WQ0001346_Residual Annual Report 2021_20220215

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0001346
Applicant/Permittee City of Monroe
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office Mooresville
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Kyle Ketchum
Email Address* Phone Number*
[e-mail] 704-282-4612
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0001346
Has Current Existing permit number
Applicant/Permittee Address* 775 Treeway Drive Monroe,NC 28110
Facility Name* City of Monroe Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
2021 Annual Report.pdf 116.29MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature
l��fL
Submission Date 2/15/2022

honroe
North Carolina
RESIDUALS LAND APPLICATION
PROGRAM
CITY
OF
MONROE
ANNUAL REPORT
2021
PERMIT NUMBER
WQ0001346

-.,
onroe
North Carolina
City of Monroe
Water & Wastewater Residuals Land Application Program
2021
Annual Report
Table of Contents
1. Certification Form & Annual Operations Summary
2. Annual Residual Sampling Summary Forms & Biosolids Analysis
3. TCLP Analysis
4. Field Summary Forms
5. Pathogen Reduction & Vector Attraction Reduction
6. Soil Analysis

TAB l
CERTIFICATION FORM & ANNUAL
OPERATIONS SUMMARY

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001346 County: Union Year: 2021
Facility Name(as shown on permit): City of Monroe
Land Application Operator: Ken Morris, Land Residual Coordinator Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No -If No, skip Part A,and Part B and proceed to Part C. Also, If residuals were
generated but not land applied,please attach an explanation on how the residuals were handled.
Part A- Residuals Application Summary:
Total number of application fields in the permit: 35
Total number of fields utilized for land application during the year: 22
Total amount of dry tons applied during the year for all application sites: 1,286
Total number of acres utilizes for Iand application during the year: 291.4
Part B-Annual Compiance Statement:
Facility was compliant during calendar year 2021 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 1J Yes ❑ No
If no please, provide a written description why the facility was not compliant,the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed)to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required)was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a)or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with(applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C -Certification:
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true, accurate,
and complete. I am aware that there are significant penalties for submitting false information,including the
possibility of fines and imprisonment for knowing violations."
Russell Colbath, P.E.,Water Res. Director Z 2�
Permittee Name and Title(type or print) Signature of Permittee Date
10-- a141?) �. r'€ a -
Si ature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T .1102 (26) DENR FORM ACF(12/2006)

OPERATION SUMMARY
Permit # WQ0001346
FIELDS USED IN 2021
SI S WWTP WTP WWII' " i N WTP PAN
NAME NO. GALS GALS YARDS YARDS Dry Tons Dry Tons llbs/ac)
Calvin Morris 1 April 11.6 54 7.55 21.205
NC-AN-19 April 54 13.38 16.188
May 126 17.62 49.479
May 18 4.45 5.396
Ben Myers 1 June 44.6 316 44.'10 32.274
NC-UN-18 June 332 82.20 25.885
July l 162 31.40 16.295
July ' 144 38.94 12,560
Dec 108 25.73 19.519
Dec 18 s 5.22 1.385
2 ' Sept 27.6 216 41.84 35.109
Sept 342 92.46 -_ 48.204
7 May 5.7 126 17.61 100.694
Dec 54 15.65 32.522
8 May 16 270 37.74 76.869
May 18 4.46 3.912
Dec 72 17.17 36.272
Dec ' 54 15.65 11.586
William Griffin 1 May 24.5 344 48.09 63.958
N C-U N-29 May 136 33.66 19.303
2 Aug 5.7 64 12.40 50.370
Aug 32 8.65 21.839
3 July 7.4 64 12.40 38.799
July 48 12.98 25.233
Aug 18 3.49 10.912
Aug 54 14.60 28.388
4 June 2.9 36 5.03 56.547
June 18 4.46 21.583
5 Aug 2.2 16 3.10 32.626
Aug 16 4.33 28.292
Tom Appenzelfer 1 June 13.1 126 17.62 43.813
NC-UN-30 June 144 35.66 38.224
4 June 15.2 220 30.75 65.930
June 80 19.81 18.302
5 June 10.8 112 15.66 47.239
June 96 23.77 30.910 "
Henry Myers 3 May 2.5 I 36 5.03 65.595
NC-UN-31 May 36 8.91 50.074
4 May 4.7 72 10.07 69.782
May 36 8.92 26.635
5 Sept 17.6 208 40.29 53.017
Sept 194 52.45 42.880
6 Sept 7.8 54 10.46 31.058
Sept 126 34.06 62.841
Danny Baker 1 Aug 23.5 54 10.46 10.308
NC-UN-32 Aug 36 9.73 5.959
Sept 342 66.247 65.287
Sept 18 4.865 2.98
2 Nov 15.5 162 38.611 84.245
Nov 126 - 36.503 - 27.906
3 Sept 10 ¶98 38.55 - _ 88.825
4 Nov 3.2 36 8.5T9 _ 90.681
5 Nov 1'3:3 230 69.113 121.116
Nov 48 13.915 8.538
Totals 291.4 0 0 3,902 2,278 686.61 599.66
Total Dry
Total Gallons 0 I Total Yards 6 180 I Tons 1,286
WWTP- Metric Tons 622.75
WTP- Metric Tons 543.90
Total Metric Tons 1166.65

TAB 2
ANNUAL RESIDUAL SAMPLING SUMMARY
FORMS & BIOSOLIDS ANALYSIS

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF-B
WQ Permit Number: WQ0001346 Laboratory: 1) Contract Labs
Facility Name: City of Monroe 2)
Residual Source WQ#or NC0024333 3)
NPDES#: 4)
WWTP Name: Monroe WWTP (cake) 5)
Residual Analysis Data
Conc. Sample or Composite Date
Parameter Limit
(mg/kg) (mg}a 1-5-21 4-5-21 7-6-21 10-4-21 10-21-21
Percent Solids(%) NA 16.8 16.6 23 20.8 28.3
Arsenic 75 10.7 12 9.48 10.3
Cadmium 85 1.02 1.16 2.91 1.31
Copper 4,300 349 383 400 345
Chromium NA 74.4 74.7 87 69.2
Lead 840 _ 26.2 22.7 16.1 22
Mercury 57 0.72 0.489 0.37 0.477
Molybdenum 75 19 18.1 20.2 16.8
Nickel 420 74.4 77.1 60 63.9
Selenium 100 11.6 5 <2.17 6.73
Zinc 7,500 1060 1090 835 1030
Total Phosphorus NA 24600 24000 19300 - 22600
TKN NA 62500 51900 35000 50000
•
Ammonia-Nitrogen NA 2140 3280 3470 2400
Nitrate and Nitrite NA 170 65.7 386 1430
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
/54 ilk-- ?hi>X
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0001346 Laboratory: 1) Contract Labs
Facility Name: City of Monroe 2)
Residual Source NC0024333 3)
NPDES #or WQ#: 4)
WWTP Name: Monroe WWTP (cake) 5)
Residual Analysis Data
Sample or Composite Date
Parameter
(mg/kg) 1-5-21 4-5-21 7-6-21 10-4-21 10-21-21
Potassium 2400 2010 1540 2070
Sulfur 9760 11400 8520 9570
Calcium 13800 18300 13800 _ 15500
Magnesium 2200 2540 2110 2220
Sodium 532 651 709 606 _
Iron 57900 62000 92600 55300
Aluminum 17400 15400 12600 13900
Manganese 1360 1780 1520 1690
Organic N 60100 48700 31570 47600
pH ( standard units) 5.8 6.6 7 5.7
Volitile Solids% 59 58.1 52.6 47.8
PAN 38.696 32.5834 23.16 33.82 33.82
SAR 0.45 0.49 0.71 0.55 0.64
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Y&P---- .7/9/ >)-
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF-B
WQ Permit Number: WQ0001346 Laboratory: 1) Contract Labs
Facility Name: City of Monroe 2)
Residual Source WQ#or NC0024333 3)
NPDES#: 4)
WWTP Name: Monroe WTP (cake) 5)
Residual Analysis Data
Conc. Sample or Composite Date
Parameter Limit
(mg/kg) (m g)a 1-5-21 4-5-21 7 6 21 10-4-21
Percent Solids (%) NA 26.6 29.4 32.1 34.4
Arsenic 75 41.7 27.1 14 41.3
Cadmium 85 <3.76 2.58 4.02 3.23
Copper 4,300 429 473 461 442
Chromium NA 210 236 223 195
Lead 840 <11.3 <5.10 7.38 <8.72
Mercury 57 <0.0578 0.0479 <0.0482 <0.0415
Molybdenum 75 49.6 58.2 50.5 49.1 _
Nickel 420 39.8 35 27.4 32
Selenium 100 <18.8 <8.50 <7.79 <14.5
Zinc 7,500 121 74.5 60.7 125
Total Phosphorus NA 3170 2970 2260 3080
TKN NA 18900 17300 14700 14400
Ammonia-Nitrogen NA 3180 473 1650 834
Nitrate and Nitrite NA 72.2 54.8 1150 81.4
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0001346 Laboratory: 1) Contract Labs
Facility Name: City of Monroe 2)
Residual Source NC0024333 3)
NPDES #or WQ#: 4)
WWTP Name: Monroe WTP (cake) 5)
Residual Analysis Data
Sample or Composite Date
Parameter
(mg/kg) 1-5-21 4-5-21 7-6-21 10-4-21
Potassium <376 243 266 <291
Sulfur 2410 2690 _ 2360 3280
Calcium 1950 1660 1690 2970
Magnesium 414 408 424 500
Sodium <940 <425 <389 <727
Iron 338000 354000 368000 _ 320000
Aluminum 4020 7210 5230 3460
Manganese 1020 524 _ 526 1220
Organic N 15800 16800 - 13020 13610
pH(standard units) 5 5.2 6.4 6.3
Volitile Solids % 34.2 32.8 34.8
PAN 15.9004 14.0442 14.39 11.8496
SAR 2.6 1.31 1.24 1.9
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
41r/r--- ?hi?)-
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (1212006)

City of Monroe
Reports of Lab
Analysis
1 St Quarter

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Waypoint- 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalyticaicom
1/12/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 21-007-0003
Project Description: RAS
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/7/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
firj7Cra
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 5

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d% pO I nt, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-007-0003
Client Project Description: RAS
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
74573 RAS Solids 01/05/2021 10:45 01/07/2021 SM-2540G WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN,Memphis,TN
Page 2 of 5

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Waypai nt.. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.corn
46205
City of Monroe Project RAS
Ken Morris Report Date : 01/12/2021
775 Treeway Dr Information : Received :01/07/2021
Monroe, NC 28110
Taxes., Ini G(vaO
Pauric Mc Groary Ph.D.,CPA
Report Number:21-007-0003 REPORTOFANALYSIS Agronomist
Lab No: 74573 Matrix: Solids
Sample ID:RAS Sampled: 1/5/2021 10:45
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Moisture 98.7 % 0.010 1 01/08/21 16:09 FMM SM-2540G
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Total Solids 1.33 % 0.010 1 01/08/21 16:09 FMM SM-2540G
Total Volatile Solids 72.8 % 0.010 1 01/08/21 16:09 FMM SM-2540G
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 5

•
vv
Waypoi nt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.ccm
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-007-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
UPS O Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? • Yes O No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No • Not Present
Custody seals intact on sample bottles? O Yes 0 No 0Not Present
Chain of Custody(COC) present? • Yes 0 No
COC agrees with sample fabel(s)? • Yes 0 No
COC properly completed • Yes 0 No
Samples in proper containers? • Yes 0 No
Sample containers intact? • Yes 0 No
Sufficient sample volume for indicated test(s)? • Yes 0 No
All samples received within holding time? • Yes 0 No
Cooler temperature in compliance? • Yes O No
Cooler/Samples arrived at the laboratory on ice. • Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No 0N/A
Water-VOA vials free of headspace 0 Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No • N/A
Soil VOA method 5035—compliance criteria met 0 Yes O No • N/A
High concentration container(48 hr) ( Low concentration EnCore samplers (48 hr)
r High concentration pre-weighed (methanol -14 d) I Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0No
Comments:
Signature: Samantha Clarke Date&Time: 01/07/2021 13:11:36
Page 4 of 5

sArPI 'fillll iiliit ili,Il!l1.11l!!ll!!1!11N11 a za°°3 F CUSTODY
City of Monme t3:11 14
RAS JS
_ . . __ 14QI [�
Office Information Customer Information
Rept# Submitted By 4 Charge To Copy To Project
Kan frk r-% y _ City of Monroe
Acct# POB 69
Email
46205 Monroe NC 28111
Lab Number(Lab Use Only) Sample ID Container Type Sampled Date: i -;.a - : i, Date Recd:
Glass (Y or:15a) Sampled Time: r : -tom Time Reed:
RAS Plastic Ilitbarfoie) Sampled By: kwk iv1ar.:•a Recd By:
Relinquished By: (Signature) Date Time Received By: (Signature) Date Time
..,_.t.,...— )v1 wx-iz. i -A5-:2 t I a','t
)Q V-{) iii.fit,n U7 i c I--I- 21 1 00 Sim
Please Place a "X" by Desired Tests j internal Lab Code:
Solids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N
w
X o
ln
CaCO3 Volatile _ o)
Cd Cr Ni Pb As Hg Se pH Eq. % Solids% Org-N Mo CI B Ba a
X
SO4 Ag Sb Co Sn Ti V Be ALK SS • Avail P Sol K Cond ' WIN ` SOL B
SOL NA O&G SP.GR. TSS Sieve#20 Sieve#60 Sieve#100 ASH Ca0 CaCO3 MgCO3 MgO C!N ' TOC Env
TOTAL TOTAL REACT
P205 K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS CN FECAL TCLP !CR
State Certification Needed: NORTH CAROLINA os 1et “ 0
Special Instructions or Remarks Comments

YY
Waypoint.. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
1/15/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 21-007-0001
Project Description: WWTP Cake
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s)on 1/7/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012)and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
C &to air
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

•
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Waypoint, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-007-0001
Client Project Description: WWTP Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
74571 WWTP Cake Solids 01/05/2021 10:50 01/07/2021
74571 WWTP Cake Solids 01/05/2021 10:50 01/07/2021 SM-4500-NH3C WP MTN
74571 WWTP Cake Solids 01/05/2021 10:50 01/07/2021 9045D WP MTN
74571 WWTP Cake Solids 01/05/2021 10:50 01/07/2021 4500NO3F-2011 WP MTN
74571 WWTP Cake Solids 01/05/2021 10:50 01/07/2021 6010D WP MTN
74571 WWTP Cake Solids 01/05/2021 10:50 01/07/2021 SW-7471B WP MTN
74571 WWTP Cake Solids 01/05/2021 10:50 01/07/2021 SM-4500-NH3C-TKN WP MTN
74571 WWTP Cake Solids 01/05/2021 10:50 01/07/2021 SM-2540G WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN,Memphis,TN
Page 2 of 6

W
Waypni nt-
7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project WWTP Cake
Ken Morris Report Date : 01/15/2021
775 Treeway Dr Information : Received :01/07/2021
Monroe, NC 28110 U
tuoict MC G vaKr
Pa uric Mc Groary Ph.D.,CPA
Report Number:21-007-0001 REPORT OF ANALYSIS Agronomist
Lab No : 74571 Matrix: Solids
Sample ID:WWTP Cake Sampled: 1/5/2021 10:50
Test Results Units MOL DF Date/Time By Analytical
Analyzed Method
Moisture 83.2 % 0.010 1 01/08/21 16:09 FMM SM-2540G
Test Results Units MOL DF Date/Time By Analytical
Analyzed Method
Ammonia Nitrogen 2140 mg/Kg-dry 149 1 01/14/21 15:30 3P3 SM-4500-NH3C
Nitrate+Nitrite-N 170 mg/Kg-dry 29.1 1 01/13/21 10:41 ZBD 4500NO3F-2011
Organic N 60100 mg/Kg-dry 1490 1 01/14/21 10:00 CALCULATION
pH 5.8 s.u. 1 01/14/21 15:18 CxC 9045D
Total Solids 16.8 % 0.010 1 01/08/21 16:09 FMM SM-2540G
Total Volatile Solids 59.0 % 0.010 1 01/08/21 16:09 FMM SM-2540G
Total Kjeldahl Nitrogen 62500 mg/Kg-dry 1490 1 01/14/21 10:00 JPJ iM-4500-NH3C-TKP
Phosphorus 24600 mg/Kg-dry 29.8 1 01/11/21 16:47 TJS 6010D
Aluminum 17400 mg/Kg-dry 29.8 1 01/11/21 16:47 TJS 6010D
Arsenic 10.7 mg/Kg-dry 2.98 1 01/12/21 17:48 TJS 6010D
Calcium 13800 mg/Kg-dry 298 1 01/12/21 17:48 TJS 6010D
Cadmium 1.02 mg/Kg-dry 0,595 1 01/11/21 16:47 TJS 6010D
Chromium 74.4 mg/Kg-dry 1.49 1 01/11/21 16:47 TJS 6010D
Copper 349 mg/Kg-dry 2.98 1 01/12/21 17:48 TJS 6010D
Iron 57900 mg/Kg-dry 59.5 1 01/11/21 16:47 TJS 6010D
Lead 26.2 mg/Kg-dry 1.79 1 01/11/21 16:47 TJS 6010D
Magnesium 2200 mg/Kg-dry 29.8 1 01/11/21 16:47 TJS 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 6

vvYY,
•
WaipOlWaypoint,
7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical-com
46205
City of Monroe Project WWTP Cake
Ken Morris Report Date : 01/15/2021
775 Treeway Dr Information : Received : 01/07/2021
Monroe, NC 28110
Tillage in &tangy
Pauric Mc Groary Ph.D.,CPA
Report Number:21-007-0001 REPORT OF ANALYSIS
Agronomist
Lab No : 74571 Matrix: Solids
Sample ID:WWTP Cake Sampled: 1/5/2021 10:50
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Method
Manganese 1360 mg/Kg-dry 2.98 1 01/12/21 17:48 TJS 6010D
Mercury 0.720 mg/Kg-dry 0.0827 1 01/11/21 13:10 DDB SW-7471B
Molybdenum 19.0 mg/Kg-dry 1.49 1 01/11/21 16:47 TJS 6010D
Nickel 74.4 mg/Kg-dry 1.49 1 01/11/21 16:47 TJS 6010D
Potassium 2400 mg/Kg-dry 59.5 1 01/11/21 16:47 TJS 6010D
Selenium 11.6 mg/Kg-dry 2.98 1 01/11/21 16:47 TJS 6010D
Sodium 532 mg/Kg-dry 149 1 01/11/21 16:47 TJS 6010D
Zinc 1060 mg/Kg-dry 7.44 1 01/11/21 16:47 TJS 6010D
Sulfur 9760 mg/Kg-dry 59.5 1 01/11/21 16:47 TJS 6010D
Qualifiers/ OF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 4 of 6

• Yv
"af130111t 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalyticai.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-007-0001
Shipping Method
0 Fed Ex 0 US Postal 0 Lab O Other :
• UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? Yes 0 No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present
Custody seals intact on sample bottles? 0 Yes 0 No • Not Present
Chain of Custody(COC) present? 0 Yes 0 No
COC agrees with sample label(s)? • Yes 0 No
COC properly completed 0Yes 0 No
Samples in proper containers? • Yes 0 No
Sample containers intact? • Yes 0 No
Sufficient sample volume for indicated test(s)? 0Yes O No
All samples received within holding time? • Yes 0 No
Cooler temperature in compliance? • Yes 0 No
Cooler/Samples arrived at the laboratory on ice. • Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water-Sample containers properly preserved 0 Yes 0 No • N/A
Water- VOA vials free of headspace 0 Yes 0 No • N/A
Trip Blanks received with VOAs 0 Yes 0 No • N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No • N/A
r High concentration container(48 hr) 7 Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) r Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0No
Comments:
Signature: Samantha Clarke Date&Time: 01/07/2021 12:58:21
Page 5 of 6

SAMPLE T 111111111131 HIM IINIIIt Ill III 7- 01 JSTOD'Y
Cold of Mom x• 12 58 02 t4ATP C.ik
r6:
Office Information Customer Information
Rept# ciibmiHed By L Charge To Copy To Project
�e_.1-. ivt.�r City of Monroe
Acct# POB 69 Email
46205 Monroe NC 28111
� ir,s e 1vlar,toCTt4..a.
Lab Number(Lab Use Only) Sample ID Container Type Sampled Date: 1 - ro -..9. I Date Recd:
1 1/51 1 WWTP Cake Glass (Yes or No) Sampled Time: a Time Recd:
Plastic (Yes or No) Sampled By: lc�,•-\ M,,,,r,L Recd By:
Relinquished By: (Signature) Date Time Received By: (Signature) Date Time
iKe lv\,..rt A i r5 ` ,2 \ i.4:•?
litY. r A.ixID Pul Cc I-1- 9l 1: lp(
Please Place a "X" by Desired Tests Internal Lab Code: SLMONR
Solids % TKN P K S Ca Mg Na Fe Al Mn Cu Zn NH4-N NO3-N `
W
x x x x x x x x x x x x o
tn
.Cd Cr Ni ` • As Hg Se pH • Org-N Mo CI B Ba ro
x x x x x x x x x
'504 Ag Sbi Sn TI V Be ALK SS Avail P Sol K Cond WIN SOL B
SOL NA O&G SP,GR. TSS Sleve#20 Sleve#60 Sieve#100 ASH • CaCO3 MgCO3 MgO C/N TOC Env
TOTAL TOTAL REACT
P205 K20 TN TKNW NH4W NO3W ORGN-W PA CERT AZ CERT BTU PCBS CN FECAL TCLP ICR
State Certification Needed: NORTH CAROLINA IA A°S IN., V ‘Wllt
Special Instructions or Remarks _ Comments
{i • • 1 , ■li Au, I-1-

Waypoint. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
1/15/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 21-007-0002
Project Description: WTP Ferric Cake
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s)on 1/7/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
pit 6vipaer
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option,repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

o
/aypo i nt. 7621 White pine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-007-0002
Client Project Description: WTP Ferric Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
74572 WTP Ferric Cake Solids 01/05/2021 11:15 01/07/2021
74572 WTP Ferric Cake Solids 01/05/2021 11:15 01/07/2021 SM-4500-NH3C WP MTN
74572 WTP Ferric Cake Solids 01/05/2021 11:15 01/07/2021 9045D WP MTN
74572 WTP Ferric Cake Solids 01/05/2021 11:15 01/07/2021 4500NO3F-2011 WP MTN
74572 WTP Ferric Cake Solids 01/05/2021 11:15 01/07/2021 6010D WP MTN
74572 WTP Ferric Cake Solids 01/05/2021 11:15 01/07/2021 SW-7471B WP MTN
74572 WTP Ferric Cake Solids 01/05/2021 11:15 01/07/2021 SM-4500-NH3C-TKN WP MTN
74572 WTP Ferric Cake Solids 01/05/2021 11:15 01/07/2021 SM-2540G WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN, Memphis,TN
Page 2 of 8

ws
WaypoInt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypaintanalytical.com
46205
City of Monroe Project WTP Ferric Cake
Ken Morris Report Date : 01/15/2021
775 Treeway Dr Information : Received : 01/07/2021
Monroe, NC 28110
tawty I4c Groan
Pauric Mc Groary Ph.D.,CPA
Report Number:21-007-0002 REPORT OF ANALYSIS Agronomist
Lab No : 74572 Matrix: Solids
Sample ID:WTP Ferric Cake Sampled: 1/5/2021 11:15
Test Results Units MOL DF Date/Time By Analytical
Analyzed Method
Moisture 73.4 % 0.010 1 01/08/21 16:09 FMM SM-2540G
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Ammonia Nitrogen 3180 mg/Kg-dry 94.0 1 01/14/21 15:30 JPJ SM-4500-NH3C
Nitrate+Nitrite-N 72.2 mg/Kg-dry 17,1 1 01/13/21 10:42 ZBD 4500NO3F-2011
Organic N 15800 mg/Kg-dry 940 1 01/14/21 10:00 CALCULATION
pH 5.0 s.u. 1 01/14/21 15:18 CxC 9045D
Total Solids 26.6 % 0.010 1 01/08/21 16:09 FMM SM-2540G
Total Volatile Solids 34.2 % 0.010 1 01/08/21 16:09 FMM SM-2540G
Total Kjeldahl Nitrogen 18900 mg/Kg-dry 940 1 01/14/21 10:00 JPJ iM-4500-NH3C-TKO
Phosphorus 3170 mg/Kg-dry 188 10 01/12/21 17:53 TJS 6010D
Aluminum 4020 mg/Kg-dry 188 10 01/12/21 17:53 TJS 6010D
Arsenic 41.7 mg/Kg-dry 18.8 10 01/12/21 17:53 TJS 6010D
Calcium 1950 mg/Kg-dry 1880 10 01/12/21 17:53 TJS 6010D
Cadmium <3.76 mg/Kg-dry 3,76 10 01/12/21 17:53 TJS 6010D
Chromium 210 mg/Kg-dry 9.40 10 01/12/21 17:53 TJS 6010D
Copper 429 mg/Kg-dry 18.8 10 01/12/21 17:53 TJS 6010D
Iron 338000 mg/Kg-dry 3760 100 01/12/21 17:57 TJS 6010D
Lead <11.3 mg/Kg-dry 11,3 10 01/12/21 17:53 TJS 6010D
Magnesium 414 mg/Kg-dry 188 10 01/12/21 17:53 TJS 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 8

w
V/aypo i nt 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www,waypointanalytical.com
46205
City of Monroe Project WTP Ferric Cake
Ken Morris Report Date : 01/15/2021
775 Treeway Dr Information : Received :01/07/2021
Monroe, NC 28110
Tawfc Mc G nary
Pauric Mc Groary Ph.D., CPA
Report Number:21-007-0002 REPORT OF ANALYSIS Agronomist
Lab No : 74572 Matrix: Solids
Sample ID :1NTP Ferric Cake Sampled: 1/5/2021 11:15
Test Results Units MQL DF Date I Time By Analytical
Analyzed Method
Manganese 1020 mg/Kg-dry 18.8 10 01/12/21 17:53 TJS 6010D
Mercury <0.0578 mg/Kg-dry 0.0578 1 01/11/21 13:11 DDB SW-7471B
Molybdenum 49.6 mg/Kg-dry 9.40 10 01/12/21 17:53 TJS 6010D
Nickel 39.8 mg/Kg-dry 9,40 10 01/12/21 17:53 TJS 6010D
Potassium <376 mg/Kg-dry 376 10 01/12/21 17:53 TJS 6010D
Selenium <18,8 mg/Kg-dry 18,8 10 01/12/21 17:53 TJS 6010D
Sodium <940 mg/Kg-dry 940 10 01/12/21 17:53 TJS 6010D
Zinc 121 mg/Kg-dry 47.0 10 01/12/21 17:53 TJS 6010D
Sulfur 2410 mg/Kg-dry 376 10 01/12/21 17:53 TJS 6010D
Qualifiers/ OF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 4 of 8

iV
Waypoi nt- 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Client: City of Monroe CASE NARRATIVE
Project: WTP Ferric Cake
Lab Report Number: 21-007-0002
Date: 1/14/2021
Metals Analysis Method 6010D
Sample 74572 (WTP Ferric Cake)
Analyte:Aluminum
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte:Arsenic
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Calcium
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Cadmium
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Chromium
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Copper
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Iron
QC Batch No: L5307181L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Potassium
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Magnesium
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Manganese
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Anaiyte: Molybdenum
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 5 of 8

wo
Waypoi nt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Analyte: Sodium
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Nickel
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Phosphorus
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Lead
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Sulfur
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Selenium
QC Batch No: L530718/L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Zinc
QC Batch No: L5307181L530387
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 6 of 8

YV
Waypoint. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-007-0002
Shipping Method
0 Fed Ex 0 US Postal O Lab 0 Other :
• UPS O Client O Courier Thermometer ID: I
Shipping container/cooler uncompromised? • Yes 0 No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No • Not Present
Custody seals intact on sample bottles? 0 Yes 0 No • Not Present
Chain of Custody(COC) present? • Yes 0 No
COC agrees with sample label(s)? • Yes 0 No
COC properly completed Yes O No
Samples in proper containers? • Yes 0 No
Sample containers intact? 1111Yes 0 No
Sufficient sample volume for indicated test(s)? • Yes 0 No
All samples received within holding time? • Yes 0 No
Cooler temperature in compliance? • Yes 0 No
Cooler/Samples arrived at the laboratory on ice. • Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water-Sample containers properly preserved 0 Yes 0 No N/A
Water- VOA vials free of headspace 0 Yes 0 No 0N/A
Trip Blanks received with VOAs 0 Yes 0 No • N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No • N/A
J High concentration container(48 hr) r Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) I Low conc pre-weighed vials (Sod Bis-14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Samantha Clarke Date&Time: 01/07/2021 13:09'34
Page 7 of 8

SAMPLE TB 11111111111111111111111111 0z ;TODYCity or Monroe w
i309•13
i R
1 WTPFereic Cake
Office Information Customer Information
Rept# Submitted By J Charge To Copy To Project
g,u' Harr;. City of Monroe
Acct# POB 69 Email
46205 Monroe NC 28111 tf--vvii.r,, t rvvzv-ecrzn(....-„^.t
Lab Number(Lab Use Only) Sample ID Container Type Sampled Date: 1-5-.1 i Date Recd: _
Glasscy Sampled Time: r 1.;r, Time Recd:
��5��} V4'TP Ferric Cake Plasticey,...ir
e) Sampled By: , k," Ma f,,- ,s Recd By:
Relinquished By: (Signature) Date Time Received By:(Signature) Date Time
K j✓toti...6c i -5-,71 ii : 15
4,1,AVOLA& A C c , 1 Q. t-1-'1 , I .50 911
Please Place a "X" by Desired Tests Internal Lab Code: SLMONR
m
Solids% '`TICH;11 :, lit? ''j'-044.10 A:: ...-riS^ Ca m•' Mg. . ; Nig F` -:Fe -t. , Al' Mn. ..• Cu - Zn - NH4-N No3-N o
X x X X x X x X X X X X X X x
F .�.' r+ y S: ,r 4 , 'k'�'�IkY1 i �a'�, �„+- .X S rV 03''Vieri. tfr`.'rr , -
ea Y1.i;N p, 'i AS $sr� p 1_ I .S$1 AbrE6N :Mo.a 'CI` , B -Be : j w
X x x x x x x x x x x
. :s040 :::. ,:4 1sb1 aI : 17 r ,4 s valliP . 3 lI
_ ��~�..� `' ��i!� � �.� •� �•.� � � �,soLK': co��: wlr� :sfl>,s,
SOL NA . 08, °?SPAR-1 wi , i#21:u #$fei le0 sio9010, Si:Yilr ip) tCO3F, *cos-, l'higoIii; c,N .p ',IOC. K Eni► r!
I p2O, N#.X � . e,t -AlYY ! _. . :� MO$JUF& --4 . MI' -$E 2 ''lrc i' 3 iCR .
State Certification Needed: NORTH CAROLINA Vt,PS IN) 41 W °
Special instructions or Remarks Comments

City of Monroe
Reports of Lab
Analysis
2nd Quarter

s YY�
Waypoint. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
4/9/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 21-096-0004
Project Description: RAS
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s)on 4/6/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012)and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
�Qq/r c Plc 6-rawr
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 5

W
Waypoint, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-096-0004
Client Project Description: RAS
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
75756 RAS Solids 04/05/2021 04/06/2021 SM-2540G WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN, Memphis,TN
Page 2 of 5

VvYY•
/ la4rpoIflt
a, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project RAS
Ken Morris Report Date : 04/09/2021
775 Treeway Dr Information : Received :04/06/2021
Monroe, NC 28110
?asvrc pi; Gtowr.
Pauric Mc Groary Ph.D.,CPA
Report Number:21-096-0004 REPORT OF ANALYSIS Agronomist
Lab No : 75756 Matrix: Solids
Sample ID:RAS Sampled: 4/5/2021 0:00
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Total Solids 1.59 % 0.010 1 04/07/21 16:43 FMM SM-2540G
Total Volatile Solids 73.0 % 0.010 1 04/07/21 15:43 FMM SM-2540G
Analytical Method: SM-2540G
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Moisture 98,4 % 0.010 1 04/07/21 16:43 FMM L545979
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 3 of 5

,Ao
w YY
Waypoi nt.. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalyticai.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-096-0004
Shipping Method
O Fed Ex O US Postal O Lab 0 Other :
• UPS 0 Client 0 Courier Thermometer ID: I
Shipping container/cooler uncompromised? 0Yes 0 No
Number of coolers/boxes received 11
Custody seals intact on shipping container/cooler? 0 Yes 0 No • Not Present
Custody seals intact on sample bottles? 0 Yes 0 No • Not Present
Chain of Custody(COC) present? Yes 0 No
COC agrees with sample label(s)? Yes 0 No
COC properly completed • Yes 0 No
Samples in proper containers? • Yes O No
Sample containers intact? • Yes 0 No
Sufficient sample volume for indicated test(s)? • Yes 0 No
All samples received within holding time? • Yes 0 No
Cooler temperature in compliance? • Yes 0 No
Cooler/Samples arrived at the laboratory on ice. • Yes O No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No • N/A
Water- VOA vials free of headspace 0 Yes 0 No • N/A
Trip Blanks received with VOAs 0 Yes 0 No • N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No • N/A
High concentration container(48 hr) r Low concentration EnCore samplers (48 hr)
r High concentration pre-weighed (methanol -14 d) r Low conc pre-weighed vials (Sod Bis-14 d)
Special precautions or instructions included? 0 Yes • No
Comments:
Signature: Samantha Clarke Date &Time: 04/06/2021 10:47:58
Page 4 of 5

