HomeMy WebLinkAboutWQ0001953_Residual Annual Report 2021_20220210Non -Discharge Branch Upload/Submittal Form
NORTH CAROLINA
En.anmemfal Qualify
Version 2 - Revised June 23, 2020
Initial Review
Reviewer
EADS\ndthornburg
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?*
Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0001953
Applicant/Permittee Town of Spindale
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office
CO Reviewer
Admin Reviewer
Asheville
Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name*
Guy O'Connor
Email Address* Phone Number*
goconnor@spindalenc.net 8282863403
Project Information
Application/Document Type *
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
Permit Number:* WQ0001953
Has Current Existing permit number
Applicant/Permittee Address* PO Box 186 Spindale NC 28160
Facility Name*
Town of Spindale Class B Residuals Program
Please provide comments/notes on your current submittal below.
High -Rate Infiltration
Reclaimed Water
Residuals
Other
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at nathaniel.thornburg@ncdenr.gov.
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2020 LAND APPICATION ANNUAL REPORT.pdf 13.56MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
lj 0Cor ve
Submission Date 2/10/2022
2020
Town of Spindale
Wastewater Treatment Plant
2020 Annual Report
Land Application Program
Permit No. WQ0001953
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0001953 County:
Facility Name (as shown on permit):
Land Application Operator:
Rutherford
Year: 2020
Town of Spindale
US Biosolids, Inc.
Phone: 336-957-7871
Land application of residuals as allowed by the permit occurred during the past calendar year?
Yes No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit:
6
Total number of fields utilized for land application during the year:
4
Total amount of dry tons applied during the year for all application sites:
10.2
Total number of acres utilizes for land application during the year:
58.3
Part B - Annual Compiance Statement:
Facility was compliant during calendar year
2020 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. 0 Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Sc71✓t ct.,c ,) , -2 /7 0_(
Permittee Name and Title (type or print) Signature of Permittee Date
Signature of Preparer* Date Signature of Land ATier
(if different from Permittee)
2-$-29at
Date
(if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
Waypoint Analytical
0
Town of Spindale
Facility Name:
Town of Spindale WWTP
Sample or Composite Date
O
0
N
v)
00•
M
O
N
25
—
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—
Vl
•
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00
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i
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ZI
M
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)
9330
0
O
N
31800
0
O
-
Conc.
Limit
(mg/kg)a
Q
z
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v,
0
0
M
NA
840
LS
420
0
C)
NA
<
z
<
z
NA
Parameter
(mg/kg)
Percent Solids (%)
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
)
U
z
E
.=•
8
U
•-
N
Total Phosphorus
TKN
Ammonia -Nitrogen
Nitrate and Nitrite
DENR FORM RSSF (12/2006)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
CAS
A
RS
Cd
6J
L
•
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et E
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Waypoint Analytical
WQ Permit Number: WQ0001953
Town of Spindale
Facility Name:
Residual Source
NPDES # or WQ#:
Town of Spindale WWTP
Sample or Composite Date
O
v)
97000
.
6230
12500
cc.O
N
117000
255
23500 1
2950
O
3.29 1
Parameter
(mg/kg)
Organic N
A.
E
C
c
Q
O_
U
U
O
Magnesium
Maganese
Poatassium
Sodium
Sulfur
PAN
SAR
Signature of Preparer
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF -
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Town of Spindale
WQ0001953
Total Dry Tons Applied (Annual): 2.05
Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series: PaC2
Acres Used:
15.1 Acres Permitted:
15.1
Site #:
M
Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, "A) Solids use Raw Percent #
Sample or
Com-
posite
Date
1
6/5/20
2
3 j
4'
5
6
7
8
9
10 i
11 .
12
Solids
0.38
Arsenic
25
Cadmium
25
Copper
131
Chromium
62.5
Lead
75
Mercury
3.83
Molyb-
denum
62.5
Nickel
62.5
Selenium
12
Zinc
313
Total
Phos-
phorus
9330
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
App.
Event
1 ''
0.14
2 j
3
4.
5
6
7
8 i
9
10 £
11
12
Totals:
Arsenic
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.036
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Chromium
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Lead
0.020
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb
denum
0 017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Nickel
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Selenium
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Zinc
0.085
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.085
Total
Phos-
phorus
2.538
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.538
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
t-$J03\
Date
DENR FORM MFLSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
It•
Acres Utilized:
Facility Name: Town of Spindale
Acres Permitted:
Land Owner: John McFadden
Cation Exchange Capacity (non 503):
Predominant Soil Series: PaC2
John McFadden
0
z
a
L
2
L.
U
Name of Crop Type
Receiving Residual
Application
Crop 2
I Lime Applied I
Ual
O
O
O
N
—
=-
O
U
0
U
N
ti
PAN Applied
( lbs/acre)
N
o.
