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HomeMy WebLinkAboutWQ0010615_Residual Annual Report 2021_20220215Non -Discharge Branch Upload/Submittal Form NORTH CAROLINA EnvironmentalQuul1ty Version 2 - Revised June 23, 2020 Initial Review Reviewer Thornburg, Nathaniel D Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Year* Permit Number (IR) * Applicant/Permittee Email Notifications Does this need review by the hydrogeologist? * Regional Office CO Reviewer Admin Reviewer Annual Report Residual Annual Report Additional Information Other 2021 WQ0010615 Town of Maggie Valley 0Yes ®No Asheville Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Michael Mehaffey Email Address* mmehaffey@maggievalleync.gov Project Information Application/Document Type * New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 828-926-0866 O Modification - Minor O Renewal O GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type: * Permit Number:* Applicant/Permittee Address * Facility Name* Wastewater Irrigation Other Wastewater Closed -Loop Recycle Single -Family Residence Wastewater Irrigation WQ0010615 Has Current Existing permit number 3987 Soco rd. Maggie Valley, NC 28751 Town of Maggie Valley Class A Residuals Program Please provide comments/notes on your current submittal below. High -Rate Infiltration Reclaimed Water Residuals Other At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. * (Application Form, Engineering Plans, Specifications, Calculations, Etc.) 2021 SEWAGE SLUDGE ANNUAL REPORT.pdf 1.08MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/15/2022 iPr own of Maggie Valley 1974 zcija Phone 828-926-0866 3987 Soco Road Maggie Valley,NC 28751 VA if CO Facility Name Town of Maggie Valley Wastewater Treatment Plant NPDES Permit# NC0056561 NC Water Quality# WQ0010615 Responsible Official Nathan Clark nclark@maggievalleync.gov Town Manager Town of Maggie Valley 3987 Soco Road Maggie Valley,NC 28751 828-926-0866 ext. 103 Operator Michael Mehaffey 94 Indian Springs Road Clyde,NC 28721 828-926-0866 ext. 102 Engineer McGill Associates, P.A. Post Office Box 2259 Asheville,NC 28802 828-252-0575 Dry Tons Processed in 2021 164 Dry Tons Dewatered Tons Landfilled in 2021 118 Tons Dry Tons Stockpiled in 2021 0 Dry Tons Plant Location 5320 Jonathan Creek Road Waynesville,NC 28785 ANNUAL DISTRIBUTION AND MARKET PERMIT #: 4,/J f o /o( /S` FACILITY NAME: PHONE: $deg u61(9,4 COUNTY: GI SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM OPERATOR: FACILITY TYPE (please check one): Surface Disposal (complete Part A (Source(s) and "Residual In" olume only) and Part C) Distributiopand Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? IYes ❑No No If No skip parts A B. C and certify form below Part A*: Part B*: Month Sources NPDES # if Volume (dry tons) Recipient Information s include () (. applicable) Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January 6 00 g'6/ February March 13'7-4/ /s'7. / .3o TN , 74 Re h iy 30 7 i/ 41 `M r Aptit, /Huy April IA 741 - /A 7i,/ ,'' TA/ Apt 614,4d4a/ gL 7✓v May June is-7-A/ /rr,i/ 30 TA/ /44 il',84 .(fey 30 rAl 44,,.,/, 9, - Asf're July /d 7r, ID TA/ 20 7 �o hrf dy �O T> August September October November / Asf� oky December 3O7 / 30 7 V 10 71 I'k/ y /ikyd G4 7` / Totals: Annual d tons): 9/ 7-41 �,2 7'A/ A �% .,. :` ' v " .: ? r. ; Amendment(s) used: I i /h 1.; rn� ,� S 7A/ Bulking Agent(s) used more space than given is required, please attach additional information sheet(s). ❑ Check box if additional sheet(s) are attached Part C: Facility was compliant during calendar year .), j with all conditions of the permit (including but not limited to items 1-3 below) issued by the Division of Water Resources. ISA Yes 0 No If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there