WQ0035720_Residual Annual Report 2021_20220126

Non -Discharge Branch Upload/Submittal Form
NORTH CAROLINA
EnWrvnmemfal Qualify
Version 2 - Revised June 23, 2020
Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?*
Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0035720
Applicant/Permittee Denali Water Solutions LLC
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name*
Jeff J Retzke
Email Address* Phone Number*
[e-mail] 2565034300
Project Information
Application/Document Type *
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deg.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Permit Number: *
Applicant/Permittee Address*
Facility Name*
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
WQ0035720
Has Current Existing permit number
3308 Bernice Avenue, Russellville, AR 72802
Denali Water Solutions Class A Residuals Program
Please provide comments/notes on your current submittal below.
High -Rate Infiltration
Reclaimed Water
Residuals
Other
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2021 Annual Report Lake Kilby WTP.pdf 3.28MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 1/26/2022

Denali
WATER SOLUTIONS
January 26, 2022
3308 Bernice Avenue
Russellville, AR 72802
PO Box 3036 • Russellville, AR 72811
Phone: [phone]
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: 2021 Annual Report - Distribution of Class A Residuals: Denali Water
Solutions (Lake Kilby Water Treatment Plant) Permit No. WQ0035720
To Whom it May Concern:
Denali Water Solutions is submitting the required 2021 Annual Report for Permit No.
WQ0035720. This permit is associated with the distribution of water treatment residuals
produced at the City of Portsmouth - Lake Kilby Water Treatment Plant located in Suffolk,
Virginia, with distribution in Gates County, North Carolina.
This Annual Report contains the following information:
• Form DMSDF
• Form RSSF
• Lab Reports
If you have any questions, or need any additional information, please do not hesitate to
contact me at [phone] or via email at [e-mail].
Sincerely,
Jeff Retzke
Senior Environmental Manager, East Region
cc: Richard Hurr (Water Plant Manager, City of Portsmouth, Virginia)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0035720 FACILITY NAME: Lake Kilby Water Treatment Plant
PHONE: [phone] COUNTY: OPERATOR: Richard Hurr (Water Plant Manager)
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes No ❑ -* If No skip parts A, B, C and certify form below
0
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
Lake Kilby WTP
0
218.8
218.8
Ed Miller Farms
218.8
Soil Amendment
February
March
April
May
June
July
August
September
Lake Kilby WTP
0
340.84
340.84
Ed Miller Farms
340.84
Soil Amendment
October
Lake Kilby WTP
0
935.43
935.43
Ed Miller Farms
935.43
Soil Amendment
November
Lake Kilby WTP
0
332.55
332.62
Ed Miller Farms
332.62
Soil Amendment
December
Total from FORM DMSDF (sup)
Totals:
Annual (dry tons):
0
1827.62
1827.69
1827.69
Amendment(s) used:
Bulking Agent(s) used:
DMSDF (Supp)
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit o Yes
(including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
'144-
Signature of Permittee
1/26/22
Date Signature ofPreparer**
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
Suffolk, VA
DENR FORM DMSDF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0035720
Facility Name: Lake Kilby WTP
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
Laboratory: 1) Waypoint Analytical, Richmond, VA
2)
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
(mg/kg)a
Sample or Composite Date
11/4/20
9/21/21
9/21/21
10/5/21
10/5/21
10/20/21
10/20/21
Max
Percent Solids (%)
NA
17.1
16.5
16.4
16.7
16.6
17.9
16.9
17.9
Arsenic
75
9.3
7.27
7.87
13.4
13.2
7.54
7.93
13.4
Cadmium
85
0.585
0.606
0.61
0.599
0.602
0.559
0.592
0.61
Copper
4,300
37.8
117
92.1
61.7
37
79.9
83.4
117
Chromium
NA
133
144
145
140
134
131
137
145
Lead
840
14.2
7.52
6.89
10.7
8.73
10
11
14.2
Mercury
57
0.0912
0.0818
0.0841
0.0946
0.0897
0.0754
0.0822
0.0946
Molybdenum
75
1.46
1.79
1.83
1.5
1.51
2.44
2.78
2.78
Nickel
420
13.3
10.1
10.2
9.82
9.46
11.7
12.4
13.3
Selenium
100
4.49
10.4
9.45
2.99
3.01
2.79
2.96
10.4
Zinc
7,500
74.9
46.9
45.3
87.4
71.1
115
120
120
Total Phosphorus
NA
1060
1080
1070
1180
1080
1160
1220
1220
TKN
NA
10500
9450
14200
16900
14200
17400
13600
17400
Ammonia -Nitrogen
NA
292
606
1090
1260
602
620
592
1260
Nitrate and Nitrite
NA
31.1
29.9
31.3
32.6
60.2
46.5
36.8
60.2
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permi for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
� 1 /26/22
ure of Sign iPrep er
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