SAMPLE TR !IJ!IIIl1IIIIi1fftIIIIllillH 0004 ;TODY
Agilt 10 47 45
7621
Office Information
Rept# - Submitted By Charge To Copy To Project
Kz p4 v-e• -1. _ City of Monroe L
Acct# POB 69 Email
46205 Monroe NC 28111 kwt r
Lab Number(Lab Use Only) Sample ID Container Type _Sampled Date: Date Recd:
�{ - ,� 5 Glass (Y•ee-or 10 . Sampled Time: Time Recd:
131 1 Plastic 4,117.11 Sampled By: K<.v, M o r r;.5 Recd By:
Relinquished By: (Signature) Date Time Received By: (Signature) Date Time
mac_ t hAPE OS 1-4.�g Li-U•11 q Iron nil
Please Place a "X" by Desired Tests Internal Lab Code:
Ln
Solids % TKN P K S Ca Mg [ Na Fe Al Mn Cu Zn NH4-N NO3-N w
xA o
CaCO3 Volatile rn
Cd Cr Ni Pb As Hg _ Se pH Eq. % Solids % Org-N Mo Cl Ba I Bio
w
X
SO4 Ag Sb Co Sn Ti V Be ALK SS Avail P Sol K Cond 'I WIN , SOL B I
I SOL NA O&G SP.GR. TSS Sieve#20 Sieve#60 Sieve#100' ASH CaO - CaCO3 . MgCO3 MgO - CIN TOC Env I
TOTAL TOTAL REACT
P205 K20 TN TKNW NH4W NO3W ORGN W-PA CERT AZ CERT BTU PCBS CN FECAL TCLP 1CR
State Certification Needed: NORTH CAROLINA W
Special Instructions or Remarks Comments
JtcL l[ O) 1 t) ° ,S/VZ,lti

w°
Waypoint, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
4/14/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 21-096-0003
Project Description: WWTP Cake
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/6/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
1444/11 G/aaer
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

wWaypoint .
7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-096-0003
Client Project Description: WWTP Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
75755 WWTP Cake Solids 04/05/2021 09:30 04/06/2021
75755 WWTP Cake Solids 04/05/2021 09:30 04/06/2021 SM-4500-NI3C WP MTN
75755 WWTP Cake Solids 04/05/2021 09:30 04/06/2021 9045D WP MTN
75755 WWTP Cake Solids 04/05/2021 09:30 04/06/2021 4500NO3F-2011 WP MTN
75755 WWTP Cake Solids 04/05/2021 09:30 04/06/2021 6010D WP MTN
75755 WWTP Cake Solids 04/05/2021 09:30 04/06/2021 SW-7471B WP MTN
75755 WWTP Cake Solids 04/05/2021 09:30 04/06/2021 SM-4500-NH3C-TKN WP MTN
75755 WWTP Cake Solids 04/05/2021 09:30 04/06/2021 SM-2540G WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN, Memphis,TN
Page 2 of 6

r■Q
Waypoint 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalyticaicom
46205
City of Monroe Project WWTP Cake
Ken Morris Report Date : 04/14/2021
775 Treeway Dr Information : Received : 04/06/2021
Monroe, NC 28110 y�
Tixrrc PI 6rrod0
Pauric Mc Groary Ph.D.,CPA
Report Number:21-096-0003 REPORT OF ANALYSIS
Agronomist
Lab No: 75755 Matrix: Solids
Sample ID :WWTP Cake Sampled: 4/5/2021 9:30
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Total Solids 16.6 % 0.010 1 04/08/21 16:36 FMM SM-2540G
Total Kjeldahl Nitrogen 51900 mg/Kg-dry 1510 1 04/13/21 10:00 JPJ ;M-4500-NH3C-TKP
Phosphorus 24000 mg/Kg-dry 30.1 1 04/09/21 19:52 TJS 6010D
Potassium 2010 mg/Kg-dry 60.2 1 04/13/21 12:03 TJS 6010D
Sulfur 11400 mg/Kg-dry 60.2 1 04/09/21 19:52 TJS 6010D
Calcium 18300 mg/Kg-dry 301 1 04/09/21 19:52 TJS 6010D
Magnesium 2540 mg/Kg-dry 30,1 1 04/09/21 19:52 TJS 6010D
Sodium 651 mg/Kg-dry 151 1 04/09/21 19:52 TJS 6010D
Iron 62000 mg/Kg-dry 301 5 04/12/21 22:40 JTR 6010D
Manganese 1780 mg/Kg-dry 3.01 1 04/09/21 19:52 TJS 6010D
Copper 383 mg/Kg-dry 3.01 1 04/09/21 19:52 TJS 6010D
Zinc 1090 mg/Kg-dry 7,53 1 04/09/21 19:52 TJS 6010D
Organic N 48700 mg/Kg-dry 1510 1 04/13/21 10:00 CALCULATION
Nitrate+Nitrite-N 65,7 mg/Kg-dry 29.0 1 04/08/21 15:09 ZBD 4500NO3F-2011
Nickel 77,1 mg/Kg-dry 1.51 1 04/09/21 19:52 TJS 6010D
Mercury 0.489 mg/Kg-dry 0.0885 1 04/09/21 12:10 DDB SW-7471B
Selenium 5.00 mg/Kg-dry 3.01 1 04/09/21 19:52 TJS 6010D
pH 6.6 s.u. 1 04/13/21 15:59 CxC 9045D
Total Volatile Solids 58.1 % 0.010 1 04/08/21 16:36 FMM SM-2540G
Qualifiers/ * Outside QC Limit B Analyte detected in blank
Definitions C GCMS Confirmation Analysis E Result above cal range
g GGA Outside QC Limits H Beyond holding time
J Estimated value M Minimum value
NA Not on Scope of Accreditation NC Not confirmed
Q RPD>40%dual column results T Sample exhibits toxicity
U Unconfirmed Refer to cover letter.
Page 3 of 6

YYw,
•
Waypo I nt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanaiytical.com
46205
City of Monroe Project WWTP Cake
Ken Morris Report Date : 04/14/2021
775 Treeway Dr Information : Received :04/06/2021
Monroe, NC 28110
I eft Pit GlOar
Pauric Mc Groary Ph.D.,CPA
Report Number:21-096-0003 REPORT OFANALYSIS Agronomist
Lab No: 75755 Matrix: Solids
Sample ID :WWTP Cake Sampled: 4/5/2021 9:30
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Ammonia Nitrogen 3280 mg/Kg-dry 602 1 04/13/21 15:00 JPJ SM-4500-NH3C
Aluminum 15400 mg/Kg-dry 30.1 1 04/09/21 19:52 TJS 6010D
Arsenic 12.0 mg/Kg-dry 3.01 1 04/09/21 19:52 TJS 6010D
Cadmium 1.16 mg/Kg-dry 0.602 1 04/09/21 19:52 TJS 6010D
Chromium 74.7 mg/Kg-dry 1.51 1 04/09/21 19:52 TJS 6010D
Lead 22.7 mg/Kg-dry 1.81 1 04/09/21 19:52 TJS 6010D
Molybdenum 18.1 mg/Kg-dry 1.51 1 04/09/21 19:52 TJS 6010D
Analytical Method: SM-2540G
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Moisture 83.4 % 0.010 1 04/08/21 16:36 FMM L546224
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 4 of 6

•
Q
W YPOI lit , 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanaiyticai.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-096-0003
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
• UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? Yes 0 No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No • Not Present
Custody seals intact on sample bottles? 0 Yes 0 No • Not Present
Chain of Custody(COC) present? 0 Yes 0 No
COC agrees with sample label(s)? • Yes 0 No
COC properly completed • Yes 0 No
Samples in proper containers? • Yes 0 No
Sample containers intact? 0Yes 0 No
Sufficient sample volume for indicated test(s)? Yes 0 No
All samples received within holding time? • Yes 0 No
Cooler temperature in compliance? • Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No • N/A
Water-VOA vials free of headspace O Yes 0 No • N/A
Trip Blanks received with VOAs 0 Yes 0 No • N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No • N/A
r High concentration container(48 hr) r Low concentration EnCore samplers (48 hr)
r High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis-14 d)
Special precautions or instructions included? 0 Yes • No
Comments:
Signature: Samantha Clarke Date&Time: 04/06/2021 10:46:59
Page 5 of 6

SAMPLE T- - }} 21 USTODY
1UII111I1 p 3021 AI
L
7( City d Nbnroe
W WTP Cake115 q,
Office Information
Rept# 4t'bmittedB .,,,a'ye to Copy To Project
ke" /Awer.5 City of Monroe
• Acct# _ POB 69 Email
46205 Monroe NC 28111 key,.0 -r;yereletQe,e0.,-AC,, rt9
Lab Number(Lab Use Only) Sample ID Container Type Sampled Date: A y ..5.1 i Date Recd:
Glass (ies oil j Sampled Time: i; 3 Time Recd:
1 �'{
l 5 w WTP Cake Plastic Cf9sor Ple) 'Sampled By: K M„r -, Recd By:
Relinquished By: (Signature) Date Time Received By: (Signature) Date Time
UkE %iNhitAOtiABizi, loD. 4. (0•21 pit_Qryi
Please Place a "X" by Desired Tests I Internal Lab Code: SLMONR
S;,lIlds'Ye -TKN P -K =::5 Ca Mg Na Fe Al Mn. Cu Zn NH4-N NO3-N w
X X X X x X X X X X x X x x x
,:•, =: V- _ - CaCO3 Volatile _ a,
ET
Ted Cr Ni Pb As Hg Se pH Eq. % Solids% • Org-N Mo CI '::B Ba . w
x x x x x x x x x x X
1SO4 Ag Sb ' Co Sn y TI - V Be ALK` ' SS ;' Avail.P' -;Sol K Cond WIN:: •.SOL"B
1 Si)LNA O&G ,SP.GR. - TSS Sieve##20 Sleve#80 Slevs#100- ASH CaO CaCO3 MgCO3. Mg0 C/N. . TOC:. Env
TOTAL TOTAL REACT
Nos K2O TN TKNW NH4W . NO3W ORGN-W PA CERT AZ CERT BTU PCBS CN FECAL TCLP ICR
-
State Certification Needed: NORTH CAROLINA
Special Instructions or Remarks Comments

Waypoint 7621 Whitepine Road,Richmond,VA23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
4/14/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 21-096-0002
Project Description: WTP Ferric Cake
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s)on 4/6/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Tpzyic (rl� &Ivor-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

w•
WaypOl nt 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-096-0002
Client Project Description: WTP Ferric Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
75754 WTP Ferric Cake Solids 04/05/2021 09:15 04/06/2021
75754 WTP Ferric Cake Solids 04/05/2021 09:15 04/06/2021 SM-4500-NH3C WP MTN
75754 WTP Ferric Cake Solids 04/05/2021 09:15 04/06/2021 9045D WP MTN
75754 WTP Ferric Cake Solids 04/05/2021 09:15 04/06/2021 4500NO3F-2011 WP MTN
75754 WTP Ferric Cake Solids 04/05/2021 09:15 04/06/2021 6010D WP MTN
75754 WTP Ferric Cake Solids 04/05/2021 09:15 04/06/2021 SW-7471B WP MTN
75754 WTP Ferric Cake Solids 04/05/2021 09:15 04/06/2021 SM-4500-NH3C-TKN WP MTN
75754 WTP Ferric Cake Solids 04/05/2021 09:15 04/06/2021 SM-2540G WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN, Memphis,TN
Page 2 of 9

WaypOi nt 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project WTP Ferric Cake
Ken Morris Report Date : 04/14/2021
775 Treeway Dr Information : Received : 04/06/2021
Monroe, NC 28110 {{}} rr�
1AwlZ plc 6„,i,r
Report Number:21-096-0002 REPORT OFANALYSIS Pauric Mc Groary Ph.D.,CPA
Agronomist
Lab No : 75754 Matrix: Solids
Sample ID:WTP Ferric Cake Sampled: 4/5/2021 9:15
Test Results Units MOL DF Date I Time By Analytical
Analyzed Method
Total Solids 29.4 °A) 0,010 1 04/08/21 16:36 FMM SM-2540G
Total Kjeldahl Nitrogen 17300 mg/Kg-dry 850 1 04/13/21 10:00 JPJ ;M-4500-NH3C-TKP
Phosphorus 2970 mg/Kg-dry 85.0 5 04/09/21 16:51 TJS 6010D
Potassium 243 mg/Kg-dry 170 5 04/09/21 16:51 TJS 6010D
Sulfur 2690 mg/Kg-dry 170 5 04/09/21 16:51 TJS 6010D
Calcium 1660 mg/Kg-dry 850 5 04/09/21 16:51 TJS 6010D
Magnesium 408 mg/Kg-dry 85,0 5 04/09/21 15:51 TJS 6010D
Sodium <425 mg/Kg-dry 425 5 04/09/21 16:51 TJS 6010D
Iron 354000 mg/Kg-dry 680 20 04/12/21 19:26 JTR 6010D
Manganese 524 mg/Kg-dry 8.50 5 04/09/21 16:51 TJS 6010D
Copper 473 mg/Kg-dry 8.50 5 04/09/21 16:51 TJ5 6010D
Zinc 74.5 mg/Kg-dry 21.3 5 04/09/21 16:51 TJS 6010D
Organic N 16800 mg/Kg-dry 850 1 04/13/21 10:00 CALCULATION
Nitrate+Nitrite-N 54.8 mg/Kg-dry 17.0 1 04/08/21 15:08 ZBD 4500NO3F-2011
Nickel 35.0 mg/Kg-dry 4.25 5 04/09/21 16:51 TJS 6010D
Mercury 0.0479 mg/Kg-dry 0.0476 1 04/09/21 12:09 DDB SW-7471B
Selenium <8.50 mg/Kg-dry 8.50 5 04/09/21 16:51 TJS 6010D
pH 5.2 s.u. 1 04/13/21 15:59 CxC 9045D
Total Volatile Solids 32.8 °A° 0.010 1 04/08/21 16:36 FMM SM-2540G
Qualifiers/ * Outside QC Limit B Analyte detected in blank
Definitions C GCMS Confirmation Analysis E Result above cal range
g GGA Outside QC Limits H Beyond holding time
J Estimated value M Minimum value
NA Not on Scope of Accreditation NC Not confirmed
Q RPD>40%dual column results T Sample exhibits toxicity
U Unconfirmed Refer to cover letter.
Page 3 of 9

w
Waypoint 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanaiytical.com
46205
City of Monroe Project WTP Ferric Cake
Ken Morris Report Date : 04/14/2021
775 Treeway Dr Information : Received :04/06/2021
Monroe, NC 28110
tAw c M; 6,teaiq/
Pauric Mc Groary Ph.D.,CPA
Report Number:21-096-0002 REPORT OF ANALYSIS
Agronomist
Lab No : 75754 Matrix: Solids
Sample ID:WTP Ferric Cake Sampled: 4/5/2021 9:15
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Ammonia Nitrogen 473 mg/Kg-dry 340 1 04/13/21 15:00 JPJ SM-4500-NH3C
Aluminum 7210 mg/Kg-dry 85.0 5 04/09/21 16:51 TJS 6010D
Arsenic 27.1 mg/Kg-dry 8.50 5 04/09/21 16:51 TJS 6010D
Cadmium 2.58 mg/Kg-dry 1.70 5 04/09/21 16:51 TJS 6010D
Chromium 236 mg/Kg-dry 4.25 5 04/09/21 16:51 TJS 6010D
Lead <5.10 mg/Kg-dry 5.10 5 04/09/21 15:51 TJS 6010D
Molybdenum 58.2 mg/Kg-dry 4.25 5 04/09/21 16:51 TJS 6010D
Analytical Method: SM-2540G
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Moisture 70.6 % 0.010 1 04/08/21 16:36 FMM L546224
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 4 of 9

YY
Waypoi lit 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalyticaicom
Client: City of Monroe CASE NARRATIVE
Project: WTP Ferric Cake
Lab Report Number: 21-096-0002
Date: 4/13/2021
Metals Analysis Method 6010D
Sample 75754 (WTP Ferric Cake)
Analyte:Aluminum
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to !EC interference/matrix interference.
Analyte:Aluminum
QC Batch No: L546572/L546032
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte:Arsenic
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte:Arsenic
QC Batch No: L546572/L546032
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Calcium
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Cadmium
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Chromium
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Copper
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Iron
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Iron
QC Batch No: L546875/L546032
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 9

Waypoint ■■Q
7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Analyte: Potassium
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Potassium
QC Batch No: L546572/L546032
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Magnesium
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Manganese
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Manganese
QC Batch No: L546572/L546032
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Molybdenum
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Sodium
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Nickel
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Phosphorus
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Lead
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Sulfur
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Selenium
QC Batch No: L546342/L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Selenium
Page 6 of 9

�Ao
YY
Waypoi nt 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanaiyticai.com
QC Batch No: L546572/L546032
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges.A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Zinc
QC Batch No: L5463421L546032
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 7 of 9

•
p
Waypoi nt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-096-0002
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
• UPS 0 Client 0 Courier Thermometer ID: I
Shipping container/cooler uncompromised? • Yes 0 No
Number of coolers/boxes received r--- 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No • Not Present
Custody seals intact on sample bottles? 0 Yes 0 No • Not Present
Chain of Custody(COC) present? • Yes 0 No
COC agrees with sample label(s)? • Yes 0 No
COC properly completed Yes 0 No
Samples in proper containers? • Yes 0 No
Sample containers intact? • Yes 0 No
Sufficient sample volume for indicated test(s)? • Yes 0 No
All samples received within holding time? • Yes 0 No
Cooler temperature in compliance? • Yes O No
Cooler/Samples arrived at the laboratory on ice. • Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water-Sample containers properly preserved 0 Yes 0 No • N/A
Water- VOA vials free of headspace 0 Yes O No • N/A
Trip Blanks received with VOAs 0 Yes 0 No • N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No • N/A
High concentration container(48 hr) 7 Low concentration EnCore samplers (48 hr)
( High concentration pre-weighed (methanol -14 d) r Low conc pre-weighed vials (Sod Bis-14 d)
Special precautions or instructions included? 0 Yes • No
Comments:
Signature: Samantha Clarke Date&Time: 04/06/2021 10:44:47
Page 8 of 9

,00608
SAMPLE ' !` l' 11 111 111 111 z
City of Maneoe L1 S i OD Ir
WTP Ferns Cake A -,1‘\,
76 __...... .,uu .:i.3237 Tel: [phone]
Office information Customer Information
Rept# Submitted By I ChargeTo _
Ka.4 /At,rrTS City of onroe Copy To Project
Acct# FOB 69
Email
46205 Monroe NC 28111 14rn0eri›@mar.ra:inc. 't
Lab Number(Lab Use Only) Sample ID Container Type Sampled Date: 4/-.-a f Date Reed:
-7 51 514 �4'TP Ferric Cake AGlass ( orb Sampled Time: :,a Time Reed:
Plastic or Me) Sampled By: p.Q,,., Mo r r,s Reed By:
Relinquished By: (Signature) Date Time Received By: (Signature) Date Time
„ AMf1gY2ta) cfrOlAkt. 'i-lo• i 11,Moging
Please Place a "X" by Desired Tests i Interval Lab Code: SLMONR
r4 7, i,p K1 _ 'S_. :;:t-Ca! Mg ..°> Nay .,FB .. AI -v- Mn. Cu. Zn .. ' NH4•N NO3-N o
X X x X X X X X X X _ X X X X X
01
Z , �R 1/40 i s +- f � ,0. �' ~}...,, ws'yei^ ,., ie f, Y COJt ti %
' V. ..,
‘ gavok. q .-brg-N* MO:< CI B
�
X X X X X x X X X X
r
I :S '71'g .. 1;Sb4' 4,'.C$f ` h . . TI :e_`MY ' _-'~:Bo . s E: AMK ? SSi i valltP sSoI K• Coig: } ;WIN K SOL B
Sol:NA Wax t.SP.GR.i' . SS-..- sla*ti#201ISiI Bo'Sle#0.100 +MASH L. •I Cao.2 taCO3�• MgCO3 „'MgO 2! ON TOC . , Env
4cti .,.�;s;� f�'�M6,y ' F 1 I.,,:_
,_Siii....- -a a t� -� ;„iiiitscAttil tii •2.07,1.4
. ,1 C ads _�_ t
AL
State Certification Needed: NORTH CAROLINA
Special Instructions or Remarks Comments
ACC i r.Of L 1n° .DWYK`,
ir COO 142,11 PWArn 14

City of Monroe
Reports of Lab
Analysis
3rd Quarter

w°
Waypoint 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
7/13/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 21-189-0006
Project Description: RAS
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s) on 7/8/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Ti144irc (f)t (y(0c '
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 5

w
d1aypO I nt 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-189-0006
Client Project Description: RAS
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
76971 RAS Solids 07/06/2021 09:55 07/06/2021 SM-2540G WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN, Memphis,TN
Page 2 of 5

o
Waypo i nt 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project RAS
Ken Morris Report Date: 07/13/2021
775 Treeway Dr Information : Received :07/08/2021
Monroe, NC 28110
l awrc Plc Gorier
Pauric Mc Groary Ph.D.,CPA
Report Number:21-189-0006 REPORT OF ANALYSIS Agronomist
Lab No: 76971 Matrix: Solids
Sample ID : RAS Sampled: 7/6/2021 9:55
Test Results Units MQL DF Date I Time By Analytical
Analyzed Method
Total Solids 1.46 % 0.010 1 07/09/21 15:48 FMM SM-2540G
Total Volatile Solids 69.8 % 0.010 1 07/09/21 15:48 FMM SM-2540G
Analytical Method: SM-2540G
Test Results Units MQL DF Date 1 Time By Analytical
Analyzed Batch
Moisture 98.5 % 0.010 1 07/09/21 15:48 FMM L562991
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 3 of 5

•
�p
Waypoi lit 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalyticai.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-189-0006
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: I
Shipping container/cooler uncompromised? # Yes 0 No
Number of coolers/boxes received 11
Custody seals intact on shipping container/cooler? Q Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No # Not Present
Chain of Custody(COC) present? 0 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COG properly completed 0 Yes 0 No
Samples in proper containers? 0 Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? j Yes 0 No
Cooler temperature in compliance? # Yes Q No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved 0 Yes 0 No 0 N/A
Water- VOA vials free of headspace 0 Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No 0 N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A
r High concentration container (48 hr) r Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) r Low conc pre-weighed vials (Sod Bis-14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Brandi Watson J Date&Time: 07/08/2021 09:31:08
Page 4 of 5

(P
W WASTEWATER SAMPLE 'USTODY Account#
II I 21.189-0006
07zos
City of ltAo�ece `"�07-08-2021 4k, 0 S
7621 Whitepine Road Richmond VA 23237 Tel RAS 09.30.39 lical.com
C
�/ y�Submitted By Charge To Copy To
T-,ZvA MaY (•S C;. I o Mores.4e
.--P— mo,x (A g
I•\o ryr».L N c.- ,Q V i 1 I
Project Phone:0,3,1) 3tc 1 - (oe 3 5 Fax: E-mail: •
`` KrvAryrr.}E2r-.orir4 . /lc • `'')
Sample Information
Lab Number Collection Information Container Information Please Write in Desired Tests
Sample ID (Lab Use
Only) Type Date Time Number Type Volume
of Bottles
�J� '---(--Grab _Glass Oi
fi+.�'�S /1� l�/1�\ Composite r�_ _,3i .�; j'j 1 X Plastic _pint
qt
_Grab _Glass -- oz.
—Composite Plastic _pint o
in
qt
_Grab Glass — °Z
—Composite ___..Plastic _pmt rn
gt W
Grab Glass oz
Composite —Plastic _p'ni
_ _ of
Relinquished By:(Signature) Date Time Received By:(Signature) Dale Time
/Vt 7-4-..AI )e,c.5
Test Available Special Instructions or Remarks
Nitrogen Series:Total Kjeldahl,Ammonium,Nitrate&Organic Nitrogen.
Phosphorus(total,orthor), Poatssium,Sulfate-Sulfur, Calcium,Magnesium,Sodium,Iron,Aluminum,
Manganese,Copper,Zinc,Arsenic,Barium,Cadmium, Chromium, Cobalt, Molybdenum,Mercury,Lead,
Selenium, Silver. Nickel.Acidity(Total),Alkalinity(Total), Biochemical Oxygen Demand(5 days),Boron,
Chemical Oxygen Demand, Chloride,Conductance(Specific), Hexavalent Chromium, Oil and Grease(EPA),
pH, Phenol,Solids(Dissolved,Suspended,Total,Volatile)

'Ao
Waypoint- YY 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
7/19/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 21-189-0005
Project Description: WWTP Cake
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s)on 7/8/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
4gq/ic 6•07wr
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option,repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

YYw
Waypoint, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.corn
Sample Summary Table
Report Number: 21-189-0005
Client Project Description: WWTP Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
76970 WWTP Cake Solids 07/06/2021 09:40 07/08/2021
76970 WWTP Cake Solids 07/06/2021 09:40 07/08/2021 SM-4500-NH3C WP MTN
76970 WWTP Cake Solids 07/06/2021 09:40 07/08/2021 9045D WP MTN
76970 WWTP Cake Solids 07/06/2021 09:40 07/08/2021 4500NO3F-2011 WP MTN
76970 WWTP Cake Solids 07/06/2021 09:40 07/08/2021 6010D WP MTN
76970 WWTP Cake Solids 07/06/2021 09:40 07/08/2021 SW-7471B WP MTN
76970 WWTP Cake Solids 07/06/2021 09:40 07/08/2021 SM-4500-NH3C-TKN WP MTN
76970 WWTP Cake Solids 07/06/2021 09:40 07/08/2021 SM-2540G WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN, Memphis,TN
Page 2 of 6

wWaypoint, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project WWTP Cake
Ken Morris Report Date: 07/19/2021
775 Treeway Dr Information : Received :07/08/2021
Monroe, NC 28110
1)ouurc Mc Grow/
Pauric Mc Groary Ph.D.,CPA
Report Number:21-189-0005 REPORT OF ANALYSIS Agronomist
Lab No: 76970 Matrix: Solids
Sample ID :WWTP Cake Sampled: 7/6/2021 9:40
Test Results Units MQL DF Date I Time By Analytical
Analyzed Method
Total Solids 23.0 % 0.010 1 07/09/21 15:48 FMM SM-2540G
Total Kjeldahl Nitrogen 35000 mg/Kg-dry 1090 1 07/14/21 11:00 JP) ;M-4500-NH3C TKO
Phosphorus 19300 mg/Kg-dry 21.7 1 07/13/21 22:09 DADS 6010D
Potassium 1540 mg/Kg-dry 217 5 07/15/21 22:30 DADS 6010D
Sulfur 8520 mg/Kg-dry 43.5 1 07/13/21 22:09 DADS 6010D
Calcium 13800 mg/Kg-dry 217 1 07/13/21 22:09 ]ADS 6010D
Magnesium 2110 mg/Kg-dry 21.7 1 07/13/21 22:09 ]ADS 6010D
Sodium 709 mg/Kg-dry 109 1 07/13/21 22:09 DADS 6010D
Iron 92600 mg/Kg-dry 217 5 07/14/21 22:58 DADS 6010D
Manganese 1520 mg/Kg-dry 2.17 1 07/13/21 22:09 JADS 6010D
Copper 400 mg/Kg-dry 2.17 1 07/13/21 22:09 DADS 6010D
Zinc $35 mg/Kg-dry 5.43 1 07/13/21 22:09 DADS 6010D
Organic N 31570 mg/Kg-dry 1087 1 07/14/21 11:00 CALCULATION
Nitrate+Nitrite-N 386 mg/Kg-dry 21.2 1 07/14/21 14:53 ZBD 4500NO3F-2011
Nickel 50.0 mg/Kg-dry 1.09 1 07/13/21 22:09 JADS 6010D
Mercury 0.370 mg/Kg-dry 0.0673 1 07/14/21 15:23 TJS SW-7471B
Selenium <2.17 mg/Kg-dry 2.17 1 07/13/21 22:09 DADS 6010D
pH 7.0 s.u. 1 07/13/21 15:06 DRS 9045D
Total Volatile Solids 52.6 % 0.010 1 07/09/21 15:48 FMM SM-2540G
Qualifiers/ * Outside QC Limit B Analyte detected in blank
Definitions C GCMS Confirmation Analysis E Result above cal range
g GGA Outside QC Limits H Beyond holding time
J Estimated value M Minimum value
NA Not on Scope of Accreditation NC Not confirmed
Q RPD >40%dual column results T Sample exhibits toxicity
U Unconfirmed ti Refer to cover letter.
Page 3 of 6

w•
Waypo I nt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project WWTP Cake
Ken Morris Report Date: 07/19/2021
775 Treeway Dr Information : Received : 07/08/2021
Monroe, NC 28110 T*W C 141 61447
/
Pauric Mc Groary Ph.D.,CPA
Report Number:21-189-0005 REPORT OF ANALYSIS
Agronomist
Lab No: 76970 Matrix: Solids
Sample ID:WWTP Cake Sampled: 7/6/2021 9:40
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Ammonia Nitrogen 3470 mg/Kg-dry 435 1 07/14/21 15:30 JP] SM-4500-NH3C
Aluminum 12600 mg/Kg-dry 21.7 1 07/13/21 22:09 ]ADS 6010D
Arsenic 9.48 mg/Kg-dry 2.17 1 07/13/21 22:09 ]ADS 6010D
Cadmium 2.91 mg/Kg-dry 0.435 1 07/13/21 22:09 ]ADS 6010D
Chromium 87.0 mg/Kg-dry 1.09 1 07/13/21 22:09 JADS 6010D
Lead 16.1 mg/Kg-dry 1.30 1 07/13/21 22:09 JADS 6010D
Molybdenum 20.2 mg/Kg-dry 1.09 1 07/13/21 22:09 ]ADS 6010D
Analytical Method: SM-2540G
Test Results Units MIL DF Date/Time By Analytical
Analyzed Batch
Moisture 77.0 % 0.010 1 07/09/21 15:48 FMM L562991
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 4 of 6

•
Wapo I lit., 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanaiytical.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-189-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
13 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? 3 Yes 0 No
Number of coolers/boxes received 11
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody(COC) present? 13 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? 13 Yes 0 No
Sample containers intact? 0 Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 13 Yes 0 No
Cooler temperature in compliance? 13 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 13 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water-Sample containers properly preserved 0 Yes 0 No 0 N/A
Water- VOA vials free of headspace 0 Yes 0 No 13 N/A
Trip Blanks received with VOAs 0 Yes 0 No 13 N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No 0 N/A
r High concentration container(48 hr) 7 Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis-14 d)
Special precautions or instructions included? O Yes 13 No
Comments:
Signature: Brandi Watson Date&Time: 07/08/2021 09:29:53
Page 5 of 6

Icy
WASTEWATER SAMPLE TRANS
ly Account#W Waypoint 1111111111111111111113110 4 Z/(,:z o
7621 Whitepine Road Richmond VA 23237 Tel:[phone] City of Monroe 09.27 43
WTP Ferric Cake
Customer Info'
Submitted By Mil Mfb� ,.,
hQ.t^ f tO y,5 c,..ty
O} Nta yAirat 1111111111011111111111111111
City of Monroe 21-189-0005
C J K 1 WWTPCake 09:29:37
-
Project Phone: 0. q) -34r 1 - (4;,-3 5 Fax: E-mail:
k,�o e✓•i C?Wt, (&"JIc n c , *fit
Sample Information
Lab Number Collection Information Container Information Please Write in Desired Tests
Sample ID (Lab Use
Only) Type Date Time NumberType Volume
`IL Grab °Z
of Bottles
T 14 f� irk�I� _Glass — -
'j
`�e —Composite ✓�-{,,.-,2 l L3= a r� I - Plastic pint
qt
5 vJVktTi? K Grab Glass oZ
C.C4-,� —Composite 1-4,- a t 9 ; ;.> (
Plastic - prnt
qt o
`o
Grab _Glass — oZ
—Composite' w Plastic q pint ro
Grab Glass -- oz -
Composite Plastic pint
�
4t
Relinquished By:(Signature) Date Time Received By:(Signature) Date Time
• ,e.4,\_ Wlvti 7-4 at l '
Test Available Special Instructions or Remarks
Nitrogen Series:Total Kjeldahl,Ammonium,Nitrate&Organic Nitrogen.
Phosphorus(total,orthor), Poatssium,Sulfate-Sulfur,Calcium, Magnesium,Sodium, Iron,Aluminum,
Manganese, Copper,Zinc,Arsenic, Barium,Cadmium,Chromium, Cobalt,Molybdenum,Mercury,Lead,
Selenium,Silver.Nickel.Acidity(Total),Alkalinity(Total),Biochemical Oxygen Demand(5 days).Boron,
Chemical Oxygen Demand, Chloride,Conductance(Specific), Hexavalent Chromium, Oil and Grease(EPA),
pH. Phenol,Solids(Dissolved,Suspended,Total,Volatile)

w°
Waypoint_ 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
7/19/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 21-189-0004
Project Description: WTP Ferric Cake
Dear Ken Morris:
Waypoint Analytical Virginia, inc. received sample(s) on 7/8/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters(NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012)and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
6Yo air
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

o
Waypoint, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-189-0004
Client Project Description: WTP Ferric Cake
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
76969 WTP Ferric Cake Solids 07/06/2021 09:25 07/08/2021
76969 WTP Ferric Cake Solids 07/06/2021 09:25 07/08/2021 SM-4500-NH3C WP MTN
76969 WTP Ferric Cake Solids 07/06/2021 09:25 07/08/2021 9045D WP MTN
76969 WTP Ferric Cake Solids 07/06/2021 09:25 07/08/2021 4500NO3F-2011 WP MTN
76969 WTP Ferric Cake Solids 07/06/2021 09:25 07/08/2021 6010D WP MTN
76969 WTP Ferric Cake Solids 07/06/2021 09:25 07/08/2021 SW-7471B WP MTN
76969 WTP Ferric Cake Solids 07/06/2021 09:25 07/08/2021 SM-4500-NH3C-TKN WP MTN
76969 WTP Ferric Cake Solids 07/06/2021 09:25 07/08/2021 SM-2540G WP MTN
WP MTN -Memphis,TN: Waypoint Analytical-TN, Memphis,TN
Page 2 of 8

w
YY
Waypoi nt 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project WTP Ferric Cake
Ken Morris Report Date: 07/19/2021
775 Treeway Dr Information : Received :07/08/2021
Monroe, NC 28110
twice Mc brae/
Pauric Mc Groary Ph.D.,CPA
Report Number:21-189-0004 REPORT OF ANALYSIS Agronomist
Lab No: 76969 Matrix: Solids
Sample ID:WTP Ferric Cake Sampled: 7/6/2021 9:25
Test Results Units MQL DF Date!Time By Analytical
Analyzed Method
Total Solids 32.1 % 0.010 1 07/09/21 15:48 FMM SM-2540G
Total Kjeldahl Nitrogen 14700 mg/Kg-dry 779 1 07/14/21 11:00 JPJ ;M-4500-NH3C-TKI'
Phosphorus 2260 mg/Kg-dry 77.9 5 07/14/21 22:53 JADS 6010D
Potassium 266 mg/Kg-dry 156 5 07/15/21 22:20 JADS 6010D
Sulfur 2360 mg/Kg-dry 156 5 07/14/21 22:53 JADS 6010D
Calcium 1690 mg/Kg-dry 779 5 07/14/21 22:53 JADS 6010D
Magnesium 424 mg/Kg-dry 77,9 5 07/14/21 22:53 JADS 6010D
Sodium <389 mg/Kg-dry 389 5 07/14/21 22:53 JADS 6010D
Iron 368000 mg/Kg-dry 623 20 07/15/21 22:25 JADS 6010D
Manganese 526 mg/Kg-dry 7.79 5 07/14/21 22:53 JADS 6010D
Copper 461 mg/Kg-dry 7,79 5 07/14/21 22:53 JADS 6010D
Zinc 60.7 mg/Kg-dry 19.5 5 07/14/21 22:53 JADS 6010D
Organic N 13020 mg/Kg-dry 778,8 1 07/14/21 11:00 CALCULATION
Nitrate+Nitrite-N 1150 mg/Kg-dry 14.6 1 07/14/21 14:53 ZBD 4500NO3F-2011
Nickel 27.4 mg/Kg-dry 3.89 5 07/14/21 22:53 JADS 6010D
Mercury <0,0482 mg/Kg-dry 0,0482 1 07/14/21 15:22 TJS SW-7471B
Selenium <7.79 mg/Kg-dry 7,79 5 07/14/21 22:53 JADS 6010D
pH 6.4 s.u. 1 07/13/21 15:06 DRS 9045D
Total Volatile Solids 34.8 % 0.010 1 07/09/21 15:48 FMM SM-2540G
Qualifiers/ * Outside QC Limit B Analyte detected in blank
Definitions C GCMS Confirmation Analysis E Result above cal range
g GGA Outside QC Limits H Beyond holding time
J Estimated value M Minimum value
NA Not on Scope of Accreditation NC Not confirmed
Q RPD>40%dual column results T Sample exhibits toxicity
U Unconfirmed - Refer to cover letter.
Page 3 of 8

wo
\ /aypoi nt.. 7621 White pine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project WTP Ferric Cake
Ken Morris Report Date : 07/19/2021
775 Treeway Dr Information : Received :07/08/2021
Monroe, NC 28110
Iowa pit 6,00,r-
Pauric Mc Groary Ph.D.,CPA
Report Number:21-189-0004 REPORT OF ANALYSTS Agronomist
Lab No: 76969 Matrix: Solids
Sample ID :WTP Ferric Cake Sampled: 7/6/2021 9:25
Test Results Units MOL DF Date/Time By Analytical
Analyzed Method
Ammonia Nitrogen 1650 mg/Kg-dry 312 1 07/14/21 15:30 JPJ SM-4500-NH3C
Aluminum 5230 mg/Kg-dry 77.9 5 07/14/21 22:53 DADS 6010D
Arsenic 14.0 mg/Kg-dry 7,79 5 07/14/21 22:53 DADS 6010D
Cadmium 4.02 mg/Kg-dry 1.56 5 07/14/21 22:53 DADS 6010D
Chromium 223 mg/Kg-dry 3.89 5 07/14/21 22:53 3ADS 6010D
Lead 7.38 mg/Kg -dry 4.67 5 07/14/21 22:53 JADS 6010D
Molybdenum 50.5 mg/Kg-dry 3.89 5 07/14/21 22:53 3ADS 6010D
Analytical Method: SM-2540G
Test Results Units MQL DF Date/Time By Analytical
Analyzed Batch
Moisture 67.9 % 0.010 1 07/09/21 15:48 FMM L562991
Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit
Definitions
Page 4 of 8

o
Waypoi nt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Client: City of Monroe CASE NARRATIVE
Project: WTP Ferric Cake
Lab Report Number: 21-189-0004
Date: 7/16/2021
Metals Analysis Method 6010D
Sample 76969(WTP Ferric Cake)
Analyte:Aluminum
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte:Arsenic
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Calcium
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Cadmium
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Chromium
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Copper
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Iron
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Potassium
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Magnesium
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Manganese
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Molybdenum
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 5 of 8

,AO
Waypoi nt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-4401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Analyte: Sodium
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Nickel
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Phosphorus
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Lead
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Sulfur
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Selenium
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Zinc
QC Batch No: L563653/L563100
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 6 of 8

o
•
Waypoi ft.. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-189-0004
Shipping Method
O Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: I
Shipping container/cooler uncompromised? #Yes 0 No
Number of coolers/boxes received 9 '
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody(COC) present? 0 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? 0 Yes 0 No
Sample containers intact? *Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water-Sample containers properly preserved 0 Yes 0 No 0 N/A _
Water- VOA vials free of headspace 0 Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No 0 N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No a N/A
High concentration container(48 hr) — Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Brandi Watson Date&Time: 07/08/2021 09:28:26
Page 7 of 8

Lk
W WASTEWATER SAMPLE TRANS I II!! II kY Account#
Waypom t 1111.111111111111111M III �11111111 11 o 2szo y(6 205
7621 Whitepine Road Richmond VA 23237 Tel;804-743-9401 C;iv of Monroe os 27 43
VVTP Ferric Cake
Customer Info!
gib" y�� Submitted By / ` ...r..�y� .,. 111.11111111111111111111111
t '1 e r✓y C.r r tV v- a yN�4 City of Monroe 46205
2021
g0005 i
ll�, d WWTPCake 09 29 37
fI
! lr:..'\a` (.3 N c._ Si!.,Si I r
Project Phone: -) �,;1 _ Fax:
? - ) 3 �� 3a E-mail: k✓+�o ✓.5C�yK•1.0vnc . ,.e?
Sample Information
Lab Number Collection Information Container Information Please Write in Desired Tests
Sample ID (Lab Use Number
Only) Type Date Time of Bottles Type Volume
W T ti [A �/ Grab _Glass — o,
LiW r r .r- Composite PI-L.-,� el; ,2 S ( Plastic pint
�%4'K-4- qt
5 uvwtr-t. �`� _. Grab Glass oz
V Composite �-4,- at 9 1 . .j j 7( Plastic pint
�
tit 0
Grab _Glass oZ
Composite _Plastic Finttn
. tit a
Grab Glass ---- °Z
Composite Plastic _pint
at
Relinquished By:(Signature) Date Time Received By:(Signature) Date Time
Test Available Special Instructions or Remarks
Nitrogen Series:Total Kje€dahl,Ammonium,Nitrate&Organic Nitrogen,
Phosphorus(total, orthor), Poatssium,Sulfate-Sulfur, Calcium, Magnesium,Sodium, Iron,Aluminum,
Manganese, Copper,Zinc,Arsenic, Barium,Cadmium,Chromium, Cobalt, Molybdenum, Mercury,Lead,
Selenium, Silver, Nickel.Acidity(Total), Alkalinity(Total),Biochemical Oxygen Demand(5 days), Boron,
Chemical Oxygen Demand,Chloride, Conductance(Specific), Hexavaient Chromium, Oil and Grease(EPA),
pH, Phenol, Solids(Dissolved,Suspended,Total,Volatile)

City of Monroe
Reports of Lab
Analysis
4th Quarter

,Ao
Waypoint, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
10/12/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 21-279-0008
Project Description: RAS
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received samples) on 10/6/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
1putfr'c Plc GYP(le ,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option,repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 5

w
Waypoint, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalyticaicom
Sample Summary Table
Report Number: 21-279-0008
Client Project Description: RAS
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
50036 RAS Solids 10/04/2021 09:30 10/06/2021 SM-2540G WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN, Memphis,TN
Page 2 of 5

YY
wo
•
WaypoI lit` 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project RAS
Ken Morris Report Date : 10/12/2021
775 Treeway Dr Information : Received : 10/06/2021
Monroe, NC 28110
Tait Plc G/owy/
Pauric Mc Groary Ph.D.,CPA
Report Number:21-279-0008 REPORT OF ANALYSIS Agronomist
Lab No : 50036 Matrix: Solids
Sample ID:RAS Sampled: 10/4/2021 9:30
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Moisture 98.4 % 0,010 1 10/08/21 15:50 FMM SM-2540G
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Total Volatile Solids 71.0 % 0.010 1 10/08/21 15:50 FMM SM-2540G
Total Solids 1.57 % 0.010 1 10/08/21 15:50 FMM SM-2540G
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions
Page 3 of 5

• IA?
Waypoi lit 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalyticai.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-279-0008
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
* UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? * Yes 0 No
Number of coolers/boxes received I '
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody(COC) present? ©Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed *Yes 0 No
Samples in proper containers? 0 Yes 0 No
Sample containers intact? * Yes 0 No
Sufficient sample volume for indicated test(s)? *Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water-Sample containers properly preserved 0 Yes 0 No 0 N/A
Water- VOA vials free of headspace 0 Yes 0 No * N/A
Trip Blanks received with VOAs 0 Yes 0 No © N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No Q N/A
r High concentration container(48 hr) r Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol-14 d) r Low conc pre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: Jill Mauler Date&Time: 10/06/2021 09:02:03
Page 4 of 5

o WASTEWATER SAMPLE TRA I I J flII11U f 1I 11I111I11 1 ODY Account#
Waypoi cav of Monroe 09:0o se /oa
7621 Whitepine Road Richmond VA 23237 Tel:8N-743-5
RAS ' °5
Customer.
�/ Submitted By Charge To Copy To
1 �:-yti MOYveirS C4y orM o r.,roe-
PAob.yae Oc- a3'11\
Project Phone:(i.7 ) 34 1,4tz,-3:s Fax: E-mail:
k rno r r rrt @ rAo inYae.nc. .o r1
Sample Information
Lab Number Collection Information Container Information Please Write in Desired Tests
Sample ID (Lab Use
Only) Type Date Time Number Type Volume
of Bottles
��c �� Grab _Glass — o.
7 50� Composite 0— .21 r�:3,3 1 ?C Plastic ---pint
d qt
—
,o Grab Glass °Z
iq ^ Composite Plastic —pint
0 qt
`l Grab _Glass — oz
o Composite Plastic --pint
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Composite —Plastic ----1-nt
• at
Relinquished By:(Signature) Date Time Received By:(Signature) Date Time
1- .. Yv1114.4.. f-}-y-.2I _ I o: ^
Test Available Special Instructions or Remarks
Nitrogen Series:Total Kjeldahl,Ammonium, Nitrate&Organic Nitrogen.
Phosphorus(total,orthor), Poatsslum,Sulfate-Sulfur.Calcium,Magnesium,Sodium,Iron,Aluminum.
Manganese,Copper.Zinc,Arsenic,Barium,Cadmium,Chromium,Cobalt,Molybdenum,Mercury,Lead,
Selenium,Silver.Nickel.Acidity(Total),Alkalinity(Total),Biochemical Oxygen Demand(5 days),Boron,
Chemical Oxygen Demand, Chloride,Conductance(Specific), Hexavalent Chromium,Oil and Grease(EPA),
pi-I,Phenol.Solids(Dissolved.Suspended,Total,Volatile)

Waypoint_ Y1l 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
10/14/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC,28110
Ref: Analytical Testing
Report Number: 21-279-0009
Project Description: City of Monroe
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/6/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...)are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 10

• YYD
WaypOI lit, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanaiytical.corn
Sample Summary Table
Report Number: 21-279-0009
Client Project Description: City of Monroe
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
50037 WTP Ferric Cake Solids 10/04/2021 09:10 10/06/2021
50037 WTP Ferric Cake Solids 10/04/2021 09:10 10/06/2021 SM-4500-NH3C WP MTN
50037 WTP Ferric Cake Solids 10/04/2021 09:10 10/06/2021 SW-7471B WP MTN
50037 WTP Ferric Cake Solids 10/04/2021 09:10 10/06/2021 9045D WP MTN
50037 WTP Ferric Cake Solids 10/04/2021 09:10 10/06/2021 4500NO3F-2011 WP MTN
50037 WTP Ferric Cake Solids 10/04/2021 09:10 10/06/2021 6010D WP MTN
50037 WTP Ferric Cake Solids 10/04/2021 09:10 10/06/2021 SM-4500-NH3C-TKN WP MTN
50037 WTP Ferric Cake Solids 10/04/2021 09:10 10/06/2021 SM-2540G WP MTN
50038 WWTP Cake Solids 10/04/2021 09:50 10/06/2021
50038 WWTP Cake Solids 10/04/2021 09:50 10/06/2021 6010D WP MTN
50038 WWTP Cake Solids 10/04/2021 09:50 10/06/2021 4500NO3F-2011 WP MTN
50038 WWTP Cake Solids 10/04/2021 09:50 10/06/2021 SM-4500-NH3C-TKN WP MTN
50038 WWTP Cake Solids 10/04/2021 09:50 10/06/2021 SM-4500-NH3C WP MTN
50038 WWTP Cake Solids 10/04/2021 09:50 10/06/2021 SW-7471B WP MTN
50038 WWTP Cake Solids 10/04/2021 09:50 10/06/2021 SM-2540G WP MTN
50038 WWTP Cake Solids 10/04/2021 09:50 10/06/2021 9045D WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN,Memphis,TN
Page 2 of 10

r rQ
Waypoi ntz. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalyticaicom
46205
City of Monroe Project City of Monroe
Ken Morris Report Date : 10/14/2021
775 Treeway Dr Information : Received : 10/06/2021
Monroe, NC 28110
Report Number:21-279-0009 REPORT OF ANALYSIS
Lab No : 50037 Matrix: Solids
Sample ID:WTP Ferric Cake Sampled: 10/4/2021 9:10
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Moisture 65.6 % 0.010 1 10/07/21 17:02 FMM SM-2540G
Potassium <291 mg/Kg-dry 291 10 10/13/21 19:35 JTR 6010D
Calcium 2970 mg/Kg-dry 1450 10 10/13/21 19:35 JTR 6010D
Aluminum 3460 mg/Kg-dry 145 10 10/13/21 19:35 JTR 6010D
Manganese 1220 mg/Kg-dry 14.5 10 10/13/21 19:35 JTR 6010D
Copper 442 mg/Kg-dry 14.5 10 10/13/21 19:35 JTR 6010D
Nickel 32.0 mg/Kg-dry 7.27 10 10/13/21 19:35 JTR 6010D
Lead <8.72 mg/Kg-dry 8.72 10 10/13/21 19:35 JTR 6010D
Arsenic 41.3 mg/Kg-dry 14.5 10 10/13/21 19:35 3TR 6010D
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Ammonia Nitrogen 834 mg/Kg-dry 291 1 10/12/21 14:00 JP] SM-4500-NH3C
Organic N 13610 mg/Kg-dry 726.7 1 10/12/21 14:00 CALCULATION
Total Solids 34.4 °10 0.010 1 10/07/21 17:02 FMM SM-2540G
Phosphorus 3080 mg/Kg-dry 145 10 10/13/21 19:35 JTR 6010D
Cadmium 3.23 mg/Kg-dry 2.91 10 10/13/21 19:35 JTR 6010D
Chromium 195 mg/Kg-dry 7.27 10 10/13/21 19:35 JTR 6010D
Iron 320000 mg/Kg-dry 581 20 10/13/21 19:40 JTR 6010D
Magnesium 500 mg/Kg-dry 145 10 10/13/21 19:35 JTR 6010D
Mercury <0.4415 mg/Kg-dry 0.0415 1 10/12/21 14:07 JW2 SW-7471B
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 3 of 10

laA,o
Waypoi n , 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project City of Monroe
Ken Morris Report Date : 10/14/2021
775 Treeway Dr Information : Received : 10/06/2021
Monroe, NC 28110
Report Number:21-279-0009 REPORT OF ANALYSIS
Lab No: 50037 Matrix: Solids
Sample ID:WTP Ferric Cake Sampled: 10/4/2021 9:10
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Selenium <14.5 mg/Kg-dry 14.5 10 10/13/21 19:35 JTR 6010D
Sulfur 3280 mg/Kg-dry 291 10 10/13/21 19:35 JTR 6010D
Total Kjeldahl Nitrogen 14400 mg/Kg-dry 727 1 10/13/21 09:00 JPJ ;M-4500-NH3C-TKP
Sodium <727 mg/Kg-dry 727 10 10/13/21 19:35 JTR 6010D
Zinc 125 mg/Kg-dry 36.3 10 10/13/21 19:35 JTR 6010D
Nitrate+Nitrite-N 81.4 mg/Kg-dry 13.8 1 10/13/21 13:49 ZBD 4500NO3F-2011
pH 6.3 s.u. 1 10/12/21 15:14 DRS 9045D
Molybdenum 49.1 mg/Kg-dry 7.27 10 10/13/21 19:35 JTR 6010D
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time MQL Method Quantitation Limit
Page 4 of 10

t��o
YY
Waypoint. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project City of Monroe
Ken Morris Report Date : 10/14/2021
775 Treeway Dr Information : Received : 10/06/2021
Monroe, NC 28110
Report Number:21-279-0009 REPORT OF ANALYSIS
Lab No : 50038 Matrix: Solids
Sample ID:WWTP Cake Sampled: 10/4/2021 9:50
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Moisture 79.2 % 0.010 1 10/07/21 17:02 FMM SM-2540G
Calcium 15500 mg/Kg-dry 240 1 10/13/21 19:45 JTR 6010D
Aluminum 13900 mg/Kg-dry 24.0 1 10/13/21 04:19 TJS 6010D
Manganese 1690 mg/Kg-dry 2.40 1 10/13/21 04:19 TJS 6010D
Copper 345 mg/Kg-dry 2.40 1 10/13/21 19:45 JTR 6010D
Zinc 1030 mg/Kg-dry 6.01 1 10/13/21 04:19 TJS 6010D
Nickel 63.9 mg/Kg-dry 1.20 1 10/13/21 04:19 TJS 6010D
Lead 22.0 mg/Kg-dry 1.44 1 10/13/21 04:19 TJS 6010D
Arsenic 10.3 mg/Kg-dry 2.40 1 10/13/21 04:19 TJS 6010D
Test Results Units MQL OF Date/Time By Analytical
Analyzed Method
Ammonia Nitrogen 2400 mg/Kg-dry 481 1 10/12/21 14:00 JPJ SM-4500-NH3C
Organic N 47600 mg/Kg-dry 1202 1 10/12/21 14:00 CALCULATION
Total Kjeldahl Nitrogen 50000 mg/Kg-dry 1200 1 10/13/21 09:00 JPJ ;M-4500-NH3C-TKP
Phosphorus 22600 mg/Kg-dry 24.0 1 10/13/21 04:19 TJS 6010D
Cadmium 1.31 mg/Kg-dry 0.481 1 10/13/21 04:19 TJS 6010D
Chromium 69.2 mg/Kg-dry 1.20 1 10/13/21 04:19 TJS 6010D
Iron 55300 mg/Kg-dry 240 5 10/13/21 19:50 JTR 6010D
Molybdenum 16.8 mg/Kg-dry 1.20 1 10/13/21 04:19 TJS 6010D
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 5 of 10

wo
/àypo I nt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalyticaicom
46205
City of Monroe Project City of Monroe
Ken Morris Report Date: 10/14/2021
775 Treeway Dr Information : Received : 10/06/2021
Monroe, NC 28110
Report Number:21-279-0009 REPORT OF ANALYSIS
Lab No: 50038 Matrix: Solids
Sample ID:WWTP Cake Sampled: 10/4/2021 9:50
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Sodium 606 mg/Kg-dry 120 1 10/13/21 04:19 TJS 6010D
Total Solids 20.8 % 0.010 1 10/07/21 17:02 FMM SM-2540G
Potassium 2070 mg/Kg-dry 48.1 1 10/13/21 04:19 TJS 6010D
Sulfur 9570 mg/Kg-dry 48.1 1 10/13/21 19:45 JTR 6010D
Magnesium 2220 mg/Kg-dry 24.0 1 10/13/21 04:19 TJS 6010D
Nitrate+Nitrite-N 1430 mg/Kg-dry 22.9 1 10/13/21 13:51 ZBD 4500NO3F-2011
Mercury 0.477 mg/Kg-dry 0.0649 1 10/12/21 14:09 JW2 SW-7471B
Selenium 6.73 mg/Kg-dry 2.40 1 10/13/21 04:19 TJS 6010D
pH 5.7 s.u. 1 10/12/21 15:14 DRS 9045D
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time MQL Method Quantitation Limit
Page 6 of 10

v
YY
Waypoi nt 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Client: City of Monroe CASE NARRATIVE
Project: City of Monroe
Lab Report Number: 21-279-0009
Date: 10/14/2021
Metals Analysis Method 6010D
Sample 50037(WTP Ferric Cake)
Analyte: Aluminum
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte:Arsenic
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Calcium
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Cadmium
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Chromium
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Copper
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Iron
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Potassium
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Magnesium
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Manganese
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to lEC interference/matrix interference.
Analyte: Molybdenum
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 7 of 10

• r•Q
WaypOl nt_ 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Analyte: Sodium
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Nickel
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Phosphorus
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Lead
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Sulfur
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Selenium
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Analyte: Zinc
QC Batch No: L578901/L578170
This analyte was analyzed at a dilution due to 1EC interference/matrix interference.
Page 8 of 10

1Ao
• YY
'A'a ,pOI nt 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-279-0009
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised? 0 Yes 0 No
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? O Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No # Not Present
Chain of Custody(COC) present? #Yes 0 No
COC agrees with sample fabel(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? *Yes 0 No
Sample containers intact? J Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? #Yes 0 No
Cooler temperature in compliance? *Yes 0 No
Cooler/Samples arrived at the laboratory on ice. C) Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water- Sample containers properly preserved (Yes 0 No 0 NIA
Water- VOA vials free of headspace O Yes 0 No © N/A
Trip Blanks received with VOAs 0 Yes 0 No 0 N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No C) N/A
r High concentration container(48 hr) r Low concentration EnCore samplers (48 hr)
r High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis-14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Jill Mauler Date&Time: 10/06/2021 09:04:54
Page 9 of 1D

W WASTEWATER SAMPLE TRANSMIT' 111111111111ningt Account#
Waypoint Analy cm,of ,rce 0_�2021 T4 ao5
7621 Whitepine Road Richmond VA 23237 Tel:[phone] Fax 80 "y°ram"�' 090407
Customer Informatio..
�/ n�lSubmitted By Charge To uouy ,u
Kc . r'3oVY:,-, C.+' 61. Me.--rae
, IT c) '3 it X (o i
i- tiOkWWJit tJc a7r1i1
Project Phone(10,) 3 c I— (,,,d 3 5 Fax:
E-mail: ,,Vloyr:5 @rhor r,xr14•flyq
Sample Information
Lab Number Collection Information Container Information Please Write in Desired Tests
Sample ID (Lab Use _^
Only) Type Date Time Number of Bottles Type Volume
�[1+�T 5003� /'Grab _Glass — oz - -
Ftrr; Composite 1..]`�.a l Q;j J I jc Plastic .—Pin'
to�4G,t qt
1,4 WI? �j Grab oz -
ss
m G Ge ✓ O�v Composite E o-4-.21 9 . So i Plastic pint
qt
o _Grab Glass — oz
o _ Composite _Plastic —pint
rn et
oz
o Grab Glass ——Pin
Composite Plastic -Pt
i
Relinquished By:(Signature) Date Time Received By:(Signature) Date Time
X . ritem. o I. -!{-21 /s o: o -
Test Available Special instructions or Remarks
Nitrogen Series:Total Kjeldahl,Ammonium,Nitrate&Organic Nitrogen.
Phosphorus(total,orthor). Poatssium,Sutfale-Sulfur. Calcium.Magnesium,Sodium.Iron,Aluminum,
Manganese,Copper,Zinc.Arsenic,Barium,Cadmium.Chromium,Cobalt,Molybdenum, Mercury,Lead,
Selenium,Silver.Nickel.Acidity(Total),Alkalinity(Total),Biochemical Oxygen Demand(5 days), Boron,
Chemical Oxygen Demand, Chloride,Conductance(Specific),Hexavalent Chromium, Oil and Grease(EPA).
pH,Phenol,Solids(Dissolved,Suspended,Total,Volatile)

.■Q
Waypoint._ 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanaiytical.com
10/29/2021
City of Monroe
Ken Morris
775 Treeway Dr
Monroe, NC, 28110
Ref: Analytical Testing
Report Number: 21-295-0002
Project Description: City of Monroe
Dear Ken Morris:
Waypoint Analytical Virginia, Inc. received sample(s)on 10/22/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub-contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP)were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
cum Grocir
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to,at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6

O
s
Waypoint, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743.9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 21-295-0002
Client Project Description: City of Monroe
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
55222 WWTP Cake Solids 10/21/2021 10:40 10/22/2021 5M-2540G WP MTN
55223 RAS Solids 10/21/2021 11:05 10/22/2021 5M-2540G WP MTN
WP MTN-Memphis,TN: Waypoint Analytical-TN,Memphis,TN
Page 2 of 6

wWaypo i nt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
46205
City of Monroe Project City of Monroe
Ken Morris Report Date: 10/29/2021
775 Treeway Dr Information : Received : 10/22/2021
Monroe, NC 28110
,wilt Mc toary/
Report Number:21-295-0002 REPORT OF ANALYSIS
Pauric Mc Groary Ph.D.,COPA
Agronomist
Lab No: 55222 Matrix: Solids
Sample ID:WWFP Cake Sampled: 10/21/2021 10:40
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Moisture 71.7 % 0,010 1 10/27/21 16:41 FMM SM-2540G
Test Results Units MQL DF Date/Time By Analytical
Analyzed Method
Total Volatile Solids 47.8 % 0.010 1 10/27/21 16:41 FMM SM-2540G
Total Solids 28.3 % 0,010 1 10/27/21 16:41 FMM SM-2540G
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time MQL Method Quantitation Limit
Page 3 of 6

vo
Waypoi■ ■t. 7621 White pine Road,Richmond,VA 23237
Main 804-743-9401°fax [phone]
ANALYTICAL www.waypointanaiytical.com
46205
City of Monroe Project City of Monroe
Ken Morris Report Date: 10/29/2021
775 Treeway Dr Information : Received : 10/22/2021
Monroe, NC 28110
?awa Pit Gtowg/
Pauric Mc Groary Ph.D.,CPA
Report Number:21-295-0002 REPORT OF ANALYSIS Agronomist
Lab No: 55223 Matrix: Solids
Sample ID :RAS Sampled: 10/21/2021 11:05
Test Results Units MQL OF Date I Time By Analytical
Analyzed Method
Total Solids 1.25 % 0.010 1 10/27/21 16:41 FMM SM-2540G
Moisture 98.7 % 0.010 1 10/27/21 16:41 FMM SM-2540G
Total Volatile Solids 73.8 % 0.010 1 10/27/21 16:41 FMM SM-2540G
Qualifiers/ B Analyte detected in blank DF Dilution Factor
Definitions H Beyond holding time MQL Method Quantitation Limit
Page 4 of 6

• YYe
1Naypoi nt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number:46205
Customer Name: City of Monroe
Report Number: 21-295-0002
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID: I
Shipping container/cooler uncompromised? # Yes 0 No
Number of coolers/boxes received r 1
Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present
Custody seals intact on sample bottles? O Yes 0 No # Not Present
Chain of Custody(COC) present? 0 Yes 0 No
COC agrees with sample label(s)? 0 Yes 0 No
COC properly completed 0 Yes 0 No
Samples in proper containers? # Yes 0 No
Sample containers intact? C)Yes 0 No
Sufficient sample volume for indicated test(s)? 0 Yes 0 No
All samples received within holding time? 0 Yes 0 No
Cooler temperature in compliance? (Yes 0 No
Cooler/Samples arrived at the laboratory on ice. #Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water-Sample containers properly preserved 0 Yes O No 0 N/A
Water-VOA vials free of headspace 0 Yes 0 No 0 N/A
Trip Blanks received with VOAs 0 Yes 0 No © N/A
Soil VOA method 5035—compliance criteria met 0 Yes 0 No # N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) r Low conc pre-weighed vials (Sod Bis-14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: Brandi Watson Date & Time: 10/22/2021 15:00:16
Page 5 of 6

WA; Zt z I FORM/CHAIN OF CUSTODY Account#
willINIIII1kIFt III1II� �0 !, ��s
7621 M Monroe 7
City of Monroe 14 57 57 -6446 Email:support [e-mail]
3e To Copy To
T44. a O I-l✓i 5 CA-1 DA- rAovJ QC
."-Pc73c=.X ( /
f 4.cwroc NL aThl i %
Project Phone(1 3(a(_�o 3 5 Fax: E-mail:
l kmorr,..�.rvvonr•tnc .a.r,
Sample Information
Lab Number Collection Information Container Information Please Write in Desired Tests
Sample ID (Lab Use Number
Only) Type Date Time of Bottles Type Volume
W 1rl l .,�I x Grab -_Glass oZ - -
CO � 5S[.�2 —Composite ! a f-.?1 10,....10 I Plastic —pint
qt
Grab oZ
-5-6-Glass
S Z3 ,._.Composite j 0.a I .zt /1 5. C X Plastic ---qi t o
up
oz
Grab Glass —
Composite �Plastic —pint si
qt - a
Grab Glass — az
•—Composite ,Plastic —pint
qt
Relinquished By:(Signature) Date Time Received By:(Signature) Date Time
41."- AA u0.47 iz ai-a.1 11= 10
Test Available Special Instructions or Remarks
Nitrogen Series:Total Kjeldahl,Ammonium,Nitrate&Organic Nitrogen. -
Phosphorus(total,orthor), Poatssium,Sulfate-Sulfur. Calcium. Magnesium,Sodium, Iron,Aluminum,
Manganese, Copper,Zinc,Arsenic,Barium,Cadmium,Chromium,Cobalt,Molybdenum,Mercury,Lead,
Selenium,Silver.Nickel.Acidity(Total),Alkalinity(Total),Biochemical Oxygen Demand(5 days),Boron,
Chemical Oxygen Demand,Chloride.Conductance(Specific),Hexavalent Chromium, Oil and Grease(EPA).
pH,Phenol,Solids(Dissolved,Suspended,Total,Volatile)
T 1,Qej Y o la,4:I a 5-1;d5 le LAO o vt co.1t-4- 5o.ebet lA-
Land � L'"-P,MS 504.^P1t-
`-fl P5
\J L

TAB 3
TCLP ANALYSIS

0
ace Analytical
Report of Analysis
City of Monroe
PO Box 69
Monroe, NC 28111
Attention: Ken Morris
Project Name: Land Application
Lot Number:WJ07063
Date Completed:10/28/2021
11/02/2021 8:19 AM
Approved and released by:
Project Manager II: Marcia K. McGinnity
_......., Aliko
ata BolWaUknel,taf+oa Bard
/°; ACCREDITED
TESTING L BORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety,without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 1 of 20

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
City of Monroe
Lot Number: WJ07063
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non-Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W' qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Comments:
Sample WJ07063-002 (WTP Cake) (Run 1) (Analysis Batch 20316) TCLP Volatiles was diluted due to the
nature of the sample matrix. The LOQ has been elevated to reflect the dilution.
No other issues were identified.
Pace Analytical Services,LLC(formerly ShealyEnvironmetal Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2 of 20

PACE ANALYTICAL SERVICES, LLC
Sample Summary
City of Monroe
Lot Number: WJ07063
Sample Number Sample ID Matrix Date Sampled Date Received
001 WWTP Cake Solid 10/04/2021 0750 10/06/2021
002 WTP Cake Solid 10/04/2021 0815 10/06/2021
(2 samples)
Pace Analytical Services,LLC (formerly Shealy Environmental Services,inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 20

Inorganic non-metals
Client:City of Monroe Laboratory ID:WJ07063-001
Description:WWTP Cake Matrix:Solid
Date Sampled:10/04/2021 0750 %Solids:21.8 10/12/2021 0017
Date Received:10/0612021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Flashpoint()1010B 1 10/15/2021 1219 KMC 19005
1 (Reactive Cya)7.3.3 1 10/08/2021 1715 AAB 10/08/2021 1239
1 (Reactive Sul)7.3.4 1 10/08/2021 1538 SJL 10/08/2021 1239
2 (Soil pH meas)9045D 1 10/20/2021 1458 NBW 19580
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Flashpoint(Pensky-Martens Closed-Cup) 1010B >140 140 °F 1
Reactive Cyanide 7.3.3 ND 50 mg/kg 1
Reactive Sulfide 7.3.4 ND 50 mg/kg 1
Soil pH measured in water @ 19.3°C 9045D 5.7 su 2
LOQ=Limit of Quantilation B=Detected in the method blank E=Quantttation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCSILCSD failure
H=Out of holding time W=Reported on wet weight basis S=MSIMSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacefabs.com
Page 4 of 20

TCLP Volatiles
Client:City of Monroe Laboratory ID:WJ07063-001
Description:WWTP Cake Matrix:Solid
Date Sampled:10/04/2021 0750 %Solids:21.8 10/12/2021 0017
Date Received:10/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/5030B 8260D 10 10/27/20211535 TML 20316 10/17/20211643
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 8260D ND 0.050 mgfL 1
2-Butanone(MEK) 78-93-3 8260D ND 0.10 mg/L 1
Carbon tetrachloride 56-23-5 8260D ND 0.050 mglL 1
Chlorobenzene 108-90-7 8260D ND 0.050 mg/L 1
Chloroform 67-66-3 8260D ND 0.050 rng/L 1
1,2-Dichloroethane 107-06-2 8260D ND 0.050 mglL 1
1,1-Dichloroethene 75-35-4 8260D ND 0.050 mg/L 1
Tetrachloroethene 127-18-4 8260D ND 0.050 mg/L 1
Trichloroethene 79-01-6 8260D ND 0.050 mg/L 1
Vinyl chloride 75-01-4 8260D ND 0.010 mglL 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Bromofluorobenzene 93 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 101 70-130
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 46% L=LCSILCSD failure
H=Out of holding time W=Reported on wet weight basis S=MSIMSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 20

TCLP Semivolatiles
Client:City of Monroe Laboratory ID:WJ07063-001
Description:WWTP Cake Matrix:Solid
Date Sampled:10/04/2021 0750 %Solids:21.8 10/12/2021 0017
Date Received:10/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 10/25/20211342 STM 10/21/2021 1700 19708 10/16/20210006
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
1,4-Dichlorobenzene 106-46-7 8270E ND 0.040 mglL 1
2,4-Dinitrotoluene 121-14-2 8270E ND 0.080 mg/L 1
Hexachlorobenzene 118-74-1 8270E ND 0.040 mglL 1
Hexachlorobutadiene 87-68-3 8270E ND 0.040 mg1L 1
Hexachloroethane 67-72-1 8270E ND 0.040 mglL 1
2-Methylphenol 95-48-7 8270E ND 0.040 mglL 1
3+4-Methylphenol 106-44-5 8270E ND 0.040 mglL 1
Nitrobenzene 98-95-3 8270E ND 0.040 mglL 1
Pentachlorophenol 87-86-5 8270E ND 0.20 mg/L 1
Pyridine 110-86-1 8270E ND 0.040 mg/L 1
2,4,5-Trichlorophenol 95-95-4 8270E ND 0.040 mg/L 1
2,4,6-Trichlorophenol 88-06-2 8270E ND 0.040 mg/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
2-Fluorobiphenyl 68 37-129
2-Fluorophenol 37 24-127
Nitrobenzene-d5 64 38-127
Phenol-d5 48 28-128
Terphenyl-d14 84 10-148
2,4,6-Tribromophenol 60 41-144
LOG=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range C]=Surrogate failure
ND=Not detected at or above the LOG N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Mc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 20

TCLP Herbicides
,
Client:City of Monroe Laboratory ID:WJ07063-001
Description:WWTP Cake Matrix:Solid
Date Sampled:10104/2021 0750 %Solids:21.8 10/12/2021 0017
Date Received:10/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/8151A 8151A 1 10/22/20211642 CMF 10/20/2021 1617 19461 10/16/20210006
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
2,4-D 94-75-7 8151A ND 0.020 mg1L 1
2,4,5-TP(Silvex) 93-72-1 8151A ND 0.0050 mg/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
DCAA 83 50-112
LOa-Limit of Quantitalion B=Detected in the method blank E=QuanUtation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The PPG between two GC columns exceeds 40% L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MS0 failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 7 of 20

PCBs by GC
Client:City of Monroe Laboratory lD:WJ07063-001
Description:WWTP Cake Matrix:Solid
Date Sampled:1010412021 0750 %Solids:21.8 10/1212021 0017
Date Received:11010612021
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 3660B/3665A 8082A 1 10/20120211141 CMF 10/19/2021 1607 19365
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aroclor 1016 12674-11-2 8082A ND 45 ug/kg 1
Aroclor 1221 11104-28-2 8082A ND 45 ug/kg 1
Aroclor 1232 11141-16-5 8082A ND 45 ug/kg 1
Aroclor 1242 53469-21-9 8082A ND 45 ug/kg 1
Aroclor 1248 12672-29-6 8082A ND 45 ug/kg 1
Aroclor 1254 11097-69-1 8082A ND 45 ug/kg 1
Aroclor 1260 11096-82-5 8082A ND 45 ug/kg 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Decachlorobiphenyl 62 41-132
Tetrachloro-m-xylene 85 35-106
LOCI=Limit of Quantitation B=Detected in the method blank E=Quantization of compound exceeded the calibration range a=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCSILCS❑failure
H=Out of holding time W=Reported an wet weight basis S=MSIMSA failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 8 of 20

TCLP Pesticides
Client:City of Monroe Laboratory ID:WJ07063-001
Description:WWTP Cake Matrix:Solid
Date Sampled:10/04/2021 0750 %Solids:21.8 10/12/2021 0017
Date Received:10/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081E 1 10/26/20211443 DAL1 10/22/2021 1730 19855 10/16/2021 0006
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
gamma-BHC(Lindane) 58-89-9 8081B ND 0.00040 mg/L 1
Chlordane 57-74-9 8081B ND 0.0040 mg/L 1
Endrin 72-20-8 8081B ND 0.00040 mg/L 1
Heptachlor 76-44-8 8081B ND 0.00040 mglL 1
Heptachlor epoxide 1024-57-3 8081B ND 0.00040 mglL 1
Methoxychlor 72-43-5 8081B ND 0.0016 mglL 1
Toxaphene 8001-35-2 8081B ND 0.0080 mglL 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Decachlorobiphenyl 62 20-131
Tetrachloro-m-xylene 73 26-132
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 9 of 20

TCLP Metals
Client:City of Monroe Laboratory ID:WJ07063-001
Description:WWTP Cake Matrix:Solid
Date Sampled:1010412021 0750 %Solids: 21.8 10112/2021 0017
Date Received:10/0612021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3010A 6010D 1 10/19/2021 1218 KSH2 10118/20211131 19151 10/16/2021 0006
1 1311/7470A 7470A 1 10/18/2021 1747 CMS2 10/18/2021 1323 19156 10/16/2021 0006
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Arsenic 7440-38-2 601013 ND 0.15 mg/L 1
Barium 7440-39-3 6010D ND 0.25 mg/L 1
Cadmium 7440-43-9 6010D ND 0.050 mg/L 1
Chromium 7440-47-3 6010D ND 0.10 mg/L 1
Lead 7439-92-1 6010D ND 0.10 mg/L 1
Mercury 7439-97-6 7470A ND 0.0020 mg/L 1
Selenium 7782-49-2 6010D ND 0.20 mg/L 1
Silver 7440-22-4 6010D ND 0.10 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCS/LCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page l0 of20

Inorganic non-metals
Client:City of Monroe Laboratory ID:WJ07063-002
Description:WTP Cake Matrix:Solid
Date Sampled:10/04/2021 0815 %Solids: 34.0 10/12/2021 0017
Date Received:10/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Flashpoint()1010B 1 10/16/2021 1247 KMC 19005
1 (Reactive Cya)7.3.3 1 10/08/2021 1718 AAB 10/08/2021 1239
1 (Reactive Sul)7.3.4 1 10/08/2021 1538 SJL 10/08/2021 1239
2 (Soil pH meas)9045D 1 10/20/2021 1500 NBW 19580
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Flashpoint(Pensky-Martens Closed-Cup) 1010E >140 140 °F 1
Reactive Cyanide 7.3.3 ND 50 mg/kg 1
Reactive Sulfide 7.3.4 ND 50 mg/kg 1
Soil pH measured in water @ 19.3°C 9045D 6.0 su 2
LOQ=Limit of Quanllation B=Detected in the method blank E=Quantiiation of compound exceeded the calibration range a=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCS/LCSD failure
H=Out of holding lime W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 11 of 20

TCLP Volatiles
Client:City of Monroe Laboratory ID:WJ07063-002
Description:WIP Cake Matrix:Solid
Date Sampled:10/0412021 0815 %Solids:34.0 10/1212021 0017
Date Received:10/0612021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/5030B 82600 50 10/27/20211711 TML 20316 10/17/20211643
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Benzene 71-43-2 8260D ND 0.25 mg/L 1
2-Butanone(MEK) 78-93-3 8260D ND 0.50 rng1L 1
Carbon tetrachloride 56-23-5 8260D ND 0.25 mg1L 1
Chlorobenzene 108-90-7 8260D ND 0.25 mg/L 1
Chloroform 67-66-3 8260D ND 0.25 mg/L 1
1,2-Dichloroethane 107-06-2 8260D ND 0.25 mg/L 1
1,1-Dichloroethene 75-35-4 8260D ND 0.25 mg/L 1
Tetrachloroethene 127-18-4 8260D ND 0.25 mg/L 1
Trichloroethene 79-01-6 8260D ND 0.25 mg/L 1
Vinyl chloride 75-01-4 8260D ND 0.050 mg/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Bromofluorobenzene 94 70-130
1,2-Dichloroethane-d4 108 70-130
Toluene-d8 101 70-130
LDQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOO N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCSILCSD failure
R=Out of holding lime W=Reported on wet weight basis S=MSIMSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 {803)791-9700 Fax{803)791-9111 www.pacelabs.com
Page 12 of20

TCLP Semivolatiles
Client:City of Monroe Laboratory ID:WJ07063-002
Description:WTP Cake Matrix:Solid
Date Sampled:10/04/2021 0815 %Solids: 34.0 10112/2021 0017
Date Received:10/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8270E 1 10/24/20211727 STM 10/21/20211700 19708 10/16/20210006
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
1,4-Dichlorobenzene 106-46-7 8270E ND 0.040 mg/L 1
2,4-Dinitrotoluene 121-14-2 8270E ND 0.080 mg/L 1
Hexachlorobenzene 118-74-1 8270E ND 0.040 mg/L 1
Hexachlorobutadiene 87-68-3 8270E ND 0.040 mg/L 1
Hexachloroethane 67-72-1 8270E ND 0.040 mg/L 1
2-Methylphenol 95-48-7 8270E ND 0.040 mg/L 1
3+4-Methylphenol 106-44-5 8270E ND 0.040 mg/L 1
Nitrobenzene 98-95-3 8270E ND 0.040 mglL 1
Pentachlorophenol 87-86-5 8270E ND 0.20 mglL 1
Pyridine 110-86-1 8270E ND 0.040 mg/L 1
2,4,5-Trichlorophenol 95-95-4 8270E ND 0.040 mglL 1
2,4,6-Trichlorophenol 88-06-2 8270E ND 0.040 mglL 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
2-Fluorobiphenyl 82 37-129
2-Fluorophenol 26 24-127
Nitrobenzene-d5 81 38-127
Phenol-d5 32 28-128
Terphenyl-d14 100 10-148
2,4,6-Tribromophenol 74 41-144
LOQ=Limit of Quantitalion B=Detected in the method blank E=Quantitation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCSILCSD failure
H=Out of holding time W=Reported on wet weight basis S=MSIMSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 13 of 20

TCLP Herbicides
Client:City of Monroe Laboratory ID:WJ07063-002
Description:WTP Cake Matrix:Solid
Date Sampled:10104/2021 0815 %Solids: 34.0 1011212021 0017
Date Received:10/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/8151A 8151A 1 10122/20211705 CMF 10/20/2021 1617 19461 10116120210006
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
2,4-D 94-75-7 8151A ND 0.020 mg1L 1
2,4,5-TP(Silvex) 93-72-1 8151A ND 0.0050 mg1L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
DCAA 83 50-112
LOQ=Limit of Quantitation 6=Detected in the method blank E=Quanttation of compound exceeded the calibration range a=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCSILCSD failure
H=Out of holding time W=Reported on wet weight basis S=MS/MSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 14 of 20

PCBs by GC
Client:City of Monroe Laboratory ID:WJ07063-002
Description:WTP Cake Matrix:Solid
Date Sampled:10/0412021 0815 %Solids: 34.0 10/12/2021 0017
Date Received:10l06l2021
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 3660B/3665A 8082A 1 10/20/20211222 CMF 10/19/2021 1607 19365
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aroclor 1016 12674-11-2 8082A ND 29 ug/kg 1
Aroclor 1221 11104-28-2 8082A ND 29 ug/kg 1
Aroclor 1232 11141-16-5 8082A ND 29 ug/kg 1
Aroclor 1242 53469-21-9 8082A ND 29 ug/kg 1
Aroclor 1248 12672-29-6 8082A ND 29 ug/kg 1
Aroclor 1254 11097-69-1 8082A ND 29 ug/kg 1
Aroclor 1260 11096-82-5 8082A ND 29 ug/kg 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Decachlorobiphenyl 64 41-132
Tetrachloro-m-xylene 51 35-106
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantifadon of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCSILCSD failure
H=Out of holding time W=Reported on wet weight basis S=MSIMSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.paceiabs.com
Page 15 of 20

TCLP Pesticides
Client:City of Monroe Laboratory ID:WJ07063-002
Description:WTP Cake Matrix: Solid
Date Sampled:10104/2021 0815 %Solids: 34.0 10/12/2021 0017
Date Received:10/06/2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081B 1 10/26/2021 1514 DAL1 10/22/2021 1730 19855 10/16/20210008
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
gamma-BHC(Lindane) 58-89-9 8081B ND 0.00040 mg/L 1
Chlordane 57-74-9 8081B ND 0.0040 mg/L 1
Endrin 72-20-8 8081B ND 0.00040 mglL 1
Heptachlor 76-44-8 8081B ND 0.00040 mg/L 1
Heptachlor epoxide 1024-57-3 8081B ND 0.00040 mg/L 1
Methoxychlor 72-43-5 8081B ND 0.0016 mg/L 1
Toxaphene 8001-35-2 8081B ND 0.0080 mglL 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Decachlorobiphenyl 68 20-131
Tetrachloro-m-xylene 82 26-132
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range 0=Surrogate failure
ND=Not detected at or above the LOCI N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCSILCSD failure
Ft=Out of holding time W=Reported on wet weight basis S=MSIMSD failure
Pace Analytical Services,LLD {formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive west Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 16 of 20

TCLP Metals
Client:City of Monroe Laboratory ID:WJ07063-002
Description:WTP Cake Matrix:Solid
Date Sampled:1010412021 0815 %Solids: 34.0 10112(2021 0017
Date Received:10106(2021
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3010A 6010D 1 10/19/2021 1222 KSH2 10/18/2021 1131 19151 10/16/2021 0006
1 1311/7470A 7470A 1 10/18/2021 1750 CMS2 10/18/2021 1323 19156 10/16/2021 0006
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Arsenic 7440-38-2 6010D ND 0.15 mg/L 1
Barium 7440-39-3 6010D 1.1 0.25 mglL 1
Cadmium 7440-43-9 6010D ND 0.050 mg/L 1
Chromium 7440-47-3 6010D ND 0.10 mg/L 1
Lead 7439-92-1 6010D ND 0.10 mg/L 1
Mercury 7439-97-6 7470A ND 0.0020 mglL 1
Selenium 7782-49-2 6010D ND 0.20 mg/L 1
Silver 7440-22-4 6010D ND 0.10 mglL 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantlation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCS/LCSD failure
Ii=Out of holding time W=Reported on wet weight basis S=MSIMSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 17 of 20

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 18 of 20

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receipt unless other arrangements are made. r notated en Ice iChe: ...„:"Kg Li NI r;Ice Parkkiereirr iempTL— •G [ Trrp.grant,Er ?a ro
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PACE ANALYTICAL SERVICES, LLC
Samples Receipt Checklist(SRCI(MCOOI8C-15) 1 see sed:9/29/2320
2e1ksrl tie.71 Issuing Aut non ty:Pane ENV-WOO._ Page 1 of 1
Sample Receipt Checklist (SRC)
C]icn1: City ofrvtonrm Cooler'nspectedbyhlate: JRG2 / :0+r•N202t LotMi: moos;
ce1L77' 0;. S Cr
Means of rccer t: I aye Client ,:P4 FctiEx {7t'ncr, I
FYe:. 1511 No I.Were custody seals presenr on the cooler'? j i_...., .
Yes No ElNA 2.If custody seals were pnsesii,were thc;ip:ectand unbroken? 1 -
pH Strip 1D: NA Chlorin Strip ID: v^ Tested by:N''.-._
Original temperature upon receipt!Derived(Corrected)temperature u on receipt %Said Son p•Cup ID. 2:-lt2R
2.3 �2.3 cc NA /NA Ax NA 1NA cc N. /N„ aL+
Method:[Temperature Blank❑A iuinst Bo:tics lit Gun ID: ` __ IR Gun Cnrrecrion'Factor: 0 CC
Method of coolant: 0 Wet Ice LI ice Packs ElDiv toe El one I
• 3. If temperature of nay cooler exceeded 6. 4C,was Project Managed Notified?
r[ Y ❑Nn RNA PM was Notified by:plane I*mail!fa to-facc(circle one). !
❑Ye,r ❑No J❑NA 4. 1s the commercial courier's pack.hT,.li pitched to this ibnn?
]v' Yes ❑No 5. Were proper custody pru::eoures(rclinqu :redheceived)followed'
EiYcy U Na O. Were sample IDs listed on the CCC? i
Yes 7 No 7. Weres:suplc IDs list:ci on all sample ootltainers?
0 Yes .:1 Na S. Was collection date&time listed on the :CIC? . ..._.. ...
2]Ycs No cl. Wes collection date&time listed oar ail 4unple containers? i
Yes No 10_Did all container label information(ID HOC$ate,tune)agree wirh the 7
❑J Yes g No 1 I_Were tests;A be perfonned listed on the :OC'.? i
ID Yes ❑No f 2.Did al:&maples arrive in arc proper containers for each test andinrl in goal ecrtri nn
(unbroken, lids on,etc.)? _
©Yes U No It Was adequate sample v'oleme uvai:abk? i
= 0 Yes U 1+4o 14. Were all samples received within is tlla Ooldin Lillie car 48 ho;rrs,kehishcvcr comes first?
I!! • Yes No 35,Were any samples containers inissindes{:ess(circle one)sam?]es Not listed on COC?
❑Yea ❑tilo' QNA'ld. Fur VOA and RSK-l7'samples,were bubbles prczent›"pea-s zed'(Woe drum in diameter)
. l
ut any of the VOA olds? I
Yes JNu d NA I?.Ware all DROMrnetalshrutrienl samples rttccivcd at a p11 of<:2?
Ycs .J No _NA 18.Were all cyanide s,LmplcA received at a II> 12 and sulfide samples received at a pFi>9? .
❑Yes ❑No 2NA 19_ Were all applicable N1•IyTKNIcyan del»erinllti25.'?(SIR.' (e:0,5ritg1L)samples tree of
residual chlorine?
❑Yes I:]No DNA 20. Were client remtuks/requests c.a.reques ed dilulior.s.M5/MSD designations,etc...)
correctly transcribed front the COC into the l win:nt section in LIM+
❑Yes [ ]No 21.Was the quote number listed on the a onl4iner tubed!If yes.Quote .
,...,eta. ,...._.
I-Snnitple Preservation (Must be completed for any sample(,)inverse- ly preserved or with hcadspace.)
Sarnple(s) NA - wrrr received ncorrectiy preserved and were adjusted accordingly
in sample receiving with mL of circle one:I I2SO'1, 1ENC}'s,HCI Na0l1 using SR 4 NA ,
Dice of preservation NA - If more Than one preservative is ri ed,please nole in the aliments below.
Sam.,"IN .NA !
(S) __. were received with bahbi,C's>6 mm rn diameter.
Samples(s) NA were receive will'TRC> 0-5 era/I.(1 4:9 is t1o)and were
adjusred aceerdingly in sample receiving with blxl:t:m thiusulfate(Nazi 0,)with Shea:y ID: NA
SR barcede labels applied by, -11461 Date: IU/u7 vet
Comm cots:
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 20 of 20

0
ace Analytical
Report of Analysis
City of Monroe
PO Box 69
Monroe, NC 28111
Attention: Kyle Ketchum
Project Name: Land Application
Lot Number:WJ22046
Date Completed:10/31/2021
11/14/2021 5:35 PM
Approved and released by:
Project Manager II: Marcia K. McGinnity
Ali=
AINNorwAttadWm,bud
�?:� ACCREDITED
-1111211113M-
nsnmG LAEORAYGnr
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC(formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax: [phone] www.pacelabs.com
Page I of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No:32010001 NELAC No: E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
City of Monroe
Lot Number: WJ22046
This Report of Analysis contains the analytical result(s)for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue:All, Non-Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006&SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Drinking Water:VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W'qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Comments:
Recovery of surrogate tetrachloro-m-xylene was slightly below limit of 35% at 27%with no detectable
aroclors present and good recovery for decachlorobiphenyl in sample WJ22046-001. Results are qualified
„Q»
Pace Analytical Services,LLC(formerly Shealy Environmetal Services,Inc.)
106 Vantage Point Drive West Columbia.SC 29172(803)791-9700 Fax[phone] www.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
City of Monroe
Lot Number: WJ22046
Sample Number Sample ID Matrix Date Sampled Date Received
001 WTP Cake Solid 10/21/2021 1550 10/22/2021
002 WTP Cake Solid 10/21/2021 1620 10/22/2021
(2 samples)
Pace Analytical Services,LLC (formerly Shealy Environmental Services,inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 3 of 9

PACE ANALYTICAL SERVICES, LLC
Detection Summary
City of Monroe
Lot Number: WJ22046
Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
Pace Analytical Services,LLC (formerly Shealy Environmental Services,inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 4 of 9

Client:City of Monroe Laboratory ID:WJ22046-001
Description:WTP Cake Matrix:Solid
Date Sampled:1012112021 1550 %Solids: 33.4 10/24/2021 1941
,Date Received:1 012 212 0 2 1
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 36608/3665A 8082A 1 10/27/2021 1210 CMF 10/25/2021 1657 20067
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aroclor 1016 12674-11-2 8082A ND Q 30 ug/kg 1
Aroclor 1221 11104-28-2 8082A ND Q 30 ug/kg 1
Aroclor 1232 11141-16-5 8082A ND Q 30 ug/kg 1
Aroclor 1242 53469-21-9 8082A ND Q 30 ug/kg 1
Aroclor 1248 12672-29-6 8082A ND Q 30 ug/kg I
Aroclor 1254 11097-69-1 8082A ND Q 30 ug/kg 1
Aroclor 1260 11096-82-5 8082A ND Q 30 ug/kg 1
Run I Acceptance
Surrogate Q %Recovery Limits
Decachlorobiphenyl 62 41-132
Tetrachloro-m-xylene N 27 35-106
LOQ=Limit of Quanttation B=Detected in the method blank E=Quarditalicn of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCSILCSD failure
H=Out of holding time W=Reported on wet weight basis S=MSIMSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 5 of 9

Client:City of Monroe Laboratory ID:WJ22046-002
Description:WTP Cake Matrix:Solid
Date Sampled:10121/2021 1620 %Solids: 18.1 10/24/2021 1941
Date Received:10122/2021
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 3660B/3665A 8082A 1 10/27/2021 1224 CMF 10/25/2021 1657 20067
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aroclor 1016 12674-11-2 8082A ND 55 ug/kg 1
Aroclor 1221 11104-28-2 8082A ND 55 ug/kg 1
Aroclor 1232 11141-16-5 8082A ND 55 ug/kg 1
Aroclor 1242 53469-21-9 8082A ND 55 ug/kg 1
Aroclor 1248 12672-29-6 8082A ND 55 ug/kg I
Aroclor 1254 11097-69-1 8082A ND 55 ug/kg 1
Aroclor 1260 11096-82-5 8082A ND 55 ug/kg 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Decachforobiphenyl 67 41-132
Tetrachloro-m-xylene 59 35-106
LOQ=Limit of Quantitafion B=Detected in the method blank E=Quantitation of compound exceeded the calibration range Q=Surrogate failure
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40% L=LCSILCSD failure
H=Out of holding time W=Reported on wet weight basis S=MSIMSD failure
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 6 of 9

Chain of Custody
and
Miscellaneous Documents
Pace Anarytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 {803)791-9700 Fax{803)791-9111 www.pacelabs.com
Page 7 of 9

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Add // iciephone No. or¢ 341-6,a 35 Page
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N +tfsf ate ,�t a 11)%% t1inxes. 4.fiNCf I Co'rai'+e•Tipa le-- Gd?ase
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1umAreursd Tire Requited(Prlci1 approval reqdrodfor exFeditedTAt.) Sa i he Disposal 0 Requirements I.SpccI yj Pcieibae Hazard Ident?6eetlan
t Sqr and n Bust(Please Speelly1 r Rem 10 Cnl KUssxva G t
9 Lab Kum.law/ u Rammatle 0 Skin trlart 0 l+al 0 Untrue/r
1. Inqulshed y' /Sampler Dale Time 1,1iecci:ec lay Date Tme
sr- a''n'h jo-ail-_3L ic,:'3S _ Secwriza Coeaiar
2.Relinquished ay Dale Time 2.Re
AU.-1, AZ7.tr r .1e �� /o L•tf r fus-
3.FG,lirrquid,cd`y Date JIL
r/ S.P.aceivaa by Date Tale
4_Relinquished by Dale Time ;A Labora toe ty 4!lAi! , Time
i 3 Noce;All samples are retained for four weeks from [Lab use ALY •
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receipt unless other A'tmangement9 are made. M Rlcai,retl xt Ica;Caetk) Ll<as o�1n b l P K li.�o},l 1[mrp.S.` °c Temp.Shirk. tad;
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1

PACE ANALYTICAL SERVICES, LLC
Samples Receipt checklist(SRC)(ME0016C-1S) Revised:9f2e/2C2e
t esltalyf;GN' Issuing Authority:Para FNV-WCOL Page 1 at 1
Saluple Receipt Checklist(SRC)
rchw It: City�ormnurtiu _ Cooler Inspected malt: 1RO? i 1OO22i202 Lot#: t4122C46
Means of receiui: 19 face ❑{'lieu J--r UPS IIIIZEME Oder.
EJ Yes END'_ I,Were custody seals present en the cooler? _
j J Y i NoJ NA 2.If custod•seats were present,wcrc__ they intact and-unbroken? _
pli Strip ID: NA Chlorine Strip ID; t4A Twecd by:NA __..
Original temp:renlr0 upon receipt/Derived(Corrected)temperature epon receipt %.Solid Snap-Cup 1D: 2 t-1928
3.4 /3,a et: NA /NA nC NA /NA g: NA NA ec
tlde.htrd;❑Tamperaturu Blank CjAn}tor,st Bottles 1R Gun ID; S Ile Gin Comrct:on Factor: I ae
Method of coolant: n Wet Ice ❑ ice Packs ❑Dry Ice ❑ Nona _
❑Yes ❑N) C�]NA.3. IT t temperatere of any cooler exceeded(UPC,was Project Manager Notified?
I'M was Notified by;phone/email/face-to-ace(circle one).
Ycs ❑Nu [DNA 4. Is the commercial courier's packing stip attached to this form? I
Q Yes LJNo 5. Were proper custocy procedures(relinquishedlreceived)foLowed? 1
i Yes, U No 6. Were sample]Ds listed on the COC?
Z Yes ❑No '7. Were sample IDe listed on all sample containers?
Q Yes eiN0 li. Was collection date&time lstcd on the COC?
Cd Yes ❑No' 9. Was collection date&time listed on all sample containers?
_
rYes 0 No 111.Did all container label informatior.(iD,deto,time)tens S'
weh the COC'?
No 11.Were boats to be perfenrcd listed on the teOt_e
I I2,Did ail samples arrive in the proper containers for each test vad i1a-in good condition n Yes ❑N+,
(enhrnlcce,lids ore etc.)?
D Yes U No 13. Was adequate sample volume available?
1]Yes 1__f No i4.Nero all samples received within ie the holding time or 4S hours,whichever comes first?
0 Yes 1JNo 13,Were any samples containers nissin excess(chyle one)samples Not:iste+i on COC?
['Yes El Na �J]NA 16.For VOA and RSK-I75 samples;were bubbles present e"pea-stzen(le ur 6min in diameter)
in any of the VOA vials?
8 Yes' ii No' DNA 17.Were all DR 11:ctaIs/nutr•ient samplee received at a pH o:'c 2? ,�
IYcs leiNo DI/A 1 R.Were all cyanide samples nweived at a pH> t 2 and 3111Gde etrnples received at a pH>9?
0Ycs ❑Not z NA,:9.Were Trapplicnhle NIIe."rKN/crrnideiphenol/62e.:16o33(•.0.5neg'Lj samples free of -
restduai c#tl-xirc?
L`I Yes ❑Nu ��A 20.Were client remarkelrequcsts(i.e.requcncd dilutions,MS/MSD cesignatitms,etc...)
ctnm lly transcribed From the COC into the comment section in LIMS?
'Yes_ 0 No 2l, Was the quote rnunbcr listed on IFr,container label?If yes,Quote h
Sample Preservation (Mils!be completed for any sample(s)it-correct:ypreserveed or with hearequicc.)
Sample(s) " I were received incorrectly preserved and were ladjuytctl eueordutgly
in sample rci civitto with NA i inL of circle one:li2SQ,I,HNO3,I!CI,NaOH using SR k NA
rime of prescrva_inn NA ': . If more than one preservative is hec:ed.please note in the comments eelinv.
Sneeple,$)_•_
NA — _ were received with bubbles=eti nun ill die rmaer, I
Sampleses) me were received with'IRC.1 0.5 mg/(if ii19 IA no)and were
adjusted accordingly in sample receivieg with sodium(hiosaltate(Na,S2O.i)with Mettle IL):"
Sit barcode labe:s applied by:;K1)kw .. Date: Inaan021
Comments:
1
Pace Analytical Services,LLC (formerly Shealy Environmental Services,Inc.)
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.pacelabs.com
Page 9 of 9

TAB 4
FIELD SUMMARY FORMS

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 1 Acres Utilized: 11.6
Land Owner: Calvin Morris Annual Dry Tons Applied: 42.9913 Site#: NC-AN-19 Acres Permitted: 11.6
Operator: Same Predominant Soil Series: GoB-Golston Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(past.) Crop 1 Max.PAN: 126 Crop 2 Name: Fescue (past.) Crop 2 Max.PAN: 50
Volume applied Volume Soil
pp Residual Sources Precip. a c Z a Nitrate Name of Crop Type
(enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 ri d w TKN o g and PAN Applied Receiving Residual
Liquid (Dry, s 'n' 'if - I✓ 1bs/acre
Q 9 Solids Acre Fert.,Animal Wet Hrs. * * Nitrite ( ) Application
Cu.Yds Gallons Waste,etc) co
"`
(Dry Tons/Ac) Moist) inches . mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop I Crop 2
April 21 54 16.6 0.651 WWTP Cake D 0 S 0.5 0.3 51,900 3,280 _ 65.7 21.205 NA Fescue
April 21 54 29.4 1.153 WTP Cake D 0 S 0.5 0.4 17,300 473 54.8 16.188 NA Fescue
May 21 126 16.6 1.519 WWTP Cake D 0 S 0.5 0.3 51,900 3,280 65.7 49.479 NA Fescue
May21 18 29.4 0.384 WTP Cake D 0 S 0.5 0.4 17300 473 54.8 5.396 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 252 0 ...:: As Cd Cu Cr 1 Pb Hg Mo Ni Se Zn P 92.267 0.000 Lime Applied
Annual lbs/acre 0.135 0.013 3.115 1.050 0.114 0.002 0.257 0.442 0.048 4.957 113.242 : :; Date lbs/ac
Prior Years Cumulative lbs/ac 1.597 0.26 20.92 25.127 3.111 0.098 2.842 4.78 0.697 93.897 ::
Current Cumulative lbs/ac 1.732 0.273 24,035 26.177 3.225 0.100 3.099 5.222 0.745 98.854
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit lst/2nd Crop
126 I 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
� *Application Method: S-Surface,IN-Injection,INC-Incorporation
,r-,. / ' ftrrli �� 3 �a o2a **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 42.99
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Calvin Morris Owner: Same Predominant Soil Series: GoB-Goldston
Acres Used: 11.6 Acres Permitted: 11.6 Site#: NC-AN-19 Field#: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample ors 2 J3 161 ? ,g.J 191 i0 11 112
Com-
posite
Date 415121 4/5/21
% Solids 16.6 29.4
Arsenic 12 27.1
Cadmium 1.16 2.58
Copper 383 473
Chromium 74.7 236
Lead 22.7 5.1
Mercury 0.489 0.0479
Molyb- 18.1 58.2
denum -
Nickel 77.1 35
Selenium 5 8.5
Zinc 1090 74.5
Total
Phos- 24000 2970
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total J j L r4 J 110 I y
DT/Ac./
App. 7
Event 2.17 1.54 "
Arsenic 0.000 0.000 0.000 0.052 0.083 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.135
Cadmium 0.000 0.000 0.000 0.005 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013
Copper 0.000 0.000 0.000 1.661 1.454 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.115
Chromium 0.000 0.000 0.000 0.324 0.725 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.050
Lead 0.000 0.000 0.000 0.098 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.114
Mercury 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb- 0.000 0.000 0.000 0.079 0.179 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.257
denum
Nickel 0.000 0.000 0.000 0.334 0.108 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.442
Selenium 0.000 0.000 0.000 0.022 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.048
Zinc 0.000 0.000 0.000 4.728 0.229 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.957
Total
Phos- 0.000 0.000 0.000 104.112 9.130 0.000 0.000 0.000 0.000 0.000 0.000 0.000 113.242
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
-PA." v ar 3-.2,3 Q a
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 1 Acres Utilized: 44.6
Land Owner: Ben Myers Annual Dry Tons Applied: 227.6428 Site#: NC-UN18 Acres Permitted: 44.6
Operator: Same Predominant Soil Series: BdB2-Badin Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 122 Crop 2 Name: Fescue(Past.) Crop 2 Max.PAN: 50
Volume applied Volume Soil
�, PP Residual Sources Precip. a o 3 z Y Nitrate Name of Crop Type
a°i G (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 n w °: m 5 TKN o B and PAN Applied Receiving Residual
° Liquid Pert.,Animal (Dry' Hrs. o m ; N' * 44 ° (Ibs/acre)
Q 9 Solids Acre Wet, a o * P. Nitrite Application
Cu.Yds Gallons (DryTons/Ac) Waste,etc) inches ' ° o'
Moist) � � mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop I Crop 2
June 21 316 16.6 0.991 WWTP Cake D 0 S 0.5 0.3 51,900 3,280 65.7 32.274 NA Fescue
June 21 332 29.4 1.843 WTP Cake D 0 S 0.5 0.4 17,300 473 55 25.885 NA Fescue
July 21 162 23 0.704 WWTP Cake D 0 S 0.5 0.3 35,000 3,470 386 16.295 NA Fescue
July 21 144 32.1 0.873 WTP Cake D 0 S _0.5 0.4 14,700 1,650 1150 12.560 NA Fescue
Dec 21 108 28.3 0.577 WWTP Cake D 0 S 0.5 0.3 50,000 2400 1430 19.519 NA Fescue
Dec 21 18 34.4 0.117 WTP Cake D 0 S 0.5 0.4 14400 834 81.4 1.385 NA Fescue
0.000 0.000 0.000
J
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 - 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): I
TOTALS: 1080 0 As Cd Cu Cr Pb ' Hg Mo Ni Se Zn P 107.9191 0.000 Lime Applied
Annual lbs/acre 0.183 0.025 4.372 1.655 0.127 0.002 0.398 0.495 0.069 4.935 116.437 :: Date lbs/ac
Prior Years Cumulative lbs/ac 1.312 0.152 20.531 17.869 2.148 0.037 1.341 3.282 0.302 53.833 .:<•.•....
Current Cumulative lbs/ac 1.495 0.177 24.903 19.524 2.275 0.039 1.739 3.777 0.371 58.768
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit lst/2nd Crop .. .. . ..... . 122> 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
Ket" Fill *Application Method: S-Surface,IN-Injection,INC-Incorporation
01/114:2 02-3 -a?3 a a **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 227.68
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Ben Myers Owner: Same Predominant Soil Series: BdB2-Badin
Acres Used: 44.6 Acres Permitted: 44.6 Site#: NC-UN18 Field#: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or.J J J 1 5 1 6 ± J J 10 11 12
Com-
posite
Date 4/5/21 4/5/21 7/6/21 7/6/21 10/4/21 10/21/21 10/4/21
% Solids 16.6 29.4 23 32.1 20.8 28.3 34.4
Arsenic 12 27.1 9.48 14 10.3 41.3
Cadmium 1.16 2.58 2.91 4.02 1.31 3.23
Copper 383 473 400 s 461 345 442
Chromium 74.7 236 87 223 69.2 195
Lead 22.7 5.1 16.1 7.38 22 8.72
Mercury _ 0.489 0.0479 0.37 0.0482 0.477 0.0415
Molyb 18.1 58.2 20.2 50.5 16.8 49.1
denum
Nickel 77.1 35 60 27.4 63.9 32
Selenium 5 8.5 2.17 7.79 6.73 14.5
Zinc 1090 74.5 835 60.7 1030 125
Total
Phos- 24000 2970 19300 2260 22600 3080
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total J J 3 4 5 J 7 J 1101 11 12 y
DT/Ac./
App.
Event 0.99 1.84 0.70 0.87 0.58 0.12
Arsenic 0.000 0.000 0.000 0.024 0.100 0.000 0.013 0.024 0.000 0.012 0.000 0.010 0.183
Cadmium 0.000 0.000 0.000 0.002 0.010 0.000 0.004 0.007 0.000 0.002 0.000 0.001 0.025
Copper 0.000 0.000 0.000 0.759 1.743 0.000 0.563 0.805 0.000 0.398 0.000 0.103 4.372
Chromium 0.000 0.000 0.000 0.148 0.870 0.000 0.122 0.389 0.000 0.080 0.000 0.046 1.655
Lead 0.000 0.000 0.000 0.045 0.019 0.000 0.023 0.013 0.000 0.025 0.000 0.002 0.127
Mercury 0.000 0.000 0.000 0.001 0.000 0.000 0.001 0.000 0.000 0.001 0.000 0.000 0.002
Molyb- 0 000 0.000 0.000 0.036 0.215 0.000 0.028 0.088 0.000 0.019 0.000 0.011 0.398
denum
Nickel 0.000 0.000 0.000 0.153 0.129 0.000 0.084 0.048 0.000 0.074 0.000 0.007 0.495
Selenium 0.000 0.000 0.000 0.010 0.031 0.000 0.003 0.014 0.000 0.008 0.000 0.003 0.069
Zinc 0.000 0.000 0.000 2.160 0.275 0.000 1.176 0.106 0.000 1.189 0.000 0.029 4.935
Total
Phos- 0.000 0.000 0.000 47.568 10.947 0.000 27.174 3.946 0.000 26.080 0.000 0.721 116.437
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 2 Acres Utilized: 27.6
Land Owner: Ben Myers Annual Dry Tons Applied: 134.2946 Site#: NC-UN18 Acres Permitted: 27.6
Operator: Same Predominant Soil Series: GoB-Golston Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 135 Crop 2 Name: Fescue (Past.) Crop 2 Max.PAN: 50
y Volume applied Volume Residual Sources Soil Precip. > C
o Z. Nitrate Name of CropType
ou . (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 ? w ° m i2 TKN o ,, and PAN Applied ReceivingResidual
O Liquid Solids Acre Fert.,Animal (Dry' Hrs. o m * N' : (lbs/acre)
Q Wet, w w Nitrite Application
Cu.Yds Gallons (Dry Tons/Ac) Waste,etc) Moist) inches * =5. * E. mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Sept 21 216 23 1.516 WWTP Cake D 0 S 0.5 0.3 35,000 3,470 386 35.109 NA Fescue
Sept 21 342 32.1 3.350 WTP Cake D 0 S 0.5 0.4 14,700 1,650 1150 48.204 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 - 0.000 0.000 -
0.000 0.000 0.000
0.000 0.000 -
0.000
0.000 _ - 0.000 0.000
0.000 0.000 0.000
. : Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):-
TOTALS: 558 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 83.313 0.000 Lime Applied
Annual lbs/acre 0.123 0.036 4.302 1.758 0.098 0.001 0.400 0.366 0.059 2.938 73.660 Date lbslac
Prior Years Cumulative lbs/ac 4.994 0.497 31.014 21.067 5.286 1.443 4.097 5.466 2.465 71.38
Current Cumulative lbs/ac 5.117 0.533 35.316 22.825 5.384 1.444 4.497 5.832 2.524 74.318 ;.:
Permitted C.P.L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit lstl2nd Crop . .
13S 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
y�/j *Application Method: S-Surface,IN-Injection,INC-Incorporation
`-vV` / - f,1-14w 02- 3-09 Ida **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 134.30
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Ben Myers Owner: Same Predominant Soil Series: GoB-Golston
Acres Used: 27.6 Acres Permitted: 27.6 Site#: NC-UN18 Field#: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 31 5 6 _7_1 8 9 10 11 12
Com-
posite
Date 7/6/21 7/6/21
% Solids 23 32.1
Arsenic 9.48 14
Cadmium 2.91 4.02
Copper 400 461
Chromium 87 223
Lead 16.1 7.38
Mercury 0.37 0.0482
Molyb 20.2 50.5
denum
Nickel 60 27.4
Selenium 2.17 7.79
Zinc 835 60.7
Total
Phos- 19300 2260
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 J 3 4 J U 7 8 10 11 12
DT/Ac./
App.
Event 1.52 3.35
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.029 0.094 0.000 0.000 0.000 0.000 0.123
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.009 0.027 0.000 0.000 0.000 0.000 0.036
Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.213 3.089 0.000 0.000 0.000 0.000 4.302
Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.264 1.494 0.000 0.000 0.000 0.000 1.758
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.049 0.049 0.000 0.000 0.000 0.000 0.098
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.001
Molyb 0.000 0.000 0.000 0.000 0.000 0.000 0.061 0.338 0.000 0.000 0.000 0.000 0.400
denum
Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.182 0.184 0.000 0.000 0.000 0.000 0.366
Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.052 0.000 0.000 0.000 0.000 0.059
Zinc 0.000 0.000 0.000 0.000 0.000 0.000 2.532 0.407 0.000 0.000 0.000 0.000 2.938
Total
Phos- 0.000 0.000 0.000 0.000 0.000 0.000 58.518 15.142 0.000 0.000 0.000 0.000 73.66
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 7 Acres Utilized: 5,7
Land Owner: Ben Myers Annual Dry Tons Applied: 33.2591 Site#: NC-UNI8 Acres Permitted: 5.7
Operator: Same Predominant Soil Series: CmB-Cid Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 141 Crop 2 Name: Fescue (Past.) Crop 2 Max.PAN: 50
SoilVolume applied Volume Residual Sources Precip. > Co a
Nitrate Name of CropType
0 (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 0 r a m g TKN o and PAN Applied Receiving Residual
Liquid Solids Acre Fert. Animal (Dry' Hrs. o Cl F * ' c°Q, o (lbs/acre)
A Wet, * s; * ,�, �, Nitrite Application
Cu.Yds Gallons (DryTons/Ac) Waste,etc) inches * ° ° * o
Moist) g mg/kg mg/kg mg/kg Crop i Crop 2 Crop 1 Crop 2
May 21 126 16.6 3.090 WWTP Cake D 0 S 0.5 0.3 51,900 3,280 65.7 100.694 NA Fescue
Dec 21 54 34.4 2.745 WTP Cake D 0 S 0.5 0.4 14,400 834 81.4 32.522 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 - 0.000 0.000
- 0.000 - 0.000 0.000
0.000 _ 0.000 0.000 _
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
. Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 180 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 133.216 0.000 Lime Applied
Annual lbslacre 0.301 0.025 4.794 1.532 0.188 0.003 0.381 0.652 0.111 7.422 165.229 ;:,: :: Date lbs/ac
Prior Years Cumulative lbs/ac 0.855 0.126 20.582 7.689 1.166 0.021 1.414 3.282 0.357 37.765
Current Cumulative lbs/ac 1.156 0.151 25.376 9.221 1.354 0.024 1.795 3.934 0.468 45.187
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 1;.
Permit PAN Limit 1 st/2nd Crop
.. .. .. ..:I . 141 I 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
g1/ *Application Method: S-Surface,IN-Injection,INC-Incorporation
e-1..- M a- 3-a a a **Volatilization Rate: Surface-0.5,Injection/Incorporation-1.0
***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
Signature of Land Applier Date
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 33.26
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Ben Myers Owner: Same Predominant Soil Series: CmB-Cid
Acres Used: 5.7 Acres Permitted: 5.7 Site#: NC-UN18 Field#: 7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % SoIids use Raw Percent#):
Sample on 1 1 2 1 3 I 4 f 5 6 U 181 9 10 11 12
Com-
posite
Date 4/5/21 10/4/21
% Solids 16.6 34.4
Arsenic 12 41.3
Cadmium 1.16 3.23
Copper 383 442
Chromium 74.7 195
Lead 22.7 8.72
Mercury 0.489 0.0415
Molyb- 18.1 49.1
denum
Nickel 77.1 32
Selenium s 5 14.5
Zinc 1090 125
Total
Phos- 24000 3080
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total ?J 13 J 6 7 3 J 10 11 112 y
DT/Ac./ a
eq-
App.
Event 3.09 2.75
Arsenic 0.000 0.000 0.000 0.074 0.000 0.000 0.000 0.000 0.000 0.227 0.000 0.000 0.301
Cadmium 0.000 0.000 0.000 0.007 0.000 0.000 0.000 0.000 0.000 0.018 0.000 0.000 0.025
Copper 0.000 0.000 0.000 2.367 0.000 0.000 0.000 0.000 0.000 2.427 0.000 0.000 4.794
Chromium 0.000 0.000 0.000 0.462 0.000 0.000 0.000 0.000 0.000 1.071 0.000 0.000 1.532
Lead 0.000 0.000 0.000 0.140 0.000 0.000 0.000 0.000 0.000 0.048 0.000 0.000 0.188
Mercury 0.000 0.000 0.000 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003
Molyb 0.000 0.000 0.000 0.112 0.000 0.000 0.000 0.000 0.000 0.270 0.000 0.000 0.381
denum
Nickel 0.000 0.000 0.000 0.476 0.000 0.000 0.000 0.000 0.000 0.176 0.000 0.000 0.652
Selenium 0.000 0.000 0.000 0.031 0.000 0.000 0.000 0.000 0.000 0.080 0.000 0.000 0.111
Zinc 0.000 0.000 0.000 6.736 0.000 0.000 0.000 0.000 0.000 0.686 0.000 0.000 7.422
Total
Phos- 0.000 0.000 0.000 148.320 0.000 0.000 0.000 0.000 0.000 16.909 0.000 0.000 165.23
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 8 Acres Utilized: 16
Land Owner: Ben Myers Annual Dry Tons Applied: 75.0073 Site#: NC-UN18 Acres Permitted: 16
Operator: Same Predominant Soil Series: CmB-Cid Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 141 Crop 2 Name: Fescue(Past.) Crop 2 Max.PAN: 50
Volume applied Volume Soil
6. pp Residual Sources Precip. o 4 z Nitrate Name of Crop Type
c (enter one)Solids) oho Appliedper Cond. 3,� ;e m �, PAN Applied
y pp (NPDES#,WQ#, Fast 24 w m TKN o g and ReceivingResidual
2 8 Liquid Fert. Animal (pry' Hrs. o 9 N nr r°Oc ° (]bs/acre)
Q 4 Solids Acre Wet y * ❑ w. Nitrite Application
Cu.Yds Gallons (DryTons1Ac Waste,etc) inches * = 5 * o
) Moist) B mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
May 21 270 16.6 2.359 WWTP Cake D 0 S 0.5 0.3 51,900 3,280 65.7 76.869 NA Fescue
May 21 18 29.4 0.279 WTP Cake D 0 S 0.5 0.4 17,300 473 54.8 3.912 NA Fescue
Dec 21 72 28.3 1.073 WWTP Cake D 0 S 0.5 0.3 50000 2400 1430 36.272 NA Fescue
'
Dec 21 54 34.4 0.978 WTP Cake D 0 S 0.5 0.4 14400 834 81.4 11.586 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS:_ 414 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 128.639 0.000 Lime Applied
Annual lbs/acre 0.175 0.016 3.676 1.014 0.174 0.003 0.250 0.583 0.071 7.639 169.413 .::: :::::::::•:•:::::.:.::. Date lbs/ac
Prior Years Cumulative lbs/ac 0.789 0.123 17.84 4.441 1.176 0.027 1.268 1.543 0.212 34.792
Current Cumulative lbs/ac 0.964 0.139 21.516 5.455 1.350 0.030 1.518 2.126 0.283 42.431
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit 1 st/2nd Crop [ . ... ..... .. .. ... . ... 141 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
t'a"- is/1 e ittiy- 07- 3-2"'a **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 75.02
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Ben Myers Owner: Same Predominant Soil Series: CmB-Cid
Acres Used: 16 Acres Permitted: 16 Site#: NC-UN18 Field#: 8
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1- ?1 3 J 51 J 9 10 11 12
Com-
posite
Date 4/5/21 415/21 10/4/21 10/21/21 10/4/21
%Solids 16.6 29.4 20.8 28.3 34.4
Arsenic s 12 27.1 10.3 41.3
Cadmium 1.16 2.58 1.31 3.23
Copper 383 473 345 442
Chromium 74.7 236 69.2 195
Lead 22.7 5.1 22 8.72
Mercury 0.489 0.0479 0.477 0.0415
Molyb-
denum 18.1 58.2 16.8 49.1
Nickel 77.1 35 63.9 32
Selenium 5 8.5 6.73 14.5
_ Zinc 1090 74.5 1030 125
Total
Phos- 24000 2970 22600 3080
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 2J 13I J 151 J 7 J 9J 10 11 12
DT/Ac./ o
App. ?o
Event 2.36 0.28 1.07 0.98
Arsenic 0.000 0.000 0.000 0.057 0.015 0.000 0.000 0.000 0.000 0.022 0.000 0.081 0.175
Cadmium 0.000 0.000 0.000 0.005 0.001 0.000 0.000 0.000 0.000 0.003 0.000 0.006 0.016
Copper 0.000 0.000 0.000 1.807 0.264 0.000 0.000 0.000 0.000 0.740 0.000 0.865 3.676
Chromium 0.000 0.000 0.000 0.352 0.132 0.000 0.000 0.000 0.000 0.149 0.000 0.381 1.014
Lead 0.000 0.000 0.000 0.107 0.003 0.000 0.000 0.000 0.000 0.047 0.000 0.017 0.174
Mercury 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.003
Molyb 0 000 0.000 0.000 0.085 0.032 0.000 0.000 0.000 0.000 0.036 0.000 0.096 0.250
denum
Nickel 0.000 0.000 0.000 0.364 0.020 0.000 0.000 0.000 0.000 0.137 0.000 0.063 0.583
Selenium 0.000 0.000 0.000 0.024 0.005 0.000 0.000 0.000 0.000 0.014 0.000 0.028 0.071
Zinc 0.000 0.000 0.000 5.143 0.042 0.000 0.000 0.000 0.000 2.210 0.000 0.245 7.639
Total
Phos- 0.000 0.000 0.000 113.232 1.657 0.000 0.000 0.000 0.000 48.500 0.000 6.024 169.41
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
.�a,. )1/1 ►.6c• a- 07044
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 1 Acres Utilized: 24.5 _
Land Owner: William Griffin Annual Dry Tons Applied: 81.7649 Site#: NC-UN29 Acres Permitted: 24.5
Operator: Same Predominant Soil Series: GoC-Golston Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 116 Crop 2 Name: Fescue(Past.) Crop 2 Max.PAN: 50
Volume applied Volume Soil
PP Residual Sources Precip. y o Z Y Nitrate Name of Crop Type
(enter one)Solids/ % Appliedper Cond. ;n m ;v q PAN Applied
y PP (NPDES#,WQ#, Past 24 cn m .i
o D n. = TKN o and (ibs/acre) Receiving Residual
ro Liquid Solids Acre Fert.,Animal ( ry' Hrs. o N' * ro
QWet, c, * m * w Nitrite Application
Cu.Yds Gallons Waste,etc)
(Dry Tons/Ac) Moist) inches * s * . mg/kg mg/kg mg/kg Crop I Crop 2 ^Crop 1 Crop 2
May 21 344 16.6 1.963 WWTP Cake D 0 S 0.5 0.3 51,900 3,280 65.7 63.958 NA Fescue
May 21 136 29.4 1.374 WTP Cake D 0 S 0.5 0.4 17,300 473 54.8 19.303 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
J
0.000 0.000 0.000
0.000 0.000 0.000
0.000 -
0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 1 1 0.000 0.000
..,. Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS; 480 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 83.261 10.000 Lime Applied
Annual lbs/acre 0.122 0.012 2.803 0.942 0.103 0.002 0.231 0.399 0.043 4.484 102.386 Date lbs/ac
Prior Years Cumulative lbs/ac 0.475 0.068 11.195 4.698 0.766 0.031 0.857 1.804 0.2 19.973
Current Cumulative lbs/ac 0.597 0.080 13.998 5.640 0.869 0.033 1.088 2.203 0.243 24.457
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit l st/2nd Crop 116 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
� *Application Method: S-Surface,IN-Injection,INC-Incorporation
i' 1�I.n. e11. 02-- 3-o2 0 z a- **Volatilization Rate: Surface-0.5,Injection/Incorporation-1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 81.76
Permit#: WQ0003146 Cation Exchange Capacity(non 503 only): N/A
Operator: William Griffin Owner: Same Predominant Soil Series: GoC-Golston
Acres Used: 24.5 Acres Permitted: 24.5 Site#: NC-UN29 Field#: 1
Residual Analysis Data (Heavy1 Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 9 2 i J 9 10 11 12
Com-
posite
Date 4/5/21 4/5/21
% Solids 16.6 29.4
Arsenic 12 27.1
Cadmium 1.16 2.58
Copper 383 473
Chromium 74.7 236
Lead 22.7 5.1
Mercury 0.489 0.0479
Molyb-
denum 18.1 58.2
Nickel 77.1 35
Selenium 5 8.5
Zinc 1090 74.5
Total
Phos- 24000 2970
phorus
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total 9 12 1 3 4J 5 7 L 1 9 I IL I) • 1 12 y
DT/Ac./ o
App. CA
Event 1.96 1.37
Arsenic 0.000 0.000 0.000 0.047 0.074 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.122
Cadmium 0.000 0.000 0.000 0.005 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012
Copper 0.000 0.000 0.000 1.504 1.300 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.803
Chromium 0.000 0.000 0.000 0.293 0.649 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.942
Lead 0.000 0.000 0.000 0.089 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.103
Mercury 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb- 0 000 0.000 0.000 0.071 0.160 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.231
denum
Nickel 0.000 0.000 0.000 0.303 0.096 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.399
Selenium 0.000 0.000 0.000 0.020 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.043
Zinc 0.000 0.000 0.000 4.279 0.205 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.484
Total
Phos- 0.000 0.000 0.000 94.224 8.162 0.000 0.000 0.000 0.000 0.000 0.000 0.000 102.386
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
-Kg- Wl,1vU-- a- 3- ao..2a.
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 2 Acres Utilized: 5.7
Land Owner: William Griffin Annual Dry Tons Applied: 21.0476 Site#: NC-UN29 Acres Permitted: 5.7
Operator: Same Predominant Soil Series: GoC-Goldston Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 116 Crop 2 Name: Fescue (Past.) Crop 2 Max.PAN: 50
Volume applied Volume Soil
L pp Residual Sources Precip• a o Z. a Nitrate Name of CropType
(enter one)Solids/ % Appliedper Cond. q z PAN Applied
:) pp (NPDES#,WQ#, Past 24 'o F M o
TKN o and ReceivingResidual
Q Liquid Solids Acre Fert.,Animal (Dry' Hrs. o w N' * B (lbs/acre)
Wet n * �, * w• Nitrite Application
Cu.Yds GallonsWaste,etc) * ' E.
(DryTonslAc) Moist) inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Aug 21 64 23 2.175 WWTP Cake D 0 S 0.5 0.3 35,000 3,470 386 50.370 NA Fescue
Aug 21 32 32.1 1.518 WTP Cake D 0 S 0.5 0.4 14,700 1650 1150 21.839 NA Fescue
0.000 - 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 -
0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 96 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 72.210 0.000 Lime Applied
Annual lbs/acre 0.084 0.025 3.140 1.055 0.092 0.002 0.241 0.344 0.033 3.817 90.816 Date lbs/ac
Prior Years Cumulative lbs/ac 0.755 0.106 18.328 6.548 1.315 0.017 1.456 2.682 0.25 30.798
July 18 2165
Current Cumulative lbs/ac 0.839 0.131 21.468 7.603 1.407 0.019 1.697 3.026 0.283 34.615
Permitted C. P.L. R.**** 36 34 1338 X 267 15 X 374 89 2498 '::::: :: : l
Permit PAN Limit lstl2nd Crop ..'....
116 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
X.a.--1,-. /14erJ1/L.- a.-3 -j a a a'` **Volatilization Rate: Surface-0.5,Injection/Incorporation-1.0
Signature of Land Applier Date ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.:Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 21.05
Permit#: WQ0001346 Cation Exchange Capacity (non 503 only): N/A
Operator: William Griffin Owner: Same Predominant Soil Series: GoC-Goldston
Acres Used: 5.7 Acres Permitted: 5.7 Site#: NC-UN29 Field#: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, °A) Solids use Raw Percent#):
Sample or 2 13 I 4 5 ? 8 1101 11 j 12
Com-
posite
Date 7/6/21 7/6/21
%Solids 23 32.1
Arsenic 9.48 14
Cadmium 2.91 4.02
Copper 400 461
Chromium 87 223
Lead 16.1 7.38
Mercury 0.37 0.0482
Molyb- 20.2 50.5
denum
Nickel 60 27.4
Selenium 2.17 7.79
Zinc 835 60.7
Total
Phos- 19300 2260
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 1 21 J a 5 1 B 7 f 8 9 110 I 11 112 I
DT/Ac./
App.
Event 2.18 1.52
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.041 0.043 0.000 0.000 0.000 0.000 0.084
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.013 0.012 0.000 0.000 0.000 0.000 0.025
Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.740 1.400 0.000 0.000 0.000 0.000 3.140
Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.378 0.677 0.000 0.000 0.000 0.000 1.055
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.070 0.022 0.000 0.000 0.000 0.000 0.092
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.000 0.000 0.000 0.000 0.000 0.000 0.088 0.153 0.000 0.000 0.000 0.000 0.241
denum
Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.261 0.083 0.000 0.000 0.000 0.000 0.344
Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.009 0.024 0.000 0.000 0.000 0.000 0.033
Zinc 0.000 0.000 0.000 0.000 0.000 0.000 3.632 0.184 0.000 0.000 0.000 0.000 3.817
Total
Phos- 0.000 0.000 0.000 0.000 0.000 0.000 83.955 6.861 0.000 0.000 0.000 0.000 90.816
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
/V?9-vu a -3-aDaa
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 3 Acres Utilized: 7.4
Land Owner: William Griffin Annual Dry Tons Applied: 43.4578 Site#: NC-UN29 Acres Permitted: 7.4'
Operator: Same Predominant Soil Series: BaB-Badin Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max.PAN: 50
Volume applied Volume Soil
PP Residual Sources Precip. > c Z 8 Nitrate Name of Crop Type
° (enter one)Solids/ % Appliedper Cond. a ;� �, �' PAN Applied
o (NPDES#,WQ#, D Past 24 C' m 16 TKN 1 o and (lbs/acre) ReceivingResidual
cC Liquid Solids Acre Fert.,Animal ( ry' Hrs. o * Fr * N 0 °
q Wet, o �• +� w d Nitrite Application
Waste,etc) * o
Cu.Yds Gallons (Dry Tons/Ac) Moist) inches a g' mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
July 21 64 23 1.675 WWTP Cake D 0 S _ 0.5 0.3 35,000 3,470 386 38.799 NA _Fescue
July 21 48 32.1 1.754 WTP Cake D 0 S 0.5 0.4 14,700 1650 1150 25.233 NA Fescue
Aug 21 18 23 0.471 WWTP Cake D 0 S 0.5 0.3 35000 3470 386 10.912 NA Fescue
Aug 21 54 32.1 1.973 WTP Cake D 0 S 0.5 0.4 14700 1650 1150 28.388 NA Fescue
- 0.000 0.000 0.000
0.000 _ 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000 •
0.000 0.000 0.000 T I
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 184 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 103.3321 0.000 Lime Applied
Annual lbs/acre 0.145 0.042 5.153 2.036 0.124 0.002 0.463 0.462 0.067 4.036 99.682 Date lbs/ac
Prior Years Cumulative lbs/ac 1.05 0.138 27.936 10.899 1.458 0.027 2.079 4.095 0.917 44.613 :
Current Cumulative lbs/ac 1.195 0.180 33.089 12.935 1.582 0.029 2.542 4.557 0.984 48.649
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit 1st12nd Crop : .. .. . H H in 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
�( 1,,A *Application Method: S-Surface,IN-Injection,INC-Incorporation
<tfi- i 14014.E 02- 3-a3a9Z **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobiaily digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 43.46
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: William Griffin Owner: Same Predominant Soil Series: BaB-Badin
Acres Used: 7.4 Acres Permitted: 7.4 Site#: NC-UN29 Field#: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 J f 4 6 7 8 9 10 11 12
Com-
posite
Date 7/6/21 7/6/21
% Solids 23 32.1
Arsenic 9.48 14
Cadmium 2.91 4.02
Copper _ 400 461
Chromium 87 223
Lead 16.1 7.38
Mercury 0.37 0.0482
Molyb-
denum 20.2 50.5
Nickel 60 27.4
Selenium 2.17 7.79
Zinc 835 60.7
Total
Phos- 19300 2260
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 11 i 2 4 5 J L J 9J 10 11j 1121 y
DT/Ac./
App.
Event 2.15 3.73 "
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.041 0.104 0.000 0.000 0.000 0.000 0.145
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.012 0.030 0.000 0.000 0.000 0.000 0.042
Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.717 3.436 0.000 0.000 0.000 0.000 5.153 _
Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.373 1.662 0.000 0.000 0.000 0.000 2.036
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.069 0.055 0.000 0.000 0.000 0.000 0.124
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.000 0.000 0.000 0.000 0.000 0.000 0.087 0.376 0.000 0.000 0.000 0.000 0.463
denum
Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.258 0.204 0.000 0.000 0.000 0.000 0.462
Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.009 0.058 0.000 0.000 0.000 0.000 0.067
Zinc 0.000 0.000 0.000 0.000 0.000 0.000 3.584 0.452 0.000 0.000 0.000 0.000 4.036
Total
Phos- 0.000 0.000 0.000 0.000 0.000 0.000 82.836 16.846 0.000 0.000 0.000 0.000 99.682
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
/V1yi. .
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 4 Acres Utilized: 2.9
Land Owner: William Griffin Annual Dry Tons Applied: 9.4896 Site#: NC-UN29 Acres Permitted: 2.9
Operator: Same Predominant Soil Series: BdB2-Badin Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max.PAN: 50
Volume applied Volume Soil
,� PP Residual Sources Precip. Y o Z. a Nitrate Name of Crop Type
Q -. (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 '' m TKN o and PAN Applied Receiving Residual
Q Liquid Solids Acre Fert.,Animal (Dry' Hrs. o w * Nl If =: g Ibs/acre
N ❑ Nitrite ( ) Application
Wet, * 0' ' * °: =
Cu.Yds Gallons (DryTons/Ac) Waste,etc) inches = 5 mg/kg mg/kg mg/kg Crop1 Crop2 Crop1 Crop2
Moist) ❑ s 9 9 s s s
June 21 36 16.60 1.735 WWTP Cake D 0 S 0.5 0.3 51,900 3,280 65.7 56.547 NA Fescue
June 21 18 29.4 1.537 WTP Cake D 0 S 0.5 0.4 17300 473 54.8 21.583 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 541 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 78.131 10.000 Lime Applied
Annual lbs/acre 0.125 0.012 2.783 0.985 0.094 0.002 0.242 0.375 0.043 4.011 92.410 Date ' lbs/ac
Prior Years Cumulative lbs/ac 0.841 0.091 16.458 7.07 0.707 0.013 1.48 1.756 0.359 20.197
Current Cumulative lbs/ac _ 0966 0.103 19.241 8.055 _ 0.801 0.015 1.722 2.131 0.402 24.208
Permitted C. P. L.R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit l stl2nd Crop :::; 122 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
KL., .2 - 3 02 0aa **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.:Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 9.49
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: William Griffin Owner: Same Predominant Soil Series: BdB2-Badin
Acres Used: 2.9 Acres Permitted: 2.9 Site#: NC-UN29 Field#: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use rng/kg, % Solids use Raw Percent#):
Sample orb J 3 J 5 ? J 9 110 I 11 j I12
Com-
posite
Date 4/5/21 4/5/21
% Solids 16.6 29.4
Arsenic 12 27.1
Cadmium 1.16 2.58
Copper 383 473
Chromium 74.7 236
Lead 22.7 5.1
Mercury 0.489 0.0479
Molyb-
denum 18.1 58.2
Nickel 77.1 35
Selenium 5 8.5
Zinc 1090 74.5
Total
Phos- 24000 2970
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 J 13I 141 5 6I J 9 •I 11 12
DT/Ac./ c
App. m
Event 1.74 1.54
Arsenic 0.000 0.000 0.000 0.042 0.083 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.125
Cadmium 0.000 0.000 0.000 0.004 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012
Copper 0.000 0.000 0.000 1.329 1.454 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.783
Chromium 0.000 0.000 0.000 0.259 0.725 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.985
Lead 0.000 0.000 0.000 0.079 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.094
Mercury 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.000 0.000 0.000 0.063 0.179 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.242
denum
Nickel 0.000 0.000 0.000 0.268 0.108 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.375
Selenium 0.000 0.000 0.000 0.017 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.043
Zinc 0.000 0.000 0.000 3.782 0.229 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.011
Total
Phos- 0.000 0.000 0.000 83.280 9.130 0.000 0.000 0.000 0.000 0.000 0.000 0.000 92.410
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 5 Acres Utilized: 2.2
Land Owner: William Griffin Annual Dry Tons Applied: 7.4246 Site#: NC-UN29 Acres Permitted: 2.2
Operator: Same Predominant Soil Series: CmB-Cid Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 141 Crop 2 Name: Fescue(Past.) Crop 2 Max.PAN: 50
Volume applied Volume Residual Sources Soil Precip. s. o z Nitrate Name of Crop Type
0 (enterone) % Applied per (NPDES# WQ#, Cond. Past 24 co j° ?; w c PAN Applied
Solids! „ ,- TKN o 3 and Receiving Residual
c� Liquid Fert.,Animal (Dry' Hrs. a w� * w ' 0 = {lbs/acre)
9 Solids Acre N 5 Nitrite Application
Q Wet, �. a• * ^ * w' pP
Cu.Yds Gallons (Dry Tons/Ac) Waste,etc) Moist) inches 5 0g. mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Aug 21 16 23 1.409 WWTP Cake D 0 S 0.5 0.3 35,000 3,470 386 32.626 NA Fescue
Aug 21 16 32.1 1.966 WTP Cake D 0 S 0.5 0.4 14,700 1650 1 150 28.292 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
-
0.000 0.000 0.000
- 0.000 0.000 0.000
0.000 0.000 0.000
-
0.000 - 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
- Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 32 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 60.918 I 0.000 Lime Applied
A.nnuallbs/acre 0.082 0.024 2.940 1.122 0.074 0.001 0.255 0.277 0.037 2.592 63.274 Date lbs/ac
Prior Years Cumulative lbs/ac 0.755 0.106 18.328 6.548 1.315 0.017 1.456 2.682 0.25 30.798 July 18 2165
Current Cumulative lbs/ac 0.837 0.130 21.268 7.670 1.389 0.018 1.711 2.959 0.287 33.390
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit lst/2nd Crop ... . . .... .. .. 141 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
Ko.4.--. ja 01.4.0 a -3 -az2 **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 7.43
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: William Griffin Owner: Same Predominant Soil Series: CmB-Cid
Acres Used: 2.2 Acres Permitted: 2.2 Site#: NC-UN29 Field#: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample on 1 J J t 4 I 5 6 7 8 9 10 11 12
Com-
posite
Date 7/6/21 7/6/21
% Solids 23 32.1
Arsenic 9.48 14
Cadmium 2.91 4.02
Copper 400 461
Chromium 87 223
Lead 16.1 7.38
Mercury 0.37 0.0482
Molyb- 20.2 50.5
denum
Nickel 60 27.4
Selenium _ 2.17 7.79
Zinc 835 60.7
Total
Phos- 19300 2260
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 J J 4 J 6 21 8 9 10 11 12 y
DT/Ac./
App.
_ Event 1.41 1.97
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.027 0.055 0.000 0.000 0.000 0.000 0.082
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.008 0.016 0.000 0.000 0.000 0.000 0.024
Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.127 1.813 0.000 0.000 0.000 0.000 2.940
Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.245 0.877 0.000 0.000 0.000 0.000 1.122
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.045 0.029 0.000 0.000 0.000 0.000 0.074
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.001
Molyh- 0.000 0.000 0.000 0.000 0.000 0.000 0.057 0.199 0.000 0.000 0.000 0.000 0.255
denum
Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.169 0.108 0.000 0.000 0.000 0.000 0.277
Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.006 0.031 0.000 0.000 0.000 0.000 0.037
Zinc 0.000 0.000 0.000 0.000 0.000 0.000 2.353 0.239 0.000 0.000 0.000 0.000 2.592
Total
Phos- 0.000 0.000 0.000 0.000 0.000 0.000 54.387 8.886 0.000 0.000 0.000 0.000 63.274
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
�-t,- i14.%-vut..„ a 3 ^ a,D a a-.
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 1 Acres Utilized: 13.1
Land Owner: Tom Appenzeller Annual Dry Tons Applied: 53.2691 Site#: UN-UN30 Acres Permitted: 13.1
Operator: William Griffin Predominant Soil Series: BdB2-Badin Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max.PAN: 50
Volume applied Volume Soil
s., PP Residual Sources Precip. y c a Nitrate Name of Crop Type
c' (enter one)Solids/ % Applied per (NPDES#,WQ#, C°nd' Past 24 w TKN o and PAN Applied Receiving Residual
Fert.,Animal (Dry' Hrs. F a % N' * -• 2 (lbs/acre)
Q Liquid Solids Acre Wet, * °� * w �. Nitrite Application
Waste,etc) a o'
Cu.Yds Gallons (Dry Tons/Ac) Moist) inches * § mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
June 21 126 16.6 1.345 WWTP Cake D 0 S 0.5 0.3 51,900 3,280 65.7 43.813 NA Fescue
June 21 144 29.4 2.722 WTP Cake D 0 S 0.5 0.4 17,300 473 54.8 38.224 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 r 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 270 4:: ::H: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 82.037 0.000 Lime Applied
Annual lbs/acre 0.180 0.017 3.605 1.486 0.089 0.002 0.366 0.398 0.060 3.338 80.729 Date lbs/ac
Prior Years Cumulative lbs/ac 1.305 0.154 23.559 9.756 1.221 0.023 2.104 2.902 0.562 37.272
Current Cumulative lbs/ac 1.485 0.171 27.164 11.242 1.310 0.025 2.470 3.300 0.622 40.610
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit l stl2nd Crop ::.; :>::>: ...... 122 I 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
�/ *Application Method: S-Surface,IN-Injection,INC-Incorporation
/ -h s'y...So a - 3- a`:a al **Volatilization Rate: Surface-0.5,Injection/Incorporation-1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 53.28
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Tom Appenzeller Owner: William Griffin Predominant Soil Series: BdB2-Badin
Acres Used: 13.1 Acres Permitted: 13.1 Site#: NC-UN30 Field#: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 2 3 4_1 15 I 16 I 7 ' 8 9 10 11 12
Com-
posite
Date 4/5/21 4/5/21
% Solids 16.6 29.4
Arsenic 12 27.1
Cadmium 1.16 2.58
Copper 383 473
Chromium 74.7 236
Lead 22.7 5.1
Mercury 0.489 0.0479
Molyb- 18.1 58.2
denum
Nickel _ 77.1 35
Selenium 5 8.5
Zinc 1090 74.5
Total
Phos- 24000 2970
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total J J 5 6 9 10 11 12
DT/Ac./
rt
App.
Event 1.35 2.72
Arsenic 0.000 0.000 0.000 0.032 0.148 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.180
Cadmium 0.000 0.000 0.000 0.003 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017
Copper 0.000 0.000 0.000 1.030 2.575 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.605
Chromium 0.000 0.000 0.000 0.201 1.285 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.486
Lead 0.000 0.000 0.000 0.061 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.089
Mercury 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.000 0.000 0.000 0.049 0.317 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.366
denum
Nickel 0.000 0.000 0.000 0.207 0.191 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.398
