WQ0013263_Residual Annual Report 2021_20220201

Non -Discharge Branch Upload/Submittal Form
NORTH CAROLINA
EnWrvnmemfal Qualify
Version 2 - Revised June 23, 2020
Initial Review
Reviewer
Thornburg, Nathaniel D
Is this submittal an application? (Excluding additional information.)*
Yes No
If not an application what is the submittal type?*
Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2021
Permit Number (IR) * WQ0013263
Applicant/Permittee Town of Boone
Email Notifications
Does this need review by the hydrogeologist?* Yes • No
Regional Office
CO Reviewer
Admin Reviewer
Winston-Salem

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name*
Mike Everett
Email Address*
[e-mail]
Project Information
Application/Document Type *
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
8282686270
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
NDAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type: *
Permit Number: *
Applicant/Permittee Address*
Facility Name*
Wastewater Irrigation
Other Wastewater
Closed -Loop Recycle
Single -Family Residence Wastewater
Irrigation
WQ0013263
Has Current Existing permit number
PO Drawer 192, Boone, NC 28607
Town of Boone Class A Residuals Program
Please provide comments/notes on your current submittal below.
High -Rate Infiltration
Reclaimed Water
Residuals
Other
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here. *
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
20220201123517209. pdf 6.01 M B
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
By checking this box, I acknowledge that I understand the application will not be
accepted for pre -review until the fee (if required) has been received by the Non -
Discharge Branch. Application fees must be submitted by check or money order and
made payable to the North Carolina Department of Environmental Quality (NCDEQ).
I also confirm that the uploaded document is a single PDF with all parts of the
application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Q (Needzr
Submission Date 2/1/2022

ANNUAL DISTRIBUTION AND MARKETING/SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
FACILITY NAME: Town of Boone Jimmy Smith W WTP
FACILITY TYPE(please check one):
X
PERMIT #: WQ0013263 COUNTY: Watauga
Surface Disposal (complete Part A (Sources(s) and "Residual IN" Volume Only) and Part C)
Distribution and Marketing (complete Parts A,B, and C)
YES X NO
If NO, skip Parts A,B,and C and certify form below.
VV HJ 1 fir, Tlll.1L111 ur vl lal.,..-iiivi..�v.....•... ................... ....
Part A*
Part B*
Month
Sources
(Include NPDES # if applicable)
Volume
Recipient Information
Amendment/
Balding Agent IN
Residual IN
Product OUT
Name(s) Volume
(thy tons)
Intended Use(s)
January
Town of Boone Permit # NC0020621
None
***
36.30
6.3
February
Town of Boone Permit # NC0020621
None
95.10
Please see attachment for
43.3
Please see attachment
March
Town of Boone Permit # NC0020621
None
73.80
recipient information on
323.75
April
Town of Boone Permit # NC0020621
None
64.80
a monthly basis.
87.5
May
Town of Boone Permit # NC0020621
None
62.10
52.75
June
Town of Boone Permit # NC0020621
None
52.70
57.0
July
Town of Boone Permit # NC0020621
None
55.00
0.0
August
Town of Boone Permit # NC0020621
None
60.50
77.5
Town of Boone Permit # NC0020621
None
90.60
12.5
September
October
Town of Boone Permit # NC0020621
None
43.30
0.00
November
Town of Boone Permit # NC0020621
None
79.20
23.5
December
Town of Boone Permit # NC0020621
None
37.20
0.0
Totals:
Annual (dry tons)
750.60
684.0
Amendment(s) used:
None Bulking Agent(s) used: None
dditisneet(s)
*If more space is required than geiven, please use the comment space provided below or attach aonal .
Comments:
Part C
Facility was compliant during calender year 2021 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality x YES NO. If NO, please provide a written description of why the facility was not compliant.
1. All monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified lab results are attached.
2. All operations and maintenance requirements were compiled with or, in the case of deviation, prior to authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY KNOWLEDGE AND BELIEF, TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING
ORAATION, INCLUDING THE POSSIBILITY OF FINES AND EMPRISONMENTS FOR KNOWING VIOLATIONS."
�= v% ,F.g
ATURE OF PE TTEE DATE SIGNATURE OF PREPARER DATE
(If different from Pennittee) *Preparer is defined in 40 CFR Part 503.90

