HomeMy WebLinkAboutWQ0028653_Residual Annual Report 2021_20220129Non -Discharge Branch Upload/Submittal Form
NORTH CAROLINA
En.anmemfal Qualify
Version 2 - Revised June 23, 2020
Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?*
Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0028653
Applicant/Permittee Pilgrim's Pride Corporation
Email Notifications
Does this need review by the hydrogeologist?* Yes No
Regional Office
CO Reviewer
Admin Reviewer
Raleigh
Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name*
Robert T. Branch
Email Address*
bbranch@branchrs.com
Project Information
Application/Document Type *
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363129007
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Permit Number: *
Applicant/Permittee Address*
Facility Name*
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
WQ0028653
Has Current Existing permit number
484 Zimmerman Road Sanford, NC 27331
Pilgrim's Pride - Sanford Class A Residuals Program
High -Rate Infiltration
Reclaimed Water
Residuals
Other
Please provide comments/notes on your current submittal below.
Attached is the annual distribution report for the alum residuals. All materials were generated
and applied on the Pilgrim's property.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at nathaniel.thornburg@ncdenr.gov.
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
PP_Sanford_2021_AR_final.pdf 1.27MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
cOefezc1�7" 9raor.4s
Submission Date 1/29/2022
2021 ANNUAL REPORT
PILGRIM'S PRIDE CORPORATION
WATER TREATMENT PLANT
SANFORD, NORTH CAROLINA
PERMIT #WQ0028653
Prepared For:
Pilgrim's Pride Corporation
484 Zimmerman Road
Sanford, N.C. 27331-3668
Prepared By:
Branch Residuals & Soils, LLC
1735 Heckle Blvd. Suite 103-291
Rock Hill SC, 29732
January 2022
BRANCH RESIDUALS & SOILS, LLC
1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732
PHONE (336) 312-9007
January 29, 2022
North Carolina Department of Environmental Quality
Division of Water Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2021 LAND APPLICATION ANNUAL REPORT
Pilgrim's Pride Corporation.
Sanford, North Carolina
Permit No. WQ0028653
BR&S Project No. 2007-66
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in
the referenced permit on behalf of Pilgrim's Pride Corporation for their facility in Sanford, North
Carolina. This report includes: 1) Distribution and Marketing Certification and Summary Forms,
2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms,
4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP
Lab Sheets, 7) Pathogen & Vector Attraction Form, 8) Pathogen and Vector Attraction
Reduction Documentation, 9) Soils Lab Data 10) 2021 Application Summary Table, and 11)
2021 Application Condition Summaries.
A total of 995,300 gallons (53.30 dry tons) of alum residuals were distributed to sites on the
Pilgrim's Pride Facility at Sanford, NC in November of 2021.
If any further information is required regarding this land application program, please do not
hesitate to contact me at (336) 312-9007.
Robert T. Branch, L.S.S.
Land Application/Residuals Operator
#15676
RTB
Enclosures
TABLE OF CONTENTS
SECTION NO. TITLE
I Distribution and Marketing Certification and Summary
Forms
II Annual Residual Sampling Summary Form
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary Forms
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Form
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Report
X 2021 Application Summary Table
XI 2021 Application Condition Summaries
DISTRIBUTION AND MARKETING CERTIFICATION AND SUMMARY FORM
FACILITY NAME:
a
Co
A
0
U
c m Z
1
O ▪ a0poi
C a
At 0.
cis co
• Oa.
g LEI
0$�
u a
1.
▪ G `
as
a.
0
u
d
t
h
02
d rr
0. e
T.
gaI
- -a
-'
a
o
Ls▪ .
w
w
. 0
N
O
i.
Ca
t
es
0.
0
0
Z
E
O
C
V
a.
Intended use(s)
Soil Amendment
Volume (dry tons)
M
CO
r►
enV! 1
If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)I
Name(s)
Pilgrim's Pride Corporation
Bulking Agent(s) used:
e
r
Volume (dry tons)
Product Out
i1
rn
.41
0
M
in
c
lei
zo0
Amendment/
Bulking Agent
o
e
o
Amendment(s) used:1
Sources(s) (include NPDES # if
applicable)
PWS 03-53-130
Total from FORM DMSDF (sup)
I:(suot kip) iunnuv 1 :sleto
Month
g
ebruary
a
0.
02
e
:ptember
ctober
ovember
a..
.0
z • • a
� la 000
xa • Z
W C
N O
Z .>
0 Ci
Le u
Z
"
en � -
+• `..3
- O
S. .0
O • •-, 0
a
CO u
R
CS..o
• O C
CO ▪ 0
Cr 14
f. 4.1 . N A =
O 0 co 4..
q 3 as„
O 0>1 120
'O O +•c Lki
Z.
