WQ0012346_Residual Annual Report 2021_20220203

Non -Discharge Branch Upload/Submittal Form
NORTH CAROLINA
En.anmemfal Qualify
Version 2 - Revised June 23, 2020
Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?*
Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0012346
Applicant/Permittee US MCB Camp Lejeune
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office
CO Reviewer
Admin Reviewer
Wilmington

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name*
Travis Voorhees
Email Address*
[e-mail]
Project Information
Application/Document Type *
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
910-451-9518
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Permit Number: *
Applicant/Permittee Address*
Facility Name*
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
WQ0012346
Has Current Existing permit number
High -Rate Infiltration
Reclaimed Water
Residuals
Other
Commanding General Attn: EMD 12 Post Lane Camp Lejeune, NC 28547-2540
US MCB Camp Lejeune Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2021 NCDEQ Class A Residuals Application Annual
Report.pdf
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
7.08MB
By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/3/2022

CLASS "A" WASTEWATER RESIDUALS
APPLICATION ANNUAL REPORT
YEAR 2021
,.,t,•
UNITED STATES
MARINE CORPS BASE
CAMP LEJEUNE, N. C.
PERMIT NO. WQ0012346

CLASS "A" WASTEWATER
RESIDUALS APPLICATION ANNUAL
REPORT FOR THE YEAR 2021
MARINE CORPS BASE, CAMP
LEJEUNE PERMIT NO. WQ0012346
• Cover Letter SECTION 1
• Class A Annual Distribution and Marketing/Surface Disposal SECTION 2
Certification and Summary Form (Form DMSDF)
• Annual Residuals Sampling Summary Forms
(Forms RSSF & RSSF-B) SECTION 3
• Residuals Analysis Lab Sheets including TCLP Lab Sheets SECTION 4
Annual Pathogen & Vector Attraction Reduction Forms • SECTION 5
(Form PVRF 2T) and Vector Attraction Reduction Lab Sheets

144;
Application to Forested Sites
Camp Lejeune Advanced Wastewater Treatment Plant
ATAD Facility
Application to TLZ Training Areas
Transferring Biosolids from Tanker to Applicator

SECTION 1
Cover Letter

UNITED STATES MARINE CORPS
MARINE CORPS INSTALLATIONS EAST -MARINE CORPS BASE
PSC SOX 20005
CAMP LEJEUNE NC 28542-0005
5090.20.1
G-F/BEMD
FEB 0 2 2022
Mr. Nathaniel Thornburg
North Carolina Department
of Environmental Quality
Division of Water Resources
Non -Discharge Permitting Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Dear Mr. Thornburg:
In accordance with requirements of 15A NCAC 02T, the
enclosure forwards Marine Corps Base Camp Lejeune's (MCB CAMLEJ)
Class "A" Wastewater Residuals Annual Application Report for
calendar year 2021. The forms in this report were prepared by
Charles "Sonny" Scozzari, MCB CAMLEJ Wastewater and Land
Application Supervisor, for the Permittee Robert A. Lowder,
Director, Environmental Management Division (EMD).
If you have any questions please contact Mr. Travis
Voorhees, Environmental Quality Branch, EMD, at [phone].
ROBEA LOWDER P.E.
Director, -• onmental Management
By direction of
the Commanding General
Enclosure: MCB CAMLEJ's Class "A" Wastewater Residuals Annual
Application Report Year 2021
Copy to:
File (ODI #26695)

SECTION 2
Class A Distribution & Marketing/Surface
Disposal Certification & Summary Forms
(Form DMSDF)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0012346 FACILITY NAME:
PHONE: [phone] COUNTY: ONSLOW
FACILITY TYPE (please check one): r❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A, B, and C)
US MCB Camp Lejeune AWWTP
OPERATOR: Charles "Sonny" Scozzari
Vas the facility in operation during the past calendar year? Yes 0 No L] -0. If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
anuary
CAMLEJ AWWTP NC0063029
0
'ebruary
CAMLEJ AWWTP NC0063029
0
?larch
CAMLEJ AWWTP NC0063029
27.83
►pril
CAMLEJ AWWTP NC0063029
78.84
day
CAMLEJ AWWTP NC0063029
52.05
une
CAMLEJ AWWTP NC0063029
27.42
my
CAMLEJ AWWTP NC0063029
31.93
►ugust
CAMLEJ AWWTP NC0063029
37.98
teptember
CAMLEJ AWWTP NC0063029
37.7
)ctober
CAMLEJ AWWTP NC0063029
6.75
iovember
CAMLEJ AWWTP NC0063029
14.89
)ecember
CAMLEJ AWWTP NC0063029
8.4
Total from FORM DMSDF (sup)
0
0
0
0
'otals: I
Annual (dry tons):
0
323.79
0
0
Amendment(s) used: 0
Bulking Agent(s) used: 0
DMSDF (Supp)
If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form
'art C:
'acility was compliant during the past calendar year with all conditions of the land application permit p Yes
including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No -IP. If No, Explain in Narrative
. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
. No contravention of Ground Water Quality Standards occurred at a monitoring well.
1 certify, under penalt f law, that the above information is, to the best of my knowledge and beli , r e, accurate and complete. 1 am aware that there are significant
len : ' s for submittin fa information, including the possibility of fines and imprisonment for/Cnowg violations."
,ignure
"Preparer is define
art 503.9(r) and 15A NCAC 2T .1102 (26)
1
Sig ure of Preparer**
(if fferent from Permittee)
ate

Landfill Load Receipts
Load Date
Load Time
Sludge
5/12/2021
5/13/2021
5/17/2021
5/18/2021
5/19/2021
5/20/2021
5/21/2021
5/24/2021
5/25/2021
5/26/2021
5/26/2021
5/27/2021
5/27/2021
5/28/2021
6/1/2021
6/2/2021
6/2/2021
6/3/2021
6/10/2021
6/21/2021
6/22/2021
6/23/2021
6/24/2021
6/25/2021
6/28/2021
6/29/2021
7/1/2021
7/6/2021
7/9/2021
7/23/2021
7/26/2021
7/27/2021
7/28/2021
7/29/2021
7/30/2021
8/2/2021
8/3/2021
8/5/2021
8/6/2021
8/9/2021
8/19/2021
8/23/2021
8/26/2021
31,120
42,660
31,260
30,620
32,100
30,860
30,740
31,340
32,320
31,860
3 2, 400
33,400
17,060
23,480
33,380
31,560
32,100
32,080
18,880
31,620
3 2, 600
32,560
34,160
30,840
25,040
28,300
31,220
22,600
27,560
28,560
32,340
3 2, 360
3 2, 540
32,740
34,000
33,400
34,780
32,300
29,240
26,760
28,340
29,000
26,520

8/27/2021
9/1/2021
9/7/2021
9/7/2021
9/8/2021
9/9/2021
9/13/2021
9/15/2021
9/16/2021
9/16/2021
9/17/2021
9/17/2021
9/21/2021
9/23/2021
9/27/2021
10/12/2021
10/13/2021
10/15/2021
Total Pounds
Tons, Wet
Total Gallons
Yearly Solids
Tons, Dry metric
25,220
27,900
30,520
34,460
30,660
29,080
3 2, 600
33,960
30,380
30,520
31,260
27,040
28,640
30,740
29,400
30,640
31,720
28,180
1,851,520
925.76
3,000,000
3.12
390.31

BIODYNAMIC VOLATILITY ENHANCEMENT LOG
WT-310CS SWEET CANE SYRUP
(SUGAR WATER)
TRAIN 1
TRAIN 2
TRAIN 3
TRAIN 4
DATE
A/B
AMOUNT
DATE
A/B
AMOUNT
DATE
A/B
AMOUNT
DATE
A/B
AMOUNT
2/17/2021
T1B
250 GAL
1/8/2021
T2B
250 GAL
1/14/2021
T3B
250 GAL
1/8/2021
T4B
250 GAL
1/13/2021
T2B
125GAL
2/4/2021
T3A
250 GAL
1/13/2021
T4B
125 GAL
4/27/2021
T2A
250 GAL
2/17/2021
T3B
250 GAL
5/20/2021
T4A
250 GAL
10/7/2021
T2B
250 GAL
10/18/2021
T3B
250 GAL
5/20/2021
T4B
250 GAL
10/26/2021
T2A
250 GAL
10/26/2021
T3B
250 GAL
9/29/2021
T4A
125 GAL
11/12/2021
T2A
250 GAL
9/29/2021
T4B
125 GAL
11/12/2021
T2B
250 GAL
10/7/2021
T4B
250 GAL
11/3/2021
T4B
250 GAL

SECTION 3
Annual Residuals Sampling Summary Forms
(Forms RSSF & RSSF-B)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ00I2346
Laboratory: 1) EMD, ELS
Facility Name: US MCB CAMP LEJEUNE 2) Environmental Chemists, Inc.
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
NC0063029
Camp Lejeune Advanced WWTP
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
(mg/kg)a
Sample or Composite Date
1.'4/21
4.`6/21
7 13/21
10. 5/21
Percent Solids (°•o)
NA
3.62
3.67
2.67
4.85
Arsenic
75
29.3
18.1
34
11.7
Cadmium
85
<13.3
-=13.4
<17.5
.-10.2
Copper
4,300
331
289
352
359
Chromium
NA
23.I
21.7
24.9
21.9
Lead
840
18.8
16.6
20.8
14
Mercury
57
<0.445
= 0.469
<0.603
<0.344
Molybdenum
-5
<13.3
- 13.4
<17.5
<10.2
Nickel
420
16.7
14.5
<17.5
16.5
Selenium
100
'::13.3
• .13.4
<17.5
:.10.2
Zinc
7,500
1530
1340
1730
1480
_
Total Phosphorus
NA
46300
52000
54500
55800
TKN
NA
55700
45900
60700
48700
Ammonia -Nitrogen
NA
23900
20900
35600
22300
Nitrate and Nitrite
NA
198
11
1.87
0.81
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty w, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualifi d per i nnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for suljmi ng < Ise information, including the possibility of fines and imprisonment for knowing violations."
v
Signature of �fj eparer
//yr/z�
�Uate
*Preparer ig/defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0012346
Facility Name: US MCB CAMP LEJEUNE
Residual Source
NPDES # or WQ#:
NC0063029
WWTP Name: Camp Lejeune Advanced WWTP
Residual Analysis Data
Laboratory: 1) EMD, ELS
2) Environmental Chemists, Inc.
3)
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
1'4/21
4:6. 21
7:' 13/21
10; 5/21
PAN
21700
19800
25300
19100
SAR
0.61
0.58
0.56
0.47
Aluminum
74800
66800
67800
63100
Calcium
55900
45000
61800
73300
Magnesium
2380
2220
3730
3240
Potassium
3260
3410
5540
3630
Sodium
2870
2450
3250
2160
pH
8.32
7.88
8.3
7.66
Nitrite Nitrogen
60.4
119
<26.9
4.66
Nitrate Nitrogen
137
<0.545
1.88
<0.41
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that . ified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penaltiesi ; mitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Pre
*Preparer is
t
med in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
,�t�a

SECTION 4
Residuals Analysis Lab Sheets
including TCLP Lab Sheets

TCLP Analysis Lab Sheets

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention:
Revised Report: Jan 28, 2021
Original Report Date: Jan 18, 2021
Report #: 2021-00063
Customer ID: 12060026
Project ID: Crom Tank
Lab ID
21-00132
Test
Sample ID:
Site: CRAM Tank
Method
Collect Date/Time Matrix Sampled by
1/4/2021 9:55 AM Solid/Sludge Client
Results
Date Analyzed
Total Solids (%)
lgnitability
Chlordane (TCLP)
Endrin (TCLP)
Heptachlor (TCLP)
Heptachlor epoxide (TCLP)
Lindane (TCLP)
Methoxychlor (TCLP)
Toxaphene (TCLP)
1,4-Dichlorobenzene (TCLP)
2,4,5-Trichlorophenoi (TCLP)
2,4,6-Trichlorophenol (TCLP)
2,4-Dinitrotoluene (TCLP)
Cresol (TCLP)
Hexachloro-1,3-butadiene (TCLP)
Hexachlorobenzene (TCLP)
Hexachloroethane (TCLP)
m + p-Cresol (TCLP)
Nitrobenzene (TCLP)
o-Cresol (TCLP)
Pentachlorophenol ;TCLP)
Pyridine (TCLP)
2,4,5-TP (TCLP)
2,4-D (TCLP)
1,1-Dichloroethylene (TCLP)
1,2-Dichloroethane (TCLP)
SM 2540 8
SW 846 method TWO
S W 846 Method 8081 BI3510
SW 846 Method 80811313510
SW 846 Method 6081 B/3510
SW 846 Method 8081B/3510
5 W 846 Method 8061 BI3510
SW 846 Method 8081B/3510
SW 846 Method 8081B/3510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW 846 me:hod 6270/3510
SW 846 me:hod 8270/3510
SW 846 meted 8270/3510
SW 846 melhod 827013510
SW 846 melhod 6270/3510
SW 846 melhod 8270/3510
SW 846 melhod 8270/3510
SW 646 melhod 6270/35T0
SW 846 melhod 827613510
SW 846 method 8270/3510
SW 846 method 8270/3510
SW846 Method 8151A
SW846 Method 8T51A
SW848 Method 8260/5030
SW646 Method 8260/5030
3.39% 01/05/2021
> 185 °F 01 /15/2021
<0.02 mg/L 01/08/2021
<0.0005 mg/L 01/08/2021
<0.0005 mg/L 01/08/2021
<0.0005 mg/ 01/08/2021
<0.0005 mg/L 01/08/2O21
<0.0005 mg/L 01/08/2021
<0.05 mg/L 01/08/2O21
<0,050 mg/L 01/06/2021
<0.050 mg/L 01/06/2021
<0.050 mg/L 01/06/2O21
<0.050 mg/L 01/06/2021
<0.050 mg/L 01/06/2021
<0 050 mg/L 01/06/2021
<0.050 mg/L 01/06/2021
<0.050 mg/L 01/06/2021
<0.050 mg/L 01/06/2021
<0.050 mg/L 01/06/2O21
<0.050 mg/L 01/06/2021
<0.250 mg/L 01/06/2021
<0, 050 mg/L 01/06/2021
<0.003 mg/L 01/07/2O21
<0.003 mg/L 01/07/2021
<0.1 mg/L 01/14/2021
<0.1 mg/L 01/14/2O21
Report 4 2021.00063 Page 1 of 2

Environmental Chemists, Inc.
envirochem
SM,
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5843 Lab/Fax
[e-mail]
erwironmentalchernists,com
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Revised Report: Jan 28, 2021
Original Report Date: Jan 18, 2021
Camp Lejeune NC 28547 Report#: 2021-00063
Attention Customer ID: 12060026
Project ID: Crom Tank
Benzene (TCLP)
Carbon Tetrachloride (TCLP)
Chlarobenzene (TCLP)
Chloroform (TCLP)
Methyl ethyl ketone (TCLP)
Tetrachloroethylene (TCLP)
Trichloroethylene (TCLP)
Vinyl Chloride (TCLP)
RC!
Cyanide
Sulfide
pH
TCLP Metals
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Sliver
Mercury
SW846 Mehod 8260/5030
SW846 Method 8260/5030
SW846 Method 628015030
SW846 Melhod 8260/5030
SW846 Melhod 8260/5030
SW846 Melhod 8260/5030
SW846 Melhod 8260/5030
SW846 Melhod 8260/5030
SM 4500 CH D
SM 4500 S D
SW 846 Method 90450
EPA 200 7
EPA 200.7
EPA 200 7
EPA 200 7
EPA 2907
EPA 200 7
EPA 200 7
EPA 295.1
<0,1 mg/L 01/14/2021
<0.1 mg/L 01/14/2021
<0.1 mg/L 01/14/2021
<0.1 mg/L 01/14/2021
<0.1 rng/L 01/14/2021
<0.1 mg/L 01/14/2021
<0.1 mg/L 01/14/2021
<0.1 mg/L 01/14/2021
1.19mg/kg 01/21/2021
0.36 mg/kg 01/25/2021
8.18 units 01/19/2021
<1.0 mg/L 01/08/2021
<1.0 mg/L 01/08/2021
<1.0 mg/L 01/08/2021
<1.0 mg/L 01/08/2021
<1.0 mg/L 01/08/2021
<1.0mg/L 01/08/2021
<1.0 mg/L 01/08/2021
<0.0002 mg/L 01/08/2021
Comment: Revised to add trichlorethylene, cyanide, sulfide and pH.
.1 i;r
Reviewed by: --74r, -7'- -,— /
Report # 2021-00063 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client:\5W'
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Date: (Xi Report Number: Da I 006 (
'Receipt of sample: ECHEM Pickup Client Delivery 0 UPS • FedEx ❑ Other ❑
❑ YES
'❑ NO
t N/A
I.ere custody seals present on the cooler?
❑ YES
0 NO
N/A 2. if custody seals were present, were they intact/unbroken?
L
Original temperature upon receipt s : °C orrected temperature upon receipt °C
How temperature taken: 0 Temperature Blank Against Bottles
fR Gun ID: Thomas Traceable 5/N 192511657 fR Gun Correction Facttar °C: 0.0
❑ YES
0 NO 3. if temperature of rooter exceeded 6°C, was Project Mgr_/CI.A notified?
YES
~
0 NO 4. Were proper custody procedures {relinquished/received) followed?
YES
❑ NO 5. Were sample ID's listed on the COC?
YES
❑ NO 6. Were samples !D's fisted on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
YES
YES
❑ NO
❑ NO
10. Did samples arrive in good condition for each test?
11. Was adequate sample volume available?'
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were add preserved samples received at a pH of.z2? *
O YES
❑ NO
14. Were cyanide samples received at a pH >12?
O YES
❑ NO
15 Were sulfide samples received at a pH >9?
O YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 mil.? *"
O YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO 18. Were orthophosphate samples filtered in the field within IS minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
`* Bacteria samples are checked for Chlorine at time of analysis and recorded on the henchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H5O4 HNO3 HCI NaOH
Time of preservation: if more than one preservative is needed, notate in comments below
Note Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NGDENR_ ❑WQ CERTIFICATION # 94 NCOHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT: Commanding General
PROJECT NAME: Camp Lejeune MCB
REPORT NO: 016— 0001e3
ADDRESS: G-F/EMD/EQB/Environmental Lab
CONTACT NAME: Alberta Y. Okamoto
PO NO:
12 Post Lane
REPORT TO: Lauren Acosta
PHONE/FAX: [phone] (fax) 910-451-7195
Camp Leietsne, NC 28547
COPY TO:
a;hena okarnotnausrac mil
email: linif r- iaysmervi c[1anlr detanevMussr mL
Sampled Bv: L. -AO
SAMPLE TYPE: i = Influent, E = Effluent, W = Well. ST = Stream, SO = Soil, SL = Sludge, Other:
Sample
Collection
a
E T
en
m
o g
c
Container
(Pore)
o
r.
"
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
`
Identification
Date
Time
Temp
r
x
u
*
E;0
x
$
o
x
g
CR011
TANK 5
OLL
.r}' 55
C
P
/3
TCLP Volatile. Semi-vclat ii e,
lestacides, herbicides.
G
G
C
P
RCRA i8 metals)
G
G
r'
P
-teactivity, Corrosivity,
Tgnir;Abiliry
G
, �'
C
P
G
G
G
P
1
G
G
C
P
G
G
+
C
P
G
G
C
P
J
1
-
G
G
C
P
l
G
G
C
P
_
G
4 G
Transfer
Relinquished By: _
Date/Time
Received By:
DatetTiime
�{.
!
-�•J"_]r-: � � r.ri�a� 1 s.�f -I,. 1' Z1 t
1Refrigerator
2.
RefrigerptoL
I.
Temperature when Received:
Accepted:
Delivered By: Received By"
Comments:
ed: Resample
Date:t
e•uested:
n-D Time: j
TURNAR UND:
114ezr