2
V
<
z
O
o
O
o
co
0
0
0
co
0
O
0
O
0
O
0
O
0
O
0
0
0
O
0
O
0
O
0
0
0
0
0
O
0
0
0
0
o
O
0
0
O
O
0
0
0
0
0
CO
.r
^
0
2
U
00
N
0
0
O
O
0
0
CD
O
0
0
CD
O
0
0
CD
O
0
o
O
0
O
0
O
0
o
0
O
0
0
0
O
0
o
0
O
0
O
0
O
0
o
0
O
O0
rV
y •y.
a • •� m
'z `t z E
c
—
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): I
—en
00
N
c
N
00
00
O
O
so
r`
N
N
00
c,
N
N
o0
o.
N
Ammonia CA
0,
Nitrogen E
O
o
cc
--re,
�o��o.
O
O
O
z OD
F' E
0
N
I
Z
0.017
3.004
o
ri
374
Mineralization
Rate***
o
Volatilization
Rate**
.n
o
o
-
o
rn
0
o
z
Z
0
o
0
0
0-
0
^
Application
Method*
y
.
c,_O
O
Cl c,
N
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O
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N
cc
rn
Residual Sources
' (NPDES #. WQ#.
Fert.. Animal
Waste. etc)
M
V,
O
0
0
3
U
co
0
0.047
0.054
M
Volume
Applied per
Acre
(Dry Tons/Ac)
—
O
0.000 I
0.000
O
O
0.000
O
0
0
O
0
O
0.000
0.000
0.000
O
d
<
0
O
0
O
O
O
I 36
cA
-G
cn
CO
O
Annual lbs/acre
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
'Permit PAN Limit lst/2nd Crop
Volume applied
(enter one) Solids/
Liquid
Cu. Yds I Gallons
0
O
0
rn
I 130000'
glumW
JO MG
4-2020
TOTALS:
0
Signature of Land Applier
DENR FORM FSF (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Town of Spindale
WQ0001953
Total Dry Tons Applied (Annual): 2.17
Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series: PaC2
Acres Used:
15.5 Acres Permitted:
15.5
Site #:
M Field #:
3
Residual Analysis Data (Ekeavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
6/5/20
2!
3_._
4
5'
6
7+
v
8
v 9
10 1
11 '
12 I
.............
% Solids
0.38
Arsenic
25
Cadmium
25
Copper
131
Chromium
62.5
Lead
75
Mercury
3.83
Molyb-
denum
62.5
Nickel
62.5
Selenium
12
Zinc
313
Total
Phos-
phorus
9330
nnual Heavy Metal Ficld Loadings (Calculated in lbs/acre):
Iota I
App.
Event
1
0.14
2
3;
4
5 '.
6
7 '.'
8
9
10
11
12 1
Totals:
Arsenic
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Chromium
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
I,ead
0.021
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.021
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb
denum
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Nickel
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.018
Selenium
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Zinc
0.088
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.088
Total
Phos-
phorus
IIN
2.612
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.612
certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
1 am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Acres Utilized:
Field #: M3
WQ Permit #: WQ0001953
Facility Name: Town of Spindale
Acres Permitted:
Annual Dry Tons Applied: 2.1630
Land Owner: John McFadden
Cation Exchange Capacity (non 503):
Predominant Soil Series: PaC2
John McFadden
Crop 2 Max. PAN:
R
Z
0
00
Name of Crop Type
Receiving Residual
Appl ication
Crop 2
I Lime Applied
cod
VI
o
O
O
0.
O
y
v
[i
L...1
ON
CV
PAN Applied
( Ibs/acre)
N
Ci
o
U
<
z
O
o
o
O
O
0
o
o
O
0
O
0
O
0
o
0
O
0
o
0
O
0
c
0
O
0
o
0
O
0
o
0
O
0
O
C
O
0
o
0
O
0
0
0
O
0
0
0
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0
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0
0
0
0
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0
0
0
0
0
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0
0
0
0
0
0
0
0
0
o
0
o
0
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0
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0
o
0
0
0
0
0
o
0
0
0
o
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0
0
O
0
^
o
M
N 412
CZ b • C m
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^
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
rl
r‘i
Ammonia m
Nitrogen E
f.,
c
N
o
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V1
oo
N
M
N
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Mineralization
Rate***
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0
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0
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Volatilization
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Application
Method*
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N
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Residual Sources
(NPDES #, WQ#.
Pert.. Animal
Waste. etc)
n
Q,
0
0
0
a
O
U
O
O
I.
N
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N
en
-
b
U
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0
0
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0
0
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en
Volume
Applied per
Acre
(Dry Tons/Ac)
•--
O
o
CD
O
0
CDO
O
0.000
0.000
0
O
0.000
0.000
0.000 I
0.000
0.000
0.000
sd
0.007
.o
O
O
L 0.068
M
00
M
O
(Annual lbs/acre
Prior Years Cumulative lbs/ac
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop
Volume applied
(enter one) Solids/
Liquid
Cu. Yds I Gallons
136500
136500
0
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4-2020
(TOTALS:
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to
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ti CA •q
L
E
o
L
v ea
— w.
