","inurce(s)'r and"ResiduR]In"columns only)
X Chl irihuliOn&red;larkuiin.(cornpretu Parts A,and BJ
P�kri A": - - Part ii':
Volume!dry ions) Redpk.t IrfWYYido11
unto Month Sourcec( (include NFDL:'N if applicable) lJgtrryc(s) +ol liMteSddd
.lonendrnent, Bulking Agent Residual]n Prodpci Qut Ions) use(s)
dooabd Chriuwe
Larry Coln
sit 15E96 sg ISM
Aden C.ccikt
5.8.15190
+- Rcs itCi
L50.13114 k50.13114 ilot={rangier E54.13114 au
MIME lig
86. 793
4.24.85094
21.9..21986
4
4
a •
4 21 WQO009-177 L9.521Di1 I4.5$1Di1 i2mmne Blalock I4.5$4D0
W000094177 234.38376 231.38376 Dorn Brcols 21.38376
W4:101:104177 18LIr52,64 I21&652,fi4 Hasten Cautlill ]$41.01£4 as
WQ0029a77 2111.6368 213.16348 P01,INgini6 213.16MS
W 0009477 I 31538308 315-38808 Ler Farms 315.38808
- --W 9477 61.03272 6].01272 franld'in Lee 61.03272
WQ4049A77 44 R143 44 R192 Michyol Rosa 44 R142
W'Q40419477 20 7472 2(0.7672 Wa}neSadriders 20 7672 II . ..
Tgmise Annual{dry inns): 0 3116.41 5i 3116.49$55 3116:49855
AintIldan L({s)tried. Bulking Agenb(a)used:
.Ifinoot egad is requited_wield add'uianok informs{ion all (FORM[Y-S.L }Flsupp)): Tocal NpmbcrofFarce f)MSDF(Sapp) 8

CLASS A ANNUAL D1MIBLI TION AND MAR KETINCl SURFACE.DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental 1nfbrrnutlgn
WO.PERMIT a: 94 140DO4.77 HACILk7'Y FiANE! (- S,.4.-s. ao„4[inno0-14r111 Carolina.aJisisam of{ao,ail kkl�rw LB Ir,c
PHONE;0104954033 7-afKr. CO(i TY; Richmond OAERAlDit! Karon V B5N3If#
PACILLT3:T30E Iratose check oat)! Surface TYnipobl{eeamplele Pan A-^Memdi",'54nrte1i) and'Residual In-columns oob}
Si 04ir+h*Iinn ami ttarkrling fcoenpleir Paris A,and B]
Puy Ar! Purr h"r
-
_ Volume SonsJ Re:ipe tlehrmauae
Sawses(s){inch„dr?F11E-5 H it Volume
nlondud 4l4IS7
e Product h'am x 1
appGra4k) Amendment Bulking Agent Residual In Out (dgton)
Con 3p21(. Al ued 44'Qiw709477 3B2 213TS4 2R:A37744 In.:t it 5,,,:Ih 262.23714 ag
WapS00471 36.02 L52 3192151 Latvia Su, 3H p2L$2 a.
▪i-Agt0a7T - - - ...247.3948g 247.3448E grid Undernood 2.4116 81i _ ore
1.441,.31 tiy'QQ.7094- 164C12aa3 166.141 ElioBl.los3; '106.02192 {g
W IXE14194- 95.79[62 95 741694 5 MaoHRwkS _ 93 79168 ..
W'{}rrL10447? -02.4351a 42.43636 ionic Caudle 4343535 ite
14'4400'14T7 1042456 1042416 Adam Cooke _ 1O42416 kit
W030¢9477 2523057n 252.10176 Jody111enm4 N 3N1576 .3
vozo1014?7 114.42A}: 144 4202 Pranklm LIM 12-0_42p3"_ i3
wQ30p94� 34d49632 346.43693 Los.Farms. 346153.533
W Q5009477 n15{1A4 221.5C0na I . T. liar 22L.50600 ,
w®II094T7 60L.95741 60l.95744 D vid L1ndonsood 66L 95744 is
.ace-21 - - Wip6(19477 241557% 242.55136 iasan Bhock.Yt#atr 24255736 e3 155 75S2
WQ2D11.94T? 37.62512 37 O2512 Ramie Blalock 17.62511 e.0 l 3E6£7
WQ600941`7 945.9% 94A096 _ don Brooks_- _ 9 qg 9.4154h 98b3P4
- -WQ1:10¢4477- 2190421 2190422 Rimeeat�4 1151:1466 Pi_ 14A13T
W 25009477 4&6W24 96.60024 Lain:Caley 9BM0E4 as
WQ00lM77 52.15}}6 52.25336 Adam Cooke 5215332 pg
WQOOO'477 4$21.924M -IAA92oa IxeyCur ins. 4229206 PS____ 460.1M*2
W Q901114417 r 1465}36 14.4138 Jaiy llfinin 14614336 at I
Toiab; Annual ldgMedic 0 3E1931722 30.93,3733 349L3722
Amendmenl(s]used.' L9ldking,sesefsli axed --
•11'Mart space:.,requdoa.anxh eddirimml information sheets{Fl RRI>}l.LSDF(suppp. Tact kumtfcr of Fonts I)INSOF'($„pp)I A

PRONL. .REF! COUNTY: Ric!wawa OPERATOR: Karen V. Betamy
FA(:11,lTYTYPF{rime checkpne)t SInfeCe 440osal(complete Part A-"Monde","Sanreeis)'and"Residue]In"cdumna only)
7ti Disuribuliaot and Markcling(eom.tee ParIx A,and IS)
PRrt An; Nrd 114!
Volume ldry Fon, 1 Recipient lnformutiao
-
Soernes(x),Iinduele dxPDE5i if Voluinc
Month appNesEk] AmendrnenL. Bulking Agent Residual In Pradoct Out m(i} (dryioos) !Mended on(5)
_ 1
Dec 2I-Cant _ WQaO094T7 252.G7372 252..0172 Brent 3larrinistan 252.67372! k2
W'Q(1O09477 21416581 21td6i$d Franklin Les 28A6581
Weeo.m477 Io.l41 U Io.14oio . Lee Parrot 11).1144tk P&
-
WQOOO477 2281126$ 228.73268 Mu=liael His ' 228,33261# ag
W(p00'1477 _ '2a1.61216 201.61216 Ta4&null 201.61216 _at
WQ0n09.477 460.I56i 160.t56U4 Tony Taylor 460.1354U
'WQ,KIp3477 20.0707 2063¢72 DWid Underwood 20.07072
i
Totals, Annual(dry tons]= 0 1201.8515 1201.8515 124)1.8315
--- AOrenthocnl(sIuscd:I &MMims A$tul(Y)use.d:
•I f more spate it required,a Lath aeldiuoaal infonfi alioa Ahci s l FORM DMSDF tat ip)]: Total Numb of Form DMSDF(Sapp} S

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can he reported in FORM RSSF- B
WQ Permit Number: W 0009477 laboratory: 1) Pace Analytical Services LLC.
FacilityName: Cascades Tissue Group-North Carolina, a U4�a point Analytical
division ofascades_Holdings US Inc.
l Residual Source WQ# or [1009477 3) Summit
W
NPDE.S#: 4)
WWTP Name: 5)
Residual Analysis Data
1 Sample or Composite Date
Ceiling
Conc.
Parameter Limit 0112112.1 02/16/21 03. 18/21 04/15121 05/10/21 06/10/21 07/08/21 08112f21 09/09/21 10/07121 11/09121 12/02/21
(mpg (rrigik a
Percent Solids(%) NA 39.50 41.6 40.80 43.6 42.3 34.2 41.8 42.2 43.3 4{1-8 43.2 40,4
Arsenic 75 Not P .rmit Rccluircd
Cadmium 85 Not Permit Required
Copper 4,300 14.7 15-7 30 21-9 16.2 16.7 20-9 14.2 13,4 82.6 19, _ 13,2
Chromium NA Not Permit Required
Lead 840 Not Permit Required
Mercury 57 Not Permit Required
Molybdenum 75 Not Permit Required
Nickel 420 1,4 1-3 I.I I 1.10 1.2 1.5 1.6 0,96 I 2 1-50 1.9 3.7
Selenium 100 Not Permit Req_uired
Zinc 7,500 68,2 46,1 82.4 I 83,3 130 147 89.3 66,3 61.8 95,1 74.9 71.8
Total Phosphorus NA Not Permit Required
TKN NA 2250 1360 1340 1580 17S0 1570 1420 1730 1290 1520 1430 1460
Ammonia-Nitrogen NA 22.6 23,1 23,5 22,5 25.1 27-1 22.5 23.7 I 22.2 22.7 23,2 24.3 1
Nitrate and Nitrite NA 4,9 , 4-6 J 4.9 4_5 4.6 5.8 4_7 4.7 I 4.5 4.8 4.3 4.8
'For Surface disposal fci Li tics the ceiling concentration limits listed in this farm are not applicable. Reference the individual permit for metals limits,
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for su mitting false inform lion, including the possibility of fines and imprisonment for knowing violations."
t
Signature of Pparer Date
*Preparcr is dcfncd in 40 CFR Part 503.9(r}and 15A NCAC 2T,1102(26) DENR FORM RSSF F (12J2006)

ANNUAL.RESIDUAL SAMPLING SUMMARY FORM-B
Report ail eatnpling analysis results for parameters not listed in FORM RSSF drat are Barn Di thc WQ permit or were arudIveed fur arcer the past strode r rs ar- t.se addilioard
forms as needed,
Vs'Q Permit Number- WE-P:109477 Laboratory! fJ Pace Analytical Services,LLC
—
Facility afire Casmides Tissue Group-North Carolina a division of r ra tna Analytical
a1
Cascades kidding lPS int..
Residual Somme filiD See 3) Summer
or WQf �1 QG+p09477 4)
W WTP Name: 5)
Residual:Ana.kvsis Data
-— J — Sample or Colnpp5 ir4 Date
01+21+21 02.1i.•21 03118.2I 0411512] 05110121 ChM 0J71 0710 .21 0312.71 {Ir +21 10.1FW21 11149+21 12+241
Parameter (ingik }
Pan Cal 675 408 402 474 534 471 4.26 519 387 4,56 429 438
Aluminum Nor Permii Rewired
8b 74 64 85 86 100 52 98 120 72 96. 93
Not Permit Required
aisalenev
PH 6.8 7 7.6 7 7 10 7 6 7.9 7,8 7.8 7.3 8 8.2
Ma estarn 1420 1600 1790 1870 1810 1.900 I.680 1610 1740 E530 1830 1150
Sodium Not: Pefrrrit Rewired
Potassium Npt Permit Herluirdcl
calcium
120000 11G0000 154000 16700013 161000 189000 157000 163000. 161000. 112000 16500a II9000
Non-
Flammable
N u-0.485
mgrkg
CYanick
ND•25.0
rng1KG
Sulfide
6.8. j
Toad22 1340 1580 1780 1570 1420 1730 1290 1520 1430 1460
Nitrogen
TOC 370000 280000 3150(0 307000 322000 317000 328000 345000 3k4000 353000 301000 0
36340
Volatile Solids 637000 4 a pocio 542G00 528000 554000 544000 365000 594000 540000 60800&i 518000 625000
"1 rcerttfy,under penalty of taw,that this document was prepared under my direction or snperrision in accordance with a system dcsigecd to assure null qualified
personnel properlp gathered and ova hsaied the information submitted. I am aware#Ant there are signifi ni penalties for suhmilting false information,including the
possibility o es and impn oo ea (or fog ripiationz_"
SIgnaoi UFPreparer4 Dale
a Prepare is defined io 40 CFR Part 503.9(r)and 15 CAC 2T.1102(25}
DEUR FARM 3RSSF•ft(1202036)

�7 Pace Analytical Services,LLC
ve
a eA1 fat Analytical
` Afbi Ceigh, nce 7607
J Rareigh,NC 27807
wwu.paatiha.wm {919)D344994
February 04, 2021
Ms. Karen Bellamy
Cascades Tissue Group-NC
805 Midway goad
PO Box 578
Rockingham, NC 28380
RE: Project: SLUDGE
Pace Project No.: 92517595
Dear Ms. Bellamy_
Enclosed are the analytical results for sample(s)received by the laboratory on January 21, 2021. The results relate only to
the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicted on the sample anaryte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network.The lest report From the external subcontractor is
attached to this report iri,its entirety.
The test results provided in this final report were generated by each of the fotrowing laboratories within the Pace Network:
•Pace Analytical Services-Asheville
- Pace Analytical Services-Charlotte
if you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
tyriek.hookse pacalabs.corn
[phone]
Project Manager
Endosures
cc: Cascades Tissue Group-Rockingham,Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report nail not to repra]uced..except in MI,
without lhewniten consent of Pace Anatylical Services,LIC Paget of21

Pace Anehrtical Services,Lr,C
+��* Analytical f e701 Conference Drive
ace Analytical Rd191ga.NO 27507
'1111ny.Rac.1l a4asorl 019)834404
ANALYTICAL RESULTS
Project SLUDGE
Pace Prajecl tit}.: 92517895
Sample: SLUDGE --- Lab ID: 92517895001 Ca!leeled; 01121 1 08;05 Received: 01i21/21 11:25 Matrix; Solid
Results reported on a"dry weight"basis and are aiegirsted€orperaentmoistnre,sample size and any dilutions.
Report
Perimeters Results Units Limit MDL OF Prepared Analy2ed CAS No. Qua!
5010 MET ICP Analyllca! Method:EPA 601OD Prenercition Method:EPA 3050E
Pace Malyfical Services•Asheville
Calcium 120000 mg/kg 945 189 20 01124,2115_45 01126/21 07;42 7440-70-2
Copper 14.T mg/kg 9.5 0.47 1 01/24/2115;45 0112512115;38 7440-50-13
Magnesium 1420 mg/kg 18.9 0.47 1 01t2412115:45 0112512115:38 7439.95-4
Nickel 1.4 inglkg 0.95 0.47 1 01124/21 15.45 01 5121 15:38 7440.02-0
Zinc 68.2 mg+kg 1-9 0.95 1 01/24121 15.45 41/25I2115:18 744D-33-6
2640E Total Percent S01ids AnalyliC6I Method=2M 2640G-2011
Pace Analytical ervlpes-Charlotte
Tole!Solids 39,55 °h O. e.0004R 1 t1f21/21 17;36
Percent Ntaieture Analytical Melhod: SVV-946
Pace Art lyliCal Services-Charlotte
Percent Moist4,re 60,5 % 0-t4 o-i0 1 ta1t21 1 17:34 N2
9045 H Sail Analytical Method; EPA 9045D
Pace Analytical Services-Asheville
pH at 25 Degrees C 8.8 Std.Units 0.10 0.10 1 0.2/01121 15;20 H3
Plant Available Nitrogen Analytical McIhod: None
race Analy1i a!Services-Asheville
plant Available Nitrogen 875 mg/kg 1 42f04i21 13;49 N2
Total Nitrogen Calculation flnaNtical Mellod; TKN+1103+NO2 Calculation
Pace Analytical Services-Asheville
Nitrogen 2250 rn ?kg 40.0 20.0 1 02/04/21 13;26 7727-37-9
360,1 Ammonia Artaalyticat Method: EPA 35D.1 Rev 2.0 1993 Mod. Preparation fulelhol:EPA 350-1 Rev 2-0 1993 Mod.
Face Analytical Services-Asheville
Nitrogen,Ammonia ND mpg 22.6 22.6 1 01t28/21 11:21 01129121 09:50 7664-41-7
351-2 Total Kieldattl Nitrogen Analylical Method:EPA 351.2 Rev 2.0 1993 Preparation Method; EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Kjeldahl.Total 2250 mg/kg 127 53.3 I 02102i21 20-.19 02144/21 03-.45 7727-37-] M1.R1
353-2 Nitrogen,NO2JN03 Analytical Method:EPA353.2 Rev 2.0 1993 Preparation Method; EPA 353.2 Reit 2.0 1991
Pace Analytical Services-Asheville
Nitrogen, NO2 plus NO3 ND rng/kg 9.9 4.9 1 01122121 14;09 0U122.12f 20:21 Ml
Nitrogen, Nitrite ND rngNg 9.9 4.9 1 01l22t1 t4:09 01i2212t 20:21 14797.55.8
Nitrogen, Nitrite ND mg/kg 9.9 2.5 1 01122121 14:09 01/22/21 20:21 14197-65-0 M1
REPORT OF LABORATORY ANALYSIS
This ripen shall not be reproduces,excel]; ^full,
Data:021O4/2021 05;02 PM without the written consent of Pace Analytical Services.LLC Page 5 of 21

•
V o l nt . 7621 Whitepine Road,REchmond,VA 23237
Main 804-743-4401 a Fax [phone]
ANALYTICAL www,waypaintanaiytical.m»1
211f2021
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 213078
Ref: Analytical Testing
Report Number: 21-022-0004
Project Description: 925/17895 Sludge
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc- received samples) on 1 f22021 for the analyses presented in the following
report.
Theabove referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012)and NELAQ unless otherwise indicated.
Certain parameters(chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling- Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated- This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
t 6'67cwr
air
Pauric McGroary
Agronomist
Laboratory's liabih'ty Th any claim relating to analyses performed shall be limited fo, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refwid of the charges paid for performance of said analysis-
Page 17of21
Paco 1 of 5

. .
w
VIaypoi n 7621 White pine load, Richmond,VA 23237
Main 80-743-9401°Fax [phone]
ANALYTICAL www,waypaintanalyticul,com
11769
Pace Analytical labs Charlotte Project 92S17895 Sludge
Tynek Ft:4k5 Report Gate = 02j01/2021
9800 Kindey Ave information ' Received :01)22/2021
+luntersvilte , NC 28578 p@
1au;rFc lit Jrrior
Patric McReport Number i 21-022-0004 REPORT OF ANALYSTS Agronomist
Groary ph.l],, CPA
rarst
Lab No: 74752 Matrix: Solih
Sample ID :Sludge 9251789S001 5inipled: 1/2142021 B:0S
Test Results Units MQL OF Date iTime By Analytical
Analyzed Melhod
Moisture 60,2 ° 0.010 1 01/2E/2117.25 FMM SM-2540G
Calcium Carbonate Equivalent 31.8 °l5 0,1 1 01/27/21 16=18 DXI AOAC 955.01
C/N RATIO 85 Ratio 0 1 01/26/21 17:25 CALCULATION
Test Results Units MOL DF Date r Time By Analytical
Analyzed Method
Total Solids 39,8 94, 0.010 1 01/26)21 17;25 FMM SM-2540G
Total Volatile Solids 63,7 % 0.010 1 01/26/21 17:25 JMM SM-2540G
Total Kjeldahr Nitrogen 4300 mg/Kg-dry 623 1 01/28)21 10;30 3P3 ill-4500-NII3C-TKP
Carbon(l OC) 37.0 To 0.010 1 01/26/21 17.25 CALCULATION
Qualifiers/ pH Dilution Factor L Limit Exceeded
Definitions h1QL Method Quantitatioo Limit
Page 19 of 21
Page 3 of 5

Pace Analytical Services.1-LC
r 5709 Canferenaa drive
{ Raleigh,NC 27607
umpe[ulads.cum pig1E134-40bl
March 04, 2021
Ms. Karen Bellamy
Cascades Tissue Group-NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Proiect: SLUDGE
Pace Project Nu: 92$22414
Dear Ms. Bellamy:
Enclosed are the analytic l results for sample(s)received by the laboratory on February 16, 2021, The results relate only
to the samples included in this report.
Analyses were performed at the Pace Analytical services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network.The test report from the external subcontractor is
attached to Ihis report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
If you have any questions concerning this report. please feel free to contact me.
Sincerely,
Tyrlek Hooks
tyriek,hoc kspace labs-com
(-M4)875-9092
Project Manager
nciosiures
oc: Cascades Tissue Group-Rockingham,Divsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be repicgiuced,except in full,
without the written consent of Pace Analytlrat Services,LLG. Paget of 21