Waypoint
ANALYTICAL
11/16/2020
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 20-310-0005
Project Description: Lake Kilby WTP 2019 5&6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.tom
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/5/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
c ciy
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypoint,
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Sample Summary Table
Report Number: 20-310-0005
Client Project Description: Lake Kilby WTP 2019 5&6
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
74112 5 Solids 11/04/2020 11:40 11/05/2020
74112 5 Solids 11/04/2020 11:40 11/05/2020 4500NO3F-2011 WP MTN
74112 5 Solids 11/04/2020 11:40 11/05/2020 SW-7471B WP MTN
74112 5 Solids 11/04/2020 11:40 11/05/2020 SM-4500-NH3C WP MTN
74112 5 Solids 11/04/2020 11:40 11/05/2020 6010D WP MTN
74112 5 Solids 11/04/2020 11:40 11/05/2020 SM-2540G WP MTN
74112 5 Solids 11/04/2020 11:40 11/05/2020 AOAC 955.01 WP MTN
74112 5 Solids 11/04/2020 11:40 11/05/2020 9045D WP MTN
74112 5 Solids 11/04/2020 11:40 11/05/2020 SM-4500-NH3C-TKN WP MTN
74113 6 Solids 11/04/2020 11:40 11/05/2020
74113 6 Solids 11/04/2020 11:40 11/05/2020 SM-4500-NH3C-TKN WP MTN
74113 6 Solids 11/04/2020 11:40 11/05/2020 SM-4500-NH3C WP MTN
74113 6 Solids 11/04/2020 11:40 11/05/2020 SM-2540G WP MTN
74113 6 Solids 11/04/2020 11:40 11/05/2020 4500NO3F-2011 WP MTN
74113 6 Solids 11/04/2020 11:40 11/05/2020 AOAC 955.01 WP MTN
74113 6 Solids 11/04/2020 11:40 11/05/2020 9045D WP MTN
74113 6 Solids 11/04/2020 11:40 11/05/2020 SW-7471B WP MTN
74113 6 Solids 11/04/2020 11:40 11/05/2020 6010D WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2019 5&6
Information :
Report Number :20-310-0005 REPORT OF ANALYSIS
Lab No : 74112
Sample ID : 5
Report Date : 11/16/2020
Received : 11/05/2020
%'�QU GJG
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 11/ 4/ 2020 11:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture 83.7
Calcium Carbonate Equivalent 9.7 % - dry
Test Results Units
0.010 1 11/09/20 17:05 FMM SM-2540G
0.1 1 11/09/20 10:25 DXT AOAC 955.01
MQL
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen 681 mg/Kg - dry 153 1 11/12/20 14:30 JPJ SM-4500-NH3C
Nitrate+Nitrite-N <31.0 mg/Kg - dry 31.0 1 11/12/20 15:47 CLP 4500NO3F-2011
Organic N 12300 mg/Kg - dry 1530 1 11/12/20 10:00 CALCULATION
pH 6.7 s.u. 1 11/09/20 16:44 ADM 9045D
Total Solids 16.3 % 0.010 1 11/09/20 17:05 FMM SM-2540G
Total Volatile Solids 51.8 % 0.010 1 11/09/20 17:05 FMM SM-2540G
Total Kjeldahl Nitrogen 13000 mg/Kg - dry 1530 1 11/12/20 10:00 JPJ ;M-4500-NH3C-TKI`
Phosphorus 1190 mg/Kg - dry 30.7 1 11/12/20 00:10 TJS 6010D
Aluminum 96300 mg/Kg - dry 307 10 11/12/20 19:06 TJS 6010D
Arsenic 9.45 mg/Kg - dry 3.07 1 11/12/20 00:10 TJS 6010D
Calcium 1500 mg/Kg - dry 307 1 11/12/20 00:10 TJS 6010D
Cadmium <0.613 mg/Kg - dry 0.613 1 11/12/20 00:10 TJS 6010D
Chromium 148 mg/Kg - dry 1.53 1 11/12/20 00:10 TJS 6010D
Copper 43.3 mg/Kg - dry 3.07 1 11/12/20 00:10 TJS 6010D
Iron 22900 mg/Kg - dry 61.3 1 11/12/20 00:10 TJS 6010D
Lead 16.6 mg/Kg - dry 1.84 1 11/12/20 00:10 TJS 6010D
Qualifiers/
Definitions
B Analyte detected in blank DF Dilution Factor
L Limit Exceeded MQL Method Quantitation Limit
Page 3 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2019 5&6
Information :
Report Number :20-310-0005 REPORT OF ANALYSIS
Lab No : 74112
Sample ID : 5
Report Date : 11/16/2020
Received : 11/05/2020
%'�QU GJG
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 11/ 4/ 2020 11:40
Test Results Units MOL DF Date / Time By Analytical
Analyzed Method
Magnesium 724 mg/Kg - dry 30.7 1 11/12/20 00:10 TJS 6010D
Manganese 2360 mg/Kg - dry 3.07 1 11/12/20 00:10 TJS 6010D
Mercury <0.0871 mg/Kg - dry 0.0871 1 11/10/20 12:42 DDB SW-7471B
Molybdenum <1.53 mg/Kg - dry 1.53 1 11/12/20 00:10 TJS 6010D
Nickel 14.5 mg/Kg - dry 1.53 1 11/12/20 00:10 TJS 6010D
Potassium 125 mg/Kg - dry 61.3 1 11/12/20 00:10 TJS 6010D
Selenium 5.66 mg/Kg - dry 3.07 1 11/12/20 00:10 TJS 6010D
Sodium 291 mg/Kg - dry 153 1 11/12/20 00:10 TJS 6010D
Zinc 84.0 mg/Kg - dry 7.67 1 11/12/20 00:10 TJS 6010D
Sulfur 14800 mg/Kg - dry 61.3 1 11/12/20 00:10 TJS 6010D
Sodium Absorption Ratio <5.00 Ratio 5.00 1 11/12/20 00:10 CALCULATION
Qualifiers/
Definitions
B Analyte detected in blank DF Dilution Factor
L Limit Exceeded MQL Method Quantitation Limit
Page 4 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2019 5&6
Information :
Report Number :20-310-0005 REPORT OF ANALYSIS
Lab No : 74113
Sample ID : 6
Report Date : 11/16/2020
Received : 11/05/2020
%'�QU GJG
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 11/ 4/ 2020 11:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture 82.9 iyo
Calcium Carbonate Equivalent 9.2 % - dry
Test Results Units
0.010 1 11/09/20 17:05 FMM SM-2540G
0.1 1 11/09/20 10:25 DXT AOAC 955.01
MQL
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen 292 mg/Kg - dry 146 1 11/12/20 14:30 JPJ SM-4500-NH3C
Nitrate+Nitrite-N 31.1 mg/Kg - dry 30.1 1 11/12/20 15:48 CLP 4500NO3F-2011
Organic N 10200 mg/Kg - dry 1460 1 11/12/20 10:00 CALCULATION
pH 6.7 s.u. 1 11/09/20 16:44 ADM 9045D
Total Solids 17.1 % 0.010 1 11/09/20 17:05 FMM SM-2540G
Total Volatile Solids 52.4 % 0.010 1 11/09/20 17:05 FMM SM-2540G
Total Kjeldahl Nitrogen 10500 mg/Kg - dry 1460 1 11/12/20 10:00 JPJ ;M-4500-NH3C-TKI`
Phosphorus 1060 mg/Kg - dry 29.2 1 11/12/20 00:15 TJS 6010D
Aluminum 90600 mg/Kg - dry 292 10 11/12/20 19:11 TJS 6010D
Arsenic 9.30 mg/Kg - dry 2.92 1 11/12/20 00:15 TJS 6010D
Calcium 1350 mg/Kg - dry 292 1 11/12/20 00:15 TJS 6010D
Cadmium <0.585 mg/Kg - dry 0.585 1 11/12/20 00:15 TJS 6010D
Chromium 133 mg/Kg - dry 1.46 1 11/12/20 00:15 TJS 6010D
Copper 37.8 mg/Kg - dry 2.92 1 11/12/20 00:15 TJS 6010D
Iron 20300 mg/Kg - dry 58.5 1 11/12/20 00:15 TJS 6010D
Lead 14.2 mg/Kg - dry 1.75 1 11/12/20 00:15 TJS 6010D
Qualifiers/
Definitions
B Analyte detected in blank DF Dilution Factor
L Limit Exceeded MQL Method Quantitation Limit
Page 5 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2019 5&6
Information :
Report Number :20-310-0005 REPORT OF ANALYSIS
Lab No : 74113
Sample ID : 6
Report Date : 11/16/2020
Received : 11/05/2020
%'�QU GJG
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 11/ 4/ 2020 11:40
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Magnesium 655 mg/Kg - dry 29.2 1 11/12/20 00:15 TJS 6010D
Manganese 2110 mg/Kg - dry 2.92 1 11/12/20 00:15 TJS 6010D
Mercury <0.0912 mg/Kg - dry 0.0912 1 11/10/20 12:44 DDB SW-7471B
Molybdenum <1.46 mg/Kg - dry 1.46 1 11/12/20 00:15 TJS 6010D
Nickel 13.3 mg/Kg - dry 1.46 1 11/12/20 00:15 TJS 6010D
Potassium 116 mg/Kg - dry 58.5 1 11/12/20 00:15 TJS 6010D
Selenium 4.49 mg/Kg - dry 2.92 1 11/12/20 00:15 TJS 6010D
Sodium 271 mg/Kg - dry 146 1 11/12/20 00:15 TJS 6010D
Zinc 74.9 mg/Kg - dry 7.31 1 11/12/20 00:15 TJS 6010D
Sulfur 13200 mg/Kg - dry 58.5 1 11/12/20 00:15 TJS 6010D
Sodium Absorption Ratio <5.00 Ratio 5.00 1 11/12/20 00:15 CALCULATION
Qualifiers/
Definitions
B Analyte detected in blank DF Dilution Factor
Page 6 of 8

