WQ0006101_Residual Annual Report 2021_20220215

Non-Discharge Branch Upload/Submittal Form
NORTH CAROLINA
EnWron.M&IQualfty
Version 2-Revised June 23.2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0006101
Applicant/Permittee City of Dunn
Email Notifications
Does this need review by the hydrogeologist?* 0 Yes • No
Regional Office Fayetteville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Drew Matthews
Email Address* Phone Number*
[e-mail] 2528839301
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0006101
Has Current Existing permit number
Applicant/Permittee Address* PO Box 1065,Dunn,NC 28335
Facility Name* City of Dunn Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
2021 Dunn Annual Report.pdf 3.83MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature /
OteitI Ql tdd
Submission Date 2/15/2022

CITY OF DUNN
2021 ANNUAL LAND APPLICATION OF
RESIDUAL BIOSOLIDS REPORT
CLASS B PROGRAM
WQ0006101
Submitted by:
Soil Plus
PO Box 1396
Oxford, North Carolina 27565
February 15, 2022
SOIL PLUS
'411111111r.w

SOIL PLUS
February 15,2022
NCDEQ-DWR
Information Processing Unit
1617 Mail Service Center
Raleigh,North Carolina 27699-1617
Re: 2021 LAND APPLICATION ANNUAL REPORT
City of Dunn"Class B" Program
NC Permit No.: WQ0006101
Soil Plus Project No. 202009
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the City of Dunn on behalf of Granville
Farms, Inc. Soil Plus compiled this report using data gathered during the compliance year.
This data includes (1) certification form, (2) residual sampling, (3) field loading calculations,
(4) pathogen and vector attraction reduction documentation, (5) standard soil fertility
nutrient analysis.
The City of Dunn conducted application events on permitted fields in Cumberland and
Harnett counties during 2021. A total of 1,417,000 gallons or 197.94 dry tons of permitted
residual biosolids were land applied to the City of Dunn's permitted fields.
If there is any further information required or questions regarding this report, please do
not hesitate to contact me or the City of Dunn (910-766-0997) for further assistance.
Respectfully,
'Pe.0 NAPilltn
Drew Matthews, Soil Plus
Heather Adams, City of Dunn
Jason Smith, Granville Farms
PO Box 1396
Oxford,NC 27565
[phone]
[e-mail]
www.soilplus.net

Annual Land Application
Certification Form
Annual Residual Sampling
Summary Forms
City of Dunn
2021 Annual Land
Application of
Residual Biosolids
Report
WQ0006101 Field Loading
Summary Forms
Dunn, NC
Pathogen & Vector Attraction
Reduction Forms
2021 Soil Samples

City of Dunn
2021 Class B Annual Report
WQ Permit# WQ0006101
Annual Certification Form
Source Summary
Field Loading Summary

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityNanae Land Application Operator County Phone Number
WQ0006101 City of Dunn Granville Farms,Inc. Harnett [phone]
Year: 2021
Land application of residuals as allowed by the permit occurred during the past calendar year? If No,skip Part A,and Part yes No
B and proceed to Part C. Also,If residuals were generated but not land applied,please attach an explanation on how the Ei
residuals were handled.
Part A-Residuals Application Summary:
Total number of application fields in the permit: 7
Total number of Fields utilized for land application during the year: 7
Total amount of dry tons applied during the year for all application sites: 197.94
Total number of acres utilizes for land application during the year: 67
Part B-Annual Compliance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below)issued by the Division of Water Quality 0
If no please,provide a written description why the facility was not compliant,the dates,and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2.Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6
3.Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)copies of laboratory
results are attached
4.Annual TCLP analysis(if required)was performed and three(3) copies of certified laboratory results are attached
5.All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)copies of
certified laboratory results are attached
6.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7.All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503 regulated facilities
8.All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503 regulated facilities)
9.All operations and maintenance requirements in the permit were complied with or,in the case of a deviation, prior authorization was
received from the Division of Water Quality
10.No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and retnediations.
11,Vegetative cover was maintained and proper crop management was performed on each site receiving residuals,as specified in the permit.
12,No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C-Certification:
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief, true,accurate,and
complete.I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations."
Heather Adams,Public Utilities Director
P rnuttee Name an�itle( pe or print): Signature of Perrnittee Date
� alias � - 2/14/22
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee)
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T 1102(26)
Friday,January 28,2022

Source Summary Report
WWTP VolumeApplied Total ii
Dunn WTP 390,000 45.05
Dunn WWTP 1,027,000 152.89
Total 1,417,000 197.94
Friday,January 28,2022 Page 1 of 1

YEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES
Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2
Field Used Applied Total DT lbs/Ac. lbs/Ac. Crop 1 Name pAN Used Crop 2 Name pAN Used
Site# CU-34
1 4.8 71,500 10.64 38.45 Common 230 16.7%
Bermudagrass Hay
2 4 78,000 11.61 50.34 Common 230 21.9%
Bermudagrass Hay
3 4.3 65,000 9.68 39.02 Common 230 17.0%
Bermudagrass Hay
4 6.2 188,500 28.06 46.01 32.48 Common 225 20.4% Annual Ryegrass- 50 65.0%
Bermudagrass Hay Hay
5 9.7 260,000 38.71 39.79 29.41 Common 230 17.3% Annual Ryegrass- 50 58.8%
Bermudagrass Hay Hay
Site# HA-08
8 18.3 487,500 59.56 16.42 Common 225 7.3%
Bermudagrass Hay
9 19.7 266,500 39.67 34.92 Common 225 15.5%
Bermudagrass Hay
Total 1,417,000 197.94
Friday,January 28,2022 Page 1 of 1

City of Dunn
2021 Class B Annual Report
WQ Permit# WQ0006101
Residual Sampling Summary Forms
Dunn WWTP
Dunn WTP
Field Loading Calculations
2021 Analytical
2021 TCLP

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ000G101 Facility Name City of Dunn Source Permit No. NC0043176 Source Name Dunn W\VTP
Laboratory 1 Merited),Inc.
Laboratory 2
Sample or CompositeDate 4/13/2021
Parameter(mg/Kg) Class A Class B
Aluminum N/A N/A 19,500
Ammonia Nitrogeni N/A N/A 13,600
Arsenic 41 75 1.4
Cadmium 39 85 1.36
Calcium N/A N/A€ 8,660
Copper] 1,500 4,300 227
Lead. 300 840 39.8
Magnesium N/A ', N/A 3,280
Mercury 17 57 0.308
Molybdenum N/A 75 'I 6.22
Nickell 420 420 16.2
Nitrate-Nitrite Nitrogen N/A N/A 280.00
Percent Solids N/A ` N/A 3.57
pH(no units) N/A N/A 7.56
Phosphorus, N/A N/A' 23,000
Potassium; N/A N/A 6,500
PAN(In}./Inc.) N/A N/A 15,470
PAN(Surface) N/A N/A; 8,670
i I
Selenium 100 100 1.4
Sodium! N/A N/A 1,280
SAR N/A N/A 0.56
• TEN N/A N/A 18,900
•
Zinc 2,800 j 7,500 343
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information,including the possibility of fines and imprisonment for knowing violations."
Cerlft,A•Ck,
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r)and I5A NCAC 2T.1102(26)

v AGMAN FIELD LOADING ESTIMATES
Facility Dunn WWTP
Sampling Date 4/13/2021
Solids 3.57
Mineralization Rate 0.3
Gallons per DT 6,717.32
pH 7.5
Sodium Absorpotion 0.56 <5.0 Safe 5.0- 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 18,900 lbs./1,000 gal 5.63 Potassium lbs./1,000 gal 1.94
Ammonia Nitrogen(mg/Kg) 13,600.00 lbs./1,000 gal 4.05 Phosphorus lbs./1,000 gal 6.85
Nitrate-Nitrite (mg/Kg) 280.00 lbs./1,000 gal 0.08 Calcium lbs./1,000 gal 2.58
PLANT AVAILABLE NITROGEN SURFACE APPLIED Magnesium lbs./1,000 gal 0.98
PAN(mg/Kg) 8,670 lbs./1,000 gal 2.58 Manganese lbs./1,000 gal
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./1,000 gal
PAN(mg/Kg) 15,470 lbs./1,000 gal 4.61 Molybdenum lbs./1,000 gal 0.00
Volatization Rate=0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits (mg/Kg) HEAVY METAL CONCENTRATION HEAVY METAL LOADING
41 75 Arsenic(mg/Kg) 1.40 Arsenic lbs./1,000 gal 0.00
39 85 Cadmium(mg/Kg) 1.36 Cadmium lbs./1,000 gal 0.00
1,500 4,300 Copper(mg/Kg) 227.00 Copper lbs./1,000 gal 0.07
300 840 Lead(mg/Kg) 39.80 Lead lbs./1,000 gal 0.01
17 57 Mercury(mg/Kg) 0.31 Mercury lbs./1,000 gal 0.00
420 420 Nickel(mg/Kg) 16.20 Nickel lbs./1,000 gal 0.00
100 100 Selenium(mg/Kg) 1.40 Selenium lbs./1,000 gal 0.00
2,800 7,500 Zinc(mg/Kg) 543.00 Zinc lbs./1,000 gal 0.16
RESIDUAL NITROGEN CALCULATION
Surface Application Injection/Incorporation Application
Remaining Remaining
Organic Organic
PAN PAN Nitrogen PAN PAN Nitrogen
TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) Equations
1st Year 18,900 8,670 17.34 10,230 18,900 15,470 30.94 3,430 1st Yr.PAN(mg/Kg)=(MR x(TKN-NH3))+(VR x NH3)+NOx
2nd Year 10,230 1,535 3.07 8,696 3,430 515 1.03 2,916 2nd Yr PAN(mg/Kg)=2nd Yr.TKN x(MR/2)
3rd Year 8,696 652 1.30 8,043 2,916 219 0.44 2,697 3rd Yr PAN(mg/Kg)=3rd Yr.TKN x(MR/4)
4th Year 8,043 302 0.60 7,742 2,697 101 0.20 2,596 4th Yr PAN(mg/Kg)=4th Yr.TKN x(MR/8)
5th Year 7,742 145 0.29 7,597 2,596 49 0.10 2,547 5th Yr PAN(mg/Kg)=5th Yr.TKN x(MR/16)
Total 11,303 22.61 Total 16,353 32.71

