WQ0018525_Residual Annual Report 2021_20220208

Non-Discharge Branch Upload/Submittal Form �.
NORTH CAROLINA
EnWrvnmenfol Quoity
Version 2-Revised June 23,2020
Initial Review
Reviewer Thornburg,Nathaniel D
Is this submittal an application?(Excluding additional information.)*
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number(IR)* WQ0018525
Applicant/Permittee Barnes Environmental Waste and Hauling,Inc.
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office Wilmington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal,confirmation of receipt,and other correspondence.
............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Name* Martin Mabe
Email Address* Phone Number*
[e-mail] 3363121396
Project Information
Application/Document Type* New(Fee Required) Modification-Minor
Modification-Major(Fee Required) Renewal
Renewal with Major Modification(Fee GW-59, NDMR,NDMLR, NDAR-1,
Required) NDAR-2
Annual Report Residual Annual Report
Additional Information Change of Ownership
Other
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High-Rate Infiltration
Other Wastewater Reclaimed Water
Closed-Loop Recycle Residuals
Single-Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0018525
Has Current Existing permit number
Applicant/Permittee Address* PO Box 654,Newport,NC 28570
Facility Name* Barnes Environmental Class B Residuals Program
Please provide comments/notes on your current submittal below.
2021 Class B Annual Report for WQ0018525
At this time,paper copies are no longer required.If you have any questions about what is required,please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.*
(Application Form,Engineering Plans,Specifications,Calculations,Etc.)
Barnes Environmental 2021 Annual Report WQ0018525.pdf 26.83MB
Upload only 1 PDF document(less than 250 MB).Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be
accepted for pre-review until the fee(if required)has been received by the Non-
Discharge Branch.Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality(NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order(as specified by the application).
Mail payment to:
NCDEQ—Division of Water Resources
Attn:Non-Discharge Branch
1617 Mail Service Center
Raleigh,NC 27699-1617
Signature
CPrz W
Submission Date 2/8/2022

2021 ANNUAL REPORT
LAND APPLICATION PROGRAM
BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
PERMIT #WQ0018525
WMSS Project No. 15-02 Ph: 01
Prepared for:
Barnes Environmental Waste and Hauling, Inc.
Post Office Box 654
Newport,North Carolina 28570
Compiled by:
Willcox &Mabe Soil Solutions,PLLC
7231B Summerfield Road
Summerfield,North Carolina 27358
February 2022

willcox&mabe
SOIL SOLUTIONS
February 8,2022
NCDEQ-DWR Non-Discharge Compliance Unit
512 North Salisbury Street
9th Floor,Office#942X
Raleigh,North Carolina 27604
Attention: Non-Discharge Compliance Unit
Reference: 2021 ANNUAL REPORT FOR WQ0018525
Barnes Environmental Waste and Hauling,Inc.
WMSS,Inc.Project No. 15-02 Ph:01
Non-Discharge Compliance Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting all monitoring and reporting
requirements as specified in the above referenced permit on behalf of Barnes Environmental Waste
and Hauling, Inc. (Barnes Environmental Waste). WMSS compiled this report using data gathered
during the compliance year by Barnes Environmental Waste.
If there is any further information required or questions regarding this land application program
please do not hesitate to contact Mr. Steve Barnes,with Barnes Environmental Waste 252-241-5014
for further assistance.
Sincerely,
Willcox& Mabe Soil Solutions,PLLC
Martin Mabe
NC Land Application/Residuals Operator
#22753
Enclosure(s)
cc Barnes Environmental Waste
Shared\WMSS Projects12015115-02 Barnes EnvironmentaI2021 Annual Report12021 ANNUAL REPORT,doc
Willcox&Mahe Soil Solutions,PLLC 17231 B Summerfield Road 1 Summerfield,NC 27358/Rob 336.339.9128 or Martin
336.312.13961 www.willcoxmabesoil.com

TABLE OF CONTENTS
SECTION NO. TITLE
I Certification Form
II Residuals Analyses&Pathogen and Vector Attraction
III Application Summary and Field Loading Rate Reports
IV Soil Analysis

CERTIFICATION FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0018525 County; Carteret Year::. 2021
Facility Name(as shown on permit): Barnes Environmental Waste and Hauling,Inc.
Land Application Operator: Steven M.Barnes Phone: (252)247=0354 -
Land application of residuals as allowed by the permit.occu.rred during the past calendar year?
CI Yes ❑ No -If Na,skip Part A,and Part Band proceed to Part C: Also.,If residuals were.
generated but not land applied,please attach an explanation on how the residuals were handled.
Part A Residuals Application Summary:
Total nuniber.of application fields in the permit: 6
Total number of fields utilized for land application during the year: 5
Total.amount of dry torts.applied:d.uring the year.for all application sites:I 29:14:
Total number of acres utilized for land application during the year: 24.7
Part B-Annual Compliance Statement:
Facility was compliant during.calendar year 2021 with all conditions of.the land application permit f`
(including but not limited to itcrirs 1-13 below)issued by the Division of Water Quality. El Yes ❑ No
If no please,provide a written.description why the facility was.not compliant,the dates,and explain.corrective
action taken.
1) Only residuals approved for;this permit were applied to the permitted sites..
2) Soil pH was adjusted as specified.in.the permit.and.liine was applied(if needed)to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual'soils analysis were performed on each site receiving residuals during the past calendar year and three-(3)copies
of laboratory results are attached.
4) Annual TCLP analysis (if required)was performed and three(3)copies of certified laboratory results are.attached,
5) All other monitoring was performed.in accordande with the permit and reported during the year as required and three
(3)copies of certified laboratory results are attached.
6) The facility did not exceed any of the.Poliutant Concentration'Limits in 15A NCAC.02T.11.05(a)orthe Pollutant
Loading Rates in 15A NCAC 02T .1.105(b)(applicable to 40 CFR Part 503 regulated facilities). j
7) All general requirements in as specified in the-Land Application Permit were complied with(applicable to 40 CFR Part i
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T.1.I 11 were complied with(applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance.requirements-in the permit were complied with or, in the case Of a deviation, prior
authorization was received fi-om the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring'well or-explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on•each site receing residuals,.as
specified in the permit.
1.2) No runoff of residuals from the application sites outo..adjacent property or nearby surface waters has occurred,
13) All buffer requirements as specified on the perinit,were maintained during each application of residuals,
Part C-Certification:
"I certify,'under penalty of law,that the above.information is,to..the best of my knowledge and belief,true, accurate,
and complete.I am aware that there are significant penalties for submitting false information,including the
possibility of fines and imprisonment for knowing violations."
Steven M.Barnes, President - j A,-.ems
'Permittee Name and Title(type or print) Signature of Perriittee Date
Signature of Preparer* Date Signature of Land Applier .Date
(if different from Permittee) (if different front Permittee.and Preparer)
*Preparer is defined.in 40 CFR Part 503.9:(r):and .15A NCAC 02T.1102(26)
bENR`FORM.ACF(12/2nnm

RESIDUAL ANALYSES REPORTS AND
PATHOGEN AND VECTOR ATTRACTION REDUCTION

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form la the ear'esponeng!alma tiny.aneiysis.
Please note that your emit may contain eddbonal parameters to be 211aycte4 than those required to besummadzed on this tort.
Permit Number Wt10018525 Laboratory 1) Environment1;Inc.
Facility Name Barnes Envirenmenlal 2)Environmental.Chemists,Inc.
NPDES# See Below 3)
.WWTPName See Below
RESIDUAL ANALYSIS.DATA
NPDFSA W430004059 W00013676 W00005173 VI 16-17 14-19-13 Y1-14 13 M109003044 VI-05.13 YW00000863 VI-02-18
WWTP Name Atlantic Station Beacons Reach Cape Royal CC Sass Cedar Point Colony by5ea dunescape Eight 112 Marina_ Genesis Condos Hampton Suites
CompositedIGrab 0111421 01/07/21 11123121 11123121 11123121 01/26121 0311521 02/04221 01121121 _ 02/23121
Percent Solids 0.78 1.26 _ 1.07 1.78' 0.72' 1.56 0.50 _ 0.16 0.49 1.40
PARAMETERS(mglkg dty weight)
Arsenic 2.50 2.90 29.70 2260 59.30 250 2.50 4.90 2.60 2.50
Cadmium 0.74 1.00 29.70 22,60 59.30 1.10 0,59 0.96 1.30 :0.50
Copper 766.00 1274.00 199.00 '448.00 .375.00 217.00 560.00 738.00 564,00 986.00.
Lead 14.00 • 19.00 29,70 2260 59.30 10,00. 8:90 18.00 15_00 3.60.
Mercury 0.79 L 0.37 1.42 0.83 2,17 0.23 0.19 0:50. 0.27 027 -
Molybdenum 5.00 9.00 29.70 22$0 59.30 5.00 5.00 5.00 5:00 7.00
Nickel 14.00 1200 29,70' 2260 .59_30 11,00 _ 7.00 7.00 10.00 9.00
Selenium 5:00 5.00 29:70 22.50 59.30 5.00 5.00 5.00 5.00. 5.00
tine 1.341:00 7,181A0 619.00. 48400 903,00 1,57200 958.00 1,565:00 1;189:00 876.00
TIN _ 46.330.00 52,910.00- 18,600.00. •25.100.00 40,600.00 71;860;00 47,170_0 48,120.00 66;180.00: 42,230,00
Amtmonia+litragdm 100.10 •200.90 9.35 86200' 13.90 2,453.00 74'.97 57.88 866.30 247.30
Nitrate Mtrogen 8,92 440,70 3.440.00 3.42 '97200 3:97 6.00 33.93 _ 8.98 7.95
Total Phosphorus. _ 18,200:00 • 14,540.00 , 5,670,00 11,100.00 15,900.00 15.280.00. 14560.00, 16;790.00 9.608.00 12,150.00
RESIDUAL ANALYSIS DATA
NPDES it 111-27-17-1 W00019331 W00003067 W00018420 VI-06 76 W130902128 V1-16-13 W130000224' W00003437 W000001e6
WARP Name Hackers Point NC Aquarium Ocean Bay Villas Ocian Club Ocean Condos. Pebble Beach. Pine Knoll Point.Emerald Omens Court Sends Villa
•compdsked/Grab 02103121 10114/21 02111121 10114121 02125121 01/25/21 02/23121 01121121 11123)21, 03116121
Peters Sagas 0.59 1.24- 0.75 0.92 0:87 328. 1.39 1.97 . 6.76 0.79
PARAMETERS(mglkg'dry weight)
Arsenic 2.50 2:50. 2.50 2:50 2.50' 2.50 2.50- 2.50 _ 46:00 2_50
Cadmium 0.84 8.60 .1.20 0.79 v 0,96 0.88' 0.66. _ 0.93 46.00 0,83
Copper 486.00 361-00 298,00 31200 670.00- 420100 581.00 710.00 375.00 308.00
Lead. 28.00 33.00 20.00 10.00 18.00 13.00 10.00 74.00 46.00 910
Mercury 0.42 0:18 0.34 0,17 0.22 0,25 0.33 .0.67 2_08 0-28
Molybdenum .5.00 6.00 _ 5,00 5.00 5,00 5.00 5.00 5.00 46.00 .5.00 -I
Nickel -8.00 22,00 12,00, 9.00 1200 11.00 11.00 11.00 46.00 46.00 _
Selenium '5,00 5.00 5.00 5.00 5.00 5.00 5.00 .5.90 46.00 5.00
Zinc 1.624,00 853.00 v 1,063.00 1,69200 1.634.00 1,427_00 1,493,00 2,221.00 . 1,810.00 1,471.00
TKN 9,622.00 41.490.00 40,560.00 7,883.00' 46.220.00 74,000.00 51,130.00 54_060.00 44,900.00 31,000.00
Ammonle-Nitrogen 211,00 192-20 17420 720.50 786.10 6,326.00 527.20 420.10 13.30 63.65
Nitrate-Nitrogen _ 44.79 24.77 12,94 13.88 10.95 5.00 4.85 24.77 1,000,00 18,90
Total Phosphorus 21,110.00 27,410.00 12,200,00- 21,440.00 23,430.00 11,250,00 14,790,00 13240.00 14;800-.00 15,150.00
A7:14,0____, A" Eel,(L.C.,r--c.:>. fQ/ .///2-Z-
(SIGNATURE OF PREPARER) DATE
t certify,under penalty of.iaw,.thatihisrdoeument was prepared under my diirecllon orsupenrision in'aecardanee with a.system-designed
la assure quairfied personnel properlyr.gathered'and•evalu'ated'ihe infor mation.submittedd I aril aware that there are significant
penalties for Submitfing'faLse information,including.lhe possib2ity'ot fnes and Imprisonmenifor knowing violaioits.
Pagel:

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this Mann to the corresponding laboratory analysis.
Please note that your permit may contain add moat parameters to be onalyied than those r gored to be svmmmrzed on this tarts.
Permit Number WQ0018525 Laboratory 1) Envlrorunent 1,Inc.
Facility flame Barnes Environmental 2)Environmental Chemists.Inc.
NPDES# See Below 3)
WIMP Name See Below
RESIDUAL ANALYSIS DATA
NPDESIf I W00013027 Vt.03-17 W000071a] W00018992 VI.12-17 WQ0024756 V1-20.15
INWfP Name Sea isle plantation Sea Spray Sound of the Sea Scut winds Condos Summer Winds The Grove Whaler tan v
_ _
Co mp:she d/Grob. . 01121121 03116121 03109121 03/16/21 02123)21 04122121 10112/21
Percent Sends 1.34- 0.55 0.98 0.52 0.54 0.86 0;91
PARAIVIEfERS(mg/kg dry weight)
Arsenic 2.50 2.50 2.50 2.50 250 250 2.50
Cadmium 1.10 0.50 1.30 0.50 0,77 _ 0:50 .0.70
Copper 235.00 771.00 .834.00 729.00 '647:00 88.00 859.00
Lead 38_00 7.50 I 1i00 .t10 9.00 2.90 97
Mercury 0.20 0.25 .0.1'3 _ 0.72 0,23 0,08 0.35
Molybdenum 5.00 5;00 5.00 5,00 5.00 5.00 _ 6.00
Nickel 15.00 10.00 8.00 9.00 10,00 8.00 12.00
Selenium 5.00 5.00 5.00 5.00 5.00' 5.00 •5.00
Znc. 1;31Z00 818.00 1,344.00 1,324.00 1.490.00 690.00 4,068,00
TKN 53.970.00 34.970.00 53..190.00 35,330.00 56.150.00 56,790.00. 54,660.00
Ammonia-Nitrogen 1,233.00. 85.66 2,613.00 111.10 763.10 1,329.00 898.00
Nitrate-Wingert 9.98 3.98 4.99 1,218.00 768.10 7.00 20.91
Total Phosphorus 14.950.00 117.550.00 1 16,750.00 15,020.00 _ 14.440.00 1 13.880.00 23,150.00
pil-1:.,/----- -"i II/. 4,--'11,1-'`) C)2/7/2'Al
( NATt iRE OF PREPARER) DATE
I certify,under penalty of law.that this dacurnentues prepared under my ddrec0an.orsupervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there am significant
penalties for submitting false information.including the possibility of fines and Imprisonment for knowing violations.
Page 2

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 14,2021
Permit No.WQ0018525
Atlantic Station 0.78 %Solids
12.17 pH(taken from lime stabilization event)
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/KK x 0.002)
Nitrogen(TKN) 0.723 48,330.000 96.660
Phosphorus 0.263 18,200.000 36.400
Potassium 0.449 3,625.000 7.250
PAN(injected)* 0.255 2,546.820 5.094
PAN(surface)* 0.228 2,283.320 4.567
Ammonia Nitrogen 0.053 100.100 0.200
Calcium 3.558 43,268.000 86.536
Calcium Carbonate Eq. --- ---
Magnesium --- 3,200.000 6.400
Sodium --- 14,365.000 28.730
Sulfur ___ --- -_-
Nitrate N/Nitrite N --- 8.920 0.018
Barium --- --- --- SAR
Chloride --- --- --- 1.58
Iron --- --- --- Ceiling Concen.
Aluminum --- 4,283.00 8.566 (Mg/Kg)
Arsenic --- 2.50 0.005 75
Cadmium --- 0.74 0.001 85
Chromium --- 17.000 --- ---
Copper --- 766.00 1.532 4,300
Lead --- 14.00 0.028 840
Mercury --- _ 0.19 0.000 57
Molybdenum --- 5.00 0.010_ 75
Nickel --- 14.00 0.028 420
Selenium --- 5.00 0.010 100
Zinc --- 1,341.00 2.682 7,500
Environment 1,Incorporated 108A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

[grailI Obri t@rr« � [ftT©©ir © r
ing Wa,tar ID* 37715
' -.Naetawater IDs 16
114 OAKMONT DRIVE PHONE (25:1 i:'• .
GL C'\ENVILLE, N.C. 27858 FAX ( ?) r'
ID#: 108 A
%-ATLAN'TIC STATION (FORTIN)
k MR. DAN
FORTIN CONTRACT SERVICES DATE COLLECTED: 01/14/21
P.O. BOX 4188 1 DATE REPORTED : 02/03/21
EMERALD ISLE ,NC 28594
REVIEWED EY: ,'1/1i
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
Aluminum, (dry wt, basis), mg/kg 4283 01/29/21 LFJ . EPA200.7
EPA200,7
Arsenic (dry wt. basis), mg/kg <2.5 01/28/21 MTM '3113B-04
Calcium (dry' WI, basis), mg/kg 43268 01/29/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 0.74 02/02/21 ?'ITM 3113B-04
Copper (dry wt. basis), mg/kg 766 01/29/21 LFJ EPA200,7
Chromium, T,(dry wt. basls),mg/lcg 17 01/29/21 LET EPA200.7
Lead (dry weight basis), mg/kg 14 02/01/21 MTM 3113E-04
Magnesium (dry wt. basis), mg/kg 3200 0I/29/21 LFJ EPA200,7
Mercury (dry wt. basis), mg/kg 0.19 01/27/21 MTM EPA7471B
Nickel (dry wt, basis), mg/kg 14 01/29/21 LFJ EPA200.7
Potassium (dry wt. basis), mgllcg 3625 01/29/21 LFJ EPA200.7
Selenium (dry wt, basis), mg/kg <5,0 02/01/21 MTM 3113E-04
Sodium (dry wt, basis), mg/kg 14365 01/29/21 LFJ •EPA200.7
Zinc (dry wt, basis), mg/kg 1341 01/29/21 LFJ EPA200.7
Total Solids, % 0,78 01/14/21 KDS 2540G-11
TKN (dry wt.), mg/kg c 48330 01/22/21 TLH 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg a 100.1 01/27/21 DTL 350.1 R2-93
Phosphorus, T, (dry wt.), mg/kg c 18200 01/22/21 KES 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg a 8,92 01/27/21 KES 353,2 R2-93
Plant Available Nitrogen, mg/kg 14528 01/31/21 MAO
Molybdenum (dry wt. basis), mgfkg <5.0 01/29/21 LFJ EPA200.7
•
c uncertified data. DWR does not offer non-aqueous certification for this analytical procedure,

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 7,2021
Permit No.WQ0018525
Beacons Reach 1.26 %Solids
6.8 pH
r Parameter % Mg/Kg Dry Weight Pounds/Dry Ton 1
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 5.291 52,910.000 105.820
Phosphorus 1.454 I4,540.000 29.080
Potassium 0.326 3,264.000 6.528_
PAN(injected)* 1.645 16,454.330 32.909
PAN(surface)* 1.635 16,353.880 32.708
Ammonia Nitrogen 0.020 200.900 0.402
Calcium 4.808 48,084.000 96.168
Calcium Carbonate Eq. --- --- ---
Magnesium --- 3,328.000 6.656
Sodium --- 11,639.000 23.278
Sulfur --- --- ---
Nitrate N/Nitrite N --- 440.700 0.881
Barium --- --- --- _ SAR
Chloride --- --- --- 1.55
Iron --- --- --- Ceiling Concen.
Aluminum --- 3,038.00 _ 6.076 , (Mg/Kg)
Arsenic --- 2.90 0.006 75
Cadmium --- 1.000 0.002 85
Chromium --- 12.000
Copper --- 1,274.00 2.548 4,300
Lead --- 19.00 0.038 840
Mercury --- 0.37 0.001 57
Molybdenum --- 9.00 0.018 75
Nickel --- 12.00 0.024 420
Selenium --- 5.00 0.010 100
Zinc --- 1,181.00 2.362 7,500
Environment 1 14 554A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

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114 OAMCI-NT 17F;IVE PHON 252)756 62.08
..GREt"NVII-i E,N,C7..858 :. . - .. .- .. , ...`: ..- ..,.. FAX(252)_75C..0638
IDit: 554 A
BEACON'S REACH I/POND (HYDROTECII)
ATTN: DOLT O'1dARA
R'(DROTECH DATE COLLECTED: 01/07/21
P,O, BOX 4602 DATE REPORTED 02/02/21
EMERALD ISLE ,NC 28594
I
REVIEWED BY: A.---
Sludge Analysis Mclhod
PARAMETERS Sample Date Analyst. Code
PH (not to be used for reporting) 6,3 01/07/21 TMR 4500HB-11
Aluminum, (dry Wt. basis), mg/kg 3038 01/14/21 .LFJ EPA200,7
Arsenic (dry wt, basis), img/kg 2.9 01/14/21 MTM 311313-0.4
Calcium (dry wt, basis), mg/kg 46084 01/14/21 LFJ EPA200.7
Cadmium (dry Wt. basis), nig/kg 1,0 01/13/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 1274 01/14/21 . LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 12 01/14/21 LTJ EPA200.7
Lead (dry weight basis), mg/kg 19 02/01/21 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 3328. 01/14/21 LEI EPA200.7
Mercury (dry Wt. basis), mg/kg 0.37 01/27/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 12 01/14/21 LFJ EPA200.7
Potassium (dry wt, basis), mg/kg 3264 01/14/2I LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 01/2.7/21 MTM 3I13B-04
Sodium (dry wt. basis), mg/kg 11639 01/14/21 LFJ EPA200,7
Zinc (dry wt, basis), mg/kg 1.181 01/14/21. LW EPA200.7
Total Solids, % 1.26 01/08/21 JMS 2540G-11
TKN (dry wt.), mg/lcg c 52910 01/12/21 TLH 351.2 R2-93
Ammonia Nitrogen (dry wt.),nig/kg c 200.9 01/14/21 ICES 350.1 R2-93
Phosphorus, T. (dry :vt.), mg/Icg c 14540 01/22/21 ICS 365.4-74
Nitrate-Nilritc (dry wt.), mg/kg c 440.7 01/13/21 TLH 353,2..R2-93
Molybdenum (dry wt. basis), mg/leg 9 01/14/21 LFJ EPA200:1
a Unoartilied data.. DWR doom not otl:at non-aquad'uo aortilioation f.or this analyi•lonl prooeduse:
!`I

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: November 23,2021
Permit No.WQ0018525
Cape Royal Dolphin 1.07 %Solids
7.31 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(°/A x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 1.860 18,600.000 37.200
Phosphorus 0.567 5,670.000 11.340
Potassium 0.290 2,900.000_ 5.800_
PAN(injected)* 0.903 9,026.545 18.053
PAN(surface)* 0.902 9,021.870 18.044
Ammonia Nitrogen 0.001 9.350 0.019
Calcium 0.729 7,290.000 14.580
Calcium Carbonate Eq. --- ---
Magnesium --- 1,486.000 2.972
Sodium --- 24,100.000 48.200
Sulfur ---
Nitrate N/Nitrite N --- 3,440.000 6.880 _
Barium --- --- --- SAR
Chloride --- --- --- 6.94
Iron --- --- --- Ceiling Concen.
Aluminum --- 2,470.00 4.940 (Mg/Kg)
Arsenic --- 29.70 0.059 75
Cadmium --- 29.70 0.059 85
Chromium --- 29.700 --- ---
Copper --- 199.00 0.398 4,300
Lead --- _ 29.70 0.059 840
Mercury --- 1.420 0.003 57
Molybdenum --- 29.70 0.059 75
Nickel --- _ 29.70 0.059 420
Selenium --- 29.70 0.059 100
Zinc --- 619.00 1.238 7,500
Envirochem# 2021-20844
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

� -� x xr Environmental Chemists, Inc.
Fax
nv . 'o +'.[let G602 Windmill Way,Wilmington,NC 28405 910.392.0223 Lab 0 910.392.4424 Fax
710
73.5702
.` a l.' " '" 255-A Wilmington Highway,Jacksonville,enke°,NC NC 28540 ►4910.347.5843�Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS [e-mail]
environmentalchernists.cojn
Fortin Contract Services Date of Report: Dec 27, 2021
Post Office Box 4188 Customer PO#:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: • ' e°,,
Pro - ID: Cape Royal Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-52278 Site:Sludge 11/23/2021 9:35 AM Solid/Sludge Kevin Stanley
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200.7,Rev.4.4,1004 2470 mg/kg 12/06/2021
Arsenic EPA 200.7,Rev.4.4,1904 <29.7 mg/kg 12/06/2021
Cadmium EPA 200.7,Rev.4.4,1994 <29.7 mg/kg 12/06/2021
Calcium EPA 200,7,Rev.4.4,1994 7290 mg/kg 12/06/2021
Chromium EPA 200.7,Rev.4.4.1994 <29.7 mg/kg 12/06/2021
Copper EPA 200.7,Rev.4.4,1994 199 mg/kg 12/06/2021
Lead EPA 200.7,Rev.4.4,1994 <29.7 mg/kg 12/06/2021
Magnesium EPA200.7,Rev.4.4,1994 <1486 mg/kg 12/06/2021
Molybdenum EPA 200.7,REV.4.4,1994 <29,7 mg/kg 12/06/2021
Nickel EPA200.7,Rev.4.4.1904 <29.7 mg/kg 12/06/2021
Potassium EPA 200.7,Rev.4.4,1994 2900 mg/kg 12/06/2021
Selenium EPA 200.7,Rev.4.4,1994 <29.7 mg/kg 12/06/2021
Sodium EPA 200.7,Rev.4.4,1994 24100 mg/kg 12/06/2021
Zinc EPA 200.7,Rev.4.4,1994 619 mg/kg 12/06/2021
Nitrate+Nltrite-Nitrogen EPA 253,2 3440 mg/kg 11/29/2021
Total Solids(%) SM 2540 B 1.07% 11/29/2021
Ammonia Nitrogen SM 4500 NI 3 C-2011 <9.35 mg/kg 11/29/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011 18600 mg/kg 11/30/2021
Total Phosphorus SM 4500 P F-2011 5670 mg/kg 12/03/2021
pH SW 645 Method 9045D 7.31 units 12/22/2021
Result estimated, Analyzed out of 15 minutes hold time,
Mercury SW.648 7471 B <1.42 mg/kg 11/30/2021
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
kiati,Me‘ - '
Reviewed by:
PunnN i•• 7M179-71WA „---. _,.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: November 23,2021
Permit No. WQ0018525
CC Sass 1.78 %Solids
7.09 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 2.510 25,100.000 50.200
Phosphorus 1.110 11,100.000 22.200
Potassium 0.556 5,560.000 11.120
PAN(injected)* _ 0.814 8,136.820 16.274
PAN(surface)* 0.771 7,705.820 15.412
Ammonia Nitrogen 0.086 862.000 I.724
Calcium 1.250 12,500.000 25.000
Calcium Carbonate Eq. --- --- ---
Magnesium --- 3,130.000 6.260
Sodium --- 9,550.000 19.100
Sulfur --- _-- ___
Nitrate N/Nitrite N --- 3.420 0.007
Barium _ --- --- --- _ SAR
Chloride --- --- --- 2.63
Iron --- --- --- Ceiling Concen.
Aluminum - 1,040.00 2.080 (Mg/Kg)
Arsenic --- 22.60 0.045 75
Cadmium --- 22.60 0.045 85
Chromium --- 22.600 0.045 ---
Copper --- 448.00 0.896 4,300
Lead --- 22.60 0.045 840
Mercury --- 0.831 0.002 57
Molybdenum --- 22.60 0.045 75
Nickel --- 22.60 0.045 420
Selenium --- 22.60 0.045 100
Zinc --- 484.00 0.968 7,500
Envirochem# 2021-20847
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits arc listed as detection limits
for calculation purposes.