Cr •
Signature of Land Applier
DENR FORM FSF (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale Total Dry Tons Applied (Annual): 3.71
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: John McFadden Owner: John McFadden Predominant Soil Series: PaC2
Acres Used:
17.1 Acres Permitted:
17.1
Site #:
M
Field #:
4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
_ ?_'
6/5/20
2 j
3
4
5
6
7
8
9
10�
11 r
__.
12
_T
% Solids
0.38
Arsenic
25
Cadmium
25
Copper
131
Chromium
62.5
Lead
75
Mercury
3.83
Molyb-
denum
62.5
Nickel
62.5
Selenium
12
Zinc
313
Total
Phos-
phorus
9330
nnual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
DT/Ac./
App.
Event
1!
2
3
4
5
6
7
8!
9
10
11
12
Totals:
0.22
_
Arsenic
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
0.057
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.057
Chromium
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Lead
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb
denum
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Nickel
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Selenium
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Zinc
0.136
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.136
Total
Phos-
phorus
4.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.049
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
11 t741
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
N
L
Field #: M4
WQ Permit #: WQ0001953
Facility Name: Town of Spindale
Acres Permitted: 17.1
Annual Dry Tons Applied: 3.7080
Land Owner: John McFadden
Cation Exchange Capacity (non 503):
Predominant Soil Series: PaC2
John McFadden
Crop 2 Max. PAN:
00
Name of Crop Type
Receiving Residual
Application
Crop 2 I
Lime Applied
lbs/ac I
0
0
0
O
U
N
[i
vv
Ca.
Y
0
o
N
PAN Applied
( lbs/acre)
N
a.
2
C..)o
<
z
<
z
0
o
O
0
O
O
0
0
o
O
0
0
O
O
0
O
o
O
0
0
O
O
0
0
o
C
0
0
o
O
0
O
O
O
0
O
0
O
0
0
O
O
0
158
-
Q.
CJ
°`
ut
_
0
l�
s.0
0
O
O
0
0
o
O
C
0
0
O
0
0
0
O
0
0
0
O
0
0
0
O
0
0
0
O
0
0
0
O
0
0
0
O
0
0
0
O
O
Cr
N
ON
U O�
rn
z Z E
O
oc>
�
0Y
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
a`
0
v
Ammonia rn
Nitrogen E
00
,.,
0
,.,
c°°
N
o
to
v
0,_°
CN
N
z m
E-' E
0
0
N
-
0
0
N
-
a>
v.)
0
o
O
.1.
O
et
O
00
Mineralization
Rate***
en
o
enN
o
z
O
0^
s0
O`
o
D
—
'
M
Volatilization
Rate**
.
o
v,
0
0
c
0
o
0
_N
0
z
Application
Method*
y
op
z
o
0
o
-
0
o
o
0
c
^
d N •N
U
0
0
clt.O
en
000
C
l-
0c
r-
N
Q
cA u 'S
-,
-.
U
N
O
0
N
^^
z
Residual Sources
(NPDES #, WQ#.
Fert., Animal
Waste, etc)
M
v,
T
0
0
0.
3
M
V",
O•
0
0
0'
3
U
0.057
cr•
^
so
VI
^
1338
—
o
o
c�
0
O
00
0
O
;V
�
Volume
Applied per
Acre
(Dry Tons/Ac)
tr)
-
O
el
00
O
0.000
0
O
00
0
O
0
0
O
0
0
O
0.000
0.000
0.000
0
0
O
0.000
As
110'0
0.047
v�i
0
O
`
M°
o -
cA
00
<--)M
O
00
o
Annual Ibs/acre
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac i
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
156000
78000
234000
glumW
ao aje4
0
O
N
TOTALS:
CC
0
on
O
L
E
0
L
E
•C
0
1r'
R 0
>,
o
0
CI y
c a
c44
rOj, •�
c L
a. 0
4.
u e0 O
Signature of Land Applier
DENR FORM FSF (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Spindale . Total Dry Tons Applied (Annual):
WQ0001953
Cation Exchange Capacity (non 503 only):
2.27
John McFadden Owner: John McFadden Predominant Soil Series: CaB2
10.6 Acres Permitted:
10.6 Site #:
M Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, °Ao Solids use Raw Percent #):
Sample or
Com-
posite
Date
.._11_ `
6/5/20
2
3
4;
._. 5
6(
7,
8 1
9
10 -11
12 ;
% Solids
0.38
Arsenic
25
Cadmium
25
Copper
131
Chromium
62.5
Lead
75
Mercury
3.83
Molyb-
denum
62.5
Nickel
62.5
Selenium
12
Zinc
313
Total
Phos-
phorus
9330
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
DT/Ac./
App.
Event
11
0.21
21
3]
4
5
6!
7
8)
9
10
11
12]
Totals:
Arsenic
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.056
Chromium
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Lead
0.032
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.032
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb
denum
0 027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Nickel
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Selenium
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Zinc
0.134
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.134
Total
Phos-
phorus
3.993
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.993
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
)7i'v 7�
Signature of Land Appier
g
- -702.
Date
DENR FORM MFLSF (12/2006)
Acres Utilized: 10.6
Field #: M5
WQ Permit #: WQ0001953
Annual Dry Tons Applied: 2.2660
Land Owner: John McFadden
Cation Exchange Capacity (non 503):
Predominant Soil Series: CaB2
John McFadden.