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Alikt
411
Contact: Drew Matthews Report Date: 4/27/2021
Client: Soil Plus
P.O. Box 1396 Project: Dunn WWTP
Oxford, NC 27565 Date Sample Rcvd: 4/13/2021
Meritech Work Order# 041321161 Sample: Dunn Grab 4/13/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 3.57 % 4/14/21 0-100 % SM 2540B
Ammonia, Nitrogen 13,600 mg/kg 4/19/21 10 mg/kg EPA 350.1
TKN 18,900 mg/kg 4/20/21 20 mg/kg EPA 351.1
Nitrate/Nitrite, Nitrogen 280 mg/kg 4/14/21 31.3 mg/kg EPA 353.2
Aluminum,total 19,500 mg/kg 4/21/21 2.50 mg/kg EPA 200.7
Arsenic,total <1.40 mg/kg 4/21/21 1.40 mg/kg EPA 200.7
Cadmium,total 1.36 mg/kg 4/21/21 0.200 mg/kg EPA 200.7
Calcium,total 8,660 mg/kg 4/21/21 10.0 mg/kg EPA 200.7
Copper,total 227 mg/kg 4/21/21 1.00 mg/kg EPA 200.7
Lead,total 39.8 mg/kg 4/21/21 0.500 mg/kg EPA 200.7
Magnesium,total 3,280 mg/kg 4/21/21 10.0 mg/kg EPA 200.7
Mercury,total 0.308 mg/kg 4/20/21 0.02 mg/kg EPA 245.1
Molybdenum,total 6.22 mg/kg 4/21/21 0.500 mg/kg EPA 200.7
Nickel,total 16.2 mg/kg 4/21/21 2.0 mg/kg EPA 200.7
Phosphorus,total 23,000 mg/kg 4/21/21 2.00 mg/kg EPA 200.7
Potassium,total 6,500 mg/kg 4/21/21 20.0 mg/kg EPA 200.7
Selenium,total <1.40 mg/kg 4/21/21 1.40 mg/kg EPA 200.7
Sodium,total 1,280 mg/kg 4/21/21 20.0 mg/kg EPA 200.7
Zinc,total 543 mg/kg 4/21/21 0.500 mg/kg EPA 200.7
pH 7.5 S.U. 4/14/21 1.0 - 14.0 S.U. SM 4500-HB
I hereby certify that I have reviewed and approve these data. t,.,4{rn nicv 1-a
Laboratory Representative
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

3-20.7o13 Chain of Custody Record (COC) NPDES#:
Client: Soil Plus Phone: [phone]
MERITECH, INC. Address: PO Box 1396 Fax: [phone]
ENVIRONMENTAL LABORATORIES Oxford, NC 27565 Email: [e-mail]
.47,40 642 Tamca Rd. Phone: [phone] Project:
Dunn WWTP
Reidsville NC 27320 Fax:[phone] P.O.#:
Email: [e-mail] Attention: Turn Around Time*
- *RUSH work needs prior approval.
/�/ /�WYy How would you like your report sent?
�rY .meritech-Iabs.com Circle all that apply: Email(preferred), Fax, Mail Std(1�0days) 3 s 74-LRHrs
''
T
Person Taking Sample(Sign/Print): dJ 2 Lab Use Only
Dates & Times Drew Matthews -j-ec� l
Sample Location and/or ID # Start End _Comp? #of Test(s) Required 'emOn s l pH OK?
Date Time Date Time Grab? Cont, No CI OK?
Dunn 4/13/21 './O Ark G 3 Residual Analysis (AI, Ammonia-N,As, Cd, Ca, Cu, Pb, i c l
Mg, Hg, Mb, Ni, Nitrate-Nitrite N, %TS, pH, P, K, Se,
Na, TKN, Zn)
Temperature Upon
r 7 Receipt:
Method of
***Dechlorination(<0.5 ppm)of Ammonia,Cyanide,Phenol and TKN samples must be done In the field prior to preservation.*** LL
Comments: Please report Residual Analysis results in mg/kg Compositor#
Shipment:
0; UPS Please email results to [e-mail] Jug#
Q. Fed Ex Are these results for regulatory purposes? Yes W' No eport results in: mg/L l mg/kg 1=5 ug/L '
Relinquished by: • LJ Z Date:411317 iit Time: 1;,3� Qr"� /
Rece ?..at?:
r ,c yed' • ate: ( Time: /�
Hand Delivery
�� Other Relinquished by Date: f 1i J� // �� Received by: Date; Time:
Relinquished by: Date: J Time: Recelvr by a f/�(?`late: Time: 16 a c

Meritech, Inc.
Environmental Laboratory
r, Laboratory Certification No. 165
e:aio Page 1
Contact: Drew Matthews Report Date: 4/28/2021
Client: Soil Plus
P.O. Box 1396 Project: Dunn WWTP
Oxford, NC 27565 Date Sample Rcvd: 4/13/2021
Meritech Work Order# 041321160 Sample: Dunn Grab 4/13/2021
1311 - TCLP Metals
Parameter Results Analysis Date Det.Limit Reg.Limit Method
Arsenic <0.100 mg/L 4/26/2021 0.100 5.0 EPA 200.7
Barium 0.130 mg/L 4/26/2021 0.050 100.0 EPA 200.7
Cadmium <0.020 mg/L 4/26/2021 0.020 1.0 EPA 200.7
Chromium <0.050 mg/L 4/26/2021 0.050 5.0 EPA 200.7
Lead <0.100 mg/L 4/26/2021 0.100 5.0 EPA 200.7
Mercury <0.02 mg/L 4/20/2021 0.02 0.2 EPA 245.1
Selenium <0.100 mg/L 4/26/2021 0.100 1.0 EPA 200.7
Silver <0.050 mg/L 4/26/2021 0.050 5.0 EPA 200.7
TCLP Organics
Parameter Results Analysis Date Reporting Limit Method
Volatiles 8260 Attached 4/20/2021 - 8260
Semi Vol. 8270 Attached 4/23/2021 - 8270
Other Tests
Parameter Results Analysis Date Reporting Limit Method
Total Solids 3.58 % 4/14/2021 0-100 % SM 2540B
Cyanide,total <0.500 mg/kg 4/16/2021 0.500 mg/kg EPA 335.4
Sulfide <10.0 mg/kg 4/16/2021 10.0 mg/kg SM4500S2D
Ignitability Will Not Ignite 4/22/2021 - EPA 1020
Corrositivity(pH) 7.6 S.U. 4/14/2021 1.0 - 14.0 S.U. SM 4500 HB
642 Tamco Road, Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
let
45, Page 2
Contact: Drew Matthews Report Date: 4/28/2021
Client: Soil Plus
P.O.Box 1396 Project: Dunn WWTP
Oxford, NC 27565 Date Sample Rcvd: 4/13/2021
Meritech Work Order# 041321160 Sample: Dunn Grab 4/13/2021
1311 - TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor
Endrin Attached - - -
Chlordane Attached - - -
Toxaphene Attached - - -
Methoxychlor Attached - - -
Heptachlor Attached - - -
Lindane Attached - - -
Herbicides - SW-846 8151A
Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor
2,4-D Attached - - -
2,4,5-TP (Silvex) Attached - - -
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.
_4_ Environmental Laboratories
tocLaboratory Certificate#165
ifif
Client: Soil Plus
Project: Dunn WWTP
Client Sample ID: Dunn
Sample Collection: 04/13/21
Meritech Sample ID: 041321160
1311 - TCLP Organics
Volatiles: SW-846 8260
Analysis: 04/20/21 Extraction: 04/15/21
Analyst: VWV Report Date: 04/22/21
Parameter Result Units Det. Limit Reg.Limit Dilution Factor
Benzene <0.0100 mg/L 0.0100 0.50 10
Carbon Tetrachloride <0.0100 mg/L 0.0100 0.50 10
Chlorobenzene <0.0100 mg/L 0.0100 100 10
Chloroform <0.0100 mg/L 0.0100 6.0 10
1.2-Dichloroethane <0.0100 mg/L 0.0100 0.50 10
1,1-Di chl oroethene <0.0100 mg/L 0.0I00 0.70 10
Methyl Ethyl Ketone <0.100 mg/L 0.100 200 10
Tetrachloroethylene <0.0100 mg/i. 0.0100 0.70 10
Trichloroethene <0.0100 mg/L 0.0100 0.50 10
Vinyl Chloride <0.0200 mg/L 0.020 0.20 10
Semi-Volatiles: SW-846 8270
Analysis: 04/23/21 Extraction: 04/15/21
Analyst: PM Report Date: 04/26/21
Parameter Result Units Det. Limit Reg. Limit Dilution Factor
1,4-Dichlorobenzene <0.100 mg/L 0.100 7.5 10
Hexachlorobenzene <0.100 mg/L 0.100 0.13 10
Hexachloro-1,3-butadiene <0.100 mg/L 0.100 0.5 10
Hexachloroethane <0.100 mg/L 0.100 3.00 10
o-cresol <0.100 mg/L 0.100 200 10
m&p-cresol <0.200 mg/L 0.200 200 10
Total cresols <0.300 mg/L 0.300 200 10
Nitrobenzene <0.100 mg/L 0.100 2.00 10
Pentachlorophenol <0.500 mg/L 0.500 100 10
Pyridine <0.100 mg/L 0.100 5.0 10
2.4,5-Trichlorophenol <0.100 mg/L 0.100 400 10
2,4,6-Trichlorophenol <0.100 mg/i. 0.100 2.00 10
2,4-Dinitrotoluene <0.100 mg/L 0.100 0.13 10
I hereby certift that I have reviewed and approve these data. '
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] * [e-mail]