aar *gnif t lties for submitting false information, including t e possibility of fines nd imprisonment for knowing violations." Date Signature of Preparer* * Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) DENR FORM DMSDF (11/2005) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: ' 00 /106 S- Facility Name: 1�a` e Uu //e �,✓� f'7'' NPDES # or WQ#: Ale M5'lW WWTP Name: /��; e au /l y Residual Laboratory: 1) leg 2) t7� 3) ,%a r ‘ 01- i�G e 4) f/MO. /a/ eAeptals 5) ,' `' { :'' Parameters (mg/kg) I Sample or Composite Date , i--/g-2l y-q- _d /-/eNt rj.-77-i( /p 48 .4 Percent Solids rj.3 xi q'y 10 6 !o S 7 fey t 7 f Arsenic q, 8 i Cadmium L /.,- Chromium 0, 4f Copper S1, / Lead 6,, i1 Mercury /2, , Molybdenum z 3. 76 Nickel /.1, 3 Selenium 43, 7h Zinc 19,3 Total Phosphorus a H6O TKN 3100 Ammonia -Nitrogen /00 Nitrate and Nitrite 40,0 ••t certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." -7ed:42-6) Signature of Preparer -$-; 2— Date Please note that your Permit Number: Facility Name: NPDES # or WQ#: ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report permit may contain additional parameters to be analyzed than those required to be summarized on: this form. Laboratory: 1) jg 5 1GriQi%/06/,r WWTP Name: u/.✓ o e `!e Residual Analysis Data 2 B Sample or Composite Date �lurri% n u vvt (_'u/C/un-, y-49..zr 9-2i 1-.21-,)1 eU o /I'Iag,�/2Si uvrt 41'(%ai y "biu ,usM csod; urn /2+0 /2, 0 12,3 3$1,000 3gJv MAW SV0 "I certify, under penalty of law, that this document was pre,.... , ,...,..,�� .,.y u„ ac�,on ur supervision 1n accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer 2) /7.S 3) /6yer,S Ca lkotr 4) ill 1.4.,e1 i3? s1iG[ ! e "ts 5 ID 48 )t 12•O Date 4 Earth Environmental Services Murplry, NC Name and Address of Facility Town of Maggie Valley 3987 Soco Road Maggie Valley, NC 28751 Att: Mike Mehaffey Report Date Date and Time Received Date and Time Sampled Earth Environmental 75 Bison Lane Murphy, NC 28906 828-837-9543 (office) 828-644-4835 (lab) Lab ID# 352 9/23/2021 7/27/2021 10:05 AM 7/27/2021 10:05 AM Sampler JOHN CURTIS BROWN CLASS A Date Test BIOSOLIDS Sample Time Report Limit Units Method Analyzed Analyst NO2+NO3- N < 60.0 10:05 AM 60.0 mg/kg 9056A 8/10/21 NAR TOTAL KJELDAHL NITROGEN 8100 10:05 AM 174 mg/kg 351.2 8/3/21 LKH TOTAL PHOSPHOROUS 2460 10:05 AM 376 mg/kg 6010D 8/13/21 MLR % TOTAL SOLIDS (DRY WT) 56.7 10:05 AM 0.100 % SM 2540 G 8/10/21 PSF NO3-N < 50.0 10:05 AM 50.0 mg/kg 9056A 8/10/21 NAR SAR 0.705377 10:05 AM N/A N/A calc 9/23/21 MB PAN - SURFACE 16250 10:05 AM N/A mg/kg calc 9/23/21 MB PAN SUBSURFACE 16300 10:05 AM N/A mg/kg calc 9/23/21 MB CALCIUM 350000 10:05 AM 37600 mg/kg 6010D 8/20/21 MLR ALUMINUM 8860 10:05 AM 188 mg/kg 6010D 8/13/21 MLR CADMIUM < 1.50 10:05 AM 1.50 mg/kg 6010D 8/13/21 MLR CHROMIUM 12.4 10:05 AM 3.76 mg/kg 6010D 8/13/21 MLR COPPER 51.1 10:05 AM 1.50 mg/kg 6010D 8/13/21 MLR LEAD 6.69 10:05 AM 3.76 mg/kg 6010D 8/13/21 MLR NICKEL 12.3 10:05 AM 1.50 mg/kg 6010D 8/13/21 MLR ZINC 99.3 10:05 AM 3.76 mg/kg 6010D 8/13/21 MLR SODIUM 1530 10:05 AM 37.6 mg/kg 6010D 8/13/21 MLR POTASSIUM 5410 10:05 AM 376.0 mg/kg 6010D 8/13/21 MLR MAGNESIUM 3450 10:05 AM 188.0 mg/kg 6010D 8/13/21 MLR ARSENIC 9.84 10:05 AM 2.52 mg/kg 6010D 8/13/21 MLR SELENIUM < 3.76 10:05 AM 3.76 mg/kg 6010D 8/13/21 MLR MOLYBDENUM < 3.76 10:05 AM 3.17 mg/kg 6010D 8/13/21 MLR MERCURY 0.045 10:05 AM 0.033 mg/kg 7471B 8/9/21 NAR Lab Supervisor: Wanda G. Ladd; EES - Murphy Certified By: /..‘,/~C, PAN Maggie Valley Class A Biosolids 7/27/21 Mineralization as decimal Total dry Acres Rate 'MN 81100 100 NO3 0 NO2 % Solids tons/year Applied on 0.2 0 56.7 PAN Surface 16250 Img/kg 32.5 Ibs/dry ton 0 Ibs total PAN #DIV/0! Ibs PAN/acre PAN Injection 16300 mg/kr Dry Tons/1000 gal. 32.6 Ibs/dry ton 0 Ibs total PAN #DIV/0! Ibs PAN/acre 1st year PAN Surface Ibs. 1st year PAN Injected Ibs. Ibs./acre Surface #DIV/0! Ibs./acre Injected MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 mg/kg x .002 MR(TKN-NH3) + 1(NH3)+NO3+NO2 mg/kg x .002 =mg/kg =Ibs/dry ton =mg/kg =Ibs/dry ton 1000 X 8.34 X %solids X sp, ons/1000gal." 2000 SAR & ESP Maggie Valley Class A Biosolids 7/27/21 Sodium Absorption Ratio Na : Sodium (Mg/L) Equivalent weight: 23 Ca : Calcium (Mg/L) Equivalent weight: 20 Mg : Magnesium (Mg/L) Equivalent weight: 12 Na M L WO Ca(MWkg) Mg M /k 1530 350000 3450 Na (ME) Ca (ME) Mg (ME) 66.52174 17500 287.5 Milli Equivalent = Mg/L / Equivalent weight SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power SAR = 0.705377 (From Mg/Kg entered above) SAR= 0.705377 Na (ME) Ca (ME) Mg (ME) 66.52174 17500 287.5 (From ME entered below) The amount of exchangeable sodium ions versus the amount of exchangeable calcium & magnesium ions in a given material. Permitting guidance is if greater than 10 require ESP in permit. Exchangeable Sodium Percentage ESP = Na (Milli Equivalents) / CEC X 100 ESP = 11.74564 Na on NC soil test is expressed as meq. The percentage of sodium ions occupying the cation exchange complex of soils Na (ME) 1.56217 CEC 13.3 Should be Tess than 15% (15-20%) Earth. { Environment 4 4 Services Murphy, NC Name and Address of Facility Town of Maggie Valley 3987 Soco Road Maggie Valley, NC 28751 Att: Mike Mehaffey Report Date Date and Time Received Date and Time Sampled Earth Environmental 75 Bison Lane Murphy, NC 28906 828-837-9543 (office) 828-644-4835 (lab) Lab ID# 352 9/23/2021 7/19/2021 9:02 AM 7/19/2021 9:02 AM Sampler JOHN CURTIS BROWN CLASS A Date Test BIOSOLIDS Sample Time Report Limit Units Method Analyzed Analyst pH IN SOIL 12.3 9:02 AM 0-14 S.U. 9045 D 7/19/21 MS CORROSIVITY NOT CORROSIVE 9:02 AM SCA IGNITABILITY <0.8 9:02AM 0.8 mm/sec 1030 7/26/21 ECHM PAINT FILTER TEST < 0.1 9:02 AM 0.1 ml SW846 9095 B 7/23/21 KEK TOTAL REACTIVE CYANIDE < 1 9:02 AM 1 mg/kg 335.4 8/2/21 ECHEM REACTIVE SULFIDE 1.33 9:02 AM mg/kg SM4500 S D 8/2/21 ECHEM AMMONIA NITROGEN 100 9:02 AM 5.6 mg/kg 9045 D 7/22/21 KEK % TOTAL SOLIDS (DRY WT) 71 9:02 AM 0.10 % SM 2540 G 7/19/21 KEK * PLEASE NOTE: Fed -Ex lost cooler with samp es to be arldlyzed for TCLP Metals and Nitrogen and Phosphorous. 2nd Sample date tested on 7/27/21. -/ Lab Supervisor: Wanda G. Ladd; EES - Murphy Certified By:4}1,411.4L,.Wtiot./ Earth Environmental Services Murphy, NC Name and Address of Facility Town of Maggie Valley 3987 Soco Road Maggie Valley, NC 28751 Att: Mike Mehaffey Report Date Date and Time Received Date and Time Sampled Earth Environmental 75 Bison Lane Murphy, NC 28906 828-837-9543 (office) 828-644-4835 (lab) Lab ID# 352 8/20/2021 7/27/2021 10:05 AM 7/27/2021 10:05 AM Sampler JOHN CURTIS BROWN CLASS A Date Test BIOSOLIDS Sample Time Report Limit Units Method Analyzed Analyst EPA - 8260 D < 0.200 10:05 AM 0.200 mg/I SCA 8/9/21 LDM EPA 8270 E 0.206* 10:05 AM 0.100 mg/I SCA 8/10/21 RJM EPA 8081 B < 0.0050 10:05 AM 0.0050 mg/I SCA 8/17/21 RKH CADMIUM < 0.05 10:05 AM 0.05 mg/I 6010 D 8/9/21 MLR CHROMIUM < 0.10 10:05 AM 0.10 mg/I 6010 D 8/9/21 MLR LEAD < 0.25 10:05 AM 0.25 mg/I 6010 D 8/9/21 MLR SILVER < 0.10 10:05 AM 0.10 mg/I 6010 D 8/9/21 MLR BARIUM < 2.50 10:05 AM 2.50 mg/I 6010 D 8/9/21 MLR ARSENIC < 0.25 10:05 AM 0.25 mg/I 6010 D 8/9/21 MLR SELENIUM < 0.25 10:05 AM 0.25 mg/I 6010 D 8/9/21 MLR MERCURY < 0.0020 10:05 AM 0.0020 mg/I 7470 A 8/9/21 NAR * SEE ATTACHED PAGES FOR ORGANICS Lab Supervisor: Wanda G. Ladd; EES - Murphy Certified By: Zi.) Environmental Testing Solutions, Inc. Certificate of Analysis Project name: Earth Environmental Services Collection date: 27-Ju1-21 Date received: 27-Jul-21 PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 210727.500 Sample identification: #072121 MVS Sample number: 214555 Parameter Method Result RL Units Date Analyst Footnotes Analyzed Arsenic - TCLP 6010 D <0.25 0.25 mg/L 9-Aug-21 MLR 1 Barium - TCLP 6010 D <2.50 2.50 mg/L 9-Aug-2I MLR 1 Cadmium -TCLP 6010 D <0.05 0.05 mg/L 9-Aug-21 MLR 1 Chromium - TCLP 6010 D <0.10 0.10 mg/L 9-Aug-21 MLR 1 Lead - TCLP 6010 D <0.25 0.25 mg/L 9-Aug-21 MLR 1 Selenium - TCLP 6010 D <0.25 0.25 mg/L 9-Aug-2I MLR 1 Silver - TCLP 6010 D <0.10 0.10 mg/L 9-Aug-21 MLR 1 Mercury - TCLP 7470 A <0.0020 0.0020 mg/L 9-Aug-21 NAR 1 Full Scan TCLP Organics See attached sheets 1 Total Solids Dry Weight 56.7 0.100 % 10-Aug-21 PSF 1 Mercury 7471B 0.045 0.033 mg/kg 9-Ang-21 NAR 1 Aluminum 6010 D 8860 188 mg/kg 13-Aug-21 MLR 1 Arsenic 6010 D 9.84 3.76 mg/kg I3-Aug-21 MLR 1 Cadmium 6010 D <1.50 1.50 mg/kg 13-Aug-21 MLR 1 Calcium 6010 D 350000 37600 mg/kg 20-Aug-21 MLR 1 Chromium 6010 D 12.4 3.76 mg/kg 13-Aug-21 MLR 1 Copper 6010 D 51.1 1.50 mg/kg I3-Aug-21 MLR 1 Lead 6010 D 6.69 3.76 mg/kg I3-Aug-21 MLR 1 Magnesium 6010 D 3450 188 mg/kg 13-Aug-21 MLR 1 Nickel 6010 D 12.3 1.50 mg/kg 13-Aug-21 MLR 1 Potassium 6010 D 5410 376.0 mg/kg I3-Aug-21 MLR 1 Selenium 6010 D <3.76 3.76 mg/kg I3-Aug-21 MLR 1 Sodium 6010 D 1530 37.6 mg/kg 13-Aug-21 MLR 1 Zinc 6010 D 99.3 3.76 mg/kg 13-Aug-21 MLR 1 Nitrate + Nitrite 9056 A <60.0 60.0 mg/kg 10-Aug-21 NAR 1 Total Phosphorus 6010 D 2460 376 mg/kg 13-Aug-21 MLR 1 Total Kjeldahl Nitrogen 351.2 8100 174 mg/kg 3-Aug-21 LKH 1 Total Nitrogen Calculation 8100 17.6 mg/kg 10-Aug-2I LKH 1 Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. 1. Sample analzyed by Rogers and Callcott Environmental. Date reviewed: Data reviewed by: Signature: c3,aq.jJ Kelley E. Keenan NC Certification Number: 600 SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted for analysis. Environmental Testing Solutions, Inc. Certificate of Analysis Project name: Earth Environmental Services Collection date: 19-Ju1-21 Date received: 19-Jul-21 Sample identification: #072113 MVS PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 210719.500 Sample number: 214342 Parameter Method Result RL Units Date Analyst Footnotes Analyzed Reactive Cyanide 335.4 <1 1 mg/kg 2-Aug-21 ECHEM 2 Reactive Sulfide SM 4500 S D 1.33 mg/kg 2-Aug-21 ECHEM 2 Ignitability 1030 <0.8 0.8 mm/sec 26-JuI-21 ECHEM 2 pH in Soil 9045 D 12.3 0.1 S.U. 19-Jul-21 MS 3 Paint Filter SW846 9095 B <0.1 0.1 ml 23-Jul-21 KEK Arsenic - TCLP 6010 D 0.25 mg/L 1 Barium - TCLP 6010 D 2.50 mg/L 1 Cadmium -TCLP 6010 D 0.05 mg/L 1 Chromium - TCLP 6010 D 0.10 mg/L 1 Lead - TCLP 6010 D 0.25 mg/L 1 Selenium - TCLP 6010 D 0.25 mg/L 1 Silver - TCLP 6010 D 0.10 mg/L 1 Mercury - TCLP 6010 D 0.0020 mg/L 1 Full Scan TCLP Organics See attached sheets 1, 2 Total Solids SM 2540 G 0.10 % 1 Mercury 7471B 0.047 mg/kg 1 Aluminum 6010C 252 mg/kg 1 Arsenic 6010C 2.52 mg/kg l Cadmium 6010C 1.01 mg/kg I Calcium 6010C 10100 mg/kg 1 Chromium 6010C 2.52 mg/kg 1 Copper 6010C 1.01 mg/kg 1 Lead 6010C 2.52 mg/kg 1 Magnesium 6010C 252 mg/kg 1 Nickel 6010C 1.01 mg/kg 1 Potassium 6010C 25.2 mg/kg 1 Selenium 6010C 2.52 mg/kg 1 Sodium 6010C 50.3 mg/kg 1 Zinc 6010C 2.52 mg/kg 1 Nitrate + Nitrite 9056 A 30.00 mg/kg 1 Total Phosphorus 6010C 126 mg/kg 1 Total Kjeldahl Nitrogen 351.2 197 mg/kg 1 Total Nitrogen Calculation 12.0 mg/kg 1 Ammonia Nitrogen SM 4500 NH3 D 100 5.6 mg/kg 22-Jul-21 KEK Percent Solids SM 2540 G 71 0.10 % 19-Jul-21 KEK This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted for analysis. Environmental Testing Solutions, Inc. Certificate of Analysis PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. 1. Fedex shipping error. Sample was recevied out of temperature. Client is recollecting. 2. Sample analzyed by Enviro Chemists, Inc. 3. Sample received and analzyed outside hold time. Date reviewed: Data reviewed by: Signature: ()4.Olo.zl Kelley E. Keenan ! NC Certification Number: 600 SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted for analysis. ANALYTICAL & CONSULTING CHEMISTS Environmental Testing Solutions, Inc. Post Office Box 7565 Asheville NC 28802 Attention: Kelley Keenan (ETS) Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infcka environmentalchemists.com Date of Report: Aug 03, 2021 Customer PO #: Customer ID: 08100055 Report #: 2021-12232 Project ID: EES Lab ID 21-30460 Test Sample ID: Site: 072113MVS Method Collect Date/Time Matrix Sampled by 7/19/2021 9:02 AM Solid/Sludge Client Results Date Analyzed 2,4,5-TP (TCLP) 2,4-D (TCLP) RCI Ignitability Cyanide Sulfide Analyzed outside of hold time. SW846 Method 8151A SW646 Method 8151A EPA 1030 SM 4500 CN D SM 4500 S D <0.003 mg/L <0.005 mg/L <0.8 mm/sec <1 mg/kg 1.33 mg/kg 07/29/2021 07/29/2021 07/26/2021 08/02/2021 08/02/2021 Comment: Reviewed by: ' C Report#. 2021-12232 Page 1 of 1 08/24/2021 08:04 Rogers &Callcott �+ ENVIRONMENTAL Environmental Testing Solutions Project: Earth Environmental Services 351 Depot St. Work Order: 1071568 Asheville, NC 28801-4310 Reported: 08/24/21 08:04 Sample Data Sample Number 1071568-01 Sample Description Earth Environmental Services #072121MVS collected on 07/27/21 10:05 Parameter Reporting Result Limit Units DF Analyzed Method Flag Analyst Batch General Chemistry Parameters Nitrate as N ND 50.0 mg/kg dry 10.0 08/10/21 18:11 EPA 9056A X NAR B1H0668 NitriteasN ND 10.0 mg/kgdry 10.0 08/10/21 18:11 EPA9056A X NAR B1H0668 Total KjeldahlNitrogen 8100 174 mg/kgdry 5.00 08/03/21 13:44 EPA351.2 Z LKH B1H0058 Total Nitrogen (TKNtNitrate+Nitrite) 8100 17.6 mg/kg dry 1.00 08/10/21 18:11 - NAR B 1H0666 Total Solids 56.7 0.100 % 1.00 08/10/21 08:26 Dry Weight PSF B1H0457 Total Metals Mercury 0.045 0.033 mg/kgdiy 1.00 08/09/21 15:32 EPA7471B NAR B1H0331 Aluminum 8860 188 mg/kgdry 50.0 08/13/21 18:48 EPA6010D MLR B1H0190 Arsenic 9.84 3.76 mg/kgdsy 1.00 08/13/21 18:56 EPA6010D MLR B1H0190 Cadmium ND 1.50 mg/kg dry 1.00 08/13/21 18:56 EPA 6010D MLR B1H0190 Calcium 350000 37600 mg/kg dry 5,000 08/20/21 02:56 EPA 6010D MLR B1H0190 Chromium 12.4 3.76 mgkgdiy 1.00 08/13/21 18:56 EPA6010D MLR B1H0190 Copper 51.1 1.50 mg/kg drY 1.00 08/13/21 18:56 EPA6010D MLR B1H0190 Lead 6.69 3.76 mg/kg dry 1.00 08/13/21 18:56 EPA 6010D MLR B1H0190 Magnesium 3450 188 mg/kg diy 50.0 08/13/21 18:48 EPA 6010D MLR B1H0190 Molybdenum ND 3.76 mg/kgdlY 1.00 08/13/21 18:56 EPA6010D MLR B1H0190 Nickel 12.3 1.50 mg/kgdrY 1.00 08/13/21 18:56 EPA6010D MLR B1H0190 Potassium 5410 376 mg/kgdry 5.00 08/13/21 18:52 EPA6010D MLR B1H0190 Selenium ND 3.76 mg/kg dry I A0 08/13/21 18:56 EPA 60I0D MLR B1H0190 Sodium 1530 37.6 mg/kgdry 5.00 08/13/21 18:52 EPA6010D MLR B1H0190 Total Phosphorus as P 2460 376 mg/kg drY 50.0 08/13/21 18:48 EPA 6010D MLR B1H0190 Zinc 99.3 3.76 mg/kg dry 1.00 08/13/21 18:56 EPA 6010D MLR B1H0190 TCLP Metals Mercury ND 0.0020 mg/L 10.0 08/09/21 12:59 EPA7470A NAR B1H0390 Arsenic ND 0.25 mg/L 5.00 08/09/21 19:10 EPA6010D MLR B1H0157 Barium ND 2.50 mg/L 5.00 08/09/21 19:10 EPA 6010D MLR B1H0157 Cadmium ND 0.05 mg/L 5.00 08/09/21 19:10 EPA 6010D MLR B1H0157 Chromium ND 0.10 mg/L 5.00 08/09/21 19:10 EPA6010D MLR B1H0157 Lead ND 0.25 mg/L 5.00 08/09/21 19:10 EPA 6010D MLR B1H0157 Selenium ND 0.25 mg/L 5.00 08/09/21 19:10 EPA6010D MLR B1H0157 Silver ND 0.10 mg/L 5.00 08/09/21 19:10 EPA 6010D MLR B1H0157 TCLP Volatile Organics Benzene ND 0.100 mg/L 50.0 08/09/21 12:00 EPA8260D LDM B1H0431 PO Box 5655 : Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.232.1556 ' fax 864.232.6140 rogersandcallcott.com __ t, . . _r _ _ _ _ ._. -. .,_ _ . _ �_a� __ __ _� _ an employee -owned company This report may not be reproduced. except in full, without written permission from Rogers & Galleon, Inc. 4 Rogers &Callcott ENVIRONMENTAL Environmental Testing Solutions Project: Earth Environmental Services 351 Depot St. Work Order: 1071568 Asheville, NC 28801-4310 Reported: 08/24/21 08:04 Sample Number Sample Description Earth Environmental Services #072121MVS collected on 07/27/21 10:05 Parameter 1071568-01 Reporting Result Limit Units DE Analyzed Method Flag Analyst Batch TCLP Volatile Organics 2-Butanone (MEK) ND 0.200 mg/L 50.0 08/09/21 12:00 EPA 8260D LDM B1H0431 Carbon tetrachloride ND 0.100 mg/L 50.0 08/09/21 12:00 EPA 8260D LDM B1H0431 Chlorobenzene ND 0.100 mg/L 50.0 08/09/21 12:00 EPA 8260D LDM B 1 H0431 Chloroform ND 0.100 mg/L 50.0 08/09/21 12:00 EPA 8260D LDM B1H0431 1,2-Dichloroethane ND 0.100 mg/L 50.0 08/09/21 12:00 EPA8260D LDM B1H0431 1,4-Dichlorobenzene ND 0.100 mg/L 50.0 08/09/21 12:00 EPA8260D LDM B1H0431 1,1-Dichloroethene ND 0.100 mg/L 50.0 08/09/21 12:00 EPA8260D LDM B1H0431 Tetrachloroethene ND 0.100 mg/L 50.0 08/09/21 12:00 EPA8260D LDM B1H0431 Trichloroethene ND 0.100 mg/L 50.0 08/09/21 12:00 EPA8260D LDM B1H0431 Vinyl chloride ND 0.100 mg/L 50.0 08/09/21 12:00 EPA8260D LDM B1E0431 Surrogates %REC %REC Limits Flag 1,2-Dichloroethane-D4 96 70-130 Toluene-D8 92 70-130 4-BromoJlaorobenzene 88 70-130 TCLP Semi -Volatile Organics 2-Methylphenol (o-Cresol) ND 0.100 mg/L 10.0 08/10/21 14:04 EPA 8270E RJM B1H0213 3/4-Methylphenol (m,p-Cresol) 0.206 0.100 mg/L 10.0 08/10/21 14:04 EPA8270E RJM B1H0213 total Cresol 0.206 0.200 mg/L 10.0 08/10/21 14:04 EPA 8270E RJM B1H0213 2,4-Dinitrotoluene ND 0.100 mg/L 10.0 08/10/21 14:04 EPA 8270E RJM B1H0213 Hexachlorobenzene ND 0.100 mg/L 10.0 08/10/21 14:04 EPA 8270E RJM B1H0213 Hexachlorobutadiene ND 0.100 m8/L 10.0 08/10/21 14:04 EPA8270E RJM B1H0213 Hexachloroethane ND 0.100 m8/L 10.0 08/10/21 14:04 EPA8270E RJM B1H0213 Nitrobenzene ND 0.100 mg/L 10.0 08/10/21 14:04 EPA8270E RJM B1H0213 Pentachlorophenol ND 0.100 m8/L 10.0 08/10/21 14:04 EPA 8270E RJM B1H0213 Pyridine ND 0.100 mg/L 10.0 08/10/21 14:04 EPA8270E RJM B1H0213 2,4,5-Trichlorophenol ND 0.100 mgfL 10.0 08/10/21 14:04 EPA8270E RJM B1H0213 2,4,6-Trichlorophenol ND 0.100 mg/L 10.0 08/10/21 14:04 EPA8270E RJM B1H0213 Surrogates %REC %REC Limits Flag Nitrobenzene-D5 63 15-314 2-Fluorobiphenyl 65 32-118 2-F7uorophenol 59 20-110 Phenol-D5 50 8-424 2,4,6-Tribromopheno! 79 39-130 Tetpheny!-D14 101 26-173 PO Box 5655 1 Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 main 864.232.1556 fax 864.232.6140 rogersandcallcott.com _. _. _ _ - - - --- m.-....-----, - — - ..__ �. _ - an employee -owned company 0824/2021 08:04 This report may not be reproduced. except infra without written permission from Rogers & Callcott, Inc. 08/24/2021 08:04 la Rogers &Callcott ENVIRONMENTAL Environmental Testing Solutions Project: Earth Environmental Services 351 Depot St. Work Order: 1071568 Asheville, NC 28801-4310 Reported: 08/24/21 08:04 Sample Number 1071568-01 Sample Description Earth Environmental Services #072121MVS collected on 07/27/21 10:05 Parameter Reporting Result Limit _ Units DF Analyzed Method Flag Analyst Batch TCLP Pesticides Gamma-BHC (Lindane) ND 0.00050 mg/L 10.0 08/17/21 01:36 EPA808IB RKH B1H0463 Chlordane ND 0.0050 mglL 10.0 08/17/21 01:36 EPA80S1B RKH B1H0463 Endrin ND 0.00050 mg/L 10.0 08/17/21 01:36 EPA8081B RKH B1H0463 Heptachlor ND 0.00050 mg/L 10.0 08/17/21 01:36 EPA8081B RKH B1H0463 Heptachlor Epoxide ND 0.00050 mg/L 10.0 08/17/21 01:36 EPA808IB RKH B1H0463 Toxaphene ND 0.0050 mg/L 10.0 08/17/21 01:36 EPA8081B RKH B1H0463 Methoxychlor ND 0.00050 mg/L 10.0 08/17/21 01:36 EPA808IB RKH B1H0463 Surrogates %REC %REC Limits Flag 2.4,5,6-Tetrachlorv-m xylene 69 60-130 Decachlorobiphenyl 88 30-150 PO Box 5655 Greenville, SC 29606 426 Fairforest Way Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232.6140 rogersandcallcott.com _... — -- an employee -owned company This report may not be reproduced, except in full, without written permission from Rogers & Cailcott, Inc. 11111• VL'1sJ a Aa Ail, • -alb L. •aJv a Va\taa .. • a.a.a. v v a ava• a vama. • Monitoring Period: From /-1- 2O,i. ) Facility Name: %,gis e J� /4 f L��J 1 Permit Number:-//400/0•6/s' WWTP Name: ,‘2,4,1,43 NPDES Number:tA A)S',Ja / To /42-3r Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: I Alternative 1■ I Alternative 2 E I Alternative 3■°` -" :: Alternative 4 ■ _ Alternative 5 ■ I Alternative 6 • If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost • I Heat Drying • I Heat Treatment ■ Thermophilic • - ' - '}s Beta Ra YS' • Gamma Ra ■ Pasteurization •■ '�`� `S F b s 2 i, . ,: i e i. 3 ... ,:.L.. 5 z.Y, c , Class B: I Alternative 1 ■ I Alternative 2 • I Alternative 3 • '� 'y' =' If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization • 1 Air Drying ■ Composting • Aerobic Digestion ■ . Anaerobic Digestion❑ ;S. k - yn "s zL o �n / 3'? ''� d4i�i-.isr Y yg r, r mob: 'l4. :...sY ��i-t t„�. .., .. �`Y. ��{:,i..e 9F �,:'� .. ��5� �.'F ":;lY S,So,'z -, per' F.. o" ,. .. x $....r ..,} .,..rf ,"� ....s.... ., .T.! mom_. ... If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen DensityNumber g of Frequency Sample Analytical Minimum Geo. Mean Maximum Units Excee_ of Analysis Type Tech -pique dences Fecal Coliform 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to the 6th power CFU per gram of 1000 mpn per gram of total solid (dry weight) G / Ili / 3 Lf _ L II? 340 if „i1_� jlit raj( lr _Sill 4z71 L Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 0 'Option 2 ❑ 'Option 3 0 !Option 4 ❑ 'Option 5 ❑ Option 6 6i 'Option 7 ❑ 'Option 8 ❑ 'Option 9 ❑ 'Option 10 ❑ Pi No vector attraction reduction options were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) �.j "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." 4[6itte 1 4Loi4 Preparer Name and Title (type o rint Land Applier Name and Title (if applicable)(type or print) s-7/1i c. //// 2-1-oing. Signature of Preparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) Earth Environmental Services Murphy, NC Name and Address of Facility Town of Maggie Valley 3987 Soco Road Maggie Valley, NC 28751 Att: Mike MeHaffey Report Date Date and Time Received Date and Time Sampled Earth Environmental 75 Bison Lane Murphy, NC 28906 828-837-9543 (office) 828-644-4835 (lab) Lab ID# 352 1/28/2021 1/18/2021 8:50 AM 1/18/2021 8:50 AM Sampler JOHN CURTIS BROWN CLASS A Date Test BIOSOLIDS Sample Time Report Limit Units Method Analyzed Analyst SLUDGE FECAL < 131 8:50 AM 131 % SM9221E 1/18/21 KEK PH 12.0 8:50 AM 0.1 s.u. SM2540 G 1/18/21 MS % TOTAL SOLIDS 73 8:50 AM 0.1 % SM 2540 G 1/18/21 KEK Lab Supervisor: Wanda G. Ladd; EES - Murphy Certified By: ilierzeil/;^ Earth Environmental Services Murphy, NC Name and Address of Facility Town of Maggie Valley 3987 Soco Road Maggie Valley, NC 28751 Att: Mike MeHaffey Report Date Date and Time Received Date and Time Sampled Sampler Earth Environmental 75 Bison Lane Murphy, NC 28906 828-837-9543 (office) 828-644-4835 (lab) Lab ID# 352 4/30/2021 4/19/2021 8:35 AM 4/19/2021 8:35 AM JOHN CURTIS BROWN CI MSS A Date Test BIOSOLIDS Sample Time Report Limit Units Method Analyzed Analyst SLUDGE FECAL < 169 8:35 AM 169 % SM9221E 4/19/21 KEK PH 12.0 8:35 AM 0.1 s.u. SM2540 G 4/19/21 MS % TOTAL SOLIDS 94 8:35 AM 0.1 % SM 2540 G 4/19/21 KEK Lab Supervisor: Wanda G. Ladd; EES - Murphy Certified By: r�4 Earth Environmental Services Murphy, NC Name and Address of Facility Town of Maggie Valley 3987 Soco Road Maggie