4,,,,,,,y. 2 '?r? i-:,,_ Environmental Chemists, Inc®
�.... p,
ei 1 `oe 6602 Windmill Way,Wilmington,NC 28405 4 910.392.0223 Lab 4 910.392.4424 Fax
.=- :. 710 Bowsertown Road,Mantea,NC 27954..a 252.473,5702 Lab/Fax
. 3 !l 255-A Wilmington Highway,Jacksonville,NC 28540 * 910,347,5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info c+environnientalcheinisis,corn
Fortin Contract Services Date of Report: Dec 27, 2021
Post Office Box 4186 Customer PO#:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2091-7 847
Pr t ID: CCSASS Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-52286 Site:Sludge 11/23/2021 9:55 AM Solid/Sludge Kevin Stanley
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200.7,Rev.4.4,1994 1040 mg/kg 12/05/2021
Arsenic EPA 20U,7,Rev.4.4,1994 <22.6 mg/kg 12/06/2021
Cadmium EPA 200.7,Rev,4.4,1994 <22.6 mg/kg 12/06/2021
Calcium EPA 200.7,Rev,4.4,1904 12500 mg/kg 12/06/2021
Chromium EPA200.7.Rev.4.4,1994 <22.6 mg/kg 12/06/2021
Copper EPA 200,7,Rev.4.4,1094 448 mg/kg 12/06/2021
Lead EPA 200.7,Rev.9.4,1094 <22.6 mg/kg 12/06/2021
Magnesium EPA 200.7,Rev.4.4.1004 3130 mg/kg 12/06/2021
Molybdenum EPA 200.7,Rev.4.4,1994 <22.6 mg/kg 12/06/2021
Nickel EPA200.7.Rev.4.4,1994 <22.6 mg/kg 12/06/2021
Potassium EPA 200.7,Rev,4.4,1904 5560 mg/kg 12/06/2021
Selenium EPA 200.7,Rev.4,4,1994 <22.6 mg/kg 12/06/2021
Sodium EPA 200.7,Rev.4.4,1999 9550.mg/kg 12/06/2021
Zinc EPA 200.7,Rev.4A,1994 484 mg/kg 12/06/2021
Nitrate+Nitrite-Nitrogen EPA 353,2 3.42 mg/kg 11/29/2021
Total Solids(%) SM 2540 s 1.78% 11/29/2021
Ammonia Nitrogen SM 4500 NH3 C-2011 862 mg/kg 11/29/2021
Total KJeldahl Nitrogen (TKN) SM 4500 Nor S-2011 25100 mg/kg 11/30/2021
Total Phosphorus SM 4500 P F•2011 11100 mg/kg 12/03/2021
pH SW ads Method 9045D 7.09 units 12/22/2021
Result estimated..Analyzed out of 16 minutes hold time.
Mercury SW-a487471 a <0.831 mg/kg 11/30/2021
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: I'IOAAdJ +' J
Report 8:: 2021-20847 Plana 1 n11

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: November 23,2021
Permit No.WQ0018525
Cedar Point 0.72 %Solids
7.14 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(% x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 4.060 40,600.000 81.200
Phosphorus _ 1.590 15,900.000 31.800
Potassium 0.592 5,920.000 11.840
PAN(injected)* 1.316 13,161.730 26.323
PAN(surface)* 1.315 13,154.780 26.310
Ammonia Nitrogen 0.001 13.900 0.028
Calcium 2.190 21,900.000 43.800
Calcium Carbonate Eq. --- --- ---
Magnesium --- - 3,500.000 7.000
Sodium --- 20,000.000 40.000
Sulfur --- --- --_
Nitrate N/Nitrite N --- 972.000 1.944
Barium --- --- --- SAR
Chloride --- --- --- 2.80
Iron --- --- --- Ceiling Concen.
Aluminum --- 4,810.00 9.620 (Mg/Kg)
Arsenic --- 59.30 0.119 75
Cadmium --- 59.30 0.119. 85
Chromium --- 59.300 --- ---
Copper --- 375.00 0.750 4,300
Lead --- 59.30 0.119 840
Mercury --- 2.17 0.004 _ 57
Molybdenum --- 59.30 0.119 75
Nickel --- 59.30 0.119 420
Selenium --- 59.30 - 0.119 100
Zinc --- 903.00 1.806 7,500
1 Envirochem# 2021-20843
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

.- fWI -, Environmental Chemists, Inc.
-- a 'VsirQC -01/ M 6602 Windmill Way,Wilmington,NC 28405 : 910,392.0223 Lab • 910.392.4424 Fax
5_ a %, 0 t 710 8owsertown Road,Mantel),NC 27954 a 252.473.5702 Lab/Fax
—, 255-A Wilmington Highway,Jacksonville,NC 28540 0.910.347,5843 Lab/Fax I
i
ANALYTICAL,&CONSULTING CHEMISTS [e-mail]
environmentalchernists,cam
Fortin Contract Services Date of Report: Dec 27, 2021
Post Office Box 4188 Customer PO#:
Emerald Isle NC 28594 Customer ID: 08100061
Attention: Dan Fortin Report#: 2021-20843
Pro) Cedar Point Sludge
Lab ID Sample ID: Collect Date/Time Matt x
21-52277 Site:Sludge 11/23/2021 8:40 AM SolidlSiudge Kevin Stanley
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA200.7.Rev.4.4,1404 4810 mg/kg 12/06/2021
Arsenio EPA 200.7,Rev.4.4,1994 <59.3 mg/kg 12/06/2021
Cadmium EPA200,7.Rev,4.4,1094 <59.3 mg/kg 12/06/2021
Calcium EPA 200.7.Rev.4.4,1994 21900mg/kg 12/06/2021
Chromium EPA 200.7,Rev.4.4,1904 <59.3 mg/kg 12/06/2021
Copper EPA 200.7,Rev.4.4,1994 375 mg/kg 12106/2021
Lead EPA 200.7,Rev.4.4,1094 <59.3 mg/kg 12/06/2021
Magnesium EPA 200,7.Rev.4.4,1094 3500 mg/kg 12/06/2021
Molybdenum EPA 200.7,Rev.4.4,1904 <59.3 mg/kg 12/06/2021
Nickel EPA 2011.7,Rev.4.4,1094 <59.3 mg/kg 12/06/2021
Potassium EPA 200.7,Rev,4.4,1904 5920 mg/kg 12/06/2021
Selenium EPA 200.7.Rev.4.4,4984 <59,3 mg/kg 12/06/2021
Sodium EPA 200.7,Rev,4.4,1904 20000 mg/kg 12/06/2021
Zinc EPA 200.7,Rev.4.4,1994 903 mg/kg 12/06/2021
Nitrate+Nitrite-Nitrogen EPA 35$.2 972 mg/kg 11/29/2021
Total Solids(%) SM 2540 s 0.72% 11/29/2021
Ammonia Nitrogen SM4500 N113C•2011 <13,9 mg/kg 11/29/2021
Total Kjeldahl Nitrogen (TKN) SM 4500 Norg 8.2011 40600 mg/kg 11/30/2021
Total Phosphorus SM 4600 P F•2011 15900 mg/kg 12/03/2021
pH SW 046 Method 9045D 7.14 Units 12/22/2021
Result estimated. Analyzed out of 15 minutes hold lime.
Mercury sw•64e 7471.8 <2.17 mg/kg 11/30/2021
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis,
Reviewed by: 0.
Report 11:: 2021-20843 Page i of 1

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 26,2021
Permit No.WQ0018525
Colony By The Sea 1.56 %Solids
12.13 pH(taken from lime stabilization event)
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 7.186 _ 71,860.000 143.720
Phosphorus 1.528 15,280.000 30.560
Potassium 0.535 5,351.000 10.702
PAN(injected)* 2.328 23,279.070 46.558
PAN(surface)* 2.205 22,052.570 44.105
Ammonia Nitrogen - 0.245 2,453.000 4.906
Calcium 2,502 25,018.000 50.036
Calcium Carbonate Eq. --- ---
Magnesium --- 5,599.000 11.198
Sodium --- 8,786.000 17.572
Sulfur _-_ --- ---
Nitrate N/Nitrite N --- 3.970 0.008
Barium --- --- --- SAR
Chloride --- --- --- 1.63
Iron --- --- --- Ceiling Concen.
Aluminum --- 3,594.00 7.188 (Mg/Kg)
Arsenic --- 2.50 0.005 75
Cadmium _ --- 1.10 0.002 85
Chromium --- 12.000 --- _--
Copper --- 217.00 0.434 _ 4,300
Lead _ --- I0.00 0.020 840
Mercury --- 0.23 0.000 57
Molybdenum --- 5.00 0.010 75
Nickel --- 11.00 0.022 420
Selenium --- 5.00 0.010_ 100
Zinc --- 1,572.00 3.144 7,500
Environment I# 616A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

lVi0DO[ UgA kg©52PgreA@
Drinking Water IDJ 37715
Wastewater ID 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.G. 27858 FAX [phone]
ID#: 616 A
COLONS( BY THE SEA (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH DATE COLLECTED: 01/26/21
P.O. BOX 4602 DATE REPORTED : 02/23/21
EMERALD ISLE ,NC 28594
REVIEWED BY: ��—
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
Aluminum, (dry wt. basis), mg/kg 3594 02/09/21 LFJ EPA200.7
Arsenic (dry wt. basis), Ong/kg <2.5 02/10/21 MTM 311313-04
Calcium (dry wt. basis), mg/kg 25018 02/09/21 LIU EPA200.7
Cadmium (dry wt. basis), mg/kg 1.1 02/I2/21 MTM 311313-04
Copper (dry wt, basis), mg/kg 217 02/09/21 LFJ EPA200.7
Chromium, T.(dry wt, basis),mg/kg 12 02/09/21 LF.1 EPA200.7
Lead (dry weight basis), mg/kg 10 02/I1/21 MTM 3I13B-04
Magnesium (dry wt. basis), mg/kg 5599 02/09/21 LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.23 02/11/21 MTM EPA747113
Nickel (dry wt. basis), mg/kg 11 02/09/2I LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 5351 02/09/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 02/I0/2I MTM 3113B-04
Sodium (dry wt. basis), mg/kg 8786 02/09/21 LFJ EPA200.7
Zinc (dry wt, basis), mg/kg 1572 02/09/21 LFJ EPA200.7
Total Solids, % 1,56 01/28/21 TMR 2540G-11
TKN (dry wt.), mg/kg c 71860 02/05/21 TLH 351.2 R2-93
Ammonia Nitrogen (dry wt.),mgllcg c 2453 02/01/21 TLH 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 15280 02/05/21 KES 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 3.97 02/02/21 DTL 353.2 R2-93
Plant Available Nitrogen, mg/kg 8171 02/09/21 MAO
Molybdenum (dry wt. basis), mg/kg <5.0 02/09/21 LFJ EPA200.7
c Uncertified data. DWR does not offer non-aqueous certification for this analytical procedure.

Environment 1,Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085. 114 Oakmont Dr. Page 1 of I
Greenville.NC 27858
environmentlinc.com • DISINFECTION CHLORINENEUTR4LLZEbA7CQLLECTION
Phone[phone] •Fax[phone]
DCHLORINE - - _
CLJENT: 616 A Week:8
UV - pH CHECK(LAB)
COLONY BY THE SEA (HYDROTECH) NONE P P P P P P N CONTAINER TYPE,P/G
ATTN:DON O'MARA _ _
HYDROTECH
P.O.BOX 4602 rj A A A A A A CHEMICALPRESERVATION
EMERALD ISLE NC 28594 `a r -
'o 1- A-NONE D-NAOH
(7aZ)725-2319 c3 c 3 Cl) o co
°7 C B HNO3 E HCL
o0 �o z o z
51.- w `h z C-H22S0, F-ZINC ACETATE/NAOH
s 1- o8 o Fw 6 s d' i z < G-NATHIOSULFATE
SAMPLE LOCATION DATE TIME a o � Q o s E < o� z a <r
FN
Sludge Sample //2\b/ 4 . ' Is .�..- - " . - CLASSIFICATION:
_
LI WASTEWATER(NPDES)
- - - Li DRINKING WATER
j DWR/GW
EJSOUD WASTE SECTION
CHAIN OF CUSTODY(SEAL)MAINTAINED
_ DURING SHIPMENT/DELIVERY
N
SAMPLES COLLECTED BY:
- __ _ (Please P t)
1- - _ _ - _ C C' Qiiik/A17-
1 SAMPLES RECEIVED IN LABAT ,"i 'C
RELINQUISHED BY(SI AMPLER) DATE/TIME RE IVED •
BY(SI ) DATE/TIME COMMENTS:
r ' `. � r" '/ 19 =o5
RELINQUISHED BY(SIG.) DATEITl E RECEIVED BY(SIG.) DATE/liME
_ 1 - . t
RELINQUISHED BY(SIG.) DATEJfIME RECEIVED BY(51G.) DATE/TIME
� •
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a C"for composite sample or a"G"far
FORM rs _ Grab sample in the blocks above for each parameter requested. N2 388800

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 15,2021
Permit No.WQ0018525
Dunescape 0.50 %Solids
7.3 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 4.717 47,170.000 94.340
Phosphorus 1.466 14,660.000 29.320
Potassium 0.657 6,566.000 13.132
PAN(injected)* 1.421 14,209.479 28.419
PAN(surface)* 1.417 14,171.994 28.344
Ammonia Nitrogen 0.007 _ 74.970 0.I50
Calcium 3.692 36,915.000 73.830
Calcium Carbonate Eq. --- --- ---
Magnesium --- 4,884.000 9.768
Sodium --- 15,040.000 30.080
Sulfur --- --- --- -
Nitrate N/Nitrite N --- 6.000 0.012
Barium --- --- --- SAR
Chloride --- --- --- 1.38
Iron --- - --- --- Ceiling Concen.
Aluminum --- 1,898.00 3.796 (Mg/Kg)
Arsenic --- 2.50 0.005 _ 75
Cadmium --- 0.59 0.001 85
Chromium --- 7.000 --- ---
Copper --- 560.00 1.120_ 4,300
Lead --- 8.90 0.018 840
Mercury --- 0.19 _ 0.000 57
Molybdenum --- 5.00 0.010_ 75
Nickel --- 7.00 0.014 420
Selenium --- 5.00 0.010 100
Zinc --- 958.00 1.916 7,500
Environment l# 556 A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

Drinking Water ID, 17715
Wastewater ID! 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 556 A
DTJNESCAPE (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH DATE COLLECTED: 03/15/21 •
P.O. BOX 4602 DATE REPORTED : 04/08/21
EMERALD ISLE NC 28594
REVIEWED BY:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting) 7,3 03/16/21 DIJ 4500HB-11
Aluminum, (dry wt. basis), mg/kg 1898 04/01/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 04/05/21 MTM 31I3B-04
Calcium (dry wt, basis), mg/kg 36915 04/01/21 LFJ EPA200,7
Cadmium (dry wt. basis), mg/kg 0.59 04/01/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 560 04/01/21 LFJ EPA200.7
Chromium, T.(dry wl. basis),mg/kg 7 04/01/21 LFJ EPA200.7
Lead (dry weight basis), mg/kg 8.9 04/01/21 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 4884 04/01/21 LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.19 04/05/21 MTM EPA747I B
Nickel (dry wt. basis), mg/kg 7 04/01/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 6566 04/01/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 03/31/21 MTM 3113B-04
Sodium (dry Wt. basis), mg/kg 15040 04/01/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 958 04/01/21 LFJ EPA200.7
Total Solids, % 0.50 03/17/21 KDS 2540G-11
TKN (dry wt.), mg/kg c 47170 03/23/21 KES 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 74.97 03/24/21 DTL 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 14660 03/23/21 TLH 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 6.00 03/23/21 DTL 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg <5.0 04/01/21 LFJ EPA200.7
c Uncertified dote, DWR done not offer non-aqueous certification for thin analytical procedure.

•
Environment I,Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085. i 14 Oakmont Dr. Page 1 of 1
Greenville.NC 27858
environment 1 inc.eom DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone[phone]•Fax[phone]
CHLORINE _ . _ _- _
CLIENT: 556 A Week:8
UV _ - pH CHECK(LAB) _
DUNESCAPE(HYDROTECH) ,NONE P P P P P P P CONTAINER TYPE,PIG
ATTN:DON O'MARA .-. - _ . -
HYDROTECH
P.O.BOX 4602 A A A A A A A
CHEMICAL PRESERVATION
EMERALD ISLE NC 28594 -_ - - - - - - _
E o A-NONE D-NAOH
[phone] ,. .- "'
E'a m o z p 3 B HNO3 E-HCL
J 0 LliE Z E w C-H2SO4 F-ZINC ACETATE/NAOH
COLLECTION J¢ w - y o .
F F- = p cc G-NATHIOSULFATE
SAMPLE LOCATION DATE TIME Fo o r"'-- s o °' E" Q Z Q
5 a)j4'{h { �p'
c� �3-_Sludge Sample 7 2/ !r - _ _ CLASSIFICATION:
WASTEWATER(NPDES)
- - - _ ._ - - lij DRINKING WATER
DWR1GW
1] SOLID WASTE SECTION
CHAIN OF CUSTODY(SEAL)MAINTAINED
" - -- - DURING 'giIPMENT/DELIVERY
�J N
SAMPLES COLLECTED BY:
_ - (Please Print)
- — . bQn� OV 1 f�
SAMPLES RECEIVED IN LAB AT a,6
r _ 'C
RELNQUISHE (SIG. (SAMPLER) DATE[I1ME R EIVED BY(SIG.) DATE111ME COMMENTS
V— / 45:2tI/1P30 , 3/6/.21I -`..(o
RELINQ Et BY(SIG-I DATEIiiME RECEIVED BY(SIG.) DATETflME
1
RELINQUISHED BY(SIG.) DATE/TIME RECEIVED BY(SIG.) DATEIIIME .
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"C"for composite sample or a"G°for
FORM#5 Grab sample in the blocks above for each parameter requested. No 3 8 8 8 3 5

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 4,2021
Permit No.WQ0018525
Eight 1/2 Marina 0.16 %Solids
12.25 pH(taken from lime stabilization)
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(% x 10,000) (M I/Kg x 0.092)
Nitrogen(TKN) 2.438 48,120.000 96.240
Phosphorus 0.244 16,790.000 33.580
Potassium 0,349 6,345.000 12,690
PAN(injected)* 0.741 7,413.776 14.828
PAN(surface)* 0.737 7,365.886 14.732
Ammonia Nitrogen 0.010 57.880 0.116
Calcium 52,034.000 104.068
Calcium Carbonate Eq. --- --- ---
Magnesium --- 3,900.000 7.800
Sodium --- 34,493.000 68.986
Sulfur --- --- ---
Nitrate N I Nitrite N --- 33.930 0.068
Barium --- --- --- SAR
Chloride --- --- --- 1.57
Iron - --- --- _ Ceiling Concen.
Aluminum --- 3,212.00 6.424 (Mg/Kg)
Arsenic --- 4.90 0.010 75
Cadmium --, 0.98 0.002 85
Chromium --- 16.000 --- ---
Copper --- 738.00 1.476 4,300
Lead --- 18.00 0.036 840
Mercury --- 0.50 0.001 57
Molybdenum --- 5.00 0.010 75
Nickel --- 7.00 0.014 420
Selenium --- 5.00 0.010 100
Zinc --- 1,565.00 3.130 7,500
Environment I# I96A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

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'Cncinalum..(dt7 .wt bus14.1 irug/kg 9411 01..91.M KO( $1.11U'04
..... ,
Copper (dry wt basis , mg/kg 738 03/4121 vs gr400.11:
choilitoth !tory vt. fit4MOinigiltg. 16 03/05I4). LW' 016200+1
:bead's.(dry'•weight basis), mg/kg 'It 0/03/21 MTM 3101..04
Magne,iltury(dry.wt..b010., 1-1•015g, 3900 0196121. .11;te1: gPA26.0.1
Medory.(dry•wt basis), mg/kg :040 .02/2344- MTM tiiie7e1ti-
Mpi01. (dil.'wt.. linsfOi.mg/kg I. .03/05/21 14Y.41 IT,P420011
?otilsittor:Or'y'wt i'tio00,itiekg. .04. OVOSaL. 147., EP.A20.0..7
S.0.10.1)1m. opy•ill,. b.a0s)t. 11.000. 46..0 0310.3/21 .1$1.71Sf 3113113.:•04 •
Sodium (tb50:0t: tia0).. 00gikg. 3440 03/05/21 .TAN gPA24,0.7.
Zhi.c..(di7-ot. boli)i Oig./4. 1565 .0*06/21 LIP.1: tPA200.7
INSint-Solids, •%• •:0,16: 02/041 ittis •2$46 .;;41
Niplybilentitri .(dry w.t. bas10.,.mg/Itg .5;i) 95/0.14T TilvJ. :EPA200:7
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Code
Date Analyst
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BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 21,2021
Permit No.WQ0018525
Genesis Condos 0.49 % Solids
7.1 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 6.618 66,180.000 132.360
Phosphorus 0.961 9,608.000 19.216
Potassium 0.842 8,415.000 16.830
PAN(injected)* 2.047 20,469.390 40.939
PAN(surface)* 2.004 20,036.240 _ 40.072
Ammonia Nitrogen 0.087 866.300 1.733
Calcium _ 4.359 43,589.000 87.178
Calcium Carbonate Eq. --- ___ ---
Magnesium --- 6,273.000 12.546
Sodium --- 16,336.000 32.672_
Sulfur --- --_
Nitrate N/Nitrite N --- _ 8.980 0.018
Barium --- ___
--- SAR
Chloride --- --- --- 1.35
Iron --- --- --- Ceiling Concen.
Aluminum --- 2,784.00 5.568 (Mg/Kg)
Arsenic --- 2.60 0.005 75
Cadmium --- 1.30 0.003 85
Chromium --- _ 12.000 --- ---
Copper --- 564.00_ 1.128 4,300
Lead --- 15.00 0,030_ 840
Mercury --- 0.27 0.001 57
Molybdenum --- 5.00 0.010 75
Nickel --- 10.00 0.020 420
Selenium --- 5.00 0.010 100
Zinc --- I,189.00 2.378 7,500
Environment I # 68 C
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.U.(Not Detected)or<detection limits arc listed as detection limits
for calculation purposes.

Iii1g Ciricupcxi7Miot)
• • . .
• . Drinking' Nator 'I1)1'_ 37715,;.`
Wastewater IDi 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID1k: 6 8 C
GENESIS CONDO ASSO. (HYDROTECH)
DON O'MARA
HYDROTECH DATE COLLECTED: 01/26/21
P.O. BOX 4602 DATE REPORTED : 02/23/21
EMERALD ISLE ,NC 28594
REVIEWED BY: / t'd, 1
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting) 73 01/26/21 TMR 4500HB-11
Aluminum, (dry wt, basis), mg/kg 2784 02/09/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg 2.6 02/10/21 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 43589 02/09/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 1.3 02/12/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 564 02/09/21 LEI EPA200.7
Chromium, T.(dry wt. basis),ing/kg 12 02/09/21 LFJ EPA200.7
Lead (dry weight basis), mg/kg 15 02/11/21 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 6273 02/09/21 LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.27 02/11./21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 10 02/09/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 8415 02/09/21 LF'J EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 02/10/21 MTM 3113B-04
Sodium (dry wt. basis), mg/kg 16336 02/09/21 LFJ EPA200.7
Zinc (dry wt. basis), tug/kg 1189 02/09/21 LFJ EPA200.7
Total Solids, % 0.49 01/28/21 TMR 2540G-11
TKN (dry wt.), mg/kg c 66180 02/05/21 TLFI 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/Icg c 866.3 02/01/21 't'LH 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 9608 02/05/21 KES 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 8.98 02/02/21 DTL 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg <5.0 02/09/21 LFJ EPA200.7
c Uncertified data. DWR does not offer non-agueoue certification for this analytical procedure.

Environment 1,Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085. 114 Oakmont Dr. Page 1 of I
.5reenville,NC 27858
•nv ironrnent l inc.00m DISINFECTION
CHLORINE NEUTRAUZED AT COLLECTION •
Phone[phone] •Fax.[phone] {=-31
CHLORINE _ -
CLIENT: 68 C Week: 10 pH CHECK(LAB)
ENESIS CONDO ASSO. (HYDROTECH) PPPP P P P P P CONTAINER TYPE,PiG
ON O'MARA
YDROTECH
O.BOX 4602 A A AA A AA CHEMICAL PRESERVATION
14ERALD ISLE NC 28594
a A-NONE D-NAOH
52)725-2319 c 9 .. Q
ui Z w O .o Z _ B-HNO3 E•HCL
op [EC3 Z rn a
y _ o ± C-HZSO, F-ZINC ACETATE/NAOH
COLLECTION "a Lo J •
a. o U 4 u = o < G-NATHIOSULFATE
SAMPLE LOCATION DATE TIME o a F- Q - d w z ¢rz
Sludge Sample 5 (F -- .. CLASSIFICATION:
Ell WASTEWATER(NPDES)
' 1:11 DRINKINGWATER
DWR/GW
DSOLID WAS r t SECTION
CHAIN OF CUSTODY(SEAL)MAINTAINED
- DURING SHIPMENT/DELIVERY
V N
SAMPLES COLLECTED BY:
. _ _ _ (Please Print)
-- . 17 „
SAMPLES RECEIVED IN LAB 1�_I °C
RELINQ ]SHED BY(SIG.)(SAMPLER) DATFJIIME RECE EI]BY(SIG.) I DATEAIME COMMENTS:
1 c? ��W - /Z G12r� 2 'tyURELINQUISHED BY(SIG.) DATby(4041tVZ
TMERECE WED BY(SIG.) DATE'IIME
I
RELINQUISHED BY(SIG.) DATE/T]ME RECEIVED BY(SIG.) DATEII1ME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"Cn for composite sample or a•G"tor
FORM#5 Grab sample in the blocks above for each parameter requested. No 389430 .

