WQ0032855_Residual Annual Report Form 2021_20220215

Non -Discharge Branch Upload/Submittal Form
NORTH CAROLINA
EnWrvnmemfal Qualify
Version 2 - Revised June 23, 2020
Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?*
Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0032855
Applicant/Permittee Town of Rutherfordton
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office
CO Reviewer
Admin Reviewer
Asheville

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name*
Doug Barrick
Email Address* Phone Number*
[e-mail] 8282873520
Project Information
Application/Document Type *
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
Permit Number: * WQ0032855
Has Current Existing permit number
Applicant/Permittee Address*
Facility Name*
129 North Main Street, Rutherfordton, NC 28139
Town of Rutherfordton Class B Residuals Program
Please provide comments/notes on your current submittal below.
High -Rate Infiltration
Reclaimed Water
Residuals
Other
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
doc02037220220215094300.pdf 12.51 MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
po
Submission Date 2/15/2022

Town of Rutherfordton
2021 Annual Report
Land Application Pr1 +
Permit No. WQ0032855

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0032855 County: Rutherford Year: 2021
Facility Name (as shown on permit):
Land Application Operator:
US Biosolids, Inc.
Town of Rutherfordton
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
21 Yes CI No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
1 16
Total number of fields utilized for land application during the year:1
6
Total amount of dry tons applied during the year for all application sites:1
45.08
Total number of acres utilizes for land application during the year:
26.2
Part B - Annual Compianee Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. D Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
I ) Only residuals approved for this pen -nit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC: 021' .1 105(a) or the Pollutant
Loading Rates in 15A NCAC 021' .1 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 1 1 1 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 l) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoffof residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
�r
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Permit ee Name and Title (type or print)
r
Signature o Permittee ate
H
Signature of Pryparer* Date Signature of L>�id Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .l 102 (26) DENR FORM ACF (12/2006)