0
L
0.
0
z
0.
0
0
N
z
a
cR
C
0
co)
Name of Crop Type
Receiving Residual
Application
Crop 2
ILime Applied I
ca
v
0
0
Date
CD
N
0.
O
U
U
ti
[i
PAN Applied
( Ibs/acre)
N
0
o
U
Q
z
O
O
o
o
O
O
0
0
O
O
0
0
0
O
0
0
0
O
0
0
O
O
0
0
O
O
0
0
O
0
0
0
0
0
0
0
O
0
0
o
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0
0
c
O
0
0
o
0
�,y
'-"
O
o
U
N
a'
O
0
0
C
O
0
0
O
O
0
0
O
O
0
0
O
O
0
0
O
O
0
0
O
O
0
0
O
O
0
0
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O
0
0
O
0
0
0
O
0
0
0
6
0,
L 0)
• .1)..)
Z .....
E
CD
c::,ci.
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
Ij Cd I Cu I Cr Pb H Mo Ni Se Zn P
M
rn
M
0.134
25.642
N
2498
Ammonia
a,
Nitrogen E
000c
_
M
o
o
O
un
N
O
"0
N
O
rn
00
z $'
a
E-- E
0
oo
0
N
N
o
o
0000
c--
cti
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co
r.f
`r
M
Mineralization
Rate***
M
o
0.002 0.027
-
0
o
<
z
Volatilization
Rate**
v.,
O
Application
Method*
N
0
d
0
o
'-
v
O. i .Cc
O
0
0
0
N
O
N
N
Z
✓1 U Q 3 2
'O
40
o
O
M
r
_•
N
0
00
N
en
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
M
0
0
CD
d
_
C.
0
0.05 J
.o
0
0
f^
1' U
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F 'O . c
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Q 0
-
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0
CD
O
0
0
CD
O
0
0
CD
O
0
0
0.000 I
CD
O
O
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CD
O
O
O
CD
O
O
O
0
O
co
C
0.000
0
O
O
O
0.000
in—'0
Q
_
0
O^
0
r-
0
1 36
.-
Volume applied
o : (enter one) Solids/
Liquid Solids
0
Cu. Yds I Gallons
00
0
Annual�lbs/acre
Prior Years Cumulative Ibs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop
143000 I
I 143000
0
4-2020
TOTALS:
eu c
°
• 7...O O
• Ci •p
• S. ,
I.a,
c
CO • O y
.0 , . i tL
e0
L U a a'
O — p R 4. v
ae ea
C O CC
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ca
ea ae e e c
O R "O
a) y R
z — 0 c W
tic v On c
R
R
3
0
L •• U 1ea
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, = H >
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R 0 R?
O ar Ce ' 7
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�c N
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i:. ._ 7.. �' ..�
CO �, c u a:
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u ~ 0
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on
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1)
ignature of Land Applier
U
DENR FORM FSF (12/2006)
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Spindale
WWTP Name: Town of Spindale WWTP
WQ Permit Number: WQ0001953
NPDES Number: NC0020664
Monitoring Period: From
1 / 1 /2020
To 12/31/2020
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) 0
Alt B (Alk Treatment)❑
Alt. C (Prior Testing)i
A1t.D (No Prior Test) ®
Process to Further Reduce Pathogengs L:
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Li
Heat Drying 0
Heat Treatment C]
Thermophilic
Beta Ray 0
Gamma Ray 0
Pasteurization
Class B:
Alt. (1) Fecal Density Ltd
Alt. (2) Process to Significantly Reduce Pathogens LJ
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Li
Air Drying 0
Composting 0
Aerobic Digestion L.J.
Anaerobic Digestion 10
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
f o
NumberFrequency
Excee-
dences
Analysis of Anal
y
Sample
Type
Analytical
Tech -
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
7692
8195
8696
MPN/g
0
7
grab
sm9221
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) Q
Alt. 4 (Spec. 02 uptake)
10
Alt. 5 (14-Day Aerobic)
El
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) lJ
Alt. 8 (Drying - Unstable)
ij
Alt. 9 (Injection)
0
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed
0
CERTIFICATION STATEMENT (please check the appropriate statement)
I "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
Li "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
6,7 o e.„, or c. L Dennis Key US Biosolids, Inc.
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer*
/7 1
Date Si nafure of Land Applier if applicable) Date
g PP ( PP )
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
Waypoint.
ANALYTICAL
46381
Southern Soil Builders
Dennis Key
958 Hoots Road
Roaring River , NC 28669
Project Spindale
Information :
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 'Fax 804-271-6446
www.waypointanalyticai.com
Report Number : 20-155-0004 REPORT Of ANALYSIS
Lab No: 72556
Sample ID : Spindale
Report Date: 06/11/2020
Received : 06/03/2020
pa v« tn` G°o"fr
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 6/ 1 / 2020 10:00
Test Results
Units MOL DF Date / Time By Analytical
Analyzed Method
Moisture
99.6 0/0 0.010 1 06/05/20 16:47 FMM 5M-2540G
Test Results
Units MOL DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
Nitrate+Nitrite-N
Organic N
pH
Total Solids
Total Kjeldahl Nitrogen
Phosphorus
Aluminum
Arsenic
Calcium
Cadmium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
31800 mg/Kg - dry
1700 mg/Kg - dry
97000 mg/Kg - dry
6.3 s.u.