1ST QUARTER
Residuals Analysis lab Sheets

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client: FC Wastewater Date of Report: Feb 18, 2021
Date Collected: Jan 04, 2021 Report No.: 2021-1-RESIDUALS
Date Received: Jan 04, 2021 Lab ID: 227, 94
Sample: Quarterly Sludge
Sample ID: CROM
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
pH
8.32
SU
01/04/2021
SM 4500 H+ B
ELS
Nitrate
Nitrogen
See Attached
Envirochem
Sludge
Residuals
See Attached
Envirochem
Certified By:
LAUREN D. ACOSTA

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
Date of Report: Jan 18, 2021
Customer PO #:
Customer ID: 12060026
Report #: 2021-00057
Project ID: Camp Lejeune MCB
Lab ID
21-00124
Test
Sample ID:
Site: CROM Tank
Method
1/4/2021
Collect Date/Time Matrix Sampled by
Solid/Sludge Rubert E
Results
Date Analyzed
PAN
Used 30% Mineralization Rate.
SAR
Nitrate Nitrogen (calc)
Nitrite Nitrogen
Nitrate Nitrogen
Sludge Residuals
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Nitrate+Nitrite-Nitrogen
Total Solids (%)
pH
Ammonia Nitrogen
Total Kjeldahl Nitrogen (TKN)
Calculation
Calculation
EPA 353 2
Subtraction Method
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 353.2
SM 2540 B
SM 4500 H B
SM 4500 NH3 C
SM 4500 Org B
21700 mg/kg
0.610
01/14/2021
01/14/2021
60.4 mg/kg 01/05/2021
137 mg/kg 01/14/2021
74800 mg/kg 01/12/2021
29.3 mg/kg 01/12/2021
<13.3 mg/kg 01/12/2021
55900 mg/kg 01/12/2021
23.1 mg/kg 01/12/2021
331 mg/kg 01/12/2021
18.8 mg/kg 01/12/2021
2380 mg/kg 01/12/2021
<13.3 mg/kg 01/12/2021
16.7 mg/kg 01/12/2021
3260 mg/kg 01/12/2021
<13.3 mg/kg 01/12/2021
2870 mg/kg 01/12/2021
1530 mg/kg 01/12/2021
198 mg/kg 01/08/2021
3.62 % 01/05/2021
8.16 units 01/15/2021
23900 mg/kg 01/05/2021
55700 mg/kg 01/05/2021
Report # : 2021-00057
Page 1 of 2

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
Date of Report: Jan 18, 2021
Customer PO #:
Customer ID: 12060026
Report #: 2021-00057
Project ID: Camp Lejeune MCB
Total Phosphorus
Mercury
SM 4500 P F
SW846 74718
46300 mg/kg
<0.445 mg/kg
01/12/2021
01/08/2021
Comment: Results, except pH and SAR, reported on a dry weight basis. pH and SAR reported on an as
received basis.
Reviewed by: L
Report # • 2021-00057 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
Client: usmc aPtir0 aUNk.Date: I al
Receipt of sample: ECHEM Pickup k Client Delivery 0
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Report Number:02 l 0oO 5 y
UPS 0 FedEx 0 Other 0
.4 N/A 1. Were custody seals present on the cooler?
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt Ai— °C Corrected temperature upon receipt
❑ YES
0 YES
❑ NO
❑ NO
°
How temperature taken: • Temperature Blank IX Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
• YES
• NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
• NO
4. Were proper custody procedures (relinquished/received) followed?
YES
■ NO
5. Were sample ID's listed on the COC?
IV YES
• NO
6. Were samples ID's listed on sample containers?
iN YES
• NO
7. Were collection date and time listed on the COC?
pir YES
• NO
8. Were tests to be performed listed on the COC?
&I' YES
• NO
9. Did samples arrive in proper containers for each test?
(f YES
■ NO
10. Did samples arrive in good condition for each test?
YES
• NO
11. Was adequate sample volume available?'
RI YES
• NO
12. Were samples received within proper holding time for requested tests?
• YES
• NO
13. Were acid preserved samples received at a pH of <2? *
• YES
• NO
14. Were cyanide samples received at a pH >12?
• YES
• NO
15. Were sulfide samples received at a pH >9? •
• YES
• NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
• YES
• NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
• YES
• NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

C
z
7J
0
C
z
Transfer Relinquished By: Date/Time _ Received By: Date/Time
1.
?� k,� e f -4) !-= : ,-, e j . ur »-t -, l4 0W Refrigerator .
2. Refrigerator 0 v
x
C
3
vw..
Sample Identification
0
0'
o
m
0,
o,
0
-I
v
w
L-1
8Type
Sample
G)
O
G)
C)
G)
O
G)
O
G)
C)
G)
O
G)
O(
0
t 1
O
Composite
or
Grab
0
-0
00"0
-13
G)
-0
0-0
0-0
O
-0
Container
(P or G)
Chlorine
mgIL
LAB ID
NUMBER •
>4
NONE
PRESERVATION
HCL
H2SO4
HNO3
NAOH
THIO
OTHER
ro
u J , v .. , 16L a
hosphorus, Calcium, SAR,
PKN, Total Solids/Soils &
1 �1 A 1
Mercury Sludge, Nitrite,
Qirrale, TQi rrarP-mitritA,
vicxl, Y0La551um, Sodium,
"elenium, Zinc,
4agnesium, Molybdenum,'1
aluminum, Arsenic, Cadmiu
2hromium, Copncr. Lcnd
ANALYSIS REQUESTED
n
3
1
m
a
11
co
cn
N
a
co
0
cn
O
N
r
I
0)
a
m
g
0
LPS$c JN dUIId!d I UW J
ooel 4SOd Zl
:SS32Iaay
n
r
m
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-1
3 73
m�
o=
m-
0 5'
03 In
m�
o
cr
v
v
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PROJECT NAME: Caron Leieune MCB
email: [e-mail], [e-mail]
56I.L-i Si-O66 (Xe4) OZ00-15b-066 :Xyd/3NOHd
0
0
z
O
:ON 12IOd32l
z
0
0
z
0
0
0
m
--t
0
N
0
r
N
--t
4t
tD
m
z
0
z
m
z
r
0
1
rn
V I
M+
V
0

2ND QUARTER
Residuals Analysis Lab Sheets

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client:
FC Wastewater Date of Report: Apr 28, 2021
Date Collected: Apr 06, 2021
Date Received: Apr 06, 2021
Sample: Quarterly Sludge
Report No.: 2021-2-RESIDUALS
Lab ID: 227, 94
Sample ID: CROM
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
pH
7.88
SU
04/06/2021
SM 4500 H+ B
ELS
Nitrate
Nitrogen
See Attached
Envirochem
Sludge
Residuals
See Attached
Envirochem
Certified By:
LUREN D. ACOSTA

ANALYTICAL & CONSULTING CHEMISTS
USMC Carnp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab + 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
inlo(r�envi ronmen to lchemists.com
Revised Report: Apr 27, 2021
Original Report Date: Apr 23, 2021
Report #: 2021-05634
Customer ID: 12060026
Project ID: Camp Lejeune MCB
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-13973 Site: CROM Tank 4/6/2021 7:38 AM Solid/Sludge Client
Test Method Results Date Analyzed
PAN
Used 30%r Mineralization Rate.
Zinc
Nitrate Nitrogen (talc)
Calculation
EPA 290.7
Nitrite Nitrogen EPA 353.2 119 mg/kg 04/09/2021
Analyzed outside of hold time.
19800 mg/kg 04/23/2021
1340 mg/kg 04/13/2021
Nitrate Nitrogen Subtraction Method <0.545 mg/kg 04/23/2021
Sludge Residuals
SAR Calculation 0.580 04/19/2021
Result reported on an as received basis.
Aluminum EPA 200.7 66800 mg/kg 04/13/2021
Arsenic EPA 200.7 18.1 mg/kg 04/13/2021
Cadmium EPA 200.7 <13.4 mg/kg 04/13/2021
Calcium EPA 200.7 45000 mg/kg 04/13/2021
Chromium EPA 200.7 21.7 mg/kg 04/13/2021
Copper EPA 200.7 289 mg/kg 04/13/2021
Lead EPA 200.7 16.6 mg/kg 04/13/2021
Magnesium EPA 200.7 2220 mg/kg 04/13/2021
Molybdenum EPA 200.7 <13.4 mg/kg 04/13/2021
Nickel EPA 200.7 14.5 mg/kg 04/13/2021
Potassium EPA 200.7 3410 mg/kg 04/13/2021
Selenium EPA 200.7 <13.4 mg/kg 04/13/2021
Sodium EPA 200.7 2450 mg/kg 04/13/2021
N itrate+ Nitrite -Nitrogen EPA 353.2 11.0 mg/kg 04/19/2021
Total Solids a/o) Sys 2540 e 3.67 % 04/08/2021
pH SM 4500 H 0 8.00 units 04/12/2021
Ammonia Nitrogen SM 4500 NH3 C 20900 mg/kg 04/10/2021
Report #:: 2021-05634 Page 1 of 2

envirochem
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-FIEMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention:
Environmental Chemists, Inc,
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Roact, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
environmenialchemists.com
Revised Report: Apr 27, 2021
Original Report Date: Apr 23, 2021
Report #: 2021-05634
Customer ID: 12060026
Project ID: Camp Lejeune MCB
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
SM 4500 Org B
5M 4500 P F
S W846 7471 B
45900 mg/kg
52000 mg/kg
<0.469 mg/kg
04/12/2021
04/16/2021
04/13/2021
Comment:
Reviewed by:
Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Revised
to add zinc.
Report #.. 2021-05634 Page 2 o! 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client: Us11n C.
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Date: V oil Report Number: r -- 6-6 3 Ly
Receipt of sample:
ECHEM Pickup
Client Delivery ❑ I UPS ❑
FedEx 0 Other ❑
❑ YES
❑ NO
N/A
1+-Were custody seals present on the cooler?
• YES
0 NO
1 N/A
2, If custody seals were present, were they intact/unbroken?
Original temperature upon receipt_ Q. °C Corrected temperature upon receipt nC
How temperature taken: ❑ Temperature Blank j Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
0 NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./CIA notified?
YES
0 NO
4. Were proper custody procedures {relinquished/received) followed?
YES
0 NO
5. Were sample ID`s listed an the COC?
YES
El
6. Were samples ID's listed on sample containers?
YES
0 NO
7, Were collection date and time listed on the COC?
YES
0 NO
8. Were tests to be performed listed an the COC?
YES
0 NO
9. Did samples arrive in proper containers for each test?
YES
• NO
10. Did samples arrive in good condition for each test?
YES
• NO
11. Was adequate sample volume available?'
YES
0 NO
12. Were samples received within proper holding time for requested tests?
0 YES
0 NO
13. Were acid preserved samples received at a pH of <2? *
0 YES
0 NO
14. Were cyanide samples received at a pH >12?
O YES
❑ NO
15. Were sulfide samples received at a pH >9?
O YES
O NO
16, Were NH3/TICK/Phenol received at a chlorine residual of <0.5 m/L? *
O YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
O YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/volatiles are pH checked at time of analysis and recorded an the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 3T729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910392-0223 FAX [phone]
Info environmentalchemists_cam
CLIENT: t^omruaridina Gonerol
PROJECT NAME: Camn Leieune MCB
REPORT NO: {f eiSb3L
ADDRESS: G-F/EMDIEQB/Environmentaf Laboratory
CONTACT NAME: Albeda Y Okamoto
PO NO:
12 Post Lane
REPORT TO: Lauren Acosta
PHONEIFAX: 910-451-0020 (fax) 910-451-7195
Camn_i Apttrtp flit. 2ESd7
COPY TO:
email: [e-mail], Lauren-acosta@usmc-rr
Sampled By: r r,� � -o ,� 12-.. s,1.7t.,�2-
SAMPLE TYPE: l = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other.
Sample Identification
Collection
m
A
4v
m
Y
o
o
U
t _
c o
V a
u
LAB ID
NUMBER
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
x
2
y
x
3
s
el
=
v
x
o_
,-
LU
o
t'RUM TANK
�JY�k`,s71
O.3�
SLUDGE,
(P)
-G
j
L
X
`luminum, Arsenic, Cadmiurd
hromius, Cowper, mad,
ft
,
C
P
agnesium, Molybdenum,
G
G
C
P
'
iciei, Potassium, Sodium,
.elenium, Zinc,
G
G
C
p
-
ercury Sludge, Nitrite,
it-rat-P. Ali t-rAr�-Ni t-ri t=r
G
G
C
P
KW, Total Solids/Soils &
G
G
C
P
.luJ e. Anuuuiiia, Total
'hosphorus, Calcium, SAR,
G
G
C
p
PAN
G
G
C
P
G
G
C
P
1
G
G
C
P
G
G
Transfer
Relinquished By:
DaterTime
Received By:
Date/Time
I.
_— -
`Zj6 ,26 �°J7sJ
Refrigerator
GI Yr0( ova / /A6 75 -0
2.
_ Refrigerator
J. 702 167S\x
Temperature
Delivered By
Comments:
Resample
Date:
TURNAROUND:

3RD QUARTER
Residuals Analysis Lab Sheets

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client: FC Wastewater Date of Report: Aug 11, 2021
Date Collected: Jul 13, 2021 Report No.: 2021-3-RESIDUALS
Date Received: Jul 13, 2021 Lab ID: 227, 94
Sample: Quarterly Sludge Collected By: Droski
Sample ID: CROM
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
pH
8.30
SU
07/13/2021
SM 4500 H+ B
ELS
Nitrate
Nitrogen
See Attached
Envirochem
Sludge
Residuals
See Attached
Envirochem
NOTE: Arsenic levels this quarter are were higher than normal at 34.0 mg/kg.
Permit Thresholds:
Ceiling Concentration - 75 mg/kg
Monthly Average Concentration - 41 mg/kg
Certified By:
LRUREN D. ACOSTA

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention:
Date of Report: Jul 29, 2021
Customer PO #:
Customer ID: 12060026
Report #: 2021-11576
Project ID: Camp Lejeune MCB
Lab ID
21-28786
Test
Sample ID:
Site: MOM Tank
Collect DatelTime Matrix Sampled by
7/13/2021 7:22 AM Solid/Sludge Client
Method Results Date Analyzed
PA N
Used 30% Mineralization Rate.
SAR
Nitrate Nitrogen (calc)
Nitrite Nitrogen
Matrix Interference.
Nitrate+ Nitrite -Nitrogen
Nitrate Nitrogen
Sludge Residuals
Calculation
Calculation
EPA 353.2
EPA 353.2
Subtraction Method
Aluminum EPA 200.7
Arsenic EPA 200.7
Cadmium EPA 200.7
Calcium EPA 200.7
Chromium EPA 200.7
Copper EPA 200.7
Lead EPA 200.7
Magnesium EPA 200.7
Molybdenum EPA 200.7
Nickel EPA 200.7
Potassium EPA 200.7
Selenium EPA 200.7
Sodium EPA 200.7
Zinc EPA 200.7
Total Solids (/) SM 2540 B
pH SM4500:AB
Result estimated. Analyzed out of 15 minutes hold time.
25300 mg/kg 07/29/2021
0.560 07/29/2021
<26.9 mg/kg 07/14/2021
1,87 mg/kg 07/15/2021
1.88 mg/kg 07/29/2021
67800 mg/kg 07/20/2021
34.0 mg/kg 07/20/2021
<17.5 mg/kg 07/20/2021
61800 mg/kg 07/20/2021
24.9 mg/kg 07/20/2021
352 mg/kg 07/20/2021
20.8 mg/kg 07/20/2021
3730 mg/kg 07/20/2021
<17.5 mg/kg 07/20/2021
<17.5 mg/kg 07/20/2021
5540 mg/kg 07/20/2021
<17.5 mg/kg 07/20/2021
3250 mg/kg 07/20/2021
1730 mg/kg 07/20/2021
2.67 % 07/14/2021
8.59 units 07/21 /2021
Ammonia Nitrogen SM 4500 NH3 C-2011
35600 mg/kg 07/14/2021
Report*. 2021-11576 Page 1 of 2

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention:
Date of Report: Jul 29, 2021
Customer Pa #:
Customer ID: 12060026
Report #: 2021-11576
Project ID: Camp Lejeune MCB
Total Kjeldahl Nitrogen (TKN)
Total Phosphorus
Mercury
SM 4500 Org B
SM 4500 P F
5W646 7471B
60700 mg/kg 07/14/2021
54500 mg/kg 07/20/2021
<0.603 mg/kg 07/14/2021
Comment: Sludge results, except pH, reported on a dry weight basis.
Reviewed by:
_
Report #:- 2021-11576 Page 2 of 2

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client: lit6 v t Q
Receipt of sample:
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Date:i 1 3 ioRi Report Number: 01 — ri i 5�
ECHEM Pickup
LIPS ❑
FedEx 0 Other ❑
❑ YES
0 NO
A' N/A
1. Were custody seals present on the cooler?
❑ YES
■ NO
lF N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt 'C
How temperature taken: 0 Temperature Blank '' Against Bottles
tR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
0 NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
0 NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
5. Were sample ID's listed on the COC?
YES
0 NO
5. Were samples ID's listed on sample containers?
YES
❑ NO
7, Were collection date and time listed on the COC?
ftl YES
0 NO
8. Were tests to be performed listed on the COC?
ii VIC
❑ Nn
Q rliri camnlp . arritrn in nrnnpr rnntainrarc fnr ❑arh tact?
YES
DNO
10, Did samples arrive in good condition for each test?
YES
❑ NO
11. Was adequate sample volume available?'
Nt YES
❑ NO
12, Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2? *
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phennl received at a chlorine residual of <0.5 m/t?
0 YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
0 YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are Checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: Must be completed for any samples) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): HSO, HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
Client Delivery 0