Pace Analytical Services,LLC
®
aceAnalytical
205 East Meadow Road-Suite A
Eden,NC 27288
wwv.pacalabscom [phone]
ANALYTICAL RESULTS
Project: TCLP PEST/HERB
Pace Project No.: 92532999
Sample: 041321-160 Lab ID: 92532999001 Collected: 04/13/21 09:00 Received: 04/14/21 10:05 Matrix: Solid
Results reported on a "dry weight"basis and are adjusted for percent moisture,sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Pesticides(GC)8081 B TCLP Analytical Method: EPA 8081 B Preparation Method:3510C
Leachate Method/Date:1311;04/20/21 09:42 Initial pH:7.41;Final pH:4.83
Pace National-Mt.Juliet
Chlordane(Technical) ND mg/L 0.00500 0.00167 1 04/22/21 06:02 04/22/21 13:08 57-74-9
Endrin ND mg/L 0.00500 0.00167 1 04/22/21 06:02 04/22/21 13:08 72-20-8
Heptachlor ND mglL 0.00500 0.00167 1 04/22/21 06:02 04/22/21 13:08 76-44-8
gamma-BHC(Lindane) ND mglL 0.00500 0.00167 1 04/22/21 06:02 04/22/21 13:08 58-89-9
Methoxych#or ND mg/L 0.00500 0.00167 1 04/22/21 06:02 04/22/21 13:08 72-43-5
Toxaphene ND mg/L 0.0100 0.00333 1 04/22/21 06:02 04/22/21 13:08 8001-35-2
Surrogates
Decachlorobiphenyl(S) 88.5 % 10.0-128 1 04/22/21 06:02 04/22/21 13:08 2051-24-3
Tetrachloro-m-xylene(S) 89.4 % 10.0-127 1 04/22/21 06:02 04/22/21 13:08 877-09-8
Chlorinated Herb.(GC)8151A Analytical Method:EPA8151A Preparation Method:8151A
Leachate Method/Date:1311;04/20/21 09:42 Initial pH:7.41:Final pH:4.83
Pace National-Mt.Juliet
2,4,5-TP(Silvex) ND mg/L 0.00200 0.000667 1 04/22/21 07:43 04/22/21 19:29 93-72-1
2,4-D ND mglL 0.00200 0.000667 1 04/22/21 07:43 04/2212119:29 94-75-7
Surrogates
2,4-DCAA(S) 65.8 % 14.0-158 1 04/22/21 07:43 04/22/21 19:29 19719-28-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/27/2021 05:06 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 24

-3.20E011 Chain of Custody Record (COC) NPDES#:
Client: Soil Plus Phone: [phone]
M E R I T E CH, INC. Address: PO Box 1396 Fax: [phone]
iF'f: Oxford, NC 27565 sam les soil lus.net
i'` '' ..- ENVIRONMENTAL LABORATORIES Email: p @ p
ikl911�' 642Tamco Rd. Phone: 336 3A2 4748 Project: Dunn VWITfP
Reidsville NC 27320 Fax:[phone] P.O.#:
Email: [e-mail] Attention: Turn Around Time*
*RUSH work needs prior approval.
/��\/� How would you like your report sent?
WYV VY .meritech-labs.com Circle all that apply: Email(preferred), Fax, Mail Std 10da4s) 3-5
I Days 74-ARHrc
---
Sampling Dates & Times Person TakingSampEe(Slgn/Print):Drew Matthews 17 f Lab Use Only
Sample Location and/or ID # Start End
Comp? #of Test(s) Required e / No Cl OK?
nice? pH OK?
Date Time Date Time Grab? Cont. "I
Dunn 4/13/21 9:c01),t' G 3 Full TCLP (Ignitability, Corrositivity, Reactivity) VC()
•
Terpperature Upon
7 Receipt:
Method of
***Dechlorination(<0.5 ppm)of Ammonia,Cyanide,Phenol and TKN samples must be done in the field prior to preservation.*** d
Comments: Compositor#
Shipment: Please report TCLP results in mg/L
13 UPS Please email results to [e-mail] Jug#
I Fed Ex Are these results for regulatory purposes? Yes W No Li Report result In: mg/L [ mg/kg ug/L L.
Relinquished by: Date: I Tlrne: ReyelGe Gate Time: I r -
:Hand Delivery ' W'1�1Z1 S �(�'� / f '��' r 1
Relinquis tl'by: Date:N r �/Time: 7-‘ifys‘aeceiv-ed 6�: 2 Date: Time:
Other (� /L l�1 '`�
Relingrtlsl�ied b : L.J Date: Time: Rece ved by La : y\ i) D g: Time: 160 f
CAM , 1�.1 "L 1 V U'J

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0006101 Facility Name City of Dunn Source Permir No. 03-43-010 Source Name Dunn WIP
Laboratory 1 Meritech,Inc.
Laboratory 2
Sample or CompositeDatel 4/13/2021
Parameter(mg/Kg) Class A Class B
Aluminumi N/A N/A 1 82,300
Ammonia Nitrogen' N/A N/A 361
Arsenic 41 75 3.79
Cadmium 39 85 0361
Calcium N/A N/A 1,080
Copper 1,500 4,300 24.5
Lead 300 840 1.81
Magnesium. N/A N/A 834
i
Mercury) 17 57 0.072
Molybdenum N/A 75 2.53
Nickel 420 420 5.85
Nitrate-Nitrite Nitrogen N/A N/A' 361.00
Percent Solids N/A N/A 2.77
pfd(no units); N/A N/A 6.10
Phosphorus] N/A N/A 1.060
Potassium' N/A N/A 408
PAN(Inj./Inc.) N/A N/A 722
PAN(Surface) N/A N/A 542
Selenium 100 100 1.81
Sodium N/A N/A 603
SARI N/A N/A 0.56
TKN N/A N/A 37.200
Zinc 2,800 7,500 44.8
"E certify,under penalty of law,that this docu eat was prepared under my direction or supervision in accordance with a system designed to
assure that qualified persona r erly gash ed and evaluated the information submitted. I am aware that there are significant penalties for
submitting false informs' . eluding th ossibility of fines and imprisonment for knowing violations."
2-14f•ZZ.
Signature of Preparer* Date
*Preparer is defined in 40 CPR Part 503.9(r)and 15A NCAC 2T.1102(26)