0.380 %
129000 mg/Kg - dry
9330 mg/Kg - dry
6230 mg/Kg - dry
25 mg/Kg - dry
<12500 nig/Kg - dry
<25.0 mg/Kg - dry
<62.5 mg/Kg - dry
131 mg/Kg - dry
9730 mg/Kg - dry
<75.0 mg/,Kg - dry
1700 mg/Kg - dry
255 mg/Kg - dry
6250 1 06/10/20 14:00 JPJ SM-4500-NH3C
1210 1 06/09/20 15:40 MD 4500NO3F-2011
62500 1 06/10/20 10:00 CALCULATION
1 06/09/20 05:20 3SL 9045D
0.010 1 06/05/20 16:47 FMM SM-2540G
62500 1 06/10/20 10:00 JPJ ;M-4500-NH3C-TO
1250 1 06/09/20 22:09 KKM 60100
1250 1 06/09/20 22:09 KKM 60100
125 1 06/09/20 22:09 KKM 6010D
12500 1 06/09/20 22:09 KKM 6010D
25.0 1 06/09/20 22:09 KKM 6010D
62.5 t 06/09/20 22:09 KKM 60100
125 1 06/09/20 22:09 KKM 6010D
2500 1 06/09/20 22:09 KKM 6010D
75.0 1 06/09/20 22:09 KKM 6010D
1250 1 06/09/20 22:09 KKM 6010D
125 1 06/09/20 22:09 KKM 60100
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 3 cf 6
Waypoint
ANALYTICAL
46381
Southern Soil Builders
Dennis Key
958 Hoots Road
Roaring River , NC 28669
Project Spindale
Information
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical. com
Report Number : 20-155-0004 REPORT Of ANALYSIS
Lab No : 72556
Sample ID : Spindale
Report Date : 06/11/2020
Received : 06/03/2020
Pam« (tic 0°7-
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 6/1/2020 10:00
Test Results Units MOL LW Date / Time By Analytical
Analyzed Method
Mercury <3.83 mg/Kg - dry 3.83 1 06/09/20 11:59 DDB SW-7471B
Molybdenum <62.5 mg/Kg - dry 62.5 1 06/09/20 22:09 KKM 60100
Nickel <62.5 mg/Kg - dry 62.5 1 06/09/20 22:09 KKM 6010D
Potassium 6250 mg/Kg - dry 2500 1 06/09/20 22:09 KKM 6010D
Selenium 12 mg/Kg - dry 125 1 06/09/20 22:09 KKM 6010D
Sodium 23500 mg/Kg - dry 6250 1 06/09/20 22:09 KKM 6010D
Zinc <313 mg/Kg - dry 313 1 06/09/20 22:09 KKM 6010D
Sulfur 2950 mg/Kg - dry 2500 1 06/09/20 22:09 KKM 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 4 of 6
SAR
Sodium Absorption Ratio
Na : Sodium (Mg/L) Equivalent weight: 23
Ca : Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight: 12
Na(Mg/L) Ca(Mg/L) Mg(Mq/L)
89.3
47.5
6.46
Na_(M E.)
Ca...(M E).
Mg(ME)
3.882609
2.375
0.538333
Milli Equivalent = Mg/L / Equivalent weight
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
(From Mg/L entered above)
SAR = 3.216944
SAR= 3.296102
Na (ME)
Ca (ME)
Mg (ME)
3.9
2.3
0.5
(From ME entered below)
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Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 03/24/2020
Reported: 04/30/2020
For: Spindale
Comments:
Sample Number Parameter Sample ID Result
Unit Method Analyzed Analyst
200324-25-01 2 30 Day Benchscale Spindale <1
o/a
EPA62S.R-g210
03/24/2020 WC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 38
30 Day Bench Worksheet
WEEK 1
Sample ID # 200 j7_U . 25
Samples Total S lids
Volatile Solids
% Volatile Fraction
0.5000
1
- silL.P
-1
0
2
I
0•14'W2
3
- fAl
0. 1.0
0• `1-5/-1
Average:
0. 2 3
O. 11
0. `t 1(p
WEEK 2
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0 -
0.30
0.5351
2
1.06
G - 5LD
0.5333
3
0.1(0
O.4I
0-3R5
Average:
0- i q
0.1+2
0. c 3 (0 2
WEEK 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.42
0.22
0 523
2
O 3�S
O •1ci
0 • 5 6
3
0.20
0. 1 ?