PpCq AnglytJgal 9er�rfoasr LLC
/19
Analytical 6701 Canderenco Drive
ace Raleigh,NC 276O707
YAM pcerahawm (919)a -0--0954
ANALYTICAL RESULTS
NIojeir SLUDGE
Pace ProFect No• 92522414
Sample.: SLUDGE Lab.Id: 92522414001 Collected: 02116+21 07.45 Received: 02116/2$09:42 Matrix: Solid
Results reported on a"dry weight"basis and are adjusted forperCentmolsfure,Sample site andaJiy dilrjtlons,
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. °nal
8010 MET ICP Analyllaal Method: EPA6010D Preparation Method;EPA 30506
Pace Analylleal Services-Asheville
Calcium 180000 rr,glk9 970 194 20 02/17/21 14:30 02/19121 13;05 7440-70-2
Copper 15,7 mgJkg '17 0.49 1 02117121 14:30 02118121 16:52 7440-50-6
Magnesium 1600 rrIg+4 19.4 0.49 1 02117121 14;30 02118/2116:52 7439-05-4
Nickel 1,3 mg90 0.97 0.49 1 02/17121 14:30 02+18121 1.6;52 7440-02-0
Zinc 46.1 mg+1g 1.9 0-97 1 02117/21 14:30 0211812116;52 7440-66-6
2540G Total Percent Solids Analytical Method'Siii1 2540G-2011
Pace Analytic-at Services-Crsarlolte
Tula!Solids 41-6 % 0-10 0 04001 D 1 02118/21 17:46
Percent Molsturo Analytical Method:S846
Pace Analytical Services•Charlotte
Percent Moisture 58.4 % 0.10 0.10 t 02116121 17.26 N2
9045 plf Soil Analytical Method: EPA 0045D
Pace Analytical Services•Asheville
pH at 25 Degrees C 7.0 St<J.a rills 0.10 0.10 t 03101121 15:53 H3
Plant Available Nitrogen Analytical Method: None
Pace Analytical Services-Asheville
Plan.'Available Nitrogen 498 mgtkg 1 02124/21 11:54 N2
Total Nitrogen Calculation Analylical Method:TKN+NO3+NO2 Cal0ulation
Pace Analy+1Fcal Services•Asheville
Nl1rcgen 13541 mg+kg 40.0 20.0 1 0212312115;40 7727-37-9
350-1 Ammonia Analylka!Method: EPA 350-1 Rev 2.0 1993 Mod. Preparation Method:EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services-Asheville
Nitrogen.Ammonia ND mg/kg 23.1 23.1 i 02118+21 14:01 02119121 12:48 7664.41-7
351.2 Total Kjeldahl Nitrogen Analytical Method. EPA 351.2 Rev 2-0 1993 Preparation Melhod-EPA 351,2 Rev 2.0 1993
Face Analytical Services-Asheville
Nilrogen, FCjeldahl,xotal 1386 mg+kg t08 54.7 1 02/18121 22:09 02/19121 05;15 7727-37-9
353.2 Nitrogen, N021NO3 Analytical Method:EPA 353.2 Rev 2-0 1993 Preparation Method:EPA 353.2 Rev 2,0 1993
Pace Analytical Services-A hevllle
Nitrogen-NO2 plus NO3 ND mg/kg 9.3 4.6 1 02118/21 22:57 02117121 00:27
Nitrogen. Nitrate NO rng+kg 9.3 4.6 1 02116121 22:57 02/t7/21 00:27 14797-55.8
Nitrogen. Nitrite ND 11g+kg 9.3 2.3 1 0211i' 1 22:57 02f17121 00:27 14797-65-0
REPORT OP LABORATORY ANALYSI
This report shall nat he reproduced,eccept in rill.
Dale:03104/2021 04:68 PM without the written consent al Pact Analytical Services.L LC Page 5 of 21

W Y 'Pit 7521 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°5ax 804-271-644E
ANALYTICAL www,waypokitanaIyticel.com
3f4f 0 1
Pace Analytical Labs Charlotte
Tyriek Hooks
9300 Kindey Ave
Huntersvilie, NC- 28073
Ref: Analytical Testing
Report Number: 21-056-0009
Project Description: Sludge 92522414001
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received samples) on 2125i2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method- Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 01 ) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite-..) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do riot hesitate to contact me or client services if you have any questions or need additional information,
Sincerely,
TO-WIT Pit fF arr.
Pauric McGroary
Agronomist
Laboratory's liabifrfy in any claim relating to analyses performed shall be limited to, at labborafory's option, repealing the
analysis in question ar faboralory's expense, or the refund of the charges paid tar performance of said analysis.
Page17 of 21
Page 1 of 5

w
Waypoint.
76t1 Whitepine Road.Richmond,VA23Z37
Main 804.743-9401(Ifax 804-271.6446
ANALYTICAL www.waypaintanalytical,com
).1769
Page Analytical Labs Charlotte Proyect Sludge 92522414001
Tyriek Hooks Report Date : 03/04/2021
9804 Kindel.]:Ave Information : Received : 02/25(2021
Huntersville, MC 2807E
/10ru.t pit (moat
Report Number=21-056-00D9 kt;poRTOF ANALYSIS
Pduric MC Groary Ph,1 ,, CPr�
Agronomist
Lab No : 75081 Matrix: Scads
Sample ID ; Sludge 025224140D1 Sampled: 2/L6/2021 7:45
Test Results Units MOL OF Date;Time By Analytical
Analyzed Mottled
Moisture 57,SH % 0.010 1 02/2612116:03 FMM 5M-254tI3
Callum Carbonate Equivalent 50.7 ° 0.1 1 03/01/21 13:54 DXT AOAC 955,01
CJN RATIO 74 Ratio 0 1 02/26/21 16.03 CALCULATION
Test Results Units MQL DF Date r Time By Analytical
Analyzed Method
Taal Solide 42.2 H ° 0.010 1 02/25/21 16:03 FMM SM-2540G
Total Volatile Solids 4g.1,H ° 0.010 1 02/26/21 IG;03 FMM 54.4-2S40G
Total Kjeldahl Nitrogen 3770 mg/Kg -dry 592 1 03/03/21 14;00 JPJ 411-4500•Nl 3C-TKP
Carbon(TX) 76.0 °da 0.010 1 02/2601 16:03 CALCULATION
qua Iifiars/ OF Dilution FictCr Ft Beyond holding time
Definitions L Limit Exceeded htQL Method Quantitation Limit
Page 19of21
Page 3 oL 5

Pace Analytical Services,LLC
• 6707 C Rakich,
NC Dfiv7
tir2eAnaligical Rakiph,NC 27607
•
WWW.pacoli ,tnm (919}a3344981
April 12, 2021
Ms- Karen Bellamy
Cascades Tissue Group-NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: MONTHLY TESTING
(Race Protect No.: 92528470
Dear Ms. Bellamy_
Enclosed are the analytical results Forsarnple(s) received by the laboratory on March 18. 202t. The results relate only to
life samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated lay each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asher/ilia
• Pace Analytical Services-Charlotte
Revision 1 -This report replaces the April 1-2021 report.This report was reissued on April 12, 2021 to include Ammonia
per client's request.
IF you have any questions concerning this repot, please feel free to contact me.
Sincerely,
�.z /�.-
Tyriek Hooks
tyriek.hoo kse pacelats.corn
[phone]
Project Manager
Enclosures
pc! Cascades Tissue Group-Rockingham, Divsion of
REPORT OF LABORATORY ANALYSIS
This report shall not IA rep.VelktMi.o tept ih fule,
without the written oonsoht OF Pate Analytical$exicea,LLC. Pege I of 19

Pace Analytical 9er lcea,LLC
aceilinalytical
$rot Came.NC. Drive
Raleigh-N 27601
,rw.pace9eh�.com {1319)834-4984
(7,9
CERTIFICATIONS
Fiiject; MONTHLY TESTING
Pace Protect No.: 92528470
Paco Analytical Services Charlotte
9800 Kincey Ave.Ste IGO, Huntersville,NC 2607S South Carolina Certification#:99006001
LOuisiana+NELAP Certification#LA170028 Florid&&NELAP Certification#:E7627
North Carolina Drinking Water Certificalion#:37706 Kerrlucky LIST Cergllcelioii#:84
North Carolina Field Services Certificalion#;5342 Virginia FLAP Certification#.460221
North Carolina WaSlewater Certification#: 12
Pace Analytical Services Asheville
2225 Riverside Drive,AshewiEle, NC 298[)4 North Carolina WaSlawater Certification#:40
.FlOri{la1Ni EAP Certification#:r=87844 South Carolina Certification 9Q3t]001
forth Carolina Drinking Winder Certification#:37712 v gInla+VELAP Certification#:460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in lull,
witout the wrillerl tonseni oA Pace Anelylica+Serviaem,LLC. Page 2 of 19

Pace Analyikal SerVICVS,1.1-C
Drace Analytical 6701 Conference 7607
! Raleigh,NC 27607
�' wwrr,aaas,tom
P1$)4334•1954
ANALYTICAL RESULTS
Project, MONTHLY TESTING
Pace Project No.: 92528470
Sample: CASCADES SLUDGE LeO ID: 92528470130T ollecied: 031 8/21 08:20 ReCeived: W118[21 f19'30 Matrix: Solid
SAMPLE
Restrtts reported our a"dry weight"'Plasm and are 8dy{1Srod for percent mei5fure, saitrp+a sire aid any dilutions.
Report
Parameters Resulls Units Lirrlil tM1DL OF Prepared Arialy;ed CAS Na. Qua!
5019 MET ICP Analytical Method; EPA 601DD Preparation Method: EPA 3050E
Pace Analytical Services-Asheville
Calcium 154000 mg/kg 956 191 20 03/22/2112:20 03/25/21 08:39 7440-70-2
Copper 30-0 mgrkg 9.6 0 48 1 03i22/21 12:20 C13024121 11:06 7440-50-8
Magnesium 1790 rng+kg 19.1 0.48 1 03+2212112:20 03+24121 11:06 7439-9554
Nickel 1.1 ingrkg 0.96 0 48 1 03122T21 12:20 02024121 11:06 7440.02-0
Zinc 82.4 rngikg 1.9 0.96 1 03122121 12:20 03124/21 11:05 7440-66 6
2540G Total Percent Solids Analytical Method:SM 2540G-2011
Pace Analytical Services-Cha k:111e
Total.S Iads 40.B 3ia 0.10 0.000010 1 03119W21 15:16
Pereerlt Moisture Analyticlal Method: S -846
Pace Analytical Servlcas-Charlotte
l=ercenl Moisture 59,2 $'a 0 ID 0.10 1 03/19/21 15;07 N2
9046 pH Soil Arsalytical Method: EPA 90450.
Pace Analytical Services-Asheville
pH at 25 Degrees C 7,6 Std. Units 0.TO 9.10 1 03i29W21 to:48 Hi
Plant Available Nitrogen Ariatytical Method: None
Pace Analytical Services-Asheville
Plant Available Nitrcygers 402 mg+kg 1 04101109;50 N2
Total Nitrogen Calculation Analytical.Method: TKN+NO3-1-NO2 Calculation
Pace Analytical Services-Asheville
Nitrogen 1340 mglkg 40.0 20.0 1 03/30/21 15;10 77V-37-9
359.1 Ammonia Analytical Method:EPA 350.1 Rev 2.0 1993 Mod. Preparation Method:EPA 350,1 Rehr 2,0 1993 Mad-
Pace Analytical Services•Asheville
Nitrogen,Ammonia ND mg/kg 23-5 23.5 1 03l22i2t O7•:33 03122121 11.58 7664-41.7
351.2 Total Kjetdahl Nitrogen Analytical Method-EPA351 2 Rev 2.0 1992 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analyllcal 3erviOeS-Asheville
Nitrogen,Kleldahl,Total 1340 mg/kg 117 55.3 t 03129f21 Z0;29 03+30121 Q7:55 7727-37-9 M1.R1
363,2 Nitrogen, NO2+NO3 AnalylicaI Method:EPA 353.2 Rev 2.4 1993 Praparaltoo Method:EPA 253.2 Rev 2-0 1993
Paco Analytical Services-Asheville
Nitrogen,I402 plus NO3 NIA mg+kg 9.8 4.9 1 0311841 22:25 03/19/21 00:22
Nitrogen,Nitrate ND rng+kg 9.8 4.9 I 03/18J21 22:20 02i19+21 00:22 14797-555-8
Nitrogen,Nltrite ND mg/kg 9.8 2.4 1 03/15/21 22:28 03/19121 00;22 14797-65-0
REPORT DF LABORATORY ANALYSIS
This report shalt not to rRprpduCed.except In full,
Date:04+12t2021 02:41 PM vnthout the written consent of P CeAnalybesl Services,ILC Page 5 of 19

•
Waypoi t . 76,21.W hire ptne ROadr Richmond,VA 23237
Main 804-743- 401°Fax [phone]
ANALYTICAL www.waypointanaIytital,cam
3/31/2021
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
F-lunte rsvi l l e. NC, 2807 8
Ref, Analytical Testing
Report Number: 1-0E2-0007
Project Description: Cascades Sludge Sample
9 5 8470001
Dear Tyriek Hooks;
Waypoint Analytical Virginia, Inc, received sample(s) on 3f23/2021 for the analyses presented in the following
report
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chllorine, pH, dissolved oxygen, sulfite_..) are required to be analyzed within 16 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included Jr) this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely.
Fc f loam.
Paunc McGroary
Agronomist
Laboratory's liability in any claim relating to analyses perforrnect shall be limited ro, at laboratory's option, repeating The
QFPa1ysis in question ar laboratory's axperrse, or the refund of the charges paid for performance of said analysis.
Page 15 or 18
Page 1 'V C

Waypoi n 7621 Whitepine Road.Richmond, VA 23237
Main 804-743.9401°Fax 804-2 7 t-6446
ANALYTICAL www,t+eaypointanalyticaI.torn
Samp'e Sumrnary Table
Report Number: 21-082-0007
Client Project Description: Cascades Sludge Sample
925213470001
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
75555 Cascades sludge sample-925284700431 Solids 03/18/21:i2t OB:26 03/2312021
75SS5 Cascades sludge sample 52.84700C1 Solids 03/18/202t 08;20 0312322021 SM-2544G WP MTN
75555 Cascades sludge sample-92528470i101 Solids 03/18/2021 06=20 03/23/2021 5M-4500`Nti3C-TIKN WP MTN
75555 Cascades sludge sample-92528470001 Solids 03/18/2021 08:20 03/23/2021 AOAC 955.01 Arp MTN
WP MTN -Memphis, TN: Waypoint Anaiyeieal-TN, Memphisr TN
Page 16 of 19
Page 2 of 5

w
Waypoint.
7621 111l17ftepine Road,RiCl1m4nd,VA 23217
Main 8114-743.9401°5ax 804-271-6446
ANALYTICAL www.waypofntanafytical.cam
11769
Race Analytical Labs Charlotte Project CascadeS Sludge Sample
Tyriefc Flasks Report Date: 03/31/2021
9804 KIridey Ave ]nformaborr : 92522470001 Received : 03/2312021
Huntersuille , NC 28078 q
1ter,z 1111C 6ri9oe -
R R7 F ANALYSIS
PauriC MC Groan/Ph-D-.CPP
Report Number:21-b87-OOOJ Agronomist
Lab NO: 75555 Matrix: Solids
Sample ID :Cascades sludge saniple-9252847O001 Sampled: 3/18/2021 6:20
Carbon (TOC) 3L.5 % 0.01E 1 03124/21 16;30
Test Results Units MQL OF Dater Time Ry Ana IyrIical
Analyzed Method
Total Solids 41.0 % 0.01E 1 0304/21 16:30 FMM SM-2540G
Total Xielciall Nitrogen 4900 mg/Kg-dry 610 1 03/26/21 15:30 3131 lM-4500-NH3C-TKP
Calcium Carbonate Equivalent 43.7 °A 0.1 1 03/31/21 09152 DXT AOAC 95S-01
Total Volatile Sothis 54.2 % 0-010 1 03124/21 16;30 1MM SM-2540G
CAI RATIO 64 Ratio 0 1 03124f21 16=30 CALCULATION
Analytical Method: SF!-2590C+
TesI naski l is Units MOL DF Date I Time Sy Anglyticai
Analyzed Batch
Moisture 59,E °AO 0,010 1 D304/2L 16:30 I Mt1 L5,3390
Quaiitiers/ DF Dilution Factor MQL Method QudMItatlen Limit
Definitions
Page 17 of 19
Page 3 of 5

7l*p}��7 f +!� Pico Analytical.Serrlces,LLC
aceA alytal# $701 f.';On r nC Drive
7
R�Ieigh NC Q3a43
wmcpaeelabLco a f9t9}B34-4984
April 29, 2021
Ms. Karen Bellamy
Cascades Tissue Group-NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: CASCADES SLUDGE
Pace Project No.: 92533553
Dear Ms Bellamy:
Enclosed are the analytical results for sample(s)received by the Jeboratory on Apnl 15, 2021. The results relate only to the
samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated en the sample anatyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network.The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated try each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
•Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel Free to contact me.
Sincerely,
/-i ,94 -
Tyriek Hooks
tyriek.hocks(i paoelabs.corn
I;704}975-9092
Project Manager
Enclosures
cc: Cascades TiiSSue Group-Rockingham.Dlvsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
TTa:reperi ehall not be reproduced,excem4+n FBI.
without IMewritten cnraeent cr Rem Snalyticel Services,LLC. Page 9 or i9

aceAnalytical ?ace Anakyticel Ser k.as,LIC
8701oroe Vrive
RAleigh. MOT
www. +4s,com (919)8344984
CERTIFICATIONS
Project. CASCADES SLUDGE
Pace Project No.: 92533553
Pace Analytical ServieeS Charlotte
9900 Kincey Ave.Ste 14U,-funtersville,NC 26078 South Carolina Certification#:99006041
Louisiana&NELAP Certification#LA170028 FlonclafNELAP Certihcation# E87627
North Carolina Drinking 4Wee Certircatior3#:377D5 Kentucky UST Cerlifrc9tian#;$4
North Caroline Field Servipes Ceriiflcallorti Or:5342 WginiaNELAP Certiticatigrr#_4f3tl221
North Carolina Wastewater Certificalloi #: 12
Paco Analytical Servlccrs Asheville
2225 Riverside Drive,Asheville,NG 26804 North Carolina Wastewater Gertificalion#; 44
Floricla!NELAP Certification i E87648 Saulh Carolina Certification#-99030041
North Carolina Drinking 1N9ter CerlifiC2kion#:37712 WginiaNELAP CerEificaljom#_460222
•
REPORT OF LABORATORY ANALYSIS
This report shac nc4IA reproducecl.except in kill.
without the written consent of Pace Analytical 8anoices,LLC. Page 2 of 19