v -if AGMAN FIELD LOADING ESTIMATES
Facility Dunn WTP
Sampling Date 4/13/2021
Solids 2.77
Mineralization Rate 0
Gallons per DT 8,657.33
pH 6.1
Sodium Absorpotion 0.56 <5.0 Safe 5.0- 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 37,200 lbs./1,000 gal 8.59 Potassium lbs./1,000 gal 0.09
Ammonia Nitrogen(mg/Kg) 361.00 lbs./1,000 gal 0.08 Phosphorus lbs./1,000 gal 0.24
Nitrate-Nitrite (mg/Kg) 361.00 lbs./1,000 gal 0.08 Calcium lbs./1,000 gal 0.25
PLANT AVAILABLE NITROGEN SURFACE APPLIED Magnesium lbs./1,000 gal 0.19
PAN(mg/Kg) 542 lbs./1,000 gal 0.13 Manganese lbs./1,000 gal
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./1,000 gal
PAN(mg/Kg) 722 lbs./1,000 gal 0.17 Molybdenum lbs./1,000 gal 0.00
Volatization Rate=0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits (mg/Kg) HEAVY METAL CONCENTRATION HEAVY METAL LOADING
41 75 Arsenic(mg/Kg) 3.79 Arsenic lbs./1,000 gal 0.00
39 85 Cadmium(mg/Kg) 0.36 Cadmium lbs./1,000 gal 0.00
1,500 4,300 Copper(mg/Kg) 24.50 Copper lbs./1,000 gal 0.01
300 840 Lead(mg/Kg) 1.81 Lead lbs./1,000 gal 0.00
17 57 Mercury(mg/Kg) 0.07 Mercury lbs./1,000 gal 0.00
420 420 Nickel(mg/Kg) 5.85 Nickel lbs./1,000 gal 0.00
100 100 Selenium(mg/Kg) 1.81 Selenium lbs./1,000 gal 0.00
2,800 7,500 Zinc(mg/Kg) 44.80 Zinc lbs./1,000 gal 0.01
RESIDUAL NITROGEN CALCULATION
Surface Application Injection/Incorporation Application
Remaining Remaining
Organic Organic
PAN PAN Nitrogen PAN PAN Nitrogen
TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) Equations
1st Year 37,200 542 1.08 36,659 37,200 722 1.44 36,478 1st Yr.PAN(mg/Kg)=(MR x(TKN-NH3))+(VR x NH3)+NOx
2nd Year 36,659 0 0.00 36,659 36,478 0 0.00 36,478 2nd Yr PAN(mg/Kg)=2nd Yr.TKN x(MR/2)
3rd Year 36,659 0 0.00 36,659 36,478 0 0.00 36,478 3rd Yr PAN(mg/Kg)=3rd Yr.TKN x(MR/4)
4th Year 36,659 0 0.00 36,659 36,478 0 0.00 36,478 4th Yr PAN(mg/Kg)=4th Yr.TKN x(MR/8)
5th Year 36,659 0 0.00 36,659 36,478 0 0.00 36,478 5th Yr PAN(mg/Kg)=5th Yr.TKN x(MR/16)
Total 542 1.08 Total 722 1.44

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Revised Report Date: 5/18/2021
Contact: Drew Matthews Report Date: 5/4/2021
Client: Soil Plus
P.O.Box 1396 Project: Dunn WTP
Oxford,NC 27565 Date Sample Rcvd: 4/13/2021
Meritech Work Order# 041321163 Sample: WTP Grab 4/13/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 2.77 % 4/14/21 0-100 % SM 2540B
Ammonia, Nitrogen <361 mg/kg 4/19/21 361 mg/kg EPA 350.1
TKN 37,200 mg/kg 4/20/21 20 mg/kg EPA 351.2
Nitrate/Nitrite,Nitrogen <361 mg/kg 4/19/21 361 mg/kg EPA 353.2
Aluminum,total 82300 mg/kg 5/3/21 2.50 mg/kg EPA 200.7
Arsenic,total 3.79 mg/kg 4/21/21 0.500 mg/kg EPA 200.7
Cadmium,total <0.361 mg/kg 4/21/21 0.361 mg/kg EPA 200.7
Calcium,total 1,080 mg/kg 4/21/21 10.0 mg/kg EPA 200.7
Copper,total 24.5 mg/kg 4/21/21 0.100 mg/kg EPA 200.7
Lead,total <1.81 mg/kg 4/21/21 1.81 mg/kg EPA 200.7
Magnesium,total 834 mg/kg 4/21/21 10.0 mg/kg EPA 200.7
Mercury,total 0.072 mg/kg 4/20/21 0.02 mg/kg EPA 245.1
Molybdenum,total 2.53 mg/kg 4/21/21 1.48 mg/kg EPA 200.7
Nickel,total 5.85 mg/kg 4/21/21 2.96 mg/kg EPA 200.7
Phosphorus,total 1,060 mg/kg 4/21/21 2.00 mg/kg EPA 200.7
Potassium,total 408 mg/kg 4/21/21 20.0 mg/kg EPA 200.7
Selenium,total <1.81 mg/kg 4/21/21 1.81 mg/kg EPA 200.7
Sodium,total 603 mg/kg 4/21/21 20.0 mg/kg EPA 200.7
Zinc,total 44.8 mg/kg 4/21/21 0.500 mg/kg EPA 200.7
pH 6.1 S.U. 4/14/21 1.0 - 14.0 S.U. SM 4500-HB
I hereby certify that I have reviewed and approve these data. , I)fl{ Wino,0013
Laboratory Representative
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

I -
3.2U.EA13 Chain of Custody Record (COC) NPDES#:
Client: Soil Plus Phone: [phone]
M ERITECH, INC. Address: PO Box 1396 Fax: [phone]
'` ENVIRONMENTAL LABORATORIES Oxford, NC 27565 Email: [e-mail]
.;411/40
642 Tamco Rd. Phone: [phone] Project:
Dunn WTP
Reidsville NC 27320 Fax:[phone] P.O.#:
Email: [e-mail] Attention: Turn Around Time*
*RUSH work needs prior approval.
/��\/���/� How would you like your report sent?
• Y y Y Y y y .m e ri t e e h—1 a b s.c 0 m Circle all that apply: Email(preferred), Fax, Mail Stud(1�0 day��s) 3-5 Days 74-4R Hrs
Person Taking Sample(Sign/Print): �i%}�ZJ2 Lab Use Only
Dates & Times Drew Matthews & (AID
Sample Location and/or ID # Start End comp? #of Test(s) Required r#Iin Ice? pH OK?
Date Time Date Time Grab? Cont. ;rs / No Cl OK?
WTP 4/13/21 IJ !S PP` G 3 Residual Analysis (Al, Ammonia-N,As, Cd, Ca, C`,rb,
Mg, Hg, Mb, Ni, Nitrate-Nitrite N, %TS, pH, P, K, Se,
Na, TKN, Zn)
•
•
Temperature Upon
L .7 Receipt:
*** Dechlorination(<0.5 ppm)of Ammonia,Cyanide,Phenol and TKN samples must be done In the field prior to preservation.***
Method off
Comments: Compositor#
Shipment: Please report Residual Analysis results in mg/kg
UPS Please email results to [e-mail] Jug#
U Fed Ex Are these results for regulatory purposes? Yes i J No Q:: f Report results in: mg/L L. mg/kg ug/L
Relinquished by: 2J 2 Date: Time: Rec iv day: -L Date: Time:
Hand Delivery 2c� ��!'31 z, �S PN� ki—f ?-2 i l
E Other Reiinqulshed,by',:.• L-J ._,)/' l
L1J 4�Date: r�.I7, �I e: / Received by: Date: Time:
Relinquished by:/ Date: -lime: Recllyed by Lai: in CI _f`) _)1 Date: Time: (6Q,(

Meritech, Inc.
Environmental Laboratory
. Laboratory Certification No. 165
firviji
Page 1
Contact: Drew Matthews Report Date: 4/28/2021
CIient: Soil Plus
P.O. Box 1396 Project: Dunn WTP
Oxford, NC 27565 Date Sample Revd: 4/13/2021
Meritech Work Order# 041321162 Sample: WTP Grab 4/13/2021
1311 - TCLP Metals
Parameter Results Analysis Date Det.Limit Reg.Limit Method
Arsenic <0.100 mg/L 4/26/2021 0.100 5.0 EPA 200.7
Barium 0.074 mg/L 4/26/2021 0.050 100.0 EPA 200.7
Cadmium <0.020 mg/L 4/26/2021 0.020 1.0 EPA 200.7
Chromium <0.050 mg/L 4/26/2021 0.050 5.0 EPA 200.7
Lead <0.100 mg/L 4/26/2021 0.100 5.0 EPA 200.7
Mercury <0.02 mg/L 4/20/2021 0.02 0.2 EPA 245.1
Selenium <0.100 mg/L 4/26/2021 0.100 1.0 EPA 200.7
Silver <0.050 mg/L 4/26/2021 0.050 5.0 EPA 200.7
TCLP Organics
Parameter Results Analysis Date Reporting Limit Method
Volatiles 8260 Attached 4/20/2021 - 8260
Semi Vol. 8270 Attached 4/23/2021 - 8270
Other Tests
Parameter Results Analysis Date Reporting Limit Method
%Total Solids 2.77 % 4/16/2021 0-100 % SM 2540B
Cyanide,total <0.500 mg/kg 4/16/2021 0.500 mg/kg EPA 335.4
Sulfide <10.0 mg/kg 4/16/2021 10.0 mg/kg SM4500S2D
Ignitability Will Not Ignite 4/22/2021 - EPA 1020
Corrositivity(pH) 6.4 S.U. 4/14/2021 1.0 - 14.0 S.U. SM 4500 HE
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 2
Contact Drew Matthews Report Date: 4/28/2021
CIient: Soil Plus
P.O. Box 1396 Project: Dunn WTP
Oxford, NC 27565 Date Sample Rcvd: 4/13/2021
Meritech Work Order# 041321162 Sample: WTP Grab 4/13/2021
1311 - TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor
Endrin Attached - - -
Chlordane Attached - - -
Toxaphene Attached - - -
Methoxychlor Attached - - -
Heptachlor Attached - - -
Lindane Attached - - -
Herbicides - SW-846 8151A
Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor
2,4-D Attached - - -
2,4,5-TP (Silvex) Attached - - -
ri>LA
I hereby certify that I have reviewed and approve these data,
aboratory Representative
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