Waypoint..
ANALYTICAL
Customer Number: 07274
Customer Name: Denali Water
Report Number: 20-310-0005
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytica I.com
Shipment Receipt Form
Shipping Method
O Fed Ex O US Postal O Lab O Other :
® UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
®Yes 0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler? () Yes
Custody seals intact on sample bottles? 0 Yes
O No
O No
® Not Present
® Not Present
Chain of Custody (COC) present?
® Yes 0 No
COC agrees with sample label(s)?
® Yes 0 No
COC properly completed
® Yes O No
Samples in proper containers?
® Yes O No
Sample containers intact?
® Yes O No
Sufficient sample volume for indicated test(s)?
® Yes O No
All samples received within holding time?
® Yes 0 No
Cooler temperature in compliance?
® Yes O No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
® Yes O No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
O Yes
O Yes
O No
O No
® N/A
® N/A
Trip Blanks received with VOAs 0 Yes
O No ® N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
O No ® N/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes
Comments:
® No
Signature:
Brandi Watson
Date & Time:
Page 7 of 8
11/05/2020 13:34:49

SLI: Total Solids (Moisture) Total Kjeldahl Nitrogen, Phosphorus and Potassium
SL2: Basic Test SLI plus Sulfur. Calcium. MaMesium,Sodiunt, Iron, Aluminum, Manganese, Copper And Zinc
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium.
(Copper & Zinc included in SL2)
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)
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Page 8 of 8

Waypoint
ANALYTICAL
10/1/2021
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.tom
Ref: Analytical Testing
Revised Report Number: 21-265-9001 (Original Report 21-265-0001)
Project Description: Lake Kilby WTP 2021 1&2
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/22/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
G1oa7/
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypoint,
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Sample Summary Table
Report Number: 21-265-9001
Client Project Description: Lake Kilby WTP 2021 1&2
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
77861 1 Solids 09/22/2021
77861 1 Solids 09/22/2021 4500NO3F-2011 WP MTN
77861 1 Solids 09/22/2021 SW-7471B WP MTN
77861 1 Solids 09/22/2021 SM-4500-NH3C WP MTN
77861 1 Solids 09/22/2021 6010D WP MTN
77861 1 Solids 09/22/2021 SM-2540G WP MTN
77861 1 Solids 09/22/2021 AOAC 955.01 WP MTN
77861 1 Solids 09/22/2021 9045D WP MTN
77861 1 Solids 09/22/2021 SM-4500-NH3C-TKN WP MTN
77862 2 Solids 09/22/2021
77862 2 Solids 09/22/2021 SM-4500-NH3C-TKN WP MTN
77862 2 Solids 09/22/2021 SM-4500-NH3C WP MTN
77862 2 Solids 09/22/2021 SM-2540G WP MTN
77862 2 Solids 09/22/2021 4500NO3F-2011 WP MTN
77862 2 Solids 09/22/2021 AOAC 955.01 WP MTN
77862 2 Solids 09/22/2021 9045D WP MTN
77862 2 Solids 09/22/2021 SW-7471B WP MTN
77862 2 Solids 09/22/2021 6010D WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 21-265-9001
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2021 1&2
Information :
REPORT OF ANALYSIS
Original Report Date : 09/30/2021
Revised Report Date: 10/01/2021
Received : 09/22/2021
Lab No : 77861 Matrix: Solids
Sample ID : 1 Sampled:
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Total Solids 16.5 % 0.010 1 09/24/21 15:19 FMM SM-2540G
Calcium 1170 mg/Kg - dry 303 1 09/28/21 01:10 JTR 6010D
Iron 19000 mg/Kg - dry 60.6 1 09/28/21 01:10 JTR 6010D
Aluminum 235000 mg/Kg - dry 606 20 09/28/21 17:10 JTR 6010D
Zinc 46.9 mg/Kg - dry 7.58 1 09/28/21 01:10 JTR 6010D
Chromium 144 mg/Kg - dry 1.52 1 09/28/21 01:10 JTR 6010D
Arsenic 7.27 mg/Kg - dry 3.03 1 09/28/21 01:10 JTR 6010D
Mercury <0.0818 mg/Kg - dry 0.0818 1 09/24/21 14:54 TJS SW-7471B
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sodium Absorption Ratio <6.06 mg/Kg - dry 6.06 1 09/28/21 01:10 CALCULATION
Ammonia Nitrogen <606 mg/Kg - dry 606 1 09/29/21 13:00 JPJ SM-4500-NH3C
Organic N 9455 mg/Kg - dry 1515 1 09/29/21 11:00 DH CALCULATION
Phosphorus 1080 mg/Kg - dry 30.3 1 09/28/21 01:10 JTR 6010D
Cadmium <0.606 mg/Kg - dry 0.606 1 09/28/21 01:10 JTR 6010D
Copper 117 mg/Kg - dry 3.03 1 09/28/21 01:10 JTR 6010D