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWG CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 23405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT: rornmandina Genarnl
PROJECT NAME: Camp Leieune MICR
REPORT NO: 194 — t, ( -1
ADDRESS: G-F/EMDIEQB/Environmental Laboratory
CONTACT NAME: Alberta Y Okarnntn
P❑ NO:
12 Pnst Lane
REPORT TO: Lauren Acosta
PHONE/FAX: [phone] (fax) 0-451-7195
CAM/I I P1Al1rip Ntr- ?Rcd7
COPY TO:
„al
email: [e-mail], [e-mail]
Sampled B i0 rD.
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
it
Collection
m
m
t F
u,
m
a R
° F
z;
c o
p
� 94'
F
U
LAB I❑
NUMBER
PRESERVATION
ANALYSIS REQUESTEDDate
Sample Identification
Time
Temp
.A0
$
x
s
o
1
a
1
0
F
a"
C RUM TANK
-7/ 13 /2
p7 2_Z
SLUDGE
P
20CAP
X
kluminum, Arsenic, Cadmiutti
-ham 3 tin, Copper,
G
O
P
—Leese}.,
Magnesium, Molybdenum,
G
G
C
P
7+Ticxel,
Potassium, Sodium,
pelenium, Zinc,
G
G
C
P
INiercury
Sludge, Nitrite,
itrajLF. Ni t-ra P-1\T't n
i nit:
G
G
C
P
-SluJje
,
TKN, Total Solids/Soils &
G
G4
C
P
P-
, AL1 ilurrfjd, Total
'hospharus, Calcium, SAR,
G
G
C
P
PAN
G
G
G
p
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished
Date/Time
Received By:
Date/Time
1.
-// 3/LI Io7Z
R
`ri rater
7.{.��1
2.
Refrigerator y
�, ( 7t7� t C?7
� r
� �" `
7. r -)-( o - 0
Temperature when Received:
Delivered By:
Comments:
p ] Accepte
Received By:
Resample Req ested:
Date Time: /41(
LLL URNAROUND:

4TH QUARTER
Residuals Analysis Lab Sheets

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
12 Post Lane, Camp Lejeune, NC 28547
Client: FC Wastewater Date of Report: Nov 02, 2021
Date Collected: Oct 05, 2021 Report No.: 2021-4-RESIDUALS
Date Received: Oct 05, 2021 Lab ID: 227, 94
Sample: Quarterly Sludge Collected By: N. Droski
Sample ID: CROM
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
pH
7.66
SU
10/05/2021
SM 4500 H+B
ELS
Nitrate
Nitrogen
See Attached
Envirochem
Sludge
Residuals
See Attached
Envirochem
NOTE:
Certi 'ed By:
L UREN D. ACOSTA

ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y Okamoto
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0'223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473,5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report:
Custorer PO #:
Customer ID:
Report #:
Oct 29. 2021
12060026
2021-17558
Project ID: Crom Tank
Lab ID
21-44064
Test
Sample ID:
Site: Chrom Tank
Method
Collect DatelTime Matrix
10/5/2021 7 35 AM Solid/Sludge
Results
Sampled by
Nicholas Droski
Date Analyzed
PAN
Used 30% Mineralization Rate
SAR
Nitrate Nitrogen (calc)
Nitrite Nitrogen
Nitrate Nitrogen
Sludge Residuals
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Aluminum
Chromium
Nitrate+Nitrite-Nitrogen
Total Solids (%)
Ammonia Nitrogen
Total kjeldahl Nitrogen (TKN)
Total Phosphorus
Calculation
CatculalIan
EPA 353 2
Subtraciron Method
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 1
EPA 200 7
EPA 200 7
EPA 200 T
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7
EPA 200 7, Rev 4 4 1994
EPA 200 7. Rev 4 4 1994
EPA 3532
SM 2540 9
SM 4500 NH3 C•2011
SM 4500 Norg 8-2011
SM 4500 P F-2011
19100 mg/kg
0.470
10/29/2021
10/29/2021
4.66 mg/kg 10/08/2021
<0 41 mg/kg 10/29/2021
11.7 rnglkg 10/15/2021
<10.2 mg/kg 10/15/2021
73300 mg/kg 10115/2021
359 mg/kg 10/20/2021
14.0 mg/kg 10/15/2021
3240 mg/kg 10/15/2021
<10.2 mg/kg 10/15/2021
16.5 mg/kg 10/15/2021
3630 mg/kg 10/15/2021
<10.2 mg/kg 10/15/2021
2160 mg/kg 10/15/2021
1480 mg/kg 10/15/2021
63100 mg/kg 10/15/2021
21.9 mg/kg 10/15/2021
0.81 mglkg 10/07/2021
4.85 % 10/06/2021
22300 mg/kg 10/07/2021
48700 mg/kg 10/07/2021
55800 mg/kg 10/14/2021
Report # 2021.17556
P.iiye 1 - F

envirochem
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
Environmental Chemists, Inc.
66C2 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.397.5843 Lab/Fax
info@environmen talchemists.com
Date of Report: Oct 29, 2021
Customer PO #:
Customer ID: 12060026
Report #: 2021-17558
Project ID: Crom Tank
pH SW 846 Method 90450
Result estimated. Analyzed out of 15 minutes hold time
Mercury
SW-B46 7471 9
7.98 units
<0.344 mg/kg
10/26/2021
10/19/2021
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
Reonrt #:. 2021-17555
Page 2 02

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client:
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
V\-4 L Date: IC Report Number: 2021- 7-155i3
Receipt of sample:
E HEM Pickup V Client Delivery 0
UPS ❑ FedEx ❑ Other ❑
O YES
O YES
❑ NO
❑ NO
N/A
N/A
1. Were custody seals present on the cooler?
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt �G
How temperature taken:
eipt °C Corrected temperature Upon receipt
0 Temperature Blank 14 Against Bottles
°C
IR Gun ID: Thomas Tracea
ble 5/N 192511657 IR Gun Correction Factor °C: 0.0
YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
YES
❑ NO
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
5. Were sample ID's listed on the COC?
Oil YES
❑ NO
6. Were samples 1D's listed on sample containers?
X YE5
)1 YES
❑ NO
❑ NO
7. Were collection date and time listed on the COC?
8. Were tests to be performed listed on the COC?
YES
14 YES
NO
9. Did samples arrive in proper containers for each test?
O NO
10. Did samples arrive in good condition for each test?
YES
Itif YES
O NC)
11. WF.las Friars
❑ NO
12. Were samples received within proper hclding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
O YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YE5
❑ NO
15. Were sulfide samples received at a pH >9?
O YE5
O YES
❑ NO
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/t.2
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
Sample(s)
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one):
Time of preservation:
H2SO4 HNO3 MCI NaOH
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

Analyt,sf & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
HCDENR: DWCI CERTIFICATION # 94 NCOHI4S; DLS CERTIFICATION # 37729
COLLECT}ON AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392.0223 FAX [phone]
InfoCienvirenmenta Ichemists.com
CLIENT: rarnmar;dina Gener34
PROJECT NAME: Camo I- eieune MCB
REPORT NO: .2 I - I -155 &
ADDRESS; G-FEMDIEQBIEnvironmental Laboratory
CONTACT NAME: Alberta y Okamntn
PO NO:
12 Post Lane
REPORT TO: Laurent Acosta
PHONE/FAX: [phone] (fax) 910-45j-7195
Carnia 1 Fsiel ina Ni : 7Aid7
COPY TO:
email: [e-mail]. lauren.acosta@usmi:.n
Sam pled By: N i L )�
SAMPLE TYPE: 1 = Influent, E = Effluent, W = Well, ST = Stream, SC) = Soil, SL = Sludge, Other:
Sample Identification
Collection
m
in
d
p
a `o E
o
U
c q•
o
U a
d w
o col'
[i c i
PRESERVATIONn
ANALYSIS REQUESTED
Date
Time
Temp
W
ax
,Ans6,5
=
'1x
a
'i:.'•,
TATiF
`r `
l,;rr,(;E
C
P
-4
0
X
1
aluminum, Arsenic, Cadmium
2144' iva:► C Lead,
G
G
C
P
Opt) e-r
Magnesium, Molybdenum,
G
G
C
P
�zcxel, Potassium, Sodium,
um,
ke1enium, Zinc,
G
C
P
Mercury Sludge, Nitrite,
rat-P. Nit- rdtP- tlLirrdtror
3
G
C
P
,.4'
TX , Total Solids/Soils &
C
P
�lud Alturruuict, Total
phosphorus. Calcium, SAR,
G
G
C
P
PAN
G
G
C
P
G
G
C
P
COr4"4'
.-
1 °! fl 69 +
G
G
C
P
,
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date+Tme
'i.
Ifs 4de., -
,_, -.)_ , yi+
Refrigerator
([2 5 7-0--1 073s
2.
Refrigerator -.
I'a•G -V )000
as.
• io •2 t 1 Decei
Temperature w
Delivered By:
Comments:
2,.Q Accepted: RejeeJed;� Resample Re ested:
Received By:l )
Date: )dTime:
TUR R UND: 3r i
I D L. 2.l `-C
0 o

SECTION 5
Annual Pathogen & Vector Attraction
Reduction Forms (Form PVRF 2T)
and Vector Attraction Reduction Lab
Sheets

1ST QUARTER
Pathogen and Vector Attraction Reduction Form
and Lab Sheets

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: US MCB CAMP LEJEUNE
WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune Advanced WWTP
Monitoring Period: From 1/1/2021
To
NPDES Number: NC0063029
3/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) El
Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑ I
Process to Further Reduce Pathogengs •
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying •
Heat Treatment 0
Thermophilic El
Beta Ray 0
Gamma Ray 0
Pasteurization 0
Class B: 'Alt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens ❑
I I
•
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0
Air Drying 0
Composting • (Aerobic
Digestion } 1
Anaerobic Digestion •
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
PathogenDensityNumber
o}
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
nictue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 ttl the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
oftcFtal solid (dry
weight)
4.96
9.03
102.48
MPN
Gram
0
Weekly
Grab
92 ME
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
•
Alt. 2 (40-day bench)
•
Alt. 3 (30-day bench) r2
Alt. 4 (Spec. O, uptake)
❑
Alt. 5 (14-Day Aerobic)
•
Alt. 6 (Alk. Stabilization
•
Alt 7 (Drying • Stable) 0
Alt. 8 (Drying - Unstable)
0
Alt. 9 (Injection)
❑
Alt. 10 (Incorporation)
❑
No vector attraction reduction alternatives were performed
0
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
0
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Charles Scozzari,
Preparer Na
Signat
*Prep
rvisor WW/Land App.
itle (type or print)
Charles Scozza
Land Applier
//Z if yv
Date Signature sf Land Applier (if applicable)
isor WW/Land App.
Title (if applicable)(type or print)
r is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .111. (26)

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: 2/10/2021
Report No.: 2021-JAN ATAD
Lab ID: 227
Sample ID:
T1B
Date Collected:
1/5/2021
Collected By:
RUBERTE
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.26
%
1/6/2021
SM
2540
G
DES
% Volatile Solids
48.86
%
1/6/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
1/5/2021
Collected By:
RUBERTE
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.37
%
1/6/2021
SM
2540
G
DES
% Volatile Solids
48.27
%
1/6/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
1/5/2021
Collected By:
RUBERTE
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.34
%
1/6/2021
SM
2540
G
DES
% Volatile Solids
48.12
%
1/6/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 1 of 10

Sample ID:
T4B
Date Collected:
1/5/2021
Collected By:
RUBERTE
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.26
%
1/6/2021
SM
2540
G
DES
% Volatile Solids
48.00
%
1/6/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
1/5/2021
Collected By:
RUBERTE
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.38
%
1/6/2021
SM
2540
G
DES
% Volatile Solids
63.54
%
1/6/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
1/5/2021
Collected By:
RUBERTE
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.63
%
1/6/2021
SM
2540
G
DES
% Volatile Solids
47.38
%
1/6/2021
SM
2540
G
DES
Fecal Coliforms
4.96
MPN/gram
1/5/2021
SM
9221
C E
DES
Sample ID:
T1B
Date Collected:
1/7/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.29
%
1/7/2021
SM
2540
G
DES
% Volatile Solids
48.41
%
1/7/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 2 of 10

Sample ID:
T2B
Date Collected:
1/7/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.33
%
1/7/2021
SM
2540
G
DES
% Volatile Solids
47.61
%
1/7/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
1/7/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.29
%
1/7/2021
SM
2540
G
DES
% Volatile Solids
47.44
%
1/7/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
1/7/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.48
%
1/7/2021
SM
2540
G
DES
% Volatile Solids
62.93
%
1/7/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T1B
Date Collected:
1/12/2021
Collected By:
WILLIAMS
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.00
1/12/2021
SM
2540
G
DES
% Volatile Solids
50.98
%
1/12/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 3 of 10

Sample ID:
T2B
Date Collected:
1/12/2021
Collected By:
WILLIAMS
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.34
%
1/12/2021
SM
2540
G
DES
% Volatile Solids
48.35
%
1/12/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
1/12/2021
Collected By:
WILLIAMS
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.43
1/12/2021
SM
2540
G
DES
% Volatile Solids
49.62
%
1/12/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
1/12/2021
Collected By:
WILLIAMS
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.27
%
1/12/2021
SM
2540
G
DES
% Volatile Solids
48.38
%
1/12/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
1/12/2021
Collected By:
WILLIAMS
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.05
%
1/12/2021
SM
2540
G
DES
% Volatile Solids
63.71
%
1/12/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 4 of 10

Sample ID:
CROM
Date Collected:
1/12/2021
Collected By:
WILLIAMS
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.90
%
1/12/2021
SM
2540 G
DES
% Volatile Solids
48.44
%
1/12/2021
SM
2540 G
DES
Fecal Coliforms
6.21
MPN/gram
1/21/2021
SM
9221 C E
DES
Sample ID:
T2B
Date Collected:
1/14/2021
Collected By:
RUBERTE
Time Collected:
0830
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.56
1/14/2021
SM
2540
G
DES
% Volatile Solids
48.95
%
1/14/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
1/14/2021
Collected By:
RUBERTE
Time Collected:
0830
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.58
%
1/14/2021
SM
2540
G
DES
% Volatile Solids
50.55
%
1/14/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
1/14/2021
Collected By:
RUBERTE
Time Collected:
0830
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.19
%
1/14/2021
SM
2540
G
DES
% Volatile Solids
48.51
%
1/14/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 5 of 10

Sample ID:
T2B
Date Collected:
1/19/2021
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.59
1/19/2021
SM
2540
G
DES
% Volatile Solids
48.27
%
1/19/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
1/19/2021
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.29
%
1/19/2021
SM
2540
G
DES
% Volatile Solids
50.13
%
1/19/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
1/19/2021
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.08
%
1/19/2021
SM
2540
G
DES
% Volatile Solids
47.30
%
1/19/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
1/19/2021
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.39
%
1/19/2021
SM
2540
G
DES
% Volatile Solids
63.44
%
1/19/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 6 of 10

Sample ID:
CROM
Date Collected:
1/19/2021
Collected By:
RUBERTE
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.96
%
1/19/2021
SM
2540 G
DES
% Volatile Solids
47.58
%
1/19/2021
SM
2540 G
DES
Fecal Coliforms
< 6.08
MPN/gram
1/19/2021
SM
9221 C E
DES
Sample ID:
T2B
Date Collected:
1/21/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.51
1/21/2021
SM
2540
G
DES
% Volatile Solids
49.19
%
1/21/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
1/21/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.14
%
1/21/2021
SM
2540
G
DES
% Volatile Solids
49.73
%
1/21/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
1/21/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.07
%
1/21/2021
SM
2540
G
DES
% Volatile Solids
47.11
%
1/21/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 7 of 10

Sample ID:
FEED
Date Collected:
1/26/2021
Collected By:
ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.03
%
1/26/2021
SM
2540
G
DES
% Volatile Solids
62.61
%
1/26/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T1B
Date Collected:
1/26/2021
Collected By:
ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.82
1/26/2021
SM
2540
G
DES
% Volatile Solids
59.28
%
1/26/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2A
Date Collected:
1/26/2021
Collected By:
ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.80
%
1/26/2021
SM
2540
G
DES
% Volatile Solids
61.58
%
1/26/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
1/26/2021
Collected By:
ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.50
%
1/26/2021
SM
2540
G
DES
% Volatile Solids
51.07
%
1/26/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 8 of 10

Sample ID:
T4B
Date Collected:
1/26/2021
Collected By:
ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.05
%
1/26/2021
SM
2540
G
DES
% Volatile Solids
46.66
%
1/26/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
1/26/2021
Collected By:
ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.84
1/26/2021
SM
2540 G
DES
% Volatile Solids
48.47
%
1/26/2021
SM
2540 G
DES
Fecal Coliforms
< 6.34
MPN/gram
1/26/2021
SM
9221 C E
DES
Sample ID:
T1B
Date Collected:
1/28/2021
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.86
%
1/28/2021
SM
2540
G
DES
% Volatile Solids
56.78
%
1/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2A
Date Collected:
1/28/2021
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.56
%
1/28/2021
SM
2540
G
DES
% Volatile Solids
60.75
%
1/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 9 of 10

Sample ID:
T3B
Date Collected:
1/28/2021
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.48
1/28/2021
SM
2540
G
DES
% Volatile Solids
48.91
%
1/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
1/28/2021
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.93
%
1/28/2021
SM
2540
G
DES
% Volatile Solids
45.64
%
1/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
1/28/2021
Collected By:
RUBERTE
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.40
%
1/28/2021
SM
2540
G
DES
% Volatile Solids
52.79
%
1/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Certified By:
LMIREN D. ACOSTA
Page 10 of 10

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: 3/9/2021
Report No.: 2021-FEB ATAD
Lab ID: 227
Sample ID:
T1A
Date Collected:
2/2/2021
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.64
2/2/2021
SM
2540
G
ALB
% Volatile Solids
57.90
%
2/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2A
Date Collected:
2/2/2021
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.27
2/2/2021
SM
2540
G
ALB
% Volatile Solids
60.21
%
2/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3A
Date Collected:
2/2/2021
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.42
%
2/2/2021
SM
2540
G
ALB
% Volatile Solids
48.11
%
2/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 1 of 11

Sample ID:
T4B
Date Collected:
2/2/2021
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.89
%
2/2/2021
SM
2540
G
ALB
% Volatile Solids
46.45
%
2/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
2/2/2021
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.76
2/2/2021
SM
2540
G
ALB
% Volatile Solids
64.06
%
2/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
2/2/2021
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.70
%
2/2/2021
SM 2540 G
ALB
% Volatile Solids
47.77
%
2/2/2021
SM 2540 G
ALB
Fecal Coliforms
6.67
MPN/gram
2/2/2021
SM 9221 C E
ALB
Sample ID:
T1A
Date Collected:
2/4/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.13
%
2/4/2021
SM
2540
G
ALB
% Volatile Solids
62.25
%
2/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 2 of 11

Sample ID:
T2A
Date Collected:
2/4/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.22
%
2/4/2021
SM
2540
G
ALB
% Volatile Solids
59.06
%
2/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3A
Date Collected:
2/4/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.30
2/4/2021
SM
2540
G
ALB
% Volatile Solids
49.37
%
2/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4A
Date Collected:
2/4/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.85
%
2/4/2021
SM
2540
G
ALB
% Volatile Solids
46.52
%
2/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T1B
Date Collected:
2/9/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.73
%
2/9/2021
SM
2540
G
ALB
% Volatile Solids
56.06
%
2/9/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 3 of 11