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ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Rutherfordton Total Dry Tons Applied (Annual):
WQ0032855 Cation Exchange Capacity (non 503 only):
Stuart Beam Owner: Stuart Beam Predominant Soil Series:
1.6 Acres Permitted: 1.6 Site #: HE Field #:
2.41
PbC2
5
Residual Analvsis Data (Heavy Metals and Total Phosnhorus use mfy/ke. % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1J
9/28/21
2
3
4
5
6
7
8
Al
10
11
112
% Solids
2.97
Arsenic
16.7
Cadmium
3.33
Copper
211
Chromium
19.5
Lead
13.7
Mercury
0.5
Molyb-
denum
8.33
Nickel
10.3
Selenium
16.7
"Zinc
433
Total
Phos-
horus
25700
Annual Heavv Metal Field Loadines (Calculated in Ibs/acre):
Total
t j
2
3
4j
5,
!�
7
8
9 i
1.0
11
12
DT/Ac./
_
o
App.
Event
1,51
14
Arsenic
0,050
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,050
Cadmium
0.010
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0,000
0.000
0.010
Copper
0.637
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.637
Chromium
0.059
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0,059
Lead
0.041
0,000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
1 0.041
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.002
Molyb-
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
denum
Nickel
0.031
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.031
Selenium
0.050
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.050
Zinc
1.307
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.307
Total
Phos-
77.563
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0,000
0,000
0.000
77.563
horus
..1. certily, unuer penally of maw, tnat tnls aocument was prepareu unaer my airectlon or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Rutherfordton Total Dry Tons Applied (Annual): 6.44
Permit #: WQ0032855 Cation Exchange Capacity (non 503 only):
Operator: Stuart Bear Owner: Stuart Beam Predominant Soil Series: PbC2
Acres Used: 5.1 Acres Permitted: 5.1 Site #: HF Field #: 6
Residual Analvsis Data (Heavv Metals and Total Phosnhorus use me/ke. % Solids use Raw Percent #):
posite
Date
Annual Heavv Metal Field Loadines (Calculated in Ibs/acre):
Total
Annual Heavv Metal Field Loadines (Calculated in Ibs/acre):
Total
1 !
2
3
a ,
5 ;
6�
7�
8
9;
10
11
121
DT/Ac./
App.
r
Event
1.26
Arsenic
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.042
Cadmium
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Copper
0.533
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.533
Chromium
0.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.049
Lead
0.035
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0,000
0.035
Mercury
0.001
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0,000
0.000
0.001
Molyb-
0.021
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
denum
Nickel
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.026
Selenium
0.042
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.042
Zinc
1.094
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.094
Total
11hos-
64.918
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
64.918
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit 4:
Operator:
Acres Used:
Town of Rutherfordton Total Dry Tons Applied (Annual):
WQ0032855 Cation Exchange Capacity (non 503 only):
Stuart Beam Owner: Stuart Beam Predominant Soil Series:
7.2 Acres Permitted: 7.2 Site #: HE Field #:
13.69
ApB
8
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Annual Heavy Metal Field Loadings Walculated in ibs/acre):
Total
Annual Heavy Metal Field Loadings Walculated in ibs/acre):
Total
1!
2
3
4_
5
6
7 f
8 j
9;
Loi
iiij
112
DT/Ac./
o
App.
Event
1.90
14
Arsenic
0.063
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.063
Cadmium
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Copper
0.802
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.802
Chromium
0.074
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.074
Lead
0.052
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.052
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0:002
Molyb-
0.032
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.032
denum
Nickel
0.039
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0.000
0.039
Selenium
0,063
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Zinc
1.646
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.646
Tota I
phos-
97.711
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
97.711
horus
"t certtty, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
17"`' / ..
Signature of Land App rier
a• lu•9ea I
Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Rutherfordton Total Dry Tons Applied (Annual): 5.63
WQ0032855
Stuart Beam Owner:
3.4 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Stuart Beam Predominant Soil Series:
3.4 Site #: HE Field #:
ApB
10
Residual Analvsis data (Heavv Metals and Total Phoslahorus use mE/ktr, % Solids use Raw Percent #):
Corn-
Posite
Date
Total
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
1 3
4
5;
6
7
8
9€
10
11
12
__
DT/Ac./
APP.
Event
1.66
Arsenic
0.055
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.055
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
0.699
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,699
Chromium
0.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
..ead
0.045
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.045
Mercury
0,002
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.028
denum
Nickel
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,034
Selenium
0.055
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,055
Zinc
1.435 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.435
'rotal
Phos-
85.170
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
85.170
horus
111 certify, under penalty of -law, that this document was prepared under my direction or supervision to accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
r _-
.A.t !7
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Rutherfordton Total Dry Tons Applied (Annual):
WQ0032855
Stuart Beam Owner:
4.9 Acres Permitted:
Cation Exchange Capacity (non 503 only):
Stuart Beam Predominant Soil Series:
4.9 Site #: HE Field #:
10.47
PsC2
11
RPcirinal Analvcic natn me.nvv Metals and Total Phosnhnrus use mg/kg. % Solids use Raw Percent #):
Sample or
Com-
posite
Bate
1
9/28/21
21
3
4 1
L 5
-6 ,
7
8
9
10
11 i
1121
% Solids
2.97
Arsenic
16.7
Cadmium
3.33
Copper
211
Chromium
19.5
Lead
13.7
Mercury
0.5
Molyb-
denum
8.33
Nickel
10.3
Selenium
16.7
Zinc
433
Total
Phos-
horus
25700
Annual Heavy Metal Field LoadinLys (Calculated in Ibs/acre):
Total
1 j!
L21
1314
6
61
7 j
8 j
9!
10J
11J
1�
-
-
-
_-
c
DT1Ac,/
App.
y
Event
2.14
Arsenic
0,071
0.000
0.000
0,000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0,071
Cadmium
0.014
0.000
0.000
0.000
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0.000
0,014
Copper
0.901
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0,000
0.000
0.000
0.901
Chromium
0.083
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.083
Lead
0.059
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
0.036
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
denum
Nickel
0.044
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.044
Selenium
0,071
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.071
Zinc
1.850
0.000
0.000
0.000
0.000
0.000
0.000 1
0.000
0.000
0,000
0.000
0.000
1.850
Total
Phos-
109.790
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
109.790
horus
"l certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
(7-Av 14Y."'
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
"Town of Rutherfordton Total Dry Tons Applied (Annual): 6.44
WQ0032855 Cation Exchange Capacity (non 503 only):
Stuart Beam Owner: Stuart Beam Predominant Soil Series: ApB
4 Acres Permitted: 4 Site #: HE Field #: 14
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %, Solids use Raw Percent #):
Corn-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
I 1
2
1 31
14151
16171
1 81
1 9j
jqj
1,11 f
12
DT/Ac./
o
App
Event
1.61
Arsenic
0.054
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.054
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
0.679
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.679
Chromium
0,063
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
1 0.063
Lead
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.044
Mercury
0.002
0,000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
denum
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0,000
0.000
0.027
Nickel
0.033
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.033
Selenium
0.054
0.000
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.054
Zinc
1.394
0.000
0.000
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1,394
Total
Phos-
82.754
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
82.754
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
-C _4 �
Signature of Land Applier
)'( i" k
Date
DENR FORM MFLSF (12/2006)

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Rutherfiorton
WWTP Name: Town of Rutherforton
Monitoring Period: From
WQ Permit Number:
NPDES Number:
1 / 1 /2021 To 12/31 /2021
WQ0032855
NCO25909
Pathogen Reduction (15A NCAC 02T A 106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
1 Alt B (Alk Treatment)❑
1 Alt. C (Prior' Testing)❑
Alt-D (No Prior Test) ❑
1 Process to Farther Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
lAlt, (1) Fecal Density A,
T Alt. (2) Process to Sianifteantly Reduce Pathogen ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Cum msting ❑
Aerobic Digestion ❑
Anaerobic Digestior: ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
umer o
dences cee-
Frequency
of Analysis
Sample
Type
Analytical
Tech-
nioue
Minima
Geo. Mean
Maxima
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
54852
119094
331950
Ml'N/g
0
7
grab
sm9221C
C.FU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) 0
Alt, 4 (Spec. O, uptake) JZI
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying- Stable) ❑ jAlt.
8 (Drying - Unstable)
Alt, 9 (injection) ❑
Alt. 10 (incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
G7 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T A 107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dennis Key US Biosolids, Inc.
Preparer Na and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
�� �� :.� .��� �>�- t�..z;z._ ,,�..• • yam
Signature of Preparer* Date Signature of LYpplicr (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 21'.1 102 (26)
DENR FORM PVRF 02T (12/2006)