0 - 6000
Average:
0.3.S
O - ► S
0 • F) G7 g
WEEK 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
I
0.3S
0. ►q
0•SL261
2
0-32
O.17
0-6 13
3
- ��
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Q•54 2g
Average:
()-% j
0. ' b
V, 53410
WEEK 5
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.27
0. 14
0.51'35
2
0.2ai
0.ILo
0•551/
3
G• L
G. 24
0. 5333
Average:
0.3
0 . 18
0.53 4-5
WEEK 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0-2.to
0•I5
O. I 4•,53�55
0,57(Pq
0- 55 1'7
2
O. ao
3
0.2C1
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Average:
0.2 7
0. 15
0. S'JS 7
0-Q.555-7
Van Kleeck Reduction: Initial % Vol. Frac. - Final % Vol. Frac. X 100 = %
Initial % Vol. Frac. — ( Initial % Vol. Frac. X Final % Vol. Frac.)
FINAL RESULT I
ism_Relinquished by: Y
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Relinquished by:
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Composite Sampling #1;
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Samples Transported On Ice
Initials:
gTaTRVII.I F
,i� Af'1ALYTICAL
122 Court Struet • P.O. Box 228
Statcsvillc, NC 28687
(7941872-4697
Chain of
Custody Record
r ,
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 38
.2ceAnal ical
www.pacelabs.com
ANALYTICAL RESULTS
Project: US. Bio. Spindale
Pace Project No: 92470995
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
(704)875-9092
Sample: 200324.25.01 Lab ID: 92470995001 Collected: 03/24/20 12:45 Received. 03/25/20 11:32 Matrix: Solid
Results reported on a 'dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Comments: • Samples requiring thermal preservation were received outside of recommended temperature limits of 0-6 degrees Celsius.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Chlorinated Herb. (GC) 8151A Analytical Method: EPA 8151A Preparation Method: 8151A
Leachate Method/Date: 1311: 03/28/20 15:06 Initial pH: 6.98; Final pH: 4.96
Pace National - Mt. Juliet
2,4,5-TP (Silvex) ND mg/L 0.00200 1 03/31/20 21:16 04/02/20 01:47 93-72-1
2,4-D ND mg/L 0.00200 1 03/31/20 21:16 04/02/20 01:47 94-75-7
Surrogates
2,4-DCAA (S) 89 8 % 14.0-158 1 03/31/20 21:16 04/02/20 01:47 19719-28-9
8081 TCLP Pesticides RVE Analytical Method: EPA 8081E Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 03/26/20 16:12
Pace Analytical Services - Charlotte
gamma-BHC (Lindane) ND ug/L 0.50 1 03/30/20 17:06 04/01/20 17:21 58-89-9
Chlordane (Technical) ND ug/L 3.0 1 03/30/20 17:06 04/01/20 17:21 57-74-9
Endrin ND ug/L 0.50 1 03/30/20 17:06 04/01/20 17:21 72-20-8
Heptachlor ND ug/L 0.50 1 03/30/20 17:06 04/01/20 17:21 76-44-8
Heptachlor epoxide ND ug/L 0.50 1 03/30/20 17:06 04/01/20 17:21 1024-57-3
Methoxychlor ND ug/L 1000 1 03/30/20 17:06 04/01/20 17:21 72-43-5
Toxaphene ND ug/L 3.0 1 03/30/20 17:06 04/01/20 17:21 8001-35-2
Surrogates
Decachlorobiphenyl (S) 78 % 10-138 1 03/30/20 17:06 04/01/20 17:21 2051-24-3
Tetrachloro-m-xylene (S) 86 % 10-110 1 03/30/20 17:06 04/01/20 17:21 877-09-8
8082 TCLP PCBs RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311: 03/26/20 16:12
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016) ND ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 12674-11-2
PCB-1221 (Aroclor 1221) ND ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 11104-28-2
PCB-1232 (Aroclor 1232) ND ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 11141-16-5
PCB-1242 (Aroclor 1242) ND ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 53469-21-9
PCB-1248 (Aroclor 1248) ND ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 12672-29-6
PCB-1254 (Aroclor 1254) ND ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 11097-69-1
PCB-1260 (Aroclor 1260) ND ug/L 1000 1 03/30/20 17:41 04/01/20 00:25 11096-82-5
Surrogates
Decachlorobiphenyl (S) 91 % 10-132 1 03/30/20 17:41 04/01/2000:25 2051-24-3
6010 MET ICP, TCLP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 04/05/20 1629 Initial pH: 7.79; Final pH: 4.5
Pace Analytical Services - Asheville
Arsenic ND mg/L 0.050 1 04/06/20 12:15 04/07/20 02;52 7440-38-2
Barium ND mg/L 0.25 1 04/06/20 12:15 04/07/20 02:52 7440-39-3
Cadmium ND mg/L 0.0050 1 04/06/20 12:15 04/07/20 02:52 7440-43-9
Chromium ND mg/L 0.050 1 04/06/20 12:15 04/07/20 02:52 7440-47-3
Lead ND mg/L 0.025 1 04/06/20 12:15 04/07/20 02:52 7439-92-1
Selenium ND mg/L 0.10 1 04/06/20 12:15 04/07/20 02:52 7782-49-2
Silver ND mg/L 0.025 1 04/06/20 12:15 04/07/20 02:52 7440-22-4
Date: 04/07/2020 04:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services. LLC.
