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WQ0001048_Residual Annual Report 2021_20220216
Non -Discharge Branch Upload/Submittal Form NORTH CAROLINA EnvironmentalQuul1ty Version 2 - Revised June 23, 2020 Initial Review Reviewer Thornburg, Nathaniel D Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Year* Permit Number (IR) * Applicant/Permittee Email Notifications Does this need review by the hydrogeologist? * Regional Office CO Reviewer Admin Reviewer Annual Report Residual Annual Report Additional Information Other 2021 WQ0001048 Contentnea Metropolitan Sewerage District Yes No Washington Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Charles M. Smithwick, Jr. Email Address* crosd100@embargmail.com Project Information Application/Document Type * New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 2525245584 O Modification - Minor O Renewal O GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type: * Permit Number:* Wastewater Irrigation Other Wastewater Closed -Loop Recycle Single -Family Residence Wastewater Irrigation WQ0001048 Has Current Existing permit number Applicant/Permittee Address* P.O. Box 477 Grifton, NC 28590 Facility Name* Contentnea MSD Class B Residuals Program Please provide comments/notes on your current submittal below. 2021 Sludge Land Application Report for the Contentnea MSD Permit No. WQ0001048 High -Rate Infiltration Reclaimed Water Residuals Other At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. * (Application Form, Engineering Plans, Specifications, Calculations, Etc.) 20220216122854772.pdf 7.92MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature C...f.�tlaF Submission Date 2/16/2022 ANNUAL LAND APPLIIjCATION CERTIFICATION FORM WQPermit#: tijQCCOOE. County: YI4'TLYear: 607.-) Facility Name (as shown on permit): COnie '1R.ifY Land Application Operator: Chaff -orn&Oc a - Phone: Z S.Z4; V-- Land application of residuals as allowed by the permit occurred during the past calendar year? ❑ Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in the permit: 76 Total number of fields utilized for land application during the year: d j Total amount of dry tons applied during the year for all application sites: fa 11 I) Total number of acres utilizes for land application during the year: 1.jq. (p 5 Part B - Annual Compiance Statement: Facility was compliant during calendar year ZbZj with all conditions of the land application permit (including but not limited to items 1-I3 below) issued by the Division of Water Resources. ❑ Yes El No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and renrediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowhig violations." (fin 11,f5M .5^41-hld etick AYbPAW Pennittee me and Title (type or pr t) Signature of Pernittee ' Date ild.J.1 d .2 yL Ycr.7a Signature of Preparer* Date Signature of Land Applier Date (if different from Pennittee) (if different from Pennittee and Preparer) * Preparer is defined in 40 CFR Part 503,9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) EXPLANATIONS FOR DEVIATIONS FOR THE 2021 ANNUAL SLUDGE LAND APPLICATION REPORT 10-20-21 Monitoring Well #15 Total Organic Carbon Total Chromium 10-20-21 Monitoring Well #18 Total OrganicCarbon 11.22 mg/L 20 ug/L 11.42 mg/L The TOC in this area naturally runs higher. The water table was very low at the time samples were taken, and there was quite a bit of sediment in the wells. This contributed to the higher Total Organic Carbon and the elevated Chromium in Monitoring Well #15. The monitoring wells were bailed extensively and Monitoring Well #15 was resampled for Chromium. The results were well within established limits. CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIUICATION AND SUMMARY FORM WQ PERMIT #: L)Q0001,01.44 FACILITY NAME:Clef)-} y1 P PHONE: z5-57.4%,4 COUNTY: 4 OPERATOR: e [le6 ). }( ;Tf - FACILITY TYPE (please check one): rzi Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ❑ Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes $ No ❑ --+ If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment) Bulking Agent Residual In Product Out w Names () (dry tons) VolumeIntended use(s) ( ) January February March April May June C.i11 7j k)( t--LCzi-P 1z• 4 July CYDO 114.VP CfD3 )) Z') -44 ) August C1Tla7 tt)iu t`✓37‘5)) 7L .u,55 September October November December Total from FORM DMSDF (sup) Totals: Annual (dry tons): {o j .1 fri Amendment(s) used: Bulking Agent(s) used: DMSDF (Supp) * If more space is required, attach additiolvi information sheets (FORM DMSDF (supp)): Total Number of Form art C: Facility was compliant during the past calendar year with all conditions of the land application permit ❑ Yes (including but not limited to items 1-3 below) issued by the Division of Water Resources: it No ► If No, Explain in Narrative 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." daA Signature ofPeranittee Date **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) a3'4 Signature of Preparer* * (if different from Pennittee) 27L:42_2_ Date DENR FORM DMSDF (1212006) RESIDUAL SAMPLING SUMMARY AND LAB REPORTS ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: 04)e0C3 1046 Facility Name: (yen- .0-4,n6a m6,7) Residual Source WQ # or NPDES 1#: WWTP Name: Residual Analysis Data Crreneo rf ) Laboratory: I) Err I rOr -..Z1 frc . 2) 3) 4) 5) Parameter (mg/kg) Ceiling Conc. Limit Sample or Composite Date .-fl-Z.J v Percent Solids (%) NA 1. (4,Zi Arsenic 75 < 2.5 Cadmium 85 l.5 Copper 4,300 Z(A`Z, Chromium NA t 43 Lead 840 2_1 Mercury 57 0.31p Molybdenum 75 G,'Z- Nickel 420 11 Selenium 100 S6._0 Zinc 7,500 53P1 Total Phosphorus NA &Ja) TKN NA tlicotab Ammonia -Nitrogen NA MI ! 1 Nitrate and Nitrite NA 1)32,1 g posai racuxues the telling concentration Iiz .its listed in this form are not applicable Reference the individual permit for metals limits. "Y certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penaltie or submittincr false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer *Preparer is defned in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) .27g:24S.2- Date DENR FORM RSSF (12/2006) �.. ' `'52 7:56-620 GRE ENVIL,LE. I\I.G. 2 Th8 FAX (252) f 56-06 3 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON, NC 26530 PARAMETERS Sludge Analysis Method Sample Date Analyst Code PH (not to be used for reporting) 3,6 05/27/21 DIJ 4500HB-11 Aluminum, (dry wt. basis), mg/kg 15981 06/04/21 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg <2.5 06/04/21 MTM 3113E-04 Calcium (dry wt. basis), mg/kg 16143 06/04/21 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg 1.5 06/07/21 MTM 3113B-04 Copper (dry wt. basis), mg/kg 262 06/04/21 LFJ EPA200.7 Chromium, T.(dry wt. basis),mglkg 18 06/04/21 LFJ EPA200.7 Lead (dry weight basis), mg/kg 21 06/04/21 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 6364 06/04/21 LFJ EPA200;7 Mercury (dry wt. basis), mg/kg 0.36 06/21/21 MTM EPA7471B Nickel (dry wt. basis), mg/kg 17 06/04/21 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 8137 06/11/21 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 06/07/21 MTM 3113B-04 Sodium (dry wt. basis), mg/kg 3279 06/14/21 NAB 3111B-11 Zinc (dry wt. basis), mg/kg 839 06/04/21 LFJ EPA200.7 Sodium Adsorption Ratio (calc) 5.5 Total Nitrogen, mg/kg (calc) 46792 06/22/21 Total Solids, % 2.04 06/02/21 CAW 2540G-11 TKN (dry wt.), mg/kg c 46060 06/02/21 TLH 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 1111 06/04/21 KES 350.1 R2-93 Nitrate Nitrogen(dry wt.), mg/kg c 730.2 06/03/21 KES 353.2 R2-93 Nitrite Nitrogen(dry wt.), mg/kg c 1.98 06/02/21 TLH 353.2 R2-93 Phosphorus, T. (dry wt.), mg/kg c 24900 06/02/21 KES 365.4-74 Molybdenum (dry wt, basis), mg/kg 9.2 06/09/21 MTM EPA200.7 ID#: 416 DATE COLLECTED: 05/27/21 DATE REPORTED : 06/23/21 REVIEWED HX: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. % SOLIDS, TOTAL SOLIDS, and TOTAL VOLATILE SOLIDS ANALYSIS BY: SAMPLE IDENTIFICATION DISH NUMBER A. WEIGHT OF DISH,gm .53 f Be WEIGHT OF DISH AND SAMPLE,gm 38',4- -k C. WEIGHT OF DISH DRY SOLIDS,gm *3_1(-; Do WEIGHT OF DISH AND ASH,gm E. VOLUME OF SAMPLE,m1 % SOLIDS, % t ,Loa- .* TOTAL SOLIDS,g/1 *** TOTAL VOLATILE SOLIDS 9,S Lc * % SOLIDS}% = C-A X 100 DATE:L-16'C) TIME: 15 Pi COI C ec.-1-f C 1€ end o-f dry ryt h a 1 l -he( a nc 1()6 i 3 iJc cel l Deb Z �DT3 ikkalr(6 -,:)1(Adce_ acyclrn a 4 j no! ((Waif i(-- c cL elf b- [c ) `)L) Z� TCLP LAB REPORTS The results set forth herein are provided by SGS North America Inc. Technical Report for Environment 1, Inc Contentnea Metro Sewage District; Grifton, NC 416 SGS Job Number: FA86015 Sampling Date: 05/27/21 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 abrown@environmentlinc.com ATTN: Ann Brown Total number of pages in report: 14 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. e-Hardeopy 2.0 Automated .Report Norm Farmer Technical Director Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), Nd(FLO02), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(TI04704404), PA(68-03573), VA(480177), AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, UT, VT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 SOS is the sole authority for authorizing edits or modifications to this document. Unauthorized rmidif cation ,sr this report is strictly prohibited, Review standard terms at: http:t!ww re.sgs.comferifte.rnts-and-co€tditions Please share your ideas about how we can serve you butter at: E-llS.US,CtistouterCare!a sgs.eoni 1 of 14 FAa8a15 Sections: Table of Contents -1- Section 1: Sample Summary 3 Section 2: Summary of Hits 4 Section 3: Sample Results 5 3.1: FA86015-1: SLUDGE SAMPLE 6 Section 4: Misc. Forms 12 4.1: Chain of Custody 13 SGS 2 of 14 EAa6ni5 SGS North America Inc. Sample Summary Environment 1, Inc Contentnea Metro Sewage District; Clifton, NC Project No: 416 Job No: FA86015 Sample Collected Matrix Number Date Time By Received Code Type Client Sample ID This report contains results reported as ND = Not detected The following ail) Organics ND = Not detected above the MDI. es: FA86015-1 05/27/21 11:25 AE 05/29/21 SO Sludge SLUDGE SAMPLE Soil samples reported on a dry weight basis unless otherwise indicated on result page. 3 of 14 FA88815 Summary of Hits Job Number: FA86015 Account: Environment 1, Inc Project: Contentnea Metro Sewage District: Grifton, NC Collected: 05/27/21 Page 1 of 1 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA86015-1 SLUDGE SAMPLE Corrosivity as pH Ignilability (Flashpoint) a (a) Not ignitable. 5.3 > 200 su SW846 CHAP7 Deg. F SW846 1010A MOD ill 4 of 14 FA86015 Sample Results Report of Analysis .;1111:1 5 of 14 FA86(115 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA86015-1 Matrix: SO - Sludge Method: SW846 8260E SW846 1311 Project: Contentnea Metro Sewage District; Grifton, NC Date Sampled: 05/27/21 Date Received: 05/29/21 Percent Solids: 2.0 Run #1 Run #2 File ID DF Analyzed By C0149319.D 10 06/10/21 18:58 SO 06/02/21 14:00 OP85689 VC6019 Prep Date Prep Batch Analytical Batch Run #1 Run #2 Purge Volume 5.0 m1 VOA TCLP List CAS No. Compound TCLP Leachate method SW8461311 Result IOW# MCL RL MDL Units Q 71-43-2 Benzene ND D018 0.50 0.010 0.0031 mg/I 78-93-3 2-Butanone (MEK) a ND D035 200 0.050 0.020 mg/I 56-23-5 Carbon Tetrachloride t' ND D019 0.50 0.010 0.0036 mg/1 108-90-7 Chlorobenzene ND D021 100 0,010 0.0020 mg/I 67-66-3 Chloroform ND D022 6.0 0.010 0.0030 mg/1 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.010 0.0026 mg/1 107-06-2 1,2-Dichloroethane ND D028 0.50 0.010 0.0031 mg/1 75-35-4 1, I-Dichloroethylene ND D029 0.70 0.010 0.0032 mg/I 127-18-4 Tetrachloroethylene b ND D039 0.70 0.010 0.0022 mg/I 79-01-6 Trichloroethylene ND D040 0.50 0.010 0.0035 mg/1 75-01-4 Vinyl Chloride ND D043 0.20 0.010 0.0041 mg/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 101% 83-118% 17060-07-0 1, 2-Dichloroethane-D4 107% 79-125% 2037-26-5 Toluene-D8 99% 85-112% 460-00-4 4-Bromofluorobenzene 99% 83-118% (a) Associated CCV outside of control limits low. (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound sus 6 of 14 FABGUi 5 Matrix: Method: Project: SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample .(D: SLUDGE SAMPLE Lab Sample ID: FA86015-1 SO - Sludge SW846 8270D SW846 3510C Contentnea Metro Sewage District; Grifton, NC Date Sampled: 05/27/21 Date Received: 05/29/21 Percent Solids: 2.0 Run #1 Run #2 File ID DF 91013141.D 1 Analyzed By Prep Date Prep Batch Analytical Batch 06/04/21 21:36 WH 06/04/21 08:20 OP85734 S91471 Run #1 Run #2 Initial Volume Final Volume 100 xnl 1.0 ml ABN TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 95-48-7 2-Melhylphenol ND D023 200 0.050 0.0056 mg/l 3&4-Methylphenol ND D024 200 0.050 0.0098 mg/l 87-86-5 Pentachlorophenol ND D037 100 0.25 0.050 mg/I 95-95-4 2,4,5-Trichlorophenol ND D041 400 0.050 0.0074 mg/l 88-06-2 2,4,6-Trichlorophenol ND D042 2.0 0.050 0.0075 mg/I 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.050 0.0050 mgll 121-14-2 2,4-Dinitrotoluene ND D030 0.13 0.050 0.0081 mg/I 118-74-1 Hexachlorobenzene ND D032 0.13 0.050 0.0069 mg/I 87-68-3 Hexachlorobutadiene ND D033 0.50 0.050 0.0050 mg/I 67-72-1 Hexachloroethane ND D034 3.0 0.050 0.016 mg/I 98-95-3 Nitrobenzene ND D036 2.0 0.050 0.0093 mg/l 110-86-1 Pyridine ND D038 5.0 0.10 0.020 mg/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 25% 14-67% 4165-62-2 Phenol-d5 19% 10-50% 118-79-6 2,4,6-Tribromophenol 69% 33-118% 4165-60-0 Nitrobenzene-d5 56% 42-108% 321-60-8 2-Fluorobiphenyl 57% 40-106% 1718-51-0 Terphenyl-d14 58% 39-121% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7 of 14 FA86015 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA86015-1 SO - Sludge SW846 8151A SW846 3510C Contentnea Metro Sewage District; Grifton, NC Matrix: Method: Project: Date Sampled: 05/27/21 Date Received: 05/29/21 Percent Solids: 2.0 Run #1 Run #2 File ID DF CC074606.D 1 Analyzed By Prep Date Prep Batch Analytical Batch 06/07/2113:59 SH 06/04/2108:14 OP85733 GCC1856 Run #1 Run #2 Initial Volume Final Volume 10.0 ml 5.0 ml Herbicide TCLP List CAS No. Compound 94-75-7 93-72-1 2,4-D a 2,4,5-TP (Silvex) TCLP Leachate method SW846 1311 Result IIW# MCL RL MDL Units Q ND D016 10 0.050 0.017 mg/I ND D017 1.0 0.0050 0.0013 mg/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 19719-28-9 2,4-DCAA 69% 39-135% (a) Associated CCV outside of control limits high, sample was ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8of14 FA861115 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA86015-1 Matrix: SO - Sludge Method: SW846 8081B SW846 3510C Project: Contentnea Metro Sewage District; Grifton, NC Date Sampled: 05/27/21 Date Received: 05/29/21 Percent Solids: 2.0 File ID DF Run #1 ST152719.D 1 Run #2 Analyzed By Prep Date Prep Batch Analytical Batch 06/04/21 20:28 WH 06/04/21 08:09 OP85732 GST3704 Run #1 Run #2 Initial Volume Final Volume 100 mI 5.0 ml Pesticide TCLP List CAS No. Compound TCLP Leachate method SW846 1311 Result HW# MCL RL MDL Units Q 58-89-9 gamma-BHC (Lindane) ND D013 0.40 0.00010 0.000022 mg/I 12789-03-6 Chlordane ND D020 0.030 0.0010 0.00038 mg/I 72-20-8 Endrin ND D012 0.020 0.00020 0.000021 mg/1 76-44-8 Heptachlor ND D031 0.0080 0.00010 0.000026 mg/1 1024-57-3 Heptachlor epoxide ND D031 0.0080 0.00010 0.000020 mg/I 72-43-5 Methoxychlor ND D014 10 0.00020 0.000050 mgll 8001-35-2 Toxaphene ND D015 0.50 0.0050 0.0021 mg/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09-8 Tetrachloro-m-xylene 77% 42-127% 2051-24-3 Decachlorobiphenyl 73% 27-127% ND = Not detected MDL = Method Detection Limit d = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9 of 14 FAB3D15 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA86015-1 Date Sampled: 05/27/21 Matrix: SO - Sludge Date Received: 05/29/21 Percent Solids: 2.0 Project: Contentnea Metro Sewage District; Grifton, NC Metals Analysis, TCLP Leachate SW846 1311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic < 0.10 D004 5.0 0.10 mg/1 1 06/11/21 06/11/21 LM SW846 6010D 2 SW846 3010A 4 Barium < 2.0 D005 100 2.0 mg/1 1 06/11/21 06/11/21 LM SW846 6010D 2 SW846 3010A 4 Cadmium < 0.050 D006 1.0 0.050 mg/1 1 06/11/21 06/11/21 LM SW846 6016D 2 SW846 3010A 4 Chromium < 0.10 D007 5.0 0.10 mg/I 1 06/11/21 06/11/21 LM SW846 8010D 2 SW846 3010A 4 Lead < 0.050 D008 5.0 0.050 mg/1 1 06/11/21 06/11/21 LM SW848 6010D 2 SW846 3010A 4 Mercury < 0.0050 D009 0.20 0.0050 mg/1 1 06/04/21 06/04/21 Jc SW846 7470A 1 SW846 7470A 3 Selenium < 0.10 D010 1.0 0.10 mg/1 1 06/11/21 06/11/21 LM SW846 6010D 2 SW846 3010A 4 Silver < 0.10 D011 5.0 0.10 mg/1 1 06/11/21 06/11/21 LM SW846 6010D 2 SW846 3010A 4 (1) Instrument QC Batch: MA17754 (2) Instrument QC Batch: MA17777 (3) Prep QC Batch: MP39052 (4) Prep QC Batch: MP39083 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) 10 of 14 FA86O1 s SGS North America Inc. Report of Analysis Page 1of1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA86015-1 Matrix: SO - Sludge Project: Contentnea Metro Sewage District; Griffon, NC Date Sampled: 05/27/21 Date Received: 05/29/21 Percent Solids: 2.0 General Chemistry Analyte Corrosivity as pH Cyanide Reactivity Ignitability (Flashpoint) a Solids, Percent Sulfide Reactivity (a) Not ignitable. Result RL Units DF Analyzed By Method 5.3 su 1 06/09/21 10:38 JB < 7.5 7.5 mg/kg 1 06/09/21 09:58 AC > 200 Deg. F 1 06/04/21 09:36 KSA 2 % 1 06/07/21 13:38 KSA < 250 250 mg/kg 1 06/08/21 17:00 JC SW846 CHAP7 SW846 CHAP7 SW846 1010A MOD SM19 2540G SW846 CHAP7 RL — Reporting Limit 11 of 14 FA86018 Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 12 of 14 FA36015 P Environment 1, Ine. P.O. Box 7085, 114 Oakmont Dr. Greenville., NC 27858 CHAIN OF CUSTODY RECORD F Page 1 or 1 env ironmn et I inc.cont Phone (252) 756-6208 Fax CLIENT: 416 MSD (SLUDGE & WELLS ACC') ONTENTNEA METRO. SEWAGE IS. RENEE PRrDGEN .0. BOX 477 •RIFTON NC 28530 i52) 524-5584 (252) 75G-D631 Week; 10 DIST% DISINFECTION rjCHLORINE ' UV I NONE t, ❑ — CHLORINE NEUIRAUZEOATCOLLECTION pICHECK (t14B) P PP GGGGG CONTA:NEHTYPE, PG A A A A A A A A CHEMICALPRESEBVATION A•NONE LI-NAOH B. HNO E-HCL a • H,SO, F - ZINC ACETAT£INAOH G • NATHIOSUFATE TOTAL CHLORINE, mgA OR ugi AT COLLECTOR 9 O V' ; 8 o f F4 A' $ •$ k c' TCLP VoUSvol I" w U F •� a °gym ; E. ` U E. W0 E�i E y P .. COLLECTION SAMPLE LOCATION DATE TIME Sludge Sample 5 tea\ 1 0-.S \ 5 $i '.. -..s LOTS 5 CLASSIFICATION: Ij WAST€, IATER(NPDES) OHINKINGWATER tj CWRIGW ❑ SOLIDWASTESECTION it -1 L.,\.k ToAL74Saa.... rsftu,7ltx a.. CHAIN OF CUSTODY (SEAL) MAINTAINED DURING �SHIPMENT/DELIVERY (' N SAMPLES COLLECTED BY. (Feast P64q A•N d rA S SAMPLES RECEIVED INLABAT •'.6 'C SHED .DY Sip ISNAP fR) ,an DATE/TIME SlaM RECEI BY (Se) DATEIDME Slz7I f z7 COMMENTS: file* -L.k1frog) 2' 2\ ISHED flY(SIG.) �--- DATE01ME 5•/z31z1 I $`--cr3 AEI; a/ED Y IG '_ 4 ,( 6i rf�' ATEJDME g 1 eG al- : e . .".' HUMMED By (SI } J2e , DATE/RME RE , DBY(51G.) 5aelalliteA• '� o --t DATEIRME 4 I it `) J A ; 72/74/4-1,,.f sAr--) 11..t,•.-•-• FORM eat t' vu s!?A17.( t i` 1 PLEASE EA° Instructions for cosnpledng this form op the reverse side. t5 \V Sampler must place a "C' for composite sample or a "G° tar Grab sample in the blocks above for each parameter requested. N9 389323 PA86015: Chain of Custody Page 1 of 2 43of14 FA88415 SGS Sample Receipt Summary Job Number: FA86015 Client: ENVIROMENT 1 Date l Time Received: 5/29/2021 10:15:00 AM Delivery Method; FEDEX Project: 416 Airblll #'s: 954628460857 Therm ID: IR 1; Therm CF: -1.8; Cooler Temps (Raw Measured) °C: Cooler 1: (2.8); Cooler Temps (Corrected) °C: Cooler 1: (1.0); # of Coolers: 1 Cooler Information 1. Custody Seals Present 2. Custody Seals Intact 3. Temp criteria achieved 4. Cooler temp verification 5. Cooler media Trip Blank information 1. Tip Blank present 1 cooler 2. Trip Blank listed on COC 3. Type Of TB Received Y or N tVi IR Gun ice (Ban) Y or N I ❑ 0 W or S u Sample Information 1. Sampte Labels present on bottles 2. Samples preserved properly 3. Sufficient volume/containers recvd for analysis; 4. Condition of sample 5. Sample recvd within HT 6. Dates(fimes/IDs on COC match Sampte Label 7. VOCs have headspace 8. Bottles received for unspecified Tests 9. Composlting instructions clear 10. Voa Soil Kits/Jars received past 48hrs? 11. % Solids Jar received? 12. Residual Chlorine Present? Y or N_ �I n Intac El Li El El '�i El ❑ . :r ❑ ❑ ,WI ❑ Ri Misc. Information Number of Encores: 25-Gram Test Strip Lot #s: pH 0-3 Residual Chlorine Test Strip Lot #: 5-Gram Number of 5035 Field Kits: Number of Lab Filtered Metals: 230315 pH 10-12 219813A 01her. (Specify) Comments sM001 Rev. Dale 05/24/17 Technician: BRYANG Date: 5/29/2021 10:15:00 A Reviewer: Date: FA86015: Chain of Custody Page 2 of 2 14 of 14 FA88015 LAND APPLICATION FIELD SUMMARY FORMS ANNUAL LAND APPLICATION F IELD SUMMARY FORM PLEASE MAKE A COPY OF 1111S BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WFfFN NOT APPLICABLE. Facility Name: C�ngt, WQ Permit #: u31C4 Field #: Land Owner: C'fa_ Annual Dry Tons Applied: 5 (4--) 4053 Site #: Operator: £{ , 14-r)ky -. Crop 1 Name: rinl gry"LriCt. Predominant Soil Series:' *4JL 13 Crop 1 Max. PAN: 1 t) Crop 2 Name: 2. Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Croi3 2 Max. PAN: C-�z 'If .5 41 '� 4 R Volume (enter one) Liquid Cu. Yds applied Solids/ Gallons % Solids Volume ACond.p Applied P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#,Past Fort, Animal Waste, etc} Soil (Dr' Wet, Preci 24 Hrs. inches ti 0 1 6 " 0` / 1 0 �"r h " H . r � P Q �; p TKN mg/kg u , t , mg/kg Nitrate and Nitrite mg/kg PAN Applied pp (lbslacxe) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 &r1 Z1 ( ) L. 4,Z?O i •' 4� CciO3Z0 ) Jc\it p 5 e.5 o .3o 1 o i 1 t l i3Z.l5; yS ,a. 1 ,6 i..}—] Residuals Applications totals on FORIVI FSF supp ( attach FORM FSF supp to this form): TOTALS: k6 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 145:7C(4 Lime Applied Annual lbs/acre O= (X74g A, CO5 O. S t (._ 0 • bSLo a.01c,. 0 -m l 0 0.6Zg 0.053 0 ..DI. . i1, to .641 : Date lbs/ac Prior Years Cj niulative lbs/ac 0 • (05U 6.D?b Si.45-l• 34.35) 7 4.053 0, Z. r4'-t t 4f Geo 1 0.4:g i ,z> 2.3O6TL " ii -1 Z1 woo Current Cumulativelbs/ac ..Q•(oLoZ 6-05g2.244 30,.. 3 `5 .w 0.351,3•Dlq l5 -- .plu ,37t-E- 0.4b°(oj C G Zc'rg Permitted C. P. L. R.**** 3Cp 34 i3' — Pernik PAN Limit l st/2nd Crop rLF i C5(j I certify, under penalty 0f law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false info on, including the possibility of fines and imprisonment for knowing violations." Signature oand Applier rz-6 726,22 Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORA' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Lon .- .y)ea_, jam,`) Total Dry Tons Applied (Annual): 4 6bt- L o5'3 i 2Qt oO IOL.(-4 Cation Exchange Capacity (non 503 only): 4,5 C1-•ra.fl 'fil 6rn1 high, )1Ct`r!�• Owner: CMl yl@:-A _A-6D Predominant Soil Series: --f .Jdu j L &, Z Acres Permitted: Z. /pZ Site #: Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 5-f-2._1 4 1 i ±I 7 81 1 S 1 101 '1; 12 % Solids 1. t,Z`)0 Arsenic e Z, 5 Cadmium 1.' Copper zi, Z Chromium 1 c Lead Z1 Mercury 0,3,, Molyb- denum q • Z Nickel 1 1 Selenium <5 , D Zinc 1?,„,,' Total Phos- phorus ?114bd Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event ?J g f _ j 10 I 11 j 12 1, f‘,47 0,4g 0,(15 („I-1=221 1.66Ll1 Arsenic c,C Cadmiwn 0,a,5 Copper D ,Sit 1 C"3 I I 0,-C.V. Chrornitur 0 , 09,, Lead 6.065 0,665 p ,CC> 1 Ci • 62g Mercury 0 , cc> I Molyb- denum 0. dl- Nickel -j, 063 ©.-05� 0,0/5 Selenium i:), of Zinc z. j (,0 Total Phos- phorus /n( ) rr},Ofl! "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". &411-4 Signature of Land Applier 0,72 ate. Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION _ ELD SUMMARY FORM PLEASE MAKE A COPY OF I'HIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: C.01- . lnieow �l) WQ Permit #: tA jlcco f eLa Field #: Land Owner: cill_eatntn<m6) Annual Dry Tons Applied: Z.'70Z Site#: Operator: ChAde5ro_ 1 ro-r. Predominant Soil Series:7�C u.,3 Crop 1 Name: Cce&larBeirrucia Crop 1 Max. PAN: ( ) Crop 2 Name: 3 Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Cro 2 Max. PAN: 3-34 3.3(4 4.5 Volume (enter one) Liquid Cu. Yds applied Solids/ Gallons o/, Solids Volume Applied per Acre © Tans/Ac ( �Y } Residual Sources (NPDES #, WQ#, Q , Pert, Animal waste, etc) Soil Cond. Ws ' Moist) Preci P 24 Past Hrs. inches 4 1 b �, n Q M q rt @ x i N fl H x 0 TKN mg/kg n H mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 _{o-azi Liocoo i-(Z15 ©-c6(i 1 3ZD`)) dry © 5 6. J G.a) tii,o&O i [! I 'Bill Z,3.GoZ r s° mom` c, sc Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: I As Cd Cu Cr Pb Hg Mo Ni Se Zn P a 4bZ1 Lime Applied Annual lbs/acre Q . ajU o •C)2 (>. .7(4.2".Ol eD .63(4 Q, pb1 0,615 0, 6Z7? G ./xA j. 5 7 b Z' SJ Date lbs/ac Prior Years emulative lbs/ae p ,`) 4 La 4_45161 •- ;i4 'r314_2_6' 0.1-1) 7.' —r cf.4,53 6.Gel Z .ice 1 l-(2 7 -560 Current Cumulative lbs/ac �, f5 (: L1. C{ P :- 3 (..p.(2 ,7-t4-t,z . h c� 7, c� t L1 c(- v� U [.tr6Z to • CIa. Z�1 Permitted C. P. L. R.**** 3 (., 3'(-I ),-?)g --- 2-(;7 15 — 3--)4 Z Permit PAN Limit lst/2nd Crop may, under penal y os law, tnat tn►s document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informa . ' including the possibility of fines and imprisonment for knowing violations." AA/ Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 * ** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM`` Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Chink14 a:- m3P L \Qc x OUP 4 k i lorf). omf<1D1;uicr)Tf. Owner: `3Ll Acres Permitted: Total Dry Tons Applied (Annual): Z,'Z Cation Exchange Capacity (non 503 only): 14.'5 Cary[ervin o_ fi5D Predominant Soil Series: Taco�j '�. Zif Site #: Field ##: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 3 I 1 9 1 10 1111 1121 6 n_2f _§_l % Solids l-<iz% Arsenic < x, 5 Cadmium 1 , 5 Copper ZIp- Chromiurn 1l' Lead Z1 Mercury D ,'L(n Molyb- denum 0,2 Nickel 1 Selenium <6, Q Zinc 4 2A Total Phos- phorus ' q 5 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event .J _J 3 4 f , 5J 6 r 81 9J ito 111 12 6,45 p. jL.j (.-11Zi 6.4(, .J Arsenic 0,0DLi Cadmium 0.001, _i.d)2 d , u-Z Copper 6.02.,(.1 Chr'omi€ur f*j, Gj 0.D - a,63ci Lead 0,D3i-1 Mercury tj , pO 1 0 .} 1 Molyb- denum 0 015 O. U 15 Nickel 0 , nl p_(1Z� 0, Selenium O-664 Zinc 1, 35 ) Total Phos- phorus to.nq Llano "I certify, under penalty of law, that this document was prepared under my direction or supei vision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier ,2—) Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUNIlVIARY FORM PLEASE MAKE A COPY OF TBIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WREN NOT APPLICABLE. Facility Name: Cor,4f M5 WQ Permit #: 6,�0.CC` f0(4 Field #: Land Owner: Ccik ra- F'ndr) Annual Dry Tons Applied: 2,437 Site #: Operator: ('P{�_ tl '1ui Cif Predominant Soil Series: TQrjoi{t� Crop 1 Name: 113a Crop 1 Max. PAN: j j') Crop 2 Name: 15 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Acres Utilized: Acres Permitted: 374 3[4 4.5 41 0 Jj Volume (enter one) Liquid Cu. Yds applied Solids/ Gallons % Solids Volume Applied per Acre (Dry TansfAc) Residual Sources DES #, VJ # Q,1 Fert, Animal Waste, etc) Soil Cond. (DM wet Moist) Precip.T Past 24 Hrs. inches 0 I N w p 0 p "' i t HH w C N G ,1 TKN mg/kg y mg/kg Nitrate: and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 weL, Crop 2 6-1q--2-1 31o1CL Pin ©• (65c) r-i-Co3Z(57) cry O 5 3.5 0.36 4‘ob4 i li f •ig R.71)4 T 0. {o Residutils Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 3 to COO:' As Cd Cu Cr Pb Hg Mo Ni Se Zn P "lg. zcf-1j Lime Applied Annual lbs/acre Q.PO3 0 -COZ 0-"3-4 4 C .L`I3 ©,G7.7 cpU r)-olz O.622 p-(1)lo f-C i Z,-az Date lbs/ac Prior Years G'mulative lbs/ae 0 .4g l-7 4. Koq )0-8/p ,o. 50 $_G) Ca 0.2_7 a.IG.Z et.IoO6 C*Aci 1 , Z.Z68 1)-1-Z1 0 Current Cumulative lbs/ac O' 662L) C4. ici 1 '1Cc.5f 66,iac) ° 4-103 ©-2 O .3-747L c1 •iaZ�-f` AQ.