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 23,2021
Permit No.WQ0018525
Hampton Suites 1.40 %Solids
7.70 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 4.223 42,230.000 84.460
Phosphorus 1.215 12,150.000 24.300
Potassium 0.266 2,655.000 5.310
PAN(injected)* 1.285 12,850.060 25.700_
PAN(surface)* 1.273 _ 12,726.410 25.453
Ammonia Nitrogen 0,025 247.300 0.495
Calcium 5.629 56,294.000 112.588
Calcium Carbonate Eq. --- --- _,._
Magnesium --- 2,104.000 4.208
Sodium --- 42,468.000 84.936
Sulfur --- --- ---
Nitrate N/Nitrite N --- 7.950 0.016_
Barium --- --- --- SAR
Chloride --- --- --- 5.65
Iron --- --- --- Ceiling Concen.
Aluminum --- I725.000 3.450 (Mg/Kg)
Arsenic --- 2.50 0.005 75
Cadmium --- 0.50 0.001 85
Chromium --- 6.000 --- ---
_
Copper --- 986.00 1.972 4,300
Lead --- 3.60 0.007 840
Mercury --- 0.21 0.000 57
Molybdenum --- 7.00 0.014 75
Nickel --- 9.00 0.018 420
Selenium --- 5.00 0.010 100
Zinc --- 876.00 1.752 7,500
Environment I,Incorporated 551 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits arc listed as detection limits
for calculation purposes.

ilECOU©031Mgd
Drinking Water ID1 37715
Wastewater ID! 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 551 A
HAMPTON INN (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH DATE COLLECTED: 02/23/21
P.O. BOX 4602 DATE REPORTED : 03/25/21
EMERALD ISLE ,NC 28594
�� .
REVIEWED BY:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting) 7.7 02/23/21 JMS 4500HB-11
Aluminum, (dry wt. basis), mg/kg 1725 03/05/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 03/02/21 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 56294 03/05/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg <0.5 03/0I/21 MTM 3113E-04
Copper (dry wt. basis), mg/kg 986 03/23/21 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 6 03/05/21 LFJ EPA200.7
Lead (dry weight basis), mg/kg 3.6 03/03/21 MTM 3 1 1 3 13-0 44
Magnesium (dry wt. basis), mg/kg 2104 03/05/21 LEI EPA200.7
Mercury (dry wt. basis), mg/kg 0.21 03/11/21 MTM EPA74718
Nickel (dry wt. basis), mg/kg 9 03/05/21 L1+J EPA200.7
Potassium (dry wt. basis), mg/kg 2655 03/05/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 03/03/21 MTM 3I138-04
Sodium (dry wt. basis), nig/Icg 42468 03/05/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 876 03/06/21 LEI EPA200.7
Total Solids, % 1.40 02/25/21 JMS 2540G-11
TKN (dry wt.), mg/kg c 42230 03/02/21 TLH 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 247.3 03/05/21 ICES 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 12150 03/02/21 DTL 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 7.95 03/03/21 KES 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg 7 03/05/21 LFJ EPA200.7
c Uncertified data. DWR does not offer non-aqueous certification for this analytical procedure.

Environment I,Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085. 114 Oakmont Dr. Pace 1 of 1
Greenville,NC 27858 _
environment l inc.corn DISINFECTION T
Phone[phone] .Fax[phone] CHLORINE NEUTRALIZED AT COLLECTION
CHLORINE . -
CLIENT: 551 A Week:9 UV _ pH CHECK(LAB)
EAIVIPTON INN(HYDROTECH) lj NONE PPPPPPP CONTAINER TYPE,P/G
,TTN:DON O'MARA - - - -
CYDROTECH CHEMICAL PRESERVATION
'.O.BOX 4602 A A A A A A A
:A'IERALD ISLE NC 28594 - z _
o F A-NONE D-NAOH
E 1 co _ cn
252)725-2319 z w z '' o =�' C $ HNO1 E HCL
EC1. - O z Z cc
T ° ¢ o ¢ C _ C-HzSO, F-ZINC ACETATE/NAOH
COLLECTION a u°C., -J o - e .°
o u ti z p ¢ G-NATHIOSULFATE
SAMPLE LOCATION DATE TIME o ,'-" Q s ` a
Sludge Sample •Z f(JI I' 5 {a'�3 's k : :4 ti a* Nt CLASSIFICATION:
. _ _ 1 .. _ _ _ - _ 1 WASTEWATER(NPDES)
- - DRINKING WATER
- - - - U DWR1GW
- T D SOLID WASTE SECTION
- _ _
CHAIN OF CUSTODY(SEAL)MAINTAINED
- - - DURING 51=1!<PMENT/DELIVERY
N
SAMPLES COLLECTED BY:
_ _ _ ,- (Please Rini)
SAMPLES RECEIVED IN LAB AT 3 r( aC
RELINQUISHED BY(SIG)(SAMPLER) DATET1ME RECEIVED�� BY(SIG.) DATE/TIME GOMMEMS:
—
Q%,(...,n (or /2- 3/i lt./3 'CPO Ve t4 It-Ail 0 l i 4- ' `Yi
,,�.,JJ
RELINQUISHED BY(SIG.} DATERIME RECEIVED BY(SIG.) 'DATEITIME C/C6t-t P Z- Z3-Z" 4-F d
1 1 -
RELINQUISHED BY(SIG.) DATE/TIME RECEIVED BY(SIG.) DATFITIME
1
PLEASE READ instructions for completing this form on the reverse side. Sampler must place a"C"for composite sample or a"G"for
FORM k5 Grab sample in the blocks above for each parameter requested. N2 3 8859 6

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 3,2021
Permit No.WQ0018525
Harker's Point 0.59 %Solids
12.35 pH(Taken from Lime Stabilization)
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 0.962 9,622.000 I 19.244
Phosphorus 2.111 21,110.000 _ 42.220
Potassium 0.885 8,850.000 17.700_
PAN(injected)* 0.308 3,079.090 6.158
PAN(surface)* 0.297 2,973.590 5.947
Ammonia Nitrogen 0.021 211.000 0.422
Calcium 2.036 20,361.000 40.722
Calcium Carbonate Eq. --- --- ---
Magnesium --- 5,420.000 10.840
Sodium --- 28,355.000 56.710
Sulfur --- --- ---
Nitrate N/Nitrite N _ --- 44.790 0.090
Barium --- --- _ --- SAR
Chloride --- --- -- 3.49
-
Iron --- --- --- Ceiling Concen.
Aluminum --- 3368.000 6.736 (Mg/Kg)
Arsenic --- 2.50 0.005 75
Cadmium -_. 0.84 0.002 85
Chromium --- 13.000 --- ___
Copper --- 488.00 0.976 4,300
Lead --- 28.00 0.056 840
Mercury --- 0.42 0.001 57
Molybdenum --- 5.00 0.010 75
Nickel --- 8.00 0.016 420
Selenium --- 5.00 0.010 100
Zinc --- 1,624.00 3.248 7,500
Environment 1,Incorporated 95S
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection Iimits
for calculation purposes.

!1WW11e '(011-1 �@Li1'a Ca
[lbfi(Gwiriomf: . ci) °Col
1 E .r F
' r..;"� Arin$ing,'Watsr ID, 37715
3 -f
tewater In 1
7 �
.1 [4 OAKMONT DkIVE PHONE (2r)2) !'>: ;
GREENVILLE, N.C. 27£35£3 FAX (e)!W) i',,,
ID#; 95 S
HARKER'S POINT SUBDIVISION(FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES DATE COLLECTED: 02/03/21
P.O. BOX 4188 r DATE REPORTED : 02/25/21
EMERALD ISLE ,NC 28594
REVIEWED BY:
J ` �
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
Aluminum, (dry wt, basis), mg/kg 3368 02/09/21 LFJ ,,EPA200,7
Arsenic (dry wt. basis), mg/kg <2.5 02/10/21 MTM 311313-04
Calcium (dry wt. basis), mg/kg 20361 02/09/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 0.84 02/12/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 488 02/09/21 LFJ EPA200.7
Chromium, T.(dry wt, basis),mg/kg 13 02/09/21 LFJ EPA200.7
Lead (dry weight basis), mg/kg 28 02/11/21 MTM 3113E-04
Magnesium (dry wt. basis), mg/kg 5420 02/09/21 LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0,42 02/23/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 8 02/09/21 LFJ EPA200.7
Potassium (dry wt. basis), ing/kg 8850 02/09/21 LFJ EPA200.7
Selenium (dry wt, basis), mg/kg C 5.0 02/10/21 MTM 3113B-04
Sodium (dry wt. basis), mg/kg 28355 02/09/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 1624 02/09/21 LFJ EPA200.7
Total Solids, % 0,59 02/05/21 KDS 2540G-11
TKN (dry wt.), nig/kg c 9622 02/11/21 KES 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 211.0 02/08/21 TLH 350.1 R2-93
Phosphorus, T, (dry wt.), mg/kg c 21110 02/11/21 TLH 365,4-74
Nitrate-Nitrite (dry wt.), mg/kg c 44,79 02/10/21 DTL 353.2 R2-93
Plant Available Nitrogen, mg/kg 3915 02/15/21 MAO
Molybdenum (dry wt, basis), mg/kg <5.0 02/09/21 LFJ EPA200.7
c Uncertified data. DWR does not offer non-aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: October 14,2021
Permit No.WQ0018525
NC Aquarium at Pine 1.24 %Solids
Knoll Shores 12.22 pH(taken from lime stabilization event)
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
—
'Nitrogen(TKN) 4.149 41,490.000 82.980
Phosphorus 2.741 27,410.000 54.820
Potassium 0.486 4,863.000 9.726
PAN(injected)* 1.261 12,606.3I0 25.213
PAN(surface)* 1.251 12,5I0.210 25.020
Ammonia Nitrogen 0.019 192.200 0.384
Calcium 5.476 54,759.000 _ 109.518
Calcium Carbonate Eq. --- ___ ---
Magnesium --- 7,757.000 15.514
Sodium --- 69,791.000 139.582
Sulfur _ --- _-. -__
Nitrate N/Nitrite N --- 24.770 0.050
Barium --- --- --- SAR
Chloride --- --- --- 8.21
Iron --- --- --- Ceiling Concen.
Aluminum --- 1,591.00 3.182 (Mg/Kg)
Arsenic --- 2,50 0.005 75
Cadmium --- 8.60 0.017 85
Chromium --- 20.000 --_ ___
Copper --- 361.00 0.722 4,300
Lead --- 33.00 0.066 840
Mercury --- 0.18 0.000 57
Molybdenum --- 6.00 0.012 _ 75
Nickel --- 22.00 0.044 420
Selenium --- 5.00 0.010 100
Zinc --- 853.00 1.706 7,500
Environment 1# 444 A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

EHEEITCTIE@E'R [IrCORIDEVAi Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 444 A
NC AQUARIUM AT PINE KNOLL, SHORES
MR. DAN FORTIN
FORTIN CONTRACT SERVICES DATE COLLECTED: 10/14/21
P.O. BOX 4188 DATE REPORTED : 11/11/21
EMERALD ISLE, NC 28594
REVIEWED BY:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
Aluminum, (dry wt. basis), mg/kg 1591 10/21/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 10/27/21 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 54759 10/21/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 8.6 11/03/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 361 10/21/21 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 20 10/21/21 LFJ EPA200.7
Lead (dry weight basis), mg/Icg 33 11/09/21 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 7757 10/21/2I LFJ EPA200.7
Mercury (dry wt. basis), n:g/kg 0.18 10/27/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 22 10/21/2I LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 4863 10/21/21 LFJ EPA200.7
Selenium (dry wt. basis), nig/kg <5.0 11/10/21 MTM 3113E-04
Sodium (dry wt. basis), mg/kg 69791 10/21/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 853 10/21/21 LFJ EPA200.7
Total Solids, % 1.24 10/19/21 DNS 2540G-15
TKN (dry wt.), mg/kg c 41490 10/19/21 BMD 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/Icg c 192.2 10/20/21 TRJ 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 274I0 10/19/21 TRJ 365.4-74
Nitrate+Nitrite (dry wt.), mg/kg c 24.77 10/22/21 BMD 353.2 R2-93
Plant Available Nitrogen, mg/kg 12510 10/25/21 MAO
Molybdenum (dry wt. basis), mg/kg 6 10/21/21 LFJ EPA200.7
c Uncertified data. DWR does not offer non-aqueous certification for thin analytical procedure.

:nvironnent I,Inc. CHAIN OF CUSTODY RECORD
'.O. Box 7083, 114 Oakmont Dr. Page 1 of 1
Greenville.NC 2785S,
nvi ronmen t l inc_com DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION
'hone(252)756-6208 a Fax[phone] CHLORINE _
1L�'NT. 444 A Week:22 LL••—•�� pH CHECK(LAB)
NC AQUARIUM AT PINE KNOLL SHORES s�� P P P P P P CONTAINER TYPE,PIG
MR.DAN FORTIN [J NONE -
FORTIN CONTRACT SERVICES -
P.O.BOX 4I881:11A A A A A A CHEMICAL PRESERVATION
EMERALD ISLE NC 28594 r _ -
olQ A-NONE D-NAOH
[phone] u.i u0.� U •a "'
z -, ui z w Z B-HNO3 E-HCL
-' cc o z c
0
o o lo ¢ ea C-I.1 S4, F-ZINC ACETATEJNAOH
r .0 cs� z
COLLECTION o o ° z F. L Z a G-NATHIOSULFATE
1- v a. d o x E O .4 cc
SAMPLE LOCATION DATE TIME o o IT ¢ o s E" a" Z a" _<
D_
Sludge Sample •6.111-Zt Ib- a 4 a ='' CLASSIFICATION:
II W• ASTEWATER(NPDES)
- D D• RINKING WATER
{J DWR/GW
D S• OLID WASTE SECTION
CHAIN OF CUSTODY(SEAL)MAINTAINED _
URING SHIPMENT/DELIVERY
— _ .. ._ V N
S P COLLECTE BY:
_ (Pin se
6 4JGil
SAMPLES RECEIVED IN LAB AT 3. b 0C
RE a U c', E B, (SIG.)(SAM ER) DM , R EIVED BY(SIG) DATEII1ME COMMENTS:
UNQUISI-IED BY(SIG.) DATE/TIME RECEIVED BY(SIG.) DATE/TIME
I I
RELINQUISHED BY(SIG.) DATE/TIME RECEIVED BY(SIG.) DATE/TIME
1
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"C"for composite sample or a"G"(or Ng. 398907
FnRM iis Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 11,2021
Permit No.WQ0003067
Ocean Bay Villas 0.75 %Solids
12.43 pH(taken from lime stab.)
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 4.056 40,560.000 81_120
Phosphorus 1.220 12,200.000 24.400
Potassium 0.437 4,366.000 8.732
PAN(injected)* 1.230 12,302.880 24.606
PAN(surface)* 1.222 12,215.780 24.432
Ammonia Nitrogen 0.017 174.200 0.348
Calcium 3.068 30,684.000 61.368
Calcium Carbonate Eq. --- --- -__
Magnesium --- 2,661.000 5.322
Sodium --- 14,550.000 29.100
Sulfur --- --- _--
Nitrate N/Nitrite N --- 12.940 0.026
Barium --- --- --- SAR
Chloride --- --- --- 1.85
Iron --- --- --- Ceiling Concen.
Aluminum --- 3,610.00 7.220 (Mg/Kg)
Arsenic --- 2.50 0.005 _ 75
Cadmium --- 1.20 0.002 85
Chromium --- 12.000 --- ---
Copper --- 298.00 0.596 4,300
Lead --- 20.00 0.040 840
Mercury --- 0.34 0.001 _ 57
Molybdenum --- 5.00 0.010 _ 75
Nickel --- 12.00 0.024 420
Selenium --- 5.00 0.010_ 100
Zinc --- 1,063.00 2.126 7,500 1
Environment 14 442 A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

kidrIp© ii di©CAP©176Ag
Drinking Water IDi 37715
Wastewater IDi 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 442 A
C&P ENTERPRISES (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES DATE COLLECTED: 02/11/21
P.O. BOX 4188 DATE REPORTED : 03/25/21
EMERALD ISLE ,NC 28594
REVIEWED SY:Effluent Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
Fecal Coliform (MF), /100 Mls <I 02/11/21 DNS 9222D-06
Aluminum, (dry wt. basis), mg/lig 3610 03/05/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 03/02/21 MTM 3113B-04
Calcium (dry wt, basis), mg/kg 30684 03/05/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 1.2 03/01/21 MTM 311313-04
Copper (dry wt. basis), mg/kg 298 03/23/21 LFJ EPA200.7
Chromium, T.(dry tint. basis),mg/kg 12 03/05/2I LFJ EPA200.7
Lead (dry weight basis), mg/kg 20 03/03/21 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 2661 03/05/21 LEI EPA200.7
Mercury (dry wt. basis), mg/kg 0.34 02/23/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 12 03/05/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 4366 03/05/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 03/03/21 MTM 31138-04
Sodium (dry wt. basis), mg/kg 14550 03/05/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg I063 03/06/21 LFJ EPA200.7
Sodium Adsorption Ratio (talc) 21.4
Total Solids, % 0.75 02/11/21 JMS 2540G-11
TICN (dry wt.), mg/kg c 40560 02/23/21 ICES 351.2 R2-93
Ammonia Nitrogen (dry wt,),mg/kg c 174.2 02/18/21 ICES 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 12200 02/16/21 TUT 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 12.94 02/17/21 ICES 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg <5.0 03/05/21 LFJ EPA200.7
c Uncertified data. DWR does not offer non-aqueous certification for this analytical procedure.

Environment 1,Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085. 114 Oakmont Dr.
Greenville,NC 27858 - !-
Page 1 of 1
environment 1 inc,.com Di/INFECTION
Phone[phone]*Fax[phone] CHLORINE NEUTRALIZED AT COLLECTION
iii
CHLORINE - - _ - -
CLIENT: 442 A Week: 10
pH CHECK(LAB)
Li uv - _
&P ENTERPRISES(FORTIN) [) NONE P PPPPP CONTAINERTYPE,PIG
IR.DAN FORTIN _ -
'ORTIN CONTRACT SERVICES
'.O.BOX 4188 J A A A A A A A CHEMICAL PRESERVATION
HERALD ISLE NC 28594 . _
rr
A-NONE D-NAOH
Z52)393-8720 z 2 9 _ ° W w
0 0 cc o z Z z i 8-HNO� E HCL
_, ¢ rn 4 r.
C HMSO, F ZINC ACETATE/NAOH
COLLECTION C¢ a o r c c I± "'
F- w .��. cc G-NATHIOSULFATE
SAMPLE LOCATION DATE TIME o o - ¢ o E" w -
Sludge Sample ,2--/1-11 9: ( 4 Via;:* "
CLASSIFICATION:
/ i3/ 1 .8-r --'?/f-2( 1: _ — — WASTEWATER(NPDES)
I1:1 DRINKING WATER
DWR/GW
USOLID WASTE SECTION
CHAIN OF CUSTODY(SEAL)MAINTAINED
- - - DURING SHIPMENT/DELIVERY
N
SAMP rS Ci TED BY:
. (PIP P.'nt)
ottf +fit'` .
i
SAMPLES RECEIVED IN LAB AT d.e °C
t
' D BY(SIG.) AMPLER) DATFJIIMk RE EI ED BY 5l _ DATEII1ME COMMENTS:
•/% 1)-0�
RELINQUISHED BY(SIG.) Ct
DA i ME RECEIVED BY(SIG.} • VilDATE ME
RELINQUISHED BY(SIG.) DATE/TIME RECEIVED BY(SIG.) DATEITIME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"C"for composite sample or a"G"for
FORM#5 Grab sample in the blocks above for each parameter requested. No 389318

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: October 14,2021
Permit No.WQ0018525
Ocean Club 0.92 %Solids
12.33 pH(taken from lime stabilization event)
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
()/n x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 0.788 7,883.000 15.766
Phosphorus _ 2.144 21,440.000 42.880
Potassium 0.699 6,988.000 13.976
PAN(injected)* 0.288 2,883.130 5.766
PAN(surface)* 0.252 2,522.880 5.046
Ammonia Nitrogen 0.072 720.500 1.441
Calcium 3.467 34,667.000 69.334
Calcium Carbonate Eq. --- --- ---
Magnesium --- 4,899.000 9.798
Sodium --- 15,282.000 30.564
Sulfur --- --- ---
Nitrate N/Nitrite N --- 13.880 0.028
Barium _ --- --- --- SAR
Chloride --- --- --- 1.95
Iron --- --- --- Ceiling Concen.
Aluminum --- 1,878.00 3.756 (Mg/Kg)
Arsenic --- 2.50 0.005 75
Cadmium --- 0.79 0.002 85
Chromium --- 8.000 --- ---
Copper --- 312.00 0.624 4,300
Lead --- 10.00 0.020 840
Mercury --- 0.17 0.000 57
Molybdenum --- 5.00 0.010 75
Nickel --- 9.00 0.018 420
Selenium --- 5.00 0.010 100
Zinc --- 1,692.00 3.384 7,500
Environment 1#i 404 A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

t IJ V O VIELILUIJgL.FIJ bocurpurdap, Drinking Water ID; 3T7i5
Wastewater IDr 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 404 A
OCEAN CLUB (FORTIN)
MR. DAN FORTIN
FORTIN CONTRACT SERVICES DATE COLLECTED: 10/14/21
P.O. BOX 4188 DATE REPORTED : 11/11/21
EMERALD ISLE, NC 28594
REVIEWED Bx:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
Aluminum, (dry wt. basis), mg/kg 1878 10/21/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 10/27/21 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 34667 10/21/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 0.79 11/03/21 MTM 3113E-04
Copper (dry wt, basis), mg/leg 312 10/21/21 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 8 10/21/21 LFJ EPA200.7
Lead (dry weight basis), mg/kg 10 11/09/21 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 4899 10/21/21 LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.17 10/27/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 9 10/21/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 6988 10/21/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 11/I0/21 MTM 3113B-04
Sodium (dry wt. basis), mg/kg 15282 10/21/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 1692 10/21/21 LFJ EPA200.7
Total Solids, % 0.92 10/19/21 DNS 2540G-15
TKN (dry wt.), mg/kg c 7883 10/19/21 BMD 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 720.5 10/20/21 TRJ 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 21440 10/19/21 TRJ 365.4-74
Nitrate+Nitrite (dry wt.), mg/kg c 13.88 10/22/21 BMD 353.2 R2-93
Plant Available Nitrogen, mg/kg 2523 10/25/21 MAO
Molybdenum (dry wt. basis), mg/kg 5 10/21/21 LFJ EPA200.7
c Uncertified data. DWR does not offer non-aqueous certification for this analytical procedure.

fnvironrnent 1,Inc. CHAIN OF CUSTODY RECORD
'.O.Box 7085. 114 Oakmont Dr. Page 1 of 1
3reenville.NC 27858 _
.nvironrnent1 inc.com DISINFECTION
CHLORINE NEUTRALIZEDRTCOLLECTION
'hone(252)756-6208 e Fax[phone]
CHLORINE . _ _
404 A Week:22
:TIENT: UV - — - pH CHECK{LAB)
OCEAN CLUB(FORTIN) NONE PPPPPP CONTAINER TYPE,PIG
MR.DAN FORTIN
FORTIN CONTRACT SERVICES
P.O.BOX 4188 A A A A A A CHEMICAL PRESERVATION
EMERALD ISLE NC 28594 _ _
cn o A NONE D NAOH
[phone] La,y 9 co „°�, �,
E o r o z o 2 B-IiNO, E-FCL
o 0 P w ¢ " •� m C-H2S0, F-ZINC ACETATEINAOH
COLLECTION a w - O ll -, E
a a+ E, . = 0 Q G NATHI05ULFATE
SAMPLE LOCATION DATE TIME o o L I- o F .4 �' Z py a
Sludge Sample 101 1 10:05
4 Iti ' ' -
CLASSIFICATION:
X WASTEWATER(NPDES)
_ - - - U DRINKING WATER
_ — I i DWR/GW
-
- - - _ 11 SOLID WASTE SECTION ,
CHAIN OF CUSTODY(SEAL)MAINTAINED
- - - - - - DURING SHIPMENT/DELIVERY
- - - - 5 N
SAMPLES COLLECTED BY:
, (Please Print)
' _ 1$1111%NV
SAMPLES RECEIVED IN LAB AT 34 6 °C
RE ' UISHED B (SIG.)' AMPLER) DATE/TIME R EIVED BY(SIG.) DATEMME COMMENTS:
t0J1� I II:00 iU/b01 j-2!ss
PPLINQUISHED:Y{SIG.) ATE/11ME RECEIVED BY(SIG.) DATEMME
-
RELINQUISHED BY(SIG.) DATE/TIME RECEIVED BY(SIG.) DATE/TIME
1
PLEASE READ Instructions for completing this form on the reverse side. Sampler mess place a"C'for composite sample or a"G"for NQ 398906
FORM#5 Grab sample in the blocks above for each parameter requested.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 25,2021
Permit No.WQ0018525
Oceans Condominiums 0.87 %Solids
7.1 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 0.330 46,220.000 92.440
Phosphorus 0.266 23,430.000 46.860
Potassium 0.504 5,784.000 11.568
PAN(injected)* 0.119 1,188.350 2.377
PAN(surface)* 0.105 _ 1,053.850 2.108
Ammonia Nitrogen 0.027 786.100 _ 1.572
Calcium 5.876 24,643.000 49.286
Calcium Carbonate Eq. --- --- ---
Magnesium 0.418 3,800.000 7.600_
Sodium --- 13,881.000 27.762
Sulfur __- ___
Nitrate N/Nitrite N --- 10.950 0.022
Barium --- --- --- SAR
Chloride --- ___ --- 2.02
Iron --- --- --- Ceiling Concen.
Aluminum --- 2,737.00 5.474 (Mg/Kg)
Arsenic --- 2.50 0.005 _ 75
Cadmium --- 0.98 0.002 85
Chromium --- 11.000
Copper --- 670.00 1.340 4,300
Lead --- 18.00 0.036 840
Mercury --- 0.22 0.000 57
Molybdenum --- 5.00 0.010 75
Nickel --- 12.00 0.024 420
Selenium --- 5.00 0.010 100
Zinc --- 1,634.00 3.268 7,500
Environment 1 # 566 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

Enwk©EramEq hicarparmUd
Drinking Water ID: 37715
Wastewater ID, 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
XD##: 566 A
OCEANS CONDOMINIUMS (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH DATE COLLECTED: 02/25/21
P.O. BOX 4602 DATE REPORTED : 03/30/21
EMERALD ISLE ,NC 28594
REVIEWED BY:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting) 7.1 02/25/21 J1MIS 4500HB-11
Aluminum, (dry wt. basis), mg/kg 2737 03/16/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 03/I8/21 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 24643 03/16/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 0.98 03/16/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 670 03/16/21 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 11 03/16/21 L1+'J EPA200.7
Lead (dry weight basis), mg/kg 18 03/17/21 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 3800 03/16/21 LFJ EPA200.7
Mercury (dry wt, basis), mg/kg 0.22 03/11/21 MTM EPA7471B
Nickel (dry wt, basis), mg/kg 12 03/16/21 1A.I EPA200.7
Potassium (dry wt. basis), mg/kg 5784 03/16/21 LTJ EPA200.7
Selenium (dry wt. basis), mg/Icg C 5.0 03/22/21 MTM 3113B-04
Sodium (dry wt. basis), mg/kg 13881 03/16/21 LFJ EPA200.7
Zinc (dry wt. basis), uig/leg 1634 03/16/21 LFJ EPA200.7
Total Solids, % 0.87 03/02/21 BLV 2540G-11
TKN (dry wt.), mg/kg c 46220 03/02/21 TLl1 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/Icg c 786.1 03/05/21 ICES 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 23430 03/02/21 DTL 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 10.95 03/03/21 KES 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg <5,0 03/16/21 LF,T EPA200.7
c Uncertified data. DWR does not offer non-aqueous certification for this analytical procedure.