Sample ID:
T2B
Date Collected:
2/9/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.15
%
2/9/2021
SM
2540
G
ALB
% Volatile Solids
56.69
%
2/9/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
2/9/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.87
%
2/9/2021
SM
2540
G
ALB
% Volatile Solids
53.99
%
2/9/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
2/9/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.28
%
2/9/2021
SM
2540
G
ALB
% Volatile Solids
65.78
%
2/9/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
2/9/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.69
%
2/9/2021
SM 2540 G
ALB
% Volatile Solids
48.47
%
2/9/2021
SM 2540 G
ALB
Fecal Coliforms
6.69
MPN/gram
SM 9221 C E
Page 4 of 11

Sample ID:
T1B
Date Collected:
2/11/2021
Collected By:
DROSKI
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.73
%
2/11/2021
SM
2540
G
ALB/DES
% Volatile Solids
55.57
%
2/11/2021
SM
2540
G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
2/11/2021
Collected By:
DROSKI
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.07
%
2/11/2021
SM
2540
G
ALB/DES
% Volatile Solids
55.42
%
2/11/2021
SM
2540
G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
2/11/2021
Collected By:
DROSKI
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.74
%
2/11/2021
SM
2540
G
ALB/DES
% Volatile Solids
53.82
%
2/11/2021
SM
2540
G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
2/11/2021
Collected By:
DROSKI
Time Collected:
0820
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.30
%
2/11/2021
SM
2540
G
ALB/DES
% Volatile Solids
64.54
%
2/11/2021
SM
2540
G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 5 of 11

Sample ID:
T1B
Date Collected:
2/16/2021
Collected By:
DROSKI
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.51
%
2/16/2021
SM
2540
G
ALB
% Volatile Solids
52.47
%
2/16/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
2/16/2021
Collected By:
DROSKI
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.87
%
2/16/2021
SM
2540
G
ALB
% Volatile Solids
52.15
%
2/16/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
2/16/2021
Collected By:
DROSKI
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.67
%
2/16/2021
SM
2540
G
ALB
% Volatile Solids
50.92
%
2/16/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4A
Date Collected:
2/16/2021
Collected By:
DROSKI
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.65
%
2/16/2021
SM
2540
G
ALB
% Volatile Solids
61.19
%
2/16/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 6 of 11

Sample ID:
FEED
Date Collected:
2/16/2021
Collected By:
DROSKI
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.24
%
2/16/2021
SM
2540
G
ALB
% Volatile Solids
67.66
%
2/16/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
2/16/2021
Collected By:
DROSKI
Time Collected:
0753
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.77
%
2/16/2021
SM
2540 G
ALB
% Volatile Solids
47.99
%
2/16/2021
SM
2540 G
ALB
Fecal Coliforms
6.50
MPN/gram
2/16/2021
SM
9221 C E
ALB
Sample ID:
T1B
Date Collected:
2/18/2021
Collected By:
ACOSTA
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.54
%
2/18/2021
SM
2540
G
ALB
% Volatile Solids
53.10
%
2/18/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
2/18/2021
Collected By:
ACOSTA
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.87
%
2/18/2021
SM
2540
G
ALB
% Volatile Solids
53.23
%
2/18/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 7 of 11

Sample ID:
T3B
Date Collected:
2/18/2021
Collected By:
ACOSTA
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.62
%
2/18/2021
SM
2540
G
ALB
% Volatile Solids
51.47
%
2/18/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
2/18/2021
Collected By:
ACOSTA
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.34
%
2/18/2021
SM
2540
G
ALB
% Volatile Solids
59.58
%
2/18/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM UPPER
Date Collected:
2/18/2021
Collected By:
ACOSTA
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.00
%
2/18/2021
SM
2540
G
ALB
% Volatile Solids
48.68
%
2/18/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM LOWER
Date Collected:
2/18/2021
Collected By:
ACOSTA
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.93
%
2/18/2021
SM
2540
G
ALB
% Volatile Solids
48.45
%
2/18/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 8 of 11

Sample ID:
T1A
Date Collected:
2/23/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.24
%
2/24/2021
SM
2540
G
ALB
% Volatile Solids
58.98
%
2/24/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
2/23/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.21
%
2/24/2021
SM
2540
G
ALB
% Volatile Solids
53.28
%
2/24/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
2/23/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.96
%
2/24/2021
SM
2540
G
ALB
% Volatile Solids
55.91
%
2/24/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
2/23/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.73
%
2/24/2021
SM
2540
G
ALB
% Volatile Solids
63.29
%
2/24/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 9 of 11

Sample ID:
CROM UPPER
Date Collected:
2/23/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.12
%
2/24/2021
SM
2540
G
ALB
% Volatile Solids
50.69
%
2/24/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM LOWER
Date Collected:
2/23/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.08
%
2/24/2021
SM
2540
G
ALB
% Volatile Solids
49.62
%
2/24/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
2/23/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.10
%
2/24/2021
SM
2540 G
ALB
% Volatile Solids
49.47
%
2/24/2021
SM
2540 G
ALB
Fecal Coliforms
83.87
MPN/gram
2/23/2021
SM
9221 C E
ALB
Sample ID:
T1A
Date Collected:
2/25/2021
Collected By:
DROSKI
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.24
%
2/25/2021
SM
2540
G
ALB
% Volatile Solids
51.57
%
2/25/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 10 of 11

Sample ID:
T2B
Date Collected:
2/25/2021
Collected By:
DROSKI
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.85
%
2/25/2021
SM
2540
G
ALB
% Volatile Solids
54.28
%
2/25/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
2/25/2021
Collected By:
DROSKI
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.80
%
2/25/2021
SM
2540
G
ALB
% Volatile Solids
56.27
%
2/25/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
2/25/2021
Collected By:
DROSKI
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.71
%
2/25/2021
SM
2540
G
ALB
% Volatile Solids
62.94
%
2/25/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Certified By:
REN D. ACOSTA
Page 11 of 11

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: 4/7/2021
Report No.: 2021-MAR ATAD
Lab ID: 227
Sample ID:
T2B
Date Collected:
3/2/2021
Collected By:
DROSKI
Time Collected:
0714
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.80
3/2/2021
SM
2540
G
ALB
% Volatile Solids
53.52
%
3/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
3/2/2021
Collected By:
DROSKI
Time Collected:
0714
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.75
3/2/2021
SM
2540
G
ALB
% Volatile Solids
52.94
%
3/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
3/2/2021
Collected By:
DROSKI
Time Collected:
0714
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.35
%
3/2/2021
SM
2540
G
ALB
% Volatile Solids
61.07
%
3/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 1 of 10

Sample ID:
CROM
Date Collected:
3/2/2021
Collected By:
DROSKI
Time Collected:
0714
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.22
%
3/2/2021
SM 2540 G
ALB
% Volatile Solids
50.22
%
3/2/2021
SM 2540 G
ALB
Fecal Coliforms
102.48
MPN/gram
3/2/2021
SM 9221 C E
AYO
Sample ID:
T2B
Date Collected:
3/4/2021
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.71
3/4/2021
SM
2540
G
ALB
% Volatile Solids
52.74
%
3/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
3/4/2021
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.76
%
3/4/2021
SM
2540
G
ALB
% Volatile Solids
53.73
%
3/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM UPPER
Date Collected:
3/4/2021
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.28
%
3/4/2021
SM
2540
G
ALB
% Volatile Solids
53.11
%
3/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 2 of 10

Sample ID:
CROM LOWER
Date Collected:
3/4/2021
Collected By:
RUBERTE
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.18
%
3/4/2021
SM
2540
G
ALB
% Volatile Solids
50.69
%
3/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3A
Date Collected:
3/9/2021
Collected By:
DROSKI
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.64
3/9/2021
SM
2540
G
AYO
% Volatile Solids
65.04
%
3/9/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
3/9/2021
Collected By:
DROSKI
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.68
%
3/9/2021
SM
2540
G
AYO
% Volatile Solids
53.20
%
3/9/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
3/9/2021
Collected By:
DROSKI
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.59
%
3/9/2021
SM
2540
G
AYO
% Volatile Solids
66.85
%
3/9/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 3 of 10

Sample ID:
CROM LOWER
Date Collected:
3/9/2021
Collected By:
DROSKI
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.20
%
3/9/2021
SM
2540
G
AYO
% Volatile Solids
51.34
%
3/9/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM UPPER
Date Collected:
3/9/2021
Collected By:
DROSKI
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.11
%
3/9/2021
SM
2540
G
AYO
% Volatile Solids
52.32
%
3/9/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
3/9/2021
Collected By:
DROSKI
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.21
%
3/9/2021
SM 2540 G
AYO
% Volatile Solids
51.28
%
3/9/2021
SM 2540 G
AYO
Fecal Coliforms
5.59
MPN/gram
3/9/2021
SM 9221 C E
AYO
Sample ID:
T3A
Date Collected:
3/11/2021
Collected By:
DROSKI
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.45
%
3/11/2021
SM
2540
G
AYO
% Volatile Solids
63.90
%
3/11/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 4 of 10

Sample ID:
T4B
Date Collected:
3/11/2021
Collected By:
DROSKI
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.74
%
3/11/2021
SM
2540
G
ALB/DES
% Volatile Solids
55.18
%
3/11/2021
SM
2540
G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM LOWER
Date Collected:
3/11/2021
Collected By:
DROSKI
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.35
%
3/11/2021
SM
2540
G
ALB/DES
% Volatile Solids
50.32
%
3/11/2021
SM
2540
G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM UPPER
Date Collected:
3/11/2021
Collected By:
DROSKI
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.48
%
3/11/2021
SM
2540
G
ALB/DES
% Volatile Solids
52.85
%
3/11/2021
SM
2540
G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
3/16/2021
Collected By:
DROSKI
Time Collected:
0836
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.99
%
3/16/2021
SM
2540
G
AYO
% Volatile Solids
59.15
%
3/16/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 5 of 10

Sample ID:
T4B
Date Collected:
3/16/2021
Collected By:
DROSKI
Time Collected:
0836
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.56
%
3/16/2021
SM
2540
G
AYO
% Volatile Solids
53.41
%
3/16/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM UPPER
Date Collected:
3/16/2021
Collected By:
DROSKI
Time Collected:
0836
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.27
%
3/16/2021
SM
2540
G
AYO
% Volatile Solids
51.03
%
3/16/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
3/16/2021
Collected By:
DROSKI
Time Collected:
0836
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.60
%
3/16/2021
SM
2540
G
AYO
% Volatile Solids
66.41
%
3/16/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
3/16/2021
Collected By:
DROSKI
Time Collected:
0836
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.30
%
3/16/2021
SM
2540 G
AYO
% Volatile Solids
50.73
%
3/16/2021
SM
2540 G
AYO
Fecal Coliforms
5.45
MPN/gram
3/16/2021
SM
9221 C E
AYO
Page 6 of 10

Sample ID:
T3B
Date Collected:
3/18/2021
Collected By:
DROSKI
Time Collected:
0803
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.86
%
3/18/2021
SM
2540
G
AYO
% Volatile Solids
58.77
%
3/18/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
3/18/2021
Collected By:
DROSKI
Time Collected:
0803
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.56
%
3/18/2021
SM
2540
G
AYO
% Volatile Solids
53.95
%
3/18/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM UPPER
Date Collected:
3/18/2021
Collected By:
DROSKI
Time Collected:
0803
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.29
%
3/18/2021
SM
2540
G
AYO
% Volatile Solids
53.13
%
3/18/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM LOWER
Date Collected:
3/18/2021
Collected By:
DROSKI
Time Collected:
0803
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.40
%
3/18/2021
SM
2540
G
AYO
% Volatile Solids
50.86
%
3/18/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 7 of 10

Sample ID:
T3B
Date Collected:
3/23/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.32
%
3/23/2021
SM
2540
G
ALB
% Volatile Solids
53.82
%
3/23/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
3/23/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.34
%
3/23/2021
SM
2540
G
ALB
% Volatile Solids
55.52
%
3/23/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
3/23/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.85
%
3/23/2021
SM
2540
G
ALB
% Volatile Solids
68.81
%
3/23/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
3/23/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.36
%
3/23/2021
SM
2540 G
ALB
% Volatile Solids
50.73
%
3/23/2021
SM
2540 G
ALB
Fecal Coliforms
5.36
MPN/gram
3/23/2021
SM
9221 C E
DES
Page 8 of 10

Sample ID:
T3B
Date Collected:
3/25/2021
Collected By:
DROSKI
Time Collected:
0726
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.25
%
3/29/2021
SM
2540
G
AYO
% Volatile Solids
54.17
%
3/29/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
3/25/2021
Collected By:
DROSKI
Time Collected:
0726
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.26
%
3/29/2021
SM
2540
G
AYO
% Volatile Solids
54.50
%
3/29/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
3/30/2021
Collected By:
DROSKI
Time Collected:
0713
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.02
%
3/31/2021
SM
2540
G
AYO
% Volatile Solids
53.19
%
3/31/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
3/30/2021
Collected By:
DROSKI
Time Collected:
0713
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.15
%
3/31/2021
SM
2540
G
AYO
% Volatile Solids
54.62
%
3/31/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 9 of 10

Sample ID:
FEED
Date Collected:
3/30/2021
Collected By:
DROSKI
Time Collected:
0713
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.49
%
3/31/2021
SM
2540
G
AYO
% Volatile Solids
68.13
%
3/31/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
3/30/2021
Collected By:
DROSKI
Time Collected:
0713
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.27
%
3/31/2021
SM
2540 G
AYO
% Volatile Solids
51.18
%
3/31/2021
SM
2540 G
AYO
Fecal Coliforms
5.5
MPN/gram
3/30/2021
SM
9221 C E
AYO
Certified By:
REN D. ACOSTA
Page 10 of 10

REPORT NO. 2021 BSQTR1
Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application
Report No.: 2021 BSQTR1
Date of Report: 03/04/2021
Lab ID:
227
Date Collected:
1/12/2021
Time Collected:
0745
Collected By:
DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.64
%
1/12/2021
SM
2540
G
DES
B-S
% Volatile Solids
48.56
%
1/12/2021
SM
2540
G
DES
B-S DUP
% Total Solids
1.64
%
1/12/2021
SM
2540
G
DES
B-S DUP
% Volatile Solids
48.56
%
1/12/2021
SM
2540
G
DES
QUALITY CONTROL - 1/12/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.64 %
0 %
% Volatile Solids
48.56 %
0 %
Date Collected:
1/19/2021
Time Collected:
0915
Collected By:
DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.70
%
1/19/2021
SM
2540
G
DES
B-S
% Volatile Solids
47.97
%
1/19/2021
SM
2540
G
DES
B-S DUP
% Total Solids
1.71
%
1/19/2021
SM
2540
G
DES
B-S DUP
% Volatile Solids
48.02
%
1/19/2021
SM
2540
G
DES
QUALITY CONTROL - 1/19/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.71 %
1.0 %
% Volatile Solids
48.00 %
0.1 %
Page 1 of 3

REPORT NO. 2021 BSQTR1
Date Collected:
1/25/2021
Time Collected:
0810
Collected By:
DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.68
%
1/26/2021
SM
2540
G
DES
B-S
% Volatile Solids
48.85
%
1/26/2021
SM
2540
G
DES
B-S DUP
% Total Solids
1.68
%
1/26/2021
SM
2540
G
DES
B-S DUP
% Volatile Solids
48.83
%
1/26/2021
SM
2540
G
DES
QUALITY CONTROL - 1/25/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.68
0 %
% Volatile Solids
48.84 %
0 %
Date Collected:
2/1/2021
Time Collected:
0800
Collected By:
DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.74
%
2/2/2021
SM
2540
G
ALB
B-S
% Volatile Solids
47.53
%
2/2/2021
SM
2540
G
ALB
B-S DUP
% Total Solids
1.75
%
2/2/2021
SM
2540
G
ALB
B-S DUP
% Volatile Solids
47.59
%
2/2/2021
SM
2540
G
ALB
QUALITY CONTROL - 2/1/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.75 %
0.6 %
% Volatile Solids
47.56 %
0.1 %
Page 2 of 3

REPORT NO. 2021 BSQTR1
Date Collected:
2/8/2021
Time Collected:
0845
Collected By:
ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.54
%
2/9/2021
SM
2540
G
ALB
B-S
% Volatile Solids
48.29
%
2/9/2021
SM
2540
G
ALB
B-S DUP
% Total Solids
1.55
%
2/9/2021
SM
2540
G
ALB
B-S DUP
% Volatile Solids
48.36
%
2/9/2021
SM
2540
G
ALB
QUALITY CONTROL - 2/8/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.55 %
0.6 %
% Volatile Solids
48.33 %
0.1 %
Date Collected:
2/16/2021
Time Collected:
0902
Collected By:
ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.44
%
2/16/2021
SM
2540
G
ALB
B-S
% Volatile Solids
48.35
%
2/16/2021
SM
2540
G
ALB
B-S DUP
% Total Solids
1.45
%
2/16/2021
SM
2540
G
ALB
B-S DUP
% Volatile Solids
48.59
%
2/16/2021
SM
2540
G
ALB
QUALITY CONTROL - 2/16/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.45 %
0.7 %
% Volatile Solids
48.47 %
0.5 %
*B-S: BENCH -SCALE
6-WEEK VOLATILE SOLIDS REDUCTION
0.2 %
Certified By:
LPMYJREN D. ACOSTA
Page 3 of 3

MCB CAMLEJ ELS
ATAD BENCH -SCALE VOLATILE SOLIDS REDUCTION ANALYSIS
Sample Date
Sample ID
Temp
(°C)
DO
(mg/L)
% TS
% VS
% VS Avg
Analyst
1/12/2021
BENCH
14.8
g 19
1.64
48.56
48.56
DES
BENCH-DUP
1.64
48.56
1/19/2021
BENCH
10.0
7.94
1.70
47.97
48.00
DES
BENCH-DUP
1.71
48.02
1/25/2021
BENCH
13 2
9 72
1.68
48.85
48.84
ALB
BENCH-DUP
1.68
48.83
2/1/2021
BENCH
13.0
9 75
1.74
47.53
47.56
ALB
BENCH-DUP
1.75
47.59
2/8/2021
BENCH
9.0
10.57
1.54
48.29
48.33
ALB
BENCH-DUP
1.55
48.36
2/16/2021
BENCH
17.1
g 38
1.44
48.35
48.47
DES
BENCH-DUP
1.45
48.59
INITIAL VS (%)
48.56
FINAL VS (%)
48.47
VS
REDUCTION
0.2%
VS REDUCTION = (INITIAL VS - FINAL VS) / INITIAL VS X 100
*VS REDUCTION MUST BE < 15% TO MEET VECTOR ATTRACTION REDUCTION REQUIREMENTS
REV. 01/2020