--) a. 1` z Permitted C. P. L. R.**** alp 3 4 132y -- 24j) 15 — 374 q Permit PAN Limit 1 stl2nd Crop 1 ceruiy, under penalty o#-law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informatio 'ncIuding the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: con-i-er,iryea.m5D Total Dry Tons Applied (Annual): Z,43Z Permit #: Cation Exchange Capacity (non 503 only): 4, 6 Operator: Chatle3rn•6mi itiCtja• Owner: ('C`.(-t (inertM Predominant Soil Series: `ioClehi� Acres Permitted: 3.7La Site #: fJ Field #: '5 Acres Used: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date _LI 31 41 J J J J 10 1 t 12 5,n-L1 % Solids 14%1.'6 Arsenic <2, 5 Cadrniunn j .6 Copper Z14,Z Chromium 1 g Lead Z 1 Mercury a, 3 to Molyb- denum 0 2 Nickel $ —1 Selenium < 6. p Zinc q-ag Total Phos- phorus L4c()o Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Aci App. Event J 4.-J C,7,(150 _i J ± U Jji __9i :ILI itu 12 0 0,141,5h p ,4j3 0 , 6t5Z �y i Arsenic U ,w3 Cadmium 0 , 00Z Copper el ,ail j Chromiurr p , a3 CG .623 D ,67-17 6.W6 Q.L!Z 0 7-7 0.06(.., Lead p , )7,"7 Mercury p •W0 Molyb- denum C.),DiZ Nickel 0, b22. Selenium 0 ,(t)(p Zinc `t.aci 1 1,CA, l Total Phos- phorus 3Z, 3-7)D 32.37a "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". /`% Signature of Land Applier - Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF 'I'IIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WFiFN NOT APPLICABLE. Facility Name: }eNnea D WQ Permit #: Laccol oqg Field #: Land Owner: rc,n4a0,1n -D Annual Dry Tons Applied: i, )C (p Site #: G-Tictc4 5 Operator:( e5rsi). ornikihttii ITC I Name:Irracfa, Predominant Soil Series: (4a Crop 1 Max. PAN: Cro 2 Name: Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Cro -273 q• 5 la Volume (enter one) Liquid Cu. Yds applied Solids/ Gallons % Solids Volume Applied per Acre D Ac (Dry Tons/ ) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Soil Cond. (Dry' Wet, Moist) Precip. Past 24 Hrs. Inches v G w a p P ;1' f t, 7 Fl x TKN mg/kg y 4 N, H mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acze) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 1 7-1. (A 1-621 a •5 G4 44GCGZZol--) r try () 3 o, 5 Q ?oo U► i 1 1 '23.z.J 1 ri.65G 1-1411 677.DO 1•2, ?c 4.544 4 1,40-1)3245)-) milJ►- C) 5 0. 5 n•�) •i of 1 it i ' 32 i( 01 _ i .1-5q Residulls Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: I i' .2OO As Cd Cu Cr Pb Hg Mo Ni Se Zn P 33. j Lime Applied Annual lbs/acre D ,Off(P C3.( 4Q. LP G•Dt-F 1 0.04g ©-ri p p,071 a.D3g c.at i i-Rt a .67Z `. Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative ©- (02L 7)5 54CRD 25,-) 5-433 CU•135 7 • IZ! 5 3LP 0.10() 7t_91. 3 E !-I2J land Ibs/ac 0 • (a7/ i -"f q 55.5(6U Z j -t 6 - [,ig 4 p =r65 2,• 1- �_34s5 -).1,-) ZDL )3 ._ Permitted C. P. L. R.**** Permit a (0 3� 133 — 7_io) 4 FJ — 3-i4.1 4 2(-1C[ d PAN Limit l st/2nd Crop cc __Ti Z I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalises for submitting false informati'including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Cxi-er e-ri 7 tJQ U001 Otg Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Owner: ecryt--en4-nert-rn5D Predominant Soil Series: ')3 Acres Permitted: )3 Site #: C to Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): SampleorJ Com- posite Date 5-EN-1 J &-Z? Z1 J J J 6J 7 J J 101 11 12 % Solids 1 • 6/15 1-1o7...50 Arsenic 42,6 <2.5 Cadmium 1 .6 1 .6 Copper •1422.. 7.102, Chromium 1 6 t 1 Lead Z 1 1 Mercury p.-y (.).3(a Molyb- denum G .2. G •2- Nickel 11 ("? Selenium <5, (j <5. (� Zinc 4d 3c-1 g3-G7 Total Phos- phorus Z4 CO 21-1CiO(j • Annual Heavy Metal Field Loadings (Calculated in lbslacre): Total DT/Ac./ App. Event J J 0-10-7-1 G.54t-1 31 J J ? $ 1 9 j itcli 11 12 li 0 t,) Q 30-2-4 0.5 LJ Arsenic 0. DO 0.6( 5 0 • ( (. Cadinitun p • Ct,j p , 002 Copper 0,-6.1 t 0.Z.Se5 a.�c� C> . 6q 1 Chrornhur p • (7Z 1 0 . bt.0 Lead 6, (77,_'5 c • bl- Merctny O bbO 0•CO0 0,.QO0 0.011 Molyb- denum c c t 0.0(0 Nickel 0,07_0 0, d l q (L), (-3 Selenium 0.wL 0,o. D.61 i 1.G 10 Zinc 2.ic1) 0,q 13 Total Phos- phorus 1.-Ct• 31 2.,17C j 1 ic.,•6.7Z certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier AFL-Aa62a Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION HELD SUNLVIARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: COntizirea_1-) WQ Permit #: \C Qf,(a Field #: Q Acres Utilized: Land Owner:.-1-0-144rEa.1y),6,D Annual Dry Tons Applied: I. " ) (4 2_ Site #: fC( TE Acres Permitted: Operator: l n.afy)1 lc91_ Predominant Soil Series: 4 Crop 1 Name: C4.tiaragrlytia- Crop 1 Max. PAN: 1 ") 7 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ;5 )5' 5./5 p H 4 Volume (enter one) Liquid Cu.. Yds applied Solids/ Gallons % Solids Volume Applied per Acre p Tons/Ac Residual Sources (NPDESQ #, W # Pert, Waste, etc) Soil Cond. (DrY We Precip• Past 24 Hrs. inches d P' is 0 0 p µ p 0 O• N "' W h i p ' r y T N mg/kg 1 mg/kg Nitrate and Nitrite PAN Applied (lbs/acre) Name of Crop Type ReceivingResidual Application mg/kg Crop 1 Crop 2 1 Crop 2 r;-1 4.-1 '.L-Ia21 Q 70 1. 2b 1.102- l-C.CU3.7_C5) idf•i 0 5 C3.5 o.30 Li6I6U lit 1 i)3Z) Z4 ? 1/4„Crop RA' 4 4-5100 l.(r) a -kilo aCCO3ZoT) mo f o, I 5 0.5 0.50 i-) 1 1 1 1 /E, I `f•(,cq n-"=('', 1. (pq g Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 1 9I4C)1 As Cd Cu Cr Pb Hg Mo Ni Se Zn P '50ll?S Lime Applied Annual lbs/acre o-6(;e O-CO5 C?.gc'q-1 o,a01 O.W! 6.cO1 O•Q31 0) 7a61-7 z� %f Date lbs/ac Prior Years Cumulative lbs/ac O.5 (-5 J- c"?e! . 5.grcRi zi4,, O4 6.1d1 .1113 Z-70q 6.05 0 ;-?i () 7 t 153 . 1.11 Z 4 loon Current Cumulative lbs/ac 0 T 7 (-1 i .(64S4 56 TA Zlc cii 6. lds') ,0.1 LAA Z.735 6.7L2 D iZ) Z.11. 2] Permitted C. P. L. R.**** 3t 3 Li 1334g — ZO 15 — 374 .g wed Permit PAN Limit 1 stl2nd Crop l Z I certify, under penalty of law, that thus document was prepared under my direction or supervision in accordance with. a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information l ding the po hility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 1-1Z A5.2./ **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: CAh.11-1eGt..14\6,D Total Dry Tons Applied (Annual): g.Z%Z Permit #: L.V0000(4.ta Cation Exchange Capacity (non 503 only): Operator: hadebto, dniLtihol 7. Owner: icrl`[el)ipe�1' Predominant Soil Series: Maya. Acres Used: 5• I Fj Acres Permitted: 5 j',j Site #: CT' ad--[T Field #: (;) Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample orb Com- posite Date 7 8 9 10 111 12 5:Li-21 6-Z7•ZI % Solids I- Z`?o 1.6290 Arsenic (2.r <7,rJ Cadmium 1,6 I ,6 Copper Z, Z. Z102 Chromium ) 4 1 g Lead L ! Z I Mercury p . 3- i, a 3 Molyb- denum q1 • Z r-! - Z Nickel I / 17 Selenium <6,0 <rj D Zine 1 q1 g,3q Total Phos- phorus v-ig00 2_1-44(Y, Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total DT/Ac./ App Event 1 1 I J ± __5_1 JJ LB] 9 10 ,1 [ 2 1.447/ 0.19 (5,dt15 O. (3.0W 0.671 ii Nq `1-I-21 I -(©Z 1-13-2i 0iS(' Arsenic p ,p(j(,, 0.003 Cadmium 0,(bU3 c»6(7Z Copper 0,51) O.312 Chromium a, 014, 0 0,O2.1 Lead cs,4LI'6 el, Dv, Mercury o , Cot o .Do0 . (Y)1 Molyb- denum ©• 02.0 0.01 I ..0 O. C31 Nickel p .037) 0.621) ©.15 J 0•oil Selenium O,GiI O•Coto Zinc 1. extq 1,GDO Z•(ZUe 4i1 .901 Total Phos- phorus 6(1.w)24.14d I _ "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". .--46E:9/- Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION I+'LELD SUMMARY FORM PLEASE MAKE A COPY OF MIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WREN NOT APPLICABLE. Facility Name: ( -ferlihea., i f WQ Permit #: tijQCC))Q(d-K Land Owner: CrfAerahecL i j Annual Dry Tons Applied: 3. 243 Operator: Ckya1lei•Jin 'Y,)1[ 9i'. Crop 1 Name: Cr9a rBeirf G1iJ L Predominant Soil Series: t -3 i 0 Gt . Field #: 1 3 Site #: C Tf ar.A. T Crop 1 Max. PAN: 1 jF Crop 2 Name: Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Cro 2 Max. PAN: a� 3.32 L5 ;� li 0 Volume (enter one) Liquid Cu_ Yds applied Solids/ Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual (NPDESQ Pert., Waste, Sources #, wT #, Animal Soil Cond. (DrY' Wet Moist) Preoi p• Past 24 Hrs. inches 1 (f li N n 0 G 0 ri w 1 " H ,, ? o-' r p TKN mg/kg y mg/kg Nitrate and Nitrite mg/kg PAN Applied (1%s/acre) Name of Crop Type Receiving Residual Application etc) Crop 1 Crop 2 Crop 1 Crop 2 -7.0'-21 4-KsoDo !-a (). ciq 3 H-C Z15l f is rvai ( 3 a. 5 0. 646 01 I /23z.1g zR.c 3 WM. (i) C -3 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: Lai As Cd Cu Cr Pb Ig Mo Ni Se Zn P ZQ.C1 3 ( Lime Applied Annual lbs/acre 6, C`US O .C123 0.56 o. € 5 0,041 0 . c 1 0. b1 0 0 , 33 0.0o \ .6C.e €4,6353 .. Date lbs/ac Prior Years Cumulative lbslac 0 , 37J -6-3-1 C3.4 b 1 14.1: Z). ) Z• b' 1 0. D74 I - Otpg 3. Ct 0. 4D1 0-.7 Z! �1,37p l l-c-7J ) dry) Current Cumulative lbslac p . p .col -I 1 . i00 Z,7.V2 Z. -2- 0 , b"7 5 [ • 0cs 6 3. p(•1.1 �'} . t-i 11 Permitted C. P. L. R**** 3.� 3u i33o -- -) 15 — 3 -)Lj. � ? Zw& Permit PAN Limit l st/2nd Crop l (a 1 I certz£y, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Cis -enea_rn6D Total Dry Tons Applied (Annual): ,3, ZC�3 Permit #: 14/Pjj( C.K) Cation Exchange Capacity (non 503 only): Operator: ('Licale,fil,► mf lC�' f - Owner: Con-1-enjnect,1110 Predominant Soil Series: CO ((a. i3 �Lj Site #: CTi-ad-ff Field #: 13 Acres Used: Z(j Acres Permitted: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or? Com- posite Date 5-Z7-i i 6T 7 s 9 i o 1 12 — % Solids 1, t,t Arsenic (2.6 Cadmium 1.6 Copper Zk,Z Chromiuin 1 g Lead Z 1 Mercury t) . Molyb- denum Nickel 11 Selenium < 4: O Zinc 3,4-. Total Phos- phorus 7...4G00 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DAT/p e./ Event ,0� 0, eN 3 _II _i U jj U ._9j -111 11 12 Q e 43 15.D `� Arsenic 0 , C05 Cadmium 6,W3 0 .00c3 Copper D, €.,15 p,515 6.635 00.Ott l Chromium° , 0535 Lead 0, 1 Mercury 6,00 1 0.C)0 i �,Ui'3 O 03"3 Molyb- denum 0.01 Nickel 0 ,033 Selenium 0,r)IO ,DID Zinc 1, 14,4q 1- ttKi q, , ci63 Total Phos- phorus LW q53 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) Facility Name: ( 45-31ne F j Land Owner: or,y., fj.I1&. mg) Operator: Ckv to - ct5J Crop 1 Name: 113 rnricia.. ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF TFIIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: L f 0 ( Field #: 1 l4. Site #: Annual Dry Tons Applied: z .4 ig Acres Utilized: Acres Permitted: 3,✓D Predominant Soil Series: -kr-i-opti..h Cation Exchange Capacity (non 503): 4,5 Crop 1 Max. PAN: 1i to Crop 2 Name: Croa 2 Max. PAN: �t l) liip Volume (enter one) Liquid Cu. Yds applied Solids/ Gallons(DryTons/Ac % Solids Volume Applied per Acre ) Residual Sources (NPDES #, W #, Pert., Animal Waste, Soil Cond. wry= Wet, Moist) Preci Past 24 Hrs. r r N nV " p N I N w ' -0 , y mg/kg Nitrate and Nitrite + PAN lb Applied (lbs/acre) Name of Crop Type Receiving Residual Application 1 Crop 2 Crop 1 Crop 2 r .5-0 2) � 3 5 0 I- IA /'�/� l_/, ��G7.:> yetc) � o52 !7 roi /innches bar e 5 as') / �m/g�/kg/� 4h/, 1 b 1 (t /��m'g7/kg Zlig yC�jroop 7 f3 �f1 . 0 ,460 (p Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 00 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 1,3,C131 Lime Applied Annuallbs/acre 0.004 O,D02 0.472 nLpZ�i r.0 Li o.ex;i (),015 _ C.PZ'7 6-an 1.- 52 LI.D.F Date lbs/ac Prior Years Cumulative lbs/ae 6,2.1r) 3,467 iUi35i 2,1.44a0g i,Q0Li O.D2.72 o," J 7.33ci 6,343 i0 ... 1 i!-S71 b Current Cumulative lbs/ac 3.2.7-1 5.0071 Iori)3 7.1-1.�3 � t.G"Q r).bZ9_r3• bDg ?_•3.,6 0•35k tc.1,5g:' Permitted C. P. L. R.**** & 6 L-f 133g — Ztc? i 5 — 3-) U qGT -I'? Permit PAN Limit 1st/2nd Crop rx, I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information eluding the possibility of fines and imprisonment for knowing violations." ,a,hd Signature of Land Applie Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: u e ccolo44 ( td i-6mi - Owner: d DU Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): i3,0n Site #: 4.5 Predominant Soil Series:ThJo nth Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #)• Sample or Com- posite Date ± ?J `t _i _LI 8 9i 10 1 11 12 6 fl-Zj % Solids I.6p2% Arsenic < 2.6 Cadmium 1.6 Copper z1,2 Chromium I Lead 2-1 Mercury p,36 Molyb- denum Cl • Z Nickel 11 Selenium <5.6 Zinc g,j Total Phos- phorus Z ! ?b0 Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total DTIAc.J App. Event Al 12 r 3J _i _i ±I 7 1 8 1 9 I 10 'I 1 12 G 0.4)a. d . $-II ZI t.ifp(o Arsenic p, DO{ -I Cadmium 6,062, a,tbZ Copper O •L 77 a.472 63.029 6,G?,e-t Chromimr. 0,6n Lead 0,p3U Mercury 6 , Lif l .Q • CO ! Molyb- denum 0.0i5 6,66 6.623 6 •GM3 I. Z Nickel D , b2..) Selenium c ti Y Zinc 1, i:j2 Total Phos- phorus 4A943q 4 •!'.'J "I certify, under penalty of law, that this document was prepared under my direction or supei vision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION II IELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH 1LELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Cbcl+ rer_mg) WQ Permit #: 0.4 Field #: i Land Owner: rr lam' Annual Dry Tons Applied: �702. Site #: D Operator: ctNctiit` 1. 114,,j . -t- Predominant Soil Series: /}.)Q50.., Crop 1 Name: Ccoofaer Crop p Cr 1 Max. PAN: l`) 7 Cro2 Name: o 2 Max PAN Acres Utilized: Z,5 Acres Permitted: Z,�� Cation Exchange Capacity (non 503): 4. 