It. MERITECH, INC.
r:
_ , Environmental Laboratories
Laboratory Certificate#165
e
Client: Soil Plus
Project: Dunn WTP
Client Sample ID: WTP
Sample Collection: 04/13/21
Meritech Sample ID: 041321162
1311 - TCLP Organics
Volatiles: SW-846 8260
Analysis: 04/20/21 Extraction: 04/15/21
Analyst: VWV V Report Date: 04/22/21
Parameter Result Units Det.Limit Rea.Limit Dilution Factor
Benzene <0.0100 mg/L 0.0100 0.50 10
Carbon Tetrachloride <0.0100 mg/L 0.0100 0.50 10
Chlorobenzene <0.0100 mg/L 0.0100 100 10
Chloroform <0.0100 mg/L 0.0100 6.0 10
1,2-Dichloroethane <0.0100 mg/L 0.0100 0.50 10
1,1-Dichloroethene <0.0100 mg/L 0.0100 0.70 10
Methyl Ethyl Ketone <0.100 mg/L 0.100 200 10
Tetrachtoroethylene <0.0100 mg/L 0.0100 0.70 10
Trichloroethene <0.0100 mg/L 0.0100 0.50 10
Vinyl Chloride <0.0200 mg/L 0.020 0.20 10
Semi-Volatiles: SW-846 8270
Analysis: 04/23/21 Extraction: 04/15/2I
Analyst: PM Report Date: 04/26/21
Parameter Result Units Det.Limit Rea. Limit Dilution Factor
1,4-Dichlorobenzene <0.100 mg/L 0.100 7.5 10
Hexachlorobenzene <0.100 mg/L 0.100 0.13 10
Hexachloro-1,3-butadiene <0.100 mg/L 0.100 0.5 10
Hexachloroethane <0.100 mg/L 0.100 3.00 10
o-cresol <0.100 mg/L 0.100 200 10
m&p-cresol <0.200 mg/1, 0.200 200 10
Total cresols <0.300 mg/L 0.300 200 10
Nitrobenzene <0.100 mg/L 0.100 2.00 10
Pentachlorophenol <0.500 mg/L 0.500 100 10
Pyridine <0.100 mg/L 0.100 5.0 10
2,4,5-Trichlorophenol <0.100 mg/L 0.100 400 10
2,4,6-Trichlorophenol <0.100 mg/L 0.100 2.00 10
2,4-Dinitrotoluene <0.100 mg/L 0.100 0.13 10
I hereby certify that I have reviewed and approve these data. 1�y , v,. r,/ �;� ,
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] * [e-mail]

Pace Analytical Services,LLC
�VLr ^r ' 205 East Meadow Road-Suite A
Lr�f�� i.^ Eden,NC 27288
www.pacalaps.com [phone]
ANALYTICAL RESULTS
Project: TCLP PEST 1 HERB
Pace Project No.: 92532999
Sample: 041 32 1-1 62 Lab ID: 92532999002 Collected: 04/13/21 11:00 Received: 04/14/21 10:05 Matrix: Solid
Results reported on a "dry weight"basis and are adjusted for percent moisture,sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Dual
Pesticides(GC)8081E TCLP Analytical Method:EPA 8081B Preparation Method:3510C
Leachate Method/Date:1311;04/20/21 09:42 Initial pH:6.13;Final pH:4.83
Pace National-Mt.Juliet
Chlordane(Technical) ND mg/L 0.00500 0.00167 1 04/22/21 06:02 04/22/21 13:21 57-74-9
Endrin ND mg/L 0.00500 0.00167 1 04/22/21 06:02 04/22/21 13:21 72-20-8
Heptachlor ND mg/L 0.00500 0.00167 1 04/22/21 06:02 04/22/21 13:21 76-44-8
gamma-BHC(Lindane) ND mglL 0.00500 0.00167 1 04/22/21 06:02 04/22121 13:21 58-89-9
Methoxychlor ND mglL 0.00500 0.00167 1 04/22/21 06:02 04/22/21 13:21 72-43-5
Toxaphene ND mg!L 0.0100 0.00333 1 04/22/21 06:02 04/22/21 13:21 8001-35-2
Surrogates
Decachlorobiphenyl(S) 88.8 % 10.0-128 1 04/22/21 06:02 04/22/21 13:21 2051-24-3
Tetrachloro-m-xylene(S) 87.4 % 10.0-127 1 04/22/21 06:02 04/22/21 13:21 877-09-8
Chlorinated Herb.(GC)8151A Analytical Method:EPA 8151A Preparation Method:8151A
Leachate Method/Date:1311;04/20/21 09:42 Initial pH:6.13;Final pH:4.83
Pace National-Mt.Juliet
2,4,5-TP(Silvex) ND mg/L 0.00200 0.000667 1 04/22/21 07:43 04/22/21 19:44 93-72-1
2,4-D ND mg/L 0.00200 0.000667 1 04/22/21 07:43 04/22/2119:44 94-75-7
Surrogates
24-DCAA(S) 69.2 % 14.0-158 1 04/22/21 07:43 04/22/21 19:44 19719-28-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/27/2021 05:06 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 24

340.2013 Chain of Custody Record (COC) NPDES#:
Client: Soil Plus Phone: [phone]
M ERITECH� INC. Address: PO Box 1396 Fax: [phone]
';'" ENVIRONMENTAL LABORATORIES Oxford, NC 27565 Email: [e-mail]
642 Tamco Rd. Phone: [phone] Project:
Dunn WTP
Reidsville NC 27320 Fax:[phone] P.O.#:
Email: [e-mail] Attention: Turn Around rime*
-- *RUSH work needs prior approval.
How would you like your report sent?
W Y Y�/�� Y r�/��.meritec h—Ia bs.cc m Circle all that apply: Email(preferred), Fax, Mail Std(10 days) 3-5 oa s )4-aRHrc
1
h� , _[.= .F -
Sampling Dates & Times PersonTalting5ample(Sign/Print) Drew Matthews, I" 0^44-f Lab Use Only
Sample Location and/or ID# Start End romp? #of On Ice? pH OK?
Date Time Date Time Grab? Cont. Test(s) Required Y@is / No Cl OK?
WTP _4/13/21 Il:HMO,- - G 3 Full TCLP (Ignitability, Corrositivity, Reactivity) 1(Q)_
•
Temperature Upon
(Receipt:
Method of ***Dechlorination(<0.5 ppm)of Ammonia,Cyanide,Phenol and TKN samples must be done in the field prior to preservation.*** — L t7'
Comments: Please report TCLP results in mg/L
Compositor#
Shipment:
0; UPS Please email results to [e-mail] Jug#
Q. Fed Ex Are these results for regulatory purposes? Yes W. No Q. eport ruls i mg/L LI mg/kg O. ug/L
•
Relinquished b : Date: Time: , Recew q� f prme:
Hand Delivery q y �1 } Q,.�/4 61>�l31lit j: is% ) estn:
T�f 3'.7r (5?
I ,J; Other Relinquished-b �/`�'" Date //r `., ire: I� 0 Received by: Date: Time:
Relinquished by: Date: f Time: RTC,"ed by L i?_21 Dale: Time: Q

City of Dunn
2021 Class B Annual Report
WQ Permit# WQ0006101
Land Application Field Summary Forms