Enclosure (1 }
MCB CAMLE,.1 ELS
ATAD BENCH -SCALE WORKSHEET
C1 = Kno++n residuals concentration
VI = Volume of residuals
C2 = Needed concentration (2°])
V2 = Kno++n final volume (1.1
Date Setup: 1 v �' 2-1
Date DO > 2.0 mg1L: I
1
24
(C•1r(V11=(C2)IV21
3•(c3
(.. .:s 1{VI}=f21124}
VI =-1H;1
V 1 - _j 3 _ I. ! Residuals req.'
2-11:-_�� 1.{l:f'f.rig1
f)a.
Date
Temp.
CC)
DO
(mg.1.1
knalst
-
lime Collected
I
VI('
0 li. Zl
la43
IO.LIS
ALe
l']74c7
3
OeD
L.13. ' 94
Idr. 3
br
4
ViAa.,
1 \4. ) 2-
'A-• 3
S
]
131
1 +.16: W r- i
L4- ,
r
��y.i.7
! r.-k
6
Gov
( -t . a02.1
;c o
1,ei4
_ iF '
o9tI ----
L8
ti G
.24. .2-02-(,
141
L E-S"
4•
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Cl -1 r›-
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i1
ij
(.2�4-:2b (
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12
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ik- ,.
�/�}
OC30
16
- •2-.71
Li ...3
Au
17
3.71
c.i
Ai
1g
g-
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Pktg
19
1;---
.2 -c3. mil?
13. t
040.A.o
't,
vl
2 •6. -24
et,U
l0•5/
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-
tiati5
21
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Ira _'?7
A-445
22
V`',.
2 - 10- 2- i
15 .•Z
L'>13
23
312.
2'11-2-I
i0•5
AATV-,
24
F
•l7. .70)1
li#. Lf
gi
25
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2• (f,..p•/-I
t'1. 1
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30
--r
-z: 2 ,21
(2
A
yt) 2-.29.2 j C33 2—
REV FEB 2020

2ND QUARTER
Pathogen and Vector Attraction Reduction Form
and Lab Sheets

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: US MCB CAMP LEJEUNE
WQ Permit Number: WQ0012346
WWTP Name: Camp Leieune Advanced WWTP
Monitoring Period: From
4/ 1 l2021
To
NPDES Number: NC0063029
6/30/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level
achieved and alternative performed:
Class A:
Alt. A (time.'temp) n
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ■
AIt.D (No Prior Test) 0
Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost •
Heat Drying CJ
Heat Treatment
■
Thermophilic ® J
Beta Ray •
Gamma Ray L]
Pasteurization •
Class B:
Alt. (1) Fecal Density L]
Alt (2) Process to Significantly Reduce Pathogens 0
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0 I
Air Drying [1 1
Composting 0 (Aerobic
Digestion '
Anaerobic Digestion •
1
If applicable to alternative performed
(Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
PathogenDensityNumber
o
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
5.47
7.33
59.23
Gram
0
Weekly
Grab
4221 E
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ©
Alt. 4 (Spec. O, uptake) 0
Alt. 5 (14-Day Aerobic) •
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) 0
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) •
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Charles Scozzari,
rvisor, WWILand App.
Preparer Nam= a ►itle (type or print)
J
Signature f Preparer*
Charles Scoz
Land Appl
yli
J
Date Signa re o ', d pplier (if applicable)
*Preparis defined in 40 CFR Part 503.9(r) and 15A NCAC 2T 1 02 (26)
Supervisor, WWILand App.
itle (if applicable)(type or print)
Date

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: Revised 5/17/2021
Report No.: 2021-APR ATAD REVISED 2
Lab ID: 227
Sample ID:
T3B
Date Collected:
4/1/2021
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.98
4/1/2021
SM
2540
G
AYO
% Volatile Solids
53.24
%
4/1/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
4/1/2021
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.02
4/1/2021
SM
2540
G
AYO
% Volatile Solids
54.70
%
4/1/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
4/6/2021
Collected By:
DROSKI
Time Collected:
0722
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.77
%
4/6/2021
SM
2540
G
DES
% Volatile Solids
68.00
%
4/6/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 1 of 9

Sample ID:
T3B
Date Collected:
4/6/2021
Collected By:
DROSKI
Time Collected:
0722
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.98
%
4/6/2021
SM
2540
G
DES
% Volatile Solids
53.60
%
4/6/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
4/6/2021
Collected By:
DROSKI
Time Collected:
0722
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.12
4/6/2021
SM
2540
G
DES
% Volatile Solids
53.85
%
4/6/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
4/6/2021
Collected By:
DROSKI
Time Collected:
0722
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.28
%
4/6/2021
SM 2540 G
DES
% Volatile Solids
50.21
%
4/6/2021
SM 2540 G
DES
Fecal Coliforms
< 5.47
MPN/gram
4/6/2021
SM 9221 C E
DES
Sample ID:
T3B
Date Collected:
4/8/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.01
%
4/12/2021
SM
2540
G
DES
% Volatile Solids
53.30
%
4/12/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 2 of 9

Sample ID:
T4B
Date Collected:
4/8/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.04
%
4/12/2021
SM
2540
G
DES
% Volatile Solids
55.99
%
4/12/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2A
Date Collected:
4/13/2021
Collected By:
ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.77
4/13/2021
SM
2540
G
DES
% Volatile Solids
64.83
%
4/13/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
4/13/2021
Collected By:
ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.90
%
4/13/2021
SM
2540
G
DES
% Volatile Solids
53.57
%
4/13/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
4/13/2021
Collected By:
ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.95
%
4/13/2021
SM
2540
G
DES
% Volatile Solids
54.84
%
4/13/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 3 of 9

Sample ID:
FEED
Date Collected:
4/13/2021
Collected By:
ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.43
%
4/13/2021
SM
2540
G
DES
% Volatile Solids
67.53
%
4/13/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
4/13/2021
Collected By:
ACOSTA
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.19
%
4/13/2021
SM
2540
G
DES
% Volatile Solids
49.53
%
4/13/2021
SM
2540
G
DES
Fecal Coliforms
< 5.63
MPN/gram
4/13/2021
SM
9221
C E
DES
Sample ID:
T2A
Date Collected:
4/15/2021
Collected By:
ACOSTA
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.80
%
4/20/2021
SM
2540
G
DES
% Volatile Solids
63.09
%
4/20/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
4/15/2021
Collected By:
ACOSTA
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.90
%
4/20/2021
SM
2540
G
DES
% Volatile Solids
53.23
%
4/20/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 4 of 9

Sample ID:
T4B
Date Collected:
4/15/2021
Collected By:
ACOSTA
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.01
%
4/20/2021
SM
2540
G
DES
% Volatile Solids
54.47
%
4/20/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2A
Date Collected:
4/20/2021
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.87
%
4/20/2021
SM
2540
G
DES
% Volatile Solids
59.85
%
4/20/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
4/20/2021
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.94
%
4/20/2021
SM
2540
G
DES
% Volatile Solids
54.26
%
4/20/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
4/20/2021
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.03
%
4/20/2021
SM
2540
G
DES
% Volatile Solids
54.82
%
4/20/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 5 of 9

Sample ID:
FEED
Date Collected:
4/20/2021
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.63
%
4/20/2021
SM
2540
G
DES
% Volatile Solids
66.18
%
4/20/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
4/20/2021
Collected By:
ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.10
%
4/20/2021
SM
2540 G
DES
% Volatile Solids
49.15
%
4/20/2021
SM
2540 G
DES
Fecal Coliforms
< 5.81
MPN/gram
4/20/2021
SM
9221 C E
DES
Sample ID:
T2A
Date Collected:
4/22/2021
Collected By:
ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.65
%
4/26/2021
SM
2540
G
DES
% Volatile Solids
59.44
%
4/26/2021
SM
2540
G
DES
Fecal Coliforms
NOT
ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
4/22/2021
Collected By:
ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.84
%
4/26/2021
SM
2540
G
DES
% Volatile Solids
54.86
%
4/26/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 6 of 9

Sample ID:
T4B
Date Collected:
4/22/2021
Collected By:
ACOSTA
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.94
%
4/26/2021
SM
2540
G
DES
% Volatile Solids
55.19
%
4/26/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2A
Date Collected:
4/27/2021
Collected By:
ACOSTA
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.88
%
4/27/2021
SM
2540
G
DES
% Volatile Solids
57.09
%
4/27/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
4/27/2021
Collected By:
ACOSTA
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.90
%
4/27/2021
SM
2540
G
DES
% Volatile Solids
55.82
%
4/27/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
4/27/2021
Collected By:
ACOSTA
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.02
%
4/27/2021
SM
2540
G
DES
% Volatile Solids
55.57
%
4/27/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 7 of 9

Sample ID:
FEED
Date Collected:
4/27/2021
Collected By:
ACOSTA
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.74
%
4/27/2021
SM
2540
G
DES
% Volatile Solids
65.93
%
4/27/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
4/27/2021
Collected By:
ACOSTA
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.91
%
4/27/2021
SM
2540 G
DES
% Volatile Solids
49.49
%
4/27/2021
SM
2540 G
DES
Fecal Coliforms
< 6.19
MPN/gram
4/27/2021
SM
9221 C E
DES
Sample ID:
T2A
Date Collected:
4/29/2021
Collected By:
DROSKI
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.74
%
4/29/2021
SM
2540
G
DES
% Volatile Solids
58.57
%
4/29/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
4/29/2021
Collected By:
DROSKI
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.93
%
4/29/2021
SM
2540
G
DES
% Volatile Solids
54.54
%
4/29/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 8 of 9

Sample ID:
T4B
Date Collected:
4/29/2021
Collected By:
DROSKI
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.08
%
4/29/2021
SM
2540
G
DES
% Volatile Solids
56.32
%
4/29/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Certified By:
REN D. ACOSTA
Page 9 of 9

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: 6/2/2021
Report No.: 2021-MAY ATAD
Lab ID: 227
Sample ID:
T2B
Date Collected:
5/4/2021
Collected By:
RUBERTE
Time Collected:
0805
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.25
5/4/2021
SM
2540
G
ALB
% Volatile Solids
55.13
%
5/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
5/4/2021
Collected By:
RUBERTE
Time Collected:
0805
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.51
5/4/2021
SM
2540
G
ALB
% Volatile Solids
55.12
%
5/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
5/4/2021
Collected By:
RUBERTE
Time Collected:
0805
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.15
%
5/4/2021
SM
2540
G
ALB
% Volatile Solids
54.89
%
5/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 1 of 7

Sample ID:
FEED
Date Collected:
5/4/2021
Collected By:
RUBERTE
Time Collected:
0805
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.52
%
5/4/2021
SM
2540
G
ALB
% Volatile Solids
62.75
%
5/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
5/4/2021
Collected By:
RUBERTE
Time Collected:
0835
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.86
5/4/2021
SM 2540 G
ALB
% Volatile Solids
50.69
%
5/4/2021
SM 2540 G
ALB
Fecal Coliforms
< 6.29
MPN/gram
5/4/2021
SM 9221 C E
ALB
Sample ID:
T2B
Date Collected:
5/6/2021
Collected By:
ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.16
%
5/6/2021
SM
2540
G
ALB
% Volatile Solids
53.46
%
5/6/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
5/6/2021
Collected By:
ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.36
%
5/6/2021
SM
2540
G
ALB
% Volatile Solids
52.42
%
5/6/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 2 of 7

Sample ID:
T4B
Date Collected:
5/6/2021
Collected By:
ACOSTA
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.05
%
5/6/2021
SM
2540
G
ALB
% Volatile Solids
53.37
%
5/6/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
5/11/2021
Collected By:
DROSKI
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.29
5/11/2021
SM
2540
G
ALB/DES
% Volatile Solids
53.51
%
5/11/2021
SM
2540
G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
5/11/2021
Collected By:
DROSKI
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.15
%
5/11/2021
SM
2540
G
ALB/DES
% Volatile Solids
53.31
%
5/11/2021
SM
2540
G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
5/11/2021
Collected By:
DROSKI
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
1.78
%
5/11/2021
SM
2540
G
ALB/DES
% Volatile Solids
65.53
%
5/11/2021
SM
2540
G
ALB/DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 3 of 7

Sample ID:
CROM
Date Collected:
5/11/2021
Collected By:
DROSKI
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.84
%
5/11/2021
SM 2540 G
ALB/DES
% Volatile Solids
49.67
%
5/11/2021
SM 2540 G
ALB/DES
Fecal Coliforms
< 6.34
MPN/gram
5/11/2021
SM 9221 C E
LA
Sample ID:
T2B
Date Collected:
5/13/2021
Collected By:
RUBERTE
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.12
%
5/13/2021
SM
2540
G
AYO
% Volatile Solids
52.02
%
5/13/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
5/13/2021
Collected By:
RUBERTE
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.93
%
5/13/2021
SM
2540
G
AYO
% Volatile Solids
53.40
%
5/13/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
5/18/21
Collected By:
DROSKI
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.13
%
5/18/2021
SM
2540
G
ALB/AYO
% Volatile Solids
54.89
%
5/18/2021
SM
2540
G
ALB/AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 4 of 7

Sample ID:
T4B
Date Collected:
5/18/21
Collected By:
DROSKI
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.04
%
5/18/2021
SM
2540
G
ALB/AYO
% Volatile Solids
53.52
%
5/18/2021
SM
2540
G
ALB/AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
5/18/21
Collected By:
DROSKI
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.57
%
5/18/2021
SM
2540
G
ALB/AYO
% Volatile Solids
65.38
%
5/18/2021
SM
2540
G
ALB/AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
5/18/21
Collected By:
RUBERTE
Time Collected:
0737
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.87
%
5/18/2021
SM
2540 G
ALB/AYO
% Volatile Solids
50.43
%
5/18/2021
SM
2540 G
ALB/AYO
Fecal Coliforms
59.23
MPN/gram
5/18/2021
SM
9221 C E
ALB
Sample ID:
T2B
Date Collected:
5/20/2021
Collected By:
RUBERTE
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.00
%
5/20/2021
SM
2540
G
ALB
% Volatile Solids
52.80
%
5/20/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 5of7

Sample ID:
T4B
Date Collected:
5/20/2021
Collected By:
RUBERTE
Time Collected:
0815
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.16
%
5/20/2021
SM
2540
G
ALB
% Volatile Solids
55.21
%
5/20/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
5/25/2021
Collected By:
RUBERTE
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.03
%
5/25/2021
SM
2540
G
ALB
% Volatile Solids
52.92
%
5/25/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
5/25/2021
Collected By:
RUBERTE
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.96
%
5/25/2021
SM
2540
G
ALB
% Volatile Solids
52.75
%
5/25/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
5/25/2021
Collected By:
RUBERTE
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.35
%
5/25/2021
SM
2540
G
ALB
% Volatile Solids
68.48
%
5/25/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 6 of 7

Sample ID:
CROM
Date Collected:
5/25/2021
Collected By:
RUBERTE
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.83
%
5/25/2021
SM
2540 G
ALB
% Volatile Solids
50.35
%
5/25/2021
SM
2540 G
ALB
Fecal Coliforms
< 6.36
MPN/gram
5/25/2021
SM
9221 C E
LA
Certified By:
REN D. ACOSTA
Page 7 of 7

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: 6/30/2021
Report No.: 2021-JUN ATAD
Lab ID: 227
Sample ID:
T2B
Date Collected:
6/1/2021
Collected By:
WILLIAMS
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.66
6/1/2021
SM
2540
G
AYO
% Volatile Solids
53.96
%
6/1/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
6/1/2021
Collected By:
WILLIAMS
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.83
6/1/2021
SM
2540
G
AYO
% Volatile Solids
52.42
%
6/1/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
6/1/2021
Collected By:
WILLIAMS
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.32
%
6/1/2021
SM
2540
G
AYO
% Volatile Solids
67.62
%
6/1/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 1 of 8

Sample ID:
CROM
Date Collected:
6/1/2021
Collected By:
WILLIAMS
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.78
%
6/1/2021
SM 2540 G
AYO
% Volatile Solids
49.81
%
6/1/2021
SM 2540 G
AYO
Fecal Coliforms
< 6.45
MPN/gram
6/1/2021
SM 9221 C E
AYO
Sample ID:
T2B
Date Collected:
6/3/2021
Collected By:
WILLIAMS
Time Collected:
0830
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.38
6/3/2021
SM
2540
G
AYO
% Volatile Solids
52.80
%
6/3/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
6/8/2021
Collected By:
WILLIAMS
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.03
%
6/8/2021
SM
2540
G
AYO
% Volatile Solids
52.24
%
6/8/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
6/8/2021
Collected By:
WILLIAMS
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.09
%
6/8/2021
SM
2540
G
AYO
% Volatile Solids
54.04
%
6/8/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 2 of 8

Sample ID:
FEED
Date Collected:
6/8/2021
Collected By:
WILLIAMS
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.98
%
6/8/2021
SM
2540
G
AYO
% Volatile Solids
63.81
%
6/8/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
6/8/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.86
6/8/2021
SM 2540 G
AYO
% Volatile Solids
49.97
%
6/8/2021
SM 2540 G
AYO
Fecal Coliforms
< 6.27
MPN/gram
6/8/2021
SM 9221 C E
AYO
Sample ID:
T2B
Date Collected:
6/10/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.15
%
6/10/2021
SM
2540
G
AYO
% Volatile Solids
53.17
%
6/10/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
6/10/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.29
%
6/10/2021
SM
2540
G
AYO
% Volatile Solids
54.89
%
6/10/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 3 of 8

Sample ID:
FEED
Date Collected:
6/10/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.11
%
6/10/2021
SM
2540
G
AYO
% Volatile Solids
64.62
%
6/10/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
6/15/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.09
%
6/15/2021
SM
2540
G
AYO
% Volatile Solids
50.11
%
6/15/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
6/15/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.52
%
6/15/2021
SM
2540
G
AYO
% Volatile Solids
53.70
%
6/15/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
6/15/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.03
%
6/15/2021
SM
2540
G
AYO
% Volatile Solids
65.00
%
6/15/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 4 of 8

Sample ID:
CROM
Date Collected:
6/15/2021
Collected By:
WILLIAMS
Time Collected:
0850
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.86
%
6/15/2021
SM
2540 G
AYO
% Volatile Solids
50.46
%
6/15/2021
SM
2540 G
AYO
Fecal Coliforms
< 6.27
MPN/gram
6/15/2021
SM
9221 C E
AYO
Sample ID:
T2B
Date Collected:
6/17/2021
Collected By:
WILLIAMS
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.57
%
6/17/2021
SM
2540
G
AYO
% Volatile Solids
65.38
%
6/17/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
6/17/2021
Collected By:
WILLIAMS
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.33
%
6/17/2021
SM
2540
G
AYO
% Volatile Solids
56.06
%
6/17/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
6/17/2021
Collected By:
WILLIAMS
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.91
%
6/17/2021
SM
2540
G
AYO
% Volatile Solids
66.05
%
6/17/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 5 of 8