BACKGOUND INFORMATION
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
City Boone State NC
Facility Contact Mike Everett
Signatory
Zip 28607
Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC
Zip
28607
FROM
3. REPORTING PERIOD
YEAR
MO
DAY
21
1
6. FACILITY STATUS
Preparer of sewage sludge
Land applier
Owner/operator of surface disposal site
Owner/operator of incinerator
X
TO
YEAR
MO
DAY
21
12
31
4. NPDES PERMIT NUMBER
NC0020621
7. TOTAL ANNUAL VOLUME OF SEWAGE SLUDGE
1
3
6.3
43.3
323.8
0.0
77.5
12.5
Units:
2
4
87.5
52.8
57.0
0.0
23.5
0.0
(metric tons; dry weight)
Other: dry tons
5. SLUDGE PERMIT NUMBER
WQ0013263
8. FINAL USE AND DISPOSAL METHOD
Land application
Surface disposal
Unlined or
Incineration
Other, explain
X
Lined
Bulk Distribution
See cover letter
9. Name and address
of persons performing final use or disposal (attach additional
sheets if necessary)
Facility Name
X Same as preparer
Facility Name
Address
Address
City State Zip
City State Zip
Facility Contact Phone
Facility Contact Phone
Volume of sludge received
Final use/disposal method
from preparer
Volume of sludge received from preparer
Final use/disposal method for sludge
for sludge
Facility Name
Facility Name
Address
Address
City State Zip
City State Zip
Facility Contact Phone
Facility Contact Phone
Volume of sludge received
Final use/disposal method
from preparer
Volume of sludge received from preparer
Final use/disposal method for sludge
for sludge
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared umder my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Mike Everett Chief Operator
Area Code and Phone
[phone]
Signature
Date Signed /_ 31_ ��

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone State NC
Facility Contact Mike E verett
Signatory
Zip 28607
Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC
Zip 28607
3. MONITORING PERIOD
YEAR
MO
DAY
FROM 21
1
YEAR MO DAY
TO 21 3 31
4. NPDES PERMIT NUMBER
NC0020621
5. SLUDGE PERMIT NUMBER
WQ0013263 (Class A)
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Potassium
Selenium
Sodium
Zinc
% Total Solids
Ammonia Nitrogen
Nitrate -Nitrite Nitrogen
Total Phosphorous
Total Kjeldahl Nitrogen
pH
PAN
SAR
Sample Measurement
3,100
-
MG/KG
1
Grab
EPA-6010D
Sample Measurement
6.6
100
MG/KG
1
Grab
EPA-6010D
Sample Measurement
1,000
-
MG/KG
1
Grab
EPA-6010D
Sample Measurement
744
7500
MG/KG
1
Grab
EPA-6010D
Sample Measurement
90.7
-
MG/KG
1
Grab
SM-2540G
Sample Measurement
596
-
MG/KG
1
Grab
EPA-50.1
Sample Measurement
ND
-
MG/KG
1
Grab
EPA-353.2
Sample Measurement
15,400
-
MG/KG
1
Grab
EPA-365.1
Sample Measurement
54700
-
MG/KG
1
Grab
EPA-351.2
Sample Measurement
6.1
-
su
1
Grab
EPA-9045D
NA
16500
-
NA
1
Grab
NONE
NA
2.1
9.99
NA
1
Grab
EPA-6010D
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Area Code and Phone
[phone]
Date Signed
Name and Official Title (type or print)
Mike Everett Chief Operator
J'eA)--3V-
Signature &
1-31-