Lead 7.52 mg/Kg - dry 1.82 1 09/28/21 01:10 JTR 6010D
Manganese 1320 mg/Kg - dry 3.03 1 09/28/21 01:10 JTR 6010D
Nickel 10.1 mg/Kg - dry 1.52 1 09/28/21 01:10 JTR 6010D
Selenium 10.4 mg/Kg - dry 3.03 1 09/28/21 01:10 JTR 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 3 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 21-265-9001
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2021 1&2
Information :
REPORT OF ANALYSIS
Original Report Date : 09/30/2021
Revised Report Date: 10/01/2021
Received : 09/22/2021
Lab No : 77861 Matrix: Solids
Sample ID : 1 Sampled:
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sulfur 17100 mg/Kg - dry 60.6 1 09/28/21 01:10 JTR 6010D
Analytical Method: SM-2540G
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Moisture 83.5
010
0.010 1 09/24/21 15:19 FMM L575868
Total Kjeldahl Nitrogen 9450 mg/Kg - dry 1520 1 09/29/21 11:00 JPJ ;M-4500-NH3C-TKI`
Potassium 153 mg/Kg - dry 60.6 1 09/28/21 01:10 JTR 6010D
Magnesium 493 mg/Kg - dry 30.3 1 09/28/21 01:10 JTR 6010D
Sodium 275 mg/Kg - dry 152 1 09/28/21 01:10 JTR 6010D
Nitrate+Nitrite-N <29.9 mg/Kg - dry 29.9 1 09/27/21 13:36 ZBD 4500NO3F-2011
pH 7.0 s.u. 1 09/27/21 15:05 DRS 9045D
Calcium Carbonate Equivalent 8.6 % 0.1 1 09/28/21 08:45 DXT AOAC 955.01
Total Volatile Solids 49.3 % 0.010 1 09/24/21 15:19 FMM SM-2540G
Molybdenum 1.79 mg/Kg - dry 1.52 1 09/28/21 01:10 JTR 6010D
Qualifiers/
Definitions
B Analyte detected in blank DF Dilution Factor
H Beyond holding time MQL Method Quantitation Limit
Page 4 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 21-265-9001
Lab No : 77862
Sample ID : 2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2021 1&2
Information :
REPORT OF ANALYSIS
Original Report Date : 09/30/2021
Revised Report Date: 10/01/2021
Received : 09/22/2021
Matrix: Solids
Sampled:
Test
Results
Units
MQL
DF Date / Time
Analyzed
By Analytical
Method
Total Kjeldahl Nitrogen
Aluminum
Manganese
Copper
Cadmium
Lead
Calcium Carbonate Equivalent
Total Volatile Solids
Test
14200 mg/Kg - dry
215000 mg/Kg - dry
1250 mg/Kg - dry
92.1 mg/Kg - dry
<0.610 mg/Kg - dry
6.89 mg/Kg - dry
7.9
49.1
Results
Units
1520 1 09/29/21 11:00 JPJ ;M-4500-NH3C-TKI`
610 20 09/28/21 17:15
3.05 1 09/28/21 01:15
3.05 1 09/28/21 01:15
0.610 1 09/28/21 01:15
1.83 1 09/28/21 01:15
0.1 1 09/28/21 08:45
0.010 1 09/24/21 15:19
MQL
DF Date / Time
Analyzed
JTR 6010D
JTR 6010D
JTR 6010D
JTR 6010D
JTR 6010D
DXT AOAC 955.01
FMM SM-2540G
By Analytical
Method
Sodium Absorption Ratio
Ammonia Nitrogen
Nitrate+Nitrite-N
pH
Molybdenum
Potassium
Sodium
<6.10 mg/Kg - dry
1090 mg/Kg - dry
31.3 mg/Kg - dry
6.4 s.u.
1.83 mg/Kg - dry
145 mg/Kg - dry
260 mg/Kg - dry
6.10 1 09/28/21 01:15 CALCULATION
610 1 09/29/21 13:00 JPJ SM-4500-NH3C
29.2 1 09/27/21 13:37 ZBD 4500NO3F-2011
1 09/27/21 15:05 DRS 9045D
1.52 1 09/28/21 01:15 JTR 6010D
61.0 1 09/28/21 01:15 JTR 6010D
152 1 09/28/21 01:15 JTR 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L
Limit Exceeded
Page 5 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 21-265-9001
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2021 1&2
Information :
REPORT OF ANALYSIS
Original Report Date : 09/30/2021
Revised Report Date: 10/01/2021
Received : 09/22/2021
Lab No : 77862 Matrix: Solids
Sample ID : 2 Sampled:
Total Solids 16.4 % 0.010 1 09/24/21 15:19 FMM SM-2540G
Moisture 83.6 % 0.010 1 09/24/21 15:19 FMM SM-2540G
Phosphorus 1070 mg/Kg - dry 30.5 1 09/28/21 01:15 JTR 6010D
Sulfur 17300 mg/Kg - dry 61.0 1 09/28/21 01:15 JTR 6010D
Calcium 1160 mg/Kg - dry 305 1 09/28/21 01:15 JTR 6010D
Magnesium 497 mg/Kg - dry 30.5 1 09/28/21 01:15 JTR 6010D
Iron 19400 mg/Kg - dry 61.0 1 09/28/21 01:15 JTR 6010D
Zinc 45.3 mg/Kg - dry 7.62 1 09/28/21 01:15 JTR 6010D
Organic N 13120 mg/Kg - dry 1524 1 09/29/21 11:00 DH CALCULATION
Chromium 145 mg/Kg - dry 1.52 1 09/28/21 01:15 JTR 6010D
Nickel 10.2 mg/Kg - dry 1.52 1 09/28/21 01:15 JTR 6010D
Arsenic 7.87 mg/Kg - dry 3.05 1 09/28/21 01:15 JTR 6010D
Mercury <0.0841 mg/Kg - dry 0.0841 1 09/24/21 14:56 TJS SW-7471B
Selenium 9.45 mg/Kg - dry 3.05 1 09/28/21 01:15 JTR 6010D
Qualifiers/
Definitions
B Analyte detected in blank DF Dilution Factor
H Beyond holding time MQL Method Quantitation Limit
Page 6 of 8

Waypoint..
ANALYTICAL
Customer Number: 07274
Customer Name: Denali Water
Report Number: 21-265-0001
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytica I.com
Shipment Receipt Form
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
*Yes ONo
Number of coolers/boxes received
Custody seals intact on shipping container/cooler? U Yes
Custody seals intact on sample bottles? 0 Yes
O No
O No
* Not Present
* Not Present
Chain of Custody (COC) present?
Yes O No
COC agrees with sample label(s)?
Yes O No
COC properly completed
Yes O No
Samples in proper containers?
Yes O No
Sample containers intact?
Yes O No
Sufficient sample volume for indicated test(s)?
Yes O No
All samples received within holding time?
Yes O No
Cooler temperature in compliance?
0Yes @No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0Yes @No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
O Yes
O Yes
O No
O No
* N/A
* N/A
Trip Blanks received with VOAs 0 Yes
O No @N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
O No ON/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes
Comments:
• No
Signature:
Brandi Watson
Date & Time:
Page 7 of 8
09/22/2021 14:39:54

Special instructions or Remarks
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Page 8 of 8

Waypoint
ANALYTICAL
10/15/2021
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.tom
Ref: Analytical Testing
Revised Report Number: 21-279-9013 (Original Report 21-279-0013)
Project Description: Lake Kilby WTP 2021 1&2
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/6/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
G1oa7/
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypoint,
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Sample Summary Table
Report Number: 21-279-9013
Client Project Description: Lake Kilby WTP 2021 1&2
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
55004 3 Solids 10/05/2021 10/06/2021
55004 3 Solids 10/05/2021 10/06/2021 4500NO3F-2011 WP MTN
55004 3 Solids 10/05/2021 10/06/2021 SW-7471B WP MTN
55004 3 Solids 10/05/2021 10/06/2021 SM-4500-NH3C WP MTN
55004 3 Solids 10/05/2021 10/06/2021 6010D WP MTN
55004 3 Solids 10/05/2021 10/06/2021 SM-2540G WP MTN
55004 3 Solids 10/05/2021 10/06/2021 AOAC 955.01 WP MTN
55004 3 Solids 10/05/2021 10/06/2021 9045D WP MTN
55004 3 Solids 10/05/2021 10/06/2021 SM-4500-NH3C-TKN WP MTN
55005 4 Solids 10/05/2021 10/06/2021
55005 4 Solids 10/05/2021 10/06/2021 SM-4500-NH3C-TKN WP MTN
55005 4 Solids 10/05/2021 10/06/2021 SM-4500-NH3C WP MTN
55005 4 Solids 10/05/2021 10/06/2021 SM-2540G WP MTN
55005 4 Solids 10/05/2021 10/06/2021 4500NO3F-2011 WP MTN
55005 4 Solids 10/05/2021 10/06/2021 AOAC 955.01 WP MTN
55005 4 Solids 10/05/2021 10/06/2021 9045D WP MTN
55005 4 Solids 10/05/2021 10/06/2021 SW-7471B WP MTN
55005 4 Solids 10/05/2021 10/06/2021 6010D WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 21-279-9013
Lab No : 55004
Sample ID : 3
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2021 1&2
Information :
REPORT OF ANALYSIS
Original Report Date : 10/14/2021
Revised Report Date: 10/15/2021
Received : 10/06/2021
Matrix: Solids
Sampled: 10/5/2021 0:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Total Solids 16.7 % 0.010 1 10/12/21 16:12 FMM SM-2540G
Calcium 1060 mg/Kg - dry 299 1 10/13/21 20:00 JTR 6010D
Iron 21100 mg/Kg - dry 59.9 1 10/13/21 04:39 TJS 6010D
Aluminum 175000 mg/Kg - dry 299 10 10/13/21 20:05 JTR 6010D
Zinc 87.4 mg/Kg - dry 7.49 1 10/13/21 04:39 TJS 6010D
Chromium 140 mg/Kg - dry 1.50 1 10/13/21 04:39 TJS 6010D
Arsenic 13.4 mg/Kg - dry 2.99 1 10/13/21 04:39 TJS 6010D
Mercury <0.0946 mg/Kg - dry 0.0946 1 10/12/21 14:11 JW2 SW-7471B
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sodium Absorption Ratio <5.99 mg/Kg - dry 5.99 1 10/13/21 04:39 CALCULATION
Ammonia Nitrogen 1260 mg/Kg - dry 599 1 10/13/21 13:00 JPJ SM-4500-NH3C
Organic N 15620 mg/Kg - dry 1497 1 10/13/21 09:00 DH CALCULATION
Phosphorus 1180 mg/Kg - dry 29.9 1 10/13/21 04:39 TJS 6010D
Cadmium <0.599 mg/Kg - dry 0.599 1 10/13/21 04:39 TJS 6010D
Copper 61.7 mg/Kg - dry 2.99 1 10/13/21 20:00 JTR 6010D
Lead 10.7 mg/Kg - dry 1.80 1 10/13/21 04:39 TJS 6010D
Manganese 1310 mg/Kg - dry 2.99 1 10/13/21 04:39 TJS 6010D
Nickel 9.82 mg/Kg - dry 1.50 1 10/13/21 04:39 TJS 6010D
Selenium <2.99 mg/Kg - dry 2.99 1 10/13/21 04:39 TJS 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 3 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 21-279-9013
Lab No : 55004
Sample ID : 3
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2021 1&2
Information :
REPORT OF ANALYSIS
Original Report Date : 10/14/2021
Revised Report Date: 10/15/2021
Received : 10/06/2021
Matrix: Solids
Sampled: 10/ 5/ 2021 0:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sulfur 14000 mg/Kg - dry 59.9 1 10/13/21 20:00 JTR 6010D
Analytical Method: SM-2540G
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Moisture 83.3
010
0.010 1 10/12/21 16:12 FMM L578807
Total Kjeldahl Nitrogen 16900 mg/Kg - dry 1500 1 10/13/21 09:00 JPJ ;M-4500-NH3C-TKI`
Potassium 214 mg/Kg - dry 59.9 1 10/13/21 04:39 TJS 6010D
Magnesium 496 mg/Kg - dry 29.9 1 10/13/21 04:39 TJS 6010D
Sodium 262 mg/Kg - dry 150 1 10/13/21 04:39 TJS 6010D
Nitrate+Nitrite-N <29.6 mg/Kg - dry 29.6 1 10/13/21 13:52 ZBD 4500NO3F-2011
pH 6.5 s.u. 1 10/12/21 15:14 DRS 9045D
Calcium Carbonate Equivalent 4.4 % 0.1 1 10/11/21 09:45 DXT AOAC 955.01
Total Volatile Solids 43.0 % 0.010 1 10/12/21 16:12 FMM SM-2540G
Molybdenum <1.50 mg/Kg - dry 1.50 1 10/13/21 04:39 TJS 6010D
Qualifiers/
Definitions
B Analyte detected in blank DF Dilution Factor
H Beyond holding time MQL Method Quantitation Limit
Page 4 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 21-279-9013
Lab No : 55005
Sample ID : 4
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2021 1&2
Information :
REPORT OF ANALYSIS
Original Report Date : 10/14/2021
Revised Report Date: 10/15/2021
Received : 10/06/2021
Matrix: Solids
Sampled: 10/5/2021 0:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Total Kjeldahl Nitrogen 14200 mg/Kg - dry 1510 1 10/13/21 09:00 JPJ ;M-4500-NH3C-TKI`
Aluminum 169000 mg/Kg - dry 301 10 10/13/21 20:25 JTR 6010D
Manganese 988 mg/Kg - dry 3.01 1 10/13/21 04:44 TJS 6010D
Copper 37.0 mg/Kg - dry 3.01 1 10/13/21 20:20 JTR 6010D
Cadmium <0.602 mg/Kg - dry 0.602 1 10/13/21 04:44 TJS 6010D
Lead 8.73 mg/Kg - dry 1.81 1 10/13/21 04:44 TJS 6010D
Calcium Carbonate Equivalent 3.9 % 0.1 1 10/11/21 09:45 DXT AOAC 955.01
Total Volatile Solids 43.8 % 0.010 1 10/12/21 16:12 FMM SM-2540G
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sodium Absorption Ratio <6.02 mg/Kg - dry 6.02 1 10/13/21 04:44 CALCULATION
Ammonia Nitrogen <602 mg/Kg - dry 602 1 10/13/21 13:00 JPJ SM-4500-NH3C
Nitrate+Nitrite-N 60.2 mg/Kg - dry 30.0 1 10/13/21 13:53 ZBD 4500NO3F-2011
pH 6.5 S.U. 1 10/12/21 15:14 DRS 9045D
Molybdenum <1.51 mg/Kg - dry 1.51 1 10/13/21 04:44 TJS 6010D
Potassium 199 mg/Kg - dry 60.2 1 10/13/21 04:44 TJS 6010D
Sodium 241 mg/Kg - dry 151 1 10/13/21 04:44 TJS 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 5 of 8