Valley, NC 28751 Att: Mike MeHaffey Report Date Date and Time Received Date and Time Sampled Earth Environmental 75 Bison Lane Murphy, NC 28906 828-837-9543 (office) 828-644-4835 (lab) Lab ID# 352 8/20/2021 7/19/2021 9:02 AM 7/19/2021 9:02 AM Sampler JOHN CURTIS BROWN CLASS A Date Test BIOSOLIDS Sample Time Report Limit Units Method Analyzed Analyst SLUDGE FECAL < 119 9:02 AM 119 % SM9221E 7/19/21 KEK PH 12.3 9:02 AM 0.1 s.u. SM2540 G 7/19/21 MS % TOTAL SOLIDS 66 9:02 AM 0.1 % SM 2540 G 7/19/21 KEK Lab Supervisor: Wanda G. Ladd; EES - Murphy Certified By:ais,j4.--jew bdeV,.,10".°# Earth Environmental Services Murphy, NC Name and Address of Facility Town of Maggie Valley 3987 Soco Road Maggie Valley, NC 28751 Att: Mike MeHaffey Report Date Date and Time Received Date and Time Sampled Sampler Earth Environmental 75 Bison Lane Murphy, NC 28906 828-837-9543 (office) 828-644-4835 (lab) Lab ID# 352 11/17/2021 10/18/2021 9:10 AM 10/18/2021 9:10 AM JOHN CURTIS BROWN CLASS A Date Test BIOSOLIDS Sample Time Report Limit Units Method Analyzed Analyst SLUDGE FECAL < 121 9:10 AM 121 % SM9221E 10/18/21 KEK PH 12.0 9:10 AM 0.1 s.u. SM2540 G 10/18/21 MS % TOTAL SOLIDS 67 9:10 AM 0.1 % SM 2540 G 10/18/21 KEK Lab Supervisor: Wanda G. Ladd; EES - Murphy Certified By: Town of Maggie Valley Daily Field Parameter Worksheet Dewatered Sludge/Mixed Sludge PH/Temp. Analyst: AAi Date Gallons Dewatered Calibration Buffer 7.0 Calibration Buffer 12.45 Check Buffer 10.0 Time Sampled • Time Analyzed • PH au 3-i L 3-l6r 17 yea 1/3o F3 6.3 $-Lt Zo1 ,,o f lf1) 7o1 7.01 701 id,1/5 /2..1f 5 /2V 5 12,95 10.o5 lo,v3 io. 0 5 /(5,W 13; 13000 15;10 12 ;23 !3 I5:07 15; 16 6-5 gZ7oo 70l Zol Zo 701 70 .95 12)15 12.Y5 0,06 10.06 10.0 1a03 10.06 • f2'oo T5.v,- to; tQ L5:v 15'07 l.V 07 15:of {5110t * The pH check buffer must be within ± .1 units of the buffer's true value. • If sample is measured directly at the source only time analyzed would be recorded /0132 42,51 E.Z. 72 she fy icimP Month Year oft ' Sludge Temp °C Air Temp •C Correction Factor Corrected PH i T Q 0 ° su su Comment .4' 4fe ,cT&- 4-0 vdi. -5e0 23a ,meet -11//ZY1 o �! �� %'1 i '56i Zr Wi° ° 99 1° c1° Clog Or 15''1°'23° 7yy,(/ ,c4. 7 .,/°/ Date 6 Gallons Dewatered Calibration Buffer 7.0 Calibration Buffer 12.45 Check Buffer 10.0 Time Sampled • Time Analyzed ♦ PH su Sludge Temp °C ,.htrtemp °C 71 lii00 7-1 `_' 7_,Q I [02R 5 (o.01 16:0 / 15'.0g' 1j.n gar ,Z5 9 7-1 — 1,0( P� ,ys to,° /,(; I'l is't2 12tV( gbit 2T 1,3 ,- /Let / ,W('MI 6 - 1; /2,0 ?1.1� X3- ��`� -i`a( 'P`/ � 1ael /'1Z2- /i>? ( 2) 124E 62,q) 27,1 * The pH check buffer must be within + _ 1 i nits of fh r.,.�.,e ... ....i.._ Town of Maggie Valley Daily Field Parameter Worksheet Dewatered Sludge/Mixed Sludge PH/Temp. Analyst: AV‘JQrd cv4--, Month year2v Correction Factor su Corrected PH su Comment 0 ,06 eo6 tog 12, r) 141,g1 /447ideldfr l-r� tVt nit oK • If sample is measured directly at the source only time analyzed would be recorded Analyst: .‘P11,‘ f3o,)t Town of Maggie Valley Daily Field Parameter Worksheet Dewatered Sludge/Mixed Sludge PH/Temp. S(u y m ..�/�., Tear J Date Gallons Dewatered Calibration Buffer 7.0 Calibration Buffer 12.45 Check Buffer 10.0 Time Sampled + Time Analyzed ♦ PH su Sludge 9 Temp "C •Iktr1rtrl� °C Correction Factorsu su Corrected PH Comment cl ;2,3 ii2.9 qLiqt l0o �- su I r.Z 28 -- 7-.o I 107H 5 loot' `L/ 55 / `q'55 / G7 9i. 23' l # [,r,G ti7 ,?7 - 791 1J 95/0.05 /5:2o 15'25 /2.51 g5. 7 2a,/- --d.oq 1W 12 39 — — 7.o l 12. its to-c. 15;0 7 15:l /o2.73 77 / 02l. 3 -v. I z 12,6 I _2-31 -- 7 7o1 I2.`/5 to.05 15:5045:5562,57,7,i( ozzig< -0.03 124-4 The pH check buffer must be within ± .1 units of the buffer's true value + If sample is measured directly at the source only time analyzed would be recorded