Sample ID:
T2B
Date Collected:
6/22/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.38
%
6/22/2021
SM
2540
G
AYO
% Volatile Solids
50.35
%
6/22/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
6/22/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.41
%
6/22/2021
SM
2540
G
AYO
% Volatile Solids
53.24
%
6/22/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
6/22/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.06
%
6/22/2021
SM
2540
G
AYO
% Volatile Solids
64.56
%
6/22/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
6/22/2021
Collected By:
DROSKI
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.78
%
6/22/2021
SM
2540 G
AYO
% Volatile Solids
50.27
%
6/22/2021
SM
2540 G
AYO
Fecal Coliforms
< 6.45
MPN/gram
6/22/2021
SM
9221 C E
AYO
Page 6 of 8

Sample ID:
T2B
Date Collected:
6/24/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.36
%
6/24/2021
SM
2540
G
AYO
% Volatile Solids
50.12
%
6/24/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
6/24/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.66
%
6/24/2021
SM
2540
G
AYO
% Volatile Solids
53.56
%
6/24/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
6/24/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.01
%
6/24/2021
SM
2540
G
AYO
% Volatile Solids
64.98
%
6/24/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
BELT PRESS
Date Collected:
6/24/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
18.11
%
6/24/2021
SM
2540
G
AYO
% Volatile Solids
43.87
%
6/24/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 7 of 8

Sample ID:
T2B
Date Collected:
6/29/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.89
%
6/29/2021
SM
2540
G
AYO
% Volatile Solids
50.07
%
6/29/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
6/29/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.85
%
6/29/2021
SM
2540
G
AYO
% Volatile Solids
52.36
%
6/29/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
6/29/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.59
%
6/29/2021
SM
2540
G
AYO
% Volatile Solids
64.40
%
6/29/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
6/29/2021
Collected By:
WILLIAMS
Time Collected:
0830
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.77
%
6/29/2021
SM
2540 G
AYO
% Volatile Solids
49.76
%
6/29/2021
SM
2540 G
AYO
Fecal Coliforms
< 6.45
MPN/gram
6/29/2021
SM
9221 C E
AYO
Certified By:
REN D. ACOSTA
Page 8 of 8

MCB CAMLEJ ELS
ATAD BENCH -SCALE VOLATILE SOLIDS REDUCTION ANALYSIS
Sample Date
Sample ID
Temp
(°C)
DO
(mg/L)
% TS
% VS
% VS Avg
Analyst
4/12/2021
BENCH
19 2
6 88
1.93
51.38
51.15
DES
BENCH-DUP
1.91
50.92
4/19/2021
BENCH
19.4
7 39
1.83
49.83
50.13
DES
BENCH-DUP
1.83
50.42
4/27/2021
BENCH
17.2
9.21
1.54
49.90
49.84
DES
BENCH-DUP
1.54
49.78
5/3/2021
BENCH
21.4
8 38
1.37
51.32
51.14
ALB
BENCH-DUP
1.38
50.95
5/11/2021
BENCH
20.5
8.43
1.35
48.63
48.66
ALB/DES
BENCH-DUP
1.36
48.68
5/17/2021
BENCH
20.1
8 71
1.27
49.97
49.99
ALB/AYO
BENCH-DUP
1.28
50.01
5/24/2021
BENCH
24.7
8.36
1.27
49.72
49.65
ALB
BENCH-DUP
1.26
49.57
INITIAL VS (%)
51.15
FINAL VS (%)
49.65
VS
REDUCTION
2.9%
VS REDUCTION = (INITIAL VS - FINAL VS) / INITIAL VS X 100
*VS REDUCTION MUST BE < 15% TO MEET VECTOR ATTRACTION REDUCTION REQUIREMENTS
REV. 01/2020

REPORT NO. 2021 BSQTR2
Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application
Report No.: 2021 BSQTR2
Date of Report: 06/02/2021
Lab ID:
227
Date Collected:
4/12/2021
Time Collected:
0719
Collected By:
AYO
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.93
%
4/12/2021
SM
2540
G
DES
B-S
% Volatile Solids
51.38
%
4/12/2021
SM
2540
G
DES
B-S DUP
% Total Solids
1.91
%
4/12/2021
SM
2540
G
DES
B-S DUP
% Volatile Solids
50.92
%
4/12/2021
SM
2540
G
DES
QUALITY CONTROL - 4/12/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.92 %
1.0 %
% Volatile Solids
51.15 %
0.9 %
Date Collected:
4/19/2021
Time Collected:
0905
Collected By:
AYO
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.83
%
4/20/2021
SM
2540
G
DES
B-S
% Volatile Solids
49.83
%
4/20/2021
SM
2540
G
DES
B-S DUP
% Total Solids
1.83
%
4/20/2021
SM
2540
G
DES
B-S DUP
% Volatile Solids
50.42
%
4/20/2021
SM
2540
G
DES
QUALITY CONTROL - 4/19/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.83 %
0 %
% Volatile Solids
50.13 %
1.2 %
Page 1 of 4

REPORT NO. 2021 BSQTR2
Date Collected:
4/27/2021
Time Collected:
1033
Collected By:
DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.54
%
4/27/2021
SM
2540
G
DES
B-S
% Volatile Solids
49.90
%
4/27/2021
SM
2540
G
DES
B-S DUP
% Total Solids
1.54
%
4/27/2021
SM
2540
G
DES
B-S DUP
% Volatile Solids
49.78
%
4/27/2021
SM
2540
G
DES
QUALITY CONTROL - 4/27/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.54
0 %
% Volatile Solids
48.84 %
0.2 %
Date Collected:
5/3/2021
Time Collected:
0830
Collected By:
DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.37
%
5/4/2021
SM
2540
G
ALB
B-S
% Volatile Solids
51.32
%
5/4/2021
SM
2540
G
ALB
B-S DUP
% Total Solids
1.38
%
5/4/2021
SM
2540
G
ALB
B-S DUP
% Volatile Solids
50.95
%
5/4/2021
SM
2540
G
ALB
QUALITY CONTROL - 5/3/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.38 %
0.7 %
% Volatile Solids
51.14 %
0.7 %
Page 2 of 4

REPORT NO. 2021 BSQTR2
Date Collected:
5/11/2021
Time Collected:
1440
Collected By:
ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.35
%
5/11/2021
SM
2540
G
ALB/DES
B-S
% Volatile Solids
48.63
%
5/11/2021
SM
2540
G
ALB/DES
B-S DUP
% Total Solids
1.36
%
5/11/2021
SM
2540
G
ALB/DES
B-S DUP
% Volatile Solids
48.68
%
5/11/2021
SM
2540
G
ALB/DES
QUALITY CONTROL - 5/11/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.36 %
0.7 %
% Volatile Solids
48.66 %
0.1 %
Date Collected:
5/17/2021
Time Collected:
0725
Collected By:
AYO
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.27
%
5/18/2021
SM
2540
G
ALB/AYO
B-S
% Volatile Solids
49.97
%
5/18/2021
SM
2540
G
ALB/AYO
B-S DUP
% Total Solids
1.28
%
5/18/2021
SM
2540
G
ALB/AYO
B-S DUP
% Volatile Solids
50.01
%
5/18/2021
SM
2540
G
ALB/AYO
QUALITY CONTROL - 5/17/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.28 %
0.8 %
% Volatile Solids
49.99 %
0.1 %
Page 3 of 4

REPORT NO. 2021 BSQTR2
Date Collected:
5/24/2021
Time Collected:
1300
Collected By:
ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.27
%
5/25/2021
SM
2540
G
ALB
B-S
% Volatile Solids
49.72
%
5/25/2021
SM
2540
G
ALB
B-S DUP
% Total Solids
1.26
%
5/25/2021
SM
2540
G
ALB
B-S DUP
% Volatile Solids
49.57
%
5/25/2021
SM
2540
G
ALB
QUALITY CONTROL - 5/24/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.27 %
0.8 %
% Volatile Solids
49.65 %
0.3 %
*B-S: BENCH -SCALE
6-WEEK VOLATILE SOLIDS REDUCTION
2.9 %
Certified By:
REN D. ACOSTA
Page 4 of 4

Enclosure (1)
MCB CAMLEJ ELS
ATAD BENCH -SCALE WORKSHEET
CI = ](navy n residuals concentration
V l = Volume of residuals
i 2 = Needed concentration (2°0I
V2 = Knovyn final volume (l.)
Date Setup:
Date DO>2.0 mg/L: I-t . 212`
2-1
24
(Cl )(VD tC2) (V2)
.2� uvr}=(2)(24)
Vl=48,( 3.79
1I { .) L ( Residuals req, )
24[.- L= L(Efl:req.)
DaTemp.
rate
CC)
D'
(mg l F
Anal}st
lime Collected
I
IA
1-• _ ? -2--E
0.2-
60. ,aJ
a
oil -
2
.r
'4.1' .• _(
tom[.6
..
3
'-1. 1-'z i
ZU , l
4-1
'{- t5.1a›j
7,.
_;
4i 71
1ei
TT°
k
6
- 4. (6[. W�
1 q. 4
1, `..\
oci 6v_
1-
4''
4 c1. (0,.
87
0
+l--o-'{�]~`Fl
d i. / 1�+ 1
1 r LG+
//'��-'�
Lr /1
III
4-
4,,9,2243./y
5
(GA
ti
,,,-,t.-_)-1.:2_6-2.1
0, -
ci '1-1
.`").g5
10`)i-.?
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94.3
',Two;
7i. i[7-L
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17
V*1
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AL S
r8
R
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-21lD
A-I,F
19
1
A5 l,-2,1
17.1
Ac
P
. (D e
,. c
-A
_2(}
71
`1c.,1
2.0.G
0- •5
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22
1Al
C- 0- fl
i` • D
.---'`-•
73
114
( C/2 20-2-1
? -1i
r
25
14
6•11.' ►mot
.k
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a
() y<
26
' ' `153. 24
ri . t..,
77
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i 1 ` ` .4
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28
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24• -
74
29
bit
S.'V.. Zt
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q .3t?
A
AL
( i �7
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"1'
GJ' 7
242,1 ` .2'
t
1)5
REV FEB 2020
i tS-0. Z( # 0

3RD QUARTER
Pathogen and Vector Attraction Reduction Form
and Lab Sheets

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: US MCB CAMP LEJEUNE
WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune Advanced WWTP
Monitoring Period: From
7/ 1 /2021
NPDES Number: NC0063029
To 9/30/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (timeitemp) ©
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing)
■
Alt.D (No Prior Test) •
I
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost •
Heat Drying ❑
Heat Treatment •
Thermophilic J .
I
Beta Ray •
Gamma Ray ❑
Pasteurization •
Class B:
Alt. (1) Fecal Density 0
Alt. (2) Process to Significantly Reduce Pathogens ❑
I
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization •
Air Drying 0
Composting 0 'Aerobic
Digestion 'i i
Anaerobic Digestion ❑
i
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number or
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
niaue
Minimum
Geo. Mean
Maximum
['nits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFI.
1000 mpn per _ram
of total solid (dry
weight)
3.81
7.3
33.96
Gram'
0
Weekly
Grab
9221 E
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
❑
Alt. 2 (40-day bench)
■
Alt. 3 (30-day bench) tni
Alt. 4 (Spec. 02 uptake)
❑
Alt. 5 (14-Day Aerobic)
❑
Alt. 6 (Alk. Stabilization
•
Alt 7 (Drying - Stable) 0
Alt. 8 (Drying - Unstable)
•
Alt. 9 (Injection)
0
Alt. 10 (Incorporation)
■
No vector attraction reduction alternatives were performed
0
CERTIFICATION STATEMENT (please check the appropriate statement)
0
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Charles Scozzari, Su - ry tor, WW/Land App. Charles Scozzari, Sur isor, WW/Land App.
Preparer Nam an ig'e (type or print) Land Applier , me ;g (if applicable)(type or print)
Signatuof Preparer* Da a Signature .Lands r (if applicable) a e
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102
6)

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: 8/02/2021
Report No.: 2021-JUL ATAD
Lab ID: 227
Sample ID:
T2B
Date Collected:
7/1/2021
Collected By:
DROSKI
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.39
7/1/2021
SM
2540
G
AYO
% Volatile Solids
51.35
%
7/1/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
7/1/2021
Collected By:
DROSKI
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.45
7/1/2021
SM
2540
G
AYO
% Volatile Solids
52.42
%
7/1/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4A
Date Collected:
7/1/2021
Collected By:
DROSKI
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.85
%
7/1/2021
SM
2540
G
AYO
% Volatile Solids
62.21
%
7/1/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 1 of 7

Sample ID:
T2B
Date Collected:
7/6/2021
Collected By:
DROSKI
Time Collected:
0702
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.26
%
7/6/2021
SM
2540
G
AYO
% Volatile Solids
51.90
%
7/6/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
7/6/2021
Collected By:
DROSKI
Time Collected:
0702
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.36
7/6/2021
SM
2540
G
AYO
% Volatile Solids
52.79
%
7/6/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4A
Date Collected:
7/6/2021
Collected By:
DROSKI
Time Collected:
0702
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.46
%
7/6/2021
SM
2540
G
AYO
% Volatile Solids
57.74
%
7/6/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
7/6/2021
Collected By:
DROSKI
Time Collected:
0702
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
7.29
%
7/6/2021
SM
2540
G
AYO
% Volatile Solids
62.44
%
7/6/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 2 of 7

Sample ID:
CROM
Date Collected:
7/6/2021
Collected By:
DROSKI
Time Collected:
0718
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.76
%
7/6/2021
SM 2540 G
AYO
% Volatile Solids
51.12
%
7/6/2021
SM 2540 G
AYO
Fecal Coliforms
< 6.50
MPN/gram
7/6/2021
SM 9221 C E
AYO
Sample ID:
T2B
Date Collected:
7/8/2021
Collected By:
WILLIAMS
Time Collected:
0845
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.33
7/8/2021
SM
2540
G
DES
% Volatile Solids
51.23
%
7/8/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
7/8/2021
Collected By:
WILLIAMS
Time Collected:
0845
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.73
%
7/8/2021
SM
2540
G
DES
% Volatile Solids
52.08
%
7/8/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
7/8/2021
Collected By:
WILLIAMS
Time Collected:
0845
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.57
%
7/8/2021
SM
2540
G
DES
% Volatile Solids
60.95
%
7/8/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 3 of 7

Sample ID:
T3B
Date Collected:
7/13/2021
Collected By:
DROSKI
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.40
%
7/13/2021
SM
2540
G
DES
% Volatile Solids
52.72
%
7/13/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
7/13/2021
Collected By:
DROSKI
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.31
%
7/13/2021
SM
2540
G
DES
% Volatile Solids
67.23
%
7/13/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
7/13/2021
Collected By:
DROSKI
Time Collected:
0724
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.73
%
7/13/2021
SM
2540 G
DES
% Volatile Solids
50.37
%
7/13/2021
SM
2540 G
DES
Fecal Coliforms
< 6.57
MPN/gram
7/13/2021
SM
9221 C E
DES
Sample ID:
T3B
Date Collected:
7/15/2021
Collected By:
DROSKI
Time Collected:
0737
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.44
%
7/15/2021
SM
2540
G
DES
% Volatile Solids
53.21
%
7/15/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 4 of 7

Sample ID:
T3B
Date Collected:
7/20/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.30
%
7/20/2021
SM
2540
G
DES
% Volatile Solids
51.39
%
7/20/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4A
Date Collected:
7/20/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.51
%
7/20/2021
SM
2540
G
DES
% Volatile Solids
62.78
%
7/20/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
7/20/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.91
%
7/20/2021
SM
2540
G
DES
% Volatile Solids
7.62
%
7/20/2021
SM
2540
G
DES
Fecal Coliforms
NOT
ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
7/20/2021
Collected By:
DROSKI
Time Collected:
0746
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.69
%
7/20/2021
SM
2540 G
DES
% Volatile Solids
49.65
%
7/20/2021
SM
2540 G
DES
Fecal Coliforms
< 6.67
MPN/gram
7/20/2021
SM
9221 C E
DES
Page 5of7

Sample ID:
T3B
Date Collected:
7/22/2021
Collected By:
DROSKI
Time Collected:
0707
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.32
%
7/22/2021
SM
2540
G
DES
% Volatile Solids
52.02
%
7/22/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4A
Date Collected:
7/22/2021
Collected By:
DROSKI
Time Collected:
0707
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.35
%
7/22/2021
SM
2540
G
DES
% Volatile Solids
59.15
%
7/22/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
7/27/2021
Collected By:
DROSKI
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.34
%
7/27/2021
SM
2540
G
DES
% Volatile Solids
52.30
%
7/27/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4A
Date Collected:
7/27/2021
Collected By:
DROSKI
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.10
%
7/27/2021
SM
2540
G
DES
% Volatile Solids
54.89
%
7/27/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 6 of 7

Sample ID:
FEED
Date Collected:
7/27/2021
Collected By:
DROSKI
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
6.21
%
7/27/2021
SM
2540
G
DES
% Volatile Solids
64.41
%
7/27/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
7/27/2021
Collected By:
DROSKI
Time Collected:
0733
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.68
%
7/27/2021
SM
2540 G
DES
% Volatile Solids
49.50
%
7/27/2021
SM
2540 G
DES
Fecal Coliforms
< 6.72
MPN/gram
7/27/2021
SM
9221 C E
DES
Certified By:
REN D. ACOSTA
Page 7 of 7

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: 9/02/2021
Report No.: 2021-AUG ATAD
Lab ID: 227
Sample ID:
T4A
Date Collected:
8/3/2021
Collected By:
J. ACOSTA
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.90
8/3/2021
SM
2540
G
ALB
% Volatile Solids
60.87
%
8/3/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
8/3/2021
Collected By:
J. ACOSTA
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.63
8/3/2021
SM
2540
G
ALB
% Volatile Solids
61.24
%
8/3/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
8/3/2021
Collected By:
J. ACOSTA
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.78
%
8/3/2021
SM 2540 G
ALB
% Volatile Solids
49.82
%
8/3/2021
SM 2540 G
ALB
Fecal Coliforms
< 6.47
MPN/gram
8/3/2021
SM 9221 C E
ALB
Page 1 of 5

Sample ID:
T4A
Date Collected:
8/5/2021
Collected By:
J. ACOSTA
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.57
%
8/10/2021
SM
2540
G
ALB
% Volatile Solids
61.01
%
8/10/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
8/10/2021
Collected By:
J. ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.64
8/10/2021
SM
2540
G
ALB
% Volatile Solids
52.26
%
8/10/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
8/10/2021
Collected By:
J. ACOSTA
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.53
%
8/10/2021
SM
2540
G
ALB
% Volatile Solids
53.62
%
8/10/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
8/10/2021
Collected By:
J. ACOSTA
Time Collected:
0737
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.71
%
8/10/2021
SM
2540 G
ALB
% Volatile Solids
48.88
%
8/10/2021
SM
2540 G
ALB
Fecal Coliforms
< 6.64
MPN/gram
8/10/2021
SM
9221 C E
ALB
Page 2of5