WQ oet
Z .0 y la
L."O >. c t
o O
110�0
e 3 8.
u c
0 3
`�' a 3 c
✓ e)•
a .-c u =
y a
61 Aa E12'rd
00 4 �3
0 "0 C C =
'a w s :; c
��-
`G-° E E o
.0 0 o
94...c
0 •C 0 0
3 a .o 8. c
U Lam'' a E O 0
O
t. ▪ •d O Q Q z
CtS
CIS
N
r-
es
DENR FORM DMSDF (12/2006)
•Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Waypoint Analyltical
� N
M
V1
00
g
PWS 03-53-130
WWTP Name: Pilgrim's Pride Corporation Sanford NC WTP
os
m
a
3.1
Sample or Composite Date _ i
Q
N
Vy
v
�•
x^
8
Q
Z
a
6v
[-
v
n
v
Y1
v
Oi
I
M
.-
O�
N
C
W
Conc.
Limit
(mpg)"
NA
r
ooe
o
840
57
S
7,500
NA
zz
NA 1
t-.
��
p y
IPercent Solids (%) _
Arsenic
E
_ _
U
Copper
Chromium
IMercury
E
4)
44
E
_
v)
�
ITotal Phosphorus
Ammonia -Nitrogen
Nitrate and Nitrite
4.0
0
.ro o°
l�n
g
ei y
41'
O
A ▪ .r
• S
L 00
O
EO •O
R q
L.
PO O
.'o-
•IS a
0 44
C a
sg
co
+r .r
w 0
C a
� y 1
1.0
O
A
40
on
' 0 O
0 Al
d a
0.0 as
as
a
a
0.
a
a
9
�w
aCID
"TS
O .0
C" C
ala
03
00
41
a is
2 Ts
C 0
S 0.
cis
DENR FORM DMSDF (12/2006)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
ANNUAL METALS FIELD LOADING SUMMARY FORMS
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Pilgrim's Pride Corporation
Permit #: WQ0028653 Cation Exchange Capacity (non 503 only):
Operator: Pilgrim's Pride Corporation Owner: Pilgrim's Pride Corporation Predominant Soil Series StA
Acres Used: 7.14 Acres Permitted: 7.14 Site #: 1 Field #: 1
Total Dry Tons Applied (Annual): 13.85
n/a
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
21-235-0006
Sample
or Com-
posite
Date
8/19/21
% Solids
1.28
Arsenic
35.70
Cadmium
7.14
Chromium
0.00
Copper
145.00
Lead
21.40
Mercury
0.96
Molyb-
denum
17.90
Nickel
17.90
Selenium
35.70
Zinc
89.30
Total
Phos-
phorus
1,300
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total DT/Ac./
Yr./Application
Event
1.94
r
Totals:
Arsenic
0.14
0.14
Cadmium
0.03
0.03
Chromiurr
0.00
0.00
Copper
0.56
0.56
Lead
0.08
0.08
Mercury
0.00
0.00
Molyb-
denum
0.07
0.07
Nickel
0.07
0.07
Selenium
0.14
0.14
Zinc
0.35
0.35
Total
Phos-
phorus
5.05
5.05
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
informatin submitted m aware that there are significant penalties for submitting false information,
Signature of Land Applier
nes and imprisonment for knowing violations"
/ 27h2
Date
Author Daryl D. Merritt
DENR FORM MFLSF (7/2002)
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Pilgrim's Pride Corporation
Total Dry Tons Applied (Annual): 1.35
WQ0028653 Cation Exchange Capacity (non 503 only):
n/a
Pilgrim's Pride Corporation Owner: Pilgrim's Pride Corporation Predominant Soil Series ToB
0.74 Acres Permitted: 0.74 Site #: 1 Field #:
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
21-235-0006
Sample
or Com-
posite
Date
8/ 19/21
% Solids
1.28
Arsenic
35.70
Cadmium
7.14
Chromium
0.00
Copper
145.00
Lead
21.40
Mercury
0.96
Molyb-
denum
17.90
Nickel
17.90
Selenium
35.70
Zinc
89.30
Total
Phos-
phorus
1,300
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total DT/Ac./
Yr./Application
Event
1.82
1
Totals:
Arsenic
0.13
0.13
Cadmium
0.03
0.03
Chromium
0.00
0.00
Copper
0.53
0.53
Lead
0.08
0.08
Mercury
0.00
0.00
Molyb-
denum
0.07
0.07
Nickel
0.07
0.07
Selenium
0.13
0.13
Zinc
0.33
0.33
Total
Phos-
phorus
4.74
4.'74
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
informati submitted. I aware that there are significant penalties for submitting false information,
incl >t the possibiines and imprisonment for knowing violations"
22
Date
Author Daryl D Merritt DENR FORM MFLSF (7/20021
Signature of Land Applier
ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Pilgrim's Pride Corporation
Total Dry Tons Applied (Annual): 38.10
WQ0028653 Cation Exchange Capacity (non 503 only):