(2)
Waypoint.
7521 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46381
US Biosolids Inc Project Rutherfordton
Dennis Key Report Date : 10/13/2021
958 Hoots Road Information : Received : 10/04/2021
Roaring River , NC 28669
�wurc �r (rroT
Pauric Mc Groary Ph.D., CPA
Report Number : 21-277-0008 REPORT OFANALYSIS Agronomist
Lab No : 50024 Matrix: Solids
Sample ID : Rutherfordton Sampled: 9/28/2021 12:45
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
97.0 H
%
0.010
1
10/07/21 17:02
FMM
SM-2540G
Sulfur
4330
mg/Kg - dry
333
1
10/12/21 00:58
JTR
6010D
Calcium
6970
mg/Kg - dry
1670
1
10/08/21 21:58
TJS
6010D
Aluminum
38700
mg/Kg - dry
167
1
10/08/21 21:5B
TJS
6010D
Manganese
427
mg/Kg - dry
16.7
1
10/08/21 21:S8
TJS
6010D
Organic N
45670
mg/Kg - dry
8333
1
10/11/21 10:30
CALCULATION
Nickel
10.3
mg/Kg - dry
8.33
1
10/08/21 21:58
TJS
6010D
Lead
13.7
mg/Kg - dry
10.0
1
1.0/12/21 21:35
JTR
6010D
Arsenic
<16.7
mg/Kg - dry
16.7
1
10/08/21 21:58
TJS
6010D
Selenium
<16.7
mg/Kg - dry
16.7
1
10/08/21 21:58
TJS
6010D
Test
Results
Units
MQL
OF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
2.97 H
%
0.010
1 10/07/21 17:02
FMM SM-254OG
Phosphorus
25700
mg/Kg - dry
167
1 10/08/21 21:58
TJS 6010D
Copper
211
mg/Kg - dry
16.7
1 10/08/21 21:58
TJS 6010D
Total Kjeldahl Nitrogen
45700
mg/Kg - dry
8330
1 10/11/21 10:30
JPJ ;M-4500-NH3C-TKP
Qualifiers/ B
Analyte detected in blank
OF
Dilution Factor
Definitions H
Beyond holding time
MQL
Method Quantitation
Limit

Waynto
PA
46381
US Biosolids Inc Project
Dennis Key
958 Hoots Road Information
Roaring River , NC 28669
Report Number : 21-277-0008
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 ° Fax [phone]
www,waypointanalytical.com
Rutherfordton
REPORT Of ANAL PSIS
Report Date : 10/13/2021
Received: 10/04/2021
�Awjc r+��77t I7/OOIiS�
Pauric Mc Groary Ph.D., CPA
Agronomist
Lab No : 50024
Sample ID : Rutherfordton
Matrix: Solids
Sampled: 9/28/2021 12:45
Potassium
3970
mg/Kg - dry
333
1
10/08/21 21:58
TJS
6010D
Magnesium
2650
mg/Kg - dry
167
1
10/08/21 21:58
TJS
6010D
Sodium
1820
mg/Kg - dry
833
1
10/08/21 21:58
TJS
6010D
Iron
16400
mg/Kg - dry
333
1
10/08/21 21:58
TJS
6010D
Zinc
433
mg/Kg - dry
41.7
1
10/08/21 21:58
TJS
6010D
Ammonia Nitrogen
<3330
mg/Kg - dry
3330
1
10/11/21 13:30
JPJ
SM-4500-NH3C
Nitrate+ N itrite- N
<164
mg/Kg - dry
164
1
10/11/21 14:25
ZBD
450ONO3F-2011
Cadmium
<3.33
mg/Kg - dry
3.33
1
10/08/21 21:58
TJS
6010D
Chromium
19.5
mg/Kg - dry
8.33
1
10/08/21 21:58
TJS
6010D
Mercury
<0.500
mg/Kg - dry
0.500
1
10/08/21 13:03
JW2
SW-7471B
pH
6.5
S.U.
1
10/11/21 14:50
DRS
9045D
Molybdenum
<8.33
mg/Kg - dry
8.33
1
10/08/21 21:58
TJS
6010D
Qualifiers/ B Anaiyte detected in blank DF Dilution Factor
Definitions H Beyond holding time MQL Method Quantitation Limit

_0
C:
c
i
C)
o
0
U)
C)
•
X
04
U)
O
:2
0
II
II
II
11
T
C14
0
z
Cf)
0
z
CY)
r
z
►n
N
04
CO
q
x
0)
04
0
z
0
z
r
r
z
Clq
X
CD
E
a
CD
0
40
COO
z
z
m
<
< i
C4
r
00
V7
CU (i
M iN

SAR
Sodium Absorption Ratio
Na: Sodium UNQ8j Equivalent weight23
Co: Cakcium(N1o/L) Equivalent weight: 2O
Mg : Magnesium (MgIQ Equivalent weight: 12
Milli Equivalent =Mo/L/Equivalent weight
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
(From yNg/Lentered above)
I SAR=_O (From ME entered below)
The amour
amount of(
Permitting !