Environment 1,Inc. CHAIN OF CUSTODY RECORD
O.Box 7085. 114 Oakmont Dr. Page 1 of 1
:3reenvillle,NC 27858 _
:nvironmeutlinc.cam 1 DISINFECTION
Phone[phone]•Fax[phone] CHLORINE NEUT"r ALlZEDATCOLLEC11ON
CLIENT: 566 A week 8 cHI OR1E pH CHECK(I Aa)
OCEANS CONDOMINIUMS(HYDROTECH) PPPPPPP COMAINERTYPE,FIG
%.TTN:DON O'MA.RA NONE
RYDROTECH - ,
P.O.BOX 4602 ( A A A A A AA CHEMICALPRESERVATION
EMERALD ISLE NC 2S544 _ _
0)0
�" A NONE D NAOH
z LJ m cr O z B-HNO E-HCL
o _ C-H2S06 F-ZINC ACETATE'NAOH
COLLECTION Q Lu - o 6 a z_ 5 z
o, a ca u ¢ G NATHi05ULFATE
O w v O B. �° El Pam. d
SAMPLE LOCATION DATE TIME o r- s a
... uN
Sludge Sample v 5 ; d . v f A5SIFECATION:
WASTEWATER(NPDES)
i DRINKING WATER
ij DWFVGW
SOLID WASTESEC11ON
r CHAIN OF CUSTODY(SEAL)MAINTAINED
- - DURING SHIPMENT/DELIVERY
_ T Y N
SAMPLES COLLEGI Ell BY:
(Plea Pri ) F
i
SAMPLES RECEIVED IN[AB AT AA. I 'C
HEU QUISHE D BY(SIG)(SAMPLER), DATE'I1ME RECE VED BY(SIG.) DATETTIME cofuiiUla n s:
RaINQUISHED BY(SIG.) DATFITIME RECEIVED BY(SIG.) DATEIIIME
i
:RBJNQUISHED BY(SIG.) DATEli1ME RECEIVED BY(SIG.) DATE/WE
I PLEASE READ Instructions for completing this form on the reverse side' Sampler must place a"C"for composite sample or a`G"p6i
^,• Grab sample in the blocks above for each parameter regisested. 14,113 '2Q 0 1 A Q

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 26,2021
Permit No.WQ0018525
Pebble Beach 3.28 % Solids
6.8 pH
Parameter % Mg/Kg Dry Weight I Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 7.400 74,000.000 148.000
Phosphorus 1.125 11,250.000 22.500
Potassium 0.307 3,067.000 6.134
PAN(injected)* 2.663 2,464.097 4.928
PAN(surface)* 2.347 2,435.542 4.871
Ammonia Nitrogen 0.633 6,326.000 12.652-
Calcium 2.643' 26,428.000 52.856
Calcium Carbonate Eq. --- _-- ---
-
Magnesium 3,320.000 6.640
Sodium --- 4,315.000 _ 8.630
Sulfur ___ ___
Nitrate N/Nitrite N --- 5.000 0.010
Barium --- .__
--- SAR
Chloride --- ___
_ --- 1.20
Iron --- --- --- Ceiling Concen.
Aluminum --- 2,232.000 4.464_ (Mg/Kg)
Arsenic --- 2.50 _ 0.005 75
Cadmium --- 0.88 0.002 85
Chromium --- 9.000 --- ---
Copper --- 420.00 0.840 4,300
Lead --- 13.00 0.026 840
Mercury --- 0.25 0.001 57
Molybdenum --- 5.00 _ 0.010 75
Nickel --- 11.00 0.022 420
Selenium --- 5.00 0.010 100
Zinc --- 1,427.00 2.854 7,500
Environment I # 287A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

Eildr©IflEgrfq
Drinking Water 1131 37715
Waetewater IDi 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID)#: 287 A
PEBBLE BEACH (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH DATE COLLECTED: 01/26/21
P.O. BOX 4602 DATE REPORTED : 02/23/21
EMERALD ISLE ,NC 28594
REVIEWED BY: e.--"11 /62._
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used For reporting) 6.8 01/26/21 TMR 4500HB-11
Aluminum, (dry wt, basis), mg/kg 2232 02/09/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 02/10/21 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 26428 02/09/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 0.88 02/12/21 MTM 311313-04
Copper (dry wt. basis), mg/kg 420 02/09/21 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 9 02/09/21 LET EPA200.7
Lead (dry weight basis), mg/kg 13 02/11/21 MTM 311313-04
Magnesium (dry wt. basis), mg/kg 3320 02/09/2I LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.25 02/11/21 MTM EPA747IB
Nickel (dry wt. basis), mg/kg 11 02/09/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 3067 02/09/21 LIIJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 02/10/21 MTM 311313-04
Sodium (dry wt. basis), mg/kg 4315 02/09/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 1427 02/09/21 LFJ EPA200.7
Total Solids, % 3.28 01/28/21 TMR 2540G-11
TICN (dry wt.), mg/kg c 74000 02/05/21 TLH 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 6326 02/03/21 ICES 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 11250 02/05/21 ICES 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 5.00 02/02/21 DTL 353.2 R2-93
Plant Available Nitrogen, mg/kg 23470 02/09/21 MAO
Molybdenum (dry wt. basis), mg/kg <5.0 02/09/21 LFJ EPA200.7
o Uncertified data. DWR does not offer non-aqueous certification for thin analytical procedure.

Environment 1,Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085. 114 Oakmont Dr. Page 1 of 1
Greenville,NC 27858
environment 1 irc.corn DISINFECTION 1
CHLORINE NEUTRALIZED AT COLLECTION
Phone[phone] •Fax[phone] u CHLORINE
CLIENT: week:8 — _
pH CHECK(LAB)
O I V' ONE PPPPPPP CONTAINER TYPE,PIG
AT EN: DON O'MARA _
HYDROTECH
P.O.BOX 4602 .__ AA A AA A A CHEMICALPRESERVATION
EMERALD ISLE NC 28594 z - - - - .
.'a c. A-NONE D-NAOH
_ m
(252)7252319 `=r Q `c
o_t o z 0 -. z _ B HNQ E HCL
z ¢ w g yo `n = Z C H2SOq F ZINC ACETRTElNAOH
COLLECTION c.' ¢ w 4n 5 c�
ca
3 1 o 4 F - = G NATHIOSULFATE
SAMPLE LOCATION DATE TIME o o ° Q E I - O Z a
d,:.. �': 5 't=:ice
i f ' k A�;�
Sludge Sample L) (j )--1 a 5 • 1:C., '.::-:•� ...ns w¢_ •rv;. _
. .• n CLASSIFICATION:
WASTEWATER(NPDES)
- - j DRINKING WATER
DWR/GW
• - J r SOLID WASTE SECTION
L _
CHAIN OF CUSTODY(SEAL)MAINTAINED
- - DURING IPMENT/DELIVERY gIP
N
SAMPLES COLLECTED BY:
- (Please Punt)
e-a_ Rom+
SAMPLES RECEIVED IN LAB AT • k °C
REL QUISHED BY(SIG.)(SAMPLER) DATE 'lME REC)VED BY(Si DATE/TIME. COMMENTS:
RELINQUISHED BY(SIG.) DATE/liME RECEIVED BY(SIG.) DATE/TIME
IME
I I .
RELINQUISHED BY(51G.) DATEITIME RECEIVED BY(SIG.) DATE/TIME
1
PLEASE READ Instructions for completing this farm on the reverse side. Sampler must place a"C"for composite sample or a"G"for
FORM n5 Grab sample in the blocks above for each parameter requested. No 368832

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 23,2021
Permit No.WQ0018525
Pine Knoll Townes 1.39 %Solids
6.9 pH
Parameter °A° Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 5.113 51,130.000 102.260
Phosphorus 1.479 14,790.000 29.580
Potassium 0.442 4,422.000 8.844
PAN(injected)* 1.571 15,712.990 _ 31.426
PAN(surface)* 1.545 15,449.390 30.899
Ammonia Nitrogen 0.053 527.200 _ 1.054
Calcium 4.624 46,236.000 92.472
Calcium Carbonate Eq. --- --- ---
Magnesium --- 2,814.000 5.628
Sodium --- 9,620.000 I9.240
Sulfur --- --- _-.
Nitrate N/Nitrite N --- 4.950 0.010
Barium _ --- --- --- SAR
Chloride --- --- --- 1.38
Iron --- --- --- Ceiling Concen.
Aluminum --- 2,918.00 5.836 (Mg/Kg)
Arsenic --- 2.50 0.005 75
Cadmium --- 0.68 0.001 85
Chromium --- 9.000 ---
_
Copper --- 581.00 1.162 _ 4,300
Lead --- 10.00 0.020 840
Mercury --- 0.33 _ 0.001 57
Molybdenum --- 5.00 0.010 75
Nickel --- 11.00 0.022 420
Selenium --- 5.00 0.010_ 100
Zinc --- 1,493.00 2.986 7,500
Environment I# 558 A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N—%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

ETWEInTOMEZA iu I]nig(DITipOlarM6
Drinking Water ID, 37715
Wastewater ID, 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 55B A
PINE KNOLL TOWNES (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH DATE COLLECTED: 02/23/21
P.O. BOX 4602 DATE REPORTED ; 03/30/21
EMERALD ISLE ,NC 28594
REVIEWED SY:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used l'or reporting) 6.9 02/23/21 JMS 4500H13-I1
Aluminum, (dry wt. basis), mg/leg 2918 03/16/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 03/18/21 MTM 3113B-04
Calcium (dry wt. basis), ing/kg 46236 03/16/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 0.68 03/16/21 MTM 3113E-04
Copper (dry wt, basis), nig/kg 581 03/16/21 LFJ EPA200.7
Chromium, T.(dry wl. basis),mg/kg 9 03/16/21 LEI EPA200.7
Lead (dry weight basis), mg/kg 10 03/17/21 MTM 311313-04
Magnesium (dry wt. basis), mg/kg 2814 03/16/2I LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.33 03/11/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 11 03/16/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 4422 03/16/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 03/22/21 MTM 3113B-04
Sodium (dry wt. basis), mg/kg 9620 03/16/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 1493 03/16/21 LFJ EPA200.7
Total Solids, % 1.39 02/25/21 JMS 2540G-1I
TKN (dry wt.), mg/kg c 51130 03/02/21 TLH 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 527.2 03/05/21 ICES 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 14790 03/02/21 DTL 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 4.95 03/03/21 ICES 353.2 R2-93
Molybdenum (dry wt. basis), mig/kg 5 03/16/21 LEI EPA200.7
c Uncertified data. DWR does not offer non-aqueous certification for this analytical procedure.

Environment 1,Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085. 114 Oakmont Dr. Page 1 of 1
Greenville.NC 27858 -
environmen cline.corn DISINFECTION
CHLORINE NEUTRAIJZED AT COLLECTION
Phone[phone]• Fax [phone]
CHLORINE _ — — .
CLIENT: 558 A Week:9 pH CHECK(LAB)
D UV - - —
'INE KNOLL TOWNES(HYDROTECH) D.'NONE PPP PPPP CONTAINER TYPE,P/G
.TTN:DON O'MARA i - -
IYD ROTECH
'.O. BOX 4602 A A A A A A A CHEMICAL PRESERVATION
:HERALD ISLE NC 28594 o ci) A-NONE D-NAOH
Ei= co
wa �252)725-2319 z z C B HNO, E HCL
p O Z az •-
o Q
r, w z w �' . w C-H,SOE F-ZINC ACETATE/NAOH
COLLECTION iu o W — S
a v 8 " G NATHIOSULFATE
cc
SAMPLE LOCATION DATE TIME o o ¢ .- .4 a zz c
r Z+F`}% v.•:x` ti�:.F. vv. ku.�-�Y�4f - - r
Sludge Sample /+yj\ f ; 5 Y :• '^h: CLASSIFICATION:
- Li WASTEWATER(NPDES)
' - r - DRINKING WATER
IJ DWR/GW
jSOLID WASTE SECTION
• CHAIN OF CUSTODY(SEAL)MAINTAINED
- " . - DURINGIPMENT/DELIVERY
Y N
SAMPLES COLLECTED BY:
- . (Please P'nt)
c.
C-e----01/10.11--C---.
SAMPLES RECEIVED IN LAB AT 3,3 �C
R N ISHED BY(SIG.)(SAMPLER) DATE(fiME RECEIVED BY(SIG.) DATEItiME COMMENTS:
RELINQUISHED BY(SIG.) DATEMME RECEIVED BY(SIG.) DATEIIIIME
RELINQUISHED BY(SIG.) DATE/TIME RECEIVED BY(SIG.) DATE/TIME
- .
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"C"for composite sample or a"G"for
FORM#5 Grab sample in the blocks above for each parameter requested. No 388592

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 21,2021
Permit No.WQ0018525
Point Emerald Villas 1.97 % Solids
6.6 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(°/° x 10,000) (Mg/Ks x 0.002)
Nitrogen(TKN) 5.254 54,960.000 109.920
Phosphorus 1,482 13,240.000 26.480
Potassium 0.273 2,271.000 4.542
PAN(injected)* 1.602 16,024.570 32.049
PAN(surface)* 1.585 15,854.070 31.708
Ammonia Nitrogen 0.034 420.100 0.840
Calcium 4.028 17,164.000 _ 34.328
Calcium Carbonate Eq. --- --- ---
Magnesium --- 4,206.000 8.4I2
Sodium --- 9,911.000 19.822
Sulfur - --- --- ___
Nitrate N/Nitrite N --- 24.770 0.050
Barium --- --- --- SAR
Chloride --- --- --- 2.46
Iron --- --- --- Ceiling Concen.
Aluminum --- 6,935.00 13.870 (Mg/Kg)
Arsenic 2.50 0.005 75
Cadmium --- 0.93 0.002 85
Chromium --- 21.000 --- _-
Copper --- 710.00 1.420 4,300
Lead --- 74.00 0.148 840
Mercury - --- 0.67 0.001 57
Molybdenum --- 5.00 0.010 75
Nickel --- 11.00 0.022 420
Selenium --- 5.90 _ 0.012 100
Zinc --- 2,221.00 4.442 7,500
Environment I# 348 A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection Iimits
for calculation purposes.

G
3 •3 .`nil.nking Water ID; 37715
Wa etesvatar IDi 10
F C A f<MONT DRIVE Pi IQNI: (,).!,;.,, :
NV}L_LE, N.C. 27858 FAX (;'f,;-')
•
. ID#: 348 A
POINT__EMERALD VILLAS (FORTIN)
MR. DAN FORTIN.
FORTIN CONTRACT SERVICES DATE COLLECTED: 01/21/21
P.O, BOX 4188 , HATE REPORTED : 02/12/21
EMERALD ISLE ,NC 28594
.� l (
REVIEWED SX: L ___A
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH, Units 6.6 01/27/21 TMR 1500HB-11
Aluminum, (dry wt. basis), mg/kg 6935 01/29/21 LFJ EPA200.7
Arsenic (dry ivt. basis), mg/kg <2.5 01/28121 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 17164 01/29/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 0,93 02/02/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 710 01/29/21 LFJ EPA200.7
Chromium, T,(dry WI, basis),mg/kg 21 01/29/21 LFJ EPA200.7
Lead (dry weight basis), mg/kg 74 02/01/21 MTM 3113E-04
Magnesium (dry wt, basis), mg/kg 4206 01/29/21 LFJ EPA200.7
Mercury (dry wt, basis), mg/kg 0.67 02/11/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 11 01/29/2I LFJ EPA200.7
Potassium (dry wt, basis), mg/kg 2271 01/29/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg 5,9 02/01/2l MTM 3113B-04
Sodium (dry wt, basis), mg/kg 9911 01/29/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 2221 01/29/21 LFJ EPA200.7
Total Solids, % 1,97 01/26/21 KDS 2540G-I1
TKN (dry wt.), mg/kg c 54960 02/02/21 KES 351.2 R2-93
Ammonia Nitrogen (dry ►vt.),mg/kg c 420,1 01/27/21 DTL 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 13240 02/02/21 TLH 365,4-74
Nitrate-Nitrite (dry wt.), mg/kg c 24.77 01/28/21 DTL 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg <5,0 01/29/21 LFJ EPA200.7
c Uncertified date. DWR does not offer non-aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: November 23,2021
Permit No.WQ0018525
Queens Court 0.75 %Solids
7.04 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 4.490 44,900.000 89.800
Phosphorus 1.480 14,800.000 29.600
Potassium 0.777 7,770.000 I5.540
PAN(injected)* _ 1.448 14,479.310 28.959
PAN(surface)* 1.447 14,472.660 28.945
Ammonia Nitrogen 0.001 13.300 0.027
Calcium 1.430 14,300.000 28.600
Calcium Carbonate Eq. --- --- ---
Magnesium --- 3,120.000 6.240
Sodium --- 27,700.000 55.400_
Sulfur _-- ___
Nitrate N/Nitrite N --- 1,000.000 2.000
Barium --- --- --- SAR
Chloride --- --- --- 4.72
Iron --- --- --- Ceiling Concen.
Aluminum --- 1,880.00 3.760 (Mg/Kg)
Arsenic --- 46.00 0.092_ 75
Cadmium 46.00 0.092 _ 85
Chromium --- 46.000 --- --
Copper --- 375.00 0.750 4,300
Lead --- 46.00 0.092 _ 840
Mercury --- 2.08 0.004 57
Molybdenum --- 46,00 0.092 75
Nickel --- 46.00 0.092 420
Selenium --- 46.00 0.092 100
Zinc --- 1,810.00 3.620 7,500
I
Envirochem# 2021-20846
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

1 , 2, Environmental Chemists, Inc.
Wi,i1x'U+Gh:e#1 6602 Windmill Way,Wilmington,NC 28405 ' 910.392,0223 Lab • 910,392.4424 Fax
`--rf . 5 = 710 8owsertown Road,Manteo,NC 27954 4 252.473,5702 Lab/Fax
-.---",ifr; -= `T 255-A Wilmington Highway,Jacksonville,NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS info a environmentalchornists.com
Fortin Contract Services Date of Report: Dec 27, 2021
Post Office Box 4188 Customer PO#:
Emerald isle NC 28594 Customer +: 08100061
Attention: Dan Fortin Repo 20 -20846
Pro 6: Queens Court -
Lab ID Sample ID: Collect Date/Time 5 -trix Sample. by
21-52281 Site: Sludge 11/23/2021 9:45 AM Solid rota- ortin
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA 200.7,Rev.4.4,1994 1880 mg/kg 12/06/2021
Arsenic EPA200.7,Rev.4.4,1994 <46,0mg/kg 12/06/2021
Cadmium EPA 200.7,Rev.4,4,1994 <46,0 mg/kg 12/06/2021
Calcium EPA 200.7,Rev.4.4,1994 14300 nig/kg 12/06/2021
Chromium EPA 200.7,Rev.4.4,f994 <46.0 mg/kg 12/06/2021
Copper EPA 200.7,Rev.4.4,1994 375 mg/kg 12/05/2021
Lead EPA 200.7,Rev.4,4,1994 <46.0 mg/kg 12/05/2021
Magnesium EPA 200.7,Rev,4.4,1994 3120 mg/kg 12/06/2021
Molybdenum EPA 200.7,Roy.4.4,1994 <46.0 mg/kg 12/06/2021
Nickel EPA 200,7,Rev,4.4,1994 <46.0 mg/kg 12/06/2021
Potassium EPA 200.7.Rev,4,4,1994 7770 mg/kg 12/06/2021
Selenium EPA 200.7,Rev.4.4,1994 <46.0 mg/kg 12/06/2021
Sodium EPA 200.7,Rev.4.4,1994 27700 mg/kg 12/06/2021
Zinc EPA 200.7,Rev.4.4,1994 1810 mg/kg 12/06/2021
Nitrate+Nitrite-Nitrogen EPA353.2 1000 mg/kg 11/29/2021
Total Solids (%) SM2540 B 0.75% 11/29/2021
Ammonia Nitrogen SM 4600 NH3 C-2011 <13.3 mg/kg 11/29/2021
Total Kieldahl Nitrogen (TKN) SM 4600 Norg 8.2011 44900 mg/kg 11/30/2021
Total Phosphorus SM 4600 P F•2011 14800 mg/kg 12/03/2021
pH SW 646 Method 00450 7.04 units 12/22/2021
Result estimated..Analyzed out of 15 minutes hold time.
Mercury SW646 7471 s <2.08 mg/kg 11/30/2021
Comment; Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: i' cu1oSJi , 1�
Report# 2021-20846 PeOs 1 or 1

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 16,2021
Permit No.WQ0018525
Sands Villas 0.79 % Solids
5.9 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
()/o x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 3.100 31,000.000 62.000
Phosphorus 1.515 15,150.000 30.300
Potassium 0.291 2,906.000 5.812
PAN(injected)* 0.936 9,363.455 18.727
PAN(surface)* 0.933 9,331.630 18.663
Ammonia Nitrogen 0.006 63.650 0.127
Calcium 4.189 41,894.000 83.788
Calcium Carbonate Eq. --- ___
Magnesium --- 3,162.000 6.324
Sodium --- 9,682.000 19.364_
Sulfur --- ___ ---
Nitrate N/Nitrite N --- 18.900 0.038
Barium --- --- --- SAR
Chloride --- --- --- 1.09
Iron --- --- --- Ceiling Cancers.
Aluminum --- 3,964.00 7.928 (Mg/Kg)
Arsenic --- 2.50 0.005 75
Cadmium --- 0.83 0.002 85
Chromium --- 14.000 --- _--
Copper --- 308.00 0.616 _ 4,300
Lead --- 9.I0 0.018 840
Mercury --- 0.28 0.001 57
Molybdenum --- 5.00 _ 0.010 75
Nickel --- 46.00 0.092 420
Selenium --- 5.00 0.010 100
Zinc --- 1,471.00 2.942 7,500
Environment 1# 559
*Determination of Plant Available Nitrogen(PAN):
Injected Application_
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

1Eg atium _a `'a linc erp®Tmlgi
Drinking Water IDs 37715
Wastewater ID, 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 559
SANDS VILLA (HYDROTECH)
DON O'MARA
HYDROTECH DATE COLLECTED: 03/16/21
P.O. BOX 4602 DATE REPORTED : 04/08/21
EMERALD ISLE ,NC 28594
REVIEWED BY:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting) 5.9 03/16/21 DMJ 450011B-11
Aluminum, (dry wt. basis), mg/kg 3964 04/01/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 04/05/2I IMITM 31I3B-04
Calcium (dry wt. basis), mg/kg 41894 04/01/21 LFJ EPA200.7
Cadmhmt (dry wt. basis), mg/kg 0.83 04/0I/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 308 04/01/21 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 14 04/01/21 LFJ EPA200.7
Lead (dry weight basis), mg/kg 9.1 04/0I/21 MTM 3113B-04
IW1agnesiunl (dry wt. basis), mg/kg 3162 04/01/21 LEI EPA200.7
Mercury (dry rvt. basis), mg/kg 0.28 04/05/21 MTM EPA7471I1
Nickel (dry wt. basis), mg/kg 46 04/01/21 LEI EPA200.7
Potassium (dry wt. basis), mg/kg 2906 04/01/21 LFJ EPA200.7
Selenium (dry wt, basis), mg/kg <5.0 03/31/21 MTM 3113B-04
Sodium (dry wt, basis), mg/kg 9682 04/01/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 147 t 04/01/21 LFJ EPA200.7
Total Solids, % 0.79 03/17/21 KDS 2540G-11
TKN (dry wt.), mg/kg c 31000 03/23/21 KES 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 63.65 03/24/21 DTL 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 15150 03/23/21 TLH 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 18.90 03/23/21 DTL 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg <5.0 04/01/21 I,FJ EPA200.7
c Uncertified data. DWR does not offer non-aqueous certification for this analytical procedure.