Selenium 0.000 0.000 0.000 0.013 0.046 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.060
Zinc 0.000 0.000 0.000 2.932 0.406 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.338
Total
Phos- 0.000 0.000 0.000 64.560 16.169 0.000 0.000 0.000 0.000 0.000 0.000 0.000 80.729
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
- 3-02 o 2 a.
Signature of Land AppIier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 4 Acres Utilized: 15.2
Land Owner: Tom Appenzeller Annual Dry Tons Applied: 50.5641 Site#: NC-UN30 Acres Permitted: 15.2
Operator: Same Predominant Soil Series: BaB-Badin Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max.PAN: 50
Soil
Volume applied Volume Residual Sources Precip. > c Z. a Nitrate Name of Crop Type
(enter one)Solids/ % Appliedper Cond. c z PAN Applied
y (NPDES#,WQ#, Past 24 _ w TKN o and ReceivingResidual
o D -- (]hslacre)
Liquid Solids Acre ( rY, K " a
Fert.,Animal Wet Hrs. o� * p. * �. Nitrite Application
Waste,etc) * o' o
Cu.Yds Gallons (Dry Tons/Ac) Moist) inches g o mg/kg mg/kg mg/kg Crop I Crop 2 Crop 1 Crop 2
June 21 220 16.6 _ 2.023 WWTP Cake D 0 S 0.5 0.3 51,900 3,280 65.7 65.930 NA Fescue
June 21 80 29.4 1.303 WTP cake D 0 S 0.5 0.4 17,300 473 54.8 18.302 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
_ 0.000 0.000 0.000
0.000 0.000 0.000 _
0.000 0.000 0.000 _
0.000 0.000 0.000
0.000 0.000 0.000
_
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 300 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 84.232 10.000 Lime Applied
Annual lbs/acre 0.119 0.011 2.782 0.917 0.105 0.002 0.225 0.403 0.042 4.604 104.844 :: Date lbs/ac
Prior Years Cumulative lbs/ac 0.253 0.038 5.715 2.44 0.471 0.008 0.529 0.763 0.087 11.055
Current Cumulative lbs/ac 0.372 0.049 8.497 3.357 0.576 0.010 0.754 1.166 0.129 15.659
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 : : •• .:: ` ::
Permit PAN Limit l stJ2nd Crop .... . . . 122 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
i4•L„ 1t1 91 . a -3-a .2a **Volatilization Rate: Surface-0.5,InjectionILncorporation-1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 50.56
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Tom Appenzeller Owner: Same Predominant Soil Series: BaB-Badin
Acres Used: 15.2 Acres Permitted: 15.2 Site#: NC-UN30 Field#: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample on 1 2 4 6 7 i 18 ±I 10 11 12
Com-
posite
Date 4/5121 4/5/21
•
% Solids 16.6 29.4
Arsenic 12 27.1
Cadmium 1.16 2.58
Copper 383 473
Chromium 74.7 236
Lead 22.7 5.1
Mercury 0.489 0.0479
Molyb 18.1 58.2
denum
Nickel 77.1 35
Selenium 5 8.5
Zinc 1090 74.5
Total
Phos- 24000 2970
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total J L? 3 4 J 6 L 8J 19 r 10 11 12
DT/Ac./ 0-3
App.
Event 2.02 1.30
Arsenic 0.000 0.000 0.000 0.049 0.071 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.119
Cadmium 0.000 0.000 0.000 0.005 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011
Copper 0.000 0.000 0.000 1.550 1.233 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.782
Chromium 0.000 0.000 0.000 0.302 0.615 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.917
Lead 0.000 0.000 0.000 0.092 0.013 0.000 - 0.000 0.000 0.000 0.000 0.000 0.000 0.105
Mercury 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.000 0.000 0.000 0.073 0.152 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.225
denum
Nickel 0.000 0.000 0.000 0.312 0.091 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.403
Selenium 0.000 0.000 0.000 0.020 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042
Zinc 0.000 0.000 0.000 4.410 0.194 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.604
Total
Phos- 0.000 0.000 0.000 97.104 7.740 0.000 0.000 0.000 0.000 0.000 0.000 0.000 104.844
phorus
"I certify,under penally of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
i< 1'4& a - 3- a3a
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 5 Acres Utilized: 10.8
Land Owner: Tom Appenzeller Annual Dry Tons Applied: 39.4272 Site#: NC-UN30 Acres Permitted: 10.8
Operator: Same Predominant Soil Series: BaB-Badin Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max.PAN: 50
I.
Volume applied Volume Residual Sources SOil Precip. > o 3 2 Nitrate Name of Crop Type
° (enter one)Solids/ % AppliedperCond. K I po m 7c q PAN Applied
° Pp (NPDES#,WQ#, Past 24 c- • a m TKN o and ReceivingResidual
Fert.,Animal D cm o
Firs. o ° * N' * • (lbs/acre)
Q Liquid Solids Acre We * K. * o �. Nitrite Application
Waste,etc) '" °
Cu.Yds Gallons (Dry Tons/Ac) Moist) inches ' mg/kg mg/kg mg/kg Crop I Crop 2 Crop 1 Crop 2
June 21 112 16.6 1.450 WWTP Cake D 0 S 0.5 0.3 51,900 3,280 65.7 47.239 NA Fescue
June 21 96 29.4 2.201 WTP Cake D 0 S 0.5 0.4 17,300 473 54.8 30.910 NA Fescue
0.000 0.000 - 0.000
0.000 0.000 0.000
-
0.000 _ 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 2081 o As Cd Cu Cr Pb Hg Mo Ni Se Zn P _78.149 10.000 Lime Applied
Annual lbs/acre 0.154 0.015 3.193 1.256 0.088 0.002 0.309 0.378 0.052 3.489 82.674 : ::: :.:..::..: Date lbs/ac
Prior Years Cumulative lbs/ac 0.72 0.1 14.027 6.151 0.776 0.016 1.299 1.681 0.318 22.298 ..
Current Cumulative lbs/ac 0.874 0.115 17.220 7.407 0.864 0.018 1.608 2.059 0.370 25.787
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit l st/2nd Crop 122.: 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
-4-+-.- 1'I4&ww9 o?- 3--2 as **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 39.43
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Tom Appenzeller Owner: Same Predominant Soil Series: BaB-Badin
Acres Used: 10.8 Acres Permitted: 10.8 Site#: NC-UN30 Field#: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 2 J 4 1 6 7 8_1 9 10 11 112 f
Com-
posite
Date 4/5/21 4/5/21
% Solids 16.6 29.4
Arsenic 12 27.1
Cadmium 1.16 2.58
Copper 383 473
Chromium 74.7 236
Lead 22.7 5.1
Mercury 0.489 0.0479
Molyb- 18.1 58.2
denum
Nickel 77.1 35
Selenium 5 8.5
Zinc 1090 74.5
Total
Phos- 24000 2970
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 2 J 4 s 1 j jJ 8 J 10 111 I 12
DT/Ac./ c
App.
Event 1.45 2.20
Arsenic 0.000 0.000 0.000 0.035 0.119 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.154
Cadmium 0.000 0.000 0.000 0.003 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015
Copper 0.000 0.000 0.000 1.111 2.082 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.193
Chromium 0.000 0.000 0.000 0.217 1.039 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.256
Lead 0.000 0.000 0.000 0.066 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.088
Mercury 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.000 0.000 0.000 0.052 0.256 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.309
denum
Nickel 0.000 0.000 0.000 0.224 0.154 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.378
Selenium 0.000 0.000 0.000 0.015 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.052
Zinc 0.000 0.000 0.000 3.161 0.328 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.489
Total
Phos- 0.000 0.000 0.000 69.600 13.074 0.000 0.000 0.000 0.000 0.000 0.000 0.000 82.674
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
a.- 3 -a o a a
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 3 Acres Utilized: 2.5
Land Owner: Henry Myers Annual Dry Tons Applied: 13.9464 Site#: NC-UN31 Acres Permitted: 2.5
Operator: Same Predominant Soil Series: BdB2-Badin Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max.PAN: 50
Volume applied Volume Residual Sources Soil Precip. y o 4 z a Nitrate Name of Crop Type
C (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 m b w ��, TKN o and PAN Applied ReceivingResidual
Liquid Solids Acre Fert. Animal (Dry' Hrs. o 2 * ri- + m b0 ° (lbslacre)
N' - Nitrite Application
Q Wet, * ?:_ * �'
Cu.Yds Gallons Waste,etc) c 5
(Dry Tons/Ac) Moist) inches g qg mg/kg mg/kg mg/kg Crop I Crop 2 Crop 1 Crop 2
May 21 36 16.6 2.013 WWTP Cake D 0 S 0.5 0.3 51,900 3,280 65.7 65.595 NA Fescue
May 21 36 29.4 3.565 WTP Cake D 0 S 0.5 0.4 17,300 _ 473 54.8 50.074 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
-
0.000 _ 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
-
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 72 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 115.6681 0.000 Lime Applied
Annual lbs/acre 0.242 0.023 4.914 1.983 0.128 0.002 0.488 0.560 0.081 4.920 117.800 Date lbs/ac _
Prior Years Cumulative lbs/ac 1.194 0.117 23.733 14.554 1.94 0.029 1.902 4.42 1.578 57.091 : July 18 2165
Current Cumulative lbs/ac 1.436 0.140 28.647 16.537 2.068 0.031 2.390 4.980 1.659 62.011
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
!Permit PAN Limit 1st/2nd Crop .. .. .. .. .... . .. .. .. :1 122 [.. 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
�/ 1� *Application Method: S-Surface,IN-Injection,INC-Incorporation
f��^-. /'t '43'111.it-Lo c2 3-a`).2 a **Volatilization Rate: Surface-0.5,Injection/Incorporation-1.0
Signature of Land Applier Date "*'Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 13.95
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Henry Myers Owner: Same Predominant Soil Series: BdB2-Badin
Acres Used: 2.5 Acres Permitted: 2.5 Site#: NC-UN31 Field#: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 2 1 4 1 15( 16 1 J 9 10 11 12
Com-
posite
Date 4/5/21 4/5/21
%Solids 16.6 29.4
Arsenic 12 27.1
Cadmium 1.16 2.58
Copper 383 473
Chromium 74.7 236
Lead 22.7 5.1
Mercury 0.489 0.0479
Molyb- 18.1 58.2
denum
Nickel 77.1 35
Selenium 5 8.5
Zinc 1090 74.5
Total
Phos- 24000 2970
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 11 1 21 U 1 41 5 6 ' 7 191 10 11 12
DT/Ac./
App.
Event 2.01 3.57
Arsenic 0.000 0.000 0.000 0.048 0.193 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.242
Cadmium 0.000 0.000 0.000 0.005 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023
Copper 0.000 0.000 0.000 1.542 3.372 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.914_
Chromium 0.000 0.000 0.000 0.301 1.683 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.983
Lead 0.000 0.000 0.000 0.091 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.128
Mercury 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.000 0.000 0.000 0.073 0.415 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.488
denum
Nickel 0.000 0.000 0.000 0.310 0.250 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.560
Selenium 0.000 0.000 0.000 0.020 0.061 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.081
Zinc 0.000 0.000 0.000 4.388 0.531 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.920
Total
Phos- 0.000 0.000 0.000 96.624 21.176 0.000 0.000 0.000 0.000 0.000 0.000 0.000 117.80
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
�-�,. �1/1�►�w� a -3- a as
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 4 Acres Utilized: 4.7
Land Owner: Henry Myers Annual Dry Tons Applied: 18.9792 Site#: NC-UN31 Acres Permitted: 4.7
Operator: Same Predominant Soil Series: BdB2-Badin Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(Past.) Crop 1 Max.PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max.PAN: 50
Volume applied Volume Residual Sources Soil Precip. > o 4 Z > Nitrate Name of Crop Type
y (enter one)Solids/ % Applied per Cond. K I ,y 7c 5 4 PAN Applied
c (NPDES#,WQ#, Past 24 _ 1? _ .. .3 TKN o g and Receiving Residual
Qo Fert.,Animal (Dry' Hrs. o ° * N' * c°°c R {]bs/acre)
Liquid Solids Acre Wet a.* Q * ?: * ; w. Nitrite Application
Cu.Yds Gallons (Dry Tons/Ac) Waste,etc) Moist) inches = 3 mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
May 21 72 16.6 2.142 WWTP cake D 0 S 0.5 0.3 51,900 3,280 65.7 69.782 NA Fescue _
May 21 36 29.4 1.897 WTP Cake D 0 S 0.5 0.4 17,300 473 54.8 26.635 NA Fescue
0.000 0.000 _ 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
1 0.000 0.000 0.000
0.000 - 0.000 0.000
0.000 _ 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 -
0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): I _
TOTALS: 108I 0 :':: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 96.416 10.000 Lime Applied
Annual lbs/acre 0.154 0.015 3.435 1.215 0.117 0.002 0.298 0.463 0.054 4.952 114.084 : Date lbs/ac
Prior Years Cumulative lbs/ac 1.286 0.127 25.146 15.948 2.075 0.034 2.125 4.575 0.449 60.216 ' 2-17 1904
Current Cumulative lbs/ac 1.440 0.142 28.581 17.163 2.192 0.036 2.423 5.038 0.503 65.168
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit lstl2nd Crop ::: : <H... . .. ... .. .... .. .... . . 122 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
-Ks_.4.-N. MQ-4 a - 3- a as **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 18.98
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Henry Myers Owner: Same Predominant Soil Series: BdB2-Badin
Acres Used: 4.7 Acres Permitted: 4.7 Site#: NC-UN31 Field#: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 2 5 6 L 8 1 10 11 I 12
Com-
posite
Date 4/5/21 4/5/21
% Solids 16.6 29.4
Arsenic 12 27.1
Cadmium 1.16 2.58
Copper 383 473
Chromium 74.7 236
Lead 22.7 5.1
Mercury 0.489 0.0479
Molyb 18.1 58.2
denum
Nickel 77.1 35
Selenium 5 8.5
_ Zinc 1090 74.5
Total
Phos- 24000 2970
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 2 13 4 5 6 8 10 11 12 y
DT/Ac./
App. 7
Event 2.14 1.90
Arsenic 0.000 0.000 0.000 0.051 0.103 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.154
Cadmium 0.000 0.000 0.000 0.005 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015
Copper 0.000 0.000 0.000 1.641 1.795 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.435
Chromium 0.000 0.000 0.000 0.320 0.895 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.215
Lead 0.000 0.000 0.000 0.097 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.117
Mercury 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0 000 0.000 0.000 0.078 0.221 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.298
denum
Nickel 0.000 0.000 0.000 0.330 0.133 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.463
Selenium 0.000 0.000 0.000 0.021 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.054
Zinc 0.000 0.000 0.000 4.670 0.283 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4.952
Total
Phos- 0.000 0.000 0.000 102.816 11.268 0.000 0.000 0.000 0.000 0.000 0.000 0.000 114.08
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 5 Acres Utilized: 17.6
Land Owner: Henry Myers Annual Dry Tons Applied: 92.7351 Site#: NC-UN31 Acres Permitted: 17.6
Operator: Same Predominant Soil Series: TbB2-Tatum Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Wheat Crop 1 Max.PAN: 101 Crop 2 Name: Crop 2 Max.PAN: 50
Volume applied Volume Soil
PP Residual Sources Precip. o 4 z a Nitrate Name of Crop Type
y (enterone) % Applied per (NPDES#,WQ#, Cond. Past 24 ? t= m g 0 PAN Applied
Solids/ w TKN o and Receiving Residual
& o Fert.,Animal (Dry' Hrs. o 5 N' * N• o P Nitrite (lbs/acre) Application
c� Liquid Solids Acre
Wet, a o• : V, * w m' PP
Cu.Yds Gallons (Dry Tons/Ac) Waste,etc) Moist) inches ° ° mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Sept 21 208 23 2.289 WWTP Cake D 0 S 0.5 0.3 35,000 3,470 386 53.017 NA Wheat
Sept 21 194 32.1 2.980 WTP Cake D 0 S 0.5 0.4 14,700 1,650 1150 42.880 NA Wheat
0.000 0.000 0.000
0.000 0.000 0.000
0.000 _ 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
-
0.000 0.000 0.000
0.000 ; 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): I
TOTALS: 402 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 95.898 1 0.000 Lime Applied
Annual lbs/acre 0.127 0.037 4.579 1.727 0.118 0.002 0.393 0.438 0.056 4.184 101.825 ::.:::::.::::::::::::::..:.:.:. Date lbs/ac
Prior Years Cumulative lbs/ac 1.532 0.179 25.599 24.629 2.456 0.048 2.803 3.256 0.563 61.604
Current Cumulative lbs/ac 1.659 0.216 30.178 26.356 2.574 0.050 3.196 3.694 0.619 65.788
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit lst/2nd Crop ::..: ,... . . .. .. . ..... .. 101:> . .-
: .., 50•...
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
`a-� m e/V1.14'Q o2- 3- Ro 8,2, **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 92.73
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Henry Myers Owner: Same Predominant Soil Series: TbT2-Tatum
Acres Used: 17.6 Acres Permitted: 17.6 Site#: NC-UN31 Field#: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or ? 3 J 4 ,L I 6 21 I I 9 J 0 1±I 12
Com-
posite
Date 7/6/21 7/6/21
%Solids 23 32.1
Arsenic 9.48 14
Cadmium 2.91 4.02
Copper 400 461
Chromium 87 223
Lead 16.1 7.38 _
Mercury 0.37 0.0482
Molyb-
denum 20.2 50.5
Nickel 60 27.4
Selenium 2.17 7.79
Zinc 835 60.7
Total
Phos- 19300 2260
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total jj L _I 15 8i 9J 11131 11 11?
1-3
DT/Ac./ 0
App.
Event 2.29 2.98
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.043 0.083 0.000 0.000 0.000 0.000 0.127
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.013 0.024 0.000 0.000 0.000 0.000 0.037
Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.831 2.748 0.000 0.000 0.000 0.000 4.579
Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.398 1.329 0.000 0.000 0.000 0.000 1.727
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.074 0.044 0.000 0.000 0.000 0.000 0.118
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.000 0.000 0.000 0.000 0.000 0.000 0.092 0.301 0.000 0.000 0.000 0.000 0.393
denum
Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.275 0.163 0.000 0.000 0.000 0.000 0.438
Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.010 0.046 0.000 0.000 0.000 0.000 0.056
Zinc 0.000 0.000 0.000 0.000 0.000 0.000 3.823 0.362 0.000 0.000 0.000 0.000 4.184
Total
Phos- 0.000 0.000 0.000 0.000 0.000 0.000 88.355 13.470 0.000 0.000 0.000 0.000 101.83
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
v,.. ivts/wv- a-3-- 0.2a
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 6 Acres Utilized: 7.8
Land Owner: Henry Myers Annual Dry Tons Applied: 44.5223 Site#: NC-UN31 Acres Permitted: 7.8
Operator: Same Predominant Soil Series: ChA-Chewacla Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Wheat Crop 1 Max.PAN: 101 Crop 2 Name: Crop 2 Max.PAN: 50
Volume applied Volume Soil
PP Residual Sources Precip. D o z Nitrate Name of Crop Type
° Y (enter one)Solids/ % Appliedper Cond. A ? z PAN Applied
PF (NPDES#,WQ#, Past 24 w , E 2 d TKN o and Receiving Residual
Liquid Solids Acre Fert. Animal (Dry' Hrs. -c t •* N 0« iT a n (Ibs/acre)
a o * • * R �. Nitrite Application
Q Cu.Yds Gallons (DryTons/Ac) Waste,etc) Wet' inches E o
Moist) ❑ zg mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Sept 21 54 23 1.341 WWTP Cake D 0 S 0.5 0.3 35,000 3,470 386 31.058 NA Wheat
Sept 21 126 32.1 4.367 WTP Cake D 0 S 0.5 0.4 14,700 1,650 1150 62.841 NA Wheat
0.000 0.000 0.000
0.000 _ 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000 _
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
-
0.000 0.000 0.000
0.000 0.000 0.000
II Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 180 0 As Cd Cu Cr Pb , Hg Mo Ni Se Zn P 93.899 10.000 Lime Applied
Annual lbs/acre 0.148 _ 0.043 5.099 2.181 0.108 0.001 0.495 0.400 0.074 2.770 71.501 Date lbs/ac
Prior Years Cumulative lbs/ac 1.238 0.148 19.734 18.581 2.151 0.038 2.148 3.661 0.443 59.09
Current Cumulative lbs/ac 1.386 0.191 24.833 20.762 2.259 0.039 2.643 4.061 0.517 61.860 .:
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit lst/2nd Crop .. ... ........ ..E.. .. .. .. .. 101. 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
Kate- 1: 2,- 02 - 3'20 22- **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 44.52
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Henry Myers Owner: Same Predominant Soil Series: ChA-Chewacla
Acres Used: 7.8 Acres Permitted: 7.8 Site#: NC-UN31 Field#: 6
Residual Analysis''(Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 3 _ J ? 9 10 1111 12
Com-
posite
Date 7/6/21 7/6/21
% Solids 23 32.1
Arsenic 9.48 14
Cadmium 2.91 4.02
Copper 400 461
Chromium 87 223
Lead 16.1 7.38
Mercury 0.37 0.0482
Molyb-
denum 20.2 50.5
Nickel 60 27.4
Selenium 2.17 7.79
Zinc 835 60.7
Total
Phos- 19300 2260
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 2 131 4 I s i i Al I 91 10 1111 12
DT/Ac./ c
App. 7
Event 1.34 4.37
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.025 0.122 0.000 0.000 0.000 0.000 0.148
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.008 0.035 0.000 0.000 0.000 0.000 0.043
Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.073 4.026 0.000 0.000 0.000 0.000 5.099
Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.233 1.948 0.000 0.000 0.000 0.000 2.181
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.043 0.064 0.000 0.000 0.000 0.000 0.108
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.001
Molyb 0.000 0.000 0.000 0.000 0.000 0.000 0.054 0.441 0.000 0.000 0.000 0.000 0.495
denum
Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.161 0.239 0.000 0.000 0.000 0.000 0.400
Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.006 0.068 0.000 0.000 0.000 0.000 0.074
Zinc 0.000 0.000 0.000 0.000 0.000 0.000 2.239 0.530 0.000 0.000 0.000 0.000 2.770
Total
Phos- 0.000 0.000 0.000 0.000 0.000 0.000 51.763 19.739 0.000 0.000 0.000 0.000 71.501
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
�-�-- yl/t �
Signature of Land Applier Date
DENR FORM MFLSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 1 Acres Utilized: 23.5
Land Owner: Danny Baker Annual Dry Tons Applied: 91.3034 Site#: NC-UN32 Acres Permitted: 23.5
Operator: Same Predominant Soil Series: GoB-Golston Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(past.) Crop 1 Max.PAN: 116 Crop 2 Name: Fescue Crop 2 Max.PAN:
Volume applied Volume Soil
,� PP Residual Sources Precip. a o Z > Nitrate Name of Crop Type
y (enter one)Solids/ % Appliedper Cond. K I pe m x1 n 4 PAN Applied
y p PP (NPDES#,WQ#, Past 24 _ p, w TKN o and Receiving Residual
Q Liquid Fert. Animal {DrY' Firs. o w * Z ; m P. {]bs/acre)
a Solids Acre Wet _ * * = �. Nitrite Application
Waste,etc) * © o'
Cu.Yds Gallons (Dry Tons/Ac) Moist) R inches - mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Aug 21 54 23 0.445 WWTP Cake D 0 S 0.5 0.3 35,000 3,470 386 10.308 NA Fescue
Aug 21 36 32.1 0.414 WTP Cake D 0 S 0.5 0.4 14,700 1,650 1150 5.959 NA Fescue
Sept 21 342 23 2.819 WWTP Cake D 0 S 0.5 0.3 35,000 3,470 386 65.287 NA Fescue
Sept 21 18 32.1 0.207 WTP Cake D 0 S 0.5 0.4 14700 1650 1150 2.980 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 ' 0.000 0.000
0.000 0.000 0.000
J J
0.000 0.000 0.000
-
0.000 0.000 0.000
0.000 -0.000 0.000
0.000 0.000 0.000 _
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 4501 0 As Cd Cu Cr Pb Hg Mo . Ni Se Zn P 84.534 [ 0.000 Lime Applied
Annual lbs/acre 0.079 0.024 3.184 0.845 0.114 0.002 0.195 0.426 0.024 5.526 128.797 Date lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac 0.079 0.024 3.184 0.845 0.114 0.002 0.195 0.426 0.024 5.526 ::
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit l stl2nd Crop : .` :. > .... 116
... _
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
ki r-sala-3-a o a Z **Volatilization Rate: Surface-0.5,Injection/Incorporation-1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 91.30
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Danny Baker Owner: Same Predominant Soil Series: GsB-Golston
Acres Used: 23.5 Acres Permitted: 23.5 Site#: NC-UN32 Field#: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, °Ao Solids use Raw Percent#):
Sample or 1 12 4 5 sJ 7 s J 10 11 112
Com-
posite
Date 7/6/21 7/6/21
% Solids 23 32.1
Arsenic 9.48 14
Cadmium 2.91 4.02
Copper 400 461
Chromium 87 223
Lead 16.1 7.38
Mercury 0.37 0.0482
Molyb 20.2 50.5
denum
Nickel 60 27.4
Selenium 2.17 7.79
Zinc 835 60.7
Total
Phos- 19300 2260
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total ? 4 J 16 7 8 9 10 1±I 12 y
DT/Ac./ c
App.
Event 3.26 0.62
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.062 0.017 0.000 0.000 0.000 0.000 0.079
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.019 0.005 0.000 0.000 0.000 0.000 0.024
Copper 0.000 0.000 0.000 0.000 0.000 0.000 2.611 0.573 0.000 0.000 0.000 0.000 3.184
Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.568 0.277 0.000 0.000 0.000 0.000 0.845
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.105 0.009 0.000 0.000 0.000 0.000 0.114
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.002
Molyb 0.000 0.000 0.000 0.000 0.000 0.000 0.132 0.063 0.000 0.000 0.000 0.000 0.195
denum
Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.392 0.034 0.000 0.000 0.000 0.000 0.426
Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.014 0.010 0.000 0.000 0.000 0.000 0.024
Zinc 0.000 0.000 0.000 0.000 0.000 0.000 5.451 0.075 0.000 0.000 0.000 0.000 5.526
Total
Phos- 0.000 0.000 0.000 0.000 0.000 0.000 125.990 2.807 0.000 0.000 0.000 0.000 128.797
phorus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
. rvl a -3-02 a.1;
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 2 Acres Utilized: 15.5
Land Owner: Danny Baker Annual Dry Tons Applied: 75.1134 Site#: NC-UN32 Acres Permitted: 15.5
Operator: Same Predominant Soil Series: BdB2-Badin Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(past.) Crop 1 Max.PAN: 122 Crop 2 Name: Fescue Crop 2 Max.PAN: 50
Volume applied Volume Soil
PP Residual Sources Precip. > o R Z. a Nitrate Name of CropType
o -.a. (enterone) % AppliedperCond. A .a.'. z q PAN Applied
Solids/ WQ#, mw TKN o @ and Receiving Residual
� PP (NPDES# Past 24 ;� � .,
Liquid Solids Acre Fert.,Animal {D�' Hrs. o d * N * Cr' (Ibs/acre)
Wet, n * * Nitrite Application
Waste,etc) * ° * "
Cu.Yds Gallons (Dry Tons/Ac) Moist) . inches g mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Nov 21 162 28.3 2.491 WWTP Cake D 0 S 0.5 0.3 50,000 2,400 1430 84.245 NA Fescue
^
Nov 21 - 126 34.4 2.355 WTP Cake D 0 S 0.5 0.4 14,400 834 81.4 27.906 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 _ 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
-0.000 0.000 0.000 _
0.000 0.000 0.000
0.000 0.000 0.000
. . Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 288 0 ::: ::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 112.151 10.000 Lime Applied
Annual lbs/acre 0.246 0.022 3.801 1.263 0.151 0.003 0.315 0.469 0.102 5.720 127.100 ::::::::: :::: :.:::.:::::::: Date lbs/ac
Prior Years Cumulative lbs/ac 0.199 0.024 4.927 2.456 0.261 0.003 0.347 1.104 0.119 8.795
Current Cumulative lbs/ac 0.445 0.046 8.728 3.719 0.412 0.006 0.662 1.573 0.221 14.515 • :: ::::::::::::: ::: ::.
Permitted C. P.L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit lst/2nd Crop
122 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
Ken... /'/7e' .L. a-3-a 0 as **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 75.11
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Danny Baker Owner: Same Predominant Soil Series: BdB2-Badin
Acres Used: 15.5 Acres Permitted: 15.5 Site#: NC-UN32 Field#: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 I 2 J 4 5 j 4 J 10 11 12
Com-
posite
Date 10/4/21 10/21/21 10/4/21
% Solids 20.8 28.3 34.4
Arsenic 10.3 41.3
Cadmium 1.31 3.23
Copper 345 442
Chromium 69.2 195
Lead 22 8.72
Mercury 0.477 0.0415
Moiyb 16.8 49.1
denum
Nickel 63.9 32
Selenium 6.73 14.5
Zinc 1030 125
Total
Phos- 22600 3080
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 11 I 12 3J 4 5 6 7 J 8 9 10 11j 12
DT/Ac./
App.
Event 2.49 2.36
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 0.000 0.195 0.246
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.000 0.015 0.022
Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.719 0.000 2.082 3.801
Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.345 0.000 0.918 1.263
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.110 0.000 0.041 0.151
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.003
MO'yb 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.084 0.000 0.231 0.315
_ denum
Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.318 0.000 0.151 0.469
Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 0.000 0.068 0.102
Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.131 0.000 0.589 5.720
Total
Phos- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 112.593 0.000 14.507 127.100
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
"Kt..._ Ii4 Yam a 3-a o a a
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 3 Acres Utilized: 10
Land Owner: Danny Baker Annual Dry Tons Applied: 38.3526 Site#: NC-UN32 Acres Permitted: 10
Operator: Same Predominant Soil Series: GoB-Golston Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(past.) Crop 1 Max.PAN: 116 Crop 2 Name: Fescue Crop 2 Max.PAN: 50
Volume applied Volume Soil
,� pP Residual Sources Precip. > o Z a Nitrate Name of CropType
o . (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 g. w °: w TKN o § and PAN Applied Receiving Residual
Liquid Solids Acre Fert.,Animal (Dry' Hrs. o " N' * - = (Ibslacre)
* K.
* R Nitrite Application
Cu.Yds Gallons (DryTons/Ac) Waste,etc) Wet' inches a 'o' * 5
Moist) a mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Sept 21 198 23 3.835 WWTP Cake D 0 S 0.5 0.3 35,000 3,470 386 88.825 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000 _
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 _ 0.000 0.000
0.000 0.000 0.000
. . • Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 198' 01.:,::::,:: As Cd Cu , Cr Pb Hg Mo Ni Se Zn P 88.825 10.000 Lime Applied
Annual lbs/acre 0.073 0.022 3.068 0.667 0.123 0.003 0.155 0.460 0.017 6.404 148.031 : ::::::.:..:::..::..: Date lbs/ac
Prior Years Cumulative lbs/ac 0.297 0.033 7.797 3.876 0.434 0.004 0.532 1.854 0.163 15.4
Current Cumulative lbs/ac 0.370 0.055 10.865 4.543 0.557 0.007 0.687 2.314 0.180 21.804
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit 1 stl2nd Crop ..
116 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
Y4 844.0.4:7 oZ- 3 c 2 O a a- **Volatilization Rate: Surface-0.5,Injection/Incorporation- 1.0
Signature of Land Applier Date ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 38.35
Permit#: WQ0001346 Cation Exchange Capacity (non 503 only): N/A
Operator: Danny Baker Owner: Same Predominant Soil Series: GsB-Goldston
Acres Used: 10 Acres Permitted: 10 Site#: NC-UN32 Field#: 3
Residual Analysis'' (Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or� 3 ' ? 10 11 12
Com-
posite
Date 7/6/21
% Solids 23
Arsenic 9.48
Cadmium 2.91
Copper 400
Chromium 87
Lead 16.1
Mercury 0.37
Molyb-
denum 20.2
Nickel 60
Selenium 2.17
_ Zinc 835
Total
Phos- 19300
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 2 3 4� 5 171 8J 19 10_1 11 12
DT/Ac./
App.
Event 3.84
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.073 0.000 0.000 0.000 0.000 0.000 0.073
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.022 0.000 0.000 0.000 0.000 0.000 0.022
Copper 0.000 0.000 0.000 0.000 0.000 0.000 3.068 0.000 0.000 0.000 0.000 0.000 3.068
Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.667 0.000 0.000 0.000 0.000 0.000 0.667
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.123 0.000 0.000 0.000 0.000 0.000 0.123
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.003 0.000 0.000 0.000 0.000 0.000 0.003
Molyb 0.000 0.000 0.000 0.000 0.000 0.000 0.155 0.000 0.000 0.000 0.000 0.000 0.155
denum
Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.460 0.000 0.000 0.000 0.000 0.000 0.460
Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.017 0.000 0.000 0.000 0.000 0.000 0.017
Zinc 0.000 0.000 0.000 0.000 0.000 0.000 6.404 0.000 0.000 0.000 0.000 0.000 6.404
Total
Phos- 0.000 0.000 0.000 0.000 0.000 0.000 148.031 0.000 0.000 0.000 0.000 0.000 148.031
phorus
"I certify, under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
/14 02- 3^020.2,2_
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 4 Acres Utilized: 3.2
Land Owner: Danny Baker Annual Dry Tons Applied: 8.5801 Site#: NC-UN32 Acres Permitted: 3.2
Operator: Same Predominant Soil Series: GoB-Golston Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(past.) Crop 1 Max.PAN: 116 Crop 2 Name: Fescue Crop 2 Max.PAN: 50
Volume applied Volume Soil
s. Pp Residual Sources Precip. a o z Nitrate Name of Crop Type
G (enter one)Solids/ oho Applied per (NPDES#,WQ#, Cond. Past 24 l m w w 2 TKN o § and PAN Applied ReceivingResidual
cd O Liquid Fert.,Animal (Dry' Hrs. o R * N' * c°R, (lbslacre)
Q g Solids Acre Wet * °: * a •w. Nitrite Application
Waste,etc) * a o'
Cu.Yds Gallons (Dry Tons/Ac) Moist) inches ❑ - mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Nov 21 36 28.3 2.681 WWTP Cake D 0 _ S 0.5 0.3 50,000 2,400 1430 90.681 90.681
0.000 - 0.000 0.000
-
0.000 0.000 0.000
0.000 _ 0.000 0.000 _
0.000 _ 0.000 0.000
0.000 0.000 0.000
_ 0.000 0.000 0.000
0.000 _ 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
- 0.000 0.000 0.000
0.000 0.000 0.000
I
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 36 0::::::.::'• As Cd Cu Cr Pb Hg , Mo Ni Se Zn P 90.681 90.681 Lime Applied
Annual lbs/acre 0.055 0.007 1.850 0.371 0.118 0.003 0.090 0.343 0.036 5.523 121.181 Date r lbs/ac
Prior Years Cumulative lbs/ac 0.202 0.02! 5.54 2.749 0.318 0.003 0.37 1.371 0.103 11.68
Current Cumulative lbs/ac 0.257 0,028 7.390 3.120 0.436 0.006 0.460 1.714 0.139 17.203
Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit l st/2nd Crop 116 i :>50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
�'1i- a/ -�- - 3 -.2 3 c2a. **Volatilization Rate: Surface-0.5,Injection/Incorporation-1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 8.58
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Danny Baker Owner: Same Predominant Soil Series: GsB -Goldston
Acres Used: 3.2 Acres Permitted: 3.2 Site#: NC-UN32 Field#: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or? 2 _314J 5 7J 8 sJ 10 11 12
Com-
posite
Date 10/4/21 10/21/21
% Solids 20.8 28.3
Arsenic 10.3
Cadmium _ 1.31
Copper 345
Chromium 69.2
Lead 22
Mercury 0.477
Molyb-
denum 16.$
Nickel 63.9
Selenium 6.73
Zinc 1030
Total
Phos- 22600
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 2 4 5 6 171 8 99 10 11 12
DT/Ac./
App.
Event 2.68
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.055 0.000 0.000 0.055
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.000 0.000 0.007
Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.850 0.000 0.000 1.850
Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.371 0.000 0.000 0.371
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.118 0.000 0.000 0.118
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 0.000 0.000 0.003
Molyb 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.090 0.000 0.000 0.090
denum
Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.343 0.000 0.000 - 0.343
Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.036 0.000 0.000 0.036
Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.523 0.000 0.000 5.523
Total
Phos- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 121.181 0.000 0.000 121.181
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF(12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Monroe WQ Permit#: WQ0001346 Field#: 5 Acres Utilized: 19.3
Land Owner: Danny Baker Annual Dry Tons Applied: 83.0231 Site#: NC-UN32 Acres Permitted: 19.3
Operator: Same Predominant Soil Series: CmB-Cid Cation Exchange Capacity(non 503): N/A
Crop 1 Name: Fescue(past.) Crop 1 Max.PAN: 141 Crop 2 Name: Fescue Crop 2 Max.PAN: 50
Soil
Volume applied Volume Residual Sources Precip. a o 5. Z. > Nitrate Name of Crop Type
°0 (NPDES#,WQ#, Cond. Past 24 coo b 2 27'z w �, ' PAN Applied
(enter one)Solids/ % Applied perD 2, = � TKN � o and Receiving Residual
Q Liquid ( rY, a n• - (lbs/acre)
9 Solids Acre Fert.,Anima] Hrs. o m * N' « - o
Waste,etc)
Wet, a • « : Z. w Nitrite Application
Cu.Yds Gallons (Dry Tons/Ac) Moist) inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
Nov 21 290 28.3 3.581 WWTP Cake D 0 S 0.5 0.3 50,000 2,400 1430 121.116 NA Fescue
Nov 21 48 34.4 0.721 WTP Cake D 0 S 0.5 0.4 14,400 834 81.4 8.538 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
- _ 0.000 I 0.000 0.000
0.000 _ 0.000 0.000 _
0.000 0.000 0.000
0.000 0.000 0.000
`
0.000 0.000 0.000
0.000 0.000 0.000
•
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form):
TOTALS: 338 0 _ As Cd Cu Cr Pb Hg Mo Ni Se Zn P 129.654 1 0.000 Lime Applied_
Annual lbs/acre 0.133 0.014 3.108 0.777 0.170 0.003 0.191 0.504 0.069 7.557 166.303 :: Date lbs/ac
Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0
Current Cumulative lbslac 0.133 0.014 3.108 0.777 0.170 0.003 0.191 0.504 0.069 7.557
Permitted C.P.L. R.**** 36 34 1338 X 267 15 X 374 89 2498
Permit PAN Limit 1st/2nd Crop :. .: ... - 141 50
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information,including the possibility of fines and imprisonment for knowing violations."
N� *Application Method: S-Surface,IN-Injection,INC-Incorporation
il��� /1 L or1/Wo oC•} '3'02.0 da **Volatilization Rate: Surface-0.5,Injection/Incorporation-1.0
Signature of Land Applier Date ***Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF(12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Monroe Total Dry Tons Applied(Annual): 83.03
Permit#: WQ0001346 Cation Exchange Capacity(non 503 only): N/A
Operator: Danny Baker Owner: Same Predominant Soil Series: Cmb- Cid
Acres Used: 19.3 Acres Permitted: 19.3 Site#: NC-UN32 Field#: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or t 2 3 J J _71J 10 11 12
Com-
posite
Date 10/4121 10/21/21 10/4/21
% Solids 20.8 28.3 34.4
Arsenic 10.3 41.3
Cadmium 1.31 3.23
Copper 345 442
Chromium 69.2 195
Lead 22 8.72
Mercury 0.477 0.0415
Molyb 16.8 49.1
denum
Nickel 63.9 32
Selenium 6.73 14.5
Zinc 1030 125
Total
Phos- 22600 3080
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total l J 1 3I 4 J 6 1_7_1 9 10 11 12
DT/Ac./
App.
Event 3.58 0.72
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.074 0.000 0.060 0.133
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 0.000 0.005 0.014
Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.471 0.000 0.637 3.108
Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.496 0.000 0.281 0.777
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.158 0.000 0.013 0.170
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 0.000 0.000 0.003
Molyb 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.120 0.000 0.071 0.191
_ denum
Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.458 0.000 0.046 0.504
Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.048 0.000 0.021 0.069
Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.377 0.000 0.180 7.557
Total
Phos- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 161.861 0.000 4.441 166.303
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF(12/2006)

TAB 5
PATHOGEN REDUCTION & VECTOR
ATTRACTION REDUCTION

Volatile Solids Reduction 2021
1st Quarter
RAS digested sludge
Van Kleek equation IN - OUT
In (RAS)-Out(digested sludge)= 1/5/2021 0.7280 0.5900 0.138 Reduction
In (RAS) -(In *Out) (digested sludge) = IN- (IN*OUT) 46.23%
0.728 0.42952 0.29848
2nd Quarter
IN - OUT
4/5/2021 0.7300 0.5810 0.149 Reduction
IN- (IN*OUT) 48.71%
0.73 0.42413 0.30587
3rd Quarter
IN - OUT
7/6/2021 0.6980 0.5260 0.172 Reduction
IN- (IN*OUT) 51.99%
0.698 0.367148 0.330852
4th Quarter
IN - OUT
10/21/2021 0.7380 0.4780 0.26 Reduction
IN- (IN*OUT) 67.49%
0.738 0.352764 0.385236

R
PROMPT.ACCURATE-RELIABLE
LABORATORIES, INC
WWW.PARLABS.COM
REPORT OF ANALYSES
Attn: KEN MORRIS
CITY OP MONROE WASTEWATERPLANT PROJECT NAME: JAN 21
PO BOX 69 DATE: 02/05/21
MONROE, NC 28111-
SAMPLE NUMBER- 140817 SAMPLE ID- MONROE WWIP SAMPLE MATRIX- WW
DATE SAMPLED- 01/05/21 TIME SAMPLED- 1040
DATE RECEIVED- 01/05/21 SAMPLER- KM RECEIVED BY- DJ
TIME RECEIVED- 1310 DELIVERED BY- KM TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 01 /05/21 1700 RE 40,018 MPN/g
LABORATORY DIRECTOR -
2217 Graham Park Drive•Charlotte,NC 28273
Phone: [phone]•Fax: [phone]

2217 Graham Park Drive
PL1 R PO Box 411483
Charlotte, NC 28241-1483
PROMPT•ACCLURATE•REL4A13LC
LABORATORIES, II'.TC NC Cert#20;SC Cel#99003001
CLIENT NAME: CITY OF MONROE
SAMPLE ID: MONROE WWTP
SAMPLE DATE: 01/15/21
ANALYSIS: FECAL COLIFORM, GEOMETRIC MEAN
ANALYSIS METHOD: SM 9221 E
LAB ID#: Sample# F. Coliform T. Solids % FCI gram
140817 1 7,818 19.45% 40,192.76
2 8,149 19.98% 40,785.32
3 8,439 20.30% 41 572.84
4 8,240 20.41% 40,371.58
5 7,716 20.88% 36 952.76
6 8,201 21.16% 38,756.30
7 8,159 19.56% 41,712.72
Fecal Coliform
Geometric Mean= 40,018
........................

(PAR •
I CHAIN OF CUSTODY
I.A5OniTOREsdevS, PAR Laboratories, Inc
11101111111111/ Phone [phone]-S333
Fax [phone] •
www.partabs.com
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
PP b lesuerte that W In!Duration be recorded on thy Chan of Custody document fur acceptmco by PAR t,aberatogist Inc.erb Os Pionn
meet of Vie)and Nature)Reiev*css.
omaeihr Name tbprmQl Common&! Spfcinl histruCtigrea
City of Monroe
k,..Addresa ,r-
PO Box tsg 503 BJOSOL)DS
IWINtet Mods REPORTING
Monroe,NC 28113
.
►i oTi►or rtt st 4 Taw c.. ---' . _
7 /�1.
�„ N10 .,. fr a`S479 Kv;t•arr:il,wa+,vor c.,+ri
$amp)%Taken By; !<evl polo tr,. ••z
14 THIS FOR STATE or EPA REeitaTING7 YES„, NO
ik$mpk‘yixi:DW ,_WW GWMW HW Soil ether .
Si11Fmplt Tamp at time of sampling: 1.7 °C Sample Temp upon receipt: 71
♦e Preserved: Yes— No X Teflon Liner/Zero Headspace: Yes No_ N/A
Clint Sample LD, Comp Grab Preserv. Set Up Collection Analyme kttquMted
(Semple Location/NumberL Date/Time Date I Time „ —
i+1 ► NONE " j �_�! 1,:� FECAL COLIFORRM
w X NONE r IZ r to: 0
,-
FECAL COLIFORM
3 x NONE 1,6_,2110:41FECAL COLIFORM
TrvViThi - X NONE . 1_5-4( r D..Y1 FECAL COLIFORM
VI►W't°P X NONE j,,5,z r la :yaFECAL COLIFORM
X NONE t.6-• r d :sf.2 FECAL COLIFORM
X NONE i .‘•A l r.5:4/3 FECAL COLIFORM
i.
Reiinquiebed by; Deverrirne Rocaived qy:; Daum/Moe
1 ,ter J} . ai.ps - // t310
ialinquiMhad by; DaterTirne Received by: - DategTimo
1
' IPCompoeite G-Grab D)WeDr`mking Water WWAcWasteweter GWMW=Groundwater Monitoring Wen Hi,VmHazardous Wane
'' see Outer SW*
Y

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Monroe WQ Permit Number: WQ0001346
WWTP Name: WWTP cake NPDES Number: NC0024333
Monitoring Period: From 1/1/2021 To 3/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ ;
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization Cl
Class B: AIt. (1) Fecal Density ❑ Alt. (2)Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed(Class B only) indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion 0
Anaerobic Digestion ❑ <. .
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen DensityNumber of Analytical
Parameter gExcee- Frequency Sample Tech-
in Sludge Minimum Geo. Mean Maximum Units deuces of Analysis Type ninue
2 x 10 to the MPN 36,952.76 40,018 41,712.72 MPN/g 0 quarterly grab sm9221e
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T .1107)- Please indicate alternative performed:
Alt.1 (VS reduction) Cl Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4(Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ AIt. 6 (Alk. Stabilization ❑ Alt 7 (Drying- Stable) ❑ Alt. 8 (Drying-Unstable) ❑
Alt. 9(Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
ft Jl�- . 9/))- KQ,— j14: ,L 02-3-aoaa
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T(12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM(503 Rules)
Facility Name: City of Monroe WQ Permit Number: WQ0001346
WWTP Name: Monroe WWTP cake NPDES Number: NC0024333
Monitoring Period: From 1/1/2021 To 3/31/2021
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑
Alternative 4 ❑ Alternative 5 0 Alternative 6 LI
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alternative 1 0 Alternative 2 ❑
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion 0
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Number of Analytical
Allowable Level Pathogen Density Frequency Sample
Parameter Excee- Tech-
in Sludge Minimum Geo. Mean Maximurr Units dences of Analysis Type moue
2 x 10 to the MPN 36,952.76 40,018 41,712.72 MGN/g 0 quarterly grab sm9221e
6th power
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6(Alk. Stabilization ❑ Alt 7 (Drying-Stable) ❑ Alt. 8 (Drying-Unstable) ❑
Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT(please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
'lgl > yt/i a - 3-.2aaa
Signature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

R
PROMPT•ACCURATE•RELIABLE
LABORATORIES, INC
WWWPARLABS.COM
REPORT OF ANALYSES
Attn: KEN MORRIS
CITY OF MONROE WASTEWATERPLANT PROJECT NAME: APR 21
PO BOX 69 DATE: 04/19/21
MONROE, NC 28111-
SAMPLE NUMBER- 141428 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- WW
DATE SAMPLED- 04/06/21 TIME SAMPLED- 0940
DATE RECEIVED- 04/06/21 SAMPLER- KM RECEIVED BY- DJ
TIME RECEIVED- 1150 DELIVERED BY- KM TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 04/06/21 1550 RE 39,718 MPN/g
LABORATORY DIRECTOR . ' H `�"`: ��" 4—
/
2217 Graham Park Drive•Charlotte,NC 28273
Phone: [phone] • Fax: [phone]

2217 Graham Park Drive
pixR PO Box 411483
PRDMPT•ACCURATE•REL1A©LE Charlotte, NC 28241-1483
LA.I30R_A"I'ORIES, INC", NC Cert#20,SC Cert#99003001
CLIENT NAME: CITY OF MONROE
SAMPLE ID: MONROE WWTP
SAMPLE DATE: 04/06121
ANALYSIS: FECAL COLIFORM, GEOMETRIC MEAN
ANALYSIS METHOD: SM 9221 E
LAB ID#: Sample # F. Coliform T. Solids % FCI gram
141428 1 7,448 17.92% 41,567.75
2 7,371 18.65% 39,519.57
3 7,552 19.01% 39,725.11
4 7,457 18.46% 40,397.23
5 7,645 18.18% 42,054.22
6 7,157 19.79% 36,164.62
7 7,109 18.28% 38,888.96
Fecal Coliform
Geometric Mean= 39,718

ifFPAR 1 CHAIN OF CUSTODY
PAR Laboratories, Inc
aIMMIIIIIrj Phone [phone]
Fax [phone]
Www.parfabs.com
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It la tonnnal that all inror s ion ba recorded on this Chen or Custody document ror acceptance by PAR Labormial.Inc.m0 MR 1VoiN+
r R arlrasaal et&mrorwnnrtal and Natural riasourcos.
urnplrny Name iogling Comments/ Spaniel lrrstruCtioer>x
City ofMonme
rdr+raaPO B x 69 503 T3IOSOLIDS
y. .a Rip code Monroe,NC 28111 REPOR G
'
0 r+h41�R# else •04.. ".w, ' -- - . .
ti A
�rw'rr�s oy a2$ - `he7q , k„..._.0e-r-
!w �.�.-...ram 5. "�o.r..Kr...2.11a
3ampla T,k,, sy: Ke.in N o�,.
IN THIS FOR STATE or EPA REPQ TING7 YES r .. NO
sikparp14 type: OW__WW H GWMW W Soil other
S41mple Tamp at time of sampling: I$. i °C Sample Temp upon receipt !!_
Aft Preasrvetl; Yes No X Teflon Liner/Zero Headspace: Yes No, NIA
Client Sample I.D. Comp Grab Preserv. Set Up Collection Anvyee�igt►i1
(Simple Location/Number) Date/Time Date/Time -_-
M I WWT P X NONE q_4,_a% 9 :, FECAL COLIFORM
12 WWTP X NONE _G_ � ;, FECAL COLIFORM
3 ww x NONE ,i_4_al 9- J w FECAL COLIFORM .
X NONE .�-�a% , FECAL COLIFORM
X NONE �-4_.2% q.,�I FECAL COLIFORM
X NONE .. '4_a` 9 a FECAL COLIFORM
W NONE ,�, L_a T.411.2
FECAL COLIFORM
a14•5
9Riingtilahtd by: Daternme Raceivs¢Ly: bats/1lme
ieriequishad by: Daieriime Received by: Date/ram
•
...�---
' G°1ComPooite G,RGrab DWGHazardous MeteMeteSa+a � i)rir►king.Watar WW••Wastewatar GWMWmGrourtdwetar Monitoring Well HW-
N.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Monroe WQ Permit Number: W00001346
WWTP Name: WWTP cake NPDES Number: NC0024333
Monitoring Period: From 4/1/2021 To 6/30/2021
Pathogen Reduction(15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A: Alt. A(time/temp) ❑ Alt B(Alk Treatment)❑ Alt. C (Prior Testing)❑
AIt.D (No Prior Test) LI I Process to Further Reduce Pathogengs ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑_ Heat Drying ❑ Heat Treatment ❑ Thermophilic 0
Beta Ray ❑ Gamma Ray❑ Pasteurization ❑
Class B: Alt. (1)Fecal Density p Alt. (2)Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting ❑ 'Aerobic Digestion
Anaerobic Digestion ❑
If applicable to alternative performed(Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen Density Number of Frequency Sample Analytical
Parameter Tech-
in Sludge Excee- of Analysis g Minimum Geo. Mean Maximum Units of y Type niaue
2 x 10 to the MPN 36,164.62 39,718 42,054.22 MPN/g 0 quarterly grab SM9221E
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T .1107)-Please indicate alternative performed:
Alt.1 (VS reduction) +❑ Alt.2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt.4(Spec. 02 uptake) ❑
AIt. 5 (14-Day Aerobic) ❑ Alt.6(Alk. Stabilization ❑ Alt 7 (Drying-Stable) ❑ Alt. 8 (Drying-Unstable) ❑
Alt. 9 (Injection) ❑ Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed LI
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify,under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have been met."
❑ "I certify,under penalty of law,that the pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator
Preparer Name and Title(type or print) Land Applier Name and Title(if applicable)(type or print)
1 )1t"-- )''/ . ,kit.- 1v1 84A4.10 02-3-a0aa
Sig!ature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
DENR FORM PVRF 02T(12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Monroe WQ Permit Number: WQ0001346
WWTP Name: Monroe WWTP cake NPDES Number: NC0024333
Monitoring Period: From 4/1/2021 To 6/30/2021
Pathogen Reduction (40 CFR 503.32)- Please indicate level achieved and alternative performed:
Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑
Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ ff
t.:
Beta Ray LI Gamma Ray ❑ Pasteurization ❑
Class B: Alternative 1 p ' Alternative 2 ❑
.... ..... .... .... ....
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying❑ Composting LI Aerobic Digestion 0
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen DensityNumber of Analytical
Parameter gExcee- Frequency Sample Tech-
in Sludge Minimum Geo. Mean Maximum Units deuces of Analysis Type niaue
2 x 10 to the MPN 36,164.62 39,718 42,054.22 MGN/g 0 quarterly grab sm9221e
6th power
per gram of CFiT
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4(Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying- Stable) Li Alt. 8 (Drying-Unstable) ❑
Alt. 9(Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT(please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyie Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
1 AA' 1?Y ,•h,,a 02 -3-ao.2a
Si Nature of Preparer*g p Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

piti R
PROMPT•ACCURATE•RELIABLE
LABORATORIES, INC
WWW.PARLABS.COM
REPORT OF ANALYSES
Attn: KEN MORRIS
CITY OF MONROE WASTEWATERPLANT PROJECT NAME: JUL 21
PO BOX 69 DATE: 07/22/21
MONROE, NC 28111-
SAMPLE NUMBER- 142058 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- WW
DATE SAMPLED- 07/06/21 TIME SAMPLED- 0945
DATE RECEIVED- 07/06/21 SAMPLER- KM RECEIVED BY- DJ
TIME RECEIVED- 1020 DELIVERED BY- KM TYPE SAMPLE-- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 07/06/21 1650 RE 3,234 MPN/g
LABORATORY DIRECTOR v l.r _ ''' E:::*
2217 Graham Park Drive•Charlotte,NC 28273
Phone: [phone] •Fax: [phone]
1t c1./U -'r1

2217 Graham Park Drive
Pil R PO Box 411483
Charlotte, NC 28241-1483
PROMPT•ACCURATE•RELIABLE
LABORATORIES, INC NC Cert#20,SC Cert#99003001
CLIENT NAME: CITY OF MONROE
SAMPLE ID: MONROE WWTP
SAMPLE DATE: 07/06/21
ANALYSIS: FECAL COLIFORM, GEOMETRIC MEAN
ANALYSIS METHOD: SM 9221 E
LAB 1D #: Sample# F. Coliform T. Solids % FC!gram
142058 EMI 853 25.28% 3,373.12
NEM 844 28.35% 2,977.77
1,009 26.28% 3.840.70
4 880 25.36% 3,468.61
MEM 820 28.00% 2,928.83
6 871 28.75% 3,030.26
MOM 864 27.75% 3,113.59
Fecal Coliform
Geometric Mean- 3,234

!Aar CHAIN OF CUSTODY
L45011nromes,ri PAR Laboratories, Inc
Phone [phone]
Fax [phone]
Www.parfabs.corn
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-14.83
It to eaasnthq that all Information be recorded en this Chain or Custody dOcjmern For acceptance by PAR Laboratories.Inc.and the Werth
careens Department o!E nvirnrxnentaf and Natural Resources.
omAany Name Ibrlfrngi • Comments/ Special instructions
City of Monroe
Address-
PO Box 69 503 BIOSOLIDS
Gay.Snri a al~sip code UPCR 1 3l.`I G
Monroe,NC 28111
• e of ontoot s setephon -
�`^,, ` 6161 km u`Q 1D'C r9
Sample Taken By: 6t.41 /ti.a,rr
IS THIS FOR STATE or EPA REPS TING? YES NO
*Sample type: OW WW-X GWMW _ HW Soil other
Sample Temp at time of sampling: ,4 °C Sample Temp upon receipt:
" Preserved; Yes No X Teflon Liner/Zero Headspace: Yes No NIA,X
Cllcat Sample F.D. Cotnp Grab Preserv. Set Up Collection Anelycs Requested
(Sample Location/NumberL Date/Time Date/Time _
# I W WTP X " NONE 7_4 a :�� FECAL COLIFORM
t+2 wwrP — x NONE 7_ 4 -a I 9:`I
s FECAL COLL ORM
013 ww't? x NONE 7_ : FECAL COLIFORM
____T X NONE ,yM
,4- ' � FECALCOLIFOR' X NONE 7 r -al 9:y4 FECAL COLIFORM
#6 WWTP - X NONE 7-u';1 a:`f 7 FECAL COLWORM
N 7 WW1? x NONE 7,Co a I q .17 FECAL COLIFORM
l "
Nalhqulahad by. Date/Time Received Date/Time
- ol"frcoo -2l 11'.as 67-0(e -6)1/I4
¢linquished by: Daterrime • Received by: Date/Time
C w Composite G.Grab DW=thinking Water WW=Wastewater GWMW=Groundwater Monitoring Weil WYwHazardous Waste
'' See Other Stile

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Monroe WQ Permit Number: WQ0001346
WWTP Name: WWTP cake NPDES Number: NC0024333
Monitoring Period: From 7/1/2021 To 9/30/2021
Pathogen Reduction (15A NCAC 02T .1106)- Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑
Alt.D (No Prior Test) 0 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alt. (1) Fecal Density r❑ Alt. (2)Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying 0 1 Composting ❑ Aerobic Digestion 0
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen DensityNumber of Analytical
g Frequency Sample
Parameter Tech-
in Sludge Excee- of Analysis g Minimum Geo. Mean Maximum Units of y Type niaue
2 x 10 to the MPN 2,928.83 3,234 3,840.70 MPN/g 0 quarterly Grab SM9221E
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) El Alt. 2 (40-day bench) LI Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7(Drying- Stable) ❑ Alt. 8 (Drying-Unstable) ❑
Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T ,1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator
Preparer Name and Title(type or print) Land Applier Name and Title (if applicable)(type or print)
?I41 a)- ,Yl/10 s- ,2-3-a o a a
Sig -ature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T(12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Monroe WQ Permit Number: WQ0001346
WWTP Name: Monroe WWTP cake NPDES Number: NC0024333
Monitoring Period: From 7/1/2021 To 9/30/2021
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A: Alternative 1 LI Alternative 2 Cl Alternative 3 LI
Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ •
If applicable to alternative performed(CIass A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alternative 1 0 Alternative 2 ❑ I
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion r❑
Anaerobic Digestion ❑ I ..
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Number of Analytical
Allowable Level Pathogen Density Frequency Sample
Parameter Excee- Tech-
in Sludge Minimum Geo. Mean Maximum Units deuces of Analysis Type niaue
2 x 10 to the MPN 2,928.83 3,234 3,840.70 MGN/
6th power g 0 quarterly grab sm9221e
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (40 CFR 503.33)- Please indicate option performed:
Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying- Stable) ❑ Alt. 8 (Drying-Unstable) ❑
Alt. 9(Injection) ❑ Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
$44L- ›A/A›.- ryt s a. 3-2 a,2
Signature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

PAIR.
PRQMPT•ACCU FATE•RELIABLE
LABORATORIES, INC
WW W.PARLABS.COM
REPORT OF ANALYSES
Attn: KEN MORRIS
CITY OF MONROE WASTEWATERPLANT PROJECT NAME: OCT 21
PO BOX 69 DATE: 10/18/21
MONROE, NC 28111-
SAMPLE NUMBER- 142715 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- WW
DATE SAMPLED- 10/04/21 TIME SAMPLED- 0940
DATE RECEIVED- 10/04/21 SAMPLER- KM RECEIVED BY- DJ
TIME RECEIVED- 1130 DELIVERED BY- KM TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
FECAL COLIFORM (GEOM. MEAN) SM 9221 E 10/04/21 1545 RE 11 ,726 MPN/g
LABORATORY DIRECTOR
2217 Graham Park Drive•Charlotte,NC 28273
Phone: [phone] •Fax: [phone]

2217 Graham Park Drive
Pa R PO Box 411483
Charlotte, NC 28241-1463
PAOMPT•AC UNAPE•RELIABLE
LABO RATORXES, INTC NC Cert#20;SC Cert#99003001
CLIENT NAME: CITY OF MONROE
SAMPLE ID: MONROE WWTP
SAMPLE DATE: 10/04/21
ANALYSIS: FECAL COLIFORM, GEOMETRIC MEAN
ANALYSIS METHOD: SM 9221 E
LAB ID#: Sample# F. Coliform T. Solids % FCl gram
MEM 1 2,899 24.40% 11,877.65
2 3,034 22.37% 13,562.42
MIN 3,087 23.54% 13,113.04
4 2,957 21.78% 13,575.18
1,396 22.19% 6,293.94
6 3,195 22.72% 14,059.87
2,700 22.47% 12,014.80
Fecal Coliform
Geometric Mean= 11,726

IPAR_j CHAIN OF CUSTODY
PAR Laboratories, Inc
81111111111 Phone [phone]
Fax [phone]
ww'w.parfabs.corn
Shipping: Mailing:
2217 Graham Park Drive •
PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
li 4 manes Chet all Intormatton be recorded on thtt Crud!,or Custody document tor ecceot.nce by MR Lebbried s•Inc.IInd INN"
i li?Rprrl►unnt at r rirwxm tital a1 Rrrro 6 Natural waaa.
umarny Nirn.tagltrtyl Comrrsat[s1 IrIt UUCti011ffi
City of Monroe
Addr+ai- -_ .r-
•
PO Bcx 69 503 BIOSOLIDS
% ri . ,tM r.
{ Monroe,NC 281 REPORTING
'14artrftMtMst 4'F.lepbem,•c -..., - -
. ... `5 . (41i`C 3C 1G. 0 ►T.,�to •rP. "1
Sat9Rple Taken Se: Kr" /v16,rf...,
14 THIS FOR STATE or EPA REPO TING? YES,,,,, ,,, NO
"'S,,ylmple typo: OW_ WW GWMW I-lW Soil_ other
Sample amp at time of pling:4,7°C Sample Temp upon receipt: 12•
se Pe�rserved: Yes No Teflon Liner/Zero Headapace: Yes No NIA•X
OHIO SIapia l.D. Corip ' Grab Preserv. Set Up Collection Attalyea Requested
( le Looeuon/NumberL Date/Time Date/Time
# X NONE FECAL COLLFORM
��wv�c� � X NONE l -4 �,L 1 ;`�,' _ FECAL CO
._ I -,f t2 l 4 .,4 f FECAL COLIFORM
if} ' x NONE to-q-Jl 'I .41 I FECAL COLIFORM
#;3
NONE FECAL COLIFORM
4$V11'a'i' , _ NONE ' J s~`F"� I 9:`-t I FECAL COLIFORM
l.a -'#-.2t `�-`�2
0P' X NONE 1 a -q-.2t` 4;42 FECAL COLIFORM
9r&itlquisl'4 by: DetafTime Received rj
Cit•iTime
,K - .Wl* i0_4-R1 /d-Dy-a( (1(30
t4Gn uialhad -
q 1: Date�me Received by: Date/Time
' GaComposite G=Grab DW.,Drinking
'" Syr Other Sidr :Water WW=Wastewater GWMW dGroundwator Monitoring Well Hi.V•rFiazarGovs Wane

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Monroe WQ Permit Number: WQ0001346
WWTP Name: WWTP cake NPDES Number: NC0024333
Monitoring Period: From 10/1/2021 To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) -Please indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment)❑ Alt. C (Prior Testing)❑
Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray 0 Gamma Ray ❑ Pasteurization ❑
Class B: AIt. (1) Fecal Density p Alt. (2)Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying LI Composting ❑ Aerobic Digestion LI
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen DensityNumber of Analytical
Parameter gExcee- Frequency Sample Tech-
in Sludge Minimum Geo. Mean Maximum Units deuces of Analysis Type niaue
2 x 10 to the MPN 6,293.94 11,726 14,059.87 MGN/g 0 quarterly grab sm9221e
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed:
Alt.1 (VS reduction) p Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4(Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying- Stable) LI Alt. 8 (Drying-Unstable) ❑
Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
to- �y�--- �1�i» .J� y14 us— a.2-3-.2aaa
Signature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T(12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Monroe WQ Permit Number: WQ0001346
WWTP Name: Monroe WWTP cake NPDES Number: NC0024333
Monitoring Period: From 10/1/2021 To 12/31/2021
Pathogen Reduction (40 CFR 503.32)- Please indicate level achieved and alternative performed:
Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑
Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑
If applicable to alternative performed(Class A only)indicate"Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: Alternative 1 0 Alternative 2 ❑
If applicable to alternative performed(Class B only)indicate"Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion 0
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Patho en Densi Number of Analytical
g ty Frequency Sample
Parameter Tech-
in Sludge Excee- of Analysis g Minimum Geo. Mean Maximum Units dences y Type moue
2 x 10 to the MPN 6,293.94 11,726 14,059.87 MGN/g 0 quarterly grab sm9221e
6th power
per gram of CFU
Fecal Coliform total solids
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(dry
coliform) weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4(Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying-Stable) ❑ Alt. 8 (Drying-Unstable) ❑
Alt. 9(Injection) ❑ Alt. 10(Incorporation) ❑ No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
1:1 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Kyle Ketchum, WWTP Superintendent Ken Morris, Residuals Coordinator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
/P lam`- ?l91?. 1' vwe a—3-Q
Signature of Preparer* Date Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (1 2/2006)

TAB 6
SOIL ANALYSIS

Sodium Calcium
Solids, Na, Na, Ca, Magnesium
Date/Sample decimal mg/kg mg/I Na, meq/L mg/kg Ca, mg/I Ca, meq/L Mg, mg/kg Mg, mg/I Mg, meq/L SAR
AL,,...
1/5/2021 WWTP 0.168 532 89.376' 3.89 13800 2318.4 115.92 2200 369.6 30.30 0.45
r
4/5/2021 WWTP 0.166 651 108.07 4.70 18300 3037.8 151.89 2540 421.64 34.56 0.49
7/6/2021 WWTP 0.23 709 163.07 7.09 13800 3174 158.70 2110 485.3 39.78, 0.71
10/4/2021 WWTP 0.208 606 126.05 5.48 15500 3224 161.20 2220 461.76 37.85 0.55
10/21/2021 WWTP 0.283 606 171.5 7.46 15500 4386.5 219.33 2220 628.26 51.50 0.64
O 0.00 0 0.00 0 0.00 #DIV/0!
O 0.00 0 0.00 0 0.00 #DIV/0!
O 0.00 0 0.00 0 0.00 #DIV/0!
It
1/5/2021 WTP 0.266 940 250.04 10.87 1950 518.7 25.94 414 110.124 9.03 2.60
4/5/2021 WTP 0.294 425 124.95 5.43 1660 488.04 24.40 408 119.952 9.83 1.31
7/6/2021 WTP 0.321 389 124.87 5.43 1690 542.49 27.12 424 136.104 11.16 1.24
10/4/2021 WTP 0.344 727 250.09 10.87 2970 1021.68 51.08 500 172 14.10 1.90
O 0.00 0 0.00 0 0.00 #DIV/01
O 0.00 0 0.00 0 0.00 #DIV/01
0 0.00 0 0.00 0 0.00 #DIV/0!
0 0.00 0 1 0.00 0 0.00 #DIV/0!
-
SAR= (E3/sgrt((li3+K3)/2)))
E3=Na,meq/L
H3=Ca,meq/L
IK3=Mg,meq/L

Exchangeable Sodium Percentage
ESP={(Na)/(Ca+Mg+K+Na)}x 100
Field ((Na) /(Ca+Mg+K+Na)}x100 ESP
NC-AN-19-1 0.9/ (42.4+16.8+2.3+0.9) X 100 1.44
NC-U N-18-1 0.7 / (58.2+13.6+4.1+0.7) X 100 .91
NC-U N-18-2 0.8 / (59.5+17.8+3.2+0.8) X 100 .98
NC-UN-18-7 1.0 / (57.5+18.3+2.2+1.0) X 100 1.27
NC-UN-18-8 1.0 / (49.7+13.6+1.6+1.0) X 100 1.52
NC-UN-29-1 1.6 / (46.3+21.2+4.4+1.6) X 100 2.18
NC-UN-29-2 1.1 / (49.3+19.8+11.1+1.1) X 100 1.35
NC-U N-29-3 1.2 / (56.6+22.5+4.5+1.2) X 100 1.42
N C-U N-29-4 0.9 / (54.6+23.6+9.6+0.9) X 100 1.01
NC-UN-29-5 1.9 / (43.4+19.4+4.5+1.9) X 100 2.75
NC-UN-30-1 0.9 / (49.5+25.4+11.2+0.9) X 100 1.03
NC-UN-30-4 1.4 / (58.4+23.5+1.2+1.4) X 100 1.66
NC-UN-30-5 1.4 / (53.8+22.0+1.4+1.4) X 100 1.78
NC-UN-31-3 0.7 / (45.0+13.9+15.3+0.7) X 100 .93
NC-UN-31-4 0.9 / (56.2+20.2+5.4+0.9) X 100 1.09
NC-U N-31-5 0.5 / (74.1+23.4+2.3+0.5) X 100 .50
NC-UN-31-6 0.5 / (73.0+21.4+2.4+0.5) X 100 .51
NC-U N-32-1 2.0 / (36.8+13.9+3.2+2.0) X 100 3.58
NC-UN-32-2 0.8 / (37.8+18.8+11.9+0.8) X 100 1.15
NC-UN-32-3 2.8 / (38.9+16.8+4.2+2.8) X 100 4.47
NC-UN-32-4 2.4 / (41.6+16.9+13.6+2.4) X 100 3.22
NC-UN-32-5 1.8 / (23.8+12.5+3.9+1.8) X 100 4.29

Page 1 of 1
Report Number: 22-019-1088O
Account Number:46205 Wa g oint 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: City of Monroe ANALYTICAL www.waypointanalytical.com
Ken Morris "Every acre...Every year.",. Grower: Pam Morris
775"freeway Dr 534 Hasty Rd
Monroe NC 28110
Farm: AN19
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 01/19/2022 Date Of Analysis: 01/20/2022 Date Of Report: 01/20/2022 NC=North Carolina Fertility Index Value
OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity 1 C.E.0
Sample ID Lab
Field ID Number % Soil M3 K Mg Ca Na Soil Buffer H
Rate Class lbs/A Rate ppm Rate ppmppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/100g meg1100g
AN19-1 18211 3.6 114 43 M 51 VL 113 H 475 L 12 VL 5.1 6.72 2.1 5.6
1 M MIN NC=36 NC=26
Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts
FieldSample ID ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS
% % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate
AN19-1 2.3 16.8 42.4 0.9 37.5 27 H 5.4 H 23 H 127 VH 2.8 H 0.2 VL
1 NC=56 NC=135.0 NC=144 NC=140.0
Values on this report represent the plant available nutrients in the Explanation of symbols:%(percent),ppm(parts per million),lbs/A This roport applies to sample(s)tested.Samples are retained a
soil.Rating after each value:VL(Very Low),L(Low),M(Medium), (pounds per acre),ms/cm(milli-mhos per centimeter),meq/100g maximum of thirty days after tasting.
H(High),VH(Very High).ENR-Estimated Nitrogen Release. (milli-equivalent per 100 grams).Conversions:ppm x 2=lbs/A,Soluble by: ?awa pit Grow
C.E.C.-Cation Exchange Capacity. Salts ms/cm x 640=ppm. Analysis prepared by:Wayp°intAnaly[ical Virginia,Inc.
Pauric Mc Groary Ph.D.,CPAg
Date Received: 01/19/2022
Date Of Report: 01/20/2022 SOIL FERTILITY RECOMMENDATIONS
Sample ID Yield Goal Lime Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron
Field ID Intended Crop Tons/A N P205 K2O Mg S Zn Mn Fe Cu B
Tons lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A
AN19-1
1 Pasture 3 1.8 50 40 120 0 0 0 0 0 0 0.5
Comments:
"The recommendations are based on research data and experience,but NO GUARANTEE or WARRANTY expressed or implied,concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„and may not be reproduced in whole or part,nor may any reference be made to the
wort,the results,or the company in any advertising,news release,or other public anouncements without obtaining our prior written authorization.Copy right 1977.

Page 1 of 2
Report Number: 22-019-1089 Vvo
Account Number:46205
\f (aypoi nt 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To City of Monroe ANALYTICAL www.waypointanalytical.com
Ken Morris "Every acre...Every year."rM Grower: Ben Myers
775 Treeway Dr 3208 Helms Pond Rd
Monroe NC 28110
Farm: UN 18
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Butler pH Loss On Ignition Water pH
Date Received: 01/19/2022 Date Of Analysis: 01/20/2022 Date Of Report: 01/20/2022 NC=North Carolina Fertility Index Value
OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0
Sample ID Lab
Field ID Number % Soil M3 K Mg Ca Na Soil Buffer H
Rate Class lbs/A
ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/long meq/long
UN 18-1 18212 6.0 150 428 VH 173 H 174 M 1245 M 17 VL 5.6 6.68 2.5 10.7
1278 H MIN NC=357 NC=88
UN 18-2 18213 4.4 127 90 H 95 M 160 H 893 M 14 VL 5.8 6.79 1.4 7.5
1278 M MIN NC=75 NC=49
UN 18-7 18215 3.9 118 203 VH 57 L 147 H 770 M 15 VL 5.7 6.79 1.4 6.7
1278 M MIN NC=169 NC=29
.UN 188-8 18216 3.6 I MIN 112 3NC= VH196 I I NC= VL I 111 M 676 L 15 VL 5.2 I 6.70 1 2.3 I 6.8
42
21
Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron soluble Salts
Sample ID
Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS
% % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate
.UN 18-1 4.1 13.6 58.2 0.7 23.4 18 M 20.9 VH 25 H 286 VH 8.6 VH 0.5 L
1278 NC=37 NC=522.5 NC=156 NC=430.0
UN 18-2 3.2 17.8 59.5 0.8 18.7 16 M 7.5 H 14 M 203 VH 3.5 VH 0.3 VL
1278 NC=33 NC=187.5 NC=88 NC=175.0
UN 18-7 2.2 18.3 57.5 1.0 20.9 14 L 11.6 VH 8 L 491 VH 2.0 H 0.5 L
1278 NC=29 NC=290.0 NC=50 NC=100.0
UN
1 2 7 818-8 1.6 I 13.6 I 49.7 I 1.0 33.8 I NC=29 NC4 185.0 I NC=56L I 335 VH 3.C1=1 5 0 VH 0.4 L I
Values on this report represent the plant available nutrients in the Explanation of symbols:%(percent),ppm(parts per million),lbs/A This report applies to sample(s)tested.Samples are retained a
soil.Rating after each value:VL(Very Low),L(Low),M(Medium), (pounds per acre),ms/cm(milli-mhos per centimeter),meq/100g maximum of thirty days after testing. yy
H(High),VH(Very Hlgh).ENR-Estimated Nitrogen Release. (milli-equivalent per 100 grams).Conversions:ppm x 2=lbs/A,Soluble by: Tampa Mt brow
G.E.C.-Cation Exchange Capacity. Salts ms/cm x 640=ppm. Analysis prepared by:Waypeint Analytical Virginia,Inc.
Pauric Mc Groary Ph.D.,CPAg

Page 2 of 2
Report Number: 22-019-1089O
Account Number:46205 \ Vaypou nt... 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: City of Monroe ANALYTICAL www.waypointanalytical.com
Ken Morris "Every acre...Every year."710 Grower: Ben Myers
775 Treeway Dr 3208 Helms Pond Rd
Monroe NC 28110
Farm: UN 18
Date Received: 01/19/2022
Date Of Report: 01/20/2022 SOIL FERTILITY RECOMMENDATIONS
Sample ID Field ID Intended Crop Yield Goal Tons/A
Ume
Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron
N P205 (CZO Mg S Zn Mn Fe Cu B
Tons lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A Ib1A
UN 18-1
1 2 7 8 Pasture 3 1.3 50 0 40 0 10 0 0 0 0 0
UN 18-2
1 2 7 8 Pasture 3 0.8 50 30 69 0 13 0 2 0 0 0.5
UN 18-7
1 2 7 8 Pasture 3 0.8 50 0 116 0 15 0 3 0 0 0
UN 18-8
1 2 7 8 Pasture 3 1.5 50 0 120 0 15 0 3 0 0 0
Comments:
Sample(s) :UN 18-2,UN 18-7,UN 18-8 Crop:Pasture
For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer.
For soils low in sulfur,apply 20-40 lbs of sulfur as a sulfate in the spring with the nitrogen.
"The recommendations are based on research data and experience,but NO GUARANTEE or WARRANTY expressed or implied,concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„and may not be reproduced in whole or part,nor may any reference be made to the 1 pWFt ftl t (r/owy�
work,the results,or the company in any advertising,news release,or other public anouncements without obtaining our prior written authorization.Copy right 1977. 0
Pauric Mc Groary Ph.D.,CPAg

Page 1 of 2
Report Number: 22-019-1086 W
Account Number:46205 WaYPOi nt 7621chmond,VA 23237
Main 804 itepine Road,743 9401 to Fax [phone]
Send To: City of Monroe ANALYTICAL www.waypointanalytical.com
Ken Morris 'Every acre...Everyyear."r. Grower: William Griffin
775 Treeway Dr 6705 Austin Grove Rd
Monroe NC 28110
Farm: UN 29
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 01/19/2022 Date Of Analysis: 01/20/2022 Date Of Report: 01/20/2022 NC=North Carolina Fertility Index Value
OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0
Sample ID Lab
Field ID Number % Soil lbs/A M3 K Mg Ca Na Soil Buffer H
Rate Class ppm Rate ppm Rate ppm Rateppm Rateppm Rate H ppm Rate ppm Rate P Index megl100g megl104g
UN 29-1 18201 4.0 120 140 VH 124 M 186 H 676 L 27 VL 5.5 6.74 1.9 7.3
12345 M MIN NC=117 NC=63
UN 29-2 18202 4.7 132 264 VH 358 VH 197 H 819 L 21 VL 5.8 6.77 1.6 8.3
12345 M MIN NC=220 NC=183
UN 29-3 18204 3.7 113 231 VH 138 H 213 H 895 M 21 VL 6.0 6.81 1.2 7.9
12345 M MIN NC=192 NC=71
UN 29-4 18205 4.5 130 111 VH 258 VH 195 H 754 M 14 VL 6.2 0.8 6.9
12345 M MIN NC=92 NC=132
UN 29-5 18206 4.7 136 111 VH 99 M 133 H 495 L 25 VL 5.3 6.75 1.8 5.7
12345 MP MIN NC=92 NC=51 1
Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron soluble Salts
Sample ID
Field ID K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS
% % % % % ppm Rate ppm Rate ppm Rate pprn Rate ppm Rate ppm Rate ppm Rate ms/cm Rate
W
UN 29-1 4.4 21.2 46.3 1.6 26.0 17 M 5.6 H 33 H 214 VH 7.9 VH 0.3 VL
12345 NC=35 NC=140.0 NC=206 NC=395.0
UN 29-2 11.1 19.8 49.3 1.1 19.3 20 M 6.4 H 33 H 227 VH 10.2 VH 0.4 L
12345 NC=42 NC=160.0 NC=206 NC=510.0
UN 29-3 4.5 22.5 56.6 1.2 15.2 15 L 6.8 H 14 M 155 VH 9.5 VH 0.3 VL
12345 NC=31 NC=170.0 NC=88 NC=475.0
UN 29-4 9.6 23.6 54.6 0.9 11.6 15 L 6.7 H 20 M 127 VH 8.3 VH 0.3 VL
12345 NC=31 NC=167.5 NC=125 NC=415.0I
UN 29-5 2345 4.5 19.4 I 43.4 I 1.9 31.6 14 L 3.2 M 86 NC=29 NC=800 NC=538H 189 VH NC9 2 VH 0.3 VL
Values on this report represent the plant available nutrients in the Explanation of symbols:%(percent),ppm(parts per million),lbs/A This report applies to sample)si tested.Samples are retained a
soil.Rating after each value:VL(Very Low),L(Low),M(Medium), (pounds per acre),ms/cm(milli-mhos per centimeter},meg/100g maximum of thirty days after testing.
H(High),VH(Very High).ENR-Estimated Nitrogen Release. (milli-equivalent per 100 grams).Conversions:ppm x 2=lbs/A,Soluble by: tncc pr b(aarµ/
C.E.C.-Cation Exchange Capacity. Salts ms/cm x 640=ppm. Analysis prepared by:waypoint Analytical Virginia,Inc. o
Pauric Mc Groary Ph.D.,CPAg

Page 2 of 2
Report Number: 22-019-1086O
Account Number:46205
\Atapoint, 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: City of Monroe ANALYTICAL www.waypointanalytical.com
Ken Morris "Every acre...Everyyear."TM Grower: William Griffin
775 Treeway Dr 6705 Austin Grove Rd
Monroe NC 28110
Farm: UN 29
Dale Received: 01/19/2022
Date Of Report: 01/20/2022 SOIL FERTILITY RECOMMENDATIONS
Sample ID Yield Goal Lime Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron
Field ID Intended Crop N P205 K2O Mg S Zn Mn Fe Cu B
Tons Tons/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A
UN 29-1
1 2 3 4 5 Pasture 3 1.3 50 0 40 0 11 0 0 0 0 0.5
UN 29-2
1 2 3 4 5 Pasture 3 1.0 50 0 0 0 8 0 0 0 0 0
UN 29-3
1 2 3 4 5 Pasture 3 0.8 50 0 40 0 14 0 2 0 0 0.5
UN 29-4
1 2 3 4 5 Pasture 3 0.0 50 0 0 0 14 0 2 0 0 0.5
UN 29-5
t 2 3 4 5 Pasture 3 1.3 50 0 64 0 15 0 0 0 0 0.5
Comments:
Sample(s) : UN 29-2,UN 29-3,UN 29-4,UN 29-5 Crop:Pasture
For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer.
For soils low in sulfur,apply 20-40 lbs of sulfur as a sulfate in the spring with the nitrogen.
"The recommendations are based on research data and experience,but NO GUARANTEE or WARRANTY expressed or implied,concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„and may not be reproduced in whole or part,nor may any reference be made to the lam !h t tca+ir
work,the results,or the company in any advertising,news release,or other public anouncements without obtaining our prior written authorization.Copy right 1977. U
Pauric Mc Groary Ph.D.,CPAg

Page 1 of 2
Report Number: 22-019-1085O
Account Number:46205
\/ ilani,oi u t.. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: City of Monroe ANALYTICAL www.waypointanalytical.com
Ken Morris "Every acre...Every year.'m Grower: TGom Appenzelier
775 Treeway Dr 830 Clover Rd
Monroe NC 28110
Farm: UIN 30
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 01/19/2022 Date Of Analysis: 01/20/2022 Date Of Report: 01/20/2022 NC=North Carolina Fertility Index Value
OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0
Sample ID Lab
Field ID Number % Soil lbs/A M3 K Mg Ca Na Soil Buffer H
Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate H
ppm Rate P Index megl100g meg1100g
UN 30-1 18198 4.1 123 140 VH 289 VH 201 VH 654 L 14 VL 6.1 6.84 0.9 6.6
145 M MIN NC=117 NC=148
UN 30-4 18199 3.7 116 62 H 25 VL 152 H 631 M 18 VL 6.0 6.85 0.8 5.4
145 M MIN NC=52 NC=13
UN 30-5 18200 3.2 108 49 M 24 VL 116 H 473 M 14 VL 5.7 6.84 0.9 4.4
145 M MIN NC=41 NC=12
Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts
SampFeld IIDD ID K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS
% % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate
UN 30-1 11.2 25.4 49.5 0.9 13.6 22 M 4.9 H 14 M 130 VH 5.3 VH 0.3 VL
145 NC=46 NC=122.5 NC=88 NC=265.0
UN 30-4 1.2 23.5 58.4 1.4 14.8 13 L 2.1 L 9 L 109 VH 2.7 H 0.3 VL
145 NC=27 NC=52.5 NC=56 NC=135.0
UN 50-5 1.4 22.0 I 53.8 1.4 20.5 I NC=29 NC=87S 14 L 3.5 H I NC=106 17 M 113 VH I 2.NC3 115.0 H 0.2 VL 1 +
Values on this report represent the plant available nutrients in the Explanation of symbols:%(percent),ppm(parts per million),lbs/A This report applies to sample(s)tested.Samples are retained a
soil.Rating after each value:VL(Very Low),L(Low),M(Medium), (pounds per acre),ms/cm(milli-mhos per centimeter),meg/100g maximum of thirty days after testing. Q
H(High),VH(Very High).ENR-Estimated Nitrogen Release. (milli-equivalent per 100 grams).Conversions:ppm x 2=lbs/A,Soluble by: lair am 6,1c4Ny/
C.E.C.-Cation Exchange Capacity. Salts ms/cm x 640=ppm. Analysis prepared by:Waypoint Analytical Virginia,Inc. a
Pauric Mc Groary Ph.D.,CPAg

Page 2 of 2
Report Number: 22-019-1085 Y ro
Account Number:46205 1/11
Waypoi nt... 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: City of Monroe ANALYTICAL www.waypointanalytical.com
Ken Morris 'Every acre...Every year."7m Grower:TGom Appenzeller
775 Treeway Dr 830 Clover Rd
Monroe NC 28110
Farm: UIN 30
Date Received: 01/19/2022
Date Of Report: 01/20/2022 SOIL FERTILITY RECOMMENDATIONS
Sample ID Yield Goal Llme Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron
Field Intended Crop Tons/A N P205 K20 Mg S Zn Mn Fe Cu B
Tons lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A
UN 30-1
1 4 5 Pasture 3 0.8 50 0 0 0 6 0 2 0 0 0.5
UN 30-4
Pasture 3 0.8 50 30 120 0 16 2.0 3 0 0 0.5
145
UN 30-5
1 4 5 Pasture 3 0.8 50 40 120 0 15 0 2 0 0 0.5
Comments:
Sample(s) : UN 30-4,UN 30-5 Crop: Pasture
For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer.
For soils low in sulfur,apply 20-40 lbs of sulfur as a sulfate in the spring with the nitrogen.
"The recommendations are based on research data and experience,but NO GUARANTEE or WARRANTY expressed or implied,concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„and may not be reproduced in whole or part,nor may any reference be made to the l aHnc plc &roarN -
work,the results,or the company in any advertising,news release,or other public anouncements without obtaining our prior written authorization.Copy right 1977. 00
Pauric Mc Groary Ph.D.,CPAg

Page 1 of 2
Report Number: 22-019-1087 {A_�
Account Number:46205 yy
\% jpoint 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: City of Monroe ANALYTICAL www.waypointanalytical.com
Ken Morris "Every acre...Every year."rM Grower: Henry Myers
775 Treeway Dr 3809 Farmwood Rd
Monroe NC 28110
Farm: UN31
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 01/19/2022 Date Of Analysis: 01/20/2022 Date Of Report: 01/20/2022 NC=North Carolina Fertility Index Value
OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0
Sample ID Lab
Field ID Number % Soil lbs/A M3 K Mg Ca Na Soil Buffer H
Rate Classppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meg1100g meg1100g
UN 31-3 18207 5.3 145 98 H 466 VH 130 M 702 L 12 VL 5.5 6.73 2.0 7-8
3456 H MIN NC=82 NC=238
UN 31-4 18208 6.4 150 144 VH 196 VH 225 H 1045 M 20 VL 5.9 6.77 1.6 9.3
3456 H MIN NC=120 NC=100
UN 31-5 18209 6.0 150 292 VH 105 M 329 H 1734 H 13 VL 7.0 0.0 11.7
3456 H MIN NC=243 NC=54
UN 31-6 18210 3.1 97 181 VH 95 L 264 H 1503 H 12 VL 6.8 0.3 10.3
3456 M MIN , NC=151 I I NC=49
Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron ' Soluble Salts
Sample ID
Field ID K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS
% % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate
UN 31-3 15.3 13.9 45.0 0.7 25.6 14 L 6.6 H 45 H 250 VH 3.4 VH 0.4 L
3456 NC=29 NC=165.0 NC=281 I NC=170.0
UN 31-4 5.4 20.2 56.2 0.9 17.2 18 M 11.2 VH 17 M 290 VH 5.1 VH 0.6 M
3456 NC=37 NC=280.0 NC=106 NC=255.0
UN 31-5 2.3 23.4 74.1 0.5 0.0 15 L 15.4 VH 42 H 243 VH 6.5 VH 0.8 M
3456 NC=31 NC=385.0 NC=263 NC=325.0
UN 31-6 I 2.4 21.4 73.0 0.5 I 2.9 12 L 6.8 H 96 VH 319 VH r 4.1 VH 0.6 M
3456 !I NC=25 NC=170.0 NC=600 I NC=205,0
Values on this report represent the plant available nutrients in the Explanation of symbols:%(percent),ppm(parts per million),lbs/A This report applies to sample(s)tested.Samples are retained a
soil Rating after each value:VL(Very Low),L(Low),M(Medium), (pounds per acre),ms/cm(milli-mhos per centimeter),meq/100g maximum of thirty days after tasting.
H(High),VH(Very High).ENR-Estimated Nitrogen Release. (milli-equivalent per 100 grams).Conversions:ppm x 2=lbs/A,Soluble by: t ,c plc brNT
C.E.C.-Cation Exchange Capacity. Salts ms/cm x 640=ppm. Analysis prepared by:Waypoint Analytical Virginia,Inc.
Pauric Mc Groary Ph.D.,CPAg

Page 2 of 2
Report Number: 22-019-1087o
Account Number:46205
Waypol nt. 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: City of Monroe ANALYTICAL www.waypointanalytical.com
Ken Morris "Every acre...Every year."TM Grower: Henry Myers
775 Treeway Dr 3809 Farmwood Rd
Monroe NC 28110
Farm: UN31
Date Received: 01/19/2022
Date Of Report: 01/20/2022 SOIL FERTILITY RECOMMENDATIONS
Sample ID Yield Goal Lime Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron
Field ID Intended Crop N P2O5 KZO Mg S Zn Mn Fe Cu B
Tons Tons/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A
UN 31-3
3 4 5 fi Pasture 3 1.5 50 30 0 0 15 0 0 0 0 0
UN 31-4
3 4 5 6 Pasture 3 1.0 50 0 0 0 10 0 2 0 0 0
UN 31-5
3 4 5 6 Wheat 65 0.0 67 0 70 0 14 0 0 0 0 0.5
UN 31-6
Wheat 65 0.0 82 0 76 0 17 0.6 0 0 0 0.5
345fi
Comments:
Sample(s) : UN 31-4 Crop:Pasture
For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer.
For soils low in sulfur,apply 20-40 lbs of sulfur as a sulfate in the spring with the nitrogen.
"The recommendations are based on research data and experience,but NO GUARANTEE or WARRANTY expressed or implied,concerning crop performance is made." q
Our reports and letters are for the exclusive and confidential use of our clients„and may not be reproduced in whole or part,nor may any reference be made to the 14,44ra p1t GrodOµ/
work,the results,or the company in any advertising,news release,or other public anouncements without obtaining our prior written authorization.Copy right 1977. 0
Pauric Mc Groary Ph.D.,CPAg

Page 1 of 2
Report Number: 22-019-1084 �A■�
• 11�
Account Number:46205 WaYpolnt.. 7621Ma Whitepine
9401°RichmondF x 804 2A 23237
-6446
Send To City of Monroe ANALYTICAL www.waypointanalytfcal.com
Ken Morris "Every acre...Every year."., Grower: Danny Baker
775 Treeway Dr 2015 Hasty Rd
Monroe NC 28110
Farm: UN32
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 01/19/2022 Date Of Analysis: 01/20/2022 Date Of Report: 01/20/2022 NC=North Carolina Fertility Index Value
OM WIV ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0
Sample ID Lab
Field ID Number % Soil lbs/A M3 K Mg Ca Na Soil Buffer H
Rate Classppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meg1100g meg1100g
UN 32-1 18193 4.2 127 33 M 58 L 77 M 339 L 21 VL 4.9 6.73 2.0 4.6
12345 M MIN NC=27 NC=30
UN 32-2 18194 6.2 150 133 VH 465 VH 226 H 756 L 19 VL 5.3 6.62 3.1 10.0
12345 H MIN NC=111 NC=238
UN 32-3 18195 4.8 136 28 L 116 M 141 H 545 L 45 L 5.1 6.67 2.6 7.0
12345 M MIN NC=23 NC=59
UN 32-4 18196 5.2 142 79 H 457 VH 174 H 715 L 48 L 5.5 6.71 2.2 8.6
12345 H MIN NC=66 NC=234
UN 32-5 18197 5.5 150 16 L 94 M 93 M 295 VL 26 VL 4.5 6.57 3.6 6.2
12345 I H I MIN i I NC=13 I NC=48
Percent Base Saturation Nitrate Sulfur . Zinc Manganese Iron Copper Boron Soluble Salts
Sample ID -
Field ID K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS
% % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate
•
UN 32-1 3.2 13.9 36.8 2.0 43.5 15 L 0.9 VL 58 VH 133 VH 2.0 H 0.1 VL
12345 NC=31 NC=22.5 NC=363 NC=100.0
UN 32-2 11.9 18.8 37.8 0.8 31.0 26 H 3.3 M 12 M 141 VH 2.8 H 0.2 VL
12345 NC=54 NC=82.5 NC=75 NC=140.0
UN 32-3 4.2 16.8 38.9 2.8 37.1 52 VH 0.8 VL 16 M 140 VH 1.4 M 0.2 VL
12345 NC=108 NC=20.0 NC=100 NC=70.0
UN 32-4 13.6 16.9 41.6 2.4 25.6 34 H 2.4 M 45 H 145 VH 3.2 VH 0.3 VL
12345 NC=71 NC=60.0 NC=281 NC=160.0
UN 32-5
12345 I 3.9 I 12.5 23.8 1.8 58.1 16 M 0.9 VL 85 NC=33 NC=22.5 NC=531H 147 VH NC=60.0 1.2 M 0.1 VL
Values on this report represent the plant available nutrients in the Explanation of symbols:%(percent),ppm(parts per million),lbs/A This report applies to sample(s)tested.Samples are retained a
soil.Rating after each value:VL(Very Low),L(Low),M(Medium), (pounds per acre),ms/cm(milli-mhos per centimeter),meq/t 00g maximum of thirty days after testing. pq
H(High),VH(Very High).ENR-Estimated Nitrogen Release. (milli-equivalent per 100 grams).Conversions:ppm x 2=lbs/A,Soluble by. lava pit GMT
C.E.C.-Cation Exchange Capacity. Salts ms/cm x 640=ppm. Analysis prepared by:waypointAnalytical Virginia,Inc.
Pauric Mc Groary Ph.D.,CPAg

Page 2 of 2
Report Number: 22-019-1084 W
Account Number:46205 Waypoint..: 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: City of Monroe ANALYTICAL www.waypointanalyticaicom
Ken Morris "Every acre...Every year." Grower: Danny Baker
775 Treeway Dr 2015 Hasty Rd
Monroe NC 28110
Farm: UN32
Date Received:01/19/2022
Date Of Report: 01/20/2022 SOIL FERTILITY RECOMMENDATIONS
Sample ID Yield Goal Lime Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron
Field ID Intended Crop N P205 K20 Mg S Zn Mn Fe Cu B
Tons Tons/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A lb/A
UN 32-1
1 2 3 4 5 Pasture 3 1.8 50 40 95 0 14 3.0 0 0 0 0.5
UN 32-2
1 2 3 4 5 Pasture 3 1.8 50 0 0 0 0 0 2 0 0 0.5
UN 32-3
1 2 3 4 5 Pasture 3 2.0 50 50 43 0 0 3.0 2 0 0 0.5
UN 32-4
1 2 3 4 5 Pasture 3 1.5 50 30 0 0 0 0 0 0 0 0.5
UN 32-5
1 2 3 4 5 Pasture 3 2.3 50 76 70 0 13 3.0 0 0 0 0.5
Comments:
Sample(s) : UN 32-2,UN 32-3,UN 32-4,UN 32-5 Crop:Pasture
For grass hay or pasture needing high rates split the P and K application. Apply 1/2 in the spring and 1/2 in late summer.
For soils low in sulfur,apply 20-40 lbs of sulfur as a sulfate in the spring with the nitrogen.
"The recommendations are based on research data and experience,but NO GUARANTEE or WARRANTY expressed or implied,concerning crop performance is made." Q
Our reports and letters are for the exclusive and confidential use of our clients„and may not be reproduced in whole or part,nor may any reference be made to the ;iodic Pit GrYorter
work,the results,or the company in any advertising,news release,or other public anouncements without obtaining our prior written authorization.Copy right 1977.
Pauric Mc Groary Ph.D.,CPAg