'rESV I LLE
ALYTICAL
UU,S,B^osoK~rKsInc
A58Hoots Road
Roaring River, NC28GSQ
Receive Date: 09C28/2021
Reported: 09/29/2021
For: Rutherfnnd0on
Comments: GEOMETRIC MEAN: 119004MPN/g
Sample Number
Parameter
Sample ID
Result
Unit
K4adnod
Analyzed
Analyst
210928'88-01
Fena|Co|ihnnna
1
87460
MPN/g
ow9221cse006
09/28U021
MD
218828-38'01
Percent Solids
1
2.36
%
ow2540o-201/
03/28/2021
IVID
210928'38-02
Feoo|Co|i(omns
2
210084
MPN/y
51-0922/Cs2006
09128/2021
MO
210928'38'02
Percent Solids
2
2.38
96
sm254oa-20/'
09/2812021
MD
210928-38-03
Feou|Co|ifonns
3
331950
MPN/g
m»s21cs-2006
89/28/2021
MD
210928'38'03
Percent Solids
3
2.41
96
a*25406e0/'
09/28/2821
IVID
210928'38'04
Feoa|Co|iforms
4
124481
MPW/g
nm92zICE .cuno
09/28/2021
IVID
210928-38'04
Percent Solids
4
2-41
%
sm25-I«oa011
09/28/2021
MD
210828-38'05
Fece|Cn||[orms
5
125523
MPN/g
5m922/cs'2006
09/28/2021
MD
210828'38-05
Percent Solids
5
239
%
om2540o'201'
09/28/2021
MD
210928'38-06
Feoa|CoUfurmm
O
58333
MPN/g
sm9221cs�2006
08/28/2021
MD
210928'38'08
Percent Solids
0
2.40
%
»mzw^a-'«`'
09/28C2021
MD
210928'38'07
Feco|Co|ihonns
7
54852
MPN/Q
su9221ose006
09128/2021
MD
210928'38'07
Percent Solids
7
237
Y6
^wzmooe»//
08/28/2021
MD
Respectfully submitted,
Melissa Myers
NCCert#44O.
NODVVCert#37755.
EPA#NCO0SOS
POBox 228°Statesville, N[ZO687°7U4/872/4697
Page/of 4

rATESVILLF
N A LY T I C A L
Analytical Results
US Biosolids For: Rutherfordton
958 Hoots Rd
Roaring River, NC 28669
Entered: 9/28/21
Reported: 11/8/21
Sample ID: 210928-37-01
PARAMETER• Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids
Volatile Solids
% Volatile Solids
Week
1
1.65
0.95
0.5792
Week
2
1.38
0.77
0.5580
Week
3
1.39
0.80
0.5756
Week
4
1.34
0.75
0.5597
Week
5
1.33
0.75
0.5639
Week
6
1.29
0.69
0,5349
Volatile Solids Reduction: 0.5792 - 0.5349 X 100 = 16.4%
0.5792 - (0,5792 X 0.5349)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 32 of 33

O
30 Day Bench Worksheet
Sample ID 4 210928-37-01
wvcu I
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.98
1.14
0.5758
2
1.42
0.82
0.5775
3
1.54
0.9
0.5844
Average:
1.65
0.95
0.5792
uMIU L, 11
Samples
I Total Solids
Volatile Solids
% Volatile Fraction
1
1.38
0.77
0.5580
2
1.38
0.77
0.5580
3
1.39
0.78
0.5612
Avera e:
1.38
0.77
0.5580
wTirw14
Samples
I Total Solids
Volatile Solids
% Volatile Fraction
1
1.40
0.80
0.5714
2
1.39
0.81
0.5827
3
1.39
0.80
0.5755
Average:
1.39
0.80
0.5756
1vccu A
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.36
0.76
0.5588
2
1.33
0.74
0.5564
3
1.34
0.75
0.5597
Average:
1.34
0.75
0.5597
MI-Iwnlrcy
Sam les
Total Solids
Volatile Solids
% Volatile Fraction
1
1.32
0.74
0.5606
2
1.33
0.75
0.5639
3
1.33
0.75
0.5639
Avera e:
1.33
0.75
0.5639
wvvw A
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
1.29
0.70
0.5426
2
1.29
0.69
0.5349
3
1.30
0.69
0.5308
Average:
_
1.29
0.69
0.5349
Van Kleeck Reduction: 0.5792 - 0.5349 X 100 = %
0.5792 - ( 0.5792 X 0.5349)
Final Result: 16.4%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 33 of 33

aceAnalytical
vrvw.pacdabs.cvia
ANALYTICAL RESULTS
Project: US Bio Rutherfordton
Pace Project No.: 92564416
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 210928.31.01 Lab ID: 92564416001 Collected: 09128/21 I2:05 Received: 09/30/21 11:20 Matrix: Solid
Results reported on a 'wet -weight" basis
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D TCLP
Analytical Method: EPA 8260D Preparation Method: 8260D
Leachate Method/Date: 1311; 10112/21 15:52
Pace National - Mt. Juliet
1,2-Dichloroethane
NO mg/L 0.0500 1
10114/21 11:30 10114121 11:30 107-06-2
1,4-Dichlorobenzene
NO mg/L 0.0500 1
10114/21 11:30 10/14121 11:30 10646-7
I,I-Dichloroethene
No mgfL 0.0500 1
101140 11:30 10114121 11:30 75-35-4
2-Butanone (MEK)
No mg1L 0.500 1
10/14121 11:30 10114/21 11:30 78-93-3
Tetrachlorcethene
No mg/L 0,0500 1
10114121 11:30 10114/21 11:30 127-18-4
Trichloroethene
No mg/L 0.0500 1
10114121 11:30 10114/21 11:30 79-01-6
Vinyl chloride
No mg1L 0.0500 1
10114121 11:30 10/14121 11:30 75-014
Surrogates
Toluene-c18 (S)
104 % 80.0-120 1
10/14121 11:30 10/14f21 11:30 2037-26-5
4-Bromofluorobenzene (S)
90.6 % 77.0-126 1
1011421 11:30 10114121 11:30 460-004
1,2-Dichloroelhane-d4 (S)
125 % 70.0-130 1
10/14121 11:30 10/14121 11:30 17060-07-0
1010 Flash point,Closed Cup
Analytical Method: EPA 10108
Pace Analytical Services -Asheville
Flashpoint
>200 deg F 1
10/14121 14:52
Total Solids 2540 G-2011
Analytical Method: SM 254OG Preparation Method; 2540 G
Pace National - Mt. Juliet
Total Solids
2.21 % 1
10112,121 14:06 10/12121 14:35
9045 PH Soil
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.6 Std, Units 0.10 1
10115f21 12:30
9095 Paint Filter Liquid Test
Analytical Method: EPA 9095E
Pace Analytical Services -Asheville
Free Liquids
FAIL 11.0 1
10113121 15:25
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7,13.2
Pace Analytical Services - Greensburg
Cyanide. Reactive
NO mg/kg 0,99 1
10/08121 15:52 10112121 13:29
734S Reactive Sulfide
Analytical Method: SM 4500-S2-F-2011 Preparation Method: SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive
No mg/kg 9.9 1
10108121 15.48 10106/21 16:05
REPORT OF LABORATORY ANALYSIS
This report shall riot be reproduced, except in full,
Date: 10/271202109:40 AM Mthoul the written consent of Pace Analytical Services, LLC.
H3
H3
H3
Page 7o(27
PO Box 228 - Statesville, NC 28687 * 704/872/4697
Page 11 of 33

cle AnalXical
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: US Bio Rutherfordton
Pace Project No.: 92564416
Sample: 210928.31.01
Lab ID: 92564416001
Collected: 0912EV21 12:05
Received: 09130121 11:20 Matrix: Solid
Results reported an a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units
Report Limit OF
Prepared Analyzed CAS No.
Qual
PCSs(GC) 8082 A
Analytical Method: EPA 8082A Preparation Method: 3546/3665A
Pace National - Mt. Juliet
PCB-1016 (Aroclor 1016)
No mg/kg
22.2 14A
10119121 07:23 10119/2120:32 12674-11-2
PCB-1221 (Aroclor 1221)
ND mg/kg
22.2 14.4
10/19/21 07:23 10W19121 20:32 11104-28-2
PCB-1232 (Aroclor 1232)
No mg/kg
222 14.4
10/19/21 07:23 10/19/21 20:32 11141-16-5
PCB-1242 (Aroclor 1242)
No mg/kg
222 14A
10119121 07:23 10/19/21 20:32 53469-21.9
PCB-1248 (Aroclor 1248)
No mg/kg
11.1 14.4
10/19/21 07:23 10119/21 20:32 12672-29-6
PCB-1254 (Aroclor 1254)
No nigAg
111 14.4
10/19/21 07:23 10/19/21 20:32 11097-69-1
PCB-1260 (Aroclor 1260)
NO mg/kg
111 14.4
1011912107:23 10/19/21 20:32 11096-82-5
Surrogates
Oecachloroblphenyl (S)
91.6 %
10.0-135 14A
10/19121 07:23 10/19/21 20:32 2051-24-3
Tetrachloro-m-xylene (S)
88,9 %
10.0-139 14.4
10/19/21 07:23 1011912120:32 877-09.8
Pesticides (GC) 8081 B TC LP
Analytical Method: EPA 8081 B Preparation Method: 351
OC
Leachate Method]Date: 1311;
10/12121 11:42 Initial pH:
6.58; Final pH: 4.89
Pace National - Mt. Juliet
Chlordane (Technical)
ND mg/L
0,00500 1
10122121 11:22 10122121 15:54 57-74-9
Endrin
ND mg/L
0.00500 1
10122/21 11:22 10122121 15:54 72-20-8
Heptachlor
No mg/L
0.00500 1
10/22/21 11:22 10122/21 15:54 76-44-8
gamma-SHC (I-Indane)
ND mgiL
0,00500 1
10/22/21 11:22 10122/21 15:54 58-89-9
Melhoxychlor
ND mg/L
0.00500 1
10/22121 11:22 10122121 15:54 72-43-5
LO
Toxaphene
No mg/L
0.0100 1
10122/21 11:22 10/22121 1554 8001-35-2
Surrogates
Decachlorobiphenyl (S)
117 %
10.0-128 1
10/22/21 11:22 10122/21 15:54 2051.24-3
Tetrachloro-m-xylene (S)
86.5 %
10.0-127 1
10/22/21 11:22 10122121 15:54 877-09-8
PCBs(GC) 8082 A TCLP
Analytical Method: EPA 8082A Preparation Method; 351 OC
Leachate Method/Date: 1311; 10112121 11 A2 Initial pH:
6.58: Final pH: 4.89
Pace National - Mt- Juliet
PCB-1016 (Aroclor 1016)
NO mg/L
0.0100 1
10/22121 11:22 10122121 15:54 12674-11-2
MH,R1
PCB-1221 (Aroclor 1221)
ND mg/L
0.0100 1
10/22/21 11:22 10/22121 15:54 11104-28-2
PCB-1232 (Amcor 1232)
NO mg/L
0.0100 1
10122/21 11:22 10122/21 15:54 11141-16-5
PCB-1242 (Aroclor 1242)
No mg/L
0,0100 1
10/22/21 11:22 10122121 15:54 53469-21-9
PCB-1248 (Aroclor 1248)
NO mg/L
0.0100 1
10122121 11:22 10122/21 15:54 12672-29-6
PCB-1254 (Aroclor 1254)
ND mgJL
0.0100 1
10122J21 11:22 10/22/21 15:54 11097-69-1
PCB-1260 (Aroclor 1260)
ND mg/L
0.0100 1
10/22/21 11:22 10122/21 15:54 11096-82-5
LO
Surrogates
Decachlorobiphenyl (S)
116 %
10.0-128 1
10122)21 11:22 10122/21 15:54 2051-24-3
Tetraciiioro-m-xylene (S)
958 %
10.0-127 1
10122/21 11:22 10122121 15:54 877-09-8
Chlorinated Herb. (GC) 8151 A
Analytical Method: EPA8151A Preparation Method: 8151A
Leachate Method/Date: 1311; 10/12/21 11:42 Initial pH:
6.58; Final pH: 4.89
Pace National - Mt, Juliet
2,4,5-TP (Silvex)
NO mg/L
0,00200 1
10/14/2109:39 10115121 09:20 93-72-1
2,4-D
No mg]L
0.00200 1
1OJ14/21 09:39 10/15121 09:20 94-75-7
Surrogates
2,4-OCAA (S)
49.0 %
14.0-158 1
10/14/21 09:39 10115/21 09:20 19719-28-9
REPORT OF
LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 10127/2021 09:40 AM
without the written consent
of Pace Analytical Services, I.I.C.
Page 5 of 27
PO Box 228 o Statesville, NC 28687 - 704/872/4697
Page 9 of 33

a ceAnalytical a WWwP4c#I&bsxdM
ANALYTICAL RESULTS
Pace Analytical Services, ULC
9600 Kincey Ave, Suite IGO
Hunte(sville, NC 28078
[phone]
Project: US Bio Rutherfordton
Pace Project No.: 92564416
Sample: 210928.31.01 Lab ID: 92564416001 Collected: 09128121 12:05 Received: 09/30/21 11:20 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6010D ATL ICR TCLP
Analytical Method: EPA 60100 Preparation Method: EPA 3010A
Leachate MethocIlDate: EPA 1311: 10/15121 13:08 Initial
pH;; Final pH: 6,59
Pace Analytical Services - Peachtree Comers, GA
Arsenic
ND mglL 0.30 1
10115121 13:20 10/15121 21:05 7440-38-2
Barium
NO mg/L 0.50 1
1011512113:20 10/15/2121:05 7440-39-3
Cadmium
NO mgiL 0.10 1
10115121 13:20 1011512121:05 7440-43-9
Chromium
ND mg/L 0.10 1
10115/21 13:20 10115/2121:05 744047-3
Lead
NO mg[L 0.25 1
10115121 13:20 t0115121 21:05 7439-92-1
Selenium
NO mg/L 0.40 1
10/15121 13:20 1011512121:05 7782-49-2
Silver
NO mg/L 0.10 1
1 Of I 5f2l 1120 1011512121:05 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 74 70A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 10115J21 13:08 Initial
pH:; Final pH: 6.59
Pace Analytical Services - Peachtree Corners, GA
Mercury
NO MgJL 0,0050 1
10118t2108:30 10/18[21 12:20 7439-97-6
SVGA (GC/MS) 8270E TCLP
Analytical Method: EPA8270E Preparation Method: 3510C
Leachate Method/Date: 1311; 10/12/21 11:42 Initial pH:
6,58: Final pH: 4.89
Pace National - Mt. Juliet
1,4-Dichlorobenzene
NO mgfL 0,100 1
10116121 05:07 1011612122:47 106-46-7
2,4-Dinitrotoluene
NO mgiL 0.100 1
10/16/2105:07 10/1612122:47 121-14-2
Hexachlorobenzene
NO nng1L 0100 1
10116/21 05:07 1011612122:47 1118-74-1
Hexachi4oro-1,3-butadiene
NO mg/L 0A00 1
10/1612105:07 1011612122:47 87.68-3
Hexachloroethane
NO mg/L 0.100 1
101160 05;07 10116/2122:47 67-72-1
Nitrobenzene
NO mg/L 0.100 1
10/16/21 05:07 1011612122:47 98-95-3
Pyridine
NO mg/L 0.100 1
10116/2105:07 10116/2122:47 110-86-1
W-Methylphenol(m6p Cresol)
NO mg/L 0.100 1
10116/2105:07 1006/21122:47 15831-10-4
2-Methylphenol(o.Cresol)
NO mg/L 0.100 1
1011612105:07 1011612122:47 95-48-7
Pentachlorciphenol
NO mg/L 0.100 1
10/16121 05:07 10116121 22A7 87-86-5
2,4,5-Trichlaroplienal
NO mgfL 0,100 1
1011612105:07 1011612122:47 95-95-4
2,4,6-Trichlorophenof
NO mg/L 0.100 1
10/16/21 05:07 10116121 22:47 88-06-2
Surrogates
2-Fluorophenol (S)
23.6 % 10.0-120 1
1011612105:07 1011612122:47 367-124
Phenol-d5(S)
14.1 % 10.0-120 1
10111612105:07 10116f21 22:47 4165-62-2
Nitrobenzene-d5 (S)
47.3 % 10.0-127 1
10/1612105:07 1011 W21 22:47 4165-60-0
2-Fluorobiphanyl (S)
61.0 % 10.0-130 1
1011612105:07 10116121 22:47 321-60-6
2,4,6-Tribromophenot (S)
50.0 % 10.0-155 1
10116/2105:07 1GI16121 22:47 118-79-6
Terphenyl-04 (S)
63.0 % 10-0-128 1
101160 05:07 10116/21 22A7 1718-51-0
VOA (GC/MS) 82600 TCLP
Analytical Method: EPA 8260D Preparation Method: 82600
Leachate Method/Date: 1311; 10/12121 15:52
Pace National - Mt. Juliet
Benzene
NO mg/L 0.0500 1
10114J21 11:30 10114121 1130 7143-2
Carbon tetrachloride
NO mglL 0.0500 1
t0/14121 11:30 I0/14121 11:30 56-23-5
Chlorobenzene
NO mg/L 0,0500 1
10114121 11:30 10f14121 11:30 108-90-7
Chloroform
No mg/L 0,250 1
10114121 11:30 10114121 11:30 67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 1012712021 09:40 AM
without the written consent of Pace Analytical Services, LLC
Page 6 of 27
PO Box 228 o Statesville, NC 28687 a 704/872/4697
Page 10 of 33

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/#L"4'd/' .
30 Day Bench Test- Aerobic
EPA625-R-92/0 Sr4 2540 G-2011
Date began:
knalyst: /X00
rime Started: 11,7 2
Initial Day DO: 5 , & (>2) Temp: &Z 0 C
Date: 412612Z Time: /(¢ Z6'
% Total Solids
Dish #: t/
)ry Wt. + Dish Wt.: t/2. &e R2
Dish Wt.: & 703
Sample Wt.: to
% Total Solids: /. Qa
Yo Volatile Solids
dry WU Dish Wt.: t(7,
Ash Wt.: t/2. 7.r.L?G
Sample Wt.: to
%Vol. Solids: I. /t/
%u Total Solids
Dish #: Ole
dry Wt. +Dish Wt.: (!t(. 3 , S-.
Dish Wt.: t/t/.1Z(.il
Sample Wt.: 10
% Total Solids: /_ t/Z
%u Volatile Solids
dry Wt.& Dish Wt.: Vyy J 66'z
Ash Wt.: t/<(. 2 x t/
Sample Wt.: /0
% Vol. Solids: 0, Z
Total Solids
Dish #: 5
)ry Wt. +Dish Wt.: 4S, /`f44S
Dish Wt.: t/5. 734R
Sample Wt.:
% Total Solids:
%u Volatile Solids
dry WU Dish Wt.:
Ash Wt.: t(6'. 8'0 M
Sample Wt.: / Q
% Vol. Solids: p_ Q0
Sample ID#: 2 (OQ2 f3- 3 t- d
Digester Dimensions: R. S
Volume of sample in diges : 3 '/0 D mis
Initial DO reading of sample: 5"_ (a (>2)
Day 6 DO -,I'.(/ (>2) Temp: ,2 0 C
Date: ! Time: %ha
% Total Solids
Dish#: ,3/0
Dry Wt. + Dish Wt.: qq- J 6-0/
Dish Wt.: //ty, Z// 7
Sample Wt.: /(/
%Total Solids: / ao
% Volatile Solids
Dry WU Dish Wt.: 0/. 3 50/
Ash Wt.: t/V..2 733
Sample Wt.: /p
% Vol. Solids: 0_ 77,
% Total Solids
Dish #: / /
Dry Wt. +Dish Wt.: 42, !i'73Q
Dish Wt.: 1/2, 72 57a
Sample Wt.: !O
% Total Solids: /, 36
% Volatile Solids
Dry Wt.& Dish Wt.: t/2 . B73 q
Ash Wt.: (/Z, p2o 7
Sample Wt.: /p
% Vol. Solids: 7 7
% Total Solids
Dish #:
Dry Wt. + Dish Wt.: t/2 . R.nR -1
Dish Wt.: q2_
Sample Wt.: (p
% Total Solids:
% Volatile Solids
Dry WU Dish Wt.: (12, Reg 6-1
Ash Wt.: Q2— Z30L
Sample Wt.:
% Vol. Solids: 0,78
[Type here]
RPA icPli 70010