Sample ID:
T4B
Date Collected:
8/12/2021
Collected By:
DROSKI
Time Collected:
0707
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.73
%
8/12/2021
SM
2540
G
ALB
% Volatile Solids
50.08
%
8/12/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
8/17/2021
Collected By:
J. ACOSTA
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.79
8/17/2021
SM
2540
G
DES
% Volatile Solids
47.41
%
8/17/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
8/17/2021
Collected By:
J. ACOSTA
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.87
%
8/17/2021
SM
2540
G
DES
% Volatile Solids
54.67
%
8/17/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
8/17/2021
Collected By:
J. ACOSTA
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.82
%
8/17/2021
SM
2540 G
DES
% Volatile Solids
50.44
%
8/17/2021
SM
2540 G
DES
Fecal Coliforms
< 6.38
MPN/gram
8/17/2021
SM
9221 C E
DES
Page 3of5

Sample ID:
T3A
Date Collected:
8/18/2021
Collected By:
J. ACOSTA
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.52
%
8/24/2021
SM
2540
G
ALB
% Volatile Solids
53.60
%
8/24/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
8/24/2021
Collected By:
J. ACOSTA
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.80
%
8/24/2021
SM
2540
G
ALB
% Volatile Solids
52.13
%
8/24/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
8/24/2021
Collected By:
J. ACOSTA
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.46
%
8/24/2021
SM
2540
G
ALB
% Volatile Solids
58.14
%
8/24/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
8/24/2021
Collected By:
J. ACOSTA
Time Collected:
0723
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.91
%
8/24/2021
SM
2540 G
ALB
% Volatile Solids
49.29
%
8/24/2021
SM
2540 G
ALB
Fecal Coliforms
< 6.19
MPN/gram
8/24/2021
SM
9221 C E
LA
Page 4 of 5

Sample ID:
T3B
Date Collected:
8/31/2021
Collected By:
SCOZZARI
Time Collected:
0830
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.46
%
8/31/2021
SM
2540
G
ALB
% Volatile Solids
49.57
%
8/31/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4A
Date Collected:
8/31/2021
Collected By:
SCOZZARI
Time Collected:
0830
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.89
%
8/31/2021
SM
2540
G
ALB
% Volatile Solids
46.70
%
8/31/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
8/31/2021
Collected By:
SCOZZARI
Time Collected:
0830
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.10
%
8/31/2021
SM
2540 G
ALB
% Volatile Solids
48.91
%
8/31/2021
SM
2540 G
ALB
Fecal Coliforms
< 5.81
MPN/gram
8/31/2021
SM
9221 C E
AYO
Certified By:
REN D. ACOSTA
Page 5of5

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: 10/08/2021
Report No.: 2021-SEP ATAD
Lab ID: 227
Sample ID:
T3B
Date Collected:
9/2/2021
Collected By:
S. SCOZZARI
Time Collected:
0845
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.83
9/7/2021
SM
2540
G
AYO
% Volatile Solids
51.07
%
9/7/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4A
Date Collected:
9/2/2021
Collected By:
S. SCOZZARI
Time Collected:
0845
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.62
9/7/2021
SM
2540
G
AYO
% Volatile Solids
52.69
%
9/7/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4A
Date Collected:
9/7/2021
Collected By:
DROSKI
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.36
%
9/7/2021
SM
2540
G
AYO
% Volatile Solids
51.26
%
9/7/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 1 of 7

Sample ID:
FEED
Date Collected:
9/7/2021
Collected By:
DROSKI
Time Collected:
0720
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.07
%
9/7/2021
SM
2540
G
AYO
% Volatile Solids
57.00
%
9/7/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
9/7/2021
Collected By:
DROSKI
Time Collected:
0744
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.73
9/7/2021
SM 2540 G
AYO
% Volatile Solids
46.31
%
9/7/2021
SM 2540 G
AYO
Fecal Coliforms
3.81
MPN/gram
9/7/2021
SM 9221 C E
AYO
Sample ID:
T4B
Date Collected:
9/9/2021
Collected By:
DROSKI
Time Collected:
0655
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.55
%
9/14/2021
SM
2540
G
AYO
% Volatile Solids
46.98
%
9/14/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3A
Date Collected:
9/14/2021
Collected By:
DROSKI
Time Collected:
0738
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.33
%
9/14/2021
SM
2540
G
AYO
% Volatile Solids
52.21
%
9/14/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 2 of 7

Sample ID:
T4B
Date Collected:
9/14/2021
Collected By:
DROSKI
Time Collected:
0738
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.19
%
9/14/2021
SM
2540
G
AYO
% Volatile Solids
46.31
%
9/14/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
9/14/2021
Collected By:
DROSKI
Time Collected:
0738
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.77
9/14/2021
SM
2540
G
AYO
% Volatile Solids
56.19
%
9/14/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
9/14/2021
Collected By:
DROSKI
Time Collected:
0752
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
2.79
%
9/14/2021
SM
2540
G
AYO
% Volatile Solids
47.86
%
9/14/2021
SM
2540
G
AYO
Fecal Coliforms
6.43
MPN/gram
9/14/2021
SM
9221
C E
AYO
Sample ID:
T3B
Date Collected:
9/16/2021
Collected By:
RUBERTE
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.58
%
9/20/2021
SM
2540
G
AYO
% Volatile Solids
52.88
%
9/20/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 3 of 7

Sample ID:
T4B
Date Collected:
9/16/2021
Collected By:
RUBERTE
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.07
%
9/20/2021
SM
2540
G
AYO
% Volatile Solids
47.71
%
9/20/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
9/21/2021
Collected By:
RUBERTE
Time Collected:
0814
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.13
%
9/23/2021
SM
2540
G
AYO
% Volatile Solids
49.42
%
9/23/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
9/21/2021
Collected By:
RUBERTE
Time Collected:
0814
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.95
%
9/23/2021
SM
2540
G
AYO
% Volatile Solids
46.27
%
9/23/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
9/21/2021
Collected By:
RUBERTE
Time Collected:
0814
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.36
%
9/23/2021
SM
2540
G
AYO
% Volatile Solids
58.44
%
9/23/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 4 of 7

Sample ID:
CROM
Date Collected:
9/21/2021
Collected By:
RUBERTE
Time Collected:
0826
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
1.68
%
9/23/2021
SM
2540 G
AYO
% Volatile Solids
51.78
%
9/23/2021
SM
2540 G
AYO
Fecal Coliforms
10.59
MPN/gram
9/21/2021
SM
9221 C E
AYO
Sample ID:
T3B
Date Collected:
9/23/2021
Collected By:
RUBERTE
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.28
%
9/23/2021
SM
2540
G
AYO
% Volatile Solids
48.91
%
9/23/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
9/23/2021
Collected By:
RUBERTE
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.90
%
9/23/2021
SM
2540
G
AYO
% Volatile Solids
46.22
%
9/23/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
9/28/2021
Collected By:
RUBERTE
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.53
%
9/28/2021
SM
2540
G
AYO
% Volatile Solids
48.31
%
9/28/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 5of7

Sample ID:
T3B
Date Collected:
9/28/2021
Collected By:
RUBERTE
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.22
%
9/28/2021
SM
2540
G
AYO
% Volatile Solids
49.34
%
9/28/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
9/28/2021
Collected By:
RUBERTE
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.04
%
9/28/2021
SM
2540
G
AYO
% Volatile Solids
47.99
%
9/28/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
9/28/2021
Collected By:
RUBERTE
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.73
%
9/28/2021
SM
2540
G
AYO
% Volatile Solids
58.57
%
9/28/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
9/28/2021
Collected By:
RUBERTE
Time Collected:
0810
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
0.52
%
9/28/2021
SM
2540 G
AYO
% Volatile Solids
64.88
%
9/28/2021
SM
2540 G
AYO
Fecal Coliforms
33.96
MPN/gram
9/28/2021
SM
9221 C E
AYO
Page 6 of 7

Sample ID:
T2B
Date Collected:
9/30/2021
Collected By:
RUBERTE
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.49
%
9/30/2021
SM
2540
G
AYO
% Volatile Solids
48.98
%
9/30/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
9/30/2021
Collected By:
RUBERTE
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.14
%
9/30/2021
SM
2540
G
AYO
% Volatile Solids
50.84
%
9/30/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
9/30/2021
Collected By:
RUBERTE
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.95
%
9/30/2021
SM
2540
G
AYO
% Volatile Solids
48.71
%
9/30/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
9/30/2021
Collected By:
RUBERTE
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
1.75
%
9/30/2021
SM
2540
G
AYO
% Volatile Solids
49.87
%
9/30/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Certified By:
REN D. ACOSTA
Page 7 of 7

REPORT NO. 2021 BSQTR3
Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application
Report No.: 2021 BSQTR3
Date of Report: 09/10/2021
Lab ID:
227
Date Collected:
7/26/2021
Time Collected:
0700
Collected By:
ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
2.07
%
7/27/2021
SM
2540
G
DES
B-S
% Volatile Solids
49.68
%
7/27/2021
SM
2540
G
DES
B-S DUP
% Total Solids
2.07
%
7/27/2021
SM
2540
G
DES
B-S DUP
% Volatile Solids
49.75
%
7/27/2021
SM
2540
G
DES
QUALITY CONTROL - 7/26/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
2.07 %
0 %
% Volatile Solids
49.72 %
0.1 %
Date Collected:
8/2/2021
Time Collected:
0715
Collected By:
ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.86
%
8/3/2021
SM
2540
G
ALB
B-S
% Volatile Solids
50.41
%
8/3/2021
SM
2540
G
ALB
B-S DUP
% Total Solids
1.87
%
8/3/2021
SM
2540
G
ALB
B-S DUP
% Volatile Solids
50.19
%
8/3/2021
SM
2540
G
ALB
QUALITY CONTROL -8/02/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.87 %
0.5 %
% Volatile Solids
50.30 %
0.4 %
Page 1 of 4

REPORT NO. 2021 BSQTR3
Date Collected:
8/9/2021
Time Collected:
ALB
Collected By:
0650
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.90
%
8/10/2021
SM
2540
G
ALB
B-S
% Volatile Solids
49.73
%
8/10/2021
SM
2540
G
ALB
B-S DUP
% Total Solids
1.91
%
8/10/2021
SM
2540
G
ALB
B-S DUP
% Volatile Solids
49.79
%
8/10/2021
SM
2540
G
ALB
QUALITY CONTROL - 8/09/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.91
0.5 %
% Volatile Solids
49.76 %
0.1 %
Date Collected:
8/16/2021
Time Collected:
1300
Collected By:
DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.79
%
8/17/2021
SM
2540
G
DES
B-S
% Volatile Solids
48.20
%
8/17/2021
SM
2540
G
DES
B-S DUP
% Total Solids
1.80
%
8/17/2021
SM
2540
G
DES
B-S DUP
% Volatile Solids
48.50
%
8/17/2021
SM
2540
G
DES
QUALITY CONTROL - 8/16/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.80 %
0.6 %
% Volatile Solids
48.35 %
0.6 %
Page 2 of 4

REPORT NO. 2021 BSQTR3
Date Collected:
8/23/2021
Time Collected:
0740
Collected By:
ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.83
%
8/24/2021
SM
2540
G
ALB
B-S
% Volatile Solids
47.70
%
8/24/2021
SM
2540
G
ALB
B-S DUP
% Total Solids
1.84
%
8/24/2021
SM
2540
G
ALB
B-S DUP
% Volatile Solids
47.83
%
8/24/2021
SM
2540
G
ALB
QUALITY CONTROL - 8/23/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.84 %
0.5 %
% Volatile Solids
47.77 %
0.3 %
Date Collected:
8/30/2021
Time Collected:
0707
Collected By:
ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.83
%
8/31/2021
SM
2540
G
ALB
B-S
% Volatile Solids
47.46
%
8/31/2021
SM
2540
G
ALB
B-S DUP
% Total Solids
1.84
%
8/31/2021
SM
2540
G
ALB
B-S DUP
% Volatile Solids
47.55
%
8/31/2021
SM
2540
G
ALB
QUALITY CONTROL - 8/30/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.84 %
0.5 %
% Volatile Solids
47.51 %
0.2 %
Page 3 of 4

REPORT NO. 2021 BSQTR3
Date Collected:
9/3/2021
Time Collected:
ALB
Collected By:
0735
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
1.78
%
9/7/2021
SM
2540
G
AYO
B-S
% Volatile Solids
47.36
%
9/7/2021
SM
2540
G
AYO
B-S DUP
% Total Solids
1.78
%
9/7/2021
SM
2540
G
AYO
B-S DUP
% Volatile Solids
46.73
%
9/7/2021
SM
2540
G
AYO
QUALITY CONTROL - 9/2/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
1.78 %
0 %
% Volatile Solids
47.05 %
1.3 %
*B-S: BENCH -SCALE
6-WEEK VOLATILE SOLIDS REDUCTION
5.4 %
Certified By:
REN D. ACOSTA
Page 4 of 4

MCB CAMLEJ ELS
ATAD BENCH -SCALE VOLATILE SOLIDS REDUCTION ANALYSIS
Sample Date
Sample ID
Temp
( g�)
% TS
% VS
% VS Avg
Analyst
7/26/2021
BENCH
24.6
3.9
2.07
49.68
49.72
DES
BENCH-DUP
2.07
49.75
8/2/2021
BENCH
25.0
6 97
1.86
50.41
50.30
ALB
BENCH-DUP
1.87
50.19
8/9/2021
BENCH
23.9
7 98
1.90
49.73
49.76
ALB
BENCH-DUP
1.91
49.79
8/16/2021
BENCH
25.9
6.2
1.79
48.20
48.35
DES
BENCH-DUP
1.80
48.50
8/23/2021
BENCH
25.1
7.05
1.83
47.70
47.77
ALB
BENCH-DUP
1.84
47.83
8/30/2021
BENCH
25 4
7 28
1.83
47.46
47.51
ALB
BENCH-DUP
1.84
47.55
9/3/2021
BENCH
20.9
8.19
1.78
47.36
47.05
AYO
BENCH-DUP1.78
46.73
INITIAL VS (%)
49.72
FINAL VS (%)
47.05
VS
REDUCTION
5.4%
VS REDUCTION = (INITIAL VS - FINAL VS) / INITIAL VS X 100
*VS REDUCTION MUST BE < 15% TO MEET VECTOR ATTRACTION REDUCTION REQUIREMENTS
REV. 01/2020

4TH QUARTER
Pathogen and Vector Attraction Reduction Form
and Lab Sheets

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: US MCB CAMP LEJEUNE
WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune Advanced WWTP
Monitoring Period: From
10/ 1 /2021
NPDES Number: NC0063029
To 12/31/2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
n I
Alt B (Alk Treatment) ■
I Alt. C (Prior Testing)
■
A
A1t.D (No Prior Test) •
I
Process to Further Reduce Pathogengs ■
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying
•
Heat Treatment
•
Thermophilic
M
I
Beta Ray
Gamma Ray •
Pasteurization •
Class B:
Alt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens ❑
•
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0
Air Drying ❑ I
Composting •
Aerobic Digestion (. I
Anaerobic Digestion Q
1
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Analyhcar
Tech-
nii.q_i_
Parameter
Allowable Level
in Sludge
g
Pathogen Density
o
NumberFrequency
Excee-
dences
of Analysis
Sample
Type
yp
Minimum
Geo. Mean
Maximum
Units
_
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
'Ft
1000 mpn per gramMPN
oftotal solid (dry
weight)
3.36
5.48
25.71
r
Gram
0
Weekly
_
Grab
92 ME
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 drams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
0
Alt. 2 (40-day bench) ■
Alt. 3 (30-day bench) 0
Alt. 4 (Spec. 0, uptake)
❑
Alt. 5 (14-Day Aerobic)
•
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable)
❑
Alt. 9 (Injection)
•
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed
•
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Charles Scozzari, Supervisor, WV/Land App. Charles Scozzari, • - rvisor,11 VV/Land App.
Preparer Nam j . n le (type or print) Land Applies amid Title (if applicable)(type or print)
Signat = of ' = r* D e Signatu of Landes: +tier if applicable) Date
g � sa g ( PP )
*Prep er is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .110 (26)

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: 11/02/2021
Report No.: 2021-OCT ATAD
Lab ID: 227
Sample ID:
T2B
Date Collected:
10/05/2021
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.40
10/5/2021
SM
2540 G
DES
% Volatile Solids
49.12
%
10/5/2021
SM
2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221 C E
Sample ID:
T3B
Date Collected:
10/05/2021
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.24
10/5/2021
SM
2540 G
DES
% Volatile Solids
49.41
%
10/5/2021
SM
2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221 C E
Sample ID:
T4B
Date Collected:
10/05/2021
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.34
%
10/5/2021
SM
2540 G
DES
% Volatile Solids
50.53
%
10/5/2021
SM
2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221 C E
Page 1 of 8

Sample ID:
FEED
Date Collected:
10/05/2021
Collected By:
DROSKI
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.57
10/5/2021
SM
2540 G
DES
% Volatile Solids
60.41
%
10/5/2021
SM
2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221 C E
Sample ID:
CROM
Date Collected:
10/05/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.21
10/5/2021
SM
2540 G
DES
% Volatile Solids
45.02
%
10/5/2021
SM
2540 G
DES
Fecal Coliforms
3.47
MPN/gram
10/5/2021
SM
9221 C E
DES
Sample ID:
T2B
Date Collected:
10/7/2021
Collected By:
DROSKI
Time Collected:
0747
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.33
%
10/7/2021
SM
2540
G
DES
% Volatile Solids
48.33
%
10/7/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
10/7/2021
Collected By:
DROSKI
Time Collected:
0747
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.03
%
10/7/2021
SM
2540
G
DES
% Volatile Solids
56.61
%
10/7/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 2 of 8

Sample ID:
T4B
Date Collected:
10/7/2021
Collected By:
DROSKI
Time Collected:
0747
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.29
10/7/2021
SM
2540 G
DES
% Volatile Solids
44.26
%
10/7/2021
SM
2540 G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221 C E
Sample ID:
T2B
Date Collected:
10/12/2021
Collected By:
WILLIAMS
Time Collected:
0705
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.51
10/12/2021
SM
2540
G
AYO
% Volatile Solids
49.68
%
10/12/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
10/12/2021
Collected By:
WILLIAMS
Time Collected:
0705
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.28
%
10/12/2021
SM
2540
G
AYO
% Volatile Solids
47.85
%
10/12/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
10/12/2021
Collected By:
WILLIAMS
Time Collected:
0705
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.30
%
10/12/2021
SM
2540
G
AYO
% Volatile Solids
49.74
%
10/12/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 3 of 8