Page 5 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 15 of 38
-� -�aceAnal lcal
VI VA*. pinhbs.com
ANALYTICAL RESULTS
Project: US. Bio. Spindale
Pace Project No.. 92470995
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilte, NC 28078
(704)875-9092
Sample: 200324.25.01 Lab ID: 92470995001 Collected: 03/24/20 12:45 Received: 03/25/20 11:32 Matrix. Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Comments • Samples requiring thermal preservation were received outside of recommended temperature limits of 0-6 degrees Celsius.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7470 Mercury, TCLP
Mercury
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311. 04/05/20 1629 Initial pH: 7.79: Final pH: 4.5
Pace Analytical Services - Asheville
ND mg/L 0.00020 1 04/07/20 10:46 04/07/20 14:07 7439-97-6
8270E TCLP RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
1,4-Dichlorobenzene ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 106-46-7
2,4-Dinitrotoluene ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 121-14-2
Hexachloro-1,3-butadiene ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 87-68-3
Hexachlorobenzene ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 118-74-1
Hexachloroethane ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 67-72-1
2-Methylphenol(o-Cresol) ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 95-48-7
384-Methylphenol(m&p Cresol) ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 15831-10-4
Nitrobenzene ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 98-95-3
Pentachlorophenol ND ug/L 100 1 03/30/20 20:50 03/31/20 17:10 87-86-5
Pyridine ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 110-86-1
2,4,5-Trichlorophenol ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 95-95-4
2,4.6-Trichlorophenol ND ug/L 50.0 1 03/30/20 20:50 03/31/20 17:10 88-06-2
Surrogates
Nitrobenzene-d5 (S) 65 % 12-102 1 03/30/20 20:50 03/31/20 17:10 4165-60-0
2-Fluorobiphenyl (S) 58 % 13-107 1 03/30/20 20:50 03/31/20 17:10 321-60-8
Terphenyl-d14 (S) 80 % 21-132 1 03/30/20 20:50 03/31/20 17:10 1718-51-0
Phenol-d6 (S) 30 % 10-110 1 03/30/20 20:50 03/31/20 17:10 13127-88-3
2-Fluorophenol(S) 20 % 10-110 1 03/30/20 20:50 03/31/20 17:10 367-12-4
2,4,6-Tribromophenol (S) 33 % 27-108 1 03/30/20 20:50 03/31/20 17:10 118-79-6
8260D MSV TCLP Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
Benzene ND ug/L 100 20 04/04/20 08:20 71-43-2
2-8utanone (MEK) ND ug/L 200 20 04/04/20 0820 78-93-3
Carbon tetrachloride ND ug/L 100 20 04/04/20 0820 56-23-5
Chlorobenzene ND ug/L 100 20 04/04/20 08:20 108-90-7
Chloroform ND ug/L 100 20 04/04/20 08:20 67-66-3
1,4-Dichlorobenzene ND ug/L 100 20 04/04/20 08:20 106-46-7
1,2-Dichloroethane ND ug/L 100 20 04/04/20 08:20 107-06-2
1,1-Dichloroethene ND ug/L 100 20 04/04/20 08:20 75-35-4
Tetrachloroethene ND ug/L 100 20 04/04/20 08:20 127-18-4
Trichloroethene ND ug/L 100 20 04/04/20 08:20 79-01-6
Vinyl chloride ND ug/L 100 20 04/04/20 08:20 75-01-4
Surrogates
1,2-Dichloroethane-d4 (S) 99 % 70-130 20 04/04/20 08:20 17060-07-0
Toluene-48 (S) 105 % 67-135 20 04/04/20 08:20 2037-26-5
4-Bromofluorobenzene (S) 97 % 70-130 20 04/04/20 08:20 460-00-4
Date: 04/07/2020 04:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, LLC. Page 6 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 16 of 38
.2eAnalytical
www.parrdabs.com
ANALYTICAL RESULTS
Project: US. Bio. Spindale
Pace Project No. 92470995
Pace Analytical Services, LLC
9800 Kinney Ave. Suite 100
iunterswlle. NC 28078
(7041875-9092
Sample: 200324.25.01 Lab ID: 92470995001 Collected: 03/24/20 12:45 Received: 03/25/20 11:32 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Comments' • Samples requiring thermal preservation were received outside of recommended temperature limits of 0-6 degrees Celsius.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Pace Analytical Services - Charlotte
Percent Moisture 99.6 % 0.10 1 04/01/20 16:15
1010 Flashpoint,Closed Cup Analytical Method: EPA 1010A
Pace Analytical Services - Asheville
Flashpoint >200 deg F 70 0 1 04/06/20 15:09
9045 pH Soil Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C 7.3 Std. Units 0.10 1 04/06/20 14:04
9095 Paint Filter Liquid Test Analytical Method: EPA 9095E
Pace Analytical Services - Asheville
Free Liquids
Fail 1.0 1 03/27/20 18:40
733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Pace Analytical Services - Greensburg
Cyanide. Reactive ND mg/kg 248 1 03/30/20 15:18 03/30/20 15:50
734S Reactive Sulfide Analytical Method: SM 4500S2F-2011 Preparation Method: SW-846 7.3.4.2
Pace Analytical Services - Greensburg
Sulfide, Reactive ND mg/kg 2480 1 03/30/20 15:18 03/30/20 15:23
H3
Sample: 200324.25.01 Lab 10: 92470995002 Collected: 03/24/20 12:45 Received: 03/25/20 11:32 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8082 GCS PCB RVE Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
PCB-1016 (Aroclor 1016) ND ug/L 1.0 1 03/31/20 15:55 04/02/20 20:28 12674-11-2
PCB-1221 (Aroclor 1221) ND ug/L 1.0 1 03/31/20 15:55 04/02/20 20:28 11104-28-2