]Environment 1,Inc. CHAIN OF CUSTODY RECORD
P.D.Box 7085. 114 Oakmont Dr. Page 1 of 1
Greenville,NC 27858 _ _
environment 1 inc.com DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION
Phone[phone]•Fax[phone] CHLORINE - _ _ _
CLIENT: 559 Week:8 _ pH CHECK(LAB)
UV
SANDS VILLA(HYDROTECH) VLNONE PPPPPPP CONTAINER TYPE,PIG •
DON O'MARA - - - -
HYDROTECH LI CHEMICALPRESERVATION
P.O.BOX 4602 A A A A A A A
EMERALD ISLE NC 28594
o A NONE D NAOH
[phone] z w z co - := 0C B-HNC, E-HCL
s F w "4 E C-H.,SO4 F-ZINC ACETATEJNAOH
COLLECTION - w -� ., o E.a a o 0 -- 6.. Z - _ a G-NATNIOSULFATE
SAMPLE LOCATION DATE TIME o o `r" a '' 174 x * '' z
Sludge Sample 3 1 Ii9)�,1 _ 5 :oa< >r`.'$l '' }
de p r .r" CLASSIFICATION:
lWASTEWATER(NPDES)
' - - D DRINKING WATER
rj DW'JGW
L:1 SOLID WASTE SECTION
CHAIN OF CUSTODY(SEAL)MAINTAINED
` - - . -- - _ DURING NIPMENT/DELIVERY
- _ Y N
SAMPLES COLLEC I tl)BY:
- _ _ (Please P'ni
SAMPLES RECEIVED IN LAB AT 3.5 °C
REUN ISHED BY(SIG.)(SAMPLER) DAM/TIME RECEIVED BY(SIG.) DATE/TIME COMMENTS:
1 .._ - 4\u 1).1 I vices 3„,„,,;,. 1. 3/6 t 13 r2-
REUNQUISHED BY(SIG.) DA i ME RECEIVED BY(SIG) • DATE/liME
RELINQuiSHED BY(SIG) DATET1iME RECEIVED BY(SIG) DATE/l1ME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"C"for composite sample or a"G"for
FORM#5 Grab sample in the blocks above for each parameter requested. No 388834

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: January 21,2021
Permit No.WQ0018525
Sea Isle Plantation 1.34 %Solids
12.17 pH(taken from lime stabilization event)
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 1.917 53,970.000 107.940
Phosphorus 0.675 14,960.000 29.920
Potassium 0.452 4,741.000 9.482
PAN(injected)* 0.581_ 5,814.128 11.628
PAN(surface)* 0.578 5,775.308 11.551
Ammonia Nitrogen 0.008 1,233.000 2.466
Calcium 4.831 22,801.000 45.602
Calcium Carbonate Eq. --- --- ---
Magnesium --- 2,883.000 5.766
Sodium --- 11,666.000 23.332
Sulfur --- --- ---
Nitrate N/Nitrite N --- 9.980 _ 0.020
Barium --- --- --- SA R
Chloride --- --- _ --- 2.23
Iron --- --- --- Ceiling Concen.
Aluminum --- 2,470.00 4.940 (Mg/Kg)
Arsenic ._- 2.50 0.005 75
Cadmium --- 1.10 0.002 85
Chromium --- 18.000 --- ---
Copper --- 235.00 0.470 4,300
Lead --- 38.00 0.076 840
Mercury --- 0.20 0.000 57
Molybdenum --- 5.00 0.010 75
Nickel --- I5.00 0.030 420
Selenium --- 5.00 0.010 100
Zinc --- 1,312.00 2.624 i 7,500
Environment 1 i! 96A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

Water IDi 37715
•
Wastewater ID1 10
Ci K1i(.)NT DRIVE_ PI ION' :.
t?�E-;1VfLLF N.C. 27858 FA); {: •
ID#: 96 A
SEA ISLE PLANTATION (FORTIN)
RR. DAN Pa7,'= —
FORTIN CONTRACT SERVICES DATE COLLECTED: 01/21/21
P.O. BOX 4188 't DATE REPORTED : 02/12/21
EMERALD ISLE ,NC 28594
iy I
REVIEWED BY
Sludge Analysis Method
.PARAMETERS Sample Date Analyst Code
Aluminum, (dry wt, basis), mg/kg . 2470 01/29/21 L1 J _ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 01/28/21 MTM 311313-04
Calcium (dry' wt. basis), mg/kg 22801 01/29/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 1,1 02/02/21 MTM 3113E-04
Copper (dry wt. basis), mg/kg 235 01/29/21 LFJ EPA200.7
Chromium, T.(dry Wt. basis),mg/kg 18 01/29/21 LFJ EPA200.7
Lead (dry weight basis), mg/kg 38 02/01/21 MTM 3113B-04
Magnesium (dry wt, basis), mg/kg 2883 01/29/21 LFJ EPA200,7
Mercury (dry wt. basis), mg/kg 0,20 02/11/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 15 01/29/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 4741 01/29/21 LFJ EPA200.7
Selenium (dry WI. basis), mg/kg <5,0 02/01/21 MTM 3113E-04
Sodium (dry wt. basis), mg/kg 11666 01/29/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 1312 01/29/21 LFJ EPA200,7
Total Solids, % 1.34 01/26/21 KDS 2540G-11
TKN (dry wt,), mg/kg c 53970 02/02/21 KES 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 1233 01/27/21 DTL 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 14960 02/02/21 TLE 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 9,98 01/28/21 DTL 353.2 R2-93
Plant Available Nitrogen, mg/kg 16448 02/09/21 MAO
Molybdenum (dry wt. basis), mg/kg 5 01/29/21 LFJ EPA200.7
c Uncartified data, DWR does not offer non aqueous certification for this analytical procedure.

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 16,2021
Permit No.WQ0018525
Sea Spray 0.55 %Solids
7.2 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) t (Mg/Kg x 0.002)
Nitrogen(TKN) 2.885 34,970.000 69.940
Phosphorus 0.416 17,560.000 35.I20
Potassium 0.100 7,033.000 14.066
PAN(injected)* 0.888 8,882.180 17.764
PAN(surface)* 0.872 8,723.180 17.446
Ammonia Nitrogen 0.032 85.660 0.171
Calcium 3.890 44,780.000 89.560
Calcium Carbonate Eq. --- --- -_-
Magnesium --- 4,130.000 _ 8.260
Sodium --- 16,737.000 33.474
Sulfur __- --- ---
Nitrate N/Nitrite N _ --- 3.980 0.008
Barium --- --- --- - SAR
Chloride --- --- --- 1.50
Iron --- --- --- Ceiling Concen.
Aluminum --- 2,753.00 5.506 (Mg/Kg)
Arsenic --- 2.50 0.005 75
Cadmium --- 0.50 0.001 85
Chromium --- 7.000 ---
Copper --- 771.00 1.542 4,300
Lead --- 7.50 0.015 840
Mercury --- 0.25 0.001 57
Molybdenum --- 5.00 0.010 75
Nickel --- 10.00 0.020 420
Selenium --- 5.00 0.010 100
Zinc --- 818.00 I.636 7,500
1
Environment I# 560
*Determination of Plant Available Nitrogen(PAN):
injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

Ezghl©n©1©E ¶ [JE© map©gmiR©
Drinking Water I➢1 37715
Wastewater 1Di 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
µkv.. (#: 56�
„at
A PLACE AT THE BEACH II(HYDROTECH)
DON O'MARA
HYDROTECH DATE COLLECTED: 03/16/21
P.O. BOX 4602 DATE REPORTED : 04/08/21
EMERALD ISLE ,NC 28594
REVIEWED BY:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting) 7.2 03/16/21 DIJ 4500HB-11
Aluminum, (dry wt. basis), mg/kg 2753 04/01/21 LFJ EPA200.7
Arsenic (dry wt, basis), ing/kg <2.5 04/05/21 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 44780 04/01/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg <0.5 04/01/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 771 04/01/21 LFJ EPA200.7
Chromium, T.(dry wt, basis),mg/kg 7 04/01/2I LFJ EPA200.7
Lead (dry weight basis), mg/kg 7.5 04/01/21 MTM 3I1311-04
Magnesium (dry wt. basis), mg/kg 4130 04/01/21 LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.25 04/05/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 10 04/01/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 7033 04/01/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 03/3I/21 MTM 3113B-04
Sodium (dry wt. basis), nig/kg 16737 04/01/21 LFJ EPA200.7
Zinc (dry wt, basis), mg/kg 818 04/01/2I LF.1 EPA200.7
Total Solids, % 0.55 03/17/21 KDS 2540G-11
TKN (dry wt.), mg/kg c 34970 03/23/21 KES 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 85.66 03/24/21 DTL 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 17560 03/23/21 TLH 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 3,98 03/23/21 DTL 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg <5.0 04/01/21 LFJ EPA200.7
c Uncertified data, DWR does not offer non-agueouo certification for thin analytical procedure.

Environment 1,Inc. CHAIN OF CUSTODY RECORD •
-P.O.BoX 7085. 114 Oakmont Dr. Pace 1 of 1
Greenville,NC 27858 _ - -
env ironrnent 1 inc.cotn DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION
Phone[phone]•Fax[phone]
CHLORINE - - - - - -
CLIENT: 560 Week:9 pH CHECK(LAB)
Ul UV - - -
A PLACE AT THE BEACH II(HYDROTECH) NONE PPPPPPP CONTAINER TYPE,PIG
DON O'MARA _ -
HYDROTECH
P.O.BOX 46.02 A A A A A A A CHEMICAL PRESERVATION •
EVIERALD ISLE NC 223594 _a f- - _- _
E o A NONE D NAOH
[phone] z-, U J z Q _� C B-HNO3 E-HCL
00 cro z 11.1 4 o z c
i ¢ ,��", z C-H2SOa F-ZINC ACETATEINAOH
COLLECTION 1¢ w O - C F Ilj
- v LL F 0 G-NATHdOSULFATE
SAMPLE LOCATION DATE TIME g o r`-"- ¢ o m c * i. -' o. z <c
Tue
`� < <5 % ff
CLASSIFICATION:Sledge Sample Cl f(� �i3u
- _ _
El WASTEWATER(Nf DES)
7 D DRINKING WATER
Ul DWRIGW
j SOLID WASTE SECTION •
CHAIN OF CUSTODY(SEAL)MAINTAINED
- - DURING HIPMENT/DELIVERY
- _ _ Y) N
SAMPLES COLLECTED BY:
- _ (Please Print)
,
1.La fL e (O[0_-_-
SAMPLES RECEIVED IN LAB AT ‘ °C -
RELI DISHED BY(SIG.)(SAMPLER) DATET11ME R IVED BY(SIG.) DATE,TIME COMMENTS_ _
� ., CW✓ li l�tk_ u 3/1/r1 `lS
RELINQUISHED BY(SIG.) DATE'i1ME RECEIVED BY(SIG.) DATE/TIME
4
REUNQUISHED BY(SIG.) DATElTIME RECEIVED BY(SIG.) DATE(I1ME
•PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"C"for composite sample or a"G"far
FORM 45 Grab sample in the blocks above for each parameter requested. No 388590

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 9,2021
Permit No.WQ0018525
Sound Of The Sea 0.98 %Solids
6.0 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
r (%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 2.885 53,190.000 106.380
Phosphorus 0.416 16,750.000 33.500
Potassium 0.100 12,572.000 25.144_
PAN(injected)* 0.888 8,883.190 17.766
PAN(surface)* 0.872 _ 8,724.190 17.448
Ammonia Nitrogen _ 0.032 2,613.000 5.226
Calcium 3.890 13,099.000 26.198
Calcium Carbonate Eq. --- --- ---
Magnesium --- 3,949.000 7.898
Sodium --- 19,206.000 38.412
Sulfur --- --- ---
Nitrate N/Nitrite N --- 4.990 0.010 i
Barium --- --- --- SAR
Chloride _ --- --- --- 3.73
Iron --- --- --- Ceiling Concen.
Aluminum --- 2,119.00 4.238 (Mg/Kg)
Arsenic --- 2.50 0.005 75
Cadmium --- 1.30 0.003 85
Chromium --- 8.000
Copper --- 834.00 1.668 4,300
Lead --- 19.00 0.038 840
Mercury --- 0.13 0.000 57
Molybdenum _ 5.00 0.010 75
Nickel --- 8.00 0.016 420
Selenium --- 5.00 0.010 100
Zinc --- 1,344.00 2.688 7,500
Environment 1 4 561
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits arc listed as detection limits
for calculation purposes.

Ertgligiff@h1 Ala Nd©©TIICIITggi
Drinking Water ID: 377.15
Waatevater IDf 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 561
SOUND OF THE SEA CONDOMINIUMS III
ATTN: DON O'MARA
HYDROTECH DATE COLLECTED: 03/09/21
P.O. BOX 4602 DATE REPORTED : 04/06/21
EMERALD ISLE ,NC 28594
REVIEWED BY:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting) 6.0 03/09/21 DU 4500HB-11
Aluminum, (dry wt. basis), mg/kg 2119 03/16/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 03/18/21 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 13099 03/16/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 1.3 03/16/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 834 03/16/21 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 8 03/16/2I LFJ EPA200.7
Lead (dry weight basis), mg/kg 19 03/17/21 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 3949 03/16/21 LFJ EPA200.7
Mercury (dry wt, basis), mg/kg 0.13 04/05/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 8 03/16/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 12572 03/16/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 03/22/21 MTM 3113B-04
Sodium (dry wt. basis), mg/kg 19206 03/16/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 1344 03/16/21 LFJ EPA200.7
Total Solids, % 0.98 03/11/21 JMS 2540G-11
TI(N (dry wt.), mg/kg c 53190 03/16/21 KES 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 2613 03/17/21 DTL 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 16750 03/16/21 DTL 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 4.99 03/16/21 DTL 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg <5.0 03/16/21 LFJ EPA200,7
c Uncertified data. DWR does not offer non-aqueous certification for thin analytical procedure,

Environment I,Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085, 114 Oakmont Dr. Page 1 of 1
Greenville,NC 27858
environmentlinc.com- - DISINFECTION
Phone[phone]•Fax[phone] CHLORINE NEUTRAUZEDATCOLLECTION
CHLORINE - -
CLIENT: 561 Week:S pH CHECK(LAB)
gueUv _ -
DUND OF THE SEA(HYDROTECH) NONE PPP PPPP CONTAINER TYPE,P/G
TIN:DON O'MARA . —
YDROTECH
O.BOX 4602 A AA A A A A CHEMICAL PRESERVATION
1ERALD ISLE NC 2S594 - — - - - -
E o A-NONE D-NAOH
co
:52)725-2319 z w z co .� = B-HNO3 E-HCL
z • �' .... 4 C-H,SO, F-ZINC ACETATE/NAOH
COLLECTION ¢ En Lu a. o Q - .f 6 o er 2 Q G-NATHIOSULFATE
u F
SAMPLE LOCATION DATE TIME g E 'i' ¢ o e: F -, O4 z a
f� ,x gala, 48')'i£` .n4 ryi4
3 I Cl 1)-4 100. n /�v +�yr '':.`:`' h .p,1 _ CLASSIFICATION:
Sludge Sample 5
i . , ij WASTEWATER(NPDES)
IJ DRINKING WATER
UDWR/GW
_ _ - p SOUR WASTE SECTION
CHAIN OF CUSTODY(SEAL) MAINTAINED
- - — — - DURING SHIPMENT/DELIVERY
a N
SAMPLES COLLECTED BY:
W _ m _ - . (Please Print)
_ eorcg Orra lc_
SAMPLES RECEIVED IN LAB AT 2•a cc
RELINQ ISHED BY(SIG)(SAMPLER) DATE/TIME R EIVED BY(SIG.) DATE/TIME COMMENTS:
�
i-T !c( \.i. o i,--... Y/21 I 3 -
'RELINQUISHED BY(SIG.) DAi i I IME RECEIVED BY(SIG.) DATErfIME
1
RELINQUISHED BY(SIG.) DATEfriME RECEIVED BY(SIG.) DATE/TIME
I
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"C"for composite sample or a"G"for
FOAM#5 Grab sample in the blocks above for each parameter requested. No 38 8 8 31

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 16,2021
Permit No.WQ0018525
Southwinds Condominiums 0.52 %Solids
7.6 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 3.533 35,330.000 70.660
Phosphorus 1.502 15,020.000 30.040
Potassium 0.301 3,005.000 6.010_
PAN(injected)* 1.189 11,894.770 23.790
PAN(surface)* 1,184 11,839.220 23.678
Ammonia Nitrogen 0.011 111.100 0.222
Calcium 5.609 56,089.000 112.178
Calcium Carbonate Eq. --- --- ---
Magnesium --- 3,253.000 6.506
Sodium --- 8,065.000 16.130
Sulfur --- --- ---
Nitrate N/Nitrite N --- 1,218.000 2.436
Barium --- --- --- SAR
Chloride --- --- --- 0.64
Iron --- --- --- Ceiling Concen.
Aluminum --- 5558.000 11.116 (Mg/Kg)
Arsenic --- 2.50 0,005 75
Cadmium --- 0.50 0.001 85
Chromium --- 15.000
Copper --- 729.00 1.458 4,300
Lead --- 11.00 0.022 840
Mercury --- 0.72 0.001 57
Molybdenum --- 5.00 0.010 75
Nickel --- 9.00 0.018 420
Selenium --- 5.00 0.010 100
Zinc --- 1,324.00 2.648 7,500
Environment I# 562 B
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

Endurimon _u higu par ing6
Drinking Water ILt 37715 f
Wastewater ID: 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 562 B
SOUTHWINDS (HYDROTECH)
DON O'MARA
HYDROTECH DATE COLLECTED: 03/16/21
P.O. BOX 4602 DATE REPORTED : 04/08/21
EMERALD ISLE ,NC 28594
REVIEWED BY:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting) 7.6 03/16/21 DIJ 4500HB-1I
Aluminum, (dry wt. basis), mg/kg 5558 04/01/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 04/05/21 MTM 3113B-04
Calcium (dry wt. basis), mg/Itg 56089 04/01/21 LF.1 EPA200.7
Cadmium (dry wt. basis), mg/kg <0.5 04/01/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 729 04/01/21 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 15 04/01/21 LFJ EPA200.7
Lead (dry weight basis), mg/kg 11 04/01/21 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 3253 04/01/21 LFJ EPA200.7
Mercury (dry wt, basis), mg/kg 0.72 04/05/21 MT141 EPA7471B
Nickel (dry wt. basis), mg/kg 9 04/01/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 3005 04/01/21 LF;I EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 03/31/21 MTM 3113B-04
Sodium (dry wt. basis), mg/kg 8065 04/01/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 1324 04/01/21 LFJ EPA200.7
Total Solids, % 0.52 03/17/21 KDS 2540G-I1
TKN (dry wt.), mg/kg c 35330 03/23/2I KES 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 111.1 03/23/21 DTL 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 15020 03/23/21 TLII 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 1218 03/19/21 KES 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg <5.0 04/01/21 LFJ EPA200.7
c Uncertified data. DWR doeo not offer non-aqueous certification for thin analytical procedure.

Environment 1,Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085. 114 Oakmont Dr. Page I of 1
Greenville,NC 27858
-
environment l inc.com DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Phone[phone]•Fax [phone]
CHLORINE — - _
CLIENT: 562 B Week:9 pH CHECK(LAB)
[;:l UV _ _ _
SOUTHWINDS(HYDROTECH) NONE PPPPPPP CONTAINER TYPE.PIG
DON O'MARA _ _
HYDROTECH
P.O.BOX 4602 A A A AA AA CHEMICALPRESERVATION
EMERALD ISLE NC 28594 a - - —
o u, A-NONE D NAOH
cn
(252)725 23I9 z ��. � ... C B-HNO, E-HCL
Op ¢ Q z p 'o Z — cr
fen-
- w z w - z i- c-HzSO4 F-ZINC ACETATE/NAOH
COLLECTION J G W J O L
SAMPLE LOCATION DATE TIME IQ E a 2 .z. O ¢ G NATHIOSULFATE
a
Sludge Sample 5 ttaC'Y. i CLASSIFICATION:
lij
_ WASTEWATER
DRINKING WATER
lij DWR/GW
- [j SOIJD WASTE SECTION
CHAIN OF CUSTODY(SEAL)MAINTAINED
T - - DURING S IPMENTIDELIVERY
N
SAMPLES COLLECTED BY: •
_ - (Pleage rint)
fz_
SAMPLES RECEIVED IN LAB AT .D °C
RELINQUISHED BY(SIG.)(SAMPLER) ] DATE/TIME ) RECEIVED BY(SIG.)(S � } /fD/'JATE/lIMEJ COMMENTS:
J4Lf7� ' i.r 3{l�L;I �.i f 'r✓' :4- Lftl r+.. '/'^1 l J.`
RELINQUISHED B 1 G.) DA i ME RECEIVED BY(51G.) DATE/TIME
RELINQUISHED BY(SIG.) DATE/TIME 'RECEIVED BY(SIG) DATE/TIME .
I
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"G"for composite sample or a"G"for
FORM#5 - Grab sample in the blocks above for each parameter requested. N 0 3 8 8 5 8 8

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: February 23,2021
Permit No.WQ0018525
Summer Winds 0.54 %Solids
6.8 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 5.615 56,150.000 112.300
Phosphorus 1.444 14,440.000 _ 28.880
Potassium 0.614 6,138.000 12.276
PAN(injected)* 1.815 18,147.270 36.295
PAN(surface)* 1.777 17,765.720 35.531
Ammonia Nitrogen 0.076 763.100 I.526
Calcium 2.094 20,937.000 41.874
Calcium Carbonate Eq. --- --- ---
_
Magnesium --- 2,995.000 5.990
Sodium --- 19,400.000 38.800
Sulfur --- --- ---
Nitrate N/Nitrite N --- 768.100 1.536
Barium --- --- --- SAR
Chloride --- --- --- 2.43
Iron --- --- --- Ceiling Conceit.
Aluminum --- 2,027.00 4.054 (Mg/Kg)
Arsenic --- 2.50 _ 0.005_ 75
Cadmium --- 0.77 0.002 85
Chromium --- 6.000 --- --
Copper --- 647.00 1.294_ 4,300
Lead --- 9.00 0.018 840
Mercury --- 0.23 0.000 57
Molybdenum --- 5.00 0.010_ 75
Nickel --- 10.00 0.020 420
Selenium --- 5.00 0.010 100
Zinc --- 1,490.00 2.980 7,500
Environment I# 1 19A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

MW[153©F[Earl 1Ip iRg01:
Drinking Water IDi 37715 .
Wastewater ID, 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 119 A
SWNC MASTER OWNERS ASSOC, INC
ATTN: DON O'MARA
HYDROTECH; SUMMER WINDS DATE COLLECTED: 02/23/21
P.O. BOX 4602 DATE REPORTED : 03/25/21
EMERALD ISLE ,NC 28594
REVIEWED BY: ,��� ( `—`
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PII (not to be used for reporting) 6.8 02/23/21 JMS 4500HB-11
Aluminum, (dry wt. basis), nig/kg 2027 03/05/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 03/02/21 MTM 311311-04
Calcium (dry wt. basis), mg/kg 20937 03/05/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 0.77 03/01121 MTM 31I3B-04
Copper (dry wt. basis), mgllcg 647 03/23/21 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 6 03/05/21 LFJ EPA200.7
Lead (dry weight basis), mg/kg 9.0 03/03/21 MTM 311313-04
Magnesium (dry wt. basis), mg/kg 2995 03/05/21 LFJ EPA200.7
Mercury (dry ivt. basis), mg/kg 0.23 03/11/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 10 03/05/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 6138 03/05/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 03/03/21 MTM 3113B-04
Sodium (dry wt. basis), mg/kg 19400 03/05/21 LF.I EPA200.7
Zinc (dry wt. basis), mg/kg 1490 03/06/21 LFJ EPA200.7
Total Solids, % 0.54 02/25/21 JMS 2540G-11
TKN (dry wt,), mg/Icg c 56150 03/02/21 TLH 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/leg c 763.1 03/05/21 KES 350.1 R2-93
Phosphorus, T. (dry wt.), mg/leg c 14440 03/02/21 DTL 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg c 768.1 03/03/21 KES 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg 5 03/05/2I LFJ EPA200.7
e Uncertified data. DWR does not offer non-aqueous certification for this analytical procedure.

Environment I.Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085, 114 Oakmont Dr. Page 1 of 1
Greenville,NC 27858 _
envi ronmgnt]inc.qom DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION
Phone[phone]-Fax[phone]
CHLORINE - • - — •
CLIENT: 119 A Week: 10 pH CHECK(LAB)
D UV _
WNC MASTER OWNERS ASSOC,INC NONE PPPPPPP CONTAINER TYPE,RIG
.TTN:DON O'MARA
[YDROTECH;SUMMER WINDS
.O.BOX 46021:11A A A AA AA CHEMICAL PRESERVATION
,MERALD ISLE NC 28594 _ _ .
o A NONE D NAOH
_ w
:52)725-2319 LL;E y co s. m O co
z J z C B-HNO E-HCL
¢o cco z O c a
_ - et
-' L' v F q z i C-H.50 F-ZINC ACETATE/NAOH
p u w •
COLLECTION -.-,a a ti n a
o o O cc G-NATHIOSULFATE
SAMPLE LOCATION DATE TIME ° o a — — E� E Z Q
. s `t-. A w
Sludge Sample 5 v.. u : 1
- .1)2 ��t rQq�- CLASSIFICATION:
-WASTEWATER(NPDES)
1 - DRINKING WATER
DWR/GW
LjSOIJD WASTE SECTION
CHAIN OF CUSTODY(SEAL)MAINTAINED
- DURING SHIPMENT/DELIVERY
4-Y N
SAMPLES COLLECTED BY:
_ — . _ (Please Rini)
\CC,(c: 01/1.
SAMPLES RECEIVED IN LABAT Li-5 °C
RELJNIQUISHED BY(SIG.)(SAMPLER) DATE/liME RECEIVED BY(SIG.) DATE/TIME COMMENTS:
. . -M 11 \S Y 4L ,;.., ( ,,, /'z3i;.1 13 .5
RELINQUISHED BY(SIG.) DATE/TIME RECEIVED BY(51G.) DATE/TIME
I I
RELINQUISHED BY(SIG.) DATE/TIME RECEIVED BY(SIG.) DATE/iME
I 1
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"C'for composite sample or a"G"for
FORM#s Grab sample in the blocks above for each parameter requested. I P 389404

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: April 22,2021
Permit No.WQ0024756
The Grove WWTP 0.86 %Solids
7 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 5.579 55,790.000 111.580
Phosphorus 1.388 13,880.000 27.760
Potassium 0.624 6,244.000 12,488
PAN(injected)* 1.767 17,674.300 35.349
PAN(surface)* 1.701 17,009.800 34.020
Ammonia Nitrogen 0.133 1,329.000 2.658
Calcium 2.464 24,644.000 49.288
Calcium Carbonate Eq. --- --- ___
Magnesium _ --- 3,341.000 6.682
Sodium --- 20,004.000 40.008
Sulfur --- --- ___
Nitrate N/Nitrite N --- 7.000 0.014_
Barium --- ---
--- SAR
Chloride --- --- ___ 2.93
Iron --- --- --- Ceiling Concen.
Aluminum --- _ 1167.000 2.334 (Mg/Kg)
Arsenic --- 2.50 0.005 75
Cadmium _ --- 0.50 0.001 85
Chromium --- 7.000 - ---
Copper --- 88.00 0.176 4,300
Lead --- 2.90 0.006 840
Mercury --- 0.08 0.000 57
Molybdenum --- 5.00 0.010 75
Nickel --- 8.00 0.016 420
Selenium _ --- 5.00 0.010 100
Zinc --- 690.00 1.380 7,500
Environment I# 549 A
*Determination of Plant Available Nitrogen(PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits arc listed as detection limits
for calculation purposes.

hell-six nag 'fig hcoruorgiRg
•
- ,Drinking .:Water SDI 377.15
Weetewater ID1 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 549 A
THE GROVE WWTP (HYDROTECH)
ATTN: DON O'MARA
HYDROTECH DATE COLLECTED; 04/22/21
P.O. BOX 4602 DATE REPORTED ; 05/20/21
EMERALD ISLE, NC 28594
REVIEWED BY:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting) 7.0 04/22/21 11MM 4500HB-11
Aluminum, (dry wt. basis), mg/kg 1167 04/29/21 LIU EPA200.7
Arsenic (dry wt. basis), mg/kg <2.5 05/04/21 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 24644 04/29/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg <0.5 04/30/21 MTM 3113B-04
Copper (dry wt. basis), ing/kg 88 05/03/21 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 7 04/29/21 LFJ EPA200.7
Lead (dry weight basis), mg/kg 2.9 04/30/21 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 3341 04/29/21 LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.08 04/27/21 MTM EPA7471B
Nickel (dry wt, basis), mg/kg 8 04/29/21 LFJ EPA200.7
Potassium (dry wt, basis), mg/kg 6244 05/07/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 05/05/21 MTM 3113E-04
Sodium (dry wt. basis), mg/kg 20004 05/19/21 LF.1 EPA200.7
Zinc (dry wt, basis), mg/kg 690 05/03/21 LPJ EPA200.7
Total Solids, % 0.86 04/27/21 BLV 2540G-11
TKN (dry wt.), mg/kg C 55790 04/28/21 DTL 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg C 1329 04/27/21 ICES 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg C 13880 04/28/21 ICES 365.4-74
Nitrate-Nitrite (dry wt.), mg/kg C 7.00 04/27/21 DTL 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg <5.0 04/29/21 LFJ EPA200.7
c Uncertified data. DWR does not offer non-aqueoue certification for this analytical procedure.