5 iJ F -iF-2i Volume (cuter one) Liquid Cu. Yds applied Solids/ Gallons o/a Solids Volume Applied per Acre (Dry TonslAe Residual Sources DES #, WQ#, Q Fert., Animal Waste, etc) Soil Cond. iDrY We Moist) Precip. Past 24 Hrs. inches �( ^ i rt N, ri 0 G rt m N, i µ w U 0 (E 6 1 i P TKN mg/kg "f 1 n mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4 _i -6Th a .4(5 4c� ooa2b-i) rnNai- O 5 0.6 p. ()r6 111 I r Z-vv 7 gtRAL.^ r _ - . , g- --) Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: L yy As Cd Cu Cr Pb Hg Mo Ni Se Zn P Zh 1 Lime Applied Annual lbs/acre 0.005 c . cx)3 0.4-)5 0.033 0 , D3S a. L)1 Q . 017 0 , c +,-p-ce. VS ZZ 46. 1 (..R Date lbs/ac Prior Years Cumulative lbslac 6,71/15 !'�. 4, Zrd �.�5 2.214.4 O.0aq p_ Z5'Z 9.4tiq i2i.Zle5 . . j 24 56O Current Cumulative lbslac ci , 2...13 D.?fa'q 2.G4L .q lc 7-36Z 0 =C3'S O. 0 Z.543 0.1-4Zg IZ2, '} Permitted C. P. L. R.**** 61 ,3Li.• 1338 — Dir) 16 — 37O' '1 Z 1.g Permit PAN Limit 1 st/2nd Crop 44T nz certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false informati : , eluding the possibility of fines and imprisonment for knowing violations." Signature of Land Applier A�j *Application Method: S - Surface, IN - Injection, INC - Incorporation g.a **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: 4-. 5 CivileA,601huicicgt, Owner: 00-1-1- nm0 Predominant Soil Series: Acres Permitted: • CIS Z. q$ Site #: Field #: t LC/ C 4eNne -r0 Total Dry Tons Applied (Annual): z,-»z, LOQCOOKYR Cation Exchange Capacity (non 503 only): Residual Analysis Data (Heavy Metals and Total Phosphorus use zng/kg, % Solids use Raw Percent #1: Sample or Com- posite Date .� _ 3 4 11 ± 7 v 8 9 ILI 11 1. 6'Z7 Z1 % Solids „ton Arsenic < , 5 Cadmium ) .6 Copper Z(Z - Chromium )1; Lead ZJ Mercury b, 3 (0 Molyb- denum G.Z Nickel l —1 Selenium <5, 6 Zinc /3q?~ Total Phos- phorus MOO nnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total D 11Apc./ Event 11 c -11-Zi 0,467 ±I _ 4J _ j 6 J 8 J t jj irod i 1 12 0 .O D Arsenic p . co 5 Cadmium 0.17)3 6 .tj3 c.(fJ5 Copper Ca,475 Chrorniurr.0,0 3 c3.)33 Lead 0,6N ©. ate p. CO 1 Mercury 0 . w ! Molyb- denum 0,011 0,017 o , 63-1 o, Glhcr I. 6Z2 46.10 Nickel 0,031 Selenium 0,Cpq Zinc I , ; 22 - Total Phos- phorus �15! loq _ "i certrxy, under penalty of law, that this document was prepared under my direction or super vision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: 1 iiD WQ Permit #: I c( Oj1O( Field #: Land Owner: C 4 ffial Annual Dry Tons Applied: (p,( q Site #: Operator: ( L'i( -56occji. Predominant Soil Series: Ma Crop 1 Name:(4. Crop 1 Max. PAN: 11 Crop 2 Name: 1l Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Vim- a'aL. d Volume (enter one) Liquid Cu.. Yds applied Solids/ Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources DES #, W # {Q , Fert., Animal Waste, etc) Soil Cond. ��' Wet, Moist) Precip. Past 24 Hrs. inches ti {i r r� 0 " rt r+ 14 k N li d ! TKN mg/kg yy M r n mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 7-20 45206 1 into D •(3 -207) dfi (3,6 0.3 b y(aD 1 I I 1 1 Zig Z4 Bch ctvtaivck $47,21 51 C ) I -fir) I'),g4l 14Ci^� 51-) mai -.i- 0 5 .5 D ) 4 114 I 1.32.1q Z4.1fl t .1q ,5 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 4 (02D6 As Cd Cu Cr Pb Hg Mo 1 Ni Se Zn P 63.b331 Lime Applied Annual lbs/acre fig, CCP p , p,gict,1 ©.©L-L4 C.0-75 0-X2 6,0344 .•G(ol 0.01`8 3.6I2- Ssq. l Date lbs/ac Prior Years C:,z„ulative lbs/ac 0.3fl 6.47 as.306 II •q55' 3.60-7 O, C) . 53 3_321 I3, t Eg7Lg i (.;).2 r 11-t Z tC o() Current Cumulative lbs/ac C) • .35 to c ,1LiC553C.7q 1 f2., 6222 3- Lx61- o , CArto. ) 3.3ca Cl .511 Permitted C. P. L. R.**** ,3(p .4. I3g — !fp`) 15 — 5, Gq Z4ci� Permit PAN Limit lst/2nd Crop 112 I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." /I w Sigture of Land App ier *Application Method: S - Surface, IN - Injection, INC - Incorporation 01/6 -Ago" **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORA? Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:ef-('{} Total Dry Tons Applied (Annual): Permit #: tJQCCOIC Cation Exchange Capacity (non 503 only): Operator: (mil# ,o'lir ljCtp . Owner: (Mi-en-inel m Predominant Soil Series: F4 G . Acres Used: 13. 102 Acres Permitted: 3 62 Site #: D Field #: U. s 17 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date _J 5n2I 41 51 6i 7 J 9I 10 I 11 '' 5.Z7Z1 _A %Solids I.jpZLr. 1.Iono Arsenic C Z. 5 < 7, ,5 Cadtniuin I.5j 1.. Copper zi02 42 Chromium ) 1 Lead 7 I 2,1 Mercury d . -6_Iv 0 ,3-10 Molyb- denum q .2 q.2 Nickel 1 "j 11 Selenium <5, jj <54) Zinc 3qi cs3q Total Phos- phorus 24g00 &QC° Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 I 2 f ' -12 2-1 0.q51., 4J 5 f _i J 81 9 I Ai 1. 12 0 I. Y 1 'R-21, zI 0.4 3 Arsenic 0. bOti 0, 065 O. L Cadmitun 0. 55 p,U)3 0,00(. Copper 0 . itta. to,i_igci c041 (1),N0(-i Chromitur ®, 03 O, 21.1 Lead 0,03 O,OLIO e),675 O . Coz 0.U3i-I Mercury D. CO 1 (, 001 Molyb- dentun C3 . C i 1' 0.018 Nickel (1, (-2 1 6.b32, 0.061 ©.01Q 3. 012 Selenium 0,()(4 0.01D Zinc 1. (--1 16 1. 5G') Total Phos- phorus /Ala 1 e-n•/A ' qc1- 1 "I certify, under penalty of law, that this document was prepared under my direction or super vision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: ieNi u) WQ Permit #: u_DocoField #: 1 cg Land Owner: �4j r Annual Dry Tons Applied: «. � "� Site #: �•� *^ Predominant Soil Series: C- -01U 3 Cation Exchange Capacity (non 503): Operator • rim-bnkik-ocgi-- Crop 1 Name: Cccktj{ira.ICfz.• Crop 1 Max. PAN: Cron 2 Name: Acres Utilized: Acres Permitted: • Z-4Z y •5 4 0 pCI Volume (enter one) Liquid q Cu. Yds applied PP Solids/ Gallons % Solids Volume Applied per Acre (0ry Tons/Ac) Residual Sources DES #, W # Pert., Animal Waste, etc Soil Cond. (DrY' Wet, Moist) Precip. Past 24 Hrs. inches 6 r r w n 0 p Q w l" w P 0 Y x p TKN mg/kg y r N i mg/kg Nitrate and Nitrite mglkg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Pg.-Li toLletz t-6 Z-403 14C37O7) r d.2. 5 a.5 0.3O `moo t)l1 1.51tg 15-xR 7 miAL. i-2b-21 ZWDO 14„2"6 ci • lo-?U !4Cc3767) mai -- C) .5 t9 ,5 (.&) 4fr,.l,(c) f t I i /2,3LA p.- rl 3.57 -3 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): - TOTALS: I E2(60l As Cd Cu Cr Pb Hg Mo Ni Se Zn P C5:544 Lime Applied Annual.lbs/acre 0.01 6•01 i 1402 0-1Zg C3456 0.00Z 0.06.5 0.172 0.03(a 6_GG.5 mR-7 Date lbs/ac Prior Years Cumulative lbslac O. D .1L` d 5-56(„3 crnz p p ,o-z3 c).;$i4 i-cam 1 c..).1b D. d '. 11-td--2.1 t00,ID Current Cumulative lbslac C. I Z`) 0 • t 1 g 1M5 i7. c►00 1- IQ q p . 625 Q. LI6'°/ j - 71.j3 p 12-(-1 eli,. 3 Permitted C. P. L. R.**** 3 3 P /-33 — 2_a) 1 5 — 3 )4 .gq z. 8 Permit PAN Limit lst/2nd Crop 190 «I ti cer fy, under penalty of law, chat this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, ,eluding the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FOR1Ve Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: rcryl-e e0.-Kbp Total Dry Tons Applied (Annual): g, 6,L/ ) Permit #: 00 C5C0i OW Cation Exchange Capacity (non 503 only): Lk- `5 Operator: CIiQtIeill fLth Owner: ecni-eAtirlea, in D Predominant Soil Series: dok Acres Used: 7, qZ Acres Permitted: Z C/Z Site #: D Field #: j449 Residual Analysis Data (Heavy Metals and Total Phosphorus use nag/kg, % Solids use Raw Percent #): Sample or Com- posite Date FJ -Tiz1 A ±i U jj A jj ' : 11 12 Zl % Solids .„6:n 1•(o71) 140l2o Arsenic C2, 5 C 2, 5 Cadaniunn 1.6 1 Copper Z('2 7 t,Z Chroznimn 1 e 1 q Lead ji Z1 Mercury p, a 0 4 ate Molyb- denum C[- Z 0 Nickel 17 17 Selenium <6.0 C5.0 Zinc .434 q0 3ej Total Phos- phorus t4 ?OC) z.q o0 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event / lr 71 Z.V?L73 i-Z4-Z1 to•Ip-)U U 6 ± . s j Lpj -:i, 11 111 k'z.5 Ili Q 73 Arsenic 0. DI Fj 0 ,UO'a O. e1Q Cadmium 0,CX1ci 0,002 04'i 1 Copper 1, 6-Li 0, 1 1.T) z Chroiniuir ©. oil 0 . 0Zu t) • 124g Lead 0.1 7,2 0.bi.d 0.6(.) Mercury 4•052, O.CD0 p•DOZ Molyb- denum 4.D53 C..01Z p.b(6 Nickel p,bgG 0,b 3 o•1Z2 nt 66. U Selenium a , olq 0.057 Zinc c. i.4t)) 1,1 7....1-4 5, S Total Phos- phorus itIti.50 3343fp& 171.G31) "I certify, under penalty of law, that this document was prepared under my direction or super vision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 4f4 i Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION t th,LD SUMMARY FORM PLEASE MAKE A COPY OF TUTS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "NIA" IN A BLANK OR BOX WHIN NOT APPLICABLE. Facility Name: C©rkninect-- D WQ Permit #: n=)/0( .4 Field #: 1 C j Acres Utilized: Er/5 Land Owner: Ccn* i e . 1o7 Annual Dry Tons Applied: 1 1, LK i..14 Site #: C` iaCA ir Acres Permitted: Predominant Soil Series: 4 Crop1 Name: . (�`�(��i)��. Crop 1 Max. PAN: i`�1 Z Crop 2 Name: p Operator:( (l4nc��?r, Cation Exchange Capacity (non 503): Cro 2 Max. PAN: 11:15 e�_ 5 1] 0 Q Volume (enter one) Liquid Cu. Yds applied Solids/ Gallons % Solids Volume Applied per Acre (Dry Tons/AG) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet, Moist) Precip. Past 24 Hrs.fi inches � 'd r r i 0 0 G " r rt ," 7 a r w P i p TKN mg/kg N; N mg/kg Nitrate and Nitrite mg/kg p AN Applied (lbs/acne) Name of Crop Type ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 1 11 r/ocLZ7 1-laz`7( < 6 .G-1") A Ci .2)7.(5-P From 0 s ©r 5 a. 0 111 1 q3lig 2 .‘;10 Q 4 7) Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS. nDcco As Cdd Cu Cr Pb Hg Mo Ni Se .Zn P ZI.cip5 Lime Applied Annual lbs/acre 0.005 o -cD3 0.512 C..o .041 C3 CU i , () i b o.1$3 0.145O.0I--? 6.Of 0 i .13ci ZZrt 44.415 ` ' Date lbs/ac Prior Years Cumulativelbs/ae Q. Cbq 6.co4 C-(o2 6.0{01 0,CD1 0.CO66.01g lid-2.1 .dc)c Current Cumulative Ibs/ac Cs.. )(U D.007 t.3`7U O.09(e 0,11-L 0 1 o-LZ3(00 •6g O.62---) 3.Q33 Pen fitted C. P. L. R.**** y- to all 133g — zit, i — 37)L4 S'q ZCPC' Permit PAN Limit 1st/2nd Crop 1 17 i< certYfy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Appli.er Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Jc4eni-r-)€0„.m6-7 Qor0 EO( Char tebli),6Miliegi- Owner: 11.7) Acres Permitted: Total Dry Tons Applied (Annual): J 1 , L L/ Cation Exchange Capacity (non 503 only): 1t. rj CCni941@a inn Predominant Soil Series: ,L} J �, 1 I.7 5 Site #: G-1i id-fl Field #: fC1J Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample ors[ Com- posite Date $ ±1 jj a 9 1 10 11 12 5-1) 2 j % Solids 1,1,2 44) Arsenic < 2. 6 Cadmium 1.6 Copper Z.lo Z Chromium J g Lead Z } Mercury rj, 3 Molyb- denum R . 2_ Nickel 1 '] Selenium < 5 O Zinc «3 Total Phos- phorus 114400 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 4 f ± f 7 J j 11 10 11 j 12 0 4 `,Y- 0 -Cb3 16-1 Q.ci^) ._0,6419-2 Arsenic •S , fir Cadmium 6 ,603 Copper 0.5 iz o. i2 Chromium 0,036 Lead 0 , f LJ 1 a.DY--t-1 D •Ce)1 Mercury p,C 1 Molyb- denum 0-614 0.D1d Nickel 0 , 6,33 0• 633 0.016 -g Selenium p . 010 Zinc 1. (03ci Total Phos- phorus 64,1F5'5 t jg.4T5 certi y, un er pena ty o law, that t is document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 4.14/t/ '107a A, 1:11°:?1' Signature of Land Applier Date DENR FORM MFLSF (1212006) PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: WWTP Name: eA1511-frYta -D WQ Permit Number: {,owoof, fl`1-$rt iy)5 NPDES Number: j— .0:YjZ6D Monitoring Period: From ,ic�nt.lc;t1 t wit To))e_c, 3) 7 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) • Process to Further Reduce Pathogengs • If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Therrnophilic ❑ Beta Ray 0 Gamma Ray 0 Pasteurization Cl :` Class B: Alt. (1) Fecal Density IYI Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Aix Drying • [ Composting ❑ Aerobic Digestion f ' Anaerobic Di estion S If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen DensityNumber gExcee- of deuces Frequency of Analysis Sample Type Analytical Tech mane Minimum Geo. MeanMaximurr Units Fecal Coliform 2x10tothe P 6th power per gram of total solids MPN 'f�)© 1 1 3ICJQ pow" oU'Da 0 G Q.h 4ZUE-CX0 CFU 1000 rnpn pe gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal conform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ■ Alt, 3 (30-day bench) ❑ Alt. 4 (Spec, 02 uptake) IA Alt. 5 (14-Day Aerobic) 0 Alt. 6 (Alk, Stabilization 0 Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt, 10 (Incorporation) • No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) d "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you cheek this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." f �i�l�t°�b'l. nt {C j�i1Lal A{ irr a ZG C L .oroitildlc -y7/ • Prepare � ame and Title (type or print) gg Land Applier Name and � itle (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if plicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 1SA NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) OTOZ GREE VILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS G_ PHONE (252) 756-6208 FAX'(252) 756E-0633. ID#: 416 A DATE COLLECTED: 05/03/21 DATE REPORTED : 05/07/21 REVIEWED BY: Sample Sample Sample Sample Sample Analysis Method #1 #2 #3 #4 #5 Date Analyst Code Total Residue, mg/I 17540 Missing Missing Missing Missing 05/04/21 JMS 2540B-11 Fecal Coliform (MPN), /gram Solids 1300 Missing Missing Missing Missing 05/03/21 JMS 9221E-06 114 OAKMONT DR1V GREENVILLE, N.0 27858',; CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P,O, BOX 477 GRIFTON ,NC 28530 PARAMETERS Sample Analysis Method lit Date Analyst Code Total Residue, mg/1 17220 05/04/21 JMS 2540B-11 Fecal Coliform (MPN), /gram Solids 460 05/04/21 KDS 9221E-06 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 A DATE COLLECTED: 05/04/21 DATE REPORTED : 05/07/21 REVIEWED BY: 14 OAKMONT DFUVE PHONE '( a2) 756-620 GR ILLEM c 27858 FAX (252) 756-0633. CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Sample