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0006101 Site# CU-34 County Harnett Crop 1 Common Bermudagrass Hay
Facility Name City of Dunn Field Name 1 SoilSeries Goldsboro Crop 1 Pan 230
LandOwner Harold Lee Eldridge Acres Permited 4.80 Soil Abbrevation: GoA Crop 2
Operator Crop 2 Pan
Volume Acres Dry Soil Application Total Nitrate-Crop 1 Crop 2
Date Measurement Applied %Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop
04/20/2021 Gallons 58,500 3.57 4.80 1.81 8.71 Dunn WWTP Dry <0.5" Surface 83.46 0.50 0.3 18,900 13,600.00 280.00 31.46 Crop 1
04/21/2021 Gallons 13,000 3.57 4.80 0.40 1.94 Dunn WWTP Dry <0.5" Surface 18.55 0.50 0.3 18,900 13,600.00 280.00 6.99 Crop 1
Total Volume Applied 71,500 Total Dry Tons 10.64 Sum Total P 102.01 Total 38.45 Total
Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2
PAN PAN
Current Year 0.006 0.006 1.007 0.177 0.001 0.028 0.072 0.006 2.408 (lbs./Ac.) (lbs./Ac.)
Lime(T/Ac.) Date
Prior Year 0.435 0.101 11.626 1.837 1.641 0.066 0.435 0.945 0.380 20.711
Cumulative Total 0.441 0.107 12.633 1.818 0.067 0.463 1.017 0.386 23.119 1.0 T/Ac 11/30/21
Permitted CPLR 36 34 1338 267 15 374 89 2498
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
janIt SLV44:1Li *Application Method:S-Surface,IN-Injection,INC-Incorporation**Volatilization Rate:Surface-0.5,Injection/Incorporation-1.0 ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.:Cumulative Pollutant Loading Rate
1/28/2022
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0006101 Site# CU-34 County Harnett Crop 1 Common Bermudagrass Hay
Facility Name City of Dunn Field Name 2 SoilSeries Goldsboro Crop 1 Pan 230
LandOwner Harold Lee Eldridge Acres Permuted 4.00 Soil Abbrevation: GoA Crop 2
Operator Crop 2 Pan
Volume Acres Dry Soil Application Total Nitrate-Crop 1 Crop 2
Date Measurement Applied %Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop
04/19/2021 Gallons 58,500 3.57 4.00 2.18 8.71 Dunn WWTP Dry <0.5" Surface 100.15 0.50 0.3 18,900 13,600.00 280.00 37.75 Crop 1
04/20/2021 Gallons 19,500 3.57 4.00 0.73 2.90 Dunn WWTP Dry <0.5" Surface 33.38 0.50 0.3 18,900 13,600.00 280.00 12.58 Crop 1
Total Volume Applied 78,000 Total Dry Tons 11.61 Sum Total P 133.54 Total 50.34 Total
Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2
PAN PAN
Current Year 0.008 0.008 1.318 0.231 0.002 0.036 0.094 0.008 3.153 (lbs./Ac.) (lbs./Ac.)
Lime(T/Ac.) Date
Prior Year 0.418 0.093 9.914 1.588 1.387 0.059 0.378 0.776 0.371 17.585
Cumulative Total 0.426 0.101 11.232 1.618 0.061 0.414 0.870 0.379 20.738 1.0 T/Ac 11/30/21
Permitted CPLR 36 34 1338 267 15 374 89 2498
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
*Application Method:S-Surface,IN-Injection,INC-Incorporation ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
dyebt **Volatilization Rate:Surface-0.5,Injection/Incorporation-1.0
aerobically digested-0.3,raw sludge-0.4
S.,44.41,.
****C.P.L.R.:Cumulative Pollutant Loading Rate
1/28/2022
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0006101 Site# CU-34 County Harnett Crop 1 Common Bermudagrass Hay
Facility Name City of Dunn Field Name 3 SoilSeries Goldsboro Crop 1 Pan 230
LandOwner Harold Lee Eldridge Acres Permuted 4.30 Soil Abbrevation: GoA Crop 2
Operator Crop 2 Pan
Volume Acres Dry Soil Application Total Nitrate-Crop 1 Crop 2
Date Measurement Applied %Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop
04/21/2021 Gallons 65,000 3.57 4.30 2.25 9.68 Dunn WWTP Dry <0.5" Surface 103.52 0.50 0.3 18,900 13,600.00 280.00 39.02 Crop 1
Total Volume Applied 65,000 Total Dry Tons 9.68 Sum Total P 103.52 Total 39.02 Total
Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2
PAN PAN
Current Year 0.006 0.006 1.022 0.179 0.001 0.028 0.073 0.006 2.444 (lbs./Ac.) (lbs./Ac.)
Lime(T/Ac.) Date
Prior Year 0.468 0.105 11.738 1.939 1.667 0.068 0.457 1.043 0.390 20.927
Cumulative Total 0.474 0.111 12.760 1.846 0.069 0.485 1.116 0.396 23.371 1.0 T/Ac 11/30/21
Permitted CPLR 36 34 1338 267 15 374 89 2498
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
*Application Method:S-Surface,IN-Injection,INC-Incorporation ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
k
**Volatilization Rate:Surface-0.5,Injection/Incorporation-1.0
****C.P.L.R.:Cumulative Pollutant Loading Rate
1/28/2022
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0006101 Site# CU-34 County Harnett Crop 1 Common Bermudagrass Hay
Facility Name City of Dunn Field Name 4 SoilSeries Norfolk Crop 1 Pan 225
LandOwner Harold Lee Eldridge Acres Permuted 6.20 Soil Abbrevation: NoB Crop 2 Annual Ryegrass-Hay
Operator Crop 2 Pan 50
Volume Acres Dry Soil Application Total Nitrate-Crop 1 Crop 2
Date Measurement Applied %Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop
04/16/2021 Gallons 26,000 3.57 6.20 0.62 3.87 Dunn WWTP Dry <0.5" Surface 28.72 0.50 0.3 18,900 13,600.00 280.00 10.83 Crop 1
04/19/2021 Gallons 52,000 3.57 6.20 1.25 7.74 Dunn WWTP Dry <0.5" Surface 57.43 0.50 0.3 18,900 13,600.00 280.00 21.65 Crop 1
04/21/2021 Gallons 32,500 3.57 6.20 0.78 4.84 Dunn WWTP Dry <0.5" Surface 35.90 0.50 0.3 18,900 13,600.00 280.00 13.53 Crop 1
11/18/2021 Gallons 32,500 3.57 6.20 0.78 4.84 Dunn WWTP Moist <0.5" Surface 35.90 0.50 0.3 18,900 13,600.00 280.00 13.53 Crop 2
11/19/2021 Gallons 39,000 3.57 6.20 0.94 5.81 Dunn WWTP Moist <0.5" Surface 43.08 0.50 0.3 18,900 13,600.00 280.00 16.24 Crop 2
11/22/2021 Gallons 6,500 3.57 6.20 0.16 0.97 Dunn WWTP Moist <0.5" Surface 7.18 0.50 0.3 18,900 13,600.00 280.00 2.71 Crop 2
Total Volume Applied 188,500 Total Dry Tons 28.06 Sum Total P 208.20 Total 46.01 32.48 Total
Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2
PAN PAN
Current Year 0.013 0.012 2.055 0.360 0.003 0.056 0.147 0.013 4.915 (lbs./Ac.) (lbs./Ac.)
Lime(T/Ac.) Date
Prior Year 0.519 0.109 11.691 2.065 1.739 0.066 0.460 1.062 0.405 20.826
Cumulative Total 0.532 0.121 13.746 2.099 0.069 0.516 1.209 0.418 25.741 1.0 T/Ac 11/30/21
Permitted CPLR 36 34 1338 267 15 374 89 2498
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
d11/"I VI'
1/28/2022 *Application Method:S-Surface,IN-Injection,INC-Incorporation ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
'L.'
aerobically digested-0.3,raw sludge-0.4
**Volatilization Rate:Surface 0.5,Injection/Incorporation-1.0
****C.P.L.R.:Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0006101 Site# CU-34 County Harnett Crop 1 Common Bermudagrass Hay
Facility Name City of Dunn Field Name 5 SoilSeries Goldsboro Crop 1 Pan 230
LandOwner Harold Lee Eldridge Acres Permuted 9.70 Soil Abbrevation: GoA Crop 2 Annual Ryegrass-Hay
Operator Crop 2 Pan 50
Volume Acres Dry Soil Application Total Nitrate-Crop 1 Crop 2
Date Measurement Applied %Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop
04/14/2021 Gallons 26,000 3.57 9.70 0.40 3.87 Dunn WWTP Dry <0.5" Surface 18.36 0.50 0.3 18,900 13,600.00 280.00 6.92 Crop 1
04/15/2021 Gallons 97,500 3.57 9.70 1.50 14.51 Dunn WWTP Dry <0.5" Surface 68.83 0.50 0.3 18,900 13,600.00 280.00 25.95 Crop 1
04/16/2021 Gallons 26,000 3.57 9.70 0.40 3.87 Dunn WWTP Dry <0.5" Surface 18.36 0.50 0.3 18,900 13,600.00 280.00 6.92 Crop 1
11/11/2021 Gallons 26,000 3.57 9.70 0.40 3.87 Dunn WWTP Moist <0.5" Surface 18.36 0.50 0.3 18,900 13,600.00 280.00 6.92 Crop 2
11/12/2021 Gallons 6,500 3.57 9.70 0.10 0.97 Dunn WWTP Moist <0.5" Surface 4.59 0.50 0.3 18,900 13,600.00 280.00 1.73 Crop 2
11/16/2021 Gallons 32,500 3.57 9.70 0.50 4.84 Dunn WWTP Moist <0.5" Surface 22.94 0.50 0.3 18,900 13,600.00 280.00 8.65 Crop 2
11/17/2021 Gallons 45,500 3.57 9.70 0.70 6.77 Dunn WWTP Moist <0.5" Surface 32.12 0.50 0.3 18,900 13,600.00 280.00 12.11 Crop 2
Total Volume Applied 260,000 Total Dry Tons 38.71 Sum Total P 183.55 Total 39.79 29.41 Total
Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2
PAN PAN
Current Year 0.011 0.011 1.812 0.318 0.002 0.050 0.129 0.011 4.333 (lbs./Ac.) (lbs./Ac.)
Lime(T/Ac.) Date
Prior Year 0.472 0.106 12.025 1.907 1.745 0.066 0.443 1.007 0.395 21.234
Cumulative Total 0.483 0.117 13.837 2.063 0.068 0.493 1.136 0.406 25.567 1.0 T/Ac 11/30/21
Permitted CPLR 36 34 1338 267 15 374 89 2498
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
*Application Method:S Surface,IN Injection,INC Incorporation ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
y 1 •f **Volatilization Rate:Surface-0.5,Injection/Incorporation-1.0
c,AP � 1/28/2022 ****C.P.L.R.:Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0006101 Site# HA-08 County Harnett Crop 1 Common Bermudagrass Hay
Facility Name City of Dunn Field Name 8 SoilSeries Norfolk Crop 1 Pan 225
LandOwner R.Harold Dixon Acres Permuted 18.30 Soil Abbrevation: NoB Crop 2
Operator Crop 2 Pan
Volume Acres Dry Soil Application Total Nitrate-Crop 1 Crop 2
Date Measurement Applied %Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop
09/03/2021 Gallons 32,500 3.57 18.30 0.26 4.84 Dunn WWTP Dry <0.5" Surface 12.16 0.50 0.3 18,900 13,600.00 280.00 4.58 Crop 1
09/07/2021 Gallons 65,000 3.57 18.30 0.53 9.68 Dunn WWTP Dry <0.5" Surface 24.32 0.50 0.3 18,900 13,600.00 280.00 9.17 Crop 1
09/09/2021 Gallons 65,000 2.77 18.30 0.41 7.51 Dunn WTP Dry <0.5" Surface 0.87 0.50 0 37,200 361.00 361.00 0.44 Crop 1
09/13/2021 Gallons 58,500 2.77 18.30 0.37 6.76 Dunn WTP Dry <0.5" Surface 0.78 0.50 0 37,200 361.00 361.00 0.40 Crop 1
09/14/2021 Gallons 65,000 2.77 18.30 0.41 7.51 Dunn WTP Dry <0.5" Surface 0.87 0.50 0 37,200 361.00 361.00 0.44 Crop 1
09/15/2021 Gallons 71,500 2.77 18.30 0.45 8.26 Dunn WTP Dry <0.5" Surface 0.96 0.50 0 37,200 361.00 361.00 0.49 Crop 1
09/16/2021 Gallons 78,000 2.77 18.30 0.49 9.01 Dunn WTP Dry <0.5" Surface 1.04 0.50 0 37,200 361.00 361.00 0.53 Crop 1
09/17/2021 Gallons 52,000 2.77 18.30 0.33 6.01 Dunn WTP Dry <0.5" Surface 0.70 0.50 0 37,200 361.00 361.00 0.36 Crop 1
Total Volume Applied 487,500 Total Dry Tons 59.56 Sum Total P 41.70 Total 16.42 Total
Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2
PAN PAN
Current Year 0.021 0.004 0.481 0.072 0.001 0.022 0.054 0.011 1.082 (lbs./Ac.) (lbs./Ac.)
Lime(T/Ac.) Date
Prior Year 0.350 0.241 18.639 2.762 1.813 0.064 0.790 2.110 0.322 48.277
Cumulative Total 0.371 0.245 19.120 1.885 0.065 0.812 2.164 0.333 49.359 N/A
Permitted CPLR 36 34 1338 267 15 374 89 2498
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
*Application Method:S-Surface,IN-Injection,INC-Incorporation ***Minerali zation Rates:Compost-0.1,anaerobially digested-0.2,
-.t,
aerobically digested-0.3,raw sludge-0.4
jadrat **Volatilization Rate:Surface-0.5,Injection/Incorporation-1.0
3fAfif ****C.P.L.R.:Cumulative Pollutant Loading Rate
1/28/2022
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0006101 Site# HA-08 County Harnett Crop 1 Common Bermudagrass Hay
Facility Name City of Dunn Field Name 9 SoilSeries Norfolk Crop 1 Pan 225
LandOwner R.Harold Dixon Acres Permuted 19.70 Soil Abbrevation: NoB Crop 2
Operator Crop 2 Pan
Volume Acres Dry Soil Application Total Nitrate-Crop 1 Crop 2
Date Measurement Applied %Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop
09/01/2021 Gallons 97,500 3.57 19.70 0.74 14.51 Dunn WWTP Dry <0.5" Surface 33.89 0.50 0.3 18,900 13,600.00 280.00 12.78 Crop 1
09/02/2021 Gallons 117,000 3.57 19.70 0.88 17.42 Dunn WWTP Dry <0.5" Surface 40.67 0.50 0.3 18,900 13,600.00 280.00 15.33 Crop 1
09/03/2021 Gallons 52,000 3.57 19.70 0.39 7.74 Dunn WWTP Dry <0.5" Surface 18.08 0.50 0.3 18,900 13,600.00 280.00 6.81 Crop 1
Total Volume Applied 266,500 Total Dry Tons 39.67 Sum Total P 92.64 Total 34.92 Total
Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2
PAN PAN
Current Year 0.006 0.005 0.914 0.160 0.001 0.025 0.065 0.006 2.187 (lbs./Ac.) (lbs./Ac.)
Lime(T/Ac.) Date
Prior Year 0.297 0.168 14.637 2.115 1.583 0.051 0.608 1.664 0.268 35.880
Cumulative Total 0.303 0.173 15.551 1.743 0.052 0.633 1.729 0.274 38.067 N/A
Permitted CPLR 36 34 1338 267 15 374 89 2498
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
rs *Application Method:S-Surface,IN-Injection,INC-Incorporation ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
$q aerobically digested-0.3,raw sludge-0.4
dgat !t **Volatilization Rate:Surface-0.5,Injection/Incorporation-1.0
f i , ****C.P.L.R.:Cumulative Pollutant Loading Rate
1/28/2022
Signature of Land Applier Date