v12 DO:-5-,,6 (>2) Temp: 2 0 C
ate: 1121il121 Time:
u Total Solids
Dish #: (/
ry Wt. +Dish Wt.: ((Z. gVc?3
Dish Wt.: ((Z. (! (0 Q(a
Sample Wt.: (0
%Total Solids: /_ t(n
o Volatile Solids
ry Wt.& Dish WU it . 60 q3
Ash Wt.: ((Z. 72 126'
Sample Wt.: / O
% Vol. Solids: 0. Q 0
u Total Solids
Dish #: 3
ry Wt. +Dish Wt.: (M. n(o (8
Dish Wt.: t[8 . !/ 2 2. (!
Sample Wt.: (O
% Total Solids: !- 3 9
n Volatile Solids
ry Wt.& Dish Wt.: ((Q, O(e IP
Ash Wt.: ((A. 96(to
Sample Wt.: /0
% Vol. Solids: Q 131
o Total Solids
Dish #:
ry Wt. +Dish Wt.: ((5. 0(0o(/
Dish Wt.: q4(, Q2 (y
Sample Wt.: ! O
% Total Solids: / 39
b Volatile Solids
ry Wt.& Dish Wt.:
Ash Wt.: QQ. QtiDQ
Sample Wt.: /p
% Vol. Solids: 0.60
Sample ID# eU(I VA A— 9 '7
Day IS DO: _!'. '` (>2) Temp:,2 O_C
Date: /T&I21 Time: /1)1942
% Total Solids
Dish #: q
Dry Wt. + Dish Wt.: 112, }31qy e
Dish Wt.: ((2. (Q (p 4 (!
Sample Wt.: !D
%Total Solids:
% Volatile Solids
Dry Wt.& Dish Wt.: (ll- L�tL�i p)
Ash Wt.: (!2, ZZ 4 3
Sample Wt.: /0
% Vol. Solids: O.742
% Total Solids
Dish #: 3
Dry Wt. + Dish Wt.: (!Q, O 6.3 g
Dish Wt.: 4!8'. 420y
Sample Wt.: 10
%Total Solids: /-33
% Volatile Solids
Dry Wt.& Dish Wt.: ((Q , (2
Ash Wt.: (!R. Q747
Sample Wt.: /0
% Vol. Solids: O_ Y((
% Total Solids
Dish #:
Dry Wt. + Dish Wt.: ((Z - f (2 Q 7
Dish Wt.: Q2 , 7.354
Sample Wt.: /0
% Total Solids: /, 3 (/
% Volatile Solids
Dry WU Dish Wt.: ((Z. Ole) I
Ash Wt.: ((2, 7Q 52
Sample Wt.: (0
% Vol. Solids:
[Type here]

T
Day 24 DO: S (1 (>2) Temp: ZO C
Date: /O/z i , z / Time: 0QQo
Yo Total Solids
Dish #: it,
dry Wt. + Dish Wt.: qq, G QI 7
Dish Wt.: t(tl. 51,0 ! 5
Sample Wt.: /p
%Total Solids: /.3 2
Yo Volatile Solids
dry Wt. & Dish Wt.: L!t/.
Ash Wt.: i/q. (01tw3
Sample Wt.: 10
% Vol. Solids: r(1_ 7L/
Mo Total Solids
Dish #: (4
dry Wt. + Dish Wt.: t/2 , 77Yg/
Dish Wt.: L(2 , (Q M2
Sample Wt.:
% Total Solids:
Yo Volatile Solids
dry Wt. & Dish Wt.: t/I, 7-7t/t(
Ash Wt.: Liz, (0 44Z
Sample Wt.: /q
%Vol. Solids: ¢2.'7y'
Yo Total Solids
Dish #:
dry Wt. + Dish Wt.: tlL, i�(r 42
Dish Wt.: L12. 1.3(e7
Sample Wt.: /O
% Total Solids: /. 3 3
Yo Volatile Solids
)ry Wt. & Dish Wt.: 1(2. (nQ2
Ash Wu L12 _ !ZQ q 7
Sample Wt.: /Q
%Vol. Solids: 10.75
Sample ID# ,1(0 Q,l J-r
Day 30 DO: $ 2 (>2) Temp:.2 O C
Date: 10 9 Time: /D3o
% Total Solids
Dish#:
Dry Wt. + Dish Wt:
Dish Wt: t/y, S&O'i
Sample Wt: /p
%Total Solids: /. 29
% Volatile Solids
Dry Wt. & Dish Wt:
Ash Wt: t(t/, (a 2Q3
Sample Wt: / p
% Vol Solids: d_ 10
% Total Solids
Dish#: /$
Dry Wt. + Dish Wt: L(y. at, /j
Dish Wt: t/y. Q396,
Sample Wt: to
%Total Solids: 1, 2q
% Volatile Solids
Dry Wt. & Dish Wt: L(S_ ,Q(a /3
Ash Wt: t[t/. 17473
Sample Wt: / D
% Vol Solids:
% Total Solids
Dish#: S
Dry Wt. + Dish Wt: t(S. ji 1at!
Dish Wt: q�6, 7VA3
Sample Wt: / p
% Total Solids: /, Jp
% Volatile Solids
Dry Wt. & Dish Wt: t(! 67pY
Ash Wt: t{,�r. /f 2
Sample Wt: /Q
% Vol Solids: 119 _ (L, q
[Type here]
Rvvicars In010