Analysis Method M3 Date Analyst Code Total Residue, mg/1 16620 05/06/21 CAW 2540E-11 Fecal Coliform (MPN), /gram Solids 200 05/05/21 JMS 9221E-06 ID#: 416 A DATE COLLECTED: 05/05/21 DATE REPORTED : 05/12/21 REVIEWED BY: ��✓L/J 114 OAKM©NT DF UVE PHONE',(252) 7 6-620€3 GC EENVILLE,''N.C. 27858 FAX (252) 756-0633`:' CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Sample Analysis Method 14 Date Analyst Code Total Residue, mg/1 18640 05/11/21 BLV 2540B-11 Fecal Coliform (MPN), /gram Solids 560 05/10/21 BLV 9221E-06 ID#: 416 A DATE COLLECTED: 05/10/21 DATE REPORTED 05/18/21 REVIEWED BY: ��� 141 OAKMONT'DRIVE PHONE (252) 75 -6208' GREENVILLE N.C. 27858 FAX (252) 756-0633' CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Sample Analysis Method #5 Date Analyst Code Total Residue, mg/1 18200 05/11/21 BLV 2540B-11 Fecal Coliform (MPN), /gram Solids 820 05/11/21 BLV 9221E-06 ID#: 416 A DATE COLLECTED: 05/11/21 DATE REPORTED : 05/18/21 REVIEWED BY: 1M-AEIg L [Pr .4 OAKMONT`DRIVE PHONE '(252)'756-6208 GREENVILLE,'N.C. 2 856 FAX (252) 756`-0633 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIP'TON, NC 28530 PARAMETERS Sample Analysis Method 116 Date Analyst Code Total Residue, mg/l 17640 05/19/21 JMS 2540B-11 Fecal Coliform (MPN), /gram Solids 3100 05/12/21 BLV 9221E-06 ID#: 416 A DATE COLLECTED: 05/12/21 DATE REPORTED : 05/25/21 REVIEWED BY: 4 OAKMONT DRIVE PHONE (252) 756-6208 .: GREENVILLE,`'N.C. 27858 FAX (252) 756-0633 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON, NC 28530 PARAMETERS Total Residue, mg/I Fecal Coliform (MPN), /gram Solids Sample Analysis Method #7 Date Analyst Code 18720 05/19/21 JMS 2540B-11 560 05/17/21 BLV 9221E-06 ID#: 416 A DATE COLLECTED: 05/17/21 DATE REPORTED : 05/25/21 REVIEWED BY: Specific Oxygen Uptake Rate SOUR 4\ Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level (mgli) Slope: 0.0 Intercept: 8.8 Correlation Coefficient: 1.0 Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: milliliters % Dry Solids degrees Celsius degrees Celsius 2.28 mg Oxygen/hr 0.13 mg Oxygen/g/hr 20 degrees Celsius 1 Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 8.9 8.8 8.7 8.6 a) E 8.5 c m a x 8.4 0 8.1 8 7.9 Oxygen Uptake Rate Chart y =-0.038x + 8.8755 1 2 3 4 5 6 7 8 9 Time (minutes) 10 11 12 13 14 15 16 Specific Oxygen Uptake Rate SOUR 4i Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level (mg/I) Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: milliliters % Dry Solids degrees Celsius degrees Celsius 0.0 8.6 1.0 2.37 mg Oxygen/hr 0.13 mg Oxygenlglhr 22 degrees Celsius 0.907029478 Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 8.8 8.6 8.4 1713 E a 8.2 T 0 a) 8 0 N 7.8 7.6 7.4 Oxygen Uptake Rate Chart y =-0.0395x + 8.609 1 2 3 4 5 6 7 8 9 Time (minutes) 10 11 12 13 14 15 16 Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level (mg/I) Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: milliliters % Dry Solids degrees Celsius degrees Celsius 0.1 8.1 1.0 4.19 mg Oxygen/hr 0.23 mg Oxygenlglhr 22 degrees Celsius 0.907029478 Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 8.4 8.2 7.8 ass E 7.6 a a x 7.4 0 m Z. 7.2 0 6.8 6.6 6.4 y =-0.0699x + 8.211 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 Time (minutes) 10 11 12 13 14 15 16 Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level (mgll) Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: milliliters % Dry Solids degrees Celsius degrees Celsius 0.0 8.8 1.0 2.91 mg Oxygen/hr 0.16 mg Oxygen/g/hr 21 degrees Celsius 0.952380952 Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 9 8.8 8.6 E = 8.4 0 8.2 0 w cn 8 7.8 7.6 1 Oxygen Uptake Rate Chart 2 3 4 5 6 7 8 9 Time (minutes) 10 11 12 13 y =-0.0485x + 8.8213 14 15 16 Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level (mg/I) Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: CMSD Andrew Edwards 5-10-21/1350 Windy Sammond milliliters Dry Solids degrees Celsius degrees Celsius 0.1 8.6 1.0 5,78 mg Oxygen/hr 0.31 mg Oxygen/glhr 22 degrees Celsius 0.907029478 Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygenlglhr Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically. Dissolved Oxygen (mg/I) 10 9 8 7 6 5 4 3 2 1 0 -1 y =-0.0963x + 8.71 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Time (minutes) Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level (mg/I) Scope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: CMSD WQ0001048 5/11/2021 5-11-21/1340 Andrew Edwards 5-11-21/1345 Windy Sammond 1000 1.89 0.1 9.0 1.0 milliliters Dry Solids degrees Celsius degrees Celsius 4.58 mg Oxygen/hr 0.24 mg Oxygen/g/hr 22 degrees Celsius 0.907029478 Temperature Corrected Specific Oxygen Uptake Rate: 0.22f mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 9.2 9 8.8 8.6 0 -a 8 m a Q N 7.8 b 7.6 7.4 7.2 7 y =-0.0763x + 9.0458 Oxygen Uptake Rate Chart 1 2 3 4 5 6 7 8 9 Time (minutes) 10 11 12 13 14 15 16 Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level (mg/I) Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: milliliters % Dry Solids degrees Celsius degrees Celsius 0.1 8.6 1.0 3.80 mg Oxygenlhr 0.20 mg Oxygenlglhr 18 degrees Celsius 1.1449 Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygenlglhr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 8.8 8.6 8.4 8.2 73) 5 c 8 a) x 0 7.8 0 W Vl 0 7.6 7.4 7.2 7 Oxygen Uptake Rate Chart y = -0.0634x + 8.6703 1 2 3 4 5 6 7 8 9 Time (minutes) 10 11 12 13 14 15 16 GROUNDWATER MONITORING LAB REPORTS GW-59A COMPLIANCE REPORT FORM Permit # tom (Submit one each monitoring period with GW 59 forms.) 1 Enter date monitoring results were due. ( 11- 2i.) Will this monitoring report (GW-59 and GW-59A) YES `x/ NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? 'YO NO IF the answer to question 1 or 2 is "YES;', list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the requirqd information. ue_did(i % rptexc -1-4"Ve— f tOtsdt5 Pcm e eat rnakrda( tab un` 12,-k-2L ' "Tht.'YOC. 06,6 rtic-(- Min kJW) 4-hi anal\f6(5 b-eCauoe c)-P pc•.6ervaQ) 15 tik514-P4_,2b-ilE> r Ur h-e6€Ll+5 (61 I l bezeibrni t i Nen�. � Th0(0 t O nP f -1l Z 1, t.l- ton vio.rePttem.1-4L-002. boo i s caicde©-CN-hi 5 i 6hue• 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Once for guidance. YES NQ �!( 4 Are any monitored constituents equal to or above the established standards? IS NO If the answer to question 4 is "NO', skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: Qe1I-4V16 -TeX- 11..ZLt 1L ChfomiUr() Zi) qkL o€.11 1g -MC 11.-LvLmcfL 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? 'YE$ �/ NO If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). t0 tJ Zc3 Ottt 4-1 -IOC tO,Z-?rn9Ib 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YESjq' J� If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YE$ NO If the answer to question 7 is "YES", doscribe those actions in the space provided below. If the answer to question 7 is "NO'; contact the Regjonal Office within 90 days; an evaluation may be required to determine the Impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. -rh e -roc 1Neb nC }" ict I N [-on 170Py(3 n �.p�ij L`r'2GL. Lacar e- Pr -Wart t ere p1'C coe 14J1:5-C-c�r c(rn i -rht, i yet' taid,e, i 5 fiery Gt) r4 -r.JPoo anaOrre_'o 1 cc bIt4V a lrne`'t i(1 lcfi��, M et4ed�in (e+morn a tounLit t r �fi ft$S oGr I r• ,nit i4,l I e h1` el errors um lra�-ran5 are m Wej a pe rl�t owl hl',c 'Ear i r� • u►1- . (DR- totZo io c6k:0.teo�i5 i sue . g The perso completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW 59 forms for required wells to the address provided at the top of the current G W-59 form. raTIVie6 a !not �. hat=lF�eFa o�`ve nto RI a e SSW as l o f io, 4 itIifi rAJA ` re o Y�" ` hee�,�or�GWrb9A�31s�fruekantl cornpleta�t�fii'i,e,;best� f�y�kno�vle�geAMV-"-�y`'l; Signature of permittee (or Authors d Agent) Date GW-59A 12/8/2003 GW-59A COMPLIANCE REPORT FORM Permit #oOcoiO4q (Submit one each monitoring period with GYY--59 forms) I Enter date monitoring results were due. ( ) I-3b;M) Will this monitoring report (GW-59 and GW-59A) YES )J NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? Y-ees J� NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain tho problems encountered in obtaining the required information. -Thky, f Ii.5 i nc'.it de.. lc,VOC,---1- i- tab ietrap) ed cn t i-l=2-)d Litio -ile era -ken I tiOC1L.iI(nl4he 0.Zc}Z1&rnPri 11Sevrr-r 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance. YES NO 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in tho space provided below: 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? YES NO If the answer to question 5 is "NO , skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last iwo years). 6 Are the monitoring wells listed in section S located at or beyond the review boundary? YES NO !f the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL. OFFICE IMMEDIATELY FOR GUIDANCE If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality problem? YES NO If the answer to question 7 is "YES', describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW 59 form. 'ti e y ae owl e b above it for o s ev a d liM;[loOVI sy iltd`d »t [ _ _r'epott (C,o • itaace Re oatkli9AjRfs' fi�u hdre tiOT tetto the bes gfkjacwledge -. { l Signature of Fermittee (or Author ••d Agent) Date GW-59A 12/8/2003 JIMI2d 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON, NC 28530 PARAMETERS Dxinking Water ID; 37715 Waste,W.ater__IP_1.0. PRONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 10/20/21 DATE REPORTED : 11/29/21 REVIEWED BY: ,Z�y Well #9 Well #10 Well ff14 Well 1115 Well #17 Analysis Method Date Analyst Code Fecal Coliform (MF), /100 MI5 <1 <1 <1 <1 10/20/21 CAW 9222D-15 Ammonia Nitrogen as N, mg/1 1.01 0.04 0.06 0.45 3.26 10/25/21 KES 350.1 R2-93 Nitrate Nitrogen as N, mg/I 0.14 0.33 <0.04 <0.04 0.14 10/20/21 KES 353.2 R2-93 Total Organic Carbon, mg/1 6.80 2.15 1.89 11.22 2.94 11/05/21 I-IMM 5310C-14 Chloride, mg/1 4 2 3 3 4 10/25/21 RLV 4500CLB-11 Total Dissolved Residue, mg/I 43 24 13 120 35 10/21/21 CAW D5907-13 Total Chromium, ug/I <5.0 <5.0 10 20 5 10/21/21 LFJ EPA200.7 Copper, ug/I <10 <10 <10 <10 <10 10/21/21 LEI EPA200.7 Conductivity (at 25c), uMhos/cm 66 35 34 139 43 10/25/21 HMV 2510E-11 Total Ortho-Phosphate as P, mg/I 0.03 0.04 0.02 0.07 0.07 10/21/21 KES 4500PE-11 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. 8OX 477 GRIFTON, NC 28530 PARAMETERS Fecal Coliform (MF), /100 Mls Ammonia Nitrogen as N, mg/I Nitrate Nitrogen as N, mg/I Total Organic Carbon, mg/I Chloride, mgll Total Dissolved Residue, mg/1 Total Chromium, ug/1 Copper, ug/1 Conductivity (at 25c), uMhos/cm Total Ortho-Phosphate as P, mg/I Well #18 Analysis Method Date Analyst Code 2 10/20/21 CAW 9222D-15 0.10 10/25/21 KES 350.1 R2-93 <0.04 10/20/21 ICES 353,2 R2-93 11.42 11/05/21 HMM 5310C-14 3 10/25/21 BLV 4500CLB-11 100 10/21/21 CAW D5907-13 <5.0 10/21/21 LFJ EPA200.7 <10 10/21/21 LFJ EPA200.7 135 10/25/21 HMV 2510E-11 0.03 10/21/21 KES 4500PE-11 PHONE (252) 756-6208 FAX (252) 756-0633 ID*: 416 DATE COLLECTED: 10/20/21 DATE REPORTED : 11/29/21 REVIEWED BY: Environment 1, Incorporated SEA Ord tom t� <i it 2€t j%i�'ii�1�5W txlk�,r�,�E CLIENT: CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BO 477 GRIRTO REVIEWED BY VOLATILE ORGANICS METHODS 6200C-11 CLIENT ID: 416 ANALYST: JAP DATE COLLECTED: 11/17/21 DATE ANALYZED: 11/25/21 DATE REPORTED: 12/17/21 S52),17WWW02 7S 252) 7 6;0 Page: 1. PARAMETERS, ug/1 Well #9 Well #10 Well #14 Well #15 Well #17 1. Benzene <0.50 <0.50 <0.50 <0.50 <0.50 2. Bromobenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 3. Bromochloromethane < 0.50 < 0.50 < 0.50 < 0.50 < 0,50 4. Bromodichlo:•ornethane < 0.50 < 0.50 < 0.50 < 0,50 < 0.50 5, Bromoform < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 6. Bromomethane <0.50 <0.50 <0.50 <0.50 <0.50 7. N-Butylbenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 8. Sec Butylbenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 9. Tert-Butylbenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 10. Carbon Tetrachloride < 0.50 < 0.50 < 0.50 < 0,50 < 0.50 11. Chlorobenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 12. Chloroethane < 0.50 < 0.50 < 0.50 <0.50 < 0.50 13. Chloroform < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 14. Chloromethane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 15. 2-Chlorotoluene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 16. 4-Chlorotoluene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 17. Dibromochloromethane < 0.50 < 0.50 <0.50 < 0,50 < 0.50 18. 1,2-Dibromo-3-Chtoropropane < 0.50 < 0.50 <0.50 < 0.50 < 0.50 19. 1,2-Dibromoethane < 0.50 < 0.50 <0.50 < 0.50 < 0.50 20. Dibromomethane < 0.50 < 0.50 <0.50 < 0.50 < 0.50 21. 1,2-Dichlorobenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 22. 1,3-Dieliorobenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 23. 1,4-Dichlorobenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 24, Dichlorodifiuoromethane < 0.50 < 0,50 < 0.50 < 0.50 < 0.50 25. 1,1-Diehloroetl:ane < 0.50 < 0,50 < 0.50 < 0.50 < 0.50 26. 1,2-Dichloroethane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 27. 1,1-Dichloroethene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 28. Cis-1,2-Dtchloroethene < 0.50 < 0.50 < 0.50 <0.50 < 0.50 29. trans-1,2-DichIoroethene < 0.50 < 0.50 < 0.50 <0.50 < 0.50 30. 1,2-Diehloropropane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 31. 1,3-Dichloropropanc < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 32. 2,2-Diehloropropane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 33. 