City of Dunn
2021 Class B Annual Report
WQ Permit# WQ0006101
Pathogen & Vector Attraction Reduction Form
Dunn WWTP
Fecal Coliform Data
38% Volatile Solids Reduction

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Dunn WQ Permit Number: WQ0006101
WWTP Name: Dunn WWTP NPDES Number: NC0043176
Monitoring Period: 01/01/2021 to 12/31/2021
Pathogen Reduction(15A NCAC 02T .1106) -Please Indicate level achieved and alternative performed:
"Class A"Alternative: Not Applicable
If applicable to alternative performed("Class A" only)indicate"Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 1
If applicable to alternative performed("Class B"only)indicate"Process to Further Reduce Pathogens": Not Applicable
Fecal Conform Minimum Geo.Mean Maximum II of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 13,928 23,827 30,641 0 Annually Grab Samples
Weight)
Analytical Technique SiM 9222 D •
Vector Attraction Reduction Performed(15A NCAC 02T.1107): Alt. 1 (VS reduction)
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
INfi requirement in 15A NCAC 02T .1107 have been met."
"I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Donrie Dukes,WWTP Superintendent Jason Smith,VP
Preparer Name and Title(type or print) Land Applier Name and Title(if applicable)(type or print)
t 2/14/22
Signature of Prepares* Date Signature of Land Applier(if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102(26)