Sample ID:
FEED
Date Collected:
10/12/2021
Collected By:
WILLIAMS
Time Collected:
0705
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.77
%
10/12/2021
SM
2540
G
AYO
% Volatile Solids
59.71
%
10/12/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
10/12/2021
Collected By:
WILLIAMS
Time Collected:
0746
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
0.70
%
10/12/2021
SM
2540
G
AYO
% Volatile Solids
60.21
%
10/12/2021
SM
2540
G
AYO
Fecal Coliforms
25.71
MPN/gram
10/12/2021
SM
9221
C E
AYO
Sample ID:
T3B
Date Collected:
10/14/2021
Collected By:
WILLIAMS
Time Collected:
0825
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.54
%
10/14/2021
SM
2540
G
AYO
% Volatile Solids
48.42
%
10/14/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
10/14/2021
Collected By:
WILLIAMS
Time Collected:
0825
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.21
%
10/14/2021
SM
2540
G
AYO
% Volatile Solids
49.23
%
10/14/2021
SM
2540
G
AYO
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 4 of 8

Sample ID:
T2B
Date Collected:
10/19/2021
Collected By:
WILLIAMS
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.68
%
10/19/2021
SM
2540
G
DES
% Volatile Solids
50.71
%
10/19/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
10/19/2021
Collected By:
WILLIAMS
Time Collected:
0710
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.28
%
10/19/2021
SM
2540
G
DES
% Volatile Solids
49.12
%
10/19/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
10/19/2021
Collected By:
WILLIAMS
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.70
%
10/19/2021
SM
2540
G
DES
% Volatile Solids
45.51
%
10/19/2021
SM
2540
G
DES
Fecal Coliforms
4.86
MPN/gram
10/19/2021
SM
9221
C E
DES
Sample ID:
T2B
Date Collected:
10/21/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.42
%
10/21/2021
SM
2540
G
DES
% Volatile Solids
55.35
%
10/21/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 5 of 8

Sample ID:
T3B
Date Collected:
10/21/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.07
%
10/21/2021
SM
2540
G
DES
% Volatile Solids
51.53
%
10/21/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
10/26/2021
Collected By:
RUBERTE
Time Collected:
0738
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.04
%
10/28/2021
SM
2540
G
DES
% Volatile Solids
51.30
%
10/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
10/26/2021
Collected By:
RUBERTE
Time Collected:
0738
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.98
%
10/28/2021
SM
2540
G
DES
% Volatile Solids
49.34
%
10/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
10/26/2021
Collected By:
RUBERTE
Time Collected:
0738
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.36
%
10/28/2021
SM
2540
G
DES
% Volatile Solids
55.80
%
10/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 6 of 8

Sample ID:
FEED
Date Collected:
10/26/2021
Collected By:
RUBERTE
Time Collected:
0738
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.36
%
10/28/2021
SM
2540
G
DES
% Volatile Solids
59.44
%
10/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
10/26/2021
Collected By:
RUBERTE
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.87
%
10/28/2021
SM
2540
G
DES
% Volatile Solids
45.19
%
10/28/2021
SM
2540
G
DES
Fecal Coliforms
11.63
MPN/gram
10/28/2021
SM
2540
G
DES
Sample ID:
T3B
Date Collected:
10/28/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.96
%
10/28/2021
SM
2540
G
DES
% Volatile Solids
49.09
%
10/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
10/28/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.12
%
10/28/2021
SM
2540
G
DES
% Volatile Solids
51.12
%
10/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 7 of 8

Sample ID:
T4B
Date Collected:
10/28/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.27
%
10/28/2021
SM
2540
G
DES
% Volatile Solids
56.05
%
10/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
10/28/2021
Collected By:
WILLIAMS
Time Collected:
0700
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.79
%
10/28/2021
SM
2540
G
DES
% Volatile Solids
58.69
%
10/28/2021
SM
2540
G
DES
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Certified By:
REN D. ACOSTA
Page 8 of 8

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: 12/09/2021
Report No.: 2021-NOV ATAD
Lab ID: 227
Sample ID:
T2B
Date Collected:
11/2/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.08
%
11/2/2021
SM
2540
G
ALB
% Volatile Solids
51.90
%
11/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
11/2/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.89
%
11/2/2021
SM
2540
G
ALB
% Volatile Solids
49.09
%
11/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T4B
Date Collected:
11/2/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.10
%
11/2/2021
SM
2540
G
ALB
% Volatile Solids
51.79
%
11/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 1 of 6

Sample ID:
FEED
Date Collected:
11/2/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.83
%
11/2/2021
SM
2540
G
ALB
% Volatile Solids
58.46
%
11/2/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
11/2/2021
Collected By:
DROSKI
Time Collected:
0743
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.89
%
11/2/2021
SM
2540
G
ALB
% Volatile Solids
45.43
%
11/2/2021
SM
2540
G
ALB
Fecal Coliforms
5.14
MPN/gram
11/2/2021
SM
9221
C E
ALB
Sample ID:
T2B
Date Collected:
11/4/2021
Collected By:
DROSKI
Time Collected:
0757
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.98
%
11/4/2021
SM
2540
G
ALB
% Volatile Solids
51.73
%
11/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3A
Date Collected:
11/4/2021
Collected By:
DROSKI
Time Collected:
0757
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.73
%
11/4/2021
SM
2540
G
ALB
% Volatile Solids
49.97
%
11/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 2 of 6

Sample ID:
T4B
Date Collected:
11/4/2021
Collected By:
DROSKI
Time Collected:
0757
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.21
%
11/4/2021
SM
2540
G
ALB
% Volatile Solids
52.84
%
11/4/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
11/9/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.04
%
11/9/2021
SM
2540
G
ALB
% Volatile Solids
51.39
%
11/9/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
11/9/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.66
%
11/9/2021
SM
2540
G
ALB
% Volatile Solids
60.45
%
11/9/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
11/9/2021
Collected By:
DROSKI
Time Collected:
0746
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.77
%
11/9/2021
SM
2540
G
ALB
% Volatile Solids
46.20
%
11/9/2021
SM
2540
G
ALB
Fecal Coliforms
4.77
MPN/gram
11/9/2021
SM
9221
C E
ALB
Page 3 of 6

Sample ID:
T2B
Date Collected:
11/16/2021
Collected By:
DROSKI
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.84
%
11/16/2021
SM
2540
G
ALB
% Volatile Solids
50.22
%
11/16/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3A
Date Collected:
11/16/2021
Collected By:
DROSKI
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.11
%
11/16/2021
SM
2540
G
ALB
% Volatile Solids
56.86
%
11/16/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
11/16/2021
Collected By:
DROSKI
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.61
%
11/16/2021
SM
2540
G
ALB
% Volatile Solids
61.91
%
11/16/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
11/16/2021
Collected By:
DROSKI
Time Collected:
0739
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.33
%
11/16/2021
SM
2540
G
ALB
% Volatile Solids
46.59
%
11/16/2021
SM
2540
G
ALB
Fecal Coliforms
5.41
MPN/gram
11/16/2021
SM
9221
C E
ALB
Page 4 of 6

Sample ID:
T2B
Date Collected:
11/18/2021
Collected By:
DROSKI
Time Collected:
0728
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.01
%
11/23/2021
SM
2540
G
ALB
% Volatile Solids
51.54
%
11/23/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3A
Date Collected:
11/18/2021
Collected By:
DROSKI
Time Collected:
0728
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.96
%
11/23/2021
SM
2540
G
ALB
% Volatile Solids
55.76
%
11/23/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
11/23/2021
Collected By:
DROSKI
Time Collected:
0733
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.94
%
11/23/2021
SM
2540
G
ALB
% Volatile Solids
50.95
%
11/23/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
11/23/2021
Collected By:
DROSKI
Time Collected:
0740
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.31
%
11/23/2021
SM
2540
G
ALB
% Volatile Solids
49.20
%
11/23/2021
SM
2540
G
ALB
Fecal Coliforms
5.44
MPN/gram
11/23/2021
SM
9221
C E
ALB
Page 5 of 6

Sample ID:
T2B
Date Collected:
11/26
Collected By:
WILLIAMS
Time Collected:
0830
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.90
%
11/30/2021
SM
2540
G
ALB
% Volatile Solids
50.52
%
11/30/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
11/30/2021
Collected By:
WILLIAMS
Time Collected:
0725
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.93
%
11/30/2021
SM
2540
G
ALB
% Volatile Solids
62.68
%
11/30/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
11/30/2021
Collected By:
WILLIAMS
Time Collected:
0840
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.02
%
11/30/2021
SM
2540
G
ALB
% Volatile Solids
49.32
%
11/30/2021
SM
2540
G
ALB
Fecal Coliforms
5.94
MPN/gram
11/30/2021
SM
9221
C E
DES
Certified By:
REN D. ACOSTA
Page 6 of 6

Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client:
MCB CAMLEJ Land Application Date of Report: 01/06/2022
Report No.: 2021-DEC ATAD
Lab ID: 227
Sample ID:
FEED
Date Collected:
12/02/2021
Collected By:
RUBERTE
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.24
%
12/02/2021
SM
2540
G
ALB
%
Volatile Solids
65.37
%
12/02/2021
SM
2540
G
ALB
Fecal Coliforms
NOT
ANALYZED
MPN/gram
SM
9221 C
E
Sample ID:
FEED
Date Collected:
12/07/2021
Collected By:
DROSKI
Time Collected:
0734
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.24
%
12/07/2021
SM
2540
G
DES
%
Volatile Solids
67.05
%
12/07/2021
SM
2540
G
DES
Fecal Coliforms
NOT
ANALYZED
MPN/gram
SM
9221 C
E
Sample ID:
CROM
Date Collected:
12/07/2021
Collected By:
DROSKI
Time Collected:
0735
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.52
%
12/07/2021
SM
2540
G
DES
%
Volatile Solids
45.27
%
12/07/2021
SM
2540
G
DES
Fecal Coliforms
3.96
MPN/gram
12/07/2021
SM
9221 C
E
DES
Page 1 of 6

Sample ID:
T2A
Date Collected:
12/14/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.84
%
12/14/2021
SM
2540
G
ALB
% Volatile Solids
52.33
%
12/14/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3A
Date Collected:
12/14/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.96
%
12/14/2021
SM
2540
G
ALB
% Volatile Solids
55.32
%
12/14/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
12/14/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.82
%
12/14/2021
SM
2540
G
ALB
% Volatile Solids
65.47
%
12/14/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
12/14/2021
Collected By:
WILLIAMS
Time Collected:
0800
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.60
%
12/14/2021
SM
2540
G
ALB
% Volatile Solids
44.47
%
12/14/2021
SM
2540
G
ALB
Fecal Coliforms
3.90
MPN/gram
12/14/2021
SM
9221
C E
ALB
Page 2 of 6

Sample ID:
T2A
Date Collected:
12/16/2021
Collected By:
DROSKI
Time Collected:
0802
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.41
%
12/21/2021
SM
2540
G
ALB
% Volatile Solids
60.70
%
12/21/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3A
Date Collected:
12/16/2021
Collected By:
DROSKI
Time Collected:
0802
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.44
%
12/21/2021
SM
2540
G
ALB
% Volatile Solids
64.12
%
12/21/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T2B
Date Collected:
12/21/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
3.82
%
12/21/2021
SM
2540
G
ALB
% Volatile Solids
51.04
%
12/21/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
12/21/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.27
%
12/21/2021
SM
2540
G
ALB
% Volatile Solids
53.59
%
12/21/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 3 of 6

Sample ID:
FEED
Date Collected:
12/21/2021
Collected By:
WILLIAMS
Time Collected:
1027
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.82
%
12/21/2021
SM
2540
G
ALB
% Volatile Solids
66.99
%
12/21/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
12/21/2021
Collected By:
WILLIAMS
Time Collected:
0750
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.04
%
12/21/2021
SM
2540
G
ALB
% Volatile Solids
44.21
%
12/21/2021
SM
2540
G
ALB
Fecal Coliforms
3.56
MPN/gram
12/21/2021
SM
9221
C E
ALB
Sample ID:
T2B
Date Collected:
12/23/2021
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.01
%
12/28/2021
SM
2540
G
ALB
% Volatile Solids
55.96
%
12/28/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
12/23/2021
Collected By:
WILLIAMS
Time Collected:
0715
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.25
%
12/28/2021
SM
2540
G
ALB
% Volatile Solids
63.38
%
12/28/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Page 4 of 6

Sample ID:
T2B
Date Collected:
12/28/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.55
%
12/28/2021
SM
2540
G
ALB
% Volatile Solids
54.72
%
12/28/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
T3B
Date Collected:
12/28/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.51
%
12/28/2021
SM
2540
G
ALB
% Volatile Solids
59.92
%
12/28/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
FEED
Date Collected:
12/28/2021
Collected By:
WILLIAMS
Time Collected:
0730
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
4.79
%
12/28/2021
SM
2540
G
ALB
% Volatile Solids
67.28
%
12/28/2021
SM
2540
G
ALB
Fecal Coliforms
NOT ANALYZED
MPN/gram
SM
9221
C E
Sample ID:
CROM
Date Collected:
12/28/2021
Collected By:
WILLIAMS
Time Collected:
0745
Analyte
Results
Units
Date
Analyzed
Method
Analyzed By
% Total Solids
5.35
%
12/28/2021
SM
2540
G
ALB
% Volatile Solids
44.44
%
12/28/2021
SM
2540
G
ALB
Fecal Coliforms
3.36
MPN/gram
12/28/2021
SM
9221
C E
LA
Page 5 of 6

Certified By:
REN D. ACOSTA
Page 6 of 6

REPORT NO. 2021 BSQTR4
Marine Corps Installations East - Marine Corps Base Camp Lejeune
Environmental Quality Branch, Environmental Laboratory Section
FC436 Gonzalez Blvd, Camp Lejeune, NC 28547
Client: MCB CAMLEJ Land Application
Report No.: 2021 BSQTR4
Date of Report: 11/16/2021
Lab ID:
227
Date Collected:
10/7/2021
Time Collected:
1404
Collected By:
AYO
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
0.32
%
10/7/2021
SM
2540
G
DES
B-S
% Volatile Solids
56.95
%
10/7/2021
SM
2540
G
DES
B-S DUP
% Total Solids
0.32
%
10/7/2021
SM
2540
G
DES
B-S DUP
% Volatile Solids
56.72
%
10/7/2021
SM
2540
G
DES
QUALITY CONTROL - 10/7/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
0.32 %
0 %
% Volatile Solids
56.84 %
0.4 %
Date Collected:
10/12/2021
Time Collected:
0752
Collected By:
AYO
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
0.31
%
10/12/2021
SM
2540
G
AYO
B-S
% Volatile Solids
57.32
%
10/12/2021
SM
2540
G
AYO
B-S DUP
% Total Solids
0.32
%
10/12/2021
SM
2540
G
AYO
B-S DUP
% Volatile Solids
57.28
%
10/12/2021
SM
2540
G
AYO
QUALITY CONTROL - 10/12/2021
B-S/B-S DUP
Average
%RPD
% Total Solids
0.32 %
3.1 %
% Volatile Solids
57.30 %
0.1 %
Page 1 of 3

REPORT NO. 2021_BSQTR4
Date Collected:
10/18/2021
Time Collected:
AYO
Collected By:
0742
Sample ID
Anaiyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
0.27
%
10/19/2021
SM 2540 G
DES
B-S
% Volatile Solids
53.54
%
10/19/2021
SM 2540 G
DES
B-S DUP
% Total Solids
0.27
%
10/19/2021
SM 2540 G
DES
B-S DUP
% Volatile Solids
53.63
%
10/19/2021
SM 2540 G
DES
QUALITY CONTROL — 10/18/2021
B-S/B-S DUP
A„erege
%RPD
% Total Solids
0.27
0 %
% Volatile Solids
53.59 %
0.2 %
Date Collected:
10/25/2021
Time Collected:
0830
Collected By:
DES
Sample ID
Anaiyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Totei Solids
0.28
%
10/28/2021
SM 2540 G
DES
B-S
% Volatile Solids
52.20
%
10/28/2021
SM 2540 G
DES
B-S DUP
% Total Solids
0.28
%
10/28/2021
SM 2540 G
DES
B-S DUP
% Volatile Solids
53.12
%
10/28/2021
SM 2540 G
DES
QUALITY CONTROL — 10/25/2021
B-S/B-S DUP
A„erege
%RPD
% Total Solids
0.28 %
0 %
% Volatile Solids
52.66 %
1.7 %
Page 2 of 3

REPORT N0. 2021_BSQTR4
Date Collected:
11/1/2021
Time Collected:
0720
Collected By:
DES
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
0.30
%
11/2/2021
SM 2540 G
ALB
B-S
% Volatile Solids
52.87
%
11/2/2021
SM 2540 G
ALB
B-S DUP
% Total Solids
0.30
%
11/2/2021
SM 2540 G
ALB
B-S DUP
% Volatile Solids
53.57
%
11/2/2021
SM 2540 G
ALB
QUALITY CONTROL — 11/1/2021
B-S/B-S DUP
A„erege
%RPD
% Total Solids
0.30 %
0
% Volatile Solids
53.22 %
1.3 %
Date Collected:
11/5/2021
Time Collected:
0753
Collected By:
ALB
Sample ID
Analyte
Results
Units
Date Analyzed
Method
Analyzed By
B-S
% Total Solids
0.27
%
11/9/2021
SM 2540 G
ALB
B-S
% Volatile Solids
52.68
%
11/9/2021
SM 2540 G
ALB
B-S DUP
% Total Solids
0.27
%
11/9/2021
SM 2540 G
ALB
B-S DUP
% Volatile Solids
52.37
%
11/9/2021
SM 2540 G
ALB
QUALITY CONTROL — 11/5/2021
B-S/B-S DUP
A„erege
%RPD
% Total Solids
0.27 %
0 %
% Volatile Solids
52.53 %
0.6 %
*B-S: BENCH -SCALE
6-WEEK VOLATILE SOLIDS REDUCTION
7.6 %
Certified By:
Page 3 of 3

MCB CAMLEJ ELS
ATAD BENCH -SCALE VOLATILE SOLIDS REDUCTION ANALYSIS
Sample Date
Sample ID
Temp
(°C)
DO
(mg/L)
% TS
% VS
% VS Avg
Analyst
10/7/2021
BENCH
23.6
g 3
0.32
56.95
56.84
DES
BENCH-DUP
0.32
56.72
10/12/2021
BENCH
21 2
7 4
0.31
57.32
57.30
ALB
BENCH-DUP
0.32
57.28
10/18/2021
BENCH
16.2
9.9
0.27
53.54
53.59
ALB
BENCH-DUP
0.27
53.63
10/25/2021
BENCH
21.4
9.0
0.28
52.20
52.66
DES
BENCH-DUP
0.28
53.12
11/1/2021
BENCH
15.6
9.9
0.3
52.87
53.22
ALB
BENCH-DUP
0.3
53.57
11/5/2021
BENCH
12.9
10.8
0.27
52.68
52.53
ALB
BENCH-DUP
0.27
52.37
INITIAL VS (%)
56.84
FINAL VS (%)
52.53
VS
REDUCTION
7.6%
VS REDUCTION = (INITIAL VS - FINAL VS) / INITIAL VS X 100
*VS REDUCTION MUST BE < 15% TO MEET VECTOR ATTRACTION REDUCTION REQUIREMENTS
REV. 01/2020