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 21-279-9013
Lab No : 55005
Sample ID : 4
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kilby WTP 2021 1&2
Information :
REPORT OF ANALYSIS
Original Report Date : 10/14/2021
Revised Report Date: 10/15/2021
Received : 10/06/2021
Matrix: Solids
Sampled: 10/ 5/ 2021 0:00
Total Solids 16.6 % 0.010 1 10/12/21 16:12 FMM SM-2540G
Moisture 83.4 % 0.010 1 10/12/21 16:12 FMM SM-2540G
Phosphorus 1080 mg/Kg - dry 30.1 1 10/13/21 04:44 TJS 6010D
Sulfur 13400 mg/Kg - dry 60.2 1 10/13/21 20:20 JTR 6010D
Calcium 1010 mg/Kg - dry 301 1 10/13/21 20:20 JTR 6010D
Magnesium 466 mg/Kg - dry 30.1 1 10/13/21 04:44 TJS 6010D
Iron 20800 mg/Kg - dry 60.2 1 10/13/21 04:44 TJS 6010D
Zinc 71.1 mg/Kg - dry 7.53 1 10/13/21 04:44 TJS 6010D
Organic N 14220 mg/Kg - dry 1506 1 10/13/21 09:00 DH CALCULATION
Chromium 134 mg/Kg - dry 1.51 1 10/13/21 04:44 TJS 6010D
Nickel 9.46 mg/Kg - dry 1.51 1 10/13/21 04:44 TJS 6010D
Arsenic 13.2 mg/Kg - dry 3.01 1 10/13/21 04:44 TJS 6010D
Mercury <0.0897 mg/Kg - dry 0.0897 1 10/12/21 14:13 JW2 SW-7471B
Selenium <3.01 mg/Kg - dry 3.01 1 10/13/21 04:44 TJS 6010D
Qualifiers/
Definitions
B Analyte detected in blank DF Dilution Factor
H Beyond holding time MQL Method Quantitation Limit
Page 6 of 8

Waypoint..
ANALYTICAL
Customer Number: 07274
Customer Name: Denali Water
Report Number: 21-279-0013
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytica I.com
Shipment Receipt Form
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
*Yes ONo
Number of coolers/boxes received
Custody seals intact on shipping container/cooler? U Yes
Custody seals intact on sample bottles? 0 Yes
O No
O No
* Not Present
* Not Present
Chain of Custody (COC) present?
Yes O No
COC agrees with sample label(s)?
Yes O No
COC properly completed
Yes O No
Samples in proper containers?
Yes O No
Sample containers intact?
Yes O No
Sufficient sample volume for indicated test(s)?
Yes O No
All samples received within holding time?
Yes O No
Cooler temperature in compliance?
Yes O No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes O No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
O Yes
O Yes
O No
O No
* N/A
* N/A
Trip Blanks received with VOAs 0 Yes
O No @N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
O No ON/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes
Comments:
• No
Signature:
Jill Mauler
Date & Time:
Page 7 of 8
10/06/2021 12:24:53

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Page 8 of 8

Waypoint
ANALYTICAL
11 /1 /2021
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville, AL, 35801
Ref: Analytical Testing
Report Number: 21-294-0006
Project Description: Lake Kirby WTP 2021 1 &2
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.tom
Dear Jeff Retzke:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/21/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
G1oa7/
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypoint,
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Sample Summary Table
Report Number: 21-294-0006
Client Project Description: Lake Kirby WTP 2021 1&2
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
55215 5 Solids 10/20/2021 10/21/2021
55215 5 Solids 10/20/2021 10/21/2021 4500NO3F-2011 WP MTN
55215 5 Solids 10/20/2021 10/21/2021 SW-7471B WP MTN
55215 5 Solids 10/20/2021 10/21/2021 SM-4500-NH3C WP MTN
55215 5 Solids 10/20/2021 10/21/2021 6010D WP MTN
55215 5 Solids 10/20/2021 10/21/2021 SM-2540G WP MTN
55215 5 Solids 10/20/2021 10/21/2021 AOAC 955.01 WP MTN
55215 5 Solids 10/20/2021 10/21/2021 9045D WP MTN
55215 5 Solids 10/20/2021 10/21/2021 SM-4500-NH3C-TKN WP MTN
55216 6 Solids 10/20/2021 10/21/2021
55216 6 Solids 10/20/2021 10/21/2021 SM-4500-NH3C-TKN WP MTN
55216 6 Solids 10/20/2021 10/21/2021 SM-4500-NH3C WP MTN
55216 6 Solids 10/20/2021 10/21/2021 SM-2540G WP MTN
55216 6 Solids 10/20/2021 10/21/2021 4500NO3F-2011 WP MTN
55216 6 Solids 10/20/2021 10/21/2021 AOAC 955.01 WP MTN
55216 6 Solids 10/20/2021 10/21/2021 9045D WP MTN
55216 6 Solids 10/20/2021 10/21/2021 SW-7471B WP MTN
55216 6 Solids 10/20/2021 10/21/2021 6010D WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 9

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kirby WTP 2021 1&2
Information :
Report Number :21-294-0006 REPORT OF ANALYSIS
Lab No : 55215
Sample ID : 5
Report Date : 11/01/2021
Received : 10/21/2021
ow,row
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 10 / 20 / 2021 0:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Total Solids 17.9 % 0.010 1 10/27/21 16:41 FMM SM-2540G
Calcium 1330 mg/Kg - dry 279 1 10/29/21 00:23 JADS 6010D
Iron 20000 mg/Kg - dry 55.9 1 10/28/21 00:08 TJS 6010D
Aluminum 177000 mg/Kg - dry 279 10 10/29/21 00:28 JADS 6010D
Zinc 115 mg/Kg - dry 6.98 1 10/28/21 00:08 TJS 6010D
Chromium 131 mg/Kg - dry 1.40 1 10/28/21 00:08 TJS 6010D
Arsenic 7.54 mg/Kg - dry 2.79 1 10/28/21 00:08 TJS 6010D
Mercury <0.0754 mg/Kg - dry 0.0754 1 10/28/21 15:26 JW2 SW-7471B
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sodium Absorption Ratio <5.59 mg/Kg - dry 5.59 1 10/28/21 00:08 CALCULATION
Ammonia Nitrogen 620 mg/Kg - dry 559 1 10/28/21 13:30 JPJ SM-4500-NH3C
Organic N 16810 mg/Kg - dry 1397 1 10/28/21 08:00 CALCULATION
Phosphorus 1160 mg/Kg - dry 27.9 1 10/28/21 00:08 TJS 6010D
Cadmium <0.559 mg/Kg - dry 0.559 1 10/28/21 00:08 TJS 6010D
Copper 79.9 mg/Kg - dry 2.79 1 10/28/21 00:08 TJS 6010D
Lead 10.0 mg/Kg - dry 1.68 1 10/29/21 00:23 JADS 6010D
Manganese 2680 mg/Kg - dry 2.79 1 10/28/21 00:08 TJS 6010D
Nickel 11.7 mg/Kg - dry 1.40 1 10/28/21 00:08 TJS 6010D
Selenium <2.79 mg/Kg - dry 2.79 1 10/28/21 00:08 TJS 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 3 of 9