Environment 1,Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085, 114 Oakmont Dr. pane 1 of I
Greenville,NC 27858
-env ironmentl i nc.com DISINFECTION
Phone[phone]•Fax[phone] CHLORINE NEUTRALIZED AT COLLECTION -
rjCHLORINE _ . _ _ _ - _ -
CLIENT: 549 A Week: 10
a/ -
r -
pH CHECK(LAB)
THE GROVE WWTP(HYDROTECH) Ul NONE PPPPPPP CONTAINER TYPE.PIG
ATTN:DON O'MARA _
HYDROTECHUl _ CHEMICAL PRESERVATION
P.O.BOX 4602 A A A A A A A
EMERALD ISLE NC 28594 _z - — -
E o cil A-NONE Q NAOH
[phone] z 0 `.
z o a B-HNO3 E HCLit ri z S2 -1:, cc
o '.v¢ d� cE , o C HRSO, F-ZINC ACETA T E/NAOH
COLLECTION --,c ua ...s c c LI
SAMPLE LOCATION DATE TIME o o a o 2 s F. < O z ¢ r. NATHIOSULFATE
Sludge Sample 1(-aa�{ e,-�e 1� 5 g 0 :1„,,
r CLASSIFICATION:
,_ Ljj
WASTEWATER(NPDES)
—
- Ul DRINKING WATER
- _
,j DWFI/GW
U SOLID WASTE SECTION
CHAIN OF CUSTODY(SEAL)MAINTAINED
-
DURING SHIPMENT/DELIVERY
V N
SAMPLES COLLECTED BY:
- - - - - _ (Please Print)
-rD
- _ _ _ �CC� PIN„,_
SAMPLES RECEIVED IN LAB AT ,.CO =C
RELINQUISHED BY+SIG.)(SAMPLER) QATEII1ME RECEIVED BY(SIG.) DATE/TIME COMMENTS: —
� � �= 4'?3( 16730 4c4i2LO ..C•-�_ _`I/U/01 t 91
RELINQUISHED BY(SIG.) DATET]ME RECEIVED BY(SIG.) DATE/TIME
I'
REUNQUISHED BY(SIG.) DATE/lIME RECEIVED BY(SIG.) T DATE/TIME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"C"for composite sample or a"G"for
N
FORM x5 Grab sample in the blocks above for each parameter requested. 2 389289

BARNES ENVIRONMENTAL WASTE
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: October 12,2021
Permit No.WQ0018525
Whaler Inn 0.91 %Solids
7.6 pH
Parameter % Mg/Kg Dry Weight Pounds/Dry Ton
(%x 10,000) (Mg/Kg x 0.002)
Nitrogen(TKN) 1.601 54,660.000 109.320
Phosphorus 0.397 _ 23,150.000 46.300
Potassium _ 0.399 4,729.000 9.458
PAN(injected)* 0.503 5,028.110 10.056
PAN(surface)* 0.488 4,883.110 9.766
Ammonia Nitrogen 0.029 898.000 1.796
Calcium 5.591 43,171.000 86.342
Calcium Carbonate Eq. --- --- --_
Magnesium --- 4,037.000 8.074
Sodium --- 13,258.000 26.516
Sulfur --- --- ---
Nitrate N/Nitrite N --- 20.910 0.042
Barium --- --- --- SAR
Chloride --- --- --- 1.56
Iron --- --- --- Ceiling Concen.
Aluminum --- 7,596.00 15.192 (Mg/Kg)
Arsenic --- 2.50 0,005 75
Cadmium --- 0.70 0.001 85
Chromium --- 11.000 --- ---
Copper --- 859.00 1.718 4,300
Lead --- 9.70 0.019 840
Mercury --- 0.35 0.001 57
Molybdenum --- 6.00 0.012 75
Nickel --- 12.00 0.024 420
Selenium --- 5.00 0.010 100
Zinc --- 1,068.00 2.136 7,500
Environment 1#1 70A
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(TKN-Ammonia N)+Ammonia N+Nitrate N+Nitrite N=%PAN
Surface Application:
(Mineralization Rate)(TKN-Ammonia N)+(0.5)(Ammonia N)+Nitrate N+Nitrite N=%PAN
Note: Constituents N.D.(Not Detected)or<detection limits are listed as detection limits
for calculation purposes.

EBAI®AE3LILfg lY iB h©OrPCNIMINg Drinking Water ID: 37715
Wastewater ID: 10
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 70 A
THE WHALER INN (BUCK)
C/O MR. STANLEY BUCK
1745 BELGRADE-SWANSBORO RD. DATE COLLECTED: 10/12/21
MAYSVILLE, NC 28555 DATE REPORTED : 11/11/21
REVIEWED BY:
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
PH (not to be used for reporting) 7.6 10/12/21 DNS 45001-1B-11
Aluminum, (dry wt. basis), mg/kg 7596 10/21/21 LFJ EPA200.7
Arsenic (dry wt. basis), mg/Icg <2.5 10/27/21 MTM 311313-04
Calcium (dry wt. basis), mg/kg 43171 10/21/21 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 0.70 11/03/21 MTM 3113B-04
Copper (dry wt. basis), mg/kg 859 I0/21/21 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 11 10/21/2I LF.1 EPA200.7
Lead (dry weight basis), mg/Icg 9.7 11/09/21 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 4037 10/21/21 LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.35 10/27/21 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 12 10/21/21 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 4729 10/21/21 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 11/10/21 MTM 3113E-04
Sodium (dry wt. basis), mg/kg 13258 10/21/21 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 1068 10/21/21. LFJ EPA200.7
Total Solids, % 0,91 10/14/21 JMS 2540G-15
TKN (dry wt.), mg/Icg c 54660 10/19/21 13MD 351.2 R2-93
Ammonia Nitrogen (dry tivt.),mglkg c 898.0 10/18/21 KES 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 23150 10/21/21 13MD 365.4-74
Nilrate+Nitrite (dry wt.), mg/kg c 20,91 10/19/21 KES 353.2 R2-93
Plant Available Nitrogen, rug/Icg 11222 10/25/21 MAO
Molybdenum (dry wt. basis), mg/kg 6 10/21/21 LFJ EPA200.7
c Uncertified data. OWE done not offer non-aqueous certification for this analytical procedure.

Environment 1,Inc. CHAIN OF CUSTODY RECORD
P.O.Box 7085, 114 Oakmont Dr. Page I of I
Greenville,NC 27858
environment)inc.com DISINFECTION
Phone[phone]n8 •Fax[phone] CHLORINE NEUTRALJZEDATCOILECTION
CHLORINE _ _ —
CLI NT: 7a A Week:8
pH CHECK(LAB)
UV
:HE WHALER INN(BUCK) > NONE PP - P- PPPP CONTAINER TYPE,PIG
:/O MR.STANLEY BUCK
745 BELGRADE-SWANSBORO RD.
rIAYSVILLE NC 28555 L _ A A A AA AA CHEMICAL PRESERVATION
A-NONE D-NAOH
g o o ,-
252}503-5307 J Cc o z a z0.1
B-HNO3 E-HCL
o O F U ¢ o rn E cc
- w cn R C-H2SO4 F-ZINCACETATE/NADH
COLLECTION _.,, I. w S o
3 t a u_ = w - E o = z G NATHIOSULFATE
SAMPLE LOCATION DATE TIME o o " ¢ F. -- s c, z ,
Sludge Sample ., A ?Ti m 1-...:A, a.�' �;;:;
JJ 'i� 7 k��k
/e..z /0,7 — f 5 CLASSIFICATION:
r,.mS WASTEWATER(NPDES)
jDRINKING WATER
LI DWR/GW
— j SOLID WASTE SECTION
-
CHAIN OF CUSTODY(SEAL)MAINTAINED
- - DURING SHIPMENT/DELIVERY y
SAMPLES COLLECTED BY:
(Please Print)
SAMPLES RECEIVED IN LABr' °C
REL�IQUIS ED B LER) DATE/TIME RECEIVED Y(SIC.) �i DATE/TIME COMMENTS:
7 /.72-- I//-.-V Ot/t SI--SliSC
REUNQUISHE BY(SIG.) DA i ME RECEIVED BY(SIG.) ATE/TIME
REUNQUISHED BY(SIG.) DATE1flME RECEIVED BY(SIG.) DATEfIIME �``
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a"C"for composite sample or a"G"for
FORM ns Grab sample in the blocks above for each parameter requested. No 388967

PATHOGEN AND VECTOR ATTRACTION REDUCTION MONITORING

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM.(02T Rules)
Facility Name: Barnes Environmental Waste and Hauling, Inc: WQ Permit Number: WQ001.8525
WWTP Name: SEE ATTACHED LIST NPDES Number: SEE ATTACHED
Monitoring Period: From 11l/202I To 12/31/2021
Pathogen.Reduction (15A NCAC 02T.1106)-Please indicate level achieved and alternative performed:
Class A: AIt.A (time/temp) ❑ Alt B (Alk Treatment)❑ I Alt. C (Prior Testing)0
Alt.D (No Prior Test) ❑ i Process to Further Reduce Pathogengs❑
If applicable to alternative performed (Class A only)indicate"Process to FurtherReduce Pathogens":
Compost ❑ Beat Drying ❑ Heat Treatment ❑ The inophilic ❑
Beta Ra ❑ Gamma Ra ❑
Y y P,asteucization ❑
Class B: Alt. (1)Fecal Density ❑ I Alt. (2)Process to Significantly Reduce Pathogens El
If applicable to alternative performed.(Class B only)indicate"Process to Significantly Reduce Patlogens":
Lime Stabilization 0 Air.Drying 0 Composting 0 jAetobic.Digestion ❑
Anaerobic Digestion ❑ :ti .:
, T
If.applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen DensityNumber of Analytical
Parameter g _ Fregyency :Sample.
Excee- Tech-
in Sludge Minimum Geo. Mean lvtaxirnurn Units dens of Analysis Type mane
2 x 10 to the MPt4
6th power
per gram of CPU
Fecal Coliform total solids
1000'mpn per gram
of total solid (dry
weight)
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal total solid(thy
conform) weight)
Vector Attraction Reduction (15A NCAC.02T.1107)-Please indicate alternative.performed:
Alt.'I (VS reduction) El Alt. 2(40-day bench) ❑ Alt; 3 (30-day bench) ❑ Alt.4.(Spec.02 uptake). ❑'
Alt. 5 (14-Day Aerobic) 0 Alt. 6(Alit: Stabilization 0 Alt 7(Drying-Stable) ❑ Alt.8(Drying-Unstable). •❑
Alt. 9(Injection) (] Alt. 10(incorporation) Q No vector attraction reduction alternatives were performed. ❑
CERTIFICATION STATEMENT (please check the'appropriate statement)
0 "I certify, under penalty of law,that the,pathogen requirements in 15A NCAC 02T.1106 and the
vector attraction reduction requirement in 15A N.CAC 02T.1107.have been met."
0 "I certify, under penalty of law,that-the pathogen requirements in 15A NCAC 02T.110.6 and the
vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note
if you check this statement attach an explanation Why you have not met one or both of the
requirements.)
"This determination has.been made under my direction and supervision in accordance with the system
designed.to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector•attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Steven M. Barnes,President
Pre arer Name and Title(type or print) Land Applier Name and Title(if a pplicable)(type or print)
ignature of Prepares* ate Signature of Land Applier(if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r)and I 5A NCAC 2T.11'02(26)
❑ENR FORM PVRF 119T P1717nm

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: gf1 5-744— ibc.a P.O.#
Batch Size(gallons): t5-6 , O Lbs.or Gallons Used: r?'5D Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour •H Operato
Date Corr. Corrected Corr. 'Corrected Corr. Corroded Corr. Corrected Initials
pH Temp C Time pH Temp C Time pH Temp C Time pH Temp C Time
Factor+ pH Factor+ pH Factor+ pH - Factor pH
PI-2 r 6,Ai 22 0.0 8 2_ id./6 22 4• t t1 13, a 1 A !a a /2•n•7,... 22 O c3°t k.o R ?',30 57/0
3.27- ?l U 0•03 1n.k5 'Na _ 0.24 d3 n•o6 jai 1)1s— la,Do a I 6.0? /a,i Q. r�U 5,
5-•)' '2.N 7.e1 Ac2 Doz. 7.)-3 72E, 1a-)6 , 5 o•l2 1A. R7%z 19-. 4 at/ 4,0- p, /"Do 5-r6
(6-1 i) 9.12 57) O.'S 7-,,Vb roo /a.o+ ,2o 6,i< 1c3.•1co lone l�./ts c96 6,i3 ra.as es a s1rg
f-9 -2+ ').1I) 225 0.1r 7.a5 ?? . _W•DL ,S/ K.►li 1249 q1' 000 21 d. 4 I",; Ptro Stt5
7.1 -a1 7•+.4.1 - ,.6 .12.. 9.3-6, ii 0,16) ,?2 6.11 ia,a* /.,b' la.a4:1 23 a, 3°1 ally /AY
7-11-x 1 7.].S 33 o d 4 ”'`I /i'66 !a•A? ,.z3 ,5Levi 0,04, 116 0 l,,la ..)t A.a7 hd,4r i 2 it -roe
1.21.2t 7,(39 .3"'?- D.1.. 7 S`1 (f-t )2,4S 23 .O• ii tA.32 la+.70 1 . 2r . 3 6•2t1 sa•rlri A. 6 —47a
y-14-2.e 7.1.4 ,.5vd O-LS 946 4?o6 1d.bt 36 . l'.i 161.4 goo ia. t.1 20 Q lIi- 42• gpo .S4
II
C LO [V CA OD en 0 t-- C r CO 10 N m (0 M .n Lo W r to m ' v io o Q V C' e/. f') c•) [+) N N N r r 7 O. Q. Q. O O O G r g (V N M M g M C v
U O O O O O O O C b C) 0 G O O O o 0 o C G o 0 0 0 o c q O O
U 2 Co to 2 2 2 2 2 2 Co 'Jr 2 U) [A C) O = N y N Yl UN e] N fI Vi N N
7 7 7 J 7 7 5 7 7 7 7 7 7 C C C . 7 7 7 7 > C 7 C
O � S. C C C C C C C C C C C
o d a d a rl a a a a a a a a EL a 2 2 2 2 2 2 2 2 2 2 2 5 2 g 2
C.) _
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I-

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: 2pr-7\y-1e",._tii P.O.#
Batch Size(gallons): D,,BO Lbs.or Gallons Used: q(, Material Used For Stabilization: Lime
Initial pH >12 pH_ 2 Hour pH 24 Hour pH Operator
Date Corr_ Corrected Corr. Corrected Corr. Corrected Corr. Corrected Initials
pH Temp C Time pH Temp C Time pH Temp C Time pH Temp C orrecTime
Factor+ pH Factor pH Factor pH Factor pH
--ei1•al C9,4s1 i/ 0 Is _ ln.l0� `ic, ) .act, 26 b.ic -1cA lit-' l L i8 �6 U•tf la•c3'lt)?+) .die
•1.•a; 9 tl 22 o•ittr (.Pcs- io\s _ trail a'4 6.03 I ? It * a, .ig r °r p• t3 1a,ILI P.>b S17
.at, r.i °''o.'1-1 0•nu '•d4 73 0 DR, Qt+ 0,4. la•Ia Jao` 0.•/0_ 4-la a f+2 1d•15 fial.) 511.E
4.a) ‘ ,Ai) Vi 0. 12- 1,173 `.u+_w la•bi .2 5 4.12. la•°l c b id.br Irq p, l . lei,l l 230 se,
6,• 4-_,1 .•7 2. A6 D .i,1 ?•by F`t.+c _ 1a-11.' 3d Q.ie 1 4-2g,laca /2,146 ,,,;0 i,i.T 1cZ‘,.7 P_P4 5- _
P-2 al r,lai 32 a,).y '),S 73CI /a-b2- 33 D•Ay is-,re G91.1 i .1.i3 . (3 a-I=i /;.Li2. it'. ,ter?
?-/a•a+ 7,..fli 72. b.a+ 941 711‘ 1A.®8 ,.?a 2r ]a 2.c 986 /1,;Lca _.2. 4-.21 fa•t1! -2. .sra
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I'V'l-el ,•t/8 .?/ 0.115 '?•t:k. /Oro L 1d.aa" .31 6.43 1a-,a3 )zta. 1a.lo_.,1 0A A -F1 .13a $i/
c i in or m co co O w u) CJ 1 O co co c) co m C' co ( Q is. 0 m CO 0) N la
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U O O O O O O O O O O O O O a a O P o O O a O C] O O O O O O O
W U O M N N y N N CO N N CO CO CO CO N N
LA 0 N N N N N to Cl) 0 0 0 0 0 N � c' `L > a 7 7 7 7 $' 7 7 = 7 7
`0 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 C G C C C C C C C C C C C C C
Ow... CL a a a a a a a Q 0- O a a a a ; ; ; ; ; ; ; ; ; ; ;
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I—

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: 1 24 p goort..01,...\VA,941..-tfrP.0.#
i ;",
Batch Size(gallons): ll}. 0 Lbs.or Gallons Used: c.SZ Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date H Temp C Con-. Corrected TimepH Temp C Corr. Corrected Time Corr- Corrected Corr. Corrected Initials
p Factor+ pH Factor+ pH pH TempCFactor+ Time pH Temp C Time
pH Factor+ pH
y- 8 ► ?az_ ab D 63 2-c's 964 _ P.10 a6 D c is-13 ,J16o 1?./0 -26 a ? /2'13 ?3O Sig'
,R-it-a-► 2.qg c9 a.12 0.40 e60 / .a - , 36 6,if jarao Mob / t ,9O 0.Jr 1.230 &6 s1$2
la7ite-,11 2•L1 e,8 0.61 7-7o gob la•b' ar/ D'6t. /a.67 1106 .0.1° d7 O.oto fa•lto 73 ° Skt:
C L LTD N Cr) CO [�) ' O r V W u] N B) CO C'D c) cu , rn n to m Nr N- O r, O co i N �]
O O c i C l c' N N N �-- O O [7 o O O — r N N N c0 t+) Ci c+) v v
O p p O O 0 6 C O G 6 O 0 o
U p Q O O O O O O O O O O O O o
N LIC) 0 N h 0 N 0 a N InV) V) N Vi Vi
N co N 0 N N N N N N N N (� [l) 07 7 7 7 7 7 7 7 7 3 7 = 7 7
p 7 7 7 n 7 7 7 J 7 7 7 7 7 7 7 c c c c c C C c c c C C c c G
C3 d CL CL CL 0- d CL a a a a a Q. a a 2 2 2 2 5 2 5 5 5 5 5 5 2 5 g
C.)
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NSCOM C]r C C) co C) C) C'r) Cr) C') N N N N N N N N N CAI r r r s— s-- r r s— Y
i

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: �e ,/c j P.O.#
Batch Size(gallons): r�q 4 0 Lbs.or Gallons Used: 1 ._C"OMaterial Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp C Corr. Corrected Time pH Temp C COR. Corrected Time pH Temp C Corr. Corrected Time pH Temp C Corr. Corrected Time Initials
Factor+ pH Factor+ pH - Factor+ pH Factor+ pH
ii—a/ t S1O I8 6. .t 4,2c M-72 I B o.al irr •al",//OO leas /9 a•1P 0.0 ,'6 -s
3-8-._ti 1 ta.R2 d) U•t/ 4•7t) 4o b)./R t , 6,12 am. l' /cic.kt c26 a.ic a•ah' 730 3f
3-a2-,A 6. 8q- ,t O la_ 6.>3 Ptb 1t•r ,-7q p.rs /.1.•63 i626 AIR _al o ,z a n 6 Sc 5-W3
qoB-AI 7+b1 ,P'( 0+65 .,-c8 "3 /a•l° d41 6'1 jr�- 'r 93b l�,.r5" ;I/ oy0 ' 0,)2- 110 a19
5-10-24 ,7.7L , a 1. 0•(3 1.).S /bo- 1dista 4, a .64 1a-4er V hb /2.Jo 2ta 0.6. AN.IJ p&OS -- it
-
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� U O w m m m w h w w m
2 2 2 7 2 7 2 3 2 N 7 2 2 2 2 7 c c C c c 3 C a 7 C 7 E 2 L
o tl Q. a. a a a. a. a. a. a a a n. a a a 2 2 2. 2 2 2 2 2 2 2 2 2 2
0
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l= V co r) Co CO CO CO) CO CO CO, CO (V N N N N N (V N N N ,- . . . . . 7- <-
m
F

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: _ (Prlr Y! z As" P.O.#
Batch Size(gallons): 7 9O Lbs.or Gallons Used: r ?St Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp C Corr. Corrected TimepH Temp C Corr. Corrected Time Corr. Corrected Corn Corrected Initials
pH Temp C Time pH Temp C Time
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
-0a0 lo.g5 da O •04 G SL gad 02Q 20- 6.u4 OAP _lo% 13..20 23 6.06 a.ly 9.30 .."Ifs
4-,_ ,?.1i 'b )•6S 7r,r' e > i,.ao <- / _t 'a ick an_dob) 4.AtS r.2) a-tg iar3; cFg 5.43
C u7 N C) CO C') O r- - r Ca Li' N C) (O M 0 CD m CC 0 CO cr h O M cD CD NJ 41
O c7 r7 (') [') N N N O O O 0 0 O 4 w ,-- N N N r) M r9 Co Q Cr
O O O O O O O O O O O [7 6 O O G G O o O O O O G o d O a o 0
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U
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V' CO. Cr) Cr) Cr) Cr) CO Cr) c*] CR Cr) N N CV N N N N N N N . . . . . . r N— r-
I—

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: �fj� bC/ 7/'�P �'� P.O-#
Batch Size(gallons): h Lbs.or Gallons Used: r_nc Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp C Corr. Corrected Time pH Temp C Corr. Corrected Time pH Temp C Corr. corrected Time pH Temp C COrr. corrected Time Initials
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
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m U O Vl �] N N 8 N N VJ g N N
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C G C C
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F

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: Dar)e5'c cX VI/1j,S P.O.##
Batch Size(gallons): 2`f 5 JO Lbs.or Gallons Used: /r2 Material Used For Stabilization: Lime
Initial pH >12 pH 2_Hour pH 24 Hour pH Operator
Date pH Temp C Corr. corrected Time pH Temp C Corr_ corrected Time pH Temp C CDrr_ Corrected Time pH Temp C Corr. corrected Initials
Time
Factor+ pH Factor+ pH Factor+ pH Factor+_ pH
_
11-J9'a (Q.s1 2 2../ O.12 4.-IN 2 o2 o A.ea l 6.iz 1 1..a-08 6 IP.l$ �_ ' O•i 2- /a,64pb6 S!'l,
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p-1/.2i 9•11 01 . ./c3 9.�41 /2eb )a•oa 2i 6.1a /.k-20 .4215 /a.5 cif O•t8 12 3 J.23 _51/43
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tir3 N N h co a7 N N N N rh N N N N N 7 7 7 j 7 7 7 7 7 7 7 7 a ' 7
O = 7 7 7 7 7 7 7 7 7 7 7 7 = 7 C C C C C C C C C C C C G C C
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a) co co co co co co co co co el N N N N N N N N N N
I— 1

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: P.O.#
Batch Size(gallons): L i5 Lbs.or Gallons Used: Material Used For Stabilization: Lime
initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp C Corr. Corrected Time pH Temp C Corr. corrected Time pH Temp C Corr. Corrected Time pH Temp C Corr_ Corrected Time Initials
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
Cp-/y-.L+ 7•?l L2D D•Ac 2.aL 9D6 lZ.s4: 3rs i.ed` 1a.a7 //oi, J1,/0 3a 'Mu SIPS
C g Q N al 0 C] O I,- r CO LO N OD CO rO 2 2 in F. O C I `.4<r M N N O O O
U o 0 0 0 0 0 0 0 0 0 0 0 a o O O O 0 O O 0 o O 0 0 0 0 0 0
O of g u) 41 01 N 2 o) on
U) in.= 3 3 3 W co to co co 7 co 3 co 3 = = > j 3 a _ = j a _ C 0 z a
3 3 3 3 7 7 7 7 3 7 3 C C C C C C C C C CC C C C
Q a a a. a a. a a a a a iL a 2 2 2 2 2 -2 2 2 2 2 a n a s 5
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ct C) (+) M (+) C) co. c0 co (r) C7 N NNNNNN N N N r r r r
1—

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: g e4E'Sif P.O.#
Batch Size(gallons): ( S2 6 Lbs.or Gallons Used: ii<=6 Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date Con-. Corrected COrr. Corrected Con-. Corrected Corr. Corrected Initials
pH Temp C Factor+ pH Time pH Temp C Factor+ pH Time pH Temp C Factor+ Time pH Temp C Time
pH Factor+ pH
7-Itf-oli 7 / c_?t D-is I•,3`1,,_9o+' _ 12)l0 ,9/ 6./2 1248 /100 12.10 3/ t) is I2)V g 4I1 r �*I#
L
C { (D {•) O rr co {r) N C) (D en r) co 6CJ I 17 C o el 1 w o N Ls.)D
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I—

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WC) 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ,2-I/,{y ,,o t-Qv4) I1,ti P.O.#
Batch Size(gallons): 0600 Lbs.or Gallons Used: /O Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp C Corr. corrected Time pH Temp C Goff. Corrected Time pH Temp C Corr. Corrected Time pH Temp C Gorr_ Corrected Time Initials
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
Ii1'r�1 ^.e O a;/ 7dt! :e.D' ;D 6,1r a. /boo 0..10 Pe t3 i •2S" SA3
-n.•aI ra 22 Oat '?•72 9vo '!_a 32 .I IA,2-1 )I' c la•1. • 2 O.X/ /a-•, &, 9.Po 517
•
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C. IL
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m ' co M CO CO C') CO CO CO CO CO N N N N N N N N N N

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ' �(rn eY f velli 4,..,tt0e-" F.O.#
Batch Size(gallons): 2606 Lbs.or Gallons Used: Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp C Corr. Corrected Time pH Temp C Corr. Corrected Time pH Temp C Corr, Corrected Time pH Temp C CUT. Corrected Initials
Time
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
t-?..i i 10, 1 -5,6 oaf Gr ' / gay /24o ,?(1 Oar Ji.2S° /ADO /2.Zo ,,j. O fc 12.J'.17 elg, }
= 0) N 0) co co O i h 7 ' .- co 0) N co up co c) m 0) N u'i o v r- O o) [6 rn [V yr
_� 0 V V 0) co C7 m N N N O O O o 0 o — c� N cv c� c� r) r) <r v
U G O O G O O O 0 Q G 0 O O O b 0 0 0 O o O C o o G o 0 0 0 0
N U to O Vl 2- N N g g 2 g N h N 2 2
3 z 3 7 7 7 7 7 7 a 7 7 7 7 C C L c C C C C C C C C C C C
U 0_ a. 0_ 0. 0. O. 0. D. a. 0` a. 0_ (L 0_ d 2 2 2
U
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cr CO C7 c7 CO CO el c) CO Ch C•l N N N N N N N N N N r r r ,— r r
N
h

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: /VC_ gUrva le,fA _ P.O.#
U
Batch Size(gallons): a t Lbs.or Gallons Used: /S-Z) Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp C Corr_ Corrected Time pH Temp C Corr. Corrected Time pH Temp C Corr. Corrected Time pH Temp C Corr. Corrected Time Initials
Factor+ pH Factor+ pH Factor+ pH _ Factor+ pH
/0-7`e+ •7, 1t. a9 *•lz ,9-ie,11 9 /2-4V_ A? o.,i /7.4.; /ice e2ei0 ,r' ‘,4z /z,2Z fir' S
C try N Cr) l0 CO O in `Cr r CO 40 N 01 (0 O co CO coT u) co - A o ch co 0H 0
O c4) C) VIt? N N N O O O o o O — i— C' Cv C c•) o C) v.) CI: v
{ 6 w C C C O C O C C C C o O O o p
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T. N) N N N N CO N N N N ro N N IR N O 2 2 2 j 2 2 2 2 C 2 2 2 2 C 2
7 7 7 7 3 7 3 7 3 7 3 7 7 n 7 C C C C C C C C C C C C G C
0 It a a a a a a a a a a a a. a a s 2 2 2 2 2 2 2 2 2 2 2 2 .2 2
U
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E •f• co M CO CO CO CO co coco co N N N N N N N N N N
F-

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ne ect..r'} L r, 1, OP ' e c P.O.#
Batch Size(gallons): ., v OD Lbs.or Gallons Used: Material Used For Stabilization: Lime
Initial pH >12 pH 2 HourpH 24 Hour pH Operator
Date Corr. Corrected Corr. Corrected Corr. Corrected Gorr. Corrected Initials
pH Temp C Time pH Temp C Time pH Temp C Time pH Temp C Time
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
-ash) bsi,, 26 6,4v G•141 0 I,9.IX' ,46 0,Ir 1 1►r /036 /2428 0 1,,ig laar Ji 0 AO -
7 s'-X) 7.a 1 / p,18 a, ce 4i 1 qa Si 6.I R ! •,;3 Woo J J 31 e),i� ) 1/. R..Pa �i) _
R41c - ► 7•,22 0,,lq '.,i0 ,�a® /p.6i .P� . ,�'-i la•as/60. .a-0/14% j3 t•,kV! , .OV 41 s-
•
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o 0 0 0 0 o a o 0 0 0 0 0 0 o d
= 7 D 7 7 = 7 to = 7 D to N D N 7 7 7 j 7 7 7 7 7 7
�7 7 7 7 7 7 7 7 7 7 C c C c c C C c 2 c C C C C C
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: QCQt dt-ch P.O.#
Batch Size{gallons): c3f6 a O Lbs.or Gallons Used: /,1 0 Material Used For Stabilization: Lime
Initia[ pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH (Temp C Corr. Corrected Time pH Temp C Corr. Corrected Time pH Temp C Corr. Corrected Time pH Temp C Corr. Corrected Time Initials
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
^
/-9•al 10.6g 19 b.!8 toS-13 i oo ?a.V / -t 0.►S DI/3 aoo iA.AC 2' 6 .tr 1a ;o /yes sfrp
„P•1t'-2, 'I./15 01.-i O.1 1_ L.,`18 t`no 1e?-.a, .21 C.12 ldk.o 10tr03 1.,/5 ,2I A. l 1 12, 0 ,f„s 0 sive
11.2o•a.l 2. Z) ..ti 0,62 7,19 P36. /d 12 ...� O•+h 12.12 ill.?a 1c�.►.r. 2Q 0.63 tz.l2 co.) '
$-vi-a, 7 19 S'? d•OL_2",ty poi" id /® 27 O-131., 1a,11. )60v 12,4r 62-7 O.O(r a Al '+ Sd
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E � co ch M M CO Cr) 01 Crl CO CO N N N N N N N N N N �— r v r . . . . .
F

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: COnJO ; P.O.#
Batch Size(gallons): , d Lbs.or Gallons Used: /Sn Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date Corr. Corrected Corr. Corrected Corr. Corrected Corn Corrected Initials
pH Temp C Time pH Temp C Time pH Temp C Time pH Temp C Time
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
(0-23-Rr ta•yi .2, 0•12 4(.43 g-476 i fit} act 641 .1..• 1*a liar I ,ia gtt 4,12, 17_,U2- PJQ ,c1
•
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.) O O O O O O O O O O O O O O O 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
`7 O vl N N N N N N N «f N o, o,
N Vi lO Vl fR V) VY N N VS UI N N N 3 C C C C 3 C 3 3 9 C
p 3 3 3 3 3 7 = = 7 7 3 3 C C C = C C C C C C C C C C
0 a a a a a a a a a a a a a. a. a a a a a a a a a a a a a a a
U
0. O 0 Co ti C0 l() - M N r O 6) (0 N CO 1 d- CO N 4 0) DON t0 rr) Ci N o- O
c CO CO C) C') C'] CO CO CO CO m N N N N N (NI N N N N
fl/
F

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ?p,fjh/e �{a,,,, 1 P.O.#
Batch Size(gallons): /9OO(" Lbs.or Gallons Used: L.1,(—D Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp C Carr. Corrected Time pH Temp C COrr. Corrected Time pH Temp G Corr. Corrected Time pH Temp C Corr. Corrected Time Initials
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
..?-2-,21 (e S! ,, D.65 10•42 966 ,a.ao ,23 U•06 i?•lf/ //oa i�IS P3 6-at,/ ./2_ Q9O 5
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`9-�Al 7.// L�l 0.1R 7,201 73 0 /il bF ,.?l /Sfig /r•CCi rho lc2.01D _216 tr. )5 4.1.38 fav S
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.
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CO

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: 2,',le /(or,J1 7icW, P.O.#
Batch Size(gallons): 2,0 06 Lbs.or Gallons Used: Material Used For Stabilization: Lime
Initial pH >12 pH ' 2 Hour pH 24 Hour pH Operator
DatepH TempC Corr. Corrected TimepH TempC Corr. Corrected TimepH TempC Corr. Corrected Time COrn. Corrected Initials
Factor+ pH Factor+ pH Temp C Time
pH Factor+ pH Factor+ pH
1$-c11 ',DI 2 0-oto 6-� llco /a-ors 23 O 1' 1,109 ID* f -„ram 2.' a-eq.. (2•nt `1).b
0-3O-d..+ 9 Ai . �� . faq Rho fib, 11 A7 .1 , l .17 JDbO 1 , a7 6-04. /a-2f' 5rr�
•
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fA N Vl !A N N D N N N N D Ih co N 7 > > C > > > 7 7 7
3 3 7 7 3 3 3 C C C C C C C C C C C
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U
cr- 0 0) CO ti CO LO CO N 0 0) CO N- L0 r.r) - c) N r- O O) Co N (C) LC) CO N x— O
-zr Cr) r) CO CO CO COCr) cO C7 CO (V CV CV CV N CV CV N x CV N . . . . .
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: 7k,, p.o.#
Batch Size(gallons): 3.0 V Lbs.or Gallons Used: f S Material Used For Stabilization: Lirrie
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp C Corr. Corrected Time pH Temp C Corr. corrected Time pH Temp C Corr. Corrected Time pH Temp C Corr. Corrected Time Initials
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
^
6,•(.zq-0/, 7,el/ L2 A 1)qt 2r /206. /2-.10 30 4.i r i ..s• 2, 9..so 3n a•f,r- AZ Vr 1220 5'
c Lo N CD (D CO O r+ m co N Cl) CO CO CO CO O N u) CO v � 0 CO CD 0) N us
O O ' � C) CS CO CO N N N O (] 0 0 C 0 c r r N 01 01 Cl CO CO CO sr cr
U O O O O O O O O O O O O O O CD do O G O O C O O C O O C 66
d U O CON of N N CO d) m N W N W
ul N CO CO us CO us CO CO N CO m CO CO uS g 2 7 e 2 "3 2 7 7 2 3 > > 7 2
o cu 7 7 5 = 7 3 7 = = = 7 = 7 7 3 C C C C C C C C C C C C C C
c0 LL o_ a s a. a o_ a a a o_ o_ o_ a 4 a S 22 S 2 5 - 5 5 5 2 2 5 22
0
Q- 0 0) Co ti co Lo •ci- c'0) N r O Co c0 ti CO Ln 'fit 07 N O Cr) CO ti (0 L[) NI- 0) N 0
CO CO CO CO CO CO CO CO CO CO N N N N N N N N N N
ty
—

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: 0/A eeii s" (9�,-"."- P.O-#
Batch Size(gallons): 021. 0 06 Lbs.or Gallons Used: /7,P Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date Carr. Corrected COrr. Corrected Corr. Corrected Corr. Corrected Initials
pH Temp C Time pH Temp C Time pH Temp C Time pH Temp C Time
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
-)-1'4•;l to•R? 2t b i - te,V, '96b -`_2 26, is r:r 0,0-f flocs adg 26 6./r /;.oY Of . t i
.2-5•7.s 7•la 72 , V3 ). U4 I 42 h., 22 6 61 '61st:1 1Oi4 12. 16 71 D 11 IA•8, 4t.gO S't
4*•c23••,21 `"?.45 r'A O.I r `7.7. ?o Iz.a2 ,.1 O-/S 12,2e ite.,0 /z.2 ...'/ O'/4 _I2.JS.' /S ..
�-, ,VI 9,11 A , P� 6.41 ' wi Irwin lira 32 6.2) la,"A j2Isv ra,,26-, .5 p,2l 12iz1 . J 2® ;.-tom
9 - l 1.l 'I ne c;6 6•fr 7. 7-1 70' 12.06 ,4(3 D.). 1.Zr2.0 9130 /120 3730 0.tr/2,^,r 1 cw
/I-2.24) 9.1p1 29 6•1 2.. 7,7 4 P /2-ot 2c1 a iL /),.,r /Ow aa,n, °r C,,it t,1.27 6 ,45
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0
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CO CO CO CO CO CO CO CO CO CO N N N N N N N CV CV CV r ,- N-a)
I-
r

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
L? .
Facility Name: jJc P.O.#
Batch Size(gallons): r f 760 Lbs.or Gallons Used: �° Material Used For Stabilization: Lime
-
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp CCorr- Corrected Time pH Temp C Corr. Corrected Time pH Temp C Corr. Corrected Time pH Temp C Corr. Corrected InitialsInitials
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
l-c) i! ?.20 ,-71 e9. '-qt, /469 IZ 4X. . / I261# 12-V aa• ,3 •IS I /0$ c
i.. N a) CO CO O f- V W U) N C) CD el U) EO In C.4 L U o f C. 0 C) ED 0 r N En
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CI J 7 3 3 7 7 7 7 7 7 C •c C c c = c c c c c c C
EL a a a O a o a a a a o a o o 2 2 2 2 2 2 2 2 2 2 2 2 2 2
Q. O O O N. CO U) 'd C] N r CO 0 CO r— CO CO 'Cr CO N O Cr) CO ti CO CD V CO N r O
� CO Co CO C') Co CO CO CO CO CO N N N N N N N N N N
H

BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE
ff STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ,� r� �� '�le '/ui ILibr- P.O.#
Batch Size(gallons): /9 0 Qa) Lbs.or Gallons Used: 170 0 Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date pH Temp CCorr- Corrected Time pH Temp C Corr. Corrected Time pH Temp C C0� Corrected Tme pH Temp CCorr- corrected Time Initials
Factor+ pH Factor+ pH Factor+ pH Factor+ pH
S-- ' .t t..5 7 .Y O•of Eo,L/q hits , a.d& ,2tf O.0.5 Ai), .P66 /2 h V-I 0 6-0 idol`1 li ra /g
/ /•a► 6';i c12 , 1) .U9 E,,+/C . -s 12.1:1.5- aS 0 nc, , Ea.1V fCi 12.10 2 ' 0.1z. /z.2z,P'c 514
94',‘NI Er.3t 31 fI, 18 L. ° 3'& Iz.ot 31 9-r2 ) ,f° 5 a 12.70 31 d.IB ,r.).?2 . try ,516
ib-11'X/ '9•2/Z r?A 0 .1,r 2-V ,rot- 12.40 ,O i.1.1a lia1• INta a2. 6 .3 O if 1gg. C- .S744
l
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ��t� <�r,2-/ P.D.#
Batch Size(gallons): 1 / 1 .z® Lbs.or Gallons Used: 96 a Material Used For Stabilization: Lime
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: SThound of 'Me_ ft P.O.#
‘Batch Size(gallons): �7 ,.rbO Lbs.or Gallons Used: Lola) Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
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initial pH >12 pH 2 Hour pH 24 Hour pH Operator
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Time
Factor+ pH Factor+ pH Factor+ pH Factor pH
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: ,c1t,0) e.v•�,,�1N Nets P-O.##
Batch Size{gallons): 417/000 Lbs.or Gallons Used: , y-7{1)6 Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date H Tem C Corr. Corrected Time H Temp C COrr. Corrected Time Corr. Corrected Corr. Corrected Initials
p ppH p Time
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: e ar o e P.O.#
Batch Size(gallons): / 2,57)0 Lbs.or Gallons Used: ?t,2(] Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH Operator
Date H Temp G Corr_ 'Corrected Time H Temp C Corr. Corrected Time H Temp C Corr. Corrected Time Corr. Corrected Initials
p Factor+ pH p Factor+ pH A Factor+ pH Temp C Time
pH Factor+ pH
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BARNES ENVIRONMENTAL WASTE AND HAULING, INC.
WQ 0018525 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Name: /ACC e'r— 4-A/AF P.O.#
Batch Size(gallons): ?D O U Lbs.or Gallons Used: r ? } `•-' Material Used For Stabilization: Lime
Initial pH >12 pH 2 Hour pH 24 Hour pH 'Operator
Date `Corr. Corrected Con . Corrected Corr. Corrected Corr. Corrected Initials
pH Temp CT
Factor+ pH Time pH Temp C Factor+ pH Time pH Temp Factor+ Time pH Temp C Time
- pH Factor+ pH
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2021 APPLICATION SUMMARY

BARNES ENVIRONMENTAL WASTE
Permit#WQ 0018525
RESIDUALS APPLICATION
2021 APPLICATION SUMMARY
Will Turner 2021 1 6.20 56,000 2.14 5.90 1.76
Site WT 2021 2 5.00 122,500 4.53 15.13 3.92
2021 3 8.00 213,500 9.17 20.48 0.00
2021 5 2.60 132,500 6.87 39.56 22.30
2021 6 2.90 94,500 6.43 19.74 17.49
Totals 11441,01 jg09:000111111 11494411
Total Gallons 619 000
WWTP-Metric Tons 26.43

FIELD APPLICATION SUMMARIES

BARNES ENVIRONMENTAL WASTE
2021 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-01 6.2 ACRES TOTAL GALLONS 38,500
Alantic Beacons CC Sass Cape Royal Cedar Colony By Hampton Dunescape Eight 1/2 Emerald Genesis Barkers Island Kingsbridge Mariner's McGinnis NC
Station Reach Dolphin Point The Sea Suites Marina Plantation Condos Point Beach II Point Point Aquarium
JAN 3,500 3,500
FEB 7,000
MAR 3,500
APR
MAY
JUN
JUL _ v
AUG _
SEP
OCT
NOV
DEC
TOTALS 3,500 7,000 7,000 0 0 0 0 0 0 0 0 0 0 0 0 0 0
Corn 0 7,000 3,500 0 0 0 0 0 0 0 0 0 0 0 0 0 0
Rye 3,500 0 3,500 0 0 0 0 0 0 0 0 0 0 0 0 0 0
The Ocean Bay Ocean Ocean Ocean Pebble Peppertree Pine Point ' Queens Sands Sea Island Sea Sound of Southwinds Summer Whaler Inn
Grove Villas _ Club Condos Terrace Beach Resort Knoll Emerald Court Villa Plantation Spray The Sea Condos Winds
JAN 3,500 3,500 3,500
FEB 3,500 3,500 3,500
MAR
_ 17,500
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
TOTALS 0 3,500 7,000 0 0 0 0 0 0 7,000 0 0 0 3,500 0 17,500 0
Corn 0 3,500 3,500 0 0 0 0 0 0 3,500 0 0 0 0 0 17,500 0
Rye 0 0 3,500 0 0 0 0 0 0 3,500 0 0 0 3,500 0 0 0

BARNES ENVIRONMENTAL WASTE
2021 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-02 5.0 ACRES TOTAL GALLONS 80,500
Alantic Beacons CC Sass Cape Royal Cedar Colony By Hampton Dunescape Eight l/2 Emerald Genesis Harkers Island Kingsbridge Mariner's McGinnis NC
Station Reach Dolphin Point The Sea Suites Marina Plantation Condos Point Beach I1 Point Point Aquarium
I - -
JAN
FEB _
MAR
APR
MAY
JUN 10,500 7,000 - 7,000
JUL _ 14,000 7,000 3,500
AUG
SEP
v OCT _ I _
NOV
DEC
TOTALS 10,500 7,000 0 0 0 0 14,000 7,000 0 0 3,500 7,000 0 0 0 0 0
Coastal 10,500 7,000 0 0 0 0 14,000 7,000 0 _0 3,500 7,000 0 0 0 0 0
Rye 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
The Ocean Bay Ocean Ocean Ocean Pebble Peppertree Pine Point Queens Sands Sea Island Sea Sound of Southwinds Summer Whaler Inn
Grove Villas Club Condos Terrace Beach Resort Knoll I Emerald Court Villa Plantation Spray The Sea Condos Winds
JAN _
FEB _
MAR -
APR
MAY
JUN 7,000 7,000 17,500
JUL _ _ 7,000
AUG 7,000 _
SEP _ 3,500
OCT
NOV
DEC 24,500
TOTALS 0 0 0 0 0 7,000 0 0 0 3,500 0 0 7,000 7,000 7,000 42,000 0
Coastal 0 0 0 0 0 7,000 0 0 0 3,500 0 0 7,000 1 7,000 7,000 17,500 0
Rye 0 0 0 0 0 0 0 0 0 0 _ 0 0 0 0 0 24,500 0

BARNES ENVIRONMENTAL WASTE
2021 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-03 8.0 ACRES TOTAL GALLONS 147,000
Alamic Beacons CC Sass Cape Royal Cedar Colony By Hampton Dunescape Eight 112 Emerald - Genesis Barkers Island Kingsbridge Mariner's McGinnis NC
Station Reach Dolphin Point The Sea Suites Marina Plantation Condos Point Beach II Point Point Aquarium
JAN
FEB
MAR
APR 3,500
MAY _ 3,500 7,000
JUN 14,000 7,000 3,500 3,500
JUL r 3,500
AUG 3,500 3,500 3,500 3,500 10,500
SEP
OCT 3,500
NOV
DEC
TOTALS 21,000 7,000 10,500 7,000 10,500 0 3,500 10,500 3,500 0 0 0 0 0 0 0 0
Coastal 21,000 7,000 10,500 7,000 10,500 0 3,500 10,500 ' 3,500 0 0 0 0 0 0 0 0
Rye 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
The Ocean Bay Ocean Ocean Ocean Pebble Peppertree Pine Point Queens Sands Sea Island Sea Sound of Southwinds Summer Whaler Inn
Grove i Villas Club Condos Terrace t Beach Resort Knoll Emerald Court Villa Plantation Spray The Sea Condos Winds
JAN
FEB
MAR
APR 17,500 10,500
MAY 7,000 28,000
JUN 3,500 10,500 7,000 -
JUL 3,500 10,500
AUG 3,500 10,500
SEP 14,000
OCT 14,000
NOV
DEC
TOTALS 17,500 7,000 3,500 0 0 21,000 0 0 0 0 10,500 0 0 14,000 0 66,500 0
Coastal 17,500 7,000 3,500 0 0 21,000 0 0 0 0 10,500 0 0 14,000 0 66,500 0 r
Rye 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

BARNES ENVIRONMENTAL WASTE
2021 FIELD APPLICATION SUMMARY FORM
Permit WQ00I8525
FIELD WT-05 2,6 ACRES TOTAL GALLONS 118,500
Mantic Beacons CC Sass Cape Royal Cedar Colony By Hampton Dunescape Eight 1/2 Emerald Genesis Harkers Island Kingsbridge Mariner's McGinnis NC
Station Reach Dolphin Point The Sea Suites , Marina Plantation Condos Point J Beach It Point Point Aquarium
JAN
FEB
MAR 3,500 3,500
APR _ 3,500
MAY 3,500 14,000 3,500 -
JUN
JUL
AUG 14,000 10,500
SEP
OCT
_ 3,500
NOV _
DEC _ 3,500 3,000
TOTALS 7,000 28,000 7,000 3,500 0 6,500 0 10,500 0 0 0 0 0 0 0 0 3,500
Coastal 3,500 28,000 3,500 0 0 3,500 0 10,500 0 0 0 0 0 0 0 0 3,500
Rye 3,500 0 3,500 3,500 0 3,000 0 0 0 0 0 0 0 0 0 0 0
The Ocean Bay Ocean Ocean Ocean Pebble Peppertree Pine Point Queens Sands Sea Island Sea Sound of Southrvinds Summer Whaler Inn
_ Grove Villas Club Condos Terrace Beach Resort Knoll Emerald Court Villa Plantation Spray The Sea Condos Winds
JAN _
FEB
MAR
APR
3,500
MAY 3,500 _ _ 3,500
JUN 7,000 3,500 3,500 3,500 3,500
JUL _ 3,500 3,500
AUG
SEP
OCT 7,000 3,500
NOV 3,500 7,000
DEC 3,500 3,500
TOTALS 0 0 21,000 3,500 0 0 0 3,500 3,500 I0,500 0 14,000 0 0 0 7,000 3,500
Coastal 0 0 17,500 3,500 0 0 0 0 3,500 7,000 0 _ 14,000 0 0 0 0 3,500
Rye 0 0 3,500 0 0 0 0 3,500 0 3,500 0 0 0 0 0 7,000 0

BARNES ENVIRONMENTAL WASTE
2021 FIELD APPLICATION SUMMARY FORM
Permit WQ0018525
FIELD WT-06 2.9 ACRES TOTAL GALLONS 91,000
Alantic Beacons CC Sass Cape Royal Cedar Colony By Hampton Dunescape Eight 1/2 Emerald Genesis Harkers Island Kingsbridge Mariner's McGinnis NC
Station Reach Dolphin Point The Sea _ Suites _ Marina Plantation Condos Point Beach 11 Point _ Point _Aquarium
JAN
FEB
MAR
APR 7,000 7,000
MAY
JUN
JUL 10,500
AUG
SEP 14,000 _
OCT -
NOV _
DEC
TOTALS 10,500 21,000 0 0 0 0 0 7,000 0 0 0 0 0 0 0 0 0
Coastal 10,500 21,000 0 0 0 0 0 7,000 0 0 0 0 0 0 0 0 0
Rye 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
The Ocean BayOcean Ocean Ocean Pebble Pe entree Pine Point pp Queens Sands Sea Island Sea Sound of 5ou[hwinds Summer Whaler Inn
Grove Villas Club Condos , Terrace Beach Resort Knoll Emerald Court Villa Plantation Spray The Sea Condos Winds
JAN
FEB
MAR 10,500 3,500 3,500 10,500
APR
MAY
JUN
JUL 14,000 3,500
AUG
SEP 10,500
OCT
NOV
DEC
TOTALS 0 0 0 0 0 21,000 0 3,500 0 3,500 0 0 10,500 0 14,000 0 3,500
Coastal 0 0 _ 0 0 0 10,500 0 0 0 0 0 0 0 0 14,000 0 3,500
Rye 0 0 0 0 0 10,500 0 3,500 0 3,500 0 0 10,500 0 0 0 0

FIELD LOADING RATE REPORTS

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name:Barnes Environmental Waite&Hauling Permit#:W00018525. Annual Dry Tons Applied: 2.14
Owner.. Will Turner Operator Steve Barnes Cation Exchange Capacity(non 503): 2.2
Site 0:WT Field# I Acres Utilized: 6.20 Acres Permitted: 6.20
Application Method*: S. Volatilization Rate'": 0.5 Mineralization Rate: 30 % Predominant Soil Series: GoA
Iiiinii Magi . SgF'gime §- iiil#goimiIii..oe i- -
Jmt. - _ •., _ - $� ilUli ra'.&i...:>£,ttO ; iii4.:'_ tl`aimGi?ait2 00,11.,*1`i4;
2021 3.500 565 0.78 0.02 AdanGest itan GID 0.000 0:000 0.028 0.001 0.000 0.000. 0:001 0.000 0.049 0.08' 0.67 Rye 1.77 '0:00" 0.00
2021- 7,000 .1,129 1.26 0.06 Be'� it
°"Ss GM) 0.000 "0.000 :0.151' 0.002 0.000, 0.001 01001 0.001 0.140 L.94 1:73 .Corn 6:28 '0.02 _ 0.05
2021 7,000 1,129. 1.78 0.08, CC Sa s. O/D 0,004:'0.004 0.075. 0.004 0.000 0.004 0.004 0.004 0.081 0.65 __ 0.65 1.86 Corn , Rye 4.21 0.14 0.00
2021 MOO 565 0.75 -0.02 Qcgan BayYllas_G/D 0.000 0.000 _0.01 f 0.001 0.000 0:000 :0.000 0.000 0.03a 0.43 0.43 Corn 1.43 _0.01 0:00
3021 1,000 .1,129 0.92 0.04 °onn club O/D 0.000_0.000 0.027 0.001 0.000. 0.000 .0.00I -0.000. 0.147 0.11 • 0:11 1.86 Cam Rye• 0.68: 0.06 0.00.
2021 7,000 1,129 0.75 :0.04. Quecnscm11. GID 0.003 0.003 :0.026 0.003 0.000 0.003_'0.003 0.003 0.128 0.51 0.5.1 1.05 Corn Rye 3.17 .0:00. 0.07
2021 3,500 565 0.98 0.02. SoundO1Thcsca GID 0.000 0.000 0.038 0.001 0.000 0.000 0.000 0.000 0.062 0.40 0.77 Rye. 2.45 0:12 .0.00
2021 17,500 2;823 0.54 .0.06. S1.1fmnci-Winds GID, 0.000 0.000 0.082 0.001 0.000 0.001. .0:001. 0.001_0.189 2.26 1.84 Coal 7.14 0.10' 0.10
l y
•
Total v 56,000 •
Annuai lbs/acre 0.008 0.007 0.439 0.013 0.000 0.010 0.012 0.009 _0.834 5.90 W 1.76 10.20 :1,. , .,.s T=,,,.. . , ,,;,,_ Lime App..
Current Cumulative.lbslacre 0.09 0.06 21.55 0.37 0.01 0.14 0.22 -0.13 2856 I47 , 50. Permit PAN Limt Ist12nd Crop Date Lbs1Ac
Prior Years Cumulative Ibsteere 0.08 0.05 21.11 0.36 0.01 0.13 0.21. 0.12 27_73 �.
Permit(CPLR.*:* .36 34 1338 267 15. NIA 374 89 2498'
"1 certify,underpenalty:of Iaw,that this document was prepared-under my direction or supervision in'aceordance with a system"_
designed to assure that'qualified'personnelproperly.gathered and evaluated the information submitted.1-arn.aware thatthtre are
significant penalties`forsubinitting false information,.including the possibility of fines and imprisonment for knowing violations."
X. j am,.-� ✓✓1.(�` L_2. *A lice io e od:� �Y� � �� pp t e M th S-Surface,IN-Jnjectioa;INC-Q�1C-Inc
(Signature of Land Applier) ' D e **Volatilization Rate:Surface.-O,S,Injection/Incorporation-1.0
***C.P:L.R.:CumuiativePolluiantLoading:Rate
DENR FORM,FSF(7/2002)Mod.
WMSS,PLLC

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name:Earner Environmental%Vaste&Manny Permit fi:W00018525 Annual Dry Tons Applied: 4.53
Owner: Will Turner Operator: Steve Barnes Cation Exchange Capacity(non 503):. 6:8
Site ff:\VT Field#: 2 Acres Utilized: 5.00 Acres Permitted: 5.00
Application Method*: S - Volatilization Rate**: 0.5 Mineralization Rate: 30 % Predominant Soil Series: GoA
0114 .tS a•:r•o-='ii=€ _::;:a: � :; :�:;�iiiie r���='i'i'i'i':=:: Sit==:a€=S:i:3:i:i:€: :''..:._:.:.•.,:
•-N dd s.ittr fi 1. IasT; �4
2021 10,500 2,I00 0.78 .0.07 AlIenlicStatinn G/D 0.000 0.000 .0.105 0.002 0.000 0.00I 0.002 0.001 0.183 031 2.49 Coastal 6.60 0.01 0.00
2021. 7,000 1,400 1.26 .0.07 Beaetins Reach G/D 0.000 0.000 _0.187 0:003. 0.000 0:001 0.0021_0.001 0.174 2.41 2:14 Coastal . 7:78 0.03 .0:06.
2021 14,000 2,800 1.40 .A.16 llamptom Suites O/D -0.001 0.000 .0322 0.001, 0.000. 0:002 _0.003 .0.002 0.286. 4.16 , .3.97 Coastai 13.81, 0 08 0.00
2021 7,000 1,400 0.50. 0.03 aune'r- c G/D 0.000 .0.000 .0.033 0.001 .0.000 0.000 0.000. :0:000 0.056 0.83 0.86 Coastal 2.75 0.00 0.00
2021 3,500 700 0.49 0.01. Genesis.C°adns GID 0.000 .0.000 0.016 0:000. '0.000. 0.000 0:000 0.000 0.034 157 0.27 Coastal , 1.89 0.02 0.00
2021 7;000 _ 1,400 0.59 0.03 Harker's P""t O/D 0.000 .0.000 0.034 0,002 0:000. 0.000 0.001 0.000 0.112 _ 020 1:45 Coastal _ 0.66 0.0I 0.00
2021 7,000 1;400 3.28 0.I9 Fektic.Beath O/D 0.001 0.000 .0.161 0.005. 0.000 0.002 0.004 0.002 0:547 0.93 _ 431 Coastal 2834 2.42 0:00
2021 3,500 700 175 0.02 Q°eEn56 0/13 0.002 .'0.002 0.016 0.002, 0.000 0.002 0.002 0.002 0.079 0:63 0.65 Coastal _ 1.97 0.00 0.04
2021 7,000 1,400 0.55 0:03. Se1S1Jt5y O/D .0.000 0.000 0.050 0.000 0.000 0.000 0.001 0.000 0.053 0.56 1.13 Coastal 2.25 0.01 0:00
2021 7,000 1,400 0.98, 0.06 Sp9Qd0f11osca G/D 0.000._0.000 0.095 0.002 0.000 0.001 0_001 0.001 0.154 1.00 I.92 Coasai 6.09 030 0.00
'Scul1iwintls
2021 7,000 1,400 .0.52 103 ,f ondnmmevms G/D 0.000 0.000 0_044 0.001 0.0000 0.000 0.001 0.000 0.080 0.72 • 0.91 Coastal 2_15 0.01 , 0.07
202I ..42.000 8,400 0_54 0.19 Su:mnerwinds G/D 0.001 0.000 0:245 0.003 0.000: 0.002 0.004 0.002 0.564 2.80 3.92 5.46 Coastal Rye 2124 0.29. 029
Total 122,500
Annual Ibs/aere 0.006 0.003 1308 0.022 0.001 0.012 0.020 0.011 2.321 15.13 3.92 25.56 Lime App.
Current Cumulative lbs/acre I.88 0.11 78.47 25.10 0.46 032 1.02 0.66 94.75 299 50 Permit PAN.Limt lst/2nd Crop Date Lbs/Ac
Prior Years Cumulative lbs/acre 1.87 0.10 71.16 25.08 0.46 0.31 1.00 0.65 .92.43
PermittC.P.L.11:`*'' 36 34 133E 267 15 N/A 374 89 2498
certify under penalty of law,that-this document was prepared.under My direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted:l aril awarelhat:thereare
significant:penalties for submitting false information,Including the possibility offines and imprisonment for knowing violations." J
X f` i_,(J i/ e, 02/l 2 - *Application Methad:�.S-Surface,IN-Injection,INC-Incpiporation
(Si attire.of Land Applier) r !!!Da **Volatilization]later.Surface=0,5,lnjection/lncorporation:-1.0.
***C-P.L,RL°Cumulative Pollutant Loading Rate
DENR FORM FSF(7/2002)M od.
WMSS,PU=C

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name:earner enhronlncnezl Wasic&'rowing Permit#W00018525. Annual Dry Tons:Applied: 9:17
Qsvner_' Will Turner Operator: Steve Barnes Cation Exchange Capacity,(non 503): .8.2
Site#:'WT Field#: 3 Acres Utilized: 8.00 Acres Permitted: 8.00
Application Method*: S Volatilization Rate**: 0.5. Mineralization Rate: 30 % Predominant Soil Series. GoA
2 :f€::-,14s[a€0- f1: i i `a f
_ ta .� fie: -
ilivjAwii _ _ _ �t�tiifin y-•?�Q•-siiiii
- 1 1 1 1 1 I I 1 1'; -��`L 1:'��Il���tom'1�1�
==�=� €�# ,...:2.. '� ..=�N.. .gq���€i:€4€ €1k : -:mt'€ i€€ liC'r.timi o]ai'r''� rt €kii : Of�►�'.1
2021 21,000 2,625 0.78 0.09 Atlantic Slab°° G/D 0_100 0.000 .0.131 0.002 0.000 10.001 0.002' 0.001 ,0.229 0.39 3.11 _Could 825_ 0.02 0.00+
2021 7,000 875 1,26 0.05. Bcaooes,Rtslch_G/D o".000 0:000 0-117 0.002 0.000 ;0.00.1 0.0.01 0.000 0.109 1.50. 114 Coastal 4.86 0.02 0:04
'2021. 10,500 I,313 1_78 '0;10 CCS GAD 0.004 .0.004 0.087 0.004 0.000 0.004 :0.004 0:004 0.094 1-50 .2.16 Coastal. 4.89 . 017 000
Cape Royal -
2021• 7,000• 875. 1.07_0.04_ ijolohm G/D 0.002" 0.002 .0:016 "0.002 0.000 .0.002 0.002 0.002, 0.048 oa0 0.44 Coastal 1;45 0.00 027
2021 10,500 1,313 0.72 .0.04. Cedor Pcctol G/D _0.005 0:005 0.030 0.005-0.000 ;0.005 0.005 0.005 0.071 1.04 1:25 Coastal 310 0.00 0,08
2021 3,500 :438 1.40 .0:03 .H2n1pto1lsuaa5 GM. 0.000 0.000 0.050 0.000 0.000 .0.000 0.000 0.000 0.045 0.65 - 0.62 Coastal 2.16 0.01 0.00
2021. 10.500 1,313 0.50 0.03 Dump° G/D 0.000 0.000 0.031 0.000. 0.000 0.000 0.000: 0.000 0.052 0,78 0.80 Coastal 2,58 0.00 0:00
2021 3,500 438 0.16 0;00 °ht 1/3 marina O/D 0:000' 0.000 .0.004 0.000 0.000 0.0001 0.000" 0.000 0:009 0.04 0.10 , Coosai 0.28 0:00 0.00
1bctirosc .
2021 I.7,500 2,188 ,0.86 0.08 vnirns G/D 0.000 0.000 0:014 0.000: 0:000 0.00] 0.00.1 :0.001 0.108. 2_67 2.18 Coated .8,75 021. 0.00
2021 7,000 875 0,75 0.03 'Qee3n Bav visas G/D 0.000 .0.000 0.016 0.001. 0.000 0.000 0.00.1 0.000 0.058 0.67 0:67 Coastal 2.22 0.01 0.00
2021 3,500 438 0.92 0.02 _ Qcean Club G/D 0.000 0.000 0.010 0:000 0:000 0:000 0,000. 0.000 0.057 0.08 0:72 Coastal 0.26 _0.02 0.00_
2021 21.000 2;625 3.22 036 l'ebblcEc2.91 G/D 0.002 0.001 0.302 0.009 0.000 0.004 0.008-0.004. 1:025 1.75 8.011 coastal.,_ 53:I4 4.54' 0.00
2021 10,500 1,313 0.79 0.04 Sands V]Oas O/D 0.000 0.000 0.027 0.001 0.000 0.000 0.604 0.000 0.127 _0.81 '131 Ccastat _ 2.68 0.01 0.00
202I 14,000 1,750 0.98 0.07' SoundOr7he'Stu O/D _0.000 0.000 0:119: 0.003 0.000 0.001 0.001 0.001. 0_192 1.25 2:40 .Coastal 7.61 0.37 0.00
2021 66;500. 8313 0.54 0.19 summer wi,14.1 G/D 0.001 0.000 0.242 0:003 0.000 0.002 0.004 0.002 0.558 6.65 5:41 Coastal . 21.02 029 0:29
Total 213,500,
-
Annual lbs/acre 0.016 0.013 1.196 0.034 0.001 0.022 0.035`0.011 2.783. 20.48 0.00 ` 30.58 ,:'1.. ..,-,-.,.,rx:...::.....:::� Lime App.
Current Cumulative Iln/acre _0.21 _0.41 63.57 1.00 0.01 0.26 0.67 0.23 68.85 299 50 ,Per•mit.PAN Limt 1st/2nd Crop Date Lbs/Ac
Prior Years Cumulative]bs/sere '.0.20 0.40 .62.37 097 _0.01 0.24 0.63 0.21 66.07
Permitt.C,,P:L,R.••.*. 36 34 133$ 267. 15 N/A 374 89 2498
"I Certify,under penalty of-law,that this documeetwas prepared under mydirection or supervision inaccordanec'cvith.a system
designed to:assure ihat qualified personnel-properly gathered and evaluated the arifotmationtsubmitted.1 ant aware that there are
significant penalties for submitting false iafoirnation,.Including the possibility of fines-and imprisonment for knowingviolat]ons:".
•
X. ti!.sLfr _/ L c:"2 f/2 •App[ication.Mtithod:S.=Surface,.IN-Injection,d+1C-incorporation
(Signature of]andAppller / Date **VolatilizatioinRate;:Surface-0.5,Injectionllncorporation-1:0
***C:P.L.IZ Cutnuiative Pollutant Loading Rate
DENR FORM F.SF(712002)Mod.
W MSS,-PLLC

ANNUAL LAND APPLICATION FIELD SUMMARY-FORM
Facility Name:BarnesEitvirenmentaIWnste&Hauling Permit#:%Vp0018525 Anneal Dry Tons Applied: .6.87.
Owner. Will Turner Operator: Steve Barnes Cation Exchange Capacity(non 503): 5.9
Site,h WT Field#: 5- Acres Utilized: 2.60 Acres Permitted: 2.60
Application Method*: S Volatilization Rate**: 0.5 Mineralization Rate: 30 % Predominant Soil Series: GoA
Afe3M'•'•'sgiW
.. 'WA:;i_ ..��t)eggs! ii t` "'°°iIii_<-':::g: - -
_ � .tea. ..�:.:�.;.�5�� � ..k'l�:Ij �rl�2 €=� )�-�� `�1:��?t 04p:.,7r €'s A1I3:,'$24i3
2021 7,1300 2,692 0.78 . 0.09 Mantle station G/D 0.000 0.000 0.134 0.002 0.000 0.001 0.002 0.001 0.235 020 020. 3.19 Coastal Rye 8:46 0.02 0.00
2021 28,000 1069 126. 037 Beaco,tsReuch G/D 0:003 0:001 1.442 "0,022 0.000 0.0I0_0114 0.006 1.337- 18.51 16.45 Coastal 59.88 0 23 0. 0
2021 . .7,000 2;692 1.78. •020 CCSass GID 0.009_0.009 0.179 0.009. 0.000 0.009 0.009 0.009 0_193- 1.54 134 4.44 Coastal Rye 10,03 034 0.00
Cape Royal
20213;500 1,346 1.07 '.0.06 Dolptun G/D _0.004‘_0:004 .0.024 0.004 0.000. 0,004 :0.004 0.004 0.074 1.08. 0.68 Ryc. 2.23 0.00 _0.41
Colony*.The
2021 6,500 2.500 1.56 ,'0.16 sea G/D 0.001 0.000 0.071 0.003 0.000 0.002 1004 0.002 03.11 186 3.31 4.97 coastal Rye. 23:37 0.80 0:00
2021 10,500 4,038 0.50._ .0.08 p"a 'Pa O/D, 0.000 0.000 0.094 0.001 0.000 0.001 0.00.1 0.001 0.1'61 2.39 2.47 Coastal 7.94 0.01 0.00
NC Aquaritua a!
2021 3,500 -1,346 L24 0.07 pine-Khan shares O/D 0.000 0.001 0.050 0.005 0.000 0.001 0.003 0.001. 0.119 1.74 . 3.82 Coastal _5.78 0.03 -0.00
2021. 21,000' 8,077 0.92 0.31. ocean Clab O/D 0.002 0.000 :0.193 0.006 0.000 0.003 .0.006 .0.003 1.049 1:30 0:26 13.29 coastal Rye 4.89 0.45 0.01
OCeaos.
2021 , 3,500 1,346 0.87 0.05 Candammiums G/D 0.000 0.000 0.065 0.002 0.000'•0.000 0.001. 0.000 0.160 0.10 2.29 Ccastat 4.5.1 0.08 0.00.
202I _ 3,506 , 7,000 _1.39 .0.41 Pine Knoll Towns G/D 0.002 9.001 0.471 0.008 0.000 0.004 0.009 0:004 1.212 12.54 12.00 Rye 41.49. 0.43 0.00
2021 3,500 1,346 1.97 .0.I.1 SaintEmerald'Vllla GAD 0.001 0,000. 0.157 0.016: 0.000 0.001 0.002 "0.001 0.491 3:5I , 2.93 Coastal 12.16 0.09 0.01 _
2021 10,500 4,038 0.75 :0.13. QQeemcaare .GID 0:012 '0.012 0.095 0.012 0.001 0.012 0.012,0:012 0.457 144 122 3.74 , Coastal Rye _1134 '0.00 0.25
_ 2021 , 14,000 5,385 134 030 Sea Isle Plantation Gip 0.002 0.001 .0.141_0.023 0.000 0..003 _0.009 0.003 0.790 _ 3.48 9.00 Coastal . 32.48 0.74 0.01
2021 7.000 2,692 0.54 0.06 Sum,ncrw•mds G/D 0.000 0.000 :0.078: 0.001 ,0,000 0.001 0.001 0.001 0.18I 2.15 1.75 Aye 6.81 0.09 0.09_
2021 3,500 -• 1,346 0.91 0.05. whaler fan. G/D .0.000 .0.000 0.088 0_001 0.000 0.001 0.001 0,001 0.109 0.50 2.37 Coastal 5.58 0.09 0.00
Total 132306
Annual lbs/acre 0.036 0.029 3.284 0.115 0.002 0.052 0.078. 0.047 7.078 39.56 22.30 83.38 : ' .,, ' l_,•,4. 1 Lime App
Current Cumulative lbs/acre 0.120 0.084 20.428 0:526 0.010 0.178 0329 0.167 32.249 299 50 t Permit PAN Limt lstl2nd Crop Date Lbs/Ac
Prior Years Cumnlativclbs/acre 0.084 0.055 I7.145 0.411 0.008 0.126 0.252: 0.120 ,25.171
Permitt C P.LR.*** 36 . 34 1338 267 15 N/A 374 89 2498.
"I certify,under penalty of law,:thatthis docurnent was prepared under my direction or Supervision in accordance:with asystem
designed to assure that qualified personnel properly gathered and evaluated the.mformation submitted.I am aware drat there are
significant penalties for submitting.false information,including the possibility of fines and'iniprisuiutient for knowing violations." -
X -12-1-- /' L lityuk-49, t /7 G -z. *Application Method:S-Surface,IN-injection,114C:-Incorporation
(Signature.of Land.Applier) Da **Volatilization Rate:Surface-0.5;lnjectioti/lncorporation-1.0
***C:P_L R_:Cumulative Pollutant.Coading Rate
DENR FORM FSF(712002)Mod.
WMSS,PLLC

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Facility Name:Barnes Envvonmenmstvr::eae1t'aoHeir ,Permit ft:W00018525" Annual Dry Tons Applied: 6.43
Owner: Will Turner Operator. Steve Barnes Cation Exchange Capacity(non 503): 6.7
Site ft:WT Field#: 6 Acres Utilized: 2.90 Acres Permitted: 2.90
Application Method*: S Volatilization Rate"": 0S Mineralization Rate: 30 % Predominant Soil Series: GoA
.ig Si t!'i flEi�iiiif:a�3e€ii= S€:E:�EiKtftls=•li"�� - -
L�4iC €€'•,E;Ca s>....:Acss. .i� ;�x\r .S�iii'+Fei '•, `zs .''.,
Via'=:� € €s€ ::�u::s7e�'€�?=3i7 - - -
ilifiiiiiiliiii
- .r- - ,,. :.�ti �: '.: =�5>r€�€;�h€�f1'i`il!i:1E •P�kt'k2 E�� � € 0rup_1¢ Gi•`s'i��I �CI�`:':iti193; "ice
2021 10,500 3,621 0.78 0.12 Athunicsusion O/D 0.00] 0.000 0.180 0.003 0.000 0.001• 0.003 0.00.1 0.316 0.54 4.29 .Coastal 11.38 0.02 0.00
2021 21,000 , 7,241 , 1:26 0.38 Beacom Reach GOD 0,002 :0.001 0.969 0.014 0.000. 0.007 0_009 0.004 0.899 12,44 11.06 •.Ctiasta! 4026 0:'15 0.34
2021 _ 7.,000 2,414 .0.50 0.05 Aanemeape _Glp 0.000 0:000 0.056 0.001 0.000, •Q,001_ 0.001 0.001 0.096 1.43 , 1:48 ^Coastal _ 4.75 0,0] :0.00
2021 21,000 7,241. 3.28 0_99 Pebble uieh G/D 0.005 0.002 0:832 0.026 0.000 0.010. 0.022 0.010 2.827 2.41 2.41 . 22.29 Coastal Rye 14b39 ]2.53' 0.01
K rune nell •
-
2021 3;500 7.000 139. :0.41 Townes G/D 0.002 0:001 0.47.1. 0:008_1000. 0.004" 0.009 0.004 1.212 1254- 12.00 Rye _41.49 0.43 0.00
2021 3,500 1,207 0:75 :0114 QueensCovrt GiD 0.003 .01103; 0.028- 0:003 0:000 :0.003 0.003 0,003 0.137 1.09 1,12 .• Rye 3:39 0,00 0.08
2021 10,500 3,621 0.55 .0,08 scasprw 010 0.000 Q.000 0.128 0.001 0.000 0.001 0.002 0.001 0.136 1:45 2.92 Rye 5.81 0,01 0.00
soutLwutds i ,
202] 14,000 4,828 0,52 .0,10 _Coodonuniunis O/D 0.001 0.000' :0.153 0.002 0.000 0.00I 0.002 0:001 .0.277 2.48 , _. 3.14 coastal 740 0.02 026
2021 3,500 1,207 0.91 0.05 whe.rlon G/D -0_000 0.000 0.079' 0.001 0:000 0.001 0.001 0.000 _0,098 . 0:45 2.12. Coasts 5,01 0.08" 0.00
Total 194,500
'
Annuallbslaere '0:0155, 0.007 2.897 0.060 0.001 0.028. 0.052 0.025 5-997 19.74 17.49 604I :'.' ,',r,, Lime App.
Current Cumulative Ibslaere •0.103 0.058 25.365 0.580 0.010 .0.171 0.382 0.181 40.015 299 50 PermitPANLimt 1st/2nd Crop Date,Lbs/Ac
Prior Years CumuIativelbs/acre 0.088 0.051 22.468 0.520 0.009 0.142 .0.330" 0.156 34.018
Permitt.0 P L.11.***, 36 34 1338 267 15 NIA 374 .89 .2498
"1 certify.under penalty of law,that this-document.was:prepared under my direction or supervision in.accordance with"a system _
designed to.assure thatqualified personnel ptoperlygathered and evaluated the information submitted.l,amaware that there ate
significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
X "`�`/r''ii• [1'4Z�' J jat_u *Application Method:S--Sitar]ace,RV-Injction,D C-lnoatporation
re:afl.and Applier) ate **Volatilization Rate:Surface-Q.5,Injectionlhtcorporatign-1.0
•**C:I'.L.R.:Cumulative Pollutattt Loadirig.Rate
DENR FORM FSF(7/2002)Mod.
1NMSS;PLLLC

SOIL ANALYSIS REPORTS

Page 1 of 2
Report Number: 22-024-1380
Account Number:08361 Waypoi nt.w 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: Willcox&Mabe Soil Solutions, PLLC ANALYTICAL www.waypointanalytical.com
7231 B. Summerfield Rd "Every acre...Every year.". Grower: Steve Barnes
Summerfield NC 27358 WMSS Job No. 15+-02
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 SMP Buffer pH Loss On Ignition Water pH
Date Received: 01/24/2022 Date Of Analysis: 01/25/2022 Date Of Report: 01/25/2022
OM W/V ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0
Sample ID Lab % Soil M3 K
Field ID Number lbs/A Mg Ca Na Soil Buffer H
Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index megl100g meg11o0g
WRT-01 22809 1.1 70 232 VH 42 L 31 H 164 L 11 L 5.4 6.88 0.5 1.7
L NC=193 NC=21
WRT 02 22810 2.3 94 133 VH 13 VL 28 M 194 M 16 M 5.6 6.89 0.4 1.7
L NC=111 NC=7
WRT-03 22811 8.2 150 623 VH 29 VL 144 L 2650 H 35 VL 6.5 1.2 15.9
VH NC=519 NC=15
WRT-05 22812 2.3 83 472 VH 39 VL 84 L 1514 H 26 VL 6.5 0.7 9.2
L ! NC=393 NC=20
WRT-D6 22813 I 1.7L I 1 79 114
=VH
9 , 15C=SL I 44 M 1 476 M I 20 L 1 6.0 + 6.88 (I I 0.5 1 3.4
Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts
Sample ID
Field ID K Mg Ca Na H NO3 N S Zn Mn Fe Cu B SS
% % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate
WRT-01 6.3 15.2 48.2 2.8 29.4 9 VL 2.1 L 2 VL 176 VH 1.7 H 0.2 VL
NC=19 NC=52.5 NC=13 NC=85.0
WRT-02 ' 2.0 13.7 57.1 4.1 123.5 13 L 2.9 M 1 VL 367 VH 5.5 VH 0.2 VL r
NC=27 NC=72.5 NC...6 NC=275.0
WRT-03 0.5 7.5 83.3 1.0 7.5 17 M 77.8 VH 4 L 300 VH 45.8 VH 1.8 H
t NC=35 NC=1945.0 NC=25 NC=2290.0
WRT-05 1.1 7.6 82.3 1.2 7.6 25 M 56.0 VH 4 L 178 VH 17.0 VH 0.6 M
NC=52 NC=1400.0 NC=25 NC=850.0
WRT-06 1.1 10.8 170.0 I 2.6 114.7 16 =33 NC63650 NC=gVLI 179 VH I 4.4 VH 200I 0.4 L r
NC Values on this report represent the plant available nutrients in the Explanation of symbols:%u(percent),ppm(parts per million),lbs/A This report applies to samples)tested.Samples are retained a
soil.Rating after each value:VL(Very Low),L(Low),M(Medium), (pounds per acre),ms/cm(milli-mhos per centimeter),meg1100g maximum of thirty days after testing. pp
H(High),VH(Very High).ENR-Estimated Nitrogen Release. (milli-equivalent per 100 grams).Conversions:ppm x 2=tbs/A,Soluble by: Taw( Mr frrod
Analysis prepared by:Waypcint Analytical Virginia,Inc.
C.E.C.-Cation Exchange Capacity. Salts ms/cm x 640=ppm.
Pauric Mc Ornery Ph.D.,CPAg

Page 2 of 2
Report Number: 22-024-1380 ,Y1f
FAO
.
Account Number:08361 poi nt." 7621 Whitepine Road,Richmond,VA 23237
Main 804-743-9401°Fax [phone]
Send To: Willcox& Mabe Soil Solutions, PLLC ANALYTICAL www.waypointanafytical.com
7231 B.Summerfield Rd "Every acre...Every year."1., Grower: Steve Barnes
Summerfield NC 27358 WMSS Job No. 15+-02
Date Received: 01/24/2022
Date Of Report: 01/25/2022 SOIL FERTILITY RECOMMENDATIONS
Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron
Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B
Field ID bu Tons/A
lb/A lb/A lb/A lb/A lb/A lb/A lb/A i lb/A lb/A Ib/A
WRT-01
Soybeans 45 0.8 15 0 95 19 11 3.0 4 0 0 1.0
WRT-01
Corn 125 0.8 153 0 122 19 22 2.4 6 0 0 1.5
WRT-02
Bermuda,Coastal 5 0.8 75 0 467 21 22 0 4 0 0 0.5
WRT-03
Bermuda,Coastal 5 0.0 75 0 500 0 17 0 3 0 0 0
WRT-05
Bermuda,Coastal 5 0.0 75 0 492 0 9 0 3 0 0 0
WRT-06
Bermuda,Coastal 5 0.5 75 0 483 14 19 0 4 0 0 0.5
Comments:
"The recommendations are based on research data and experience,but NO GUARANTEE or WARRANTY expressed or implied,concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„and may not be reproduced in whole or part,nor may any reference be made to the 1 tutri r pie 6,,,m
work,the results,or the company In any advertising,news release,or other public anouncements without obtaining our prior written authorization.Copy right 1977. 44
Pauric Mc Groary Ph.D.,CPAg