nla
Operator: Pilgrim's Pride Corporation Owner: Pilgrim's Pride Corporation Predominant Soil Series StA
Acres Used:
16.01 Acres Permitted: 16.01 Site #: 1 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
21-235-0006
Sample
or Com-
posite
Date
8/19/21
% Solids
1.28
Arsenic
35.70
Cadmium
7.14
Chromium
0.00
Copper
145.00
Lead
21.40
Mercury
0.96
Molyb-
denum
17.90
Nickel
17.90
Selenium
35.70
Zinc
89.30
Total
Phos-
phorus
1,300
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total DT/Ac./
Yr./Application
Event
2.38
Totals:
Arsenic
0.17
0.17
Cadmium
0.03
0.03
Chromium
0.00
0.00
Copper
0.69
0.69
Lead
0.10
0.10
Mercury
0.00
0.00
Molyb-
denum
0.09
0.09
Nickel
0.09
0.09
Selenium
0.17
0.17
Zinc
0.43
0.43
Total
Phos-
phorus
6.19
6.19
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
inclhe : bility of fines and imprisonment for knowing violations"
//2/Z 2
Date
Signature of Land Applier
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL LAND APPLICATION FIELD SUMMARY FORMS
ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac) Nutrients (lbs/ac)
As — Arsenic
Cd — Cadmium
Cr — Chromium
Cu — Copper
Pb — Lead
Hg — Mercury
Mo — Molybdenum
Ni — Nickel
Se — Selenium
Zn — Zinc
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Acres Utilized:
WQ Permit #:
Acres Permitted:
eke
V1
00
Annual Dry Tons Applied:
Pilgrim's Pride Corporation
Cation Exchange Capacity (non 503):
Predominat Soil Series
Pilgrim's Pride Corporation
z
z
a
z
a
0
U
z
el
a
0
U
Zei
E
z
a
0
U
Must Select
Crop l or Crop 2
Crop 2
Lime Applied 1
U
el
2.600 I
C
CL
v
x
ag
n
o
a
PAN Applied
(lbs/acre)
N
0.
0
U
N
zo
Q
a
CD
o
a.
U
O
Z
NO
o
O
cz c Y
z ....
NO
`°
a
o
"1
Ammonia
Nitrogen a
c�
Zn
0.35
o
o;
8.70
2.498
x en
E-E
24,900
c
0.14
o
0.41
00
Mineral-azation
Rate***
o
'z
o
rno
rti
O
N
t.
M
Volitila-zation
Rate**
o
o
0
26zzz
o
0
0
0
Appli-cation
Method*
=
o
o
0
0
0
0
WI
ri.
e a'
a'a'O
'—.
00
O
-
en
N
N
N
ela
Residual Sources
(NPDES #, WQ#.
Fert., Animal Waste.
etc.)
Pilgrim's Pride WTP
U
0.00
NA
NA
NA
Cd
0.03
0.26
en
O
M
N G U
O N ' Q
.Q Q Q
Q
O�
—
As
-
d
p
-
0.90
'0
M
f71
E
% Q .�
Q
°O
l
e-
Annual lbs/acre
Current Cumulative lbs/acre
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
coU
Q
O i
H. 0-
N
en
N
•
M
N
rn
M
a'
.V
en
.-ci
cq
>-
USE--.F.
t=-
Oa e csi
8
00
N
TOTALS:
GI
CI
Date or
Month
I Nov-21
Signature of Land Applier
eFORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
r•
0
Acres Utilized:
WQ Permit #:
Acres Permitted:
N
Annual Dry Tons Applied:
Pilgrim's Pride Corporation
Cation Exchange Capacity (non 503):
Predominat Soil Series
Pilgrim's Pride Corporation
z
z
a.
ea
N
L
U
z
E
ea
z
o.
L
U
00
0
0
E
ea
z_
Q.
L
U
Must Select
Crop 1 or Crop 2
N
o
O
U
Lime Applied I
U
U
X
N
Q0.
PAN Applied
(lbs/acre)
N
O.0
U
N
zo
a
oM
U
z_M
a.
1) Yta
. -O
ti. = 0 Leo
z z E
s.0
Q.
4
Ammonia i
Nitrogen E
a
Zn
en M
0
9.03
8.70
rn
ri
4 cc
t
F- E
24,900
a)
_
0
vim,
0
0.41
00
0O
Mineral-azation
Rate***
0
z
ca
o
ri
rn
e••i
r-
M
Volitila-zation
Rate**
o�
6
o
o
0444
Q
Q
Q
Appli-cation
Method*
v,
°z
=
o
o
0
c
0
o
d�
U N L s
0. 0..,
M.
00
O •
O
M•
(NI
enO
N•
el
�p
N
-ci
C a) ,vf
iii�Q3�
U0
M
v1
r•
Cr,ff..
00
7
00
co
el
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste.
etc.)
Pilgrim's Pride WTP
0.00
NA
z
NA
Cd
0.03
cn
N
O
en
(-1
O
M
yLy
a.)R U
7 a'a) i" Q
• a Q Q
Q
00
.--�
As
-
0
p
^
0.90
�O
M
cnN E
aF.3
oCD
1.28
Annual lbs/acre
Current Cumulative lbs/acre
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop
Q
a•
4,
O
M
7
O
M
a
aJ 0
N
N
TOTALS:
El
El
Date or
Month
I Nov-21
ae
ad — L C
ra
"d as
of
L L
oo
te
.° E
C • . al
0
...0 CA
S. vo S, C.
te
O. 0 E
L ea L7
C ,.' y
o w C
u•
L 1O
,„
b'4'.
E
I. 0 y
41.1 CI) o aU
,ri1:1..a
ad 0
CI on
a TS 0
011
CLe ;o
L y 7
a. -a CJ
ow R .0
ea
b0 0
?L y,' O
C
0 aoe ea
E Q
O _Q'w
17) 4e •O
L. Ca)
co
ea a) at
izi
o >
Q L
4.
R Ca 40.
C �, d
O. I.
}• 0 ea
C ea C.
. O y
w>1 'O
• 0)
L. C
u'7, C
.,.o.FA
04
• -x
0)
0
Signature of Land Applier
'FORM FSF (12/2006)
0
a
A
W
r►�w
z
0
E.4
a44
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Acres Utilized:
WQ Permit #:
Facility Name: Pilgrim's Pride Corporation
Acres Permitted:
00
Annual Dry Tons Applied:
Pilgrim's Pride Corporation
Cation Exchange Capacity (non 503):
Predominat Soil Series
Pilgrim's Pride Corporation
0
z
z
a.
z
O
0
ro
z
R
a
0
Must Select
Crop 1 or Crop 2
N
C1
O
U
Lime Applied
V
0
0)
XI
oo
U
x
tt
PAN Applied
(Ibs/acre)
N
a.
U
N
zo
a
g�
r-
M
z�
Q
M
a) :3
c'Y X
$
a,
-
Ammonia
Nitrogen E
r '
c
'�
0
3.39
o
N
ch
r,;
.�.
E. E
24,900
a)
.--�
0
V1
0 •0
M
O-
°°
Mineral-azation
Rate***
o�
0
z
o
o
ON
0
o
M
Volitila-zation
Rate**
o
0
o
4
c
o
Q
z
<
z
<
z
Appli-cation
Method*
c�
tit
Z
o
o
0
0
0
0
,„
_
C. "*rN
U - L
co Kir. -
a.
.0
0.'
O^
O
V1
O
,.
O
(-1a.
y •'�
inUQ2
O
Uo
oN
v,
00
con
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste.
etc.)
Pilgrim's Pride V*, IP
U
0.00
z
z
NA
Cd
0.03
0.14
CO
O
M
UC ¢ .
G 'O 2 Q
7 C Q Q
Q
2.38
to•v.,
O
O
00
O
M
b E
e) < .3
a
1.28
Annual lbs/acre
Current Cumulative lbs/acre
Prior Years Cumulative lbs/acre
Permitted C. P. L. R.****
Permit PAN Limit I st/2nd Crop
U
Q
a.
7
7
et
.
d>-
(7
'C
1"' z c 1
°a;d0O
a) o
O
d;
TOTALS:
CI
Date or
Month
N
°
0) u.
� � R
++tg
• R
a 3 O
ea 'C R
• rr
C
a 44 a
• an a
a • a E
• o'
L R 0
o E R
C L �
O w C
++ CJ iw
' W
o
bimo• Tji
• O
p a
• CD a)
u ▪ • C
L R b.(
R .0 CC
CI.
L L o
a u
• b°d
?' O
b
• g
E
O L
• _a o
▪ L w
R 6) r
. tea a d
o XI
-4" Q' L
r.+
CSw
C7
a L
L R
O V C
C CO C
• C
cp u '7 b
Signature of Land Applier
FORM FSF (12/2006)
RESIDUAL ANALYSIS LAB SHEETS
Waypoi nt.
ANALYTICAL
8/27/2021
Branch Residuals and Soils LLC
Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill, SC, 29732
Ref: Analytical Testing
Report Number: 21-235-0006
Project Description: Pilgrim's Sanford
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Dear Bob Branch:
Waypoint Analytical Virginia, Inc. received sample(s) on 8/23/2021 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
4ic
Pic irioay/
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7
Waypoint,.
ANALYTICAL
Report Number: 21-235-0006
Client Project Description: Pilgrim's Sanford
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Sample Summary Table
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
77541 Pilgrim's Sanford Solids 08/19/2021 11:30 08/23/2021 SM-4500-NH3C WP MTN
77541 Pilgrim's Sanford Solids 08/19/2021 11:30 08/23/2021 SM-4500-NH3C-TKN WP MTN
77541 Pilgrim's Sanford Solids 08/19/2021 11:30 08/23/2021 4500NO3F-2011 WP MTN
77541 Pilgrim's Sanford Solids 08/19/2021 11:30 08/23/2021 6010D WP MTN
77541 Pilgrim's Sanford Solids 08/19/2021 11:30 08/23/2021 SW-7471B WP MTN
77541 Pilgrim's Sanford Solids 08/19/2021 11:30 08/23/2021 9045D WP MTN
77541 Pilgrim's Sanford Solids 08/19/2021 11:30 08/23/2021 SM-2540G WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7
Waypoint
ANALYTICAL
46368
Branch Residuals and Soils LLC
Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill , SC 29732
Report Number : 21-235-0006
Lab No : 77541
Sample ID : Pilgrim's Sanford
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project Pilgrim's Sanford
Information :
REPORT OF ANALYSIS
Report Date: 08/27/2021
Received : 08/23/2021
twill pit &fol.'
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/ 19/ 2021 11:30
Test
Results
Units
MOL
DF Date / Time By Analytical
Analyzed Method
Total Solids
Total Kjeldahl Nitrogen
Phosphorus
Potassium
Calcium
Magnesium
Sodium
Copper
Zinc
Nitrate+Nitrite-N
Nickel
Mercury
Selenium
pH
Test
1.43 % 0.010
24900 mg/Kg - dry 17900
1300 mg/Kg - dry 357
843 mg/Kg - dry 714
<3570 mg/Kg - dry 3570
900 mg/Kg - dry 357
2640 mg/Kg - dry 1790
145 mg/Kg - dry 35.7
<89.3 mg/Kg - dry 89.3
669 mg/Kg - dry 346
<17.9 mg/Kg - dry 17.9
<0.964 mg/Kg - dry 0.964
<35.7 mg/Kg - dry 35.7
6.3 s.u.
Results
Units
MOL
1 08/24/21 16:16 FMM SM-2540G
1 08/26/21 08:00 JPJ ;M-4500-NH3C-TKI
1 08/25/21 23:05 JTR 6010D
1 08/27/21 03:42 JTR 6010D
1 08/25/21 23:05 JTR 6010D
1 08/25/21 23:05 JTR 6010D
1 08/25/21 23:05 JTR 6010D
1 08/25/21 23:05 JTR 6010D
1 08/25/21 23:05 JTR 6010D
1 08/25/21 15:44 ZBD 4500NO3F-2011
1 08/25/21 23:05 JTR 6010D
1 08/26/21 13:35 TJS SW-7471B
1 08/25/21 23:05 JTR 6010D
1 08/26/21 15:30 DRS 9045D
DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
Aluminum
Arsenic
Cadmium
<7140 mg/Kg - dry
95700 mg/Kg - dry
<35.7 mg/Kg - dry
<7.14 mg/Kg - dry
7140 1 08/27/21 07:00 JP) SM-4500-NH3C
357 1 08/25/21 23:05 JTR 6010D
35.7 1 08/25/21 23:05 JTR 6010D
7.14 1 08/25/21 23:05 JTR 6010D
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
L
Umit Exceeded
Page 3 of 7
Waypoint.
ANALYTICAL
46368
Branch Residuals and Soils LLC
Bob Branch
1735 Heckle Blvd
Suite 103-291
Rock Hill , SC 29732
Report Number : 21-235-0006
Lab No : 77541
Sample ID : Pilgrim's Sanford
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Project Pilgrim's Sanford
Information :
REPORT OF ANALYSIS
Report Date: 08/27/2021
Received : 08/23/2021
4)11.4Vic m e
Groacy/
Pauric Mc Groary Ph.D., CPA
Agronomist
Matrix: Solids
Sampled: 8/ 19/ 2021 11:30
Test
Results
Units
MQL
DF Date / Time By Analytical
Analyzed Method
Lead
Molybdenum
Analytical Method: SM-2540G
Test
<21.4 mg/Kg - dry
<17.9 mg/Kg - dry
Results
Units
21.4 1 08/25/21 23:05 JTR 6010D
17.9 1 08/25/21 23:05 JTR 6010D
MQL
DF Date / Time By Analytical
Analyzed Batch
Moisture
98.6 % 0.010 1 08/24/21 16:16 FMM L570729
Qualifiers/
Definitions
DF Dilution Factor
MQL Method Quantitation Limit
Page 4 of 7
Waypoi ntti
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Client: Branch Residuals and Soils LLC
Project: Pilgrim's Sanford
Lab Report Number: 21-235-0006
Date: 8/27/2021
CASE NARRATIVE
Total, Fixed, and Volatile Solids Method 2540G-2011
QC Batch No: L570729
Relative percent difference (RPD) for the duplicate analysis was outside of the allowable quality control limits.
The sample and duplicate results are less than ten times the reporting limit. At this level, RPD is not applicable.
The data is considered to be acceptable.
Metals Analysis Method 6010D
Sample 77542
Analyte: Aluminum
QC Batch No: L571122/L570834
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L571122/L570834
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Copper
QC Batch No: L571122/L570834
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L571338/L570834
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Phosphorus
QC Batch No: L571122/L570834
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Zinc
QC Batch No: L571122/L570834
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7
Waypoint..
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46368
Customer Name: Branch Residuals and Soils LLC
Report Number: 21-235-0006
O Fed Ex
O UPS
Q US Postal
Q Client
Shipping Method
Q Lab
Q Courier
Q Other :
Thermometer ID: I
Shipping container/cooler uncompromised?
D Yes QNo
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? Q Yes 0 No 0 Not Present
Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present
Chain of Custody (COC) present? 0 Yes 0 No
COC agrees with sample label(s)?
D Yes 0No
COC properly completed
D Yes QNo
Samples in proper containers?
*Yes QNo
Sample containers intact?
D Yes QNo
Sufficient sample volume for indicated test(s)?
*Yes QNo
All samples received within holding time? 0 Yes
O No
Cooler temperature in compliance?
D Yes QNo
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes 0 No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
Q Yes
Q Yes
O No
Q No
0 N/A
0 N/A
Trip Blanks received with VOAs 0 Yes
O No ON/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A
High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) (— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: jBrandi Watson Date & Time: ;08/23/2021 14:00:55
Page 6 of 7
L 30 L e6 a
a
O
Z.
X
v.
o
N
EOZSZVN 39 •> 1003 I
Z>Hd voetH H
Z>Hd nH 9
Z>HdEONH
8T<Hd HOeN 3
poynbay .UON o
Z>HdPOSZH 3
39 => 1003
(Muo 0A31w) EOZSZeN Sot > ioo3 v
�1
t
2
."!
c
f
Client Remarks/Comments
Date Time
E
F
v
v O
g
F
Y
IIO
O
Received by: (SIGNATURE)
C
Q
z
2
d
cc
C
Received—b� (SIGNATURE)
ror Laoc
glilliguNgfl11111111111II1IIIII
iiar m's Sanford
utner
Purchase Order Number
Iuired Analysis / Preservative
w .R-►
OIL
m�
FM
N_`
`
F
4
1
z
O
Z
v i
[RGNATURE )
cc2
>
g
Z
3
ureic rrodecr manager/r.onsacc oiling miurmatn n
'?Qb Vrovv„t-
11
Project/Site location (City/State) RUSH — Additional charges app E
Special Detection Limit(s) P
ife4r s 1.4w Date Results Needed
Project Manager Em it
g d 970
PI A PP q1
('
v
ayisodwo(D) Jo geJ(g)
Project Manager Phone 11
vox 01 cam) xpleW
a
V7-
uauie3uo3 jo cagwnNcc
Unless noted, all containers
per Table II of 40 CFR Part
136.
Sample Identification
PP-5
n
For Laboratory Use Only
E
s
a
3
i`Z
Cr)
II.
C4,V
Project Description
AfkIt �f
Project Number
Waypoint
ANALYTICAL
2790 Whitton Road
Memphis, TN 311133
(901) 213-2400
}?OA 1 M z
Blank/Cooler Temp
E
^'
•
z
TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORT
TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORT
TCLP analyses are required once every five years by permit.
PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORM
PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The current permit, WQ0028653, does not have vector attraction requirements but does have Class
A requirements for pathogens. The form is marked to reflect these requirements.
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Pilgrim's Pride Corporation
WWTP Name: Pilgrim's Pride Corporation Sanford NC WTP
Monitoring Period: From 1/1/2021
WQ Permit Number: WQ0028653
NPDES Number: PWS 03-53-130
To 1 2/31 /2021
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) 0
Alt B (Alk Treatment) • I
Alt. C (Prior Testing) El
AILD (No Prior Test) •
I
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate 'Process to Further Reduce Pathogens":
Compost •
Heat Drying
■
Heat Treatment
■
Thermophilic ❑
Beta Ray •
Gamma Ray ■
Pasteurization •
Class B:
Alt. (1) Fecal Density
Alt. (2) Process to Significantly
Reduce Pathogens 0
I
■
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 0
] Air Drying 0
I Composting 0 !Aerobic
Digestion •
Anaerobic Digestion •
I -
If applicable to alternative performed
(Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
y
Sample
Type
Analytical
Tech -
niaue
Minimum
Geo. Mean
Maximus-
Units
Fecal Coliform
2x 10tothe
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
I29
141.0692
160
Gram/
0
Annually
Grab
18
9221C E
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction)
•
Alt. 2 (40-day bench)
•
Alt. 3 (30-day bench) 0
Alt. 4 (Spec. 02 uptake)
•
Alt. 5 (14-Day Aerobic)
•
Alt. 6 (Alk. Stabilization
■
Alt 7 (Drying - Stable) •
Alt. 8 (Drying - Unstable)
•
Alt. 9 (Injection)
0
Alt. 10 (Incorporation)
0
No vector attraction reduction alternatives were performed
n
CERTIFICATION STATEMENT (please check the appropriate statement)
0
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. 1 am aware that there are
significant penalties for false certification including fine and imprisonment."
Ms. Tina Pedley, WTP Lagoons ORC
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer*
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 5fll 9fr1 and 15A NCAr 7T 1 1 n0 (7A1 11PAIR Gnwnn nsscnr oionnaN
PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The current permit, WQ0028653, does not have vector attraction requirements but does have Class
A requirements for pathogens. Documentation is attached to reflect these requirements.
Data Analyzed
Pilgrim's Pride WTP
Sanford, North Carolina
WQ0028653
August, 2021
8/19/2021
Lab #
Fecal Coliform
MPN per gram
Log
21-35673
133
2.124
21-35674
160
2.204
21-35675
139
2.143
21-35676
153
2.185
21-35677
129
2.111
21-35678
138
2.140
21-35679
138
2.140
Mean Colonies / Gram
Total
Average
15.046
2.149
141
Fecal Coliform/gram
Fecal Coliform values are less than 1,000 and meets the Class A pathogen
reduction requirement
envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infofa'environmentalchemists.com
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Date of Report: Aug 30, 2021
Customer PO #:
Customer ID: 15060009
Report #: 2021-14248
Project ID: Pilgrim's - Sanford
Lab ID
21-35673
Test
Sample ID:
Site: PPS - 1
Method
Collect Date/Time Matrix Sampled by
8/19/2021 10:43 AM Solid/Sludge Client
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
1.36%
<133 MPN/g
08/23/2021
08/19/2021
Lab ID
21-35674
Test
Sample ID:
Site: PPS - 2
Method
Collect Date/Time Matrix Sampled by
8/19/2021 10:48 AM Solid/Sludge Client
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 6
SM 9221C E-2014
1.13%
<160 MPN/g
08/23/2021
08/19/2021
Lab ID
21-35675
Test
Sample ID:
Site: PPS - 3
Method
Collect Date/Time Matrix Sampled by
8/19/2021 10:53 AM Solid/Sludge Client
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
1.30%
<139 MPN/g
08/23/2021
08/19/2021
Lab ID
21-35676
Test
Sample ID:
Site: PPS - 4
Method
Collect Date/Time Matrix Sampled by
8/19/2021 10:58 AM Solid/Sludge Client
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
1.18%
<153 MPN/g
08/23/2021
08/19/2021
Lab ID
21-35677
Test
Sample ID:
Site: PPS - 5
Method
Collect Date/Time Matrix Sampled by
8/19/2021 11:03 AM Solid/Sludge Client
Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
1.40%
<129 MPN/g
08/23/2021
08/19/2021
Report #:: 2021-14248
Page 1 or 2
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info@environmentalchemists.com
Branch Residuals/Bob Branch
1735 Heckle Blvd Suite 103-291
Rock Hill SC 29732
Attention: Bob Branch
Date of Report: Aug 30, 2021
Customer PO #:
Customer ID: 15060009
Report #: 2021-14248
Project ID: Pilgrim's - Sanford
Lab ID
21-35678
Test
Sample ID:
Site: PPS - 6
Method
Collect Date/Time Matrix Sampled by
8/19/2021 11:08 AM Solid/Sludge Client
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
1.31%
<138 MPN/g
08/23/2021
08/19/2021
Lab ID
21-35679
Test
Sample ID:
Site: PPS - 7
Method
Collect Date/Time Matrix Sampled by
8/19/2021 11:13 AM Solid/Sludge Client
Results
Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
1.31%
<138 MPN/g
08/23/2021
08/19/2021
Comment: Results reported on a dry weight basis.
Reviewed by:
Report #:: 2021-14248
Page 2 of 2
o`
Analytical & Consulting Chemists
REPORT NO:
0
z
0
to.
PHONE/FAX: 284.7969 284.5073
email: bbranch@branchrs.com
PROJECT NAME: Sludge-Pilgrim's Sanford
CONTACT NAME: Bob Branch
REPORT TO:
Client: Branch Residuals/Bob Branch
ADDRESS:
d
cn
R
0Iuu9e, viper:
ANALYSIS REQUESTED
All.
'';T)
sQ
Q
,,,,c%
\J
fecal density/ %TS
fecal density/ %TS
fecal density/ %TS
fecal density/ %TS
fecal density/ %TS
fecal density/ %TS
fecal density/ %TS
CO
t 9ate/Time 1 Rtcejved By: 1
kki
1
•
I
\
PRESERVATION
213H±O
OIHL
X
X
X
X
X
X
X
HOVN
CONIC
VOSZH
13H
3NON
- LI38Wf1N
al 8Vl
''
C`i
n
`�
T
C'
\ t N
-
1 -
t —
14
C .
ll6w
. aul�olgo
I
(o,o d)
JaulJO
fi
U'
C7
C�
e
C7
lg
C7
(DC9
/p
C�
t
C�
a.
0
J O
a)lsodwo3
U
U
It
U
OclyU
0000JJJ1
c
U
ll!
�!
U
e
U/
V,
�V
U
w 3
�k/
U
0
I ��` _4 IIinquished By:
'
adFl
eldweS
.J
. .r---"---.--„___
Collection
a
E
1--
a
o
d
a
-...
_.