PCB-1232 (Aroclor 1232) ND ug/L 1.0 1 03/31/20 15:55 04/02/20 20:28 11141-16-5
PCB-1242 (Aroclor 1242) ND ug/L 1.0 1 03/31/20 15:55 04/02/20 2028 53469-21-9
PCB-1248 (Aroclor 1248) ND ug/L 1.0 1 03/31/20 15:55 04/02/20 20:28 12672-29-6
PCB-1254 (Aroclor 1254) ND ug/L 1.0 1 03/31/20 15:55 04/02/20 20:28 11097-69-1
PCB-1260 (Aroclor 1260) ND ug/L 1.0 1 03/31/20 15:55 04/02/20 20:28 11096-82-5
Surrogates
Decachlorobiphenyl(S) 64 % 10-130 1 03/31/20 15:55 04/02/20 20:28 2051-24-3
Date: 04/07/2020 04:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 28
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 17 of 38
Relinquished by: Time am, pm Date ____J__/, Holding times met:
Received by: Time am, pm Date / / _
—
Compliance work:
Composite Sampling #1;
Time begin am, pm Date / / Non-compliance work:
In
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[Customer
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Client:
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Address: Po Qox 19C
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Contact Person: 2ec is (, e Phone # 3 3 C '} I / gk vCfAXM --
PO M Requisitioned by:
--- (Time Date)
1
10
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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 6 of 38
Analytical Results
U.S. Biosolids Inc
958 Hoots Road
Roaring River, NC 28669
Receive Date: 03/24/2020
Reported: 03/26/2020
For: Spindale
Comments: GM 8,195 MPN/g
Sample Number Parameter Sample ID Result
Unit Method Analyzed Analyst
200324-26-01 Fecal Coliforms 1 8696 MPN/g
200324-26-01 Percent Solids 1 0.23 cyo
200324-26-02 Fecal Coliforms 2 8000 MPN/g
200324-26-02 Percent Solids 2 0.25
200324-26-03 Fecal Coliforms 3 8333 MPN/g
200324-26-03 Percent Solids 3 0.24 %
200324-26-04 Fecal Coliforms 4 8696 MPN/g
200324-26-04 Percent Solids 4 0.23 cyo
200324-26-05 Fecal Coliforms 5 8000 MPN/g
200324-26-05 Percent Solids 5 0.25 0/0
200324-26-06 Fecal Coliforms 6 8000 MPN/g
200324-26-06 Percent Solids 6 0.25 %
200324-26-07 Fecal Coliforms 7 7692 MPN/g
200324-26-07 Percent Solids 7 0.26
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
SM9221 CEi-2006
SM2540B-2011
SM9221 CE-2006
SM25406-2011
SM92210E-2006
SM2540B-201 1
SM9221 CE-2006
SM2540B-2011
SM9221 CE-2006
SM2540B-2011
SM92210E-2006
SM2540B -2011
SM9221 CE-2006
SM2540B-2011
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
03/25/2020 WC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4
Condition of Receipt
Sample Number 200324-26-01 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-02 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-03 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-04 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-05 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-06 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 200324-26-07 Temp on Arrival:
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4
STATFS1f1! t t-
M1ALYricAL
A- 122 court Street • PO. Box 228
Statesville, NC 28687
r (704) 872-4697
ti Chain of
Custody Record
w
_b Sampled by: Z
ZQTransported by:
-- Holding times met:
Compliance work:
Non-compliance work:
Samples Transported On Ice:
Initials:
`c
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Address: i3 o (3. , J 9
Rondo. NL
Contact Person: Zarrr i`c _._..... Phone # 23 c_
PO # Requisitioned by: (Time bete)
Time )r /f am,Gii Date 2 / 2 .
Time 14 l 5 am, ate
Time am, pm Date /_/
Time am, pm Date /_/
Lab Comments:
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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 4
FY21-SL020227
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Sampled County : Rutherford
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NCDA&CS Agronomic Division
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John McFadden Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one Ca% % CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-1 copper index
ESP exchangeable sodium percent
Fertilizer HM% percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K2O potash
for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be > 50. If they
Mg% % CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class
an excellent source; 175 to 250 Ib, per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn manganese
Mn-AI1 Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-Al2 Mn-availability index for crop 2
Mn-I manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-0 mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients In general, homeowners do not N nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find pH current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htmitisfind information that P-I phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.) P205 phosphate
S-I sulfur index
Test Results SS -I soluble salt index
W/V weight per volume
Zn-AI zinc availability index
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-I zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm