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WQ0011448_Residual Annual Report 2021_20220215
Non-Discharge Branch Upload/Submittal Form NORTH CAROLINA Enriry mmful Quoity Version 2-Revised June 23,2020 Initial Review Reviewer Thornburg,Nathaniel D Is this submittal an application?(Excluding additional information.)* Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2021 Permit Number(IR)* WQ0011448 Applicant/Permittee Town of Snow Hill Email Notifications Does this need review by the hydrogeologist?* 0 Yes ® No Regional Office Washington CO Reviewer Admin Reviewer Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence. ............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................ Name* Drew Matthews Email Address* Phone Number* dmatthews@soilplus.net 2528839301 Project Information Application/Document Type* New(Fee Required) Modification-Minor Modification-Major(Fee Required) Renewal Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1, Required) NDAR-2 Annual Report Residual Annual Report Additional Information Change of Ownership Other We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High-Rate Infiltration Other Wastewater Reclaimed Water Closed-Loop Recycle Residuals Single-Family Residence Wastewater Other Irrigation Permit Number:* WQ0011448 Has Current Existing permit number Applicant/Permittee Address* PO Box 247,Snow Hill,NC 28580 Facility Name* Town of Snow Hill Class B Residuals Program Please provide comments/notes on your current submittal below. At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form,Engineering Plans,Specifications,Calculations,Etc.) 2021 Snow Hill Annual Report.pdf 4.33MB Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre-review until the fee(if required)has been received by the Non- Discharge Branch.Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality(NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order(as specified by the application). Mail payment to: NCDEQ—Division of Water Resources Attn:Non-Discharge Branch 1617 Mail Service Center Raleigh,NC 27699-1617 Signature / OteitI llCY evtdd Submission Date 2/15/2022 TOWN OF SNOW HILL 2021 ANNUAL LAND APPLICATION OF RESIDUAL BIOSOLIDS REPORT CLASS B PROGRAM WQ0011448 Submitted by: Soil Plus P.O. Box 1396 Oxford, North Carolina 27565 February 15, 2022 SOIL PLUS SOIL PLUS February 15,2022 NCDEQ-DWR Information Processing Unit 1617 Mail Service Center Raleigh,North Carolina 27699-1617 Re: 2021 LAND APPLICATION ANNUAL REPORT Town of Snow Hill"Class B" Program NC Permit No.: WQ0011448 Soil Plus Project No. 200804.A10 Information Processing Unit: Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as specified in the above referenced permit for the Town of Snow Hill on behalf of Granville Farms, Inc. Soil Plus compiled this report using data gathered during the compliance year. This data includes (1) certification form, (2) residual sampling, (3) field loading calculations, (4) pathogen and vector attraction reduction documentation, (5) standard soil fertility nutrient analysis. The Town of Snow Hill conducted application events on permitted fields in Greene County during 2021. A total of 17.48 Dry Tons or 219,500 Gallons of permitted residual biosolids were land applied to permitted fields. If there is any further information required or questions regarding this report, please do not hesitate to contact me or the Town of Snow Hill (252-747-3414) for further assistance. Respectfully, , .