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 21-294-0006
Lab No : 55215
Sample ID : 5
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kirby WTP 2021 1&2
Information :
REPORT OF ANALYSIS
Report Date : 11/01/2021
Received : 10/21/2021
ow,row
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 10 / 20 / 2021 0:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sulfur 16000 mg/Kg - dry 55.9 1 10/29/21 00:23 JADS 6010D
Analytical Method: SM-2540G
Test Results Units MQL DF Date / Time By Analytical
Analyzed Batch
Moisture 82.1
010
0.010 1 10/27/21 16:41 FMM L581577
Total Kjeldahl Nitrogen 17400 mg/Kg - dry 1400 1 10/28/21 08:00 JPJ ;M-4500-NH3C-TKI`
Potassium 189 mg/Kg - dry 55.9 1 10/28/21 00:08 TJS 6010D
Magnesium 529 mg/Kg - dry 27.9 1 10/28/21 00:08 TJS 6010D
Sodium 225 mg/Kg - dry 140 1 10/28/21 00:08 TJS 6010D
Nitrate+Nitrite-N 46.5 mg/Kg - dry 25.9 1 10/28/21 15:53 ZBD 4500NO3F-2011
pH 6.3 s.u. 1 10/26/21 11:40 ADM 9045D
Calcium Carbonate Equivalent 1.5 % 0.1 1 10/27/21 10:41 DXT AOAC 955.01
Total Volatile Solids 48.7 % 0.010 1 10/27/21 16:41 FMM SM-2540G
Molybdenum 2.44 mg/Kg - dry 1.40 1 10/28/21 00:08 TJS 6010D
Qualifiers/
Definitions
B Analyte detected in blank DF Dilution Factor
H Beyond holding time MQL Method Quantitation Limit
Page 4 of 9

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
Report Number : 21-294-0006
Lab No : 55216
Sample ID : 6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kirby WTP 2021 1&2
Information :
REPORT OF ANALYSIS
Report Date : 11/01/2021
Received : 10/21/2021
ow,row
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 10 / 20 / 2021 0:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Total Kjeldahl Nitrogen 13600 mg/Kg - dry 1480 1 10/28/21 08:00 JPJ ;M-4500-NH3C-TKI`
Aluminum 195000 mg/Kg - dry 296 10 10/29/21 00:59 JADS 6010D
Manganese 2590 mg/Kg - dry 2.96 1 10/28/21 00:13 TJS 6010D
Copper 83.4 mg/Kg - dry 2.96 1 10/28/21 00:13 TJS 6010D
Cadmium <0.592 mg/Kg - dry 0.592 1 10/28/21 00:13 TJS 6010D
Lead 11.0 mg/Kg - dry 1.78 1 10/29/21 00:33 JADS 6010D
Calcium Carbonate Equivalent 1.8 % 0.1 1 10/27/21 10:41 DXT AOAC 955.01
Total Volatile Solids 49.3 % 0.010 1 10/27/21 16:41 FMM SM-2540G
Test
Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sodium Absorption Ratio <5.92 mg/Kg - dry 5.92 1 10/28/21 00:13 CALCULATION
Ammonia Nitrogen <592 mg/Kg - dry 592 1 10/28/21 13:30 JPJ SM-4500-NH3C
Nitrate+Nitrite-N 36.8 mg/Kg - dry 29.0 1 10/28/21 15:54 ZBD 4500NO3F-2011
pH 6.1 S.U. 1 10/26/21 11:40 ADM 9045D
Molybdenum 2.78 mg/Kg - dry 1.48 1 10/28/21 00:13 TJS 6010D
Potassium 199 mg/Kg - dry 59.2 1 10/28/21 00:13 TJS 6010D
Sodium 209 mg/Kg - dry 148 1 10/28/21 00:13 TJS 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L Limit Exceeded
Page 5 of 9

Waypoint,
ANALYTICAL
07274
Denali Water
Jeff Retzke
1001 Fraser Ave
Huntsville , AL 35801
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 o Fax [phone]
www.waypointa nalytical. com
Project Lake Kirby WTP 2021 1&2
Information :
Report Number :21-294-0006 REPORT OF ANALYSIS
Lab No : 55216
Sample ID : 6
Report Date : 11/01/2021
Received : 10/21/2021
ow,row
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 10 / 20 / 2021 0:00
Total Solids 16.9 % 0.010 1 10/27/21 16:41 FMM SM-2540G
Moisture 83.1 % 0.010 1 10/27/21 16:41 FMM SM-2540G
Phosphorus 1220 mg/Kg - dry 29.6 1 10/28/21 00:13 TJS 6010D
Sulfur 16400 mg/Kg - dry 59.2 1 10/29/21 00:33 JADS 6010D
Calcium 1380 mg/Kg - dry 296 1 10/29/21 00:33 JADS 6010D
Magnesium 554 mg/Kg - dry 29.6 1 10/28/21 00:13 TJS 6010D
Iron 21000 mg/Kg - dry 59.2 1 10/28/21 00:13 TJS 6010D
Zinc 120 mg/Kg - dry 7.40 1 10/28/21 00:13 TJS 6010D
Organic N 13550 mg/Kg - dry 1479 1 10/28/21 08:00 CALCULATION
Chromium 137 mg/Kg - dry 1.48 1 10/28/21 00:13 TJS 6010D
Nickel 12.4 mg/Kg - dry 1.48 1 10/28/21 00:13 TJS 6010D
Arsenic 7.93 mg/Kg - dry 2.96 1 10/28/21 00:13 TJS 6010D
Mercury <0.0822 mg/Kg - dry 0.0822 1 10/28/21 15:27 JW2 SW-7471B
Selenium <2.96 mg/Kg - dry 2.96 1 10/28/21 00:13 TJS 6010D
Qualifiers/
Definitions
B Analyte detected in blank DF Dilution Factor
H Beyond holding time MQL Method Quantitation Limit
Page 6 of 9

Waypol nt.M
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalyt-ical.com
Client: Denali Water
Project: Lake Kirby WTP 2021 1 &2
Lab Report Number: 21-294-0006
Date: 10/29/2021
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 55216 (6)
Analyte: Aluminum
QC Batch No: L581934/L581361
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L581544/L581361
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Manganese
QC Batch No: L581544/L581361
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Sulfur
QC Batch No: L581934/L581361
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 7 of 9

Waypoint..
ANALYTICAL
Customer Number: 07274
Customer Name: Denali Water
Report Number: 21-294-0006
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytica I.com
Shipment Receipt Form
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other :
0 UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
*Yes ONo
Number of coolers/boxes received
Custody seals intact on shipping container/cooler? U Yes
Custody seals intact on sample bottles? 0 Yes
O No
O No
* Not Present
* Not Present
Chain of Custody (COC) present?
Yes O No
COC agrees with sample label(s)?
Yes O No
COC properly completed
Yes O No
Samples in proper containers?
Yes O No
Sample containers intact?
Yes O No
Sufficient sample volume for indicated test(s)?
Yes O No
All samples received within holding time?
Yes O No
Cooler temperature in compliance?
Yes O No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes O No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
O Yes
O Yes
O No
O No
* N/A
* N/A
Trip Blanks received with VOAs 0 Yes
O No @N/A
Soil VOA method 5035 — compliance criteria met 0 Yes
O No ON/A
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes
Comments:
• No
Signature:
Brandi Watson
Date & Time:
Page 8 of 9
10/21/2021 11:16:24

SL.I: Total Solids (Moisture) Total Kjeldahl Nitrogen, Phosphorus and Potassium
SL2: Basic Test SLI plus Sulfur, Calcium, Magnetiium,Sodium, Iron, Aluminum, Manganese, Copper And 'Zinc
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead. Nickel, Selenium.
{Copper & Zinc included in SL2)
Nitrogtn Series: TotaI Kjeldahl, Anunonium, Nitrate & Organic Nitrogen.
CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)
Test Package Details
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Russellville, AR 72802
3308 Bernice Avenue
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Page 9 of 9

REPORT OF ANALYSIS
CLIENT:
ATTN:
ADDRESS: 1100 Exploration Way, Suite 302
CITY: Hampton, VA 23666
PHONE: [phone]
EMAIL/[e-mail]
Pancopia
Bill Cumbie
SPECIAL NOTES:
RE: PORTSMOUTH LAGOON
SAMPLE RECEIPT
DATE: 5/16/2019 TIME: 1 535
GRAB COLLECTION
DATE: 5/15/2019 TIME: 2143
COLLECTED BY: CLIENT
PICK UP BY: CLIENT
NUMBER OF CONTAINERS: 2
GOOD CONDITION El Good ❑ Other (See C-O-C)
REPORT NO: 19-08628 8:32
if2A
1 _
\`\sOC1ct��w
SAMPLE ID: Lagoon
SAMPLE NO 19-08628
Parameter
EPA Regulatory
HW Method JRA level
No. Number QL (mg/L) (mg/L) Result (mg/L) Analyst/Date/Time
Toxic Characteristic Leaching Procedure by SW-846 Method 1311
Arsenic D004 6010D 0.050 5 < 0.050 AME 5/24/2019 1505
Barium D005 6010D 0.500 100 < 0.500 AME 5/24/2019 1505
Benzene DO] 8 8260D 0.025 0.5 < 0.025 SDT 5/23/2019 0921
Cadmium D006 6010D 0.005 1 < 0.005 AME 5/24/2019 1505
Carbon Tetrachloride D019 8260D 0.025 0.5 < 0.025 SDT 5/23/2019 0921
Chlordane D020 8270E 0.025 0.03 < 0.025 CLH 5/30/2019 1941
Chlorobenzene D021 8260D 0.025 100 < 0.025 SDT 5/23/2019 092I
Chloroform D022 8260D 0.025 6 < 0.025 SDT 5/23/2019 0921
Chromium D007 6010D 0.010 5 < 0.010 AME 5/24/2019 1505
o-Cresol D023 8270E 0.025 200 < 0.025 CLH 5/30/2019 1941
mlp-Cresol D024 8270E 0.02 200 < 0.02 CLH 5/30/2019 1941
Cresol D026 8270E 0.02 200 < 0.02 CLH 5/30/2019 1941
2,4-D D016 8151A 0.004 10 <0.004 ADT 6/4/2019 2236
1,4-Dichlorobenzene D027 8260D 0.025 7.5 < 0.025 SDT 5/23/2019 0921
1,2-Dichloroethane D028 8260D 0.025 0.5 < 0.025 SDT 5/23/2019 0921
1,1-Dichloroethylene D029 8260D 0.025 0.7 <0.025 SDT 5/23/2019 0921
2,4-Dinitrotoluene D030 8270E 0.025 0.13 < 0.025 CLH 5/30/2019 1941
Endrin D012 8270E 0.005 0.02 < 0.005 CLH 5/30/2019 1941
James R. Reed & Associates
770 Pilot House Drive, Newport News, VA 23606
[phone] • Fax:[phone]
VELAP# 460013
EPA# VA00015
Page 1 of 3

REPORT OF ANALYSIS
SAMPLE ID: Lagoon
SAMPLE NO 19-08628
Parameter
Heptachlor (+epoxide)
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Lead
Lindane
Mercury
Methoxychlor
Methyl ethyl Ketone
Nitrobenzene
Pentachlorophenol
Pyridine
Selenium
Silver
Tetrachloroethylene
Toxaphene
Trichloroethylene
2,4, 5 -Trichlorophenol
2,4,6-Trichlorophenol
2,4,5-TP
Vinyl Chloride
EPA Regulatory
HW Method JRA level
No. Number QL (mg/L) (mg/L)
D031 8270E 0.005 0.008
D032 8270E 0.025 0.13
D033 8270E 0.025 0.5
D034 8270E 0.025 3
D008 6010D 0.050 5
D013 8270E 0.025 0.4
D009 7470A 0.0002 0.2
D014 8270E 0.025 10
D035 8260D 0.5 200
D036 8270E 0.025 2
D037 8270E 0.1 100
D038 8270E 0.025 5
D010 6010D 0.050 1
D011 6010D 0.010 5
D039 8260D 0.025 0.7
D015 8270E 0.1 0.5
D040 8260D 0.025 0.5
D041 8270E 0.025 400
D042 8270E 0.025 2
D017 8151A 0.004 1
D043 8260D 0.025 0.2
Result (mg/L)
< 0.005
< 0.025
< 0.025
< 0.025
< 0.050
< 0.025
< 0.0002
< 0.025
< 0.5
< 0.025
<0.1 M
< 0.025
< 0.050
< 0.010
< 0.025
< 0.1
< 0.025
< 0.025
< 0.025
< 0.004
< 0.025
Analyst/Date/Time
CLH 5/30/2019 1941
CLH 5/30/2019 1941
CLH 5/30/2019 1941
CLH 5/30/2019 1941
AME 5/24/2019 1505
CLH 5/30/2019 1941
SDT 5/22/2019 1346
CLH 5/30/2019 1941
SDT 5/23/2019 0921
CLH 5/30/2019 1941
CLH 5/30/2019 1941
CLH 5/30/2019 1941
AME 5/24/2019 1505
AME 5/24/2019 1505
SDT 5/23/2019 0921
CLH 5/30/2019 1941
SDT 5/23/2019 0921
CLH 5/30/2019 1941
CLH 5/30/2019 1941
ADT 6/4/2019 2236
SDT 5/23/2019 0921
James R. Reed & Associates
770 Pilot House Drive, Newport News, VA 23606
[phone] • Fax: [phone]
VELAP# 460013
EPA# VA00015
Page 2 of 3

REPORT OF ANALYSIS
NOTE:
JRA Quantification Level is the concentration of the lowest calibration standard above zero with a reliable signal.
Reproduction of this report is not permitted, except in full, without written approval from James R Reed & Associates.
The results on this report relate only to the sample(s) provided for analysis.
Results conform to NELAC standards, where applicable, unless otherwise indicated.
*SM 2011
M - Matrix spike % recovery outside QC acceptance range
Method 8270E-TCLP: Surrogate (2,4,6-tribromophenol) recovery
outside QC acceptance range
RESPECTFULLY SUBMITTED
C',--
Elaine Claiborne
Laboratory Director
06-Jun-19
James R. Reed & Associates
770 Pilot House Drive, Newport News, VA 23606
[phone] • Fax: [phone]
VELAP# 460013
EPA# VA00015
Page 3 of 3

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