CDN
1
Transfer
i
i
C4
0
I
I
N f
Sample Identification
•N
M
`'^-�
U
0—
co
I2
'a
d
N
ts
R
tn
Received B
0
z
0
z
H
Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Recei•t Checklist
ClienttRANItfl I UNA LS Date8
a
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Report Number: 021 —
Receipt of sample: ECHEM Pickup` I Client Delivery 0 UPS 0 FedEx 0 Other 0
❑ YES 0 NO 14 N/A 1. Were custody seals present on the cooler?
❑ YES 0 NO N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt .3 , 7 °C Corrected temperature upon receipt
How temperature taken: 0 Temperature Blank k Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
' YES
YES
YES
YES
YES
YES
YES
YES
O YES
O YES
O YES
O YES
O YES
O YES
❑ NO
O NO
O NO
❑ NO
❑ NO
O NO
O NO
❑ NO
❑ NO
❑ NO
❑ NO
❑ NO
❑ NO
❑ NO
❑ NO
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
4. Were proper custody procedures (relinquished/received) followed?
5. Were sample ID's listed on the COC?
6. Were samples ID's listed on sample containers?
7. Were collection date and time listed on the COC?
8. Were tests to be performed listed on the COC?
9. Did samples arrive in proper containers for each test?
10. Did samples arrive in good condition for each test?
11. Was adequate sample volume available?'
12. Were samples received within proper holding time for requested tests?
13. Were acid preserved samples received at a pH of <2? *
14. Were cyanide samples received at a pH >12?
15. Were sulfide samples received at a pH >9?
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
SOIL ANALYSIS REPORT
SOIL ANALYSIS REPORT
Soil Samples were sent to a lab for testing. Results are not available at the time of the report.
Lime will be added if needed. Soil samples will be provided as soon as they are available from
the lab.
2021 APPLICATION SUMMARY TABLE
PERMIT NO. WQ0028653
2021 APPLICATION SUMMARY
Dry Tons /
Date Spread Gallons Dry Tons Acre PAN Crop
44514 258700 13.8546051 1.940420811 44.0203865IFescue
44516 25200 1.3495788 1.82375514 41.373709 Fescue
44514 711400 38.098824 2.37968918 53.9856287 Fescue
Tract/
Farmer Site Field Acres
Pilgrim's Pride 1 1 7.14
So
o
o
N
M
O
M
M
O
O
"I.
01
QN
01
00
M
N
Branch Residuals & Soils, LLC Confidential
2021 APPLICATION CONDITION SUMMARIES
Pilgrim's Pride WTP
Sanford, North Carolina
Denali Water Solutions
WQ0028653
Annual 2021
Water Treatment Plant
Farmer: Pilgrim's Pride
Acres: 7.14
Site/Tract: 1
Application Method: Surface
Field: 1
Percent Solids : 1.28
Residual Report No.: 21-235-0006
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/14/21
1
25,870.0
Dry
warm, Partly Cloudy
0.00
11/15/21
1
51,740.0
Dry
warm, Partly Cloudy,
0.00
11/16/21
1
51,740.0
Dry
warm, Partly Cloudy
0.00
11/18/21
1
51,740.0
Moist
Cool, Partly Cloudy
0.00
11/19/21
1
51,740.0
Dry
warm, Partly Cloudy
0.00
11/21/21
1
25,870.0
Dry
warm, sunny
0.00
Total Gallons
258,700.0
Pilgrim's Pride WTP
Sanford, North Carolina
Denali Water Solutions
WQ0028653
Annual 2021
Water Treatment Plant
Farmer: Pilgrim's Pride
Acres: 0.74
Site/Tract: 1
Application Method: Surface
Field: 2
Percent Solids : 1.28
Residual Report No.: 21-235-0006
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/16/21
2
10,080.0
Dry
warm, Partly Cloudy
0.00
11/20/21
2
10,080.0
Dry
warm, sunny
0.00
11/22/21
2
5,040.0
Dry
warm, Cloudy
0.00
Total Gallons
25,200.0
Pilgrim's Pride WTP
Sanford, North Carolina
Denali Water Solutions
WQ0028653
Annual 2021
Water Treatment Plant
Farmer: Pilgrim's Pride
Acres: 16.01
Site/Tract: 1
Application Method: Surface
Field: 3
Percent Solids : 1.28
Residual Report No.: 21-235-0006
Crop: Fescue
Date
Field No.
Subfield
Gallons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11 / 14/21
3
71,140.0
Dry
Warm, Partly Cloudy
0.00
11/15/21
3
71,140.0
Dry
Warm, Partly Cloudy
0.00
11 / 16/21
3
71,140.0
Dry
warm, Partly Cloudy
0.00
11/18/21
3
71,140.0
Moist
Cool, Partly Cloudy
0.00
11/19/21
3
71,140.0
Dry
warm, Partly Cloudy
0.00
11/20/21
3
106,710.0
Dry
warm, sunny
0.00
11 /21 /21
3
106,710.0
Dry
warm, sunny
0.00
11/22/21
3
71,140.0
Dry
warm, Cloudy
0.00
11/23/21
3
71,140.0
Dry
Warm, Sunny
0.00
Total Gallons
711,400.0