-2.0 Drew Matthews, Soil Plus Todd Whaley,Town of Snow Hill Jason Smith, Granville Farms P.O.Box 1396 Oxford,NC 27565 (252)883-9301 dmatthews@soilplus.net www.soilplus.net ANNUAL LAND APPLICATION CERTIFICATION FORM Source Summary Field Loading Summary ANNUAL RESIDUAL SAMPLING SUMMARY Town of Snow Hill FORM 2021 Annual Land Analytical Data TCLP Application of Residual Biosolids Report FIELD LOADING WQ0011448 SUMMARY FORM Town of Snow Hill Farm Snow Hill, NC ANNUAL PATHOGEN & VECTOR ATTRACTION REDUCTION FORM Fecal Coliform Data 30-Day Bench Scale Test SOIL SAMPLES Town of Snow Hill Farm Town of Snow Hill 2021 Class B Annual Report WQ Permit# WQ0011448 Annual Certification Form Source Summary Field Loading Summary ANNUAL LAND APPLICATION CERTIFICATION FORM PermitNumber FacilityName Land Application Operator County Phone Number WQ0011448 Town of Snow Hill Granville Farms,Inc. Greene (252) 747-3414 Year: 2021 Land application of residuals as allowed by the permit occurred during the past calendar year?If No,skip Part A,and Part Yes No B and proceed to Part C. Also,If residuals were generated but not land applied,please attach an explanation on how the E residuals were handled. Part A-Residuals Application Summary: Total number of application fields in the permit: 1 Total number of fields utilised for land application during the year: 1 Total amount of dry tons applied during the year for all application sites: 17.48 Total number of acres utilized for land application during the year: 11.4 Part B-Annual Compliance Statement: Facility was compliant during calendar year with all conditions of the land application permit? Yes No Including but not limited to items 1-13 below)issued by the Division of Water Quality ❑� If no please,provide a written description why the facility was not compliant,the dates,and explain corrective action taken. 1.Only residuals approved for this permit were applied to the permitted sites 2.Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6 3.Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)copies of laboratory results are attached 4.Annual TCLP analysis (if required)was performed and three(3)copies of certified laboratory results are attached 5.All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)copies of certified laboratory results are attached 6.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T 7.All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503 regulated facilities) 8.All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503 regulated facilities) 9.All operations and maintenance requirements in the permit were complied with or,in the case of a deviation, prior authorization was received from the Division of Water Quality 10.No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11.Vegetative cover was maintained and proper crop management was performed on each site receiving residuals,as specified in the permit. 12.No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13.All buffer requirements as specified on the permit were maintained during each application of residuals. Part C-Certification: "I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." /� Todd Whaley,Town Manager )(4— T/2 L Signature of Permittee Date Pe�'nee Name and TitleName and Title pe or print): g /6 �� Oy 1/20/22 Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee) *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T.1102(26) Source Summary Report WWTP VolumeApplied Total Town of Snow Hill WWTP 219,500 17.48 Total 219,500 17.48 YEAR TO DATE FIELD LOADING SUMMARY CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2 Field Used Applied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name pAN Used Site# SH 3 11.4 219,500 17.48 24.78 18.74 Annual Ryegrass- 104 23.8% Common 50 37.5% Hay Bermudagrass Hay Total 219,500 17.48 Town of Snow Hill 2021 Class B Annual Report WQ Permit# WQ0011448 Residual Sampling Summary Form Field Loading Calculations 2021 Analytical 2021 TCLP ANNUAL RESIDUAL SAMPLING SUMMARY FORM WQ Permit No. WQ0011448 Facility Name Town of Snow Hill Source Permit No. NC0020842 Source Name Town of Snow Hill W WTP Laboratory 1 Meritech,Inc. .'Laboratory 2 Sample or CompositeDate 4/21/2021 Parameter(mg/Kg) Class A Class B Aluminum N/A N/A 150 Ammonia Nitrogen N/A N/A 524 Arsenic 41 75 2.62 Cadmium 39 85 0.523 Calcium N/A N/A 3,220 Copper 1,500 4,300 0.523 Lead 300 840 3.12 • Magnesium N/A N/A 355 Mercury 17 57 0.052 Molybdenum N/A 75 1.31 Nickel 420 420 2.62 Nitrate-Nitrite Nitrogen N/A N/A 524 Percent Solids N/A N/A 1.91 pH(no units) N/A N/A 6.20 Phosphorus N/A N/A 1,190 Potassium N/A N/A 190 PAN(Inj./Inc.) N/A N/A 14,451 PAN(Surface) N/A N/A 14,189 Selenium 100 100 2.62 Sodium N/A N/A 488 SAR N/A N/A 0.30 TKN N/A N/A 45,200 Zinc 2,800 7,500 153 "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." LQ //�/�� Signature of Preparer* Date *Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26) v AGMAN FIELD LOADING ESTIMATES Facility Town of Snow Hill WWTP Sampling Date 4/21/2021 Solids 1.91 Mineralization Rate 0.3 Gallons per DT 12,555.40 pH 6.2 Sodium Absorpotion 0.30 <5.0 Safe 5.0- 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION NUTRIENT APPLICATION TKN (mg/Kg) 45,200 lbs./1,000 gal 7.20 Potassium lbs./1,000 gal 0.03 Ammonia Nitrogen(mg/Kg) 524.00 lbs./1,000 gal 0.08 Phosphorus lbs./1,000 gal 0.19 Nitrate-Nitrite(mg/Kg) 524.00 lbs./1,000 gal 0.08 Calcium lbs./1,000 gal 0.51 PLANT AVAILABLE NITROGEN SURFACE APPLIED Magnesium lbs./1,000 gal 0.06 PAN (mg/Kg) 14,189 lbs./1,000 gal 2.26 Manganese lbs./1,000 gal PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./1,000 gal PAN (mg/Kg) 14,451 lbs./1,000 gal 2.30 Molybdenum lbs./1,000 gal 0.00 Volatization Rate=0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) HEAVY METAL CONCENTRATION HEAVY METAL LOADING 41 75 Arsenic(mg/Kg) 2.62 Arsenic lbs./1,000 gal 0.00 39 85 Cadmium(mg/Kg) 0.52 Cadmium lbs./1,000 gal 0.00 1,500 4,300 Copper(mg/Kg) 0.52 Copper lbs./1,000 gal 0.00 300 840 Lead(mg/Kg) 3.12 Lead lbs./1,000 gal 0.00 17 57 Mercury(mg/Kg) 0.05 Mercury lbs./1,000 gal 0.00 420 420 Nickel(mg/Kg) 2.62 Nickel lbs./1,000 gal 0.00 100 100 Selenium(mg/Kg) 2.62 Selenium lbs./1,000 gal 0.00 2,800 7,500 Zinc(mg/Kg) 153.00 Zinc lbs./1,000 gal 0.02 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) Equations 1st Year 45,200 14,189 28.38 31,011 45,200 14,451 28.90 30,749 1st Yr.PAN(mg/Kg)=(MR x(TKN-NH3))+(VR x NH3)+NOx 2nd Year 31,011 4,652 9.30 26,360 30,749 4,612 9.22 26,137 2nd Yr PAN(mg/Kg)=2nd Yr.TKN x(MR/2) 3rd Year 26,360 1,977 3.95 24,383 26,137 1,960 3.92 24,177 3rd Yr PAN(mg/Kg)=3rd Yr.TKN x(MR/4) 4th Year 24,383 914 1.83 23,468 24,177 907 1.81 23,270 4th Yr PAN(mg/Kg)=4th Yr.TKN x(MR/8) 5th Year 23,468 440 0.88 23,028 23,270 436 0.87 22,834 5th Yr PAN(mg/Kg)=5th Yr.TKN x(MR/16) Total 22,172 44.34 Total 22,366 44.73 Meritech, Inc. jik. Environmental Laboratory Laboratory Certification No. 165 ir- 'P.- -'*10' Contact: Drew Matthews Report Date: 5/11/2021 Client: Soil Plus P.O. Box 1396 Project: Snow Hill Oxford, NC 27565 Date Sample Rcvd: 4/21/2021 Meritech Work Order# 042121172 Sample: SH 042121 Grab 4/21/21 Parameters Results Analysis Date Reporting Limit Method %Total Solids 1.91 % 4/22/21 0-100 % SM 2540B Ammonia, Nitrogen <524 mg/kg 4/26/21 524 mg/kg EPA 350.1 TKN 45,200 mg/kg 4/27/21 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen <524 mg/kg 4/28/21 524 mg/kg EPA 353.2 Aluminum,total 150 mg/kg 5/6/21 2.50 mg/kg EPA 200.7 Arsenic,total <2.62 mg/kg 5/6/21 2.62 mg/kg EPA 200.7 Cadmium,total <0.523 mg/kg 5/6/21 0.523 mg/kg EPA 200.7 Calcium,total 3,220 mg/kg 5/6/21 10.0 mg/kg EPA 200.7 Copper,total <0.523 mg/kg 5/6/21 0.523 mg/kg EPA 200.7 Lead,total 3.12 mg/kg 5/6/21 0.500 mg/kg EPA 200.7 Magnesium,total 355 mg/kg 5/6/21 10.0 mg/kg EPA 200.7 Mercury,total <0.052 mg/kg 4/27/21 0.052 mg/kg EPA 245.1 Molybdenum,total <1.31 mg/kg 5/6/21 1.31 mg/kg EPA 200.7 Nickel,total <2.62 mg/kg 5/6/21 2.62 mg/kg EPA 200.7 Phosphorus,total 1,190 mg/kg 5/6/21 2.00 mg/kg EPA 200.7 Potassium,total 190 mg/kg 5/6/21 20.0 mg/kg EPA 200.7 Selenium,total <2.62 mg/kg 5/6/21 2.62 mg/kg EPA 200.7 Sodium,total 488 mg/kg 5/6/21 20.0 mg/kg EPA 200.7 Zinc,total 153 mg/kg 5/6/21 0.500 mg/kg EPA 200.7 pH 6.2 S.U. 4/26/21 1.0 - 14.0 S.U. SM 4500-HB I hereby certify that I have reviewed and approve these data. yiinandoctlanoxic � Laboratory Representative 642 Tamco Road,Reidsville,North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 I 9.10.1011 Chain of Custody Record (COC) INPDES#: Client: Soil Plus Phone: 252-883-9301 M ERITECH, INC. Address: PO Box 1396 Fax: 919-690-1157 AENVIRONMENTAL LABORATORIES Oxford, NC 27565 Email: samples©soilplus.net . .iirri410 642 Tamco Rd. Phone: 336 342 4748 Project: Town of Snow Hill Reidsville NC 27320 Fax:336-342-1522 P.O.#: Email: info@meritech-labs.corn Attention: Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. 73-GR Hrc WWW.meritee — a S.COl'Yl Circle all that apply: Email(preferred), Fax, Mail ad(10 days) 3-5 Days Lam; _ L.. . . Person Taking Sample(Sign/Print): ",�t% �J2 Lab Use Only Dates & Times Drew Matthews {, D fr Sample Location and/or 1D# Start End Comp? #of Test(s) Required On Ice? pH OK? Date Time Date Time Grab? Cont. 9 , No CI OK? SH 042121 4/21/21 ii:30:WN G 3 Residual Analysis (Al, Ammonia-N, As, Cd, Ca, Cu, Pb, Mg, Hg, Mb, Ni, Nitrate-Nitrite N, %TS, pH, P, K, Se, i P' Na, TKN, Zn) Temperature Upon i i 1 f, Receipt: Method of ***Dechlorination(<0.5 ppm)of Ammonia,Cyanide,Phenol and TKN samples must be done in the field prior to preservation,*** dV Comments: Compositor# Shipment: Please report Residual Analysis results in mg/kg _ UPS Please email results to samples@soilplus.net Jug# Q! Fed Ex Are these results for regulatory purposes? Yes 0 No Q, Report results in: mg/L L mg/kg L ug/L l� Relinquished by. �-1 Date: Time: . Received by: / t t Ti � `~:`Hand Delivery �ec� I"�'' �jZ��Zi y:�� F' 7 Relinquished by: at .Y Time: Received by: Date: Time: Ej; Other �` 2i� Lf �� Relinquished by: Date. Time: Received by Laid n_ ( A`n Date: Time: (Q!3 N, iv" \ ( Ci L Meritech, Inc. Environmental Laboratory 2111. Laboratory Certification No. 165 07: -let Page 1 Contact: Drew Matthews Report Date: 5/21/2021 Client: Soil Plus P.O. Box 1396 Project: Snow Hill Oxford, NC 27565 Date Sample Rcvd: 4/21/2021 Meritech Work Order# 042121169 Sample: SH 042121 Grab 4/21/2021 1311 - TCLP Metals Parameter Results Analysis Date Det.Limit Reg.Limit Method Arsenic <0.100 mg/L 5/4/2021 0.100 5.0 EPA 200.7 Barium 0.157 mg/L 5/4/2021 0.050 100.0 EPA 200.7 Cadmium <0.020 mg/L 5/4/2021 0.020 1.0 EPA 200.7 Chromium <0.050 mg/L 5/4/2021 0.050 5.0 EPA 200.7 Lead <0.100 mg/L 5/4/2021 0.100 5.0 EPA 200.7 Mercury <0.02 mg/L 4/27/2021 0.02 0.2 EPA 245.1 Selenium <0.100 mg/L 5/4/2021 0.100 1.0 EPA 200.7 Silver <0.050 mg/L 5/4/2021 0.050 5.0 EPA 200.7 TCLP Organics Parameter Results Analysis Date Reporting Limit Method Volatiles 8260 Attached 4/28/2021 - 8260 Semi Vol. 8270 Attached 4/29/2021 - 8270 Other Tests Parameter Results Analysis Date Reporting Limit Method %Total Solids 1.84 % 4/26/2021 0-100 % SM 2540B Cyanide,total <0.500 mg/kg 4/26/2021 0.500 mg/kg EPA 335.4 Sulfide <10.0 mg/kg 4/26/2021 <10.0 mg/kg SM4500S2D lgnitability >140 °F 4/22/2021 - EPA 1020 Corrositivity(pH) 6.2 S.U. 4/28/2021 1.0 - 14.0 S.U. SM 4500 HB 642 Tamco Road,Reidsville,North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 VII I Page 2 Contact: Drew Matthews Report Date: 5/21/2021 Client: Soil Plus P.O. Box 1396 Project: Snow Hill Oxford, NC 27565 Date Sample Rcvd: 4/21/2021 Meritech Work Order# 042121169 Sample: SH 042121 Grab 4/21/2021 1311 - TCLP Pesticides & Herbicides Pesticide - SW-846 8081A Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor Endrin Attached - - - Chlordane Attached - - - Toxaphene Attached - - - Methoxychlor Attached - - - Heptachlor Attached - - - Lindane Attached - - - Herbicides - SW-846 8151A Parameter Results Analysis Date net. Limit Reg. Limit Dilution Factor 2,4-D Attached - - - 2,4,5-TP (Silvex) Attached - - - I hereby certify thatI have reviewed and approve these data. ,Ni.fryinfiakinOTIO Laboratory Representative 642 Tamco Road,Reidsville,North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 MERI TECH, INC. „Ali Environmental Laboratories iii:,,„0: Y ' Laboratory Certificate#165 Client: Soil Plus Project: Town of Snow Hill Client Sample ID: SH 042121 Sample Collection: 04/21/21 Meritech Sample ID: 042121169 1311 - TCLP Organics Volatiles: SW-846 8260 Analysis: 04/28/2I Extraction: 04/22/21 Analyst: VWV Report Date: 05/03/21 Parameter Result Units Det.Limit Reg.Limit Dilution Factor Benzene <0.0100 mg/L 0.0100 0.50 10 Carbon Tetrachloride <0.0100 mg/L 0.0100 0.50 10 Chlorobenzene <0.0100 mg/L 0.0100 100 10 Chloroform <0.0100 mg/L 0.0100 6.0 10 1,2-Dichloroethane <0.0100 mg/L 0.0100 0.50 10 1,1-Dichloroethene <0.0100 mg/L 0.0100 0.70 10 Methyl Ethyl Ketone <0.100 mg/L 0.100 200 10 Tetrachloroethylene <0.0100 mg/L 0,0100 0.70 10 Trichloroethene <0.0100 mg/L 0.0100 0.50 10 Vinyl Chloride <0.0200 mg/L 0.020 0.20 10 Semi-Volatiles: SW-846 8270 Analysis: 04/29/21 Extraction: 04/22/21 Analyst: PM Report Date: 04/30/21 Parameter Result Units Det. Limit Reg.Limit Dilution Factor 1,4-Dichlorobenzene <0.100 mg/L 0.100 7.5 I0 Hexachlorobenzene <0.100 mg/L 0.100 0.13 10 Hexachloro-1,3-butadiene <0.100 mg/L 0.100 0.5 10 Hexachloroethane <0.100 mg/L 0.100 3.00 10 o-cresol <0.100 mg/L 0.100 200 10 m&p-cresol <0.200 mg/L 0.200 200 10 Total cresols <0.300 mg/L 0.300 200 I0 Nitrobenzene <0.100 mg/L 0.100 2.00 10 Pentachlorophenol <0.500 mg/L 0.500 I00 10 Pyridine <0.100 mg/L 0.100 5.0 10 2,4,5-Trichlorophenol <0.100 mg/L 0.100 400 10 2,4,6-Trichlorophenol <0.100 mg/L 0.100 2.00 10 2,4-Dinitrotoluene <0.100 mg/L 0.100 0.13 10 I hereby certify that I have reviewed and approve these data. L��, lc% U� 1r Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 * info@meritechlabs.com Client Sample Results Client: Meritech Inc Job ID:680-198174-1 Project/Site: TCLP Pesticides& Herbicides Client Sample ID: 042221-89 Lab Sample ID: 680-198174-1 Date Collected: 04/22/21 10:20 Matrix: Solid Date Received: 04/28/21 11:10 Method: 80818 -Organochlorine Pesticides (GC) -TCLP Analyte Result Qualifier RI MDL Unit D Prepared Analyzed Dil Fac El Chlordane(technical) ND 0.0116 mg/L 05/05/21 17:15 05/07/21 17:53 1 Endrin ND 0.00116 mg/L 05/05/21 17:15 05/07/21 17:53 1 gamma-BHC(Lindane) ND 0.00116 mglL 05/05/21 17:15 05/07/21 17:53 1 Heptachlor ND 0.00116 mg/L 05/05/21 17:15 05/07/21 17:53 1 Heptachlor epoxide ND 0.00116 mg/L 05/05/21 17:15 05/07/21 17:53 1 Methoxychlor ND 0.00116 mg/L 05/05/21 17:15 05/07/21 17:53 1 Toxaphene ND 0.116 mg/L 05/05/21 17:15 05/07/21 17:53 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 88 14-130 05/05/21 17:15 05/07/21 17:53 1 _Tetrachloro-m-xylene 82 40-130 05/05/21 17:15 05/07/21 17:53 1 Method: 8151A- Herbicides (GC)-TCLP Analyte Result Qualifier RI MDL Unit D Prepared Analyzed Dil Fac 2,4-D ND 0.0230 mg/L 05/10/21 15:31 05/13/21 21:49 1 Silvex(2,4,5-TP) ND 0.0115 mg/L 05/10/21 15:31 05/13/21 21:49 1 Pentachlorophenoi ND 0.0115 mg/L 05/10/21 15:31 05/13/21 21:49 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCAA 81 52-151 05/10/21 15:31 05/13/21 21:49 1 Client Sample ID: 042121-169 Lab Sample ID: 680-198174-2 Date Collected: 04/21/21 09:15 Matrix: Solid Date Received: 04/28/21 11:10 Method: 8081B -Organochlorine Pesticides (GC) -TCLP Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chlordane(technical) ND 0.0121 mg/L 05/05/21 17:15 05/07/21 18:08 1 Endrin ND 0.00121 mg/L 05/05/21 17:15 05/07/21 18:08 1 gamma-BHC(Lindane) ND 0_00121 mg/L 05/05/21 17:15 05/07/21 18:08 1 Heptachlor ND 0.00121 mg/L 05/05/21 17:15 05/07/21 18:08 1 Heptachlor epoxide ND 0.00121 mg/L 05/05/21 17:15 05/07/21 18:08 1 Methoxychlor ND 0.00121 mg/L 05105/21 17:15 05/07/21 18:08 1 Toxaphene ND 0.121 mg/L 05/05/21 17:15 05/07/21 18:08 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 112 14-130 05/05/21 17:15 05/07/21 18:08 1 Tetrachloro-m-xylene 85 40-130 05/05/21 17:15 05/07/21 18:08 1 Method: 8151A-Herbicides (GC) -TCLP Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 2,4-D ND 0.0247 mg/L 05/10/21 15:31 05/13/21 22:08 1 Silvex(2,4,5-TP) ND 0.0123 mg/L 05/10/21 15:31 05/13/21 22:08 1 Pentachlorophenol ND 0.0123 mglL 05/10/21 15:31 05/13/21 22:08 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCAA 81 52-151 05/10/21 15:31 05/13/21 22:08 1 Eurofins TestArnerica, Savannah Page 5 of 19 5/20/2021 3.,o.Eax3 Chain of Custody Record (COC) NPDES#: Client: Soil Plus Phone: 252-883-9301 M E R I T E C H, INC. Address: PO Box 1396 Fax: 919-690-1157 . ' Oxford, NC 27565 sam les soil lus.net ":=''•r�;� ENVIRONMENl'AI. LABORATORIES Email: � @ A 11� 642 Tamco Rd. Phone: 336-342-4748 Project: Town of Snow Hill Reidsville NC 27320 Fax:336 342 1522 P.O.#: Email: info@meritech-labs.com Attention: Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. * art(X days) 3 s I 4-4R Ire WWW.I`l'1��I��C1-I� S.C�m Circle all that apply: Email{prererred7, Fax, Mail Sampling Dates & Times PersonTakingSample{sign/Print):Drew Matthews 9.0 I . Lab Use Only Sample Location and/or ID # Start End On Ice? pH OI<? pomp. Hof Test(s) Required es / No Cl OK? Date Time Date Time Grab? Cont. SH 042121 4/21/21 'f;ISA/A G 3 Full TCLP (Ignitability, Corrositivity, Reactivity) `C • Temperature Upon ` Receipt: Method of ***Dechlorination(<0.5 ppm)of Ammonia,Cyanide,Phenol and TKN samples must be done in the field prior to preservation.*** r Comments: Compositor# Shipment: Please report TCLP results in mg/L ups Please email results to samples@soilplus.net Jug# LI Fed Ex Are these results for regulatory purposes? Yes W No Li. Report results in: mg/L L mg/kg L ug/L n Relinquished b : - 1 Date: Time: r Received by: / fate; �� Time Z ;land Delivery q v I ' ( �'t�� Z� 1i,3�Pl'' �� l/�J G�' L Other Relinquished by: I/l,� L e z J Time: j / / / Received by: Date: Time: Relinquished by: r//� Date: f Time: [/f/ ( fr Recelyrd by Lain:_n u T 1 f.✓/, Date: Time: y ,! Town of Snow Hill 2021 Class B Annual Report WQ Permit# WQ0011448 Land Application Field Summary Form ANNUAL LAND APPLICATION FIELD SUMMARY FORM PermitNumber WQ0011448 Site# SH County Greene Crop 1 Annual Ryegrass-Hay Facility Name Town of Snow Hill Field Name 3 SoilSeries Autryville Crop 1 Pan 104 LandOwner Town of Snow Hill Acres Permited 11.40 Soil Abbrevation: AuB Crop 2 Common Bermudagrass Hay Operator Crop 2 Pan 50 Volume Acres Dry Soil Application Total Nitrate-Crop 1 Crop 2 Date Measurement Applied %Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop 04/21/2021 Gallons 94,500 1.91 11.40 0.66 7.53 Town of Snow Hill WWTP Dry <0.5" Surface 1.57 0.50 0.3 45,200 524.00 524.00 18.74 Crop 2 12/28/2021 Gallons 75,000 1.91 11.40 0.52 5.97 Town of Snow Hill WWTP Dry <0.5" Surface 1.25 0.50 0.3 45,200 524.00 524.00 14.87 Crop 1 12/29/2021 Gallons 50,000 1.91 11.40 0.35 3.98 Town of Snow Hill WWTP Dry <0.5" Surface 0.83 0.50 0.3 45,200 524.00 524.00 9.91 Crop 1 Total Volume Applied 219,500 Total Dry Tons 17.48 Sum Total P 3.65 Total 24.78 18.74 Total Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2 PAN PAN Current Year 0.008 0.002 0.002 0.010 0.000 0.004 0.008 0.008 0.469 (lbs./Ac.) (lbs./Ac.) Lime(T/Ac.) Date Prior Year 0.186 0.083 33.446 2.335 2.025 0.161 0.291 1.390 0.236 41.517 Cumulative Total 0.194 0.084 33.448 2.035 0.161 0.295 1.398 0.244 41.986 Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." *Application Method:S-Surface,IN-Injection,INC-Incorporation ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2, aerobically digested-0.3,raw sludge-0.4 **Volatilization Rate:Surface-0.5,Injection/Incorporation-1.0 CAM&A:Li ****C.P.L.R.:Cumulative Pollutant Loading Rate 1-20-2022 Signature of Land Applier Date Town of Snow Hill 2021 Class B Annual Report WQ Permit# WQ0011448 Pathogen & Vector Attraction Reduction Form Fecal Coliform Geometric Mean 30-Day Bench Scale Test ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Snow Hill WQ Permit Number: WQ0011448 WWTP Name: Town of Snow Hill WWTP NPEDS Number: NC0020842 Monitoring Period: 01/01/2021 to 12/31/2021 Pathogen Reduction(15A NCAC 02T .1106) -Please Indicate level achieved and alternative performed: "Class A"Alternative: Not Applicable If applicable to alternative performed("Class A"only)indicate"Process to Further Reduce Pathogens": Not Applicable "Class B"Alternative: Alternative 1 If applicable to alternative performed("Class B"only)indicate"Process to Further Reduce Pathogens": Not Applicable Fecal Coliform Minimum Geo.Mean Maximum #of Exceedences Frequency Sample Type Colonies Per Gram of Total Solids(Dry 476 1,445 3,108 0 Annually Grab Samples Weight) Analytical Technique SM 9222 D Vector Attraction Reduction Performed(15A NCAC 02T.1107): Alt.3 (30-day bench) "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction ❑ requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." orc,ve Jason Smith,VY /< ci.r Preparer Name and Title (type or print) Land Applier Name and Title(if applicable)(type or print) 43,n042 1,20,22 Signature of Preparer* Date Signature of Land Applier(if applicable Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102(26) Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 iA. lo Page 1 Contact: Drew Matthews Report Date: 5/3/2021 Client: Soil Pius P.O. Box 1396 Project: Town of Snow Hill Oxford, NC 27565 Date Sample Rcvd: 4/21/2021 Meritech Work Order# 042121162 Sample: SH 042121 (001) Grab 4/21/21 Parameters Results Analysis Date Reporting Limit Method %Total Solids 1.91 % 4/22/21 0-100 % SM 2540B Fecal Coliform (Sludge) 952 col/g dry wt 4/21/21 130 col/g dry wt SM 9222D Meritech Work Order# 042121163 Sample: SH 042121 (002) Grab 4/21/21 Parameters Results Analysis Date Reporting Limit Method %Total Solids 1.90 % 4/22/21 0-100 % SM 2540E Fecal Coliform (Sludge) 957 col/g dry wt 4/21/21 130 col/g dry wt SM 9222D Meritech Work Order# 042121164 Sample: SH 042121 (003) Grab 4/21/21 Parameters Results Analysis Date Reporting Limit Method %Total Solids 1.17 % 4/22/21 0-100 % SM 2540B Fecal Coliform (Sludge) 3,108 col/g dry wt 4/21/21 130 col/g dry wt SM 9222D Meritech Work Order# 042121165 Sample: SH 042121 (004) Grab 4/21/21 Parameters Results Analysis Date Reporting Limit Method 0/0 Total Solids 1.91 % 4/22/21 0-100 % SM 2540B Fecal Coliform (Sludge) 476 col/g dry wt 4/21/21 130 col/g dry wt SM 9222D 642 Tamco Road,Reidsville,North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory )11 Laboratory Certification No. 165 lel Page 2 Contact: Drew Matthews Report Date: 5/3/2021 Client: Soil Plus P.O. Box 1396 Project: Town of Snow Hill Oxford, NC 27565 Date Sample Rcvd: 4/21/2021 Meritech Work Order# 042121166 Sample: SH 042121 (005) Grab 4/21/21 Parameters Results Analysis Date Reporting Limit Method %Total Solids 1.91 % 4/22/21 0-100 % SM 2540E Fecal Coliform (Sludge) 2,856 col/g dry wt 4/21/21 130 col/g dry wt SM 9222D Meritech Work Order# 042121167 Sample: SH 042121 (006) Grab 4/21/21 Parameters Results Analysis Date Reporting Limit Method %Total Solids 1.91 % 4/22/21 0-100 % SM 2540B Fecal Coliform (Sludge) 1,428 col/g dry wt 4/21/21 130 col/g dry wt SM 9222D Meritech Work Order# 042121168 Sample: SH 042121 (007) Grab 4/21/21 Parameters Results Analysis Date Reporting Limit Met od %Total Solids 1.90 % 4/22/21 0-100 % SM 2540B Fecal Coliform (Sludge) 2,392 col/g dry wt 4/21/21 130 col/g dry wt SM 9222D I hereby certify that I have reviewed and approve these data. _)knaf}( a Won no11 ) Laboratory Representative 642 Tamco Road,Reidsville,North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 3-20.2013 Chain of Custody Record (COC) NPDES#: Client: Soil Plus Phone: 252-883-9301 MERITECH, INC. Address: PO Box 1396 Fax: 919-690-1157 ,, .-_, I. ENVIRONMENTAL LABORATORIES Oxford, NC 27565 Email: samples©soilplus.net .-irs'imi 642Tamco Rd. Phone: 336-342-4748 Project; Town of Snow Hill Reidsville NC 27320 Fax:336-342-1522 P.O.#: I Email: info@meritech-labs.com Attention: Turn Around Time* *RUSH work needs prior approval. How would you like your report sent? ��/�/���p� Std{10 days} � 3-S Days 74-dA Hrs YV VV YY .meritech-labs.com Circle all that apply: Email (preferred}, Fax, Mail I Y ii J1 `4 _� - PersonTakingSample(Sign/Print):Drew Matthews eDfV v - J-^2-+# Lab Use Only Dates & Times .1� Sample Location and/or ID # Start End n Ice? pH OK? Comp? Uof Test(s) Required Date Time Date Time Grab?`Cont. qs / No aOK? SH 042121 (001) 4/21/21 g`I"o AV' G 1 Fecal Coliform I%Total Solids 1 >r, SH 042121 (002) 4/21/21 8;17 AM G 1 Fecal Coliform/% Total Solids , } SH 042121 (003) 4/21/21 FyiS AN` G 1 Fecal Coliform /%Total Solids tt_i SH 042121 (004) • 4/21/21 9:11 ANrk G 1 Fecal Coliform /%Total Solids \k4p S . SH 042121 (005) 4/21/21 g:SD AJ''. G 1 Fecal Coliform /%Total Solids M SH 042121 (006) 4/21/21 j'SZ AM G 1 Fecal Coliform 1% Total Solids k SH 042121 (007) 4/21/21 B:SSAN% G 1 Fecal Coliform/%Total Solids O A — Temperature Upon t� Receipt: ***Dechlorination(<0.5 ppm)of Ammonia,Cyanide,Phenol and TKN samples must be done in the field prior to preservation.*** �� Method of - Cornments: compositor# Shipment: Please email results to samples@soilplus.net laUPS Jug# I��tt } Fed Ex Are these results for regulatory purposes? Yes Q. No Qf Report res is in: mg/L mg/kg 0; ug/L ' Relinquished by: ."7.tJ O G� Date:iil�,/li Time:2,: �J ?et Received by: ` t / Time:, � Hand Delivery //�i 'r V 1 'IJ Relinquished by: �� fJ /`--� , —?/ Time+ / (/ Received by: D te: Time: ���,� Other 7 d�D// °'7 I _ Relinquished by: ate: Time: Recap by Ioh (R _ ('-' j Date: Time: y f i Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Or- .s- Contact: Drew Matthews Report Date: 5/27/2021 Client: Soil Plus P.O. Box 1396 Project: Town of Snow Hill Oxford, NC 27565 Date Sample Rcvd: 4/21/2021 Vector Attraction Reduction /Aerobically Digested Sludge (30 Day Test) Meritech Work Order# 042121171 Sample: SH 042121 Grab 4/21/21 Total Solids Volatile Solids %Volatile Solids Week 1 1.29 0.340 0.264 Week 2 1.46 0.370 0.254 Week 3 1.43 1.04 0.727 Week 4 1.39 1.01 0.727 Week 5 1.33 0.390 0.293 Mass Balance Equation =-11.26%Volatile Solids Reduction as per EPA Part 503 Biosolids Rule I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road,Reidsville,North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 3.2.3 Chain of Custody Record (COC) NPDES#:_ Client: Soil Plus Phone: 252-883-9301 MERITECH, INC. Address: . ! . ENVIRONMENTAL LABORATORIES PO Box 1396 Fax; 919-690-1157 Oxford, NC 27565 Email: samples@soilplus.net .li 40:4:44 642 Tamco Rd. Phone: 336-342-4748 Project: Town of Snow Hill Reidsville NC 27320 Fax:336-342-1522 P.O.#: Turn Around Times Email: infio@meritech-[abs.com Attention; *RUSH work needs prior approval. � How would you like your report sent? wA�v A Y .m erit ec h-labs.c J m Circle all that apply: Email(preferred), Fax, Mail Std(10 s)T3 s -)4.4R Hrc Sampling Dates &Times Person Taking Sample(Sign/Print): Matthews [, & y'L!„4 .LJ2 Lab Use Only Sample Location and/or ID# Start End Comp? #of Test(s) Required On Ice? pH OK? Date Time Date Time Grab? Cont. 5 / No CI OK? SH 042121 4/21/21 9:iOA\ _ G 1 30 Day Bench Scale Test \ —1 Temperature Upon [� ( < Receipt: Method of ***Dechiorination(<0.5 ppm)of Ammonia,Cyanide,Phenol and TKN samples must be done In the field prior to preservation.*** Li Comments: Compositor# Shipment: Please email results to samples@soilplus.net _[] UPS Jug# a: Fed Ex Are these results for regulatory purposes? Yes W' No Q. Report results in: mg/L L mg/kg D ug/L Q' Relinquished by: > LJ 2 Date:1112,1121Time: r� Received by: �m� at Time: LIHand Delivery �.��v r/�,A F', �' ' j��/ Zia �� Other Relinquished by: / v' /f3 /r Time: Received by: (Date: Time: / / Relinquished by: Date: 7 Time: Recei, d by Lab (12,01 Date: Time: (..f r 1 Town of Snow Hill 2021 Class B Annual Report WQ Permit# WQ0011448 Soil Samples WPage1 of 1 r o • Report No: 21-351-0868 2850 Daisy Wilson, NC 27896 Account No: 04596 aypoI I I L . Main 252 206y Lane, Fax 252 NC 27896 -9973 ANALYTICAL www.waypointanalytical.com Advisor: Soil Plus, LLC Client:Granville Farms Inc Farm:Snow Hill Joyce Barrette P.O. Box 1396 Oxford NC 27565 Date Received:12/17/2021 Date of Report: 12/20/2021 Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-I K-I S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I CEC BS% Ca% Mg% ESP Na 19315 3 MIN 0.3 4.7 2.3 253 31 27 50 67 0 340 340 275 3.8 40 26 8 1.3 0 Crop Recommendations: Rec Uom Lime(t/acre) N P205 KZO S Mn Zn Cu B Mg Last Crop 1 Bermudagrass Hay lb/acre 1.6 200 0 159 0 0 0 0 0 Comment: Test result units=CEC and Na in meq/100cm3;NO3 N in mg/dm3;WA/in g/cm3 North Carolina Division of Water Quality Certification#257,Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines,Analysis prepared by:Waypoint Analytical Carolina,Inc.