Meritech, Inc.
Environmental Laboratory
Y Laboratory Certification No. 165
iii.‘
—.‘ft.
Oir—
115,
Page 1
Contact: Drew Matthews Report Date: 4/22/2021
Client: Soil Plus
P.O. Box 1396 Project: Dunn WWTP
Oxford, NC 27565 Date Sample Rcvd: 4/13/2021
Meritech Work Order# 041321153 Sample: Dunn (001) Grab 4/13/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 3.59 % 4/14/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 30,641 col/g dry wt 4/13/21 130 col/g dry wt SM 9222D
Meritech Work Order# 041321154 Sample: Dunn (002) Grab 4/13/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 3.59 % 4/14/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 30,641 col/g dry wt 4/13/21 130 col/g dry wt SM 9222D
Meritech Work Order# 041321155 Sample: Dunn (003) Grab 4/13/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 3.58 % 4/14/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 25,140 col/g dry wt 4/13/21 130 col/g dry wt SM 9222D
Meritech Work Order# 041321156 Sample: Dunn (004) Grab 4/13/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 3.55 % 4/14/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 28,169 col/g dry wt 4/13/21 130 col/g dry wt SM 9222D
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
.8,4-
11111F:74#
Page 2
Contact: Drew Matthews Report Date: 4/22/2021
Client: Soil Plus
P.O. Box 1396 Project: Dunn WWTP
Oxford, NC 27565 Date Sample Rcvd: 4/13/2021
Meritech Work Order# 041321157 Sample: Dunn (005) Grab 4/13/21
Parameters Results Analysis Date Reporting Limit Method
0/0 Total Solids 3.59 % 4/14/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 13,928 col/g dry wt 4/13/21 130 col/g dry wt SM 9222D
Meritech Work Order# 041321158 Sample: Dunn (006) Grab 4/13/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 3.57 % 4/14/21 0-100 % SM 2540B
Fecal Coliform (Sludge) 28,011 col/g dry wt 4/13/21 130 col/g dry wt SM 9222D
Meritech Work Order# 041321159 Sample: Dunn (007) Grab 4/13/21
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 3.57 % 4/14/21 0-100 % SM 25408
Fecal Coliform (Sludge) 16,807 col/g dry wt 4/13/21 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. Arno(nact :tine
Laboratory Representative
642 Tamco Road,Reidsville,North Carolina 27320
tel.[phone] fax.[phone]

3-20.7013 Chain of Custody Record (COC) NPDES#:
Client: Soil Plus Phone: [phone]
MERITECH, INC. Address: PO Box 1396 - Fax: [phone]
ENVIRONMENTAL LABORATORIES Oxford, NC 27565 Email: [e-mail]
A
,1$7:40 642 Tamco Rd. Phone: [phone] Project: Dunn 11VIIVfP
Reidsville NC 27320 Fax:[phone] P.O.#:
Email: [e-mail] Attention: Turn Around Time*
/��\/�Y How would you like your report sent? - *RUSH work needs prior approval.
W V V Y .rn e ri t e e h-labs.c�rp Circle all that apply: Email(preferred), Fax, Mall Std(10 days) 3-5 Da s 74-4R Hrs
Sampling Dates & Times Person Taking Sample(Sign/Print): Matthews r,?-e,v iv u' '1- Lab Use Only
Sample Location and/or ID# Start End Comp? #of Test(s) Required On Ice? pH OK?
Cont.Date Time Date Time Grab? C es / No Cl OK?
R Dunn (001) 4/13/21 '.IS Pr G 1 Fecal Coliform/%Total Solids IS' 3
Dunn (002) 4/13/21 "l:11 Ar^ G 1 Fecal Coliform/%Total Solids 1 S
Dunn (003) 4/13/21 a 7P A,K G 1 Fecal Coliform /% Total Solids rC c
Dunn (004) 4/13/21 9: yyAr• G ` 1 Fecal Coliform/%Total Solids `S'-`
•
Dunn (005) '4/13/21 1:&SJ ' G 1 'Fecal Coliform/% Total Solids �,C-1
Dunn (006) 4/13/21 1:G+3AE`' G 1 Fecal Coliform J%Total Solids \ c Cl,
-
Dunn (007) 4/13/21 1:3DAh. G 1 Fecal Coliform /% Total Solids r CC)
Temperature Upon
Method of ***Dechlorination(<0.5 ppm)of Ammonia,Cyanide,Phenol and TKN samples must be done in the field prior to preservation. ***
r-?` Receipt:
Comments: Compositor#
Shipment: Please email results to [e-mail]
_L UPS Jug#
Q Fed Ex s Are these results for regulatory purposes? Yes �X No U ::_.,_,/ort results in: mg/L [. mg/kg Qs` ug/L Q'
- Relinquished by: _pep ,N/)r J2 Date: till�12iTlme: 1: P�,,, Receiyep `� ate: ,� Time:
Hand Delivery �/} i' i______7r� 3�'�
Relin ulshec L>i Dat /`� Time: Ifr<ived b : Date: Time:
�� Other q [�"�� �= �,�/`Z`� ��, � y
Relinquished by: Date: Time: Receit bylakl ( ate: Time: R(

Black River Wastewater Treatment Plant
City of Dunn
2021
April 2021 Vector Attraction
Rec.—.77
Holding Tank—.66
.77 - .66 = 42.3%
.77 - (.81x.66)
Sept. 2021 Vector Attraction
Rec.--- .72
Holding Tank----.61
.72 - .61 = 39.1%
.72—(.72x.61)

City of Dunn
2021 Class B Annual Report
WQ Permit# WQ0006101
Soil Samples

WPage1 of 1
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•
Report No: 21-285-0536 2850 Daisy Lane,Wilson, NC 27896
Account No: 04596 aypol11 L .
Main 252 206y Fax 252 NC -9973
27896
ANALYTICAL www.waypointanalytical.com
Advisor: Soil Plus, LLC Client:Granville Farms Inc Farm:CU-34
Joyce Barrette
P.O. Box 1396
Oxford NC 27565 Date Received:10/12/2021
Date of Report: 10/14/2021
Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-I K-I S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I CEC BS% Ca% Mg% ESP Na
04100 1 MIN 2.5 5.9 2.2 220 21 58 50 48 0 303 303 220 8.4 74 50 22 0.8 0.1
Crop Recommendations: Rec Uom Lime(t/acre) N P2O5 K2O S Mn Zn Cu B Mg Last Crop
1-Bermudagrass Hay lb/acre 0.5 200 0 186 0 0 0 0 0
04101 2 MIN 1.3 5.6 2.0 337 35 50 75 68 0 330 330 210 6.9 71 44 24 0.6 0
Crop Recommendations: Rec Uom Lime(t/acre) N P2O5 K2O S Mn Zn Cu B Mg Last Crop
1-Bermudagrass Hay lb/acre 0.8 200 0 149 0 0 0 0 0
04102 3 MIN 2.4 5.6 2.2 259 58 69 56 57 0 290 290 220 6.8 67 44 18 0.8 0.1
Crop Recommendations: Rec Uom Lime(t/acre) N P2O5 K2O S Mn Zn Cu B Mg Last Crop
1-Bermudagrass Hay lb/acre 0.9 200 0 30 0 0 0 0 0
04103 4 MIN 1.5 5.5 2.8 307 41 56 63 62 0 238 238 250 5.7 52 34 13 0.8 0
Crop Recommendations: Rec Uom Lime(t/acre) N P2O5 K2O S Mn Zn Cu B Mg Last Crop
1-Bermudagrass Hay lb/acre 1.3 200 0 134 0 0 0 0 0
04104 5 MIN 1.1 5.6 2.0 213 29 50 81 72 0 330 330 150 5.4 64 41 19 0.9 0
Crop Recommendations: Rec Uom Lime(t/acre) N P205 K20 S Mn Zn Cu B Mg Last Crop
1 Bermudagrass Hay lb/acre 0.8 200 0 164 0 0 0 0 0
Comment:
Test result units=CEC and Na in meq/100cm3;NO3 N in mg/dm3;WA/in g/cm3
North Carolina Division of Water Quality Certification#257,Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines,Analysis prepared by:Waypoint Analytical Carolina,Inc.

WPage1 of 1
r o
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Report No: 21 285 0535 2850 Daisy Lane,Wilson, NC 27896
Account No: 04596 aypol11 L .
Main 252 206y Fax 252 NC -9973
27896
ANALYTICAL www.waypointanalytical.com
Advisor: Soil Plus, LLC Client:Granville Farms Inc Farm:HA-08
Joyce Barrette
P.O. Box 1396
Oxford NC 27565 Date Received:10/12/2021
Date of Report: 10/14/2021
Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-I K-I S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I CEC BS% Ca% Mg% ESP Na
04098 8 MIN 1.1 5.9 1.5 569 11 64 113 86 0 398 398 225 7.5 80 71 7 0.7 0.1
Crop Recommendations: Rec Uom Lime(t/acre) N P2O5 K2O S Mn Zn Cu B Mg Last Crop
1-Bermudagrass Hay lb/acre 0.5 200 0 215 0 0 0 0 0
04099 9 MIN 1.2 5.9 1.9 432 23 60 119 90 0 340 340 255 7.3 73 62 8 0.8 0.1
Crop Recommendations: Rec Uom Lime(t/acre) N P205 K20 S Mn Zn Cu B Mg Last Crop
1 Bermudagrass Hay lb/acre 0.5 200 0 181 0 0 0 0 0
Comment:
Test result units=CEC and Na in meq/100cm3;NO3 N in mg/dm3;WA/in g/cm3
North Carolina Division of Water Quality Certification#257,Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines,Analysis prepared by:Waypoint Analytical Carolina,Inc.