++��'}'�Q��17}'�+�rf +f��]rf Paco Analytical Services,LLC
a+c J Ina/yt c l 1 ales tAf0YIG4 Drive
Raleigh.NC 27847
www,paal/Gacwe 4 (919)834-i98.4
SAMPLE SUMMARY
Project: CASCADES SLUDGE
Pa0e Pfppect No.: 92533553
Lab ID Sample ID MatrJx Data Collected Date Received
92531153001 CASACADl=S SLUDGE SAMPLE SOlod 44i15/21 09:30 04115121 70;15
REPORT OF LABORATORY ANALYSIS
Phis repoi anal!not be repredudai,extept in full.
u riout the written consent ei Pace AnalvrnaI Services,LLC. Page 3 of 19

e.
/11, + �'+❑f��7�} / /'+ Pace Analytical Serefcea,LLC
Qca rV al heal $749 Conference NC 7607
Raleigh.NC 27fi07
www.parelabt.rom 019)636-4994
ANALYTICAL RESULTS
PKojeol: CASCADES SLUDGE
Pace Project No.: 92533553
Sample: CASACADES SLUDGE Lab ID: 92533553001 Collected; 04115/21 08.39 Received: 041155/21 10:16 Matrix: Solid
SAMPLE
Results reported on a"dry weight"basis and are adjusted for percent moisture,sample size and any diiertions,
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8010 MET ICP ArtiatyliceI Method:EPA6010D Preparation Method:EPA 3050E1
Pare Analylkcal Services-Asheville
Calcium 197050 rrxgtkg 939 188 20 04129/21 12;51 04/23121 14;04 7440-70-2
Copper 21-9 rngikg 9.4 0.47 1 0412012112;51 04/22121 04;33 7440-50-3
Magnesium 1870 mgiky 18.8 0.47 1 04+20121 12;51 04/22/24 04;33 7439-95-4
Nickel 1-1 mg1k9 0.94 0.47 1 0412012112;51 0 12212104;33 7440-02-0
Zinc 83-3 Mpg t.0 0.94 1 04/20121 12:51 0412212104;33 7440-86-6
2540G Total Percent Solids Analytical Mempd: SM 2540G-2011
Pace AnaFylcel Services-Charlotte
Total Solids 43.6 96 0.10 0.090010 1 04/16121 13:58
P ercent Moisture, Analytical Method;SW-846
Pace An&Ily1ica1 Services-Charlene
Percent Moisture 56.4 % 0.10 p-1p 1 04116121 13:52 N2
9045 pH Soil Analytical Method:EPA 90450
Pace Analytical Services-Asheville
pH at 25 Degrees C 7.0 Sid-Units 0.10 0 10 1 C14127121 16:53 H3
P lant Available Nitrogen Analytical Method:None
Pace Analytical Services-ASheville
Plant AvaltaWa Nitrogen 474 mgikg 1 04/21/2115.26 N2
Total Nitrogen Calculation Analytical Method:TKN•NO3+NO2 Calculation
Pace Analytical Services•Asheville
Nitrogen 1580 ntglkg 40-0 20.0 1 04121121 14:54 7727-37-9
360.1 Ammonia Analytical Method:EPA359.1 Rev 2.0 1993 mod. Preparation Method:EPA350-1 Rev 2.0 1993 Mod.
Pace Analytical Services-Asheville
Nitrogen.Ammonia NO mike 22 5 22.5 1 04118/21 14:19 04/19121 16:06 786441.7
331,2 Total Kleldahl Nitrogen Analytical Method:EPA$51.2 Rev 2.0 1993 Preparation Method;EPA 351.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, jeldall,Total 1580 mpg 115 57.3 1 0419/21 19:27 04121/21 01;32 7727-37-9
353.2 Nitrogen,NO21NO3 Analyticak Method_EPA 353.2 Rev 2.0 1993 Preparation Method;EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,NO2 plus NO3 ND rrrgrkg 9.0 4.5 1 04/15/21 22:98 04/16121 00:12
Nitrogen,Nilrate ND rnglkg 9.0 4.5 1 04/15121 22:08 04116121 00:12 14797.55.8
Nitrogen,Nitrite ND rn lkg 9.0 2.3 1 04/15121 22:08 04115121 00:12 14797-55-0
REPORT OF LABORATORY ANALYSIS
This report shall not he.reproduced.egeept in lull.
Date: 04,29 02104.44PM without the wrilte«ar en1UPa4:eAnaIytieslServes,LLC Pap 5o[1S

•
W y I lit 7621 4Vhitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www-waypoirrtanaiyt1CaLrom
4/28/2021
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersvilie, NC, 28078
Ref, Analytical Testing
Report Number: 21-110-0018
Project Description: Cascades Sludge Sample
92533663
Dear Tyriek Hooks_
+ aypoint Analytical Virginia, Inc, received sample(s) on 41201202/1 for the analyses presented in the following
report,
The above referenced project has been analyzed per your instructions_ The analyses were performed in
accordance with the applicable analytical method_ Sub-contracted testing is noted on the Sample Summary Table
if applicable_
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012)and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite,,.),are required to be analyzed within 16 minutes of
sampling. Usually, hut not always, any field parameter analyzed at the laboratory is outside of this holding time,
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s), Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shalt not be reproduced except in full and relates only to
the samples included in this report
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
; ,'c Plc foam
Pauric McGroary
Agronomist
Laboratory's liat iity rn any claim relating to analyses performed straw be limited to, al laboratory's option, repealing the
analysis in question al laboratory's expense, or Me re4and of the charges paid for pefforrnarrce of said analysis.
Page 16of19
Page 1 of 4

W
W Y i 7621 K t#tepine road,Richmond,VA 23237
Main 844-743-94101 6 Fax 804-271•6446
ANALYTICAL www,waypointanalytical_com
11769
Pace Analytical Lags Charlotte Project Cascades Sludge Sample
Tyriek kooks Report Date : D4/28/2D21
9900 Klndey Ave Information : 92533553 Received ; 04120/2021
Hunters:Ale , NC 280'76
fx4m{ P14 ('from
'Report Number;2L-EL0-0016 REPORT OF ANAL Y51 Pauric Mc Groary Ph.D.,CPA
Agronomist
Lab No : 75937 Matrix; Solids
Sample. [U _Cascades-92533553 Sampled; 4/1S/2021 8130
Test Results Units MCA. DF Date lTime By Analylicel
Analyzed Method
Total Solids 44.7 % 0,010 I 04/21/21 16:01 FMM SM-2540G
Total Kjeldahl Nitrogen 3600 mg/Kg -dry 559 1 04J23/21 11;00 3PJ M 500-NH3C-TKP
Calcium Carbonate Equivalent 66.1 % 0.1 1 04/26/21 13:00 DXT AOAC 955,01
Total Volatile Solids 52,8 % 0.010 1 04/21/2116;01 FF4M 5M-2540G
C/N RATIO 85 Ratrc 0 1 04/21/21 16:01 CALCULATION
Test Results Units MQt bp Elate f Tlrne By Analytical
Analyzed Method
Carbon(TQC) 30,7 'Ye 0,010 1 04/21121 16:01 CALCULATION
Analytical Method; 5M-2540G
Test Results Units MOIL OP Date I Time By Analytical
Analyzed Batch
Moisture 55.3 % 0.010 1 04/21/21 16:01 F#-1M L548582
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
F}acge i8of 19
page 3 of 4

Paco Ana lylkcal Servlcas,Li0
ace Analytical 6703 ronoo Drive
Raleigh.t4C 27eo7
••
rrwrr.paea ihs.r am ($18)984-1 111
May 27, 2021
Ms, Karen Bellamy
Cascades Tissue Group-NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project- SLUDGE
Pace Project No.: 92538151
Dear Ms- Bellamy:
Enclosed are the analytical results forsarnple(s) received by the laboratory on May 11.2021, The results relate onty to the
samples included in this report.
Analyses were performed et the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network.The test report from the external subcontractor is
attached to this report in its entirety,
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
•Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free Io contact me.
Sincerely,
o a�. s 1 �Y9i� -
Tyriek Hooks
tyriek.hooks pacelabs.corn
[phone]
Project Manager
Enciosures
cc: Cascades Tissue Group-Rocidngfearre,DivsIon of
Cascades Holding US Fr c
REPORT Of LABORATORY ANALYSIS
This report shall not be reproduced-except in fur,
without the wntten consent of Pace Anblylia S siCeS.I.l. . Page 1 of 21

Pace Analytical Services,LLG
{+G}�f7 1+�7 # 87131 Conference Drive
aceAnalit ai Raleigh,tJC276a7
aew.patriabvron (919)834.4ga/
III
CERTIFICATIONS
Project: SLUDGE
Pace Protect No.: 92538151
Pace Analytical Services Charlotte
9800 Kincey Ave.Ste 100, Huntersville,NC 28075 Soutti Carolina Certification#:9941-,6001
Lauisiana+NE LAP Certification#LA170428 FlOtiCialiNELAP Certification#:E87627
North Carolina Drinking Water Certification#-37706 Kentitay UST Certification#: 54
Norlh Carolina field Services Cerlifitaiion#: 5342 VIrginiaNl=LAP Certification#:46022t
North C oiirrd Wastewater Cectificailon#: 12
Pace Analytical S-ery Ices Asheville
2225 Riverside Drive,Asheville, NC 2881:I4 North Carolina Waste.vater COrtificellen Jx:40
FloridalNELAP Certification#:E87648 South Carolina Certifi lion#: 99430041
North Carolina Drinkifpg Water Certification#: 7712 VtrglnlaNELAP Certification#:460222
REPORT OF LABORATORY ANALYSIS
This re)t e1 shell not to repredre sd,except in full,
without Ni.e.wilier)consent of Pace Analytical Services,LLC. Page 2 of 21

Paco AnsiytFcalSarvlcee,LLC
• 6701 COnfw Ce Ofi
c❑A alyti a/ Rh e NC MOT
woNLpitembs.tom { 131,53-4-4934
SAMPLE SUMMARY
PrOject; SLUDGE
Pace Pfojeci Na.: 9253915$
Lab ID Sample ID Matrix Data Collected Date Received
92638151OO1 SLUDGE Solid 05/10/210730 05111/211020
REPORT OF LABORATORY ANALYSIS
This rr3ryort stiwtl not be reproduced,except in fu:i,
w dh65n the wri1te n eonsend of Pace Anelytecal Services.LLC Page 3 or 21

ace
r}�+� Pace ArtalytIcal yervlces,LLC
ace na is l A741 Ceigh, C 7607
Ra6eigh,N�2#b4#
wniw.pueerabs,cam (919}934-4964
ANALYTICAL RESULTS
Project SLUDGE
Pace PrajeCt NO.: 925313151
Sample; SLUDGE Lab ID; 92538151081 Canted! 0, 10/21 07:30 Received: 05111l21 10:29 Matrix: SOliO
Results repor-fed on a "dry weight-495rs ana are acOusled far percent irroistura,samphi size and any dilutions,
Report
Parameters Results units Limit MDL DF Prepared Analyzed GAS NO. Qua'
6010 MET ICP Analytical Method: EPA 60100 Preparation Method;EPA 30546.
Pace Ar►elyllcal Services-Asheville
Calciurrr 181000 mgikg 909 182 20 05112/21 15;52 05/15/21 19:09 7440-70-2
Copper 16.2 mgikg 9.1 0.45 1 05//2121 15;52 05114121 23:D4 7440 50-8
Magr3esium 16t9 mgikg 18.2 0.45 1 0511312115:52 05114/2123:04 7439-95-4
Nickel 1.2 mgikg 0.91 0.45 1 05/12 1 15;52 05114121 23:04 7440-02-0
Zinc 130 mgikg 1.8 0.91 1 05112121 15:52 05/14121 23:04 7440-55--6
2540G Total Percent Solids Analytical Method:SM 2540G•2011
Pace Analylical Services-Charloiie
Total Solids 42,3 % 0,10 9,000010 t 0,511121 17:33
Percent MoiSture Analytical Me1h00,SW-640
PaOe Analytical Services-Charlotte
Percent Moisture 57-7 % 0.1D 0.10 1 45f11121 t7;22 N2
8045 pH Soil Analytical MetI Ord:EPA 9045D
Pace Arlalytlpl Services-Asheville
pH at 25 degrees C 7.1 Std. Units 0.10 0.19 1 05r24t21 16:02 H3
Plant Available Nitrogen Analytical Method:None
Pace Analytical'Services•Asheville
Plant Available Nitrogen 534 rngikg 1 05127/21 15:36 N2
Total I ttrOgen CalOtildtlon Analytical Method;Tl +NO3+NO2 Calculation
Pace Analytical Services-Asheville
Nitrogen 1780 mg+kg 4D,0 20.0 1 05/2012114:53 7727.37.9
354.1 Ammonia Analy itcal Method:EPA 350-1 Rev 2-4 19g3 Mod. Preparation Metho f:EPA 350.1 Rev 2.0199$Mod.
Pace AnalyticaF Services-Asheville
Nitrogen,Ar irionia ND mgikg 25.1 25.1 1 05i27/21 09:15 05127121 15:00 7004-41-7
351,2 Total tijeldahl Nitrogen Analytical Method:EPA 351.2 Rev 2-0 1993 Preparation Method:EPA 351-2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen.KielrIahl. Total 1780 mgikg 113 56 3 1 05i19121 20:44 O 20,+2t 04:59 7727-37.9
353.2 Nitrogen,NO2+NO3 Analytical Method:EPA 353.2 Rev 2.0 1993 Preparation Method:EPA 353.2 Rev 2.0 1993
Pace Analytical Servi0e5-Asheville
Nitrogen NO2 plus NO3 ND rrtgikg 9.2 4.6 1 05f11121 22;25 0519.2121 D4:12 R1
Nitrogen,Nitrate ND mg/kg 9.2 4.6 1 O511t1/21 22:26 05/12121 04:12 147$7-55-9
Nitrogen,Nllrlle ND rngag 9.2 2.a 1 05/11/21 22:26 0512121 94;12 14797-65-D M1,R1
REPORT OF LABORATORY ANALYSIS
Trig rapes Shall NIL De reproaucea,esocepl in full,
Date:05127/2021 D4:59 PM mahaul 1htwriPlen consent of PsceRnslyrliael Services.LLC. Page 5 of 21

• 1,5)
VVhihepiniii
+� h■ p� Road,
��rypry�y 1y �y�yf
Waypoint . � ��'I Main 80 743-�WV 1 Richmond,°Fax 5O4-2f 14 446
ANALYTICAL www.waypalntanalytical-cam
512412021
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersvilie, NC, 28078
Ref_ Analytical Testing
Report Number 21433-0008
Project Description: 92538151
Dear Tyriek Hooks_
Waypoint Analytical Virginia, Inc. received samole(s)on 5/13/20 1 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the UEFA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of
sampling_ Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
T4 c Grlo ary
Fauna Mcroary
Agronomist
Laboratory's liability on any claim:Waring to analyses performed shall be"United to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for rperformance of said analysis.
gage 17if21
Page x of 5

w
Waypoi t 7621 W hitepine Road,RithinOnid,VA 23237
Merin 8001-7413.-90101°Fart 804•271-64140
ANALYTICAL www-waypoiritanalytical.COni
Samp€e Summary Table
Report Number: 21-133-0008
Client Project Description; 92538151
--
Lab No Client Sample Id Matrix Date CoUJected Date Received Method Lab ID
76327 925381.51-sludge Solids p5}10{202107;36 05/13/2021
76327 92538151-sludge Solids 05}10i2021 07;30 OS}13/2021 SM-2S4OG WP MTN
76327 92538151-sludge 5did* 05/100O21 07:30 05/13/2021 5M-4500-NI!3C-TKN WP MTN
76327 92538151-sludge Solids 05/10}2021 07=30 05/1312021 AOAC 955.01 Nap MTN
WP MTN - htemphis,TN; Waypolnt Analytical-TN,Memphis,Thl
Page 18 of 21
Pale 2 of 5

w
W yi:t I nt 4 7621 Whltepino Road,Richmond,VA 23237
Main 804-74 3-9401°Fa K 804 271-644S
ANALYTICAL www.waypointanalytical.com
11769
Race Analytical Labs Charlotte Project 92538151
Tydek Books Report Date : 05/21/2021
9800 Kindel+Ave InfarmatlOn : Received : 05/13/2021
Hunters�itle , NC 28478 ,�r
Taw'c e+ra d
Report Number ;21-133-0008 REPORT OANAL ANALYSIS Paurie Mc Graary Ph.D.,CPP
F
Agronomist
Lab No ; 76327 Mettrx: Solidi
Sample ID:925B8151-Mudge Sampled; 5/10/2021 7:30
Test r3esulls Units FOOL, OF Date.,Time By Analytical
Analyzed Method
Total Solids 43.2 % 0.010 ] 05117121 16:11 FMM SM-2540G
Total Kjeldahl NitrOge1 3750 mg/Kg-dry 579 1 05/19/21 10:00 JP] ;M-4500-NH3C-TKP
Calcium Carbonate Equivalent 40.7 5b 0.1 1 05/20/21 14:53 MT AOAC 955.01
Total Volatile Solids 55.4 % 0.010 1 05/17/21 16:11 FMM 5M-2510G
C/Fl RATIO 86 Ratio 4 1 0511712A 15:11 CALCULATION
Teat Results Units MOL DF Dalai Time By Analytical
Analyzed Method
Carbon(TOC) 32.2 % 0.014 1 05117/21 16:11 CALCULATION
Analytical Method: 5M-2540G
Teel Resufls Unite MOIL DF Dale r Time By AnaEytFcal
Analyzed Batch
Moisture 56.8 ° 0.010 1 05117/21 16:11 FMM L55348.2
Qualifiers/ 13t. Dili Alan Factor MQL Method Qua ntitation Limit
befinittons
Page 19 of 21
Page 3 of 5

•
Pace Analytical Serviced,LLG
f+O YI4{ �++�f K 5707 Cofllerenoe drioe
ceA a/yUc�[! Rdleigh,NO 27507
wymeaCeP in.c0A1 (919)V4,4991
June 25, 2021
Ms. Karen Bellamy
Cascades Tissue Group-NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE Project: CASCADES SLUDGE SAMPLE
Pace Project No.: 92543726
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on June 10. 2021 The results relate only to the
samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyze page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network.The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
•Pace An alytrcal Services-Asheville
•Pace Analytical Services- Charlotte
If you have any questions concerning this report.please feel free to contact me.
Sincerely,
Tyriek Hooks
tyriek.hoeksi pacelabs,com
(704)875-909 2
Project Manager
Enclosures
Ca. Cascades Tissue Group-Rockingham,Diwsian of
Cascades Holding.US Inc.
REPORT OF LABORATORY ANALYSIS
Thie report shd6 not tx reproduced,except in full.
wnhoirt the written ccns'CM{Of Pace Analytical Services.LLC Page 1 of 20

Pao].Analytical SemiDee.LW
7112eAnaVical $701 COigh,N e DIM?
Raleigh,NC 27$07
xwcpaealates.cen (9 1 918 34-4 9a1
CERTIFICATIONS
Project: CASCADES SLUDGE SAMPLE
Pace Project NO.: g2543726
Pace AnalytiC.al Services Charlotte
9600 Kincey Ave.ate 100. Huntarsvllle,tiC 26078 South Carolina Certification#: 99006001
LouisianelNELAP Certification#LA170026 Florida+N FLAP Certification#:S67827
North Carolina Drinking Mier Cerlificalion it:37706 Kentucky U57 CerlifiCetion#:$+4
Nar1h Carolina Field Services Cerli6calton : 5342 Vim in& FLAP Certillptlon#:460221
North Carolina Wastewater erl4fiiceltOn e: 12
Paco Aaalytkal Services Asheville
2225 Riverside Drive_Asheville,NC 28804 North Carolina'Aastewater Certification
FlorigaiN EJAP Carltflcallan#-E67648 South Carolina Certification#;99030001
North Carolina Driniekkg Water Certification#;37712 VirginiaNELAP Certification at:460222
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced,except in full.
wi1hcu1 ihewriben consent of Pace AnaIYticdl gennrea.LLC. Page 2 of 20

Pape Analytical Services,LLC
��++ 6701 Confanaaxs Drive
a eA / f l Raleigh,NC 27007
kw•tpieelsbEtam (919}8 4-49&1
SAMPLE SUMMARY
Prated: CASCADES SLUDGE SAMPLE
Pace Protect No.: 925437213
Lab IC Sample ID Ph trlx Date Collected Date Received
92543726041 CASCADES SLUDGE SAMPLE Solid d6f1Q121 09,35 06110121 I;:05
REPORT OF LABORATORY ANALYSIS
rhos:port shall avat bo vpqucerl.except in folk,
wthi ur the.brkiten consent of Pgige Ana!pica!Seaviaes,LLC. Paige of 20

+��+ r�+� *+�f Pace Analytical Services,LiG
€7V eAf fA/ ice 6701 C{}rierrac Drive
71! Raleayh.NC 27807
www.psealalmtam (919)ii?,4-49 4
I
ANALYTICAL RESULTS
Prpf ea(' CASCADES SLUDGE SAMPLE
Pace Project Ne.: 92543726
Sample= -
CASCADES SLUDGE Lab ID: 92543726001 Colleeled: 06110l21 013;35 Received. 06110121 11:05 Matrix: Solid
SAMPLE
Resins reported on a"try weight"basis and are?Crust eor percent morslrrre,sample sire and'any dilutions,
Report
Parameters Results Units Lirnit MDL DF Prepaied Analyzed CAS No. Qua1
6O10 MET 1GP Analyilcai Melod:EPA B010D Preparation Method: EPA 3450E
Pace Analytical Services•Asheville
Calchurn 188440 rnglkg 580 116 10 0512212116:47 06124121 17-12 7440-70-2 M1
Copper 15.7 mgrlsg 11 6 0.5a rt 06122r2118:47 06124121 00:30 7440-50-9
Magnesium 1900 mgikg 23-2 0.58 1 06.r22i21 16;47 06124/21 00:30 7439-95-4
Nickel 1,5 mg/kg 1.2 0.59 1 06122121 16;47 06124/21 00:34 744 -O2-0
Zinc 147 mgikg 2.3 1.2 1 D6/22i21 16:47 06)24121 00:30 7440•66.6 M1
2540G Total Percent Solids Analytical Method: SM 2540G-2011
Pace Analytical Services-Charlotte
Total Solids 34.2 % 0.10 O.ODD010 1 08110121
Perpgnt MOleturf Analytical Method:SW-446
Pace Arlalyti{:al Sei vi es-Charlotte
Percent Moisture 65.9 %' 0.10 0-10 1 Gel0W21 17;32 N2
9045 PH sou ArialyIlcai Method:EPA 9045 D
Pace Anaty lcal Ser,eloes-Asheville
pH at 25 Degrees C 7,6 Sid. Units 0.10 0,10 1 1121 14:35 H3
Plant Avallabfle NItrogert Analytical Method•None
Pace Analytical Serviaes-ASheviile
Plant Available Nitrogen .471 mg/kg 1 96122)21 15:22 t12
Total Nitrogen Calculation Analytical f�letttiod-71CN+Na3+NO2 Calculation
Pace Analytic-at Services•AshewiNe
Nitrogen 1570 mg/kg 40.0 20.0 1 06115)2114:30 7721-37-g
350.1 Ammonia Analytical Method-EPA 350,1 Rev 2.0 193loots. Preparation Method:EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services.•Asheville
Nitrogen,Ammonia ND mgikg 27.1 27.1 1 06/16121 13;34 06/16121 16;18 7664-41-7
351-2 Total Not/Jail!Nitration Analytical Metftod:EPA 351.2 Rev 2.0 1993 Preparation Method; EPA 351.2 Rev 2,0 1993
Pace ACralytiC9t Sen+lces-Asheville
Nitrogen, Kleloahl.Total 1570 rrlgrkg 13$ 69.5 t 06114121 t8:56 05115121 07;14 7727.37.9
353-2 Nitrogen,NO2iNO3 Analytical Method:EPA 353.2 Rev 2.0 1993 Preparation Method,EPA 35.3.2 Rev 2.0 1993
PaceAnatytical Services•Asheville
Nitr ger1,NO2 plus NO3 ND mg/kg 11.5 5.8 t 06)10121 22:54 D8111121 0D:36
Nitrogen,Nitrate ND mg/kg 11.5 5.8 1 06)19121 22:54 06/11121 00:39 t4797-55-8
Nitrogen,Nitrite NCI mgikg 11.5 2.9 1 06)10121 22;54 06111121 00:39 14797-65-0
REPORT OF LABORATORY ANALYSES
Tl's report shall not be reprndueerl.except in cull.
[tale: 16i251'42t O7'd9 PM withovllha xnilaon cor'3e11 0r PaceAnalyllral Service+e.LIC. Page 5 or 20

Waypoi lit 7S21 Whitepine Road,Richmond,VA 23237
Main 804.743-9401°Fax [phone]
ANALYTICAL www.waypointan8lytleal,xom
612312021
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville. NC, 2S076
Ref: Analytical Testing
Report N umber: 21-166-U00 5
Project Description: Cascades sludge-92543726
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) an 6/15/2021 for the analyses presented in the fallowing
report.
The above referenced project has been analyzed per your instructions_ The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
enalytic:ar method, Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters{chlorine, pH. dissolved oxygen, sulfite.,,) are required to be analyzed within 15 minutes of
sampling. Usually, but not always. any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of bolding time compliance.
The results are shown on the attached Report of Analysis(s)_ Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples inruded in this report
Please do not hesitate to contact me or client services if you have any questions ar need additional information_
Sincerely,
a rFr plc {vnir
Pauric Mcroary
Agronomist
Laboratory's liability in any claim re1tinr9 Ro at aiyses performed shah be limited to, at laboratory's option, repeating the
analysis on gaiestrhn at laboratory's expense, or the refund of the charges'paid for performance or said arras}sls.
Page 143 of 20
Page I. of 5

w
Waypoi n ,621 White pine Road,Richmond,VA 23237
Moan 8,04-743-9401° ak 804-Z71-6445
ANALYTICAL www,waypoin tan alytf€al,eam
Sample Summary Table
Report Number: 21-166-OOO5
Client Project Description: Cascades sludge-92543726
Lab N Q Client Sample ID Matrix Date Collected Date Received Method Lab ID
76771 Cascades sludge-92543726 Solids 06110/2021 08,35 06115/2021
76771 Cascades sludge-92543726 Solids 06/10{242108:35 06/1512021 5M-2540G WPMTN
76771 Cascadessludge-92543726 Solids 06J10P02100:35 06/15{2021 SM 500-N113C-TKN WP MTN
76771 Cascaues sludge-92543725 Solids 06114{2021 08:35 06/15{2021 AOAC 955,01 4liP MTN
WP MIN -Mernphis,TN: Waypoint Analytical-TN, Memphis,TN
Page 17 of 20
Page of 5

w
Waypoint 7E21:White pine Road.Richmond,VA 23237
fv1 a In 804-743-9401°Fax [phone]
ANALYTICAL www,waypointanalytltal,tom
11769
Pace Analyt cal Labs Charlotte Project Cascades sludge-92543726
Tyriek Hooks Report Date; O6/23/2021
9500 Kindey Ave Information; Received : 06/15/2021
Hunter5v1lle. NC 28078 y
yauurr of ir °r6.
Pauric Mc Groary Ph,D_,CPA
Report Number '21-1fi6-DOO5 REPORT OF ANAIV Agrorionnist
Lab No; 7677L Matrix; Salida
Sample ID=Cascades sludge-92543726 Sampled; 6/L012021 8!35
Test Results Drills MQL DF Date 1 lime I3y Analytical
Analyzed Method
Total Solids 44.1 'Yu 0,010 IL 06/16/21 16:21 FMM SM-2540G
Total Kjeldahl Nitrogen 3040 mg/Kg-dry 567 1 06/18/21 10:00 JPJ 41-41500-NH3C-Tiq
Calcium Carbonate Equivalent 44.7 95 0.1 i 05/22/21 14:03 DXT AOAC 955.01
Total Volatile Solids 54.6 No 0.Di0 1 06/16/21 16:21 FMM SM-2540G
C/N RATIO 100 Ratio 0 1 06/16/21 16;21 CALCULATION
Teat Rasults Units MQt.. OF date/Time Oy Analytical
Analyzed Method
Carbon(TOC) 31.7 °Y. 0.1310 1 06/16/21 16:21 CALCULATION
Analytical Method: SM-2540G
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Balch
Moisture 55.g % 0.010 1 06/16/21 16:21 FMM t.550900
Qualifiers/ OF Dilution Fartnr MQL Method Quantitatioel Limit
Definitions
Page 18 of 20
Page 3 of 5

/'s }��+� r}'�+� Paco Ana lyIie I geralees,LLC
aRaleigh,NO 27967
wwer.pa€alanxom ;9t9}854.49414
July 23, 2021
Ms. Karen Bellamy
Cascades Tissue Group-NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
IRE: Project: MONTHLY TESTING
Pace Project No.: 025118498
Dear Ms Bellamy.
Enclosed are the analytical results for sample(s)received by the laboratory on July 08,2021. The results relate only to the
samples included in this report.
Analyses were performed et the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The lest report from the external subcontractor is
atiaohed to this report in its entirety.
The test results provided in this Mai report were generated by each of the following laboratories within the Pace Network:
•Pace Analytical Services-Asheville
•Pace Analytical Services-Charlotte
If you have any questions concerning this report, please Feel free to contact me
Sincerely,
Tyriek Hooks
tyriek.hookstpace la bs.cor'n
[phone]
Project Manager
fndosures
Cascades Tissue Group-Rockingham, Divsion of
Cascacses Holding LtS inc_
REPORT OF LABORATORY ANALYSIS
This repryl shall not be reproduced,except in full.
without trie wriLien eonsenl of Pecs Anelylical 5 rvi e .LLB Page 1 of 21)

(11!.. Paco Analytical Ser;Ices,LW
x g701 Conrereree drive
a eArialIyti I Raleigh,NC 27507
www.pxctiabS.Gam i9t9W4-499.1
CERTIFICATIONS
Project. MONTHLY TESTING
Pace Project No: 925484gE
Pace Ana lyttcal Services Charlotte
984a kincey Ave.Ste irk,1 luntersville,NC 243078 South Carolina Certification#:99006001
Louisiana+NE LAP Certification#LA170028 Florid&NELAP CertiFicatiCn tt E87827
Ntorth Carolina Drink:log W ter Certification#:377013 Kentucky UST Certification#;84
North CareEina Fielci Services Certification#;5342 VirtgIniaNELAP CerhfiCatiOn tt 4 221
North Carolina Wastewater Certification#: 12
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville, NC 28804 North Carolina Wgislewaler Certification#_40
Flarid&NELAP Certification#;E87848 South Cerodina Cer1iflcatIon#:99030001
North Carolina Drinking Water CertIllcalfan#:37712 VIN.InleNELAP Ceriificatian rk 460222
REPORT OF LABORATORY ANALYSIS
This repai shell not be rapro[1ucep.except in fal.
vrilh4Mt the writlen consent of PAce Anoly¢cel Services,LLG Page 2 of 20

+ }�}+� PBcs AnilyliCirl ServIcsi,LLC
CIVef'na! ica/x 6741 Gonferenua drive
Raleigh.NC 27607
wyrw,puelihstam (910p831-4964
SAMPLE SUMMARY
ProJOCI_ MONTHLY TESTING
Pace ProjeCt No.; 92516496
Lab ro Sam plo ID Matrix IDate Colloctod Dato Rocalvoid
9254. 4961}01 CASACADES SLUDGE SAMPLE SOlid 07/08,r21 08:00 07108121 12:50
REPORT OF LABORATORY ANALYSIS
This nstorl 311011 no te reproduced,excapk in talk,
waroul Me wrinefl cv74an1 of PeoeAnelytical Services,LLC. Page 3 of 20

Par<#A1#ly#IC#t 9aruioe6.LLC
eAnalytical
nal i al 6741 Conference drive
{ Raleigh,
igh,NC.27607
rww.pacolahs.com [phone]
ANALYTICAL RESULTS
Proiect: MONTHLY TESTING
Pate ProjeCc Np• 92546 913
Sample; CASACADES SLUDGE Lab ID: 02 54 849606 1 CollecRoa: 47O08121 08:00 Received: 07f09121 12:50 Matrix: Solid
SAMPLE
Resaii$reported QC a Tory weight"basis and are aaljusted forporcent moisture,sample size arn&any dilut'oaS-
RepOrk
Parameters Results Units Limit lV1DL DF Prepared Analyzed CAS Na- Qua!
6010 MET ICP Analytical Method: EPA 6010D Preparation Method:EPA305DD
Pace Analytical Services-Asheville
Calcium 157000 mvikg 105D 210 25 07118121 16:15 0712012122:44 7440-70-2 M1
Copper 20.9 rngrtcg $.4 0.42 1 47lt812116:15 07120121 09:39 7440.50-6
Magnesium 16E0 rngncg 16.5 0.42 1 07116/21 16:15 07120121 09.39 7439.95•4
Nickel 1-6 mg+1Q9 0.84 0.42 1 0711B121 t6:15 07.120121 09.39 7440-02-0
Zinc 69.3 mg+lcg 1.7 0.84 1 0711612116:155 07120121 09.39 7440.66-6
2540G Total Percent Solids Analytical Method:SM 2540G•2011
Pace Analytical Services-Charlotte
Total Solids 41.8 % 0.10 0-0DD01e 1 07108121 17;29
Percent MIAstura Analytical Method: -846
Noe AnalykiC F Services-Charlotte
Percent tVic'sture 68.2 °1a 0.10 0.10 1 07/08121 t7:26 N2
9045 pH Soil AThalytidal Melt h04' EPA 9045D
PaCeAnaMical Services-Asheville
pH at 25 Degrees C 7-9 Std.()nits CAD 0-10 1 0711g 1 16:00 H3
Plant Available Nitrogen Analytical Method: Norte
Pace Analytical SeniteS-AsiteVille
Plan!Available Nitrogen 426 mg14 1 07/20121 14:16 N2
Total NikOgert CalculatlOn Analytical Method;TKN+NO3+NO2 Calculation
Pace Analytical Services-AShevillle
Nitrogen 1420 n7g!4 40.0 20 0 1 07220121 14:08 7727-37-g
350.1 Ammonia Analytical Method: EPA 350 1 ReV 2.0 1993 Mod. Pmepaiskion Method:EPA 350.1 Rev 2.0 1993 Mad.
Pape Analytical Service -Asheville
Nitrogen,Ammonia ND rngi4 22.5 22.5 1 07114121 08:40 07I14121 13:57 7664-41.7
351-2 Total icjaleahl Nitrogen Analytical Melnod: EPA 351-2 Rev 2.0 1993 Preparation Method;EPA 351.2 Rev 2.0 1993
pace Analytical Services-Asheville
Nitrogen.l jetdahl,Total 1420 mgdcg 109 54-3 1 07/16121 23:11 07/17f21 07:38 7727-37-9
353.2 Nitrogen.NO21NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method:EPA 353.2 Rev 2.0 1993
Race Analytical Services-Asheville
Nitrogen,NO2 plus NO3 NO mpg. 9.4 4.7 1 p7IO i 1 22.42 0710gI21 00:47
Nitrogen,Nitrate ND Mpg 9.4 4.7 1 07/08121 22:42 07/09/21 04;47 14797-55-8
Nitrogen,Nitrite NO mpg 9.4 2,4 1 07/08/121 22.42 07109121 00:47 14707-65-0
REPORT OF LABORATORY ANALYSIS
This'wail*hall not be repredwcea,except in WI,
Cale;07123I2021 08:44 AM without am writer Consent at Pace Analytical S&tce6,LLC Page 5 of 20

W y i lit ' 7621 Whitapine Road,Richmond,VA 23237
Main B04-743-9401°5ax 504-271-6445
ANALYTICAL www,waypeintanaNtita 1.Coat
7119/2021
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref_ Analytical Testing
Report Number: 21-1 94-000 8
Project Description: Cascades Sludge Sample
925414960 01
Clear Tyriek Hooks_
Waypoint Analytical Virginia, Inc. received sample(s) on 7113/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable
The analytical data has been validated using standard quality control measures performed as required by the
analytical method- Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012)and NELACl unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite..-) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall riot be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
daVIt d''{ fIvur ,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited ttx, of laboratory's option, repeating the
analysis in question at laboratory's expense,or the refund of the charges paid for performance of said analysis.
Page 16 ar 20
Page 1 of 5

vv.
Waypoint 78214 White pine Road,Rithrttond,VA 23237
Mein 804-743-9401°Fax 1904- 71-{r446
ANALYTICAL www-va ypoink2n,Olytleal-COm
Sample Summary Table
Report Number: 21.-194-0008
Client Project Description: Cascades Sludge Sample
9254B496001
Lab Na Client Sample ID Matrix Data Collected Date llecefved Method Lab ID
77045 Cascades Sludge 92548495001 Sal1JS 07/0812021 08;00 07/13/2021
77045 Casa;des Sludge 92548496001 Solids 07108/2021 08:00 07713/2021 SM-25405 WP F4TN
77045 Caacade5 Sludge 92548498001 Solids 071081202i 08;00 07/13/2021 5144500411:13C-TKN WP MTN
77045 Cascades Sludge 92546496001 Solids 07109/2421 08:0D 07/1312021 AOAC 955.01 WP MTN
VIP MTN -Memphis,TN; Waypair t Arealytit8f-TN, Memphis,TN
Page 17 of 20
Page 2 o 5

..
\/ /aypo Waypoint,
7621 Yd hike pine!load. Richmond,VA 23237
Main 804-743.9401.D Fax 804-z71-i i46
ANALYTICAL ,+f,+f,w,waypointanalytical.cam
11769
Pace Analytical Labs Charlotte Project Caseed .Sludge Sarnple
Tynek Nooks Report Date ; 07/19/2021
9600 IKindey Ave tnfarreeti l ; 92S4A496001 Received _07/13/2021
Huntersilte , NC 26478 Q
ta.ovrz ilt w(anryr'
Report Number:21-194-0008 REPORT OFANAL Y5•1S Pauric Mc Groan/Ph.D.,CPA
Agronomist
Lab No: 77045 Matrix: Solids
Semple It) :Cascades Sedge 92540496001 Sampled: 7/8/20 21 8:00
Test Results Units VOL DF Dale+Time By Analytical
Analyzed Ntethod
Total Solids 43.0 % 0.01e 1 07114121 16:44 FMM SM-2540G
Total NeIdahi Nitrogen 63.00 mg/Kg-dry 571 I 07/19/21 14:00 JP) ;M-45O0-M13C-TKP
Calcium Carbonate Equivalent 47,0 ° 0.1 1 07/19/21 15:11 DKr AOAC 955,01
Total Volatile Solids 56.5 % 0.010 1 07114/fl 16:44 I=MM SM-2540G
CAN RATIO 52 Ratio 0 1 07114/21 16:41 CALCULATION
Test Results Units MOO OF data 1 Time By Analytical
Analyzed Method
Carbon(TOC) 32.6 56 0.010 107114/21 16:44 CALCULATION
Analytical Method: 5M•2540G
Test Results Units MOL OF dale 1 Time 8y Analylicat
Analyzed Baton
Moisture 56.2 56 0.010 1 07/14/2110:44 FMt4 L563727
Qualifiers/ OF Dilution Factor t'lQL Method Quantitalion Limit
Definitions
Page 10of20
Page 3 of 5

Pace AnaFytFcal SemIces,4.LC
ace Analytical 670i oor ren.,Dave
Raleigh,tro 27607
vww.paealibs,ean, {9t9}6.4-4084
August 25, 2021
Ms. Karen Bellamy
Cascades Tissue Group-NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: SLUDGE
Pace Project No.: 92555165
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on August 12, 2021_ The results relate only to
the samples included in this report.
Analyses were performed et the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network. The test report from the external subcontractor is
attached to Ibis report in its entirety.
The test results provided in this final report were generated by eadi of the following laboratartes within the Pace Network:
• Pace Analytical Services Asheville
• Pace Analytical Services-Charlotte
Ef you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
tynek.hook pacelabs.corn
(7Q4) 7S- O92
Project Manager
Enclosures
cc: Cascades Tissue Group-Rockirgharn.DiMsiori of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALY IS
This repay shall not be rproduoed,except in full,
withoute writlen consent of PaceAnalyticat Services,LLC. Page 1 of 21

Pace Analytle*1 Service's.LLC
A a/ icai 6741 Confale43 ,NC Drive
/112 Ra�raiph,NC MOT
ww.r.paeelalm.eae t 1978'� d964
CERTIFICATIONS
PrOjeCt: SLUDGE
Pace Project No.: 92555165
pace Analytical Services Charlotte
9800 I<incey Ave_Ste 100,Huntersville,NC 2$079 South Carolina Certification I 99006001
Louislana&NE LAP Cerliketien#LA170028 FloridaiNELAPCertificalioi#: E97627
North Carolina Drinking Water Cerliflcalion at 37706 Kentucky UST Certification*:E4
North Carolina Field Services Certification#-5342 Virgir+iaNELAP Certification 1Ak 460221
North Carolina Wastewater Cerlificetiorl ft_ 12
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28-904 t'lortn Carolina Wastewater Ceytifioalian#:40
Florid 1NELAP Certification A.E37641 South Carolina Certification It`99030001
North Carolina Drinking Water Certiiloalion#:37712 VlrgIriiaNELAP Certification#:480222
REPORT OF LABORATORY ANALYSIS
This report shall 001 ie.reproduced_except in rull.
without written consented PazeMalylical Services.LLC. Page 2 of 21

Pappp,naIyIF al Seri cea,LLC
61a1 Cnnfereno9 Driu r
aceArral t;cal Raleigh,NC 276a7
xwk,G4te1$14.eam ;9191931,49a4
I
SAMPLE SUMMARY
Project: SLUDGE
Pace Project No.: 92555165
Lab ID m pie ID Matrix Date Coiled Data Rect}Ived
9255516.5-001 MONTHLY TESTING SOJid 08112121 08:10 03112r21 09'05
REPORT OF LABORATORY ANALYSIS
This report shall not he repcodt d.except in full,
viiihout therratlert consent of PSDBAnaly1ical Serge$.I.4C Page 3 of 21

M1 Pace Analytical Sarv1cea,LLC
870i C4nrefeaee Orwe
/72ce Analytical
Raleigh,NC 27507
www.pseeEehs.eom 1919)834-4994
ANALYTICAL RESULTS
Project- SLUDGE
15ace Project No.: 92555165
Sample: MONTHLY TESTING Lab ID: 02555165001 Collected: 08012/21 08:10 Received: OB112121 09:05 Malrix: Solid
Results reported fors a%fry weight"bans and are adjusted for percent moiture,sample siao and any Cffwtron$.
Report
Parameters Results Unl1s Limit MDL OF Prepared Analyzed CAS No. Qtlal
6010 MET ICP Analylcal Method;EPA6010D PrOparalion Method;EPA 3050E
Poe@ Analytical Services-Asheville
Ca1Ciurn 163000 mgikg 6370 1270 200 08+20121121)4 0812312114;43 7440-70-2
Copper 14.2 mgtkg 6-4 0.32 1 08/20121 12;00 08123/2.i00:40 7440-50.8
Magnesium 1810 rng+kg 12-7 0-32 1 08/20121 12;00 081232t 00:40 7439-95-4
Nickel 0-96 ing.e.kg 0.64 0.32 1 08120121 12:00 08123121 00;40 7440-024]
Zinc 66,3 mg<rkg 1.3 0,64 1 08/20+2112:09 08123/2100:40 7440`66-6 8o
2540G Total Po icon(Sol id s Analytical MelhOd: SM 2540G-2011
Pace Ariatylioal Sarvlces-Charlotte
Total'Solids 42,2 % 0-t0 0.000010 1 OB1112115:39
Percent Moisture Analytical Method;SW-846
Pace Analytical Services-Charlotte
Parcel-A Moisture 57-6 96 0.10 0.10 1 011113121 15;31 N2
9046 pH Soil Analylical Method:EPA 9045D
NCO AnelytIo I Services•Asheville
pH at 25 Degrees C 7.8 Sid. Units 0.10 0.10 1 0511612t 16:31 1-E3
Plant Available Nitrogen Analytical Method:None
Pace Analytical Services-Asheville
Plant Available Nitrogen 519 mg/kg 1 06.+25121 08:19 N2
Total Nitrogen Calculation Analytical li elhcd:Tl{N+NO3+NO2 Calculation
Pace Arrelyllcal Services•Asheville
Nitrogen 1730 rnging 40.0 20.0 1 0512412109:54 7727.37-9
350.1 Ammonia Analytical Melhod; EPA 350.1 Rev 2-0 1993 MOd. Preparation Melhod:EPA 350.1 Rev 2-0 1993 MOd
Pace Analylical Services-Asheville
Nitrogen,Ammonia ND mg/kg 23 7 23-7 1 08114121 10100 08014+21 12:13 7664-41-7
351.2 Total KjeWahl Nitrogen Analytical Method; EPA 351.2 Rev 2.0 1993 Preparation Method:EPA 351.2 Ray 2.0 1993
Pace Analytical Services-Asheville
Nllragen. Kjeldehl,Total 1730 mgtkg 113 56.5 1 08123121 21:59 09i'241421 05:11 7727-37-9
353.2 Nitrogen,NOVNO3 AnatyliOdI Melhpd:EPA 353.2 Rev 2.0 1993 Preparalion Method:EPA 353.2 Rev 2,0 1993
Pere Analytical Services•Ashevile
Nitrogen-NO2 plus NO3 ND mpg 9-4 4.7 1 09112121 22:29 06f13121 00:37 Mt
Nitrogen-Nitrate ND rngikg 9.4 4.7 1 09112121 22:29 06/13121 00;37 14797-55-8
Nllrogen,Nitrite ND mgrfcg 9.4 2.4 1 06112121 22:26 08/13i21 00:37 14797-65-0 M1
REPORT OF LABORATORY ANALYSIS
This repro shall not ba Fem.-Axed.except in MI,
Date;08+2542021 05:05 PM we oar Inc wririen cansent of Pd4C Analytical$ervrces,LLC. Page 5 of 21

Waypoi lit . 76.21 Whiteprne Road, Richmond,VA 23237
Main 804-743-9401°fait R04-271-6446
ANALYTICAL www,wayppintanalytIcal.rom
8120/2 021
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 kirtdey Ave
Huntersville, NC, 25078
Ref: Analytical Testing
Report Number; 21-228-0010
Project Description: 92555165001
Dear Tyriek Hooks:
aypoint Analytical Virginia_ Inc. received samples) on 811812021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Subcontracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012)and NELAC unless otherwise indicated_
Certain parameters{chlorine, pH, dissolved oxygen, sulfite.__}are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Paurio Mc roary
Agronomist
Laboratory's s liab,'fiIy In any claim relating la analyses performed sfraii be limited to, at laboratory's option, repeating rtre
analysis in quesliorr al laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 17 of 21
page 1 oP 5

w
VVaypoi t 1E21 Whirepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www:waypolnianal+itacal:C4m
Sample Summary Table
Report Number: 21-223-0010
Client Project Description: 925 55165001
Lab No Client Sample ID Matrix Detg Collected Date Received Method Lab ID
7741 92555165001 Solids 08112{202108:10 08116/2021
77491 92555155041 Solids 00/121202108.10 08/16/2021 5M-2540G 1 P MTN
7748/ 925551155001 Solids 09112/2021 08:10 08/1E42021 SM-4500-NH3C-TKN WP MTN
77481 92555165001 Solids 08/12/2021 03;10 O8/16/2021 ADAC 955.01 WP MTN
y�P',FIN -Memphis,TN; 4 ayri+int Analytical-TN, Memphis TN
Page 18 0121
Page 2 of 5

..
\%ypoi t. 7621 Wh its pine Road,Richmond,VA 2328?
Main 804-7413-5401°PM.804-271-6446
ANALYTICAL www_waypototanatytiol_com
11769
NCR Analytical Lahr Charlotte Project 92555165001
Tynek Nooks Repot Date= 08/20/2021
9800 Kindey Aye Enfarmation : Received :08/16/2021
Huntersville, NC 28078
Report Number ;21-228-00.10 REpaterOFANALYSIS Pauric MC Groary PhD., CPA
Agronomist
Lab No ; 77481 Matrix: Solids
Sample ID : 92555165001 Sampled; a112/2021 9:10
Test ResuEts Unile MQL DF Dale Milo Sy Analytical
Analyzed Method
Tatar Solids 35.4 913 0.010 1 02/19/21 16:13 HOT SM-2540G
Total Kjeldahl Nitrogen 3530 rno/K9-dry 706 1 OS/19/2109;00 JPJ 5M-4500-NH3C-T0
Calcium Carbonate Equivalent 29.0 % 0.1 1 08/19/21 12:40 DXf AOAC 955.01
Total VdatIIeSolids 59.4 % 0.010 1 OB/i8/21 16;13 FMM SM-25406
C/N RATIO 96 Ratio 0 1 08118/21 16;13 CALCULATION
Test ResUlls Wills MQI. DF Date I Time By Analytical
Analyzed Method
Carbon (TOC) 34.5 % 0,010 1 08/12/21 16.13 CALLIJLATION
Analytical Method: SM-2540G
Test RasiuJIs Units 11Qt DF Data/Vine By Analytical
Analyzed Balch
MOi5kure 64,6 ° 0.010 1 08/18/2116:13 FMM L559823
Qualifiers{ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 19 of 21
page l of S.

Pace,4nAt rtI i 9erviGhe,LL9
7AceAr!aIJ4ieaI Ralergh.NC 27607
wwmpacthIgi.com (910)&34-4984
I
September 27, 2021
Nis. Karen Bellamy
Cascades Tissue Group-NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: SLUDGE
Pace Project No.: 92560621
Dear Ms. Bellamy:
Enclosed are the analytical results for sarnpte(s) received by the laboratory on September 09,2021. The results relate only
to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pane Analytical Services-Charlotte
If you have any questions concerning this report,please Feel free to contact me
Sincerely,
Tyrlek Hooks
tyriek,hoaks pacelabs.corn
[phone]
Project Manager
Engosunas
cc: Cascades-59341e Group-Rockingham,Oil/slim of
Cascades Holding U5 Inc.
REPORT OF LABORATORY ANALYSIS
Trim report shall not ha reproduced,axcepi in full,
withpui the written c.anaani cf Pace Analytical 5arvic25,LLC, page t of Z1

+ }} +� Pace Analytical$ervlcae,LLC
__ Arra!y ica/# 8701 Ccigh,NC
Drive
Raleigh,NC 27507
hwx,yacvlarr#,COm (919)8 -4991
ERTCFI ATCONS
Project: SLUDGE
Pace Project No.. 92580621
Pace Analytical Services Charlotte
9800 Kinsey Ave.Ste 100, 1untersville_NC 28079 South Carolina Certification#: 9'900(5001
Louisiana!NELAF Cerli:kaliOn#LA17D028 Fi❑rida+NEtAP Certitcation#; E87627
Norlh Carolina Drinking Water Certirtetion#:37708 Kentucky UST Gerlilioation#;84
Norlh Carolina Field Services Certification#P 5312 Virgini9NEL F CertiBcatipn#:480221
North Cardlir%a WASlewdter Certilloallon#: 12
Pace AmityliCdl Services A531ev Ills
2225 RiverSide Drive.AShewille,ND 29804 Nertrt Car()line VYaSlew2ter Curtillcalinn#:40
Florid&NC LAP Certification#:E97649 SKrltr CerolIna Coraitication#:99030001
North Carolina Drinking Water Certification#;37712 VirglniaNELAP Certification#:450222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduce%except in rule,
without the written consent of Pace Anelyteei&ewes,LLC. Page 2 of 21

Paea Analytical Services,LLC
(162
eAna1 /cal° 6701 anfarenca Drive87
! Raleigh,NC 27807
wrw,Racifib Om (919)93A-48-0
SAMPLE SUMMARY
Project; SLUDGE
Pace Project Na.: 92560621
Lab ID Bamplo ID M tnx Date COIlectatl I?ato Received
B2580621001 MONTHLY Solid a 109121 07:30 G9109f21 10:51
REPORT OF LABORATORY ANALYST$
Iris report shall not be rBproduced.e%Cep1 ai f+IL,
without the written consent of PaCkAfailytliNit Services,LLa. Page 3 of 21

Pace Ana I Semloos,LLC
(91
eAnalytical 67Qf Leigh, C 27Drive07
Raleigh,NC 2F647
www.pacolatis.com (919)834.49U
ANALYTICAL RESULTS
Project; SLUDGE
Pace Project No.: 92560621
Sample: MONTHLY Lab ID: 82560821091 Collected: 09/09/21 07:30 Received: 09/00121 10.51 Matrix: Solid
Results reported an a"dry weight"basf5 and are&dfriled for perc.nI moisture,Sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua!
6910 MET ICP Analytical Method:EPA 6010D Preparation Method:EPA 30500
Pace Analytical Services-Asheville
Calcium 161000 rrlgikg 451 00.2 10 49f1112108:42 0911912111:23 7440.70-2
Copper 13.4 reg+kg 9,0 0.45 1 0911117108:42 Dffl1912. 11:20 7440.50.8
Magnesium 1740 mg/kg 18,0 0.45 1 09'11121 (18:42 09119121 11:20 7439.95.4
NiC I 1.2 mg/kg 0.90 0,45 1 091t12108:42 00/1912111:20 7440.02.0
Zinc 01.8 mgikg 1.8 0.90 1 0911 tl21 0$:42 00119021 11:20 744D-66-6
2540G Total Percent Solids Analytical Method SM 254DG-2011
Pace Analytical Services-Charlotte
Total Solids 43,3 96 0.10 0.000010 1 09/10121 17:33
Percent Moisture Analytical Meihod:SW.846
Pace Analytical Services-Charlotte
Percent Moisture 56,7 96 0.10 0.10 1 09110/21 17:26 N2
9045 pH Soil Analytical Mellic.d2 EPA9045D
Pace Analytical Services-Ashevlke
pH at 25 Degrees C 7,8 Sid. Units 0-1D 0.10 1 09/21/21 14:09 H3
Plant Available Nitrogen Analytical Method-None
Pace Arla3yliUl Services-Asheville
Pia nl Available Nitrogen 307 mgrkg 1 09/23121 16:39 N2
Total Nitrogen Calculaltlen Analytical Method:TICN+NO3+NO2 Calculation
Pate AnalyIICa!Sen+lces-Asheville
Nitrogen 1290 mglkg 40.0 20,0 1 09/17/2111:18 7727-37.9
350,1 Ammonia Analytical Method,EPA 35a.1 Rev 2.0 1993 Mod. Preparation Method:EPA 350.1 Rev 2.0 1993 Mod.
Pace AnahyliCal Services-Asheville
Nitrogen,Ammonia ND rrrgfltg 22,2 22.2 t 00i21 2t 0e:15 09121121 13:12 7664.4t-7
351.2 Total Neldahl htitrageu AnalyIICal Method:EPA 351.2 Rev 2.0 1993 Preparation Method; EPA 3512 Rev 2.0 1993
Pace Analylltal Services-Asheville
Nitrogen. Kjeldahl, Total 12$0 nxglkg 110 55.0 t 09113/21 20:52 09114121 05;16 7727-37-9
1511 Nitrogen,NOZNO3 Meihod:EPA 353.2 Rev 2,0 1993 PreparaGGn Me111001: EPA 353-2 Rev 2.0/903
Pace Analytical Services•Asheville
Nitrogen-NO2 plus NO3 ND rrigr 9.1 4.5 1 09/10121 23;01 09111/21 02;52 M1,R1
Nitrogen, Nllrate ND mg/kg $.1 4.5 1 09/10121 23:01 09/11/21 02;52 14797-55-8
Nitrogen-N'irile ND mglkg 9.1 2.3 1 09110/21 23: 1 O19 11f21 02:52 11797.65.0
REPORT OF LABORATORY ANALYSIS
This report shal not he reproduced,except in full
Date:09127/2021 06:07 PM without the written consent of Pace An8lyUcal SarwitGs.tl. Page 5 of 21

va
Waypoint 7f 21 wh Itepine Road,Richmond,VA 23237
Main 804-743-9441°Fax R44-2?1-6446
ANALYTICAL www.waypoia1tanaryucai,vam
9/22/2021
Pace Analytical Labs Charlotte
Tyriek Hooks
8800 Kindey Ave
Huritersville, NC, 28078
Ref: Analytical Testing
Report Number 21-258.0003
Project Description: 92560621001
Dear Tyriek Hooks:
Waypaint Analytical Virginia, Inc. received sample(s)on 9/1512021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted or' the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NErLAP)were performed in accordance with guidelines established by the USEPA
(including 40 CPR 136 Method Update Rule May 2012)and NEIAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite.,.) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s)_ Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
lirwirpY 1 (0fur
Pa uric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited fe,at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis_
?Age 17 of 21
Page I of 5

. .
Waypoint. 7621 Whitepine Road,Richmond,VA 23237
Main 8Q4.743-94D1 D.fax$]4-271-6446
ANALYTICAL www.wawpolntanalytical.com
Sample SummaryTable
Report Numbers 21-25B-0003
Client Project Description: 92560621001
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
7771-6 92560621091 Solids 09/09/202107:30 139115/2021
77716 92569621001 Solids 0910912021 07:30 09)15/2021 SM• 5400 VW MTN
77716 92560521001 Solids 09f0912021 07:30 09)15/2921 SM-4500-NI3C-TKN WP MTN
77716 92560621001 Solids 990/202107.30 09/15/2021 AOAC 955.01 VP MTN
•
WV MTN -t lertsphis, 1 N: waypaint Analytical-TN, Memphis,TPY
Page 16of21
Page 2 aE 5

w
VVaypoi nt 76211Mhitepine Road,Richmond.VA 23237
Main 904-743-94011`Fax MA-27/-6446
ANALYTICAL yoww.waypoinlanalytical,com
ti769
PBCe AnalyttCal Labs Charlotte Pro}ect 42560621001
Tyriek Hooks Report Date; 99/22/2421
91300 Kindey Ave Information ; Received :09/15J2921
lur] rSvIlle, NC 28078
?mil[ M{ rrfv,ir
FRuric Mc
Report Number ;21-25t3-8d43 REPORT OF ANALYSIS Agrpnornmi Groary Ph.D., CPA
5t
•
Lab Ho: 77716 Matrix: Solids
Sample ID:92560621001 Sampled; 9/9/20Z1 7:30
Test Results Units MQL DF Date+Time fay Analytical
Analyzed Method
Total Solids 34.9 % 11a10 I 09}16}21 15=54 FMM SM-2540G
Total KjeIIdahl Nitrogen 2660 mg/Kg-dry 716 1 09/20/21 09.30 JP] i'M-4500-NIi3C-TKP
Calcium Carbonate Equivalent 11-1 % 0.1 1 09/22f21 09;15 DX1 AOAC955.01
Total Volatile Solids 54-0 Eik 11910 1 09/16/21 1S'54 FMM SM-2540G
C/N RATIO L20 Ratio 0 1 09116}21 15;54 CALCULATION
Test Results Units It1OL OF Date+Time Sy AneIytical
Analyzed 'Method
Carton(TOC) 31.E ° D,D=O I :19/16)2115;54 CALCULATION
Analytical Method: SM-2540G
Test Results Units N1QL DF date 1 lime By Analytical
Analyzed Satoh
Moisture SSA °fir 0-010 1 09/16/2115;54 FMM L574461
Qu2lifiersf DF Oilut:on Factor MQL Method Qtiantltation limit
Definitions
Page 19 of 21
Page 3 of 5

Pace Analytical Servlec8,LLC
670 Conference alive
/12CeAna/j/tiCal Raeigh.roc 276N
wxw.pecelabs,odm 4.01.008M-4984
October 27, 2021
Ms. Karen Bellamy
Cascades Tissue Group-NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project_ SLUDGE
Pace Project No,: 92555645
pear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on October 07, 2021. The results relate only to
the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample anatyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network.The test report from the external subcontractor is
attached to this report in its entirety.
The test results provided in this Final report were generated by each of the following laboratories within the Pace Network:
•Pace Analytical Services-Asheville
•Pace Analytical Services-Charlotte
If you have any questions concerning this report, pease feel free to contact me.
Sincerely,
Tyriek Hooks
tyriek.hooks(2 pac-elabs.corn
[phone]
Project Manager
Enclosures
cc: Cascades Tissue Group, Rockingham,Oivsioe of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This rep rt andel not be reprod.ced.except in full.
without the written oonaeirk of Pace Analytical Servicac.LLC Page 1 of 19

A(9 P qe Analytical ServIcee,LLC
It
Ce nalYtkaI 6741 Conrereru a Chive
Raleigh.NC 27807
wewpuullblzen 191 M1.1-4954
CERTIFICATIONS
Project: SLUDGE
Pace Project NO.: 92565645
Pace Analytical Services Charlotte
9600 Kirlcey A .Ste 100,Hunlersville,NC 28078 South Carakina Certification#99406001
4DuislanaiNELAP Certification#LA170023 Ftarida1NELAP Certification it.EB7627
North Carolina Drin rig Water CertifiOativn#:37706 Kentucky UST CertiIicalion X:84
North Carolina Field SSryiceS Certlfipllo1- at-:5342 Virginia/VELi P Certlikcetien#_460221
North Carolina Wegtirwater Certification# 12
Pace AMdlytloal Sarvloas AshevIlla
2225 Riyersice Drive,Asheville,NC 28804 North Carolina Wastewater Certi toaii0rl ft 4D
FloridalNELAP Certification#_E87648 South Carolina Certification#-990300O1
North Carolina Drinking Water Certification 37712 VirginiaNELAP Certification#-460222
REPORT OF LABORATORY ANALYSIS
Thus report slay not be reproduced,except in lull,
without the wtrtten consent pF Pace Aimiylirai Seivioea,LLC Page 2 of 19

��++ Pace Artalygicat Services,LLC
€7ceA alytic l Raleigh.
6701 Conf NC Drive 2760 7
CPC 7
www pgvilbS.cnm (910)1334-495,1
SAMPLE SUMMARY
Project: SLUDGE
Pace Projecil No.: 9256564S
Lau ID Sample ID Matrix Date COILeo#e.q Date Received
S2565645001 SLUDGE SAMPLES Solid 101'07121 07.20 10iD7121 11:40
REPORT OF LABORATORY ANALYSIS
This rnnort gtxpJL not to reproduced.except in fulb.
without the wi en consent Pace Analytical SerAaea.LLC Page 3 of 1

+ Paco AnmFyticltt Semites,l l
Gl VeAf a/ /ca 6709 Conference drive
_ Raleigh,NC 27607
www piceiane,com (91918M-49M
ANALYTICAL RESULTS
Proiect: SLUDGE
Pace Prci ect No.. 92565645
Semplo: SLUDGE SAMPLES Lab ID: 92565645001 olledec1: 10/0712147:20 Received: 1bf=712111:40 Matrix_ S011d
Results reparted on a"d&y weight"basis and are atlJustad for percent molslure,sample size and any di/utfons.
Report
Parameters Results Units Limit IVIDL DF Prepared Analyzed CAS No. Quill
6010 MET ICP Analytical Me1hpd:EPA6010D Preparation Method:EPA 3050E
Pace Analyiica I Services-Asheville
C*ICiurn 112000 mg/kg 1110 223 20 10109/2109:53 1011312111:04 7440.70-2
Capper 82.6 rngilkg 11.1 0-56 1 10/0912109:53 10111121 13:43 7440•660-8
Magnesiurri 1630 fllgrkg 22.3 0.56 1 10109/21 09:53 10111/21 13:43 7439-95-4
Nickel 1.6 mpg 1.1 0.56 1 10/0912109:53 10111121 13:43 7440-02-0
Zinc 95,1 mg/kg 2.2 t.1 1 1010912109;53 10111/2113:43 7440-66-6
2540G Total Percent Solids Analytical Method: BM 2540G-2011
Pace Analytical Services-Charlotte
TOW!SoII0s 40-8 % 0.10 01100010 1 10/08/21 14:50
Percent MoIeture Analytical Method:SW-846
Pace Analytical Ser i0e3•Charlotte
Percent Moisture 69.2 % 0.10 0.10 1 10108121 14:42 N2
0045 pH Solt Analytical Method:EPA 9045D
Pace Analytical Services•Asheville
pH at 25 Degrees C 7.3 SlO. Units 0.10 0.10 1 10020121 17:37 H3
Plant Available Nitrogen Anaiylical Method:None
Pace Analytical Services-Asheville
Plant Available Nilrbgen 456 mglkg 1 10127121 11:26 F42
Total Nitrogen Calculation Analytital Method. TKN+NO3+NO2 Calculation
Pate Analytical Services-Asheville
Nitrogen 1520 mglkg 40-0 20.0 1 1012/12111:00 7727-37-9
350.1 Ammonia Analytical Method:EPA 350.1 Rev 2.0 t993 Mod. Preparation Method;EPA 350 1 Rev 2.0 1993 Mod.
Pace Analytical Services-Asheville
Nitrogen,Ai-monde ND mg/kg 22.7 22.7 1 10112121 15:00 10013.21 17:48 7664-41.7
351.2 Total Kjelttlllil Nitrogen Analytical Method-EPA 351.2 Rev 2,0 1993 Preparation Melhod:EPA 301.2 Rev 2.0 1903
Pace Analytical Services-Asheville
Nitrogen. Kjeldahl,Total 1520 rng1k9 123 61.3 1 10026121 21:22 10/27121 06:50 7727-37.9
353,2 Nitrogen, NO2INO3 Analytical Method:EPA 353.2 Rev 2.0 1993 Preparation Method;EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,NO2gku5NO3 NO mg1kg 9.7 4.8 1 1010812122.54 10/09121 00:36 M1
Nitrogen,Nitrate ND rrglkg 9.7 4.B 1 1014E121 22:54 10/09/21 00:36 14797-55-8
Nitrogen_Nitrite ND mg/kg 9.7 2.4 1 1014$!21 22:54 10f09121 00.36 14707-B5-0 Ml
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except io full,
Dale: 1012712021 03.32 PM vrtihoui 1he written nonsenI cif Pace Analytical Ssrrites,LLD, Page 5 of to

Waypoint 76 1 4Vhitepine kroaci,k!china rid,VA 23237
Fain 804-743-9401°Fax [phone]
ANALYTICAL www,waypDJntanalytl€al.com
10/25/2021
Pace Analytical Labs Charlotte
Tyriek Hooks
9,800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 21-285-0003
Project Description• 9256564500f
Dear Tyriek Hooks:
Waypoint Analytical Virginia, tnc. received sample(s) on 10/1212021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method- Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NPLAP)were performed in accordance with guidelines established by the USf=PA
(including 40 CFR 13i5 Method Update Rule May 2012)and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite,..)are required to be analyzed within 15 minutes of
sampling_ Usually- but not always. any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated- This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
La6orelory's liabilrry in any ebrrn relating 60 analyses perlomred shall be limited to, at iabaraoory's option, repeating the
analysis in question al haborarory's expense, or the refund of The charges peed for performance of said analysis.
Page15 of 19
Page 1 o= S

Way i n 7621 White pine Road,Richmond,VA 23237
Main 904-743-9401°fax SO4-271-6446
ANALYTICAL www.waypointanakytical.corn
Sample Summary Table
Report Number: 21-285-0003
Client Project Description: 92565645001
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
55136 9Z5656451 1 Solids 1010712021 07:20 1011212021
55136 92565G45001 Solids 10107{2021 07;20 10112/2021 5M-2515G WP MTN
55136 92555645001 Solids 10/07/2021 0720 10/12/2021 SM-4500-NH3C-TM lAIP MTN
55136 92555645001 W69 10107/2021 07.20 10/12/2021 AOAC 955.01 WP MTN
WP MTN -Memphis,TN; Waypoint Analytical-Mr Memphis,TN
Page 16of 19
Page 2 of 5

wW
VVaypoi t. 7621%Vhltepioe Road,Richmond,VA 2327
Main BM-743-9401°Fax KA-271-6446
ANALYTICAL wvww.waypointanalytical.corre
11769
Pate Analytical Labs Charlotte Project 92565545001
Trial Hooks Report Date ; 10/25/2021
9800 Klndey Ave Information ; Received ; 10/12 021
Nuntersvllle. NC 28079 �} L
?A:n/i r 1lt r 4I$ U y
Report Number ;2L-285-0003 REPORT OFA rMLAL VSIS Pauric Mc Graary Ph.D., CPA
Agronomist
Lab No: 55136 Matrix; Solids
Sample ID ;92565645001 Sampled: 1O/7/202L 7;20
Test Results Unils MOL LW Date ITime Sy AnelytlueI
Analyzed Method
C/N RATIO 72 Rath 3 1 10/13/21 15:34 CALCULATION
Test Fteeolts Units HOL DF data+Time Sy Analytical
Analyzed Method
Carbon(TOC) 35,3 ° 0,010 1 10/13/21 15:34 CALCULATION
Total Solids 17.9 °Na 0.010 1 10/13/21 15;34 FMM SM-2540G
Analytical Method; SM-2540G
Test Results Units MOL DF Date+time By Arrelytical
Analyzed Batch
Moisture 52.1 % 0.010 1 10/i3/2115;34 FMv1 L579028
Total Kjeldahl Nitrogen 4930 rng/Kg- dry 1560 1 10/18/21 09;30 JPJ iM-4500-NH3C TKF
Calcium Carbonate Equivalent 35,0 % 0-1 1 10/21/21 10:25 DKT ADAC 955.01
Total Volatile Solids 6a..8 °da 0.010 1 10/13/21 15:34 FMM 5M-Z540G
QuaMen) B Analyte detected in blank OF Dilution Factor
definitions H Beyond holding time MQL Method Quantilaltion t.lrnit
Pagel 7or19
Page 3 of 5

+ + PaceAwfelylles'Servlcaa,LLC
aceA fCtI ll+{�+a 6707 conference Oii4rt
Raleigh.NC.27807
www.pitnliEssan {919)034-49$4
I
l
November 24, 2021 r`
Ms. Karen BelRamy
Cascades Tissue Group-NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: CASCADES SLUDGE SAMPLE
Pace Project No : 92571531
Dear Ms. Bellamy_
Enclosed are the analytical results for sarnpfe(s) received by the laboratory orn November 0R, 2021. The results relate only
to the samples included in this report.
Analyses were performed at the Pace Analytical SerdicQs location indicated on the sample analyte page For analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network.The test report from the external subcontractor is
attached to this report in itS entirety_
The test results provided in this final report were generated by each of the following Faboralories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Senrtoes- Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
ty riek,hooks pace labs.com
(704)875-go 2
Project Manager
Enclosures
cc. Cascades Tissue Group-Rockingham. DFvsion of
Cascades Holding US Inc.
REPORT OF LABORATORY ANALYSIS
This repot shall not be reproduced,except in fulI,
wilhpuL Itte Wrltien consent of PaceAnalylical Santee.LLC Page 'I of 20

Pace Anvly k iI Servaoea.LLC
a701 Coidereaee Dive
An(9 aace lyticalReleigiM.N r eo}
www.paeelatn eam (919)83A-198A
CERTIFICATIONS
Project: CASCADES SLUDGE SAMPLE
Pace Project Na_ 92571531
Pace Anatif lcal Services Charlotte
South Carolina Laboratory FD:g 1046 South Carolina Certification#;99406001
I844 Kincey Ave,Ste 10D,Huntersullla.NC 2.8078 South Carolina Drinking Water Cert.#;99[46003
Norltl Carolina Drinking Water CertIflcatIon#C 377D6 Florkla/NELAP Ceri ficalion#_E87627
North Carolina Field Ser moss Certification#:5342 Kentucky UST Certification#;64
Nc rth Carolina Wastewater Certification*: 12 Louisiana DOH Drinking Waler#:LAM
South Carolina Lagarawry ICc 99006 VkgIniatVELAP Certification#:4V422t
Face Anaiytipal Services Asheville
2225 Riverside Drive,Ashevl11e,NC 2B804 South Carolina Laboratory iD;99030
Ftorida+N ELAP Certification#:E87648 South Caroni ma Certification#: g903DDO1
North Carolina Drinking Water Certification 37712 VirginlaNELAP Certlftcallon 41460222
North Carolina Wastewater Cerlificalim#_40
REPORT OF LABORATORY ANALYSIS
This repel shall not he reproduced,except in full,
wihlout h written consent of Pace Analytical Services,LLC. Page 2 of 20

Psee Amity!Lout 9errIcee,LLC
aye Analytical 6701 Canferenae DO,*
Raleigh.NC 27607
www. calaba.eam 0191974-49M
Ii
SAMPLE SUMMARY
f rOjeCt: CASCADES SLUDGE SAMPLE
Paoe Pralect No.: 92571531
Lab ID Sample It? Matrix Date Collected Date ReCeiV9ti
92571531001 CASCADES SLUDGE SAMPLE Safio i1I09f21 07:30 11109121 09::0
REPORT OF LABORATORY ANALYSIS
This repprt shell not he(etc/educed,except in full,
wip5pu!thewrlllen consent of PeoeAnalytical Services.LLC Page 3 or 20

Pose A roityti cat Services,LLC
6701 Conference Drive
ac9Ari ly1ICaI f2�lleigtf- fc 27647
xww,RaerlaRr Co[I {979)A3l-4984
ANALYTICAL RESULTS
Project: CASCADES SLUDGE SAMPLE
Pace Projnd Plo.: S2571531
Sample: CASCADES SLUDGE Loh ID: 92571631001 Collected: 11109V21 07;30 Received. 111D9/21 09:30 Matrix: Solid
SAMPLE
Ftestaits reported on a "dry weight"$psis arid are as lusted for percent moisture,sairrpie size and any SrilutianS.
Report
Par&meler6 Re&uits Units Limit MDL DE Prepared Analyzed CAS No. Oual
5010 MET ICP Analytical Method:EPA 6010D Preparation Method: EPA 305013
Pace Analytical Services-Asheville
Calcium 185000 mgikg 491 98.1 10 11f1012110:34 1111912104:49 7440-70-2
Copper 19.5 mgikg 9.3 0,49 1 11110121 10.34 11117.21 01:04 7440.50-8
Magnesium 1830 mg/kg 19.6 0.49 1 11110/21 10:34 11/17l2101-.04 7439.955-4
NICJ el 1.9 mgikg 0.98 0.49 1 11110l21 10134 11/17/21 01:04 7440.02-0
Zinc 74.9 tngikg 2.0 0.98 1 11110121 10 34 11117121 01:04 7440.66.6
2540G Total Percent Solids Analytical Method: SM 2540Ca-2011
Pace Analytical Services-Charloile
Total Solids 43,2 % 0.10 0.000010 1 f'I109+21 17:24
Pgrcant Molrlure Analytical Method: SW-846
Pace Andlyti0a1 Services-Charta1Ec
Pereeit Moisture 56.8 96 4,10 0,10 1 11109f21 17:15 N2
9045 pH Soil Analytical Method; EPA 90450
Pace Analytical Services-Asheville
pH at 25 Degrees C 8.0 Std. Units 0.10 0.10 1 11118,21 17:37 H3
Plant Available Nitrogen Analytical Method: None
Pace Analytical Services •Asheville •
Plant Available Nitrogen 42e rrigtkg 1 11119/21 15.31 N2
Total Nitrogen CalCufaticn Analytical Method;TKN+NO3+NO2 Calculation
Pace Analyllca I Services-Asheville
Nitrogen 1430 rngilkg 40.0 20.0 t 1111112117:10 7727.37-9
350.1 Ammonia Analytical Method: EPA 350.f Rev 2.0 1993 Mod. Prepsrallen Method:EPA 350.1 Rev 2.0 1993 Mod.
Pace Analylical Services-Asheville
Nitrogen,Ammonia ND mg/kg 23.2 23.2 1 11/1212109.25 1111212111:33 7664-41-7
361.2 Total '<Jeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method:EPA 351.2 Rev 2,0 1993
Pace Analytical Services-Asheville
Nilrogen,K eIdah1,Tcia1 1430 mpg 110 55.1 1 11,10121 19:16 11fi1121 05;01 7727-37-9
353.2 Nitrogen, NO21NO3 Analytical Method:EPA 353.2 Rey 2.0 1993 Preparation Method;EPA 353.2 Ftev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,NO2 pleas NO3 ND rrlglkg 9.0 4.5 1 111.09121 22:29 11f10121 Q0:17
Nilregeri.Nitrale ND mg/kg 9.0 4.5 1 11i09121 22:29 11/10121 00;17 14797-55-8
Nitrogen,Nitrite ND mgfkp 9.0 22 1 11/09121 22:29 11/10121 00:17 14797.65-0
REPORT OF LABORATORY ANALYSIS
The remit shall not be reproduce1,eneps ati full.
Date: 11i24f2021 05:18 PM wishoul ihCwri[1en osneent of Pace Analytical Servida8.LLC. Page 5 or 20

W y I lit 7621 White pine Road,Rid-in-141nd,VA 23237
Main 804-743- 401°Fax J9Q4-271-5r446
ANALYTICAL wvMw,waypointanal}ttiLal.tam
11 f22/2021
Pace Analytical Labs Charlotte
Tyriek Hooks
9600 Kindey Ave
Huntersville, NC. 28078
Ref: Analytical Testing
Report Number: 21-315-0003
Project Description: Cascades ludge/92571531
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/11/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions- The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method- Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NE LAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite..-)are required to be analyzed within 15 minutes of
sampling- Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
Theresults are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Fc Pit 6rfortwr
Pauric Mcrcary
Agronomist
Lobarntpry's liability rn any crania relating to analyses performed shall be tirnrred ru- of laboratory's option, repo{xtrn j the
analysis rr1 question ar laboratory's expense, or the refund of the charges paid for portormance of said analysis.
Rage 1{iof20
Page 1 pf 5

W y I l 7621 White pine Road.. Richmond,VA 23237
Main S.04-743-9401°Fax&04-271,-61146
ANALYTICAL www,waypointanalytital,corn
Sample Summary Table
Report Number: 21-315-0003
Client Project Description: Cascades Sludge/92571531
Lab Fla Client Satriple ID Matrix Date Collected Date Received Method Lab ID
55497 Cascades Sludge/92571531 Solids 11(0912021 07;34 11/11/2021
55497 Cascades Sludge/92571,531 Solids 11/09/2021 07:30 11/11/2)21 SM-254OG WP MTIJ
55497 Cascades 91udg 92511531 Solids II/09/2021 07=30 tt/U/2021 SM-4500-14H3C-TKN WP MTN
55497 Cascades Sludge/92571531 Solids 11/09/2421 07:30 11/11/2021 *DAC 955,01 WP MTN
•
WP MTN -Memphis,TN: Waypclnk AnalytIcal-TN, Memphis,TN
Rage 17 of 20
Page 2 of S

w
VVaypoint.. 7621 Whitepine Road,Richmond,VA 23237
Mein 804-743-9401*Fax [phone]
ANALYTICAL www.waypairitanalytisal_com
11769
Pace Analytical Labs Charlotte Pro)ect Cascades Sludge/9257153
Tyriek Hocks Report Date : 11/2212021
9800 Kindey Ave Information ; Received ; 11f11/2021
Huntersuilte, NC 26078
ligui,nz ill 6/.9.
Patric Groiiry Ph.D.,CPA
I epoft Number:21-315.0003 REPORTOFANALYSTS Agronomist
Lab No; 55497 Matrix: Solids
Semple ID : Cascades Siudgef 92571531 Sampled: 11/9 f 2021 7:30
Test Results Units MGIL OF Date/Time By Analytical
Aresiyaett Method
Moisture 56.0 % 0.010 1 11/12/21 16:14 FMM SM-254{)G
Calcium Carbonate Equivalent 52.6 0.1 I. 11 f 19f21. 1100 DXT AOAC 955.01
Cfh4 RATIO 96 Ratio 0 1 11/12/21 16;14 CALCULATION
Test Results Units AWL DF Date, Time By AneilytIcel
Analyzed Method
Carbon(TOO 30.1 ° 0.010 1 11f 12f21 16;14 CALCULATION
To-fat Solids 43.2 % 0.0/0 1 11f12f21 16:14 FMM SM-254DG
Total Volatile SolFds 51.8 % 0.010 1 11/1201 16:14 FMM SM-2540G
Total Kjeldahl Nitrogen 3150 +I1 / -dry 579 1 11f 17121 10:00 JP] 4M-450o•NH3C-TKr,
Qtraliflers/ DF Dilution Factor L Limit Exceeded
Definitions F4QL Method Cudntitatic 1 Limit
Page 18 of 20
Page 3 of 5

Pace AnalyliOAk$Orwkie6,LLC
❑ r++ i 6T41 Conference{hive
ace Analytical Raleigh.NC 2M17
powrr.pacala46,rom [phone]
December 21, 2021
Ms. Karen Bellamy
Cascades Tissue Group-NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project SLUDGE 12102/21
Pace Project No.: 92575489
Dear Ms. Bellamy:
Enclosed are the analytical results for-sample(s) received by the laboratory on December 02, 2021. The results relate only
to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated an the sample analyte page for analysis unless
otherwise footnoted.
Some analyses were subcontracted outside of the Pace Network.The test report from the external subcontractor is
attached to this report in its entirety_
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
- Pace Analytical Services-Asheville
- Pace Analytical Services-Charlotte
If you have any questions concerning this report,please feel free to contact rne.
Sincerely,
Tyriek Hooks
tyrie .hooks pace labs.corn
(70,4)875-9C 2
Project Manager
Enclosures
cc: Cascades Tissue Group.Rockingharn, DivSiorl of
Cascades Holding US Ina
REPORT OF LABORATORY ANALYSIS
Inc{apart shall na1 be reproduced.except in hil,
vnahaul the wmlen coneen1 ad PacC. 4Iybbal yen, ea,LLC. Paget of 21

• Pace.AnalyIi I sorvrcp#,LLC
•
e Analyti al ago,Confetence
a ./C.2mo
RaAei9n.r�C 27�07
Hww.p lecabs.tom 919)83q-49$4
CERTIFICATIONS
Project. SLUDGE 12i02/21
Pace Proiect No.: 925575489
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certitic lien#: 95006001
9840 PCinceyAve. Ste 100,HunterVille,NC 28078 S4uRh Carolina Drrnkirxg Water Con.#:990D6003
North Carolina Drinking Water Certification#:37786 .rlorigl.9JNELAP Certillcallon 1#: E97621
North :Ana Field Servi es Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#: LA429
Soulh Carolina Laboratory ID:990OB Virginia ELAP Certification#:460221
Dace Analytical Sen.lces Ashe+sllFe
2225 RiverSide Drive-Asheville,NC 28804 Sol Carolina Laboratory iD: 9 O20
floriclaiNELAP Certil$C2lion#: E87648 SouU7 Carolina Certification#:90030001
North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222
Nardi Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
This report shall not bo reproduaod,on:ept in full,
without rho written consent of Pace JSn lyle al$eI lees.L4C. Page 2 ci 21

Pave Analytical Seavitas,LLC
ce Analytical RaIsigh,NC 27607
www.pgetfahe.e4m [phone]
SAMPLE SUMMARY
project: SLUDGE f2142i21
Pace Project No.: 92575489
Lab ID Earnpae ID Matrix Date C ollactetl Data RocoIved
32575489001 SLUDGE Solid 121]2i21 I]B.OD 12.W/21 t1:54
REPORT OF LABORATORY ANALYSIS
This report stall not be ceproducetl,except in Mt,
wI`.hout the written consent of Pace Analy4"rtAI SernCes,LLC. Page 3 of 21

ace +�f Pace Arialy1Lcal Services,LUG
Analytical 8701 Geleh. n4e Drive
RaACigf7_r+C 27gp7
vfL.Ar lacalabs.tpw [phone]
ANALYTICAL RESULTS
Project SLUDGE 12/02121
Pace Protect No.: 5(2575489
Sample! SLUDGE Lab ID: 92575489001 C011eCted' 12102121 08:00 Received: 12102121 11:50 Matrix: Solid
Res ifs reported cm a "dry weight"basis and are anytistad forpercent moisture,aampie size an any dltuitioros_
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS NO. Qua!
5010 MET ICP Analytical Method:EPA 6010D Prepdrdlion Method:EPA 3050E
Pace Analytical Serriae9-Asheville
Caacium 119000 mg/kg 516 103 10 12108121 11:04 12/08121 21:25 7440-70-2
Copper 13.2 Inglkg 10.3 0.52 1 12106121 11:04 12M7)21 17:42 7440-50"8
Magnesium 1150 mg/kg 20_8 0.52 1 12106121 11;04 12)07121 17.42 7439-55-4
NiCkel 3.7 mg1k8 1,0 0-52 1 t210612111:04 12/0712117:42 7440-02-0
Zinc 71.8 mg/kg 2.1 1.0 1 12106i+71 11;04 12107/21 17:42 7444-6 -6 Pd
254OG Total Percent Solids Analytical Method: SM 2540G-2011
Pace Analytical Services-Charlotte
Total souls 40,4 % 0.10 0.000010 1 12.'07/21 16:41
percent Moisture .analytical Method: SW-846
Pace Analytical Services-Charlotte
Percent MoiSlure 59,0 °k 0.10 0.10 1 12107121 16:34 N2
0046 pH Soil Analytical hleihod; EPA 9045D
Pace Analytical Services-Asheville
pH al 25 Degrees C 8.2 Std.Llriats 0.10 0.10 1 12/1)&21 14:35 H3
Plant Available Nitrogen Analytical Method: Nora
Race Analytical Services-Asheville
Plant Available Nitrogen 438 mg/kg 1 12/1612115:91 N2
Total hlitrogen Calculation Analytical Method:TKN*NO3+NO2 G ic.iiaiiOo
Pace Analytical Services-AsllevalLe
Nilragers 1460 rig/kg 40.0 20.0 1 12116121 15:09 7727-37-9
350.1 Ammonia Analytical Me#tiGl: EPA 350.1 Rev 2.0 1993 Mod. Preparation McIJiOd:EPA 350.1 Frew 2.0 15533 Mod.
Pace Analytical Services-Asheville
Nilregen,Ammonia ND mglkg 24.3 24.3 1 12109121 05:13 12109/21 12:24 7664-41-7
151.2 Total ltjcldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 t993 Preparation Method:EPA 351.2 Rev 2,0 1993
Pate Analylicak Services•Asheville
Nllragen, Kleldalil,Total 145.0 mglkg 113 56.3 1 12114121 21:54 12115121 05:32 7727-37-9
353.2 Nitrogen,NO21MO3 AnaJylical Method-EPA 353.2 Rev 2.0 no Pre;raralien Method: EPA 353.2 Rev 2.0 1993
Pace Analylica!Services-AShevIlle
Nitrogen. NO2 plus NO3 ND mglkg 9.6 4-B 1 12103121 22:54 12104121 00;10
Nitrogen.Nitrate ND rrrglkg 9,6 4-B 1 12t03121 22:54 12104+21 00:10 14797.55-8
Nitrogen, Niirile ND mgllcg 9.6 2,4 1 12103t21 22:54 12104121 00:10 14797•65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in ful!
Date; 12/21)2021 05:35 PM without the wribCn cnJsenL of Pace Analytical SBNiGOS.LLC Page 5 al 21

% y . 7621 Wititepine Road, Richmond,VA 23237
Maim$04-741-9401 6 Fax [phone]
ANALYTICAL www,waypoi'rtanalytical,com
12/14/2021
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 21-341-0004
Project Description: 92576489
Dear Tyriek Hooks:
Waypc int Analytical Virginia, Inc. received sample(s) on 1217f2021 for the analyses presented in the following
report,
The above referenced project has been analyzed per your instructions, The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite.,.) are required to be analyzed within 15 minutes of
sampling_ Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance,
The results are shown on the attached Report of Analysis(s)_ Results for solid matrices are reported on an as-
received basis unless otherwise indicated_ This report shall not be reproduced except in full and relates only to
the samples 'included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information,
Sincerely
lei e Jrl 4 oarr
Paurrc McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeafing ttre
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis_
Rage 17 0121
Pagt 1 of 5

V aY I 76t1 Whitepine boast.Richmond,VA 23n7
Main 804-743-9401 6 1 B!s 804-271-6446
ANALYTICAL www-waypoin tan alytical.com
Sample Summary Table
Report Number: 21-341-00154
Client Project Description: 92575489
Lab No Client Sample ID Matrix Data Collected Date Received Method Lab ID
55742 92575489 Sellds 121021202100.100 12/0712021
55742 925754139 Solids 12/02j2021. 08:00 12107/2021 SM-2540G WP MTN
55742 92575489 Sothis J2402/2021 0$'00 12107/2021 901-4501 N1-13C-7KN WP MTN
55742 925754139 WId5 12/02/2021 09:O 12107/2021 AOAC 955,01 6Vp ivrEN
Wp Km -MEtphisr TN: Waypaint Analytical -Thlr Memphis,TN
Page 18 of Z1
Page 2 of 5

w
\A(aypoint.
7E27 MIitepine Road,Richmond,VA 23.237
Main 8 4-743.9401°Fax 804-271 #46
ANALYTICAL ww r_waypointanalyticai.com
11769
Pace analytical Labs Charlotte Project 92575489
Tyriek Hooks Report Date : 12/14/2O21
9800 Kindey Ave Information: Received : i2/07 f 2021
Huntersville, NC 2807$
puefi; re ;,..vs--
Report Number :21-341-0004 REPORT OF ANALYSIS P$lxwC Mc Groan..Ph.D.,CPA
Agronomist
Lab No ; 55742 Matrix: Solids
Sarrtple ID:92575489 Sampled; 12/2/2021 8:00
Test Results Units MQL DP Elate iTime Sy Mrralylical
Analyzed Method
C/N RATIO 93 Patio 0 I 12/09121 09:00 CALCULATION
Test Results iJliIt MQL OF Date l Time 6y Analytical
Analyzed Method
Carbon (TOC) 36.3 % 0.010 1 12109121 16;1? CALCULATION
Total Solids 38.2 9Io thew 1 12/09/21 16;17 FMM SM-254OG
Analytical Method; SM-2S40G
Test Results Units MQL OF Date/Time By AnalytICSI
Anelyyed Balch
Moisture 61.6 ° 0.010 1 12/09/211E:17 FMM L589223
Total I jeldlahl Nitrogen 3930 mg/K9 •illy 654 1 12M9/21 09:00 JP] IM-4500-N1-13C-TIR
Calcium Carbonate Equivalent 8.1 ° 0,1 1 12/14/21 09:12 MT AOAC 955.01
Total Volatile Solids 62.5 ° 0,010 1 12/09/21 16;17 FMM SM•2540G
Qualifiers/ 8 Analyte detected in blank DF Dilution FadtOr
Definitions H 8eyorid Folding tune MQL Method Quantitation limit
Page 19 of 21
Page 3 of 5

MMIT Smarm Errnrromroenrof raduarugres-
33!0 iF7rr3f.
NM Mg Arran s iQMI:HT r limns OLb4!>r&,1kC Corya r ga Fes,Oho 44223
Arrn+yr:e�J 1 rFb +art4o+ox r 'L:f33r1�?53..2f 1 FAX:(330)233•44$9
ilehsrrr:hrep....www.settek.min
May 25, 2021
Karen Bcrlamy
Cascades Tissue Group-North Carolina Inc
a division of Cascades Holding US line.
805 Midway Road
P.O. Box 578
Rockingham, NC 28379
TEL: [phone]O33
FAX: 9€0-895-9887
RE: Waste Characterization (Revised)
Dear Karen Bellamy: Order No.: 21050833
Summit Environmental Technologies, Inc. received 2 sample(s)on 5/14/2021 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
IF you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
: tief_4611
Holly Frorea
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 9 -O735,CaILljrn,a 2945,Celorado,Connxdcut PH-OI OR,Floridn NEiL AC LR7688,1¢pha OHOth 23,I ILincig 21E061,3hthanp C-UI(-13,!Camas
L-IOF347.KCaLw Ey{Undleegruund Storage Tank)3,Ksn[uelk 90I46.Mmlan.339,Michigan 99M,Minnewep 1730279,Nevada OHDR92321320•3,Ntw
Heeilxs bra 2996.hew_lusty OFI406,New York 1 L 777,North Celina 397a5 nr 63],N4v1h Dakuea R•261.Ohio!]W,Ohm\`Al`eLo152,CJklahonra
20I9•L5S,Oregon 01E20041}1, PenusykvanmU!I.Mode LelandLAOC43I7,SamhCnrolina92O1fi40I,T ca5T1P474144{r6-19•Lfi,kltahp1p104232L126•I2,
✓irginia V FLAP I OM 1,WesS Vinyme9957C
Page 1 of 12

Suterarrd E'ia+rrptrnmetuot Tec +eniogtes,fnr. Case Narrative
33lORF'rnSt_ CI'S1Y@
111.11 E#NfRON1.IEHTALTECKNQtpG1Fs.INC Cat}o1+oga Foil.s,(Moo dd 3 V4`€]! 1050833
knarytca!La oratorFac TEL;f3301 253- 211 FirX:[phone]
Websue'A�1p::Yw!wu.settek.rvue Date' $ $ 0 !
CLIENT: Cascades Tissue Group-North Carolina Inc
Project: Waste ataraeteri7atiOn(Revised)
WorkOrder Narrative:
This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical
Results, QC Summary Report, Applicable Accreditation Information, Chain-of-Custody, Cooler
Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc_, Work Order Number assigned to this report.
Summit Environmental Technologies, Inc,, holds the accreditationslcertifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analyzes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that or the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer For which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units,
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below,
Wot'kOrder Comments:
21050833: Report provided as a level I Data Package.
Revised report provided 08Juti2 I,
Sample ID for 21050833-00 I amended, reporting Limits for TCLP Pesticides for 2 1 05 08 3 3-0 02 were
corrected, and report split into two separate report per client request.
Revision v3
Page 2 of 12

li
LIMN'IT SanrrRai� irc�+r+or�reirrvl 7'c�el�irnlugf¢s.f�`. WOO: 21050$33
3310 Win SF.
in my EN1lIAD 4H 1IT#L t CHu*Wpaeg.iF�C L;ri.unhogu Feral O1�ro.14223 Dew R purl vi: 512512{421
algeir cs1LAbnraro+ TL'L;036j 25.1.11211 Fag:(3301253-.I489 Company: Cascades Tissue Group-North Carolina i
4Pe$.sue_hun:!iruw_serrek.rwn Address: a division ofCascadtis Holding US Inc.
Rockingham NC 28379
Received_ 5/1 4/202 1
Project/#: Waste Characteri
TCLP Metals Analysis(SW131116010)
Client UM Lab ID# Collected Analytc Rep Lnit Result Units Matrix Method DF RegLvI Ruff Analyst
Sludge 002 5/11/2021 TCLP Areenic(A5) 11500 ND mg/L Sludge EPA 6010 1 5.00 511912021 ON S
0
Sludge 002 5111/2421 TCLP Barium(83) 5.00 ND mg11_ Sludge EPA 6010 1 100 5/19121321 DNS
0
Sludge 002 51T1/2021 TCLPCadmium(Cd) 0.100 ND mg/L Sludge EPA 6010 1 1.04 5/19r2021 DNS
0
Sludge 002 5/1112021 TCLP Cl remium(Ct 0.204 ND mg/L Sludge EPA 6010 1 5 00 511912021 DNS
D
Sludge 002 5111/202't TCLPLead{Pb} 0.500 ND mglL Sludge EPA 6010 1 5.04 5/T0/2021 DNS
D
Sludge 002 5/11/2021 TCLP Setenium(Se) 0.0500 NO mg1L Sludge EPA 6010 1 1.00. 5/1.9/202'4 DNS
D
Sludge 002 5111/2021 TCLP Silver(Ag). 0.500 ND r11gIL Sludge EPA 6010 1 5.00 5/1012021 DNS
D
TCLP Mercury Analysis(SW1311/7470)
Client ICY Lab Ill# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst
Sludge 002 5/11/2021 TCLP Mercury 0.00200 ND mglL Sludge EPA 7470 A 1 0.200 5r2012021. ERA
TCLP Pesticides Analysis(SWIM 118081)
Client 1D# Lab ID# Collected Analyse Rep Lint Result Units Matrix Method ER" RegLvl Run Analyst
Sludge 002 5/11/2021 Chlordane,total 0.0250 ND mglL Sludge EPA 80818 10 0.0300 5/20/2021 POP
Sludge 002 5111/2021 Toxaphene 0.0500 ND mg/L Sludge EPA 8081E 10 0 500 512012021 PGP
Sludge 002 511112021 Endrirr 0.00540 ND mg/L Sludge EPA 808i6 10 0.0200 5120r2021 POP
Sludge 002 511112021 gamma-BHC Q.00540 ND mg/L Sludge EPA81]81B 10 0_400 5120/2021 PGP
Sludge 002 5111/2021 Heptachlor 0.00500 ND moll. Sludge EPA 8081E 14 0.00800 5,20/2021 POP
Sludge 002 511112021 Heptachlarepoxide 0.00504 ND mg/L Sludge EPA8081B 10 0.00804 5+20/2021 POP
Sludge 002 511112021 Methaxychlar 0.00500 ND mgri Sludge EPA 8081E t0 10.0 5120/2021 POP
Sludge 002 511112021 5urr;TCMX 10-119 82.9 %Rec Sludge EPA 80818 10 5f2012021 POP
Sludge 002 5/11/202'1 Surr DOE 10-119 g2.9 %Rec Sludge EPA 80816 74 512012021 POP
Page3of1

Sprang!'Eflvri-e pm i ra! ihrhnnlo res,bye.
:iiii SUMMI1- V4'O ZIUSIIR3
331�!Win,sr. Date Reported: 5.12SS/ZD I
EIMPONN>/iTAL t>Ettlimatontes.{gyp Cf+}Yri+pgo Ears,Ohio 44223
4Ra0pr?cal t¢barcor;es TEl,: WO)253421I FAX:OM)7534-49 Company: Cascades'Fissile Group-North Carolina 1
11 eb.sue:&rip:?vim.serfirtetand Address: a division of Cascades Holding US inc.
Rockingham NC 28379
Received: 5/14t202I
Projectf/: Waste Characters
TCLP Volatiles Analysis
Client ID# Lab !I)# Collected Analyse Rep Lint Result Units Matrix Method DF RegLvl Run Analyst
Sludge 002 5/1112021 1,1-Dichloroethene 0.250 ND mg1L Sludge ERA 8264D 50 0,700 5118/2021 SLY
Sludge 002 511112021 1,2-Dichloroethane 0,250 ND mg1L Sludge EPA 82600 50 0,500 5/1812021 SLY
Sludge 002 511112021 MEK 5.00 ND mg1L Sludge ERA 8260D 50 200 511812021 SLY
Sludge 002 611112021 Benzene 0.250 ND mg1L Sludge EPA 826OD 50 0.500 5118/2021 SLY
Sludge 002 5111/2021 CarbontetrachIortde 0.250 ND mglL Sludge EPA82600 50 0.500 5118/2021 SIN
Sludge 002 511112021 ClIoronenzene 2.50 ND mglL Sludge EPA8260D 50 100 511812021 SLY
Sludge 002 5111i202t Chloroform 0.250 ND mglL Sludge EPA82800 50 6.00 5118/2021 SLV
Sludge 002 5111/2021 Tetrechloroelhene 0.250 ND mgll Sludge EPA82600 50 0.700 511812021 SLV
Sludge 002 511112621 TrichI rer tiene 0.250 ND eng1L Sludge EPA 826010 50 0,500 511812021 SLY
Sludge 002 511112021 Vinyl chloride 0.100 ND mglL Sludge EPA82€4]D 50 0.200 511812021 SLV
Sludge 002 5/1112021 Surr.4- 70-130 56.3 %Rec Sludge EPA 87800 50 5/18/2021 SLY
8romaluerobenzene
Sludge 002 5/1112021 Sum 70-130 99.5 %Ree Sludge ERA 82600 50 5f18/2021 SLY
Dibrarnonulremetl73r1B
Sludge 002 511112021 Sum Tpluerte-d0 70-130 99.1 %Reo Sludge EPA82fi0D 50 511612021 SLY
T LP Semi-Volatiles Analysis(8W 1 3 1 118270)
Client 11)tt Lob lDN Collected Anulyte Rep Lint Result Units Matrix Method Dr RegLvl Run Analyst
Sludge 002 5/1112021 1,4-Dichlorobenzene 0.200 ND mg1L Sludge EPA 6.270E 2 7-50 5/1912021 SFG
Sludge 002 51t112021 2,4,5-Trlchlarophen0l 0.500 ND mg1L Sludge EPA 8270E 2 400 5/1912021 $FG
Sludge 002 5511112O21 2,4,6-Trichlaropl''enal 0-500 ND rrng/L Sludge EPA 8270E 2 2 00 511912021 S .G.
Sludge 002 8f1112O21 2,4-Danitrololuene 0.100 ND mot Sludge EPA 8270E 2 0.130 511012021 SFG
Sludge 002 511112021 CresOIS,total 10.0 ND mglL Sludge EPA 8270E 2 Z06 511512021 SFG
Sludge 002 511112021 Hexed-kor.1,3- 0.0460 NO mg1L Sludge EPA 8270E 2 0.500 511512021 SFG
butadiene
Sludge 002 511112021 Hexachloiohenzene 0.100 ND mgfk Sludge EPA 8270E 2 0.130 511912021 SFG
Sludge 002 5111r2021 Hexachlaroethene 1.200 ND mgA Sludge EPA 8270E 2 3.00 511512021 SFG
Sludge 002 5111/2021 Nitrobenzene 0.200 ND mg1L Sludge EPA 8274E 2 2.00 5/1912021 SFG
Sludge 002 5/11/2021 Pentachlarorthenol 0.500 ND mg+l. Sludge EPA 8270E 2 100 511 g12021 SFG
Sludge 002 5/11/2021 Pyridine 0,500 ND mg/L Sludge EPA 5274E 2 5.00 5/191202t SFG
Mudge 042 511112021 Sum 2-Fluaraphennl 10-157 71.4 %Rea Sludge EPA 9270E 2 5/19/2021 SFG
Sludge 002 5/11/2021 Surr; Phenol-de 10-169 77.6 %Rec Sludge EPA 8270E 2 511512021 SFG
SEudge 002 5I111202'l Suer; Nitrobenzene- 32.1-130 77.0 %Pen Sludge EPA 8270E 2 511912021 5FG
d5
Sludge 002 515112021 Surr; Z,4,8- 45.4-166 123 ° Rec Sludge EPA 8270E 2 5/19f2021 SF13
Tribromophenc l
Sludge 002 5/11/2021 Surf: 2- 35.7-130 83,6 %Rec Sludge EPA 8270E 2 5115/2021 SFG
Fluarnhipneriyl
Sludge 002 511112021 Suer.p•Terphenyl- 70-145 105 %Rec sludge EPA 8270E 2 5/1912021 SFG
d14
Page 4 of 12