1,1-Dichloropropene < 0.50 < 0.50 < 0.50 <0.50 < 0.50 34. Cis-1,3-Dichloropropene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 35. trans-1,3-Dichloropropene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 36. Eutylbenzene < 0.50 < 0.50 < 0.50 < 0.50 <0.50 37. Hexachlorobutadiene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 38. lsapropylbenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 39. 4-lsopropyltoluene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 40. Methylene Chloride < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 41. Naphthalene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 42. Propylbenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 43. Styrene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 44. 1,1,1,2 TetrachIoroethane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 45. 1,1,2,2-Tetrachloroethane < 0.50 < 0.50 < 0.50 < 0.50 <0.50 46. Tetrachloroethene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 47. Toluene < 0,50 < 0,50 < 0.50 < 0.50 <0.50 48. 1,2,3-Tricblorobenzene < 0,50 < 0.50 < 0.50 < 0.50 < 0.50 Environment 1, Incorporated 'T' n 14;wivaitr q,[4 - 'Y : ill MW i tIO2 7VIZ ti e .trig ", r r A 9t,.€4,S iY t 41E0 35i1 CLIENT: CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. 1 OX 477 f'1 1 1 GRIP, �j7s NC/f 2853 REVIEWED BY: VOLATILE ORGANICS STD. METHODS 6200C-11 CLIENT ID: ANALYST: DATE COLLECTED DATE ANALYZED: DATE REPORTED: J°JEP r(JJf la�'J f rJ��ll Ali �laJilJJs�jf`l!€:},'�,.�J��!;J�lii�l f:�,�cs:•ti13Pi�ei�: �i3;�=;.�;= ypas( �:i+' ;A 416 TAP : 11/17/21 11/25/21 12/17/21 Pages 2 PARAMETERS, ug/l Well #9 Well #10 Well #14 Well #15 Well #17 49. 1,2,4-Trichlorobenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 50. 1,1,1-Trlehloroethane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 51. 1,1,2-Trichloroethane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 52. Trichloroethene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 53. Triehlorofluoromethane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 54. 1,2,3-Trichloropropane < 0.50 < 0.50 < 0.50 < 0.50 < 0,50 55. 1,2,4-Trimethylbenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 56. 1,3,5-Trlmethylbenzene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 57. Vinyl Chloride < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 58, Total Xylenes < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 59. Methyl Tert Butyl Ether < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 Environment 1, incorporated .4a ? Qa_i34�C 7p 5� 1 iE Mi$109 "iGR>:�NV1Ll,�.�1C x,27Q�5z.7,Qej gfix-y'I CLIENT: CMSD (SLUDGE & WELLS ACCT) CONTZNTNEA METRO. SEWAGE DIST. MS. REIM PRTD iEN P.O. BOX 477 ORTFT. , NC 28530 REVIEWED BY: \s CLIENT ID: .33 4 16 ANALYST: OAP DATE COLLECTED: 11/17/21 DATE ANALYZED: 11/25/21 DATE REPORTED: 12/17/21 VOLATILE ORGANICS STD. METHODS 6200C-11• Well #18 PARAMETERS, ug/i 1, Benzene 2. Bromohenzene 3. Bromochloromethane 4, Bromodichloromethane 5. Bromoform 6. Bromomethane 7. N-Butylbenzene 8. Sec-Butylhenzene 9. Tert-Butylbenzene 10. Carbon Tetrachloride 11, Chlorobenzene 12. Chloroethane 13. Chloroform 14. Chloromethane 15. 2-Chlorotoluene 16, 4-Chlorotoluene 17. Dibromochloromethane 18. 1,2-Dihromo-3-Ch ioropropane 19. 1,2-Dibroroethane 20. Dibromonkethane 21. 1,2-Dichlorohenzene 22. 1,3-Dichiorohenzene 23. 1,4-Dichlorobenzene 24. Dichlorodifluoramethaue 25. 1,1-Dichloroethane 26, 1,2-Dichloroethane 27. 1,1-Dichloroethene 28. Cis-1,2-Dichloroethene 29. trans-1,2-Dichloroethene 30. 1,2-Dichloropropane 31. 1,3-Dichloropropane 32, 2,2-Dichloropropane 33. 1,1 Dichloropropene 34. Cis-1,3-Dichloropropene 35. trans-1,3-Dichloropropene 36. Etliylbenzene 37. Hexachlorobutadiene 38. Isopropylbenzene 39. 4-Isopropyltoluene 40. Methylene Chloride 41. Naphthalene 42. Propylbenzene 43. Styrene 44. 1,1,1,2-Tetrachloroethane 45. 1,1,2,2-Tetrachloroethane 46. Tetrachloroethene 47. Toluene 48. 1,2,3 Trichlorobenzene <0.50 <0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0,50 < 0,50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 <0.50 <0.50 <0.50 <0.50 < 0.50 < 0.50 < 0.50 < 0.50 <0.50 < 0.50 <0.50 < 0.50 <0.50 < 0.50 <0.50 < 0.50 < 0.50 < 0.50 < 0.50 X-( klt 6.47'0334 Page: 3 Environment 1, Incorporated 'ha S9 �f.[1r+3�t'-E;{�" _ �s �z�R sss_,�r �3€%_ " k4 `�}�t; �ii.,� �"c- ix•r �'�4 {Lx� y''�����xiS`7 �.�'Y�} c �ry °-i- _��.4 �i f,'T C' • j'L.S t� s4F '�`�It! pit i�l' J FI ' :f1it[.fi . 7i l E 6' r CLIENT: CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. B X 477 C,RxrTO, ,, NC 2f8530 REVIEWED B VOLATILE ORGANICS STD. METHODS 6200C-11 CLIENT ID: T;5tr,Dlv�hl�aI�i4liti�5`83,xb0 �3371�RI6'i 416 ANALYST: d'AP DATE COLLECTED: 11/17/21 DATE ANALYZED: 11/25/21 DATE REPORTED: 12/17/21 PARAMETERS, ug/i Welt #18 49. 1,2,4-Trichtorobenzene < 0.50 50. 1,1,1-Trichloroethane < 0.50 51. 1,1,2-Trichloroethane < 0.50 52. Trichloroethene <0.50 53. Trichlorofluoromethane <0.50 54. 1,2,3-Trichtoropropane < 0.50 55. 1,2,4-Trimethylbenzene < 0.50 56. 1,3,5-Trimethylbenzene < 0.50 57. Vinyl Chloride < 0.50 58. Total Xylenes < 1.00 59. Methyl Tert Butyl Ether < 1.00 Page: 4 EHATORNIg 1 U 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. SOX 477 GRIFTON, NC 28530 Well #9 Analysis Method PARAMETERS Date Analyst Code Fecal Coliform (MF), /100 Nils <1 10/28/21 BL.V 9222D-15 Arinking Wetter' Waatewater. PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 10/28/21 DATE REPORTED : 11/01/21 REVIEWED BY: SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Mail original and 1 copy to: Permit Name (if different): %if ea---- 1n>�� Facility Address: ?YY h_,) I . n5 -7O}" j( Lin GrlZ IStreei �(�5 County rj 44-- ICioyl [Statel 12ip7 Contact Person: eiIltll}€[k Well Location/Site Name:..1)(4 CCU_ plor t6(+ C. Telephone#: r7 5%i-j6j0. No. of wells to be sampled: Co (from Permit) 'OW .• ! OF a- RoMIAE ii3ATIKQW: a MOO NFO D PROGESalN`� WV .._.. aOURCES u pig 14SERIIIe CENIER G N a 769916 m- on?49t5 80�-s3D,E PERMIT Number: Expiration Date: 47-3.J-zoz Non -Discharge It C 104-S' UIC NPDES L j3 tip Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery D Spray Field ❑ Remediation: ❑ Rotary Distributors Land Application of Sludge El Water Source Heat Pump El Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: ft. Depth to Water Level 82546: to ft- below measuring point Measuring Point is % 5 ft. above land surface Date sample collected: )0--Z--21 Well Diameter: Screened Interval: 3 ft. to ' ft. RelativeM.P. Elevation: ft Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: [']YES ❑ NO and field acidified: IA YES ❑ NO FIELD ANALYSES: pH 00400: 4:q units Temp. won: °C Spec. Cond. 00094: tocfo µMhos Odor 00085: 1)00t Appearance C-Ve l` If WELL WAS DRY at time of sampling, check here: LABORATORY INFORMATION Date sample analyzed: lid-70-Z.geral IQ-ZQ-l( PARAMETERS NOTE: Values should reflect dissolved COD 00335 Coliform: MF Fecal 31515 Coliform: MF Total 31504 (Nate: Use MPN method for highly turbid samples) mg/L I100mL /100mL Dissolved Solids:Total 70300 L1-5 mglL pH (Lab) 00403 4 .Cr units TOC 00680 (o _S.O mg/L Chloride 0c94o g mg/L Arsenic 01002 uglL Grease and Oils 00552 mglL Phenol 32730 ug/L Sulfate 00945 mg/L Specific Conductance 00095 (!, p.Mhos Total Ammonia 00s10 I , o j mglL (Ammonia Nitrogen: NH3 as N; Ammonia Nitrogen, Total) TKN as N 00625 mg/L Laboratory Name: and colloidal concentrations Nitrite (NO2) as N 00616 Nitrate (NO3) as N 00520 Phosphorus: Total as P 00665 Orthophosphate 70507 Ai - Aluminum o11as Ba - Barium 01007 Ca - Calcium 00916 Cd - Cadmium 01027 Chromium: Total 01034 grN f (an pnern+ I1 I nc • 0.14- p,p3 <5•U Cu - Copper 61042 <G 010, Fe - Iron o1 oas Hg - Mercury 71900 K - Potassium D0937 Mg - Magnesium 00927 Mn - Manganese 01055 Ni - Nickel 01067 mg/L mg/L mglL mg/L Other (Specify Compounds and Concentration Units): mg/L Certification No. dG ug/L mg/L uglL Pb - Lead 01051 Zn -Zinc Dio92 uglL mg/L ug/L mg/L ORGANICS: (by GC, GC/MS, HPLC) ug/L (Specify test and method #. ATTACH LAB REPORT.) uglL Lab Report Attached? ❑ Yes (1) ❑ No (0) mg/L VOC 7873 , method # mglL ug/L ug/L , method # , method # , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mglL VOC Removal% 1 certify that, to the best of my knowledge and belief, the information submilted in this report is true, accurate, and complete: and that the laboratory analytic-aat data taus produced using approved methods of analysis by a 15WR-certified laboratory. 1 am aware that there are significant penalties for submitting false information, including the possibility ai tiri s and imprisonment for knowing violations. cnctrl3 rn om ; a.-h lei ck.)�r . i � G manCf 1Z- -2A Permittee (or Authorized Agent) Name and Title - Please int or type gy Sign ure of Permittee (or Authorized Agent) (Date) GW-59 Rev. 3-1-2016 SUBMIT FORM ON YELLOW PAPER ON GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Cc +e- eC�- MO-0 Mail original and 1 copy to: Facility Name: Permit Name (if different): fc °f4€le0-. j-7 61) Facility Address: i c�ss qc l }1 aori17� e-"Pcra, [Fr) G4' eet) str14G (.g53c {City) [Stale} IZip} Contact Person: (' ec)-,(1'l1-hk.L 1 CC, Well Location/Site Name: 0 Q r-i \ u County ( of iNENTOPENV1RDNMENT QUA lY D O WAFERIRESDORCEsr 64 .SERVICE•CEN7Ef2; ' G "taZgy ` ane el• 30 1 DRINA O PROCESS Telephone#: ZoZ 5 z No. of wells to be sampled: (from Permit) PERMIT Number: Expiration Date: Non -Discharge s I oL UIC NPDES MCC ,32(j7}) Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor CZ Land Application of Sludge El Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: S' ft. E 0 Date sample collected: 13--Zi >-Z) Depth to Water Level 82546: C_. . 3 ft. below measuring point Measuring Point is 3 ft. above land surface Volume of water pumped/bailed before sampling: Samples for metals were collected unfiltered: ® YES Well Diameter. 7 in. Screened Interval: a ft. to g ft_ Relative M.P. Elevation: ft. gallons ❑ NO and field acidified: I YES ❑ NO FIELD ANALYSES: pH oo400:5• d units Temp. 00o10: ZZ DC Spec. Cond. 00094: 05 )Mhos Odor 00085: n cot Appearance car If WELL WAS DRY at time of sampling, check here: LABORATORY INFORMATION Date sample analyzed: ) D--JQ-� PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD ooss5 Coliforrn: MF Fecal 31616 <1 Col€form: MF Total 31504 (Note: Use MPN method for highly turbid samples) Dissolved Solids:Total 7oso0 pH (Lab) 00403 TOC 00680 Chloride 0o9a0 Arsenic 01002 Grease and Oils 00552 Phenol 32730 Sulfate 00945 •Specif€c Conductance 00095 ZL4 6.0 Z. t5 Total Ammonia cosio (Ammonia Nitrogen; Nli3as N: Ammonia Nitrogen, Total) TKN as N 00625 mg/L /100mL /100mL mg/L units mg/L mg/L ug1L mgfL ug/L rng/L ttMhos mg/L mg/L Nitrite (NO2) as N 00615 Nitrate (NO3) as N 00620 Phosphorus: Total as P 00665 Orthophosphate 70507 Al - Aluminum 01105 Ba - Barium o1007 Ca - Calcium 00916 Cd - Cadmium 01027 Chromium: Total 01034 Cu - Copper 01042 Fe - Iron o1045 Hg - Mercury 71900 K - Potassium 00937 Mg - Magnesium 00927 Mn - Manganese 01055 Ni - Nickel 01067 Laboratory Name: b)1 f - I) I(�. 0-33 0,oy <0,0)O mg/L mg/L mg/L mg/L mg/L ugfL mg/L ug!L ug1L mg/L ug/L ug1L mg/L mg/L ug!L ug1L Pb - Lead 01051 Zn - Zinc 01092 Certification No. IQ ug!L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) 0 No (0) VOC 7873 , method # method # , method # , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% certifylhat, to the best of my knowledge and belief, the information submitted in this report is true. accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of (cries and imprisonment for knowing violations. Caile3in,brni i eLF�-. �i i6-mar ev Permittee (or Authorized Agent) Name and`ritfe- Please print or type Signature of Permittee (or Authorize �i Agent) lZ 2) (Date) GW-59 Rev. 3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: C(_)(7-*P --PrVa.- rnaD Permit Name (if different): C OIl-}- rre[t-M'O,j7 Facility Address: qc I,JS 1 (-rn6V 5 TO J LF"7 ) C, ac53D County PH- l�l i :?foTh latreett (City) Muriel Contact Person: rttIC11, I h.,JiC.r Well Location/Site Name: ( I-k.\\I L1 g z p) Mail original and 1 copy to: Telephone#: 75.7-521 55' I - No. of wells to be sampled: (p (from Permit) CEPARi 7 0 r�TlVliiONMENTAL QIJ D OFiWATE y OURCES INFORMA� OCESSI U IVIAWSERVICeCEMER.t�uR pn, i 599c 6 i P one. 9 9 -6306 PERMIT Number: Expiration Date: ,-3.1-Z'35 Non -Discharge ,°�Q/,Q4-g UIC NPDES 'I.ficO3Z $ f Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Spray Field ❑ Rotary Distributor Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: ❑ Remediation: Infiltration Gallery ❑ Remediation: SAMPLING INFORMATION WELL ID NUMBER (from Permit): Weil Depth: 13 ft 14 Depth to Water Level a2546: 10.1 7 ft. below measuring point Measuring Point is z, ft above land surface Date sample collected: 13-6Z.f Well Diameter: Z. in. Screened Interval: ft_ Relative M.P. Elevation: to 13 ft. ft_ Volume of water pumped/bailed before sampling: 5 gallons I� Samples for metals were collected unfiltered: El YES ❑ NO and field acidified: YES ❑ NO FIELD ANALYSES: pH c04o0: S. 1 units Spec. Cond. 00094: 3-11' µMhos Odor moss: n ( t Appearance dear If WELL WAS DRY at time of sampling, check here: LABORATORY INFORMATION Date sample analyzed: j{ Z 7r7„� Laboratory Name: EMI feri[ r) j- ).11-c. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Coliform: MF Fecal s1s1s < 1 /100mL Coliform: ME Total 31504 /100mL {Note: Use MPN method far highly turbid samples) Dissolved Solids:Total 70300 13 mg/L pH (Lab) 00403 5. units TOC cosao )-�1 mg/L Chloride 00940 3 mg/L Arsenic 0-1002 uglL Grease and Oils 00552 mg/L Phenol 32730 uglL Sulfate oos45 mg/L Specific Conductance moss µMhos Total Ammonia oos10 0 _ 0Lp mg/L mg/L t34 (Ammonia Nitrogen: NI-13as N; Ammonia Nitrogen, Total) TKN as N 00625 Nitrite (NO3) as N 00615 Nitrate (NO3) as N 00620 Phosphorus: Total as P o066s Orthophosphate 70507 Al - Aluminum oi105 Ba - Barium 01007 Ca - Calcium Duals Cd - Cadmium 01027 Chromium: Total 01034 Cu - Copper o1042 Fe - Iron 01045 Hg - Mercury 71900 K - Potassium 00937 Mg - Magnesium 09927 Mn - Manganese 01055 Ni - Nickel 01067 <0.04 10 <ps010 mg/L mg/L mg/L mg/L mgJL ug!L mg/L ug(L uglL mg/L ug/L ug/L mg/L mg/L ugfL ug!L Pb - Lead 01051 Zn - Zinc 010s2 Temp. 000le: zj °C Certification No. Jti ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (I) ❑ No (0) VOC 7673 , method # , method # , method # , method # For Remediation Systems Only (Attach Lab Reports): influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information Submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of f: ie_ and imprisonment for knowing violations. C `ai 1e) rn- & ONoi C �C DI d- r v . f Permittee (or Authorized Agent) Name and Ti e - Please print or type Signature of Pennittee (or Authonzed Agent) (Date) GW-59 Rev.3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type C af\-+e fa. m Facility Name: Permit Name (if different): Con-1 -info- mop Facility L����� (_,�' t (sweet] Address: (�0 �C]'f lL�� (�CtbY 1(�C� � f'Lin (City] Contact Person: (Slate) (Zip) ChuCirn\aLinw[ d.C, Well Location/Site Name: iN-(2(.6 -1 ,..i2,4CUL °d-, .2(Ci lQ County Nl' Telephone#: Z5Z 5zq 560-1 No. of wells to be sampled: (9 (from Permit) DEp aRTNiENROFr PIVIROI w! 4[i11I 17.1r l NFORMATIOIC RocESSIN aF,VILIETF,RTESOURCESZkg PERMIT Number: Expiration Date: Non -Discharge tt,,er6r)04412 U1C NPDES }-.cco j7 ('s-r) Other R-31 - ZoZS TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Spray Field ❑ Rotary Distributor ❑ Water Source Heat Pump ❑ Remediation: Infiltration Gallery ❑ Remediation: fg Land Application of Sludge ❑ Other. SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: g ft. Depth to Water Level 62546: � ft. below measuring point Measuring Point is Z. 5 ft. above [and surface Volume of water pumped/bailed before sampling: 5 Samples for metals were collected unfiltered: 1 J YES Date sample collected: —7.0'2.-[ Well Diameter: Z in. Screened Interval: 3 ft. Relative M.P. Elevation: gallons ❑ NO and field acidified: 'YES ❑ NO FIELD ANALYSES: pH 0040051 3 units Temp. aoolo: ZJ °C to p ft. Spec. Cond_ 00094: 1-aq µMhos ft_ Odor 00085: non-e- Appearance Cloudy If WELL WAS DRY at time of sampling, check here: LABORATORY INFORMATION Date sample analyzed: 10 2 -2-1, Laboratory Name: -fi N1 hiN Z) y(c. - PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 Coliform: MF Fecal 31616 Coliform: MFTotal 31504 < (Note: Use MPN method for highly turbid samples) Dissolved Solids:Total 70300 pH (Lab) 00403 TOC 00680 1 i .zZ mg/L Chloride 00940 Arsenic 010oz Grease and Oils 00552 Phenol 32730 Sulfate 00945 Specific Conductance 00095 Total Ammonia 00610 3,. Li'S mg/l.. mg/L /100mL /100mL Zb mg/L 5 3 units .3 !q (Ammonia Nitrogen: NH,as N; Ammonia Nitrogen. Total) TKN as N 00625 mg/L ug/L mg/L ug!L mg/L µMhos mg/L Nitrite (NO2) as N 00615 Nitrate (NO3) as N 00620 Phosphorus: Total as P 00665 Orthophosphate 70507 Al -Aluminum o1105 Ba - Barium o1007 Ca - Calcium 00916 Cd - Cadmium 01027 Chromium: Total 01034 Cu - Copper 01042 Fe - Iron 01045 Hg - Mercury 71900 K - Potassium 00937 Mg - Magnesium 00927 Mn - Manganese moss Ni - Nickel 01067 Gc o-i- ©, 07 mg/L mg/L mg/L mg/L mglL ug/L mg/L ug/L ug!L Pb - Lead o1051 Zn - Zinc 01092 Certification No. f{J uglL mg/L Other (Specify Compounds and Concentration Units): CD,O10 mg/L ORGANICS: (by GC, GC/MS, HPLC) ug/L (Specify test and method #. ATTACH LAB REPORT.) uglL Lab Report Attached? mg/L VOC 7873 mg/L uglL uglL ❑ Yes (1) ❑ No (0) , method # , method # , method* , method # For Remediation Systems Only (Attach Lab Reports): influent Total VOCs: mg/L Effluent Total VOCs: mglL VOC Removal% I certify that, to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete. and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for k^awing violations. Chat] `)m-am•ik-D11,Jif ia_ 'trill] eel Permittee (orAuthorized Agent) Name and Title- Ple e print or type v Signature of Permittee (or Authorized Agent) (Date) GW-5g Rev.3-12016 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Cknn . Permit Name (if different): i -r\eQ.. }poi Mail original and 1 copy to: Facility Address: co lit I el, ('-�toluti6 46L (477-) 14G ZA53o 4tG+a, tStre6tj (City) (Stalel (Zip) Contact Person: Chtglbarn4123 Well Location/Site Name: 6, corner C p(ei6 IG? No. of wells to be sampled: Co County Telephone#: Z 6Z-LFG SLi {from Permit) as-DEPARTMENVOF ENA1ROMNRiiii NFORMknoP acEss1M iscr 141 sE1 vicEE RAL G„, NC Z699 ►k OtIRG 1 ?hone. 996 -630 PERMIT Number: Expiration Date: g-3(-ZOZ5 Non -Discharge ,WOC)I 53 U€C NPDES j-4(_c 3%j5)) Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery O Spray Field El Remediation: O Rotary Distributor NI Land Application of Sludge ❑ Water Source Heat Pump ❑ Other. SAMPLING INFORMATION WELL ID NUMBER (from Permit): Well Depth: ft. 1-7 Date sample collected: ;o zo zi Well Diameter: L in, Depth to Water Level 62546: (p•Z ft. below measuring point Screened Interval: Z ft. to q ft. Measuring Point is z. 35 ft above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: (] YES 0 NO and field acidified: Egi YES ❑ NO FIELD ANALYSES: pH 00400:4 g units Temp. cool 0: ZZ °C Spec. Cond. 00094: 43 ',Mhos Odor across: I ib7)t Appearance cs If WELL WAS DRY at time of sampling, check here. LABORATORY INFORMATION Date sample analyzed: 1(-2 j-Z1 Laboratory Name: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oos15 Cal-rform: MF Fecal 31616 Coliform: MF Total 31504 {Note; Use MPN method for highly turbid samples) C /100mL ]issolved Solids:Total70300 pH (Lab) 00403 TOC 00680 Chloride 00940 Arsenic o1002 Grease and Oils 00552 Phenol 32730 Sulfate 00945 Specific Conductance 00095 Z•G4 (-13 Total Ammonia 00610 %3.2 2 (Ammonia Nitrogen; NHS as N; Ammonia Nitrogen. Total) TKN as N 00625 /100mL mg/L units mg/L mglL ug/L mg/L uglL mg/L (.(Mhos mg/L mg/L Nitrate (NO3) as N 00620 Phosphorus: Total as P 00665 Orthophosphate 70507 Al -Aluminum o11os Ba - Barium o1007 Ca - Calcium 00916 Cd - Cadmium o1027 Chromium: Total 01034 3.14- mg/L mg/L mg/L mg/L Cu - Copper 01042 <.r,p l( Fe - Iron 01045 Hg - Mercury 71900 K - Potassium 00937 Mg - Magnesium 00927 Mn - Manganese 01055 Ni - Nickel 01067 mg/L uglL mg/L uglL ug/L mg/L uglL ugfL mg/L mg/L ug/L ug/L Pb - Lead 01051 Zn - Zinc 01092 Certification No. uglL mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 , method # , method # , method # , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mglL VOC Removal% I certify that, to the best of my knowledge and belief. the information submitted in this report ie true. accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of f res and imprisonment for knowing violations. ChouIre,S 1. l Lvt(Y l r7l. icVsfQre' Perrnittee (or Authorized Agent) Name and tie - ease print or type Sign (aLoermittee (or Authorized Agent) I C✓-(0 Z! (Date) GW-59 Rev. 3-1-2016 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: CaYFtLT r)sea-. 3/ Permit Name (if different): Con+r)"_(naD Facility Address: �()(�j P,k.)11 C-0,56r) kd �O i ISlreetj t 4 C 7C55 3' (Cilyl (Slate) (Zip) Contact Person: ChUCt,a-niC1/10 CL— Well Location/Site Name: to •P i.1+13 County Mail original and 1 copy to: Telephone#: 75Z-5Z S'L/ No. of wells to be sampled: (, {from Permit) DEPARTMENTA0 a D ENT 011A1_'I1Y UIV,'.O { INF•OR D PROCESSI 6 t7111A1L SERVIC�CEENIER, RALEIGW, ate m..�:� ..�,-_,...�..�-.k.�.. 27,69, 1B11 P one. 91 e63. PERMIT Number: Expiration Date: Non -Discharge 1N OW LAC NPDES C}ZZi) Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Remediation: Infiltration Gallery 0 Lagoon 0 Spray Field ❑ Remediation: 0 Rotary Distributor giLand Application of Sludge 0 Water Source Heat Pump 0 Other. SAMPLING INFORMATION WELL ID NUMBER (from Permit): (c2 Well Depth: r fit_ Depth to Water Level 82546: 1,3 ft. below measuring point Measuring Point is Z ft above land surface Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: al YES 0 NO and field acidified: YES ❑ NO Date sample collected: 6- -'ZI Well Diameter Screened Interval: 5 it Relative M.P. Elevation: LABORATORY INFORMATION Date sample analyzed: _ZO-u Laboratory Name: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 CORfOrm: MF Fecal 31616 7- mgfL Nitrite (NO2) as N 00615 f100mL Nitrate (NO3) as N 00620 Coliform: MF Total s15o4 1100mL (Note: Use MPN method for highly turgid samples) Dissolved Solids:Total 70300 fW pH (Lab) 004o3 5. 5 TOC 00680 Chloride o0940 Arsenic o1002 Grease and Oils 00552 Phenol 32730 Sulfate 00945 Specific Conductance 00095 IL•47_ 3 t1)� Total Ammonia ooslo ©• 1 Q (Ammonia Nitrogen: NH, as N: Ammonia Nitrogen, Total) TKN as N 00625 mg/L units mg/L mg/L uglL mglL ug!L mg/L })Mhos mg/L mg/L to LC ft. ft. FIELD ANALYSES: pH 00400: 6.5 units Spec. Cond. 00094: Temp. oo0lo: 1 U5 (.Mhos Odoroaos5: nc(Y°L Appearance C ear EnvCrc ) me.fyl Phosphorus: Total as P 0066s Orthophosphate 70507 Al - Aluminum o11os Ba - Barium 01007 Ca - Calcium Dom Cd - Cadmium o1027 Chromium: Total 01034 Cu - Copper 01042 Fe - Iron 01045 Hg - Mercury 71900 K - Potassium 0as37 Mg - Magnesium 00027 Mn - Manganese 010s5 Ni - Nickel 01067 <G.D4 o. 5- Certification No. I mglL Pb - Lead oi051 ugtL mg/L Zn - Zinc 01092 mg/L mg/L mg/L Other (Specify Compounds and Concentration Units): mg/L uglL mg/L uglL 5.p ug!L if WELL WAS DRY at time of sampling, check here: <0.010 mglL ORGANICS: (by GC, GC/MS, HPLC) uglL (Specify test and method #. ATTACH LAB REPORT.) uglL Lab Report Attached? ❑ Yes (1) ❑ No (0) mg/L VOC 7873 , method # mg/L ug/L uglL , method # method## , method # L For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWRcertified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of !lies p.;Id imprisonment for knowing violations. ChoF'O- ` ithiGiC -DrT " r 07 Permittee (or Authorized Agent) Name and die - lease print or type Signature of Pennittee (or Authorized Agent) (Date) GW-59 Rev. 3-1-2016 UXink3ng Water in$ 37714 durramoinlig ig Elgllcupervad ����N171t CMSD (SLUDGE & Wi us ACCT) CQNTENTNEA METRO. SEWAGE DXST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON, NC 28530 PARAMETERS Total Chromium, t:gll Copper, ttg/I Well #15 Analysis Method Date Analyst Code 5 12/23/21 LF<.J EPA200.7 <10 12/23/21 LFJ EPA2.00.7 252),756.108i ID# : 416 DATE COLLECTED: 12 /2 L/21. DATE REPORTED : .01/07/22 REVIEWED BY: SOILS ANALYSIS LAB REPORTS LIME APPLICATION NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomi/ Report No. FY22-SL009409 Client: CMSD Advisor: Ayden Nitrogen- PO Box 477 Ayden Nitrogen Grifton, NC 28530 P.O. Box Mehlich-3 Extraction Ayden, NC Report Sampled County :Pitt to Helpful Information Primary 7 28513 F0 `s,k Predictive '' E' r r. Soil Links Sampled: 10/01/2021 Received: Client ID: 147385 Advisor ID: 503187 10/14/2021 Completed: 10/29/2021 Farm: Wiley Gaskins Agronomist's Comments: ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce potential for toxicity, especially for Zn. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped. The CTL for copper and zinc was set to Prevent levels from accumulating to the point where they become toxic to crops grown on a field. Sample ID: 1 Lime History: Recommendations: Lime . Nutrients (lb/acre) .............. More Information Note: 12 Note: $ Crop (tons/acre) N P2O5 K20 Mg S Mn Zn Cu B 1 -Bermuda hay/past., E 0.0 60-80 0 90 0 0 0 Z 0 0 2 - 0.0 Test Results [units - WN in glcm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.56 1.07 13.0 90 1.3 6.4 853 22 69 20 36 56 44 2208 2208 1195 0.1 1 Sample ID: 2 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Note: $ Crop (tonslacre) N P205 K2O Mg S Mn Zn Cu B 1 - Bermuda hay/past., E 0.0 60-80 0 70 0 0 pH$ Z 0 0 2 - 0.0 Test Results [units - WN in glcm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-1 Mn-I Mn-AI1 Mn-Al2 Zn-1. Zn-Al Cu-I Na ESP SS -I NO3-N 0.56 1.07 13.4 91 1.2 6.6 836 33 69 21 35 56 42 2267 2267 888 0.1 1 North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Tobacco Trust Furad Commist+io s NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomil Report No. FY22-SL009409 Page 2 of 11 Sample ID: 3 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Note: 3 Crop (tonslacre) N P205 1 -Bermuda hay/past., E 0.6 60-80 0 2 - 0.0 K20 80 Mg S Mn Zn 0 0 0 Z Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm31: HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% 0.60 1.01 13.0 81 2.4 5.8 881 29 61 19 S-I 52 Mn-I 54 Soil Class: Mineral Mn All Mn-Al2 Zn-I Zn-AI 49 2429 2429 Cu-I 1271 Na 0.2 ESP 2 SS-1 NO3-N Sample ID: 4 Lime History: Recommendations: Lime Nutrients (Iblacre) More Information Note: 12 Note: $ Crop (tonslacre) N P205 1 -Bermuda hay/past., E 0.3 60-80 0 2- 0.0 K20 80 Mg S Mn Zn 0 0 0 Z Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in megl100 cm3; NO3-N in mgldm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.46 1.00 13.8 83 2.3 5.9 928 30 63 19 S-I 47 Mn-I 62 Soil Class: Mineral Mn-AI1 Mn-Al2 Zn-1 Zn-AI 54 3863 3863 Cu-1 1377 Na 0.2 ESP 1 SS -I NO3-N Sample ID: 5 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Note: $ Crop (tonslacre) N P205 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 K20 110 Mg S Mn Zn 0 0 0 Z Cu 0 B 0 Test Results [units - WN in g/cm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.66 1.10 10.4 88 1.2 6.3 784 17 70 17 S-I 41 Mn-1 51 Soil Class: Mineral Mn-All Mn-Al2 Zn-I Zn-AI 43 2246 2246 Cu-I 793 Na 0.1 ESP 1 SS-1 NO3-N NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomil Report No. FY22-SL009409 Page 3of11 Sample ID: 6 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P205 1 -Bermuda hay/past., E 0.9 60-80 0 2 - 0.0 K20 100 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meq/100 ma; NO3-N in mg/dm31: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.71 1.04 9.4 75 2.3 5.6 795 21 60 15 S-I 48 Mn-I 59 Soil Class: Mineral Mn-All Mn-Al2 Zn-I Zn-AI 52 1463 1463 Cu-I 943 Na 0.1 ESP 1 SS -I NO3-N Sample ID: 7 Lime History: Recommendations: Lime Nutrients (Ib/acre) More Information Note: 12 Note: $ Crop (tons/acre) N P205 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 K20 60 Mg S Mn Zn 0 0 pH$ Z Cu 0 B 0 Test Results [units - WN in g1cm3; CEC and Na in meq/100 cm3; NO341 in mg/dm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.18 1.20 11.8 95 0.6 6.9 779 37 72 22 S-I 28 Mn-I 64 Soil Class: Mineral Mn-All Mn-Al2 Zn-I Zn-Al 42 2368 2368 Cu-I 778 Na 0.1 ESP 1 SS -I NO3-N Sample ID: 8 Lime History: Recommendations: Lime Nutrients (Ib/acre) More Information Note: 12 Note: $ Crop (tons/acre) N Pz0s 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 K20 90 Mg S Mn Zn 0 20 pH$ Z Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.22 1.17 9.8 91 0.9 6.7 772 25 69 20 S-I 18 Mn-I 50 Soil Class: Mineral Mn-AI1 Mn-Al2 Zn-I Zn-AI 37 2092 2092 Cu-I 798 Na 0.1 ESP 1 SS -I NO3-N NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomcl Report No. FY22-SL009409 Page 4 of 11 Sample ID: 9 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P205 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 K20 100 Mg S 0 0 Mn Zn 0 0 Cu 0 B 0 Test Results [units - WN in g/cm3; CEC and Na in meg1100 cm3; NO3-N in mgldm31: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 1.25 1.16 7.5 89 0.8 6.5 145 20 66 21 S-I 28 Mn-I 43 Soil Class: Mn-All Mn-Al2 35 Mineral Zn-I Zn-AI 293 293 Cu-I 101 Na 0.1 ESP 1 SS -I NO3-N Sample ID: 10 Lime History: Recommendations: Lime Nutrients (lb/acre) More information Note: 12 Crop (tonslacre) N P205 1 -Bermuda hay/past., E 0.6 60-80 0 2 - 0.0 K20 110 Mg S 0 0 Mn Zn 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 1.08 1.19 5.5 71 1.6 5.6 295 14 55 15 S-I 31 Mn-1 34 Soil Class: Mn-All Mn-Al2 37 Mineral Zn-I Zn-AI 432 432 Cu-I 177 Na 0.1 ESP 2 SS-1 NO3-N Sample ID: 11 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tonslacre) N P205 1 -Bermuda hay/past., E 0.5 60-80 0 2 - 0.0 K20 110 Mg S 0 0 Mn Zn 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.97 1.15 6.2 74 1.6 5.7 420 17 57 16 S-I 35 Mn-I 37 Soil Class: Mn-AI1 Mn-Al2 39 Mineral Zn-1 Zn-AI 590 590 Cu-1 309 Na 0.1 ESP 2 SS -I NO3-N NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomil Report No. FY22-SL009409 Page 5 of 11 Sample ID: 12 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tonslacre) N P2O5 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 KzO 100 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meg/100 cm3; NO3-N in mgldm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.41 1.21 6.9 79 1.4 6.0 615 21 58 19 S-I 36 Mn-I 66 Soil Class: Mineral Mn-All Mn-Al2 Zn-I Zn-AI 57 1005 1005 Cu-I 369 Na 0.1 ESP 1 SS -I NO3-N Sample ID: 13 Lime History: Recommendations: Lime Nutrients (Iblacre) More Information Note: 12 Note: $ Crop (tonslacre) N P205 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 K2O 110 Mg S Mn Zn 0 0 pH$ 0 Cu 0 B 0 Test Results [units - WN in g1cm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.76 1.07 9.3 91 0.9 6.6 526 16 67 23 S-I 45 Mn-I 57 Soil Class: Mineral Mn-AI1 Mn-Al2 Zn-I Zn-AI 42 923 923 Cu-I 344 Na 0.1 ESP 1 SS -I NO3-N Sample ID: 14 Lime History: Recommendations: Lime Nutrients (Iblacre) More Information Note: 12 Crop (tonslacre) N P2Os 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 K20 100 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in g1cm3; CEC and Na in meg/100 cm3; NO3-N in mgldm3]: HM% WN CEC BS% Ac pH P-I K-1 Ca% Mg% 1.37 1.08 10.1 87 1.3 6.3 573 20 64 22 S-1 41 Mn-I 51 Soil Class: Mineral Mn-All Mn-Al2 Zn-1 Zn-Al 43 996 996 Cu-I 334 Na 0.1 ESP 1 SS -I NOa-N NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomil Report No. FY22-SL009409 Page 6of11 Sample ID: 15 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tonslacre) N P205 1 -Bermuda hay/past., E 1.1 60-80 0 2 - 0.0 K20 100 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meq/100 cm3; NO3-N in mgldm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.66 1.14 7.5 70 2.2 5.4 805 19 51 18 S-I 57 Mn-I 73 Soil Class: Mineral Mn-All Mn-AI2 Zn-I Zn-AI 61 731 731 Cu-i 530 Na 0.1 ESP 1 SS -I NO3-N Sample ID: 16 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Note: $ Crop (tons/acre) N P205 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 K20 110 Mg S Mn Zn 0 0 pH$ 0 Cu 0 B 0 Test Results [units -WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.46 1.17 8.2 91 0.8 6.7 476 15 67 23 S-I 30 Mn-I 62 Soil Class: Mineral Mn-AI1 Mn-Al2 Zn-i Zn-AI 44 979 979 Cu-I 356 Na 0.0 ESP SS -I NO3-N Sample ID: 17 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P205 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 K20 90 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mgldm31: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.27 1.18 9.1 86 1.3 6.3 759 24 64 21 5-I 39 Mn-I 56 Soil Class: Mineral Mn-All Mn-Al2 Zn-I Zn-AI 46 1648 1648 Cu-I 654 Na 0.1 ESP 1 SS -I NO3-N NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomi/ Report No. FY22-SL009409 Page 7of11 Sample ID: 18 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tonslacre) N P2Os 1 -Bermuda hay/past., E 0.8 60-80 0 2 - 0.0 K20 60 Mg S 0 0 Mn Zn 0 0 Cu 0 B 0 Test Results [units - WN in g1cm3; GEC and Na in meq/100 cm3; NO3-N in mgldm3]: HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% 0.46 1.18 7.0 72 2.0 5.6 670 37 55 15 S-I 46 Mn-I 78 Soil Class: Mn All Mn-Al2 64 Mineral Zn-I Zn-AI 521 521 Cu-I 497 Na 0.1 ESP 1 SS-1 NO3-N Sample ID: 19 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tonslacre) N P205 1 -Bermuda hay/past., E 0.5 60-80 0 2 - 0.0 K20 90 Mg S 0 0 Mn Zn 0 0 Cu 0 B 0 Test Results [units - WN in glcrrt3; CEC and Na in megl100 cm3; NO3-N in mg/dm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.41 1.16 8.3 78 1.8 5.8 719 26 59 17 S-I 39 Mn-1 85 Soil Class: Mn All Mn-Al2 68 Mineral Zn-I Zn-AI 1469 1469 Cu-I 588 Na 0.1 ESP 1 SS -I NO3-N Sample ID: 20 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tonslacre) N P205 1 -Bermuda hay/past., E 0.9 60-80 0 2 - 0.0 K20 60 Mg S 0 0 Mn Zn 0 0 Cu 0 B 0 Test Results [units -WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]: HM% WN CEC BS% Ac pH P-I K-1 Ca% Mg% 0.27 1.10 9.3 76 2.2 5.6 944 39 55 18 S-1 47 Mn-I 80 Soil Class: Mn-AI1 Mn-Al2 65 Mineral Zn-I Zn-AI 1586 1586 Cu-I 864 Na 0.1 ESP 1 SS -I NO3-N NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL009409 Page 8 of 11 Sample ID: 21 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1-Bermuda hay/past., E 0.4 60-80 0 2 - 0.0 K2O 70 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3): HM% WN CEC BS% Ac pH P-I K-1 Ca% Mg% 0.41 1.18 7.7 78 1.7 5.8 703 35 57 18 S-I 38 Mn-I 74 Soil Class: Mineral Mn-All Mn-Al2 Zn-I Zn-AI 61 1242 1242 Cu-I 546 Na 0.1 ESP 1 SS-1 NO3-N Sample ID: 22 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Note: $ Crop (tons/acre) N P2O5 1 -Bermuda hay/past., E 0.0 60-80 0 2- 0.0 K2O 90 Mg S Mn Zn 0 20 pH$ 0 Cu 0 B 0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3l: HM% WN CEC BS% Ac pH P-i K-I Ca% Mg% 0.46 1.18 9.2 95 0.5 7.0 524 23 73 21 S-I 12 Mn-I 48 Soil Class: Mineral Mn All Mn-Al2 Zn-I Zn-AI 31 1292 1292 Cu-I 413 Na 0.1 ESP 1 SS -I NO3-N Sample ID: 23 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 1(20 100 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm3l: HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% 1.80 1.06 11.6 87 1.5 6.2 659 19 71 15 S-I 31 Mn-I 48 Soil Class: Mineral Mn All Mn-Al2 Zn-I Zn-AI 43 1790 1790 Cu-I 630 Na 0.1 ESP 1 SS -I NO3-N NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi! Report No. FY22-SL009409 Page 9 of 11 Sample ID: 24 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1 -Bermuda hay/past., E 0.5 60-80 0 2 - 0.0 K2O 100 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mgldm31: HM% WN CEC BS% Ac pH P-I K-1 Ca% Mg% 1.87 1.12 9.8 80 2.0 5.8 629 19 66 13 S-1 31 Mn-I 71 Soil Class: Mineral Mn-All Mn-Al2 Zn-I Zn-AI 60 1371 1371 Cu-I 530 Na 0.1 ESP 1 SS -I NO3-N Sample ID: 25 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tonslacre) N P205 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 K20 80 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]: HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% 0.71 1.11 10.5 86 1.4 6.2 754 27 67 18 S-1 38 Mn-I 52 Soil Class: Mineral Mn-A11 Mn-Al2 Zn-1 Zn-AI 45 1690 1690 Cu-1 606 Na 0.1 ESP 1 SS -I NO3-N Sample ID: 26 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 K2O 90 Mg S Mn Zn 0 0 0 0 Cu 0 B 0 Test Results [units -WN in glcm3; CEC and Na in megl100 cm3; NO3-N in mgldm31: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 2.22 1.13 8.9 81 1.7 5.9 524 25 65 15 S-1 29 Mn-I 47 Soil Class: Mineral Mn-AI1 Mn-Al2 Zn-I Zn-AI 45 1202 1202 Cu-I 455 Na 0.1 ESP 1 SS -I NO3-N NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomi/ Report No. FY22-SL009409 Page 10 of 11 Sample ID: 27 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tonslacre) N P2O5 1 -Bermuda hay/past., E 0.7 60-80 0 2 - 0.0 K2O 70 Mg S 0 0 Mn Zn 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meg/100 cm3; NO3-N in mg/dm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.76 1.14 6.4 73 1.7 5.6 504 32 55 16 S-I 40 Mn-I 62 Soil Class: Mn-All Mn-Al2 54 Mineral Zn-I Zn-AI 881 881 Cu-1 336 Na 0.1 ESP 2 SS -I NO3-N Sample ID: 28 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1 -Bermuda hay/past., E 0.0 60-80 0 2 - 0.0 K2O 90 Mg S 0 0 Mn Zn 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meg1100 cm3; NO3-N in mg/dm3]: HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% 0.97 1.18 8.4 84 1.4 6.1 514 26 65 18 S-I 41 Mn-I 72 Soli Class: Mn-AI1 Mn-AI2 59 Mineral Zn-I Zn-AI 914 914 Cu-I 343 Na 0.1 ESP 1 SS -I NO3-N Sample ID: 29 Lime History: Recommendations: Lime Nutrients (lb/acre) More Information Note: 12 Crop (tons/acre) N P2O5 1 -Bermuda hay/past., E 0.8 60-80 0 2 - 0.0 K2O 120 Mg S 0 20 Mn Zn 0 0 Cu 0 B 0 Test Results [units - WN in glcm3; CEC and Na in meg/100 cm3; NO3-N in mgldm3]: HM% WN GEC BS% Ac pH P-I K-I Ca% Mg% 1.25 1.15 4.7 62 1.8 5.5 116 11 40 21 S-I 13 Mn-1 15 Soil Class: Mn-All Mn-AI2 26 Mineral Zn-I Zn-AI 188 188 Cu-I 60 Na 0.0 ESP SS-1 NO3-N NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY22-SL009409 Page 11 of 11 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index M-0 mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-I sulfur index SS -I soluble salt index WN weight per volume Zn-Al zinc availability index Zn-I zinc index Recommendations for field crops or other Large areas are listed separately for each nutrient to be added (in units of Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-I values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit www.ncaqr.cloviacironorni/obpart4.htmtgsfind information that may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. Test Results The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-A11, Mn-Al2, Zn-1, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely indicate levels fertility Visit www.ncagr.gov/agronomi/uyrst.htm available)] of plant nutrients or other measurement. Pow'siN Dy Grower: CMSD Farm: WILEY GASKINS RD Ayden Nitrogen 4728 Old NC 11 Ayden, NC 28513 252-746-2152 Farm Sample ID pnxete4 By SavedRX: ALL Soil Fertility Grower: CMSD Farm: WILEY GASKINS RD Field(s): Multiple Fields Tenn Lime - Fertilizer Application (Ibs/ac) Equation Variables Target pH: 6 Lab: Custom Eq: Commodity: Sample Date: Max Rate: Min Rate: Switch Rate: NCDA NCDA Recs Corn 2021-10-01 N/A 400.0 Ibslac 400.0 Ibslac Multiplier: Subtract: Min Application Rate: Max Application Rate: Avg Application Rate: Application Area: Average Field Rate: N/A N/A 400.0Ibslac 2300.0 Ibslac 1191.14 lbs/ac 41.03 ac 642.81 Ibslac Total Area: Total Product: Total Product Bulk: Product Cost / Bulk: Total Product Price: Application Cost/Area: Total Application Cost: Total Cost: 76.03 ac 48872.69 Ibs 24.44 ton $52.0/ton $1270.69 $0.0/ac $0.0 $1270.69 Ayden Nitrogen 4728 Old NC 11 Ayden, NC 28513 9J,7_74A..71 c.7 10/29/21 01:46 PM 1/2 Statement Page: 1 Ayden Nitrogen 4728 Old NC 11 / P.O. Box 7 Ayden, NC 28513 Phone 252-746-2152 Contentnea Metro Sewage Dist Po Box 477 Griifton, NC 28530 Date Number Description 1 Detail Statement Date: 11/30/2021 ID: 010202 Total Balance: $1,701.85 Amount Remitted: Terms: Unless otherwise agreed in writing by Harvey Fertilizer & Gas Co, interest will accrue at a periodic rate of 1.5% per month. To avoid additional finance charges, payments must be in office by last day of month. Quantity Price / Unit Extension I ---Your Share----1 Prepaid Regular Balance Forward 11/08/2021 1021928 Charge Invoice - Due 12/08/2021 Dolomitic Lime - Bulk App Fees - Lime 11/09/2021 1021933 Charge Invoice -Due 12/09/2021 GPS Soil Sampling 20.360 Tons 20.360 Each 75.690 Acre 0.00 0.00 51.000 /Tons 1,038,36 1,038,36 14.000 /Each 285.04 285.04 Invoice Total 1,323.40 0.00 1,323.40 5.000 /Acre 378,45 378.45 Invoice Total 378.45 0.00 378.45 Ending Total Balances 0.00 1,701.86 Current 1 - 30 31 - 60 61 - 90 Over 90 Unapplied Budget Billing Prepay Overall 1,701.85 0.00 0.00 0.00 0.00 0.00 0.00 0.00 1,701.85 Ayden Nitrogen Date: 11/30/2021 Contentnea Metro Sewage Dist