•
54 �� Sr+++r�r++f reciornlores,fx4c. V{ 21050833
IT
EHVIR41tMf##Tr4L TECH Oi aoi #,i lc C'+r}rrFrn{a Fairs,Oho �123 Date Rep4lnted; 51 512.021
um rreyficie Laboranor?ei TEL {3317)?$J- 21 r r.a.x:r3JO)253449 Company: Cascades Tissue Group-North Carolina 1
ilEakfi+fe:h+fiP=.':.irseu.setrek.err1.14 Address; a division of Cascades Holding US Inc,
Rockingham NC 28379
Received: 5/14/2021
Profectk Waste Characteri
TCLP Herbicides by EPA 8321E
Client ID# Lnb 11M Collected Annlyte Rep Lit Result Units Matrix Method C1F RegLvi Run Analyst
Sludge 4 02 5i11)2021 2,4-D 0.50tf h#d mg/L Sludge EPA 8321e 54 t4.O 5/2 31 20 2 1 TM
Sludge 002 5f1112421 2 4.5-TP 0.50U NO mgiL Sludge ERA 8321E 50 1.00 5/2312021 TM
Sludge 1)02 511112021 $urr. 2.4- 70-t30 101 %Rec Sludge EPA 0321E 50 512312021 TM
dichlor4aphenylacetir
acid
Page 5 of 12

S I. MM IT tiSNN7J1r11 Fr1VrlrJMJNenra1 rtlC�rlil0r; ;. Sr
IIal tical Report
r 33 in Win Sr.
1.7111111.
ENVIRONMENTAL ItemotoniFS,INC C1ry+t+i+rlga Falls,Ohio,314223 (L'0115{FI I{lil[dL�r
il.rtmilert.e7N L -fin rvrrc-E TEL(330 253-E211 FAX:[phone] WON: 21050833
Wabsiee:hrepjelvw1i erre*.ro Datc Rcp3arlext: 5125l2021
CLIENT: Cascades Tissue Group-North Carolina Inc Collection Date: 5/1112021 6:12:00 AM
Project: Waste Characterization (Revised)
Lab ID 21050833-002 Matrix: SLUDGE
Client Sample ID; Sludge
Analyses Result PQL Qua Units OF Date Analyzed
RCI S AID-Wf IGNITABILITVI030 SW9044 Analyst: MS
REACTIVE CYANIDE(901417.3.3_2)-SOLID
Cyanide, ReaGnra ND 0.185 m91K9 1 511712021 1:51:00 PM
RCI-SOLID-Wi IGNITABILITY1030 SW1030 Analyst: ALT
!GNITABILITY OF SOLIDS ISW-846: 1030)
I0rlitability rnonflammable mmisec 1 512112021 12;23:11 PM
RCI-SOLID WI IGNITABILITY1030 SW9046D Analyst: ALT
PH(SW9045D)
pH 6.8 s.t.I 22 6( 4 5/1812021 3:57..48 PM
RCI-SOLID-W1[GNITABFLITY1430 SW9034 Analyst: MS
REACTIVE SULFIDE I9034}17.3.4.2
Sulfide, Reactlwa ND 2.5 7 nylku t 5/1712021 1:51:00 PM
QwdiI1Er,' k Aldan sires fa prararaliun QF m 136.xsttsOe<I M 1W,aui lmarAieffi W11.0dea runt arearagporar
ND i c Waled %. Frerrm Limn
RL Repurlinit Ni l-nm W Snrret[pru,uner snrQaaurc a out orlimM a specified al krs#cwla
Revision v2
PagfS 6 of 12

7.74 S
MM'T S,oa,rjrriEi7,irnrruvurrfaf reolntDtofgr0arIYs-lIet{ Qualifiers and Acronyms
EFivin
Arty KRtIihITfL marl h(�1I0r3iEt#,rye Cuyahoga Fag'.Neu.3 7: ; Zl45flffi33
Arat}*raf Lasarasa+Y a TEL,(3311 23.3-2f1 f'.f,Y:(t,f+)1?5.3-4-/+I
II'absitr: :;«+1ar.seuek.co Dow; 51�ilZ41 t
F
These commonly used Qualifiers and Acrot]ynas may or may not be present in this report-
Quxlifrcn
1.' The compound was analyzed For but was itot detected.
t [he reported value is greater than the Method Detection Limit but less than the Rep dilig Limit.
3l Alta hold time for sample preparation and/or analysis was exceeded.
D The result is reported Irani a dilution.
E The result exceeded the linear range of the calibration or is estimate[due to interference.
MC Tile result is below the Minimum('ornpound Limit.
The result exceeds the Regulatory Limit or Mdximuttn Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
• The result is presumptive based oa]at Mass Spectral library search assuming a I:I response.
P The second column con runt a;ion exceeded 25%difference.
C The result has been confirmed by GUMS-
X The result was cot confirmed when GC/MS Analysis was perfornted-
B./MB+ The analyte was detected in the associated blank.
G The ICE#or CCB contained reportable amounts of ana[yte.
QC4t- 'The CCV recovery failed low(-I or high(f},
RIQDR The RPD was outside of accepted recovery limits-
Q Ldf The I,CS or LCS D recovery failed law(-}or high{+}.
Q1.R The E-CSJLCS[)RP[}was outside of accepted recovery limits,
Q.11-f+ The MS or MSL)recovery tailed low{-}or high(+),
Q:IR The MS/MSD RPD was outside of accepted recovery limits-
QV-/} The [CV recovery tailed]ow{-}or high(+)-
S The spike result was tilts ide of accepted recovery Limits.
7 Deviation.:A deviation from the method was performed;Please refer to the Case Narrative For
additional information
Acronyms
ND Nat Detected U. ReportmgLimtt
QC QualityConrrot IDL Method Detection Limit
NIB Method Blank LOB Level of Iktcction
LCS 1.uhoratory Control Sample I.OQ Level of Quantitat ion
LCSD Laboratory Control Sample Duplicate PQI. Practical Quarititation Limit
QCS Quality Conirnt Sample {'RQ[. Contract Required Quentiiation t,inut
Ul.'P Duplicate PC. perm itl-Im!l
MS Matrix Spike RegLvI Regulatory Limit
MSD Matrix Spike Duplicate •1ICl. MaN imum Contamination UM it
RPD Relative Percent Different lllaf'l. Minimum Compound Limit
ICV ]nitial Calibration Verification RA Reanalysis
ICi3 initial Calibration Blank RE Revitraci ion
CCV C'oniinuing Calibre ion Veritieutiurt TIC Tentative]} identified Compound
CCB Cont inuiog Cal ibrat ion Blank R-I Retention Time
RI.C: Reporting LimitCheck CF Calibration Factor
OF mho ion Factor RE Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Revision v2
Page 7 of 12

SUMMIT
Smwwlir£rriraour#a:fcrlT'srlalr;afaagres,la:r. l c'Creditation program,wi rF .U10 Win Sr-
RcNhlENTAL TEi E faaw esi,ioic Crow hogu rah's.Ohio 4-L 23 AR bytes Report
er
�M
Pirhe++lcw11 Latonifarillr Tt.L:War 2534111 FAX:(3_00 5J-4489 WOif: 21 05).413
treb. i4:Ir p:'•u'iiwv,settek.com 98-Jrrl2-21
Client: Cascades Tissue Ciroup-North Carolina Inc state: NW
Project: Waste Characterization(Revised) Program Name: N _WW_ CM
— —Tesi NP0Le Matrix Analyse Status
1gnLtubility of Solids(SW-8,16 I030) sludge IgnLLRbEIi1y A
pi'L(SW90450) Sludge Hydrogen Ion(pH) A
Rcactive Cyanide{9014r7.3.3.2)•Sohtd Sludge Cr nide,Reariive U
Reactive Sulfide{90307.3.4.2 Sludge Sulfide,Reaeuse U
TCLP[Herbicides by EPA 8321 L Sludge 2,1,5-TP A
TCLP Herbicides by EPA 832i13 Sludge 2,4-1) A
TCLP Mercury.Analysis(SW 13I Lf7470) Sludge Mercury. A
TCLP Meals Analysis(SW 133 IMi31O) Sludge Arsenic A
TCLP Erlerat5 Analysis(SW 13I 1/6010) Sludge Barium A
TCI.P Metals Analysis(SW 13l 1f6010) Sludge Cadmium A
TCLP Metals Analysis(SW 13L 1115010 Sludge Chromium A
TCL?E4tetals Analysis(SW13I 3/60E0) Sludge Lead A
TCLP Metals Analysis(SW 13I I/64LCI) Sludge Selenium A
TCLP Metals Analysis(SW 13I 1160L0) Sludge Silver A
TCLP Pesticides Ana[ysis(SW I3IIf1S1] L1 Sludge aluerdane,soca! A
TCLP Pesticides Analysis(SW13L 1'808I) Sludge Endnn A
TCLP Pesticides Analysis(SW13IIiR08I) 5Iktdgc gamma-BF[C A
IC LP Pesticides Analysts(SW 131 I AGO I) Sludge Hepiachler A
TCLP Pesticides Analysis(SW 13 111808 I) Sludge I lepsachtor epoxide A
TCLP Pesticides Analysts(SW 13 I I iROS 1) Sludge Me1IrgxyehFor A
TCLP Pesticides Analysis(SW 13 I I l8U8 I) Sludge Tuxaphene A
TCLP Semi-VolatilesAnalysis(SW 131L1827[1) Sludge 124-Drchlorobenzerae A
TCLP Semi•VolatiLes Analysis(SW13I L182709 Sludge 2,4.,5•Trichtoropheiaol A
TCLP Semi-VatatiLes Analysis{SW 131 LJ82709 Sludge 2,4,6•TrichLorophenei A
TCLP Semi•VolaLiles Analysis(SW 13I 118270) Sludge 2,4•DLnasrotattsene A
TCLP Semi-Volati les Analysis(SW 131 U8370) Sludge Cresols,Tosal A
TCLP Semi-Volatiles Analysis{SWI 31 I/8270) Sludge Ficxachlo30ben,cne A
TCLPSemi-Volatiles Analysis(SW I31I/S27I)) Sludge Hexarhburobutudi nL: A
TCLP Semi-Volutiles Analysis(SW 131 I/82.70) Sludge I low liloraeshane A
ICI.PSemi-VolatilesAnalysis{SWI31Lfilm) Sludge Nitrobenzene A
TcLP Sum i-Volatiles Analysis{WI 3]L182713) Sludge Pentachlorophenoi A
'CC LP Semi-Volatiles Analysis(SW13]Li 270) Sludge Pyridine A
Key Key
N WW SCai A Accredited NC WW SCM U Unavailable
Version#3
Page 8 at 12

SUMMIT
Srfrx,arr +nrl T3310 ,In . Accreditation Program
33`r,i►.inc... Ana! tes RepoReport
M IMI EHVFRON NrfL t1 CNNM,OWES,INC (;,r4�rrrQ �r rf:�rs,Ohio d �s
dra1}r1 !LabornParfas T1EL:(Ur 13 T-$2�fi FAA': 330J 253--U& WOi; Z It75OJ}333
li2ch-s++e:hilly'Avii'Ii..,senek,cv+1 08-Jurw 1
Client: C cadesTissue Group-North Carolina Inc State: NW
Project: Waste Characterization(Revised) Program Name; NC_WW_SCM
fist Name Prlarrix A natyge States
TCLP Volatiles Analysis Sludge 1,I-Dichloroelhene A
'CC LP Volatitns Analysis Sludge I,2-Dichtoroethane A
TCLP Volatiles Analysis Sludge 2-Rutanane rk
TCLP Volati les Analysis Sludge Benzene A
1'L;LP Volatiles Anulyyis Sluc,ge Carbon tetrachloride A
TCLP Volaiilea Analysis Sludge Chlorobenzene A
TCLP VolauJes Analysis Sludge chi vague A
ICU'Volakilo Analysis Sludge Tetrachlorc Ihena A
TCT-P Volatiles Analysts Sludge ']'richJarontlrrme: A
TCLP Voiatj Icl.Analysis `nudge Vinyl chloride A
-
Ey -- — - —Key
T ( WW SCfw1 A Accredited NC 1WW SC'}.1 L' Uu available
Version U3
Page 9 of 12

UCAJ.k4'uf'#31 rcv 4.1
5r SUMMIT r 11 l}'Sl3 Yi]II€5 �l8i1t O Custody p+ra
1 i �IFenhcsiton1TAL TtCNMQLd tE$,MC_ k g.cm
r+�
334GY11nSnrN � Fr �
On up FOR OO44223 ■■tree 1u It nu'and Covddw rP a!sn.rilaatc IMI WO II
800 216ak141 M0. *' ( 6
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i Page 1 of 1

S
�� T SYAHNNJd f NVfYriJllNpNfO1 Technologies,fN r.
331 R f F iJo St.
SEI ENVIRONMENTAL Te ilN,t mfYES.+RC ChWhOggr Facts.Ohrr,d 22 Sample Receipt 1Checklist
Jff rFJr1l11�C✓ff CohoJ'�IfoJYpw' 71EL. (330j 253-J 21 f F.-JX. (330)233.dd$9
I►sbsete,p r:riIvww.sertek-go+Jp
Clienl Name CAS-NC-79379 Work Order Numucr 21050933
RcptNo: 1 Dale and Time Receive 5f1412021 Ti.: 5:00 AM Received by• Christopher 5tofen
r
Completed by Reviewed by: (4104.14. t,4eh
Completed Data: 5/14/2021 11:17:2 J AM Reviewed Data: 5f17121]21 8:12;918
Carrier name; Summit
Chain Of CUSivdy present? Yes ve No
Chain Of CUStOdy Signed when relinquished and received? Yes !, No
Chain of custody agrees with sample labels? Yes *T No Not Present
Are mstriCe5 barrectly identified on Chain of custody? Yes *T No
is i1 cleat want analyses were requested? Yee * No
Custody seals Intact on sample bn11las? Yes Np Nol Present V
Samples to proper conlalnerrbottle? Yes No +l
Were correct preservalives used and noted? Yes +f No NA
Sample containers intact? Yes V No
Sufficient sample volume for Indicated lest? Yes ' No
Were Container tables complete(ID,Prea, Date}? Yes vs No
All samples received within hording time? Yes d NO
Was an attempt made to coat the samples? Yes w/ NO NA
Alr sarngres received at a temp.or 0°C to 6.0*C? Yes No NA
Response when temperature is outside of range-
Preservative added to bottles;
$ample Temp.taken and recorded uRnrr r eipl? Yes + No 0 To O C
Water-Were bubbles absent in VOG vials? Yes No No Vials
Water.-Was knave Chlorine Present? Yes No NA
Water-pH acceptable upon receipt? Yea Na NA d
Are Samples CanSitlered aGtepkebte? Yes ' No
Custody Seals present? Yes No *'
Traffic Report or Packing Lists preseni? Yea No d
Ai-bill of Slicker? Air 9i1l n' S1rcker Not Present
Airbill No:
Sample Tags Present? Yes No '
Sample Tags Lisled on COC? Yes No d
Tag Numbers:
Sample Condilioe? Inlaci Broken Leaking
Case Number. SOG: SAS:
J
Arajusloc? Checked by
Any No andfor NA not applicable}response musk be detailed in the comments section be
Page 11 of 12

MM IT 3jrrnrn t Environmental6CINr4�4"ies, ffJC.
girl U 3fI0k'rn„
TtCIANGLOMES,rrrc (uyahr�gerFaffa,Ohrvd+J223 Sample Receipt Checklist
mom ARiinytice LDtiCTMOIles TEL: (33O)25342.0 i TAX:[phone]
Washy:bete.Iwh.•sw.serrA.eong
Client Contacted Yes No NA Person COnt$Cied; Cammenls:
Cantact Mode: Phone: Fax: Person: Samples reCd in plastic bags
�9rtit In81nUCtiOn5:
bate Contacted: COntni.ed 8y
Regarding:
CerractiyeAOlian:
Page 12 of 12

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Maine: Cascades Tissue Group-North Cara[ina,a division of ►N0009477
Cascades Holding US inc. WQ Permit Number:
TP Name: _ ' ' NPDES Number:
El-
Monitoring Period: From 1 r1 f202 I To [2f 91202I
Pathogen Reduction (15A NCAC 02T .11116) - Please indicate level achieved and alternative performed:
_ Class A: Alt. A (tin;eltcmp) 0 I Alt B (Alk Trcatrncnt)Q I A It. C (Prior Tcstiug)U
Alt,D (No Prior Test) ❑ Process to Further Reduce Patlumcngs ❑
If applicable to alternative performed(Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑ I lent Irving Q I Heat Treatment 0Tlielmaplii1ic 0 j
CI Ray Gamma Ray 0 Pasteurix.atitni G7
Class B: IAlt. (1) Fecal Density ❑ I Alt_ (2) Process to Significantly Reduce Pathogens ❑ I
If applicable to alternative performed(Class B only) indicate"Process to Significantly Reduce Pathogens":
Limns Stabilization ❑ I Air Drying 0 I Composting ❑ (Aerobic Digestion Ga
Anaerobic Digestion ❑
If applicable to alternative ii..rformed (Class A or Class B) complete the following monitoring data: ;
Pathogen Density Number of Analytical
Parameter Allowable Level lwxcee- Frequency Sample Tech-
in Sludge Minimum Geo. Mean Maximum Units deuces of Analysis Type niq�le
2 x t 0 to the MPN NA NA
Pith power I
per gram of
Fecal Coliform total solids CPU 1 fA A
1 000 inpn per gram
of total solid (dry NA NA
weight) ,
Salmonella bacteria 3 MPN per 4 grams .00c ►e--
(in lieu of fecal total solid{dry NA NA
coliiorm] weight) ' 44fr-. I
Vector Attraction Reduction (ISA NCAC 02T .11107) - Please indicate alternative performed: _
A Li.I (VS reduction) ❑ Alt. 2(40-day bench) ❑ A]t. 3 (30-day bench) ❑ A]t. 4 (Spec. °2 uptake) ❑
Alt. 5 (i 4-Day Aerobic) 0 .It 6(Alk. Stabilization Q I Alt 7 (Drying- Stable) ❑ Alt. 8 (Drying- Unstable) 0
Alt. 0(injection) 0 Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
ERIF1ATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty ot`law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction r4. uirement in 15A NCAC 02T .1107 have been met."
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02,T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
Iv if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there arc
significant penalties for false certification including tine and imprisonment."
Karen V. Bellamy Environmental Manager Duke Goodwin Project Manager
Prepay Name and Title ( .pe or print) Land Appl i am d Title (if applicable)(type or print
ur /A4
S gnature of Preparer* Date Signa i of Land Applier(if applicable) a
MPreparer is defined in 40 CFR Part 503.9(r) and I SA NCAC 2T .1102(26)
DENR FORM PVRF 02T (1212006)

Cascades Tissue Group-North Carolina
A Division of Cascades Holding US fnc,
805 Midway Road,Post I 0 Boot 578
CascadesRockingham,NC 283N USA
Phone: [phone] Fax; [phone]
Date: Jan 31, 2022
From: Karen Bellamy
Cascades Tissue Group-North Carolina, a division of Cascades Holding US Inc_
Po Box 578 805 Midway Rd,
Rockingham, NC 28380
Phone [phone]-Ext 74280
Fax [phone]
Email: Karen Beilarmv(cC Dascacdes, om
Permit: WQ0009477
Subject: Fecal Testing
Cascades Material is a lime material, so we don't perform vector reduction.
Should your office have any question please contact me at the above nufnbers or email.
Karen V. Bellamy
Environmental Manager
Cascades Tissue Group-North Carolina, a division of Cascades Holding US Inc.