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name
Address
Town of Boone Jimmy Smith Wastewater Treatment Plant
201 Casey Lane
P.O. Box 192
City Boone State NC Zip 28607
Facility Contact
Signatory
Mike Everett Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC
Zip 28607
3. MONITORING PERIOD
YEAR
MO
DAY
FROM 21
YEAR MO DAY
1 1 TO 21 3 31
4. NPDES PERMIT NUMBER
NC0020621
5. SLUDGE PERMIT NUMBER
WQ0013263 (Class A)
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Aluminum
Sample Measurement
14,100
-
MG/KG
1
Grab
EPA-6010D
Arsenic
Sample Measurement
ND
75
MG/KG
1
Grab
EPA-6010D
Cadmium
Sample Measurement
1.7
85
MG/KG
1
Grab
EPA-6010D
Calcium
Sample Measurement
14,900
-
MG/KG
1
Grab
EPA-6010D
Copper
Sample Measurement
447
4300
MG/KG
1
Grab
EPA-6010D
Lead
Sample Measurement
15.8
840
MG/KG
1
Grab
EPA-6010D
Magnesium
Sample Measurement
2140
-
MG/KG
1
Grab
EPA-6010D
Mercury
Sample Measurement
0.360
57
MG/KG
1
Grab
EPA-7471 B
Molybdenum
Sample Measurement
ND
75
MG/KG
1
Grab
EPA-6010D
Nickel
Sample Measurement
13.2
420
MG/KG
1
Grab
EPA-6010D
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Mike E verett Chief Operator
Area Code and Phone
[phone]
Date Signed
Signature

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone State NC
Facility Contact Mike Everett
Signatory
Zip 28607
Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC
Zip 28607
3. MONITORING PERIOD
YEAR
FROM 21
6. INSTRUCTIONS:
MO
4
DAY
1
TO
YEAR
21
MO
6
DAY
30
4. NPDES PERMIT NUMBER
NC0020621
5. SLUDGE PERMIT NUMBER
WQ0013263 (Class A)
Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Sample Measurement
16,200
-
MG/KG
1
Grab
. EPA-6010D
Sample Measurement
ND
75
MG/KG
1
Grab
EPA 6010D
Sample Measurement
1.4
85
MG/KG
1
Grab
EPA-6010D
Sample Measurement
16,200
-
MG/KG
1
Grab
EPA 6010D
Sample Measurement
379
4300
MG/KG
1
Grab
EPA-6010D
Sample Measurement
12.9
840
MG/KG
1
Grab
EPA-6010D
Sample Measurement
2330
-
MG/KG
1
Grab
EPA-6010D
Sample Measurement
0.230
57
MG/KG
1
Grab
EPA-7471 B
Sample Measurement
ND
75
MG/KG
1
Grab
EPA-6010D
Sample Measurement
13.0
420
MG/KG
1
Grab
EPA-6010D
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering
submitted, it is to the best of my knowledge and belief, true, accurate, and complete_ I am aware that there are significant penalties for submitting false information.
to assure that
the information
Name and Official Title (type or print)
Mike Everett Chief perator
Area Code and Phone
[phone]
Signature •���}} a �jj
Mir nn 0 , i . F1113n774
Date Signed `��

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name
Address
Town of Boone Jimmy Smith Wastewater Treatment Plant
201 Casey Lane
P.O. Box 192
City Boone State NC
Facility Contact Mike Everett
Signatory
Zip 28607
Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC
Zip 28607
3. MONITORING PERIOD
YEAR
FROM 21
6. INSTRUCTIONS:
MO
7
DAY
1
TO
YEAR
21
0
9
DAY
30
4. NPDES PERMIT NUMBER
NC0020621
5. SLUDGE PERMIT NUMBER
WQ0013263 (Class A)
Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Potassium
Selenium
Sodium
Zinc
% Total Solids
Ammonia Nitrogen
Nitrate -Nitrite Nitrogen
Total Phosphorous
Total Kjeldahl Nitrogen
pH
PAN
SAR
Sample Measurement
2550
-
MG/KG
1
Grab
EPA-6010D
Sample Measurement
5.20
100
MG/KG
1
Grab
EPA-6010D
Sample Measurement
987
-
MG/KG
1
Grab
EPA-6010D
Sample Measurement
850
7500
MG/KG
1
Grab
EPA-6010D
Sample Measurement
91.1
-
MG/KG
1
Grab
SM2540G
Sample Measurement
1,250
-
MG/KG
1
Grab
EPA-350.1
Sample Measurement
ND
-
MG/KG
1
Grab
EPA-353.2
Sample Measurement
15000
-
MG/KG
1
Grab
EPA-365.1
Sample Measurement
47300
-
MG/KG
1
Grab
EPA-351.2
Sample Measurement
6.3
-
su
1
Grab
EPA-9045D
NA
14400
-
NA
1
Grab
NONE
NA
2
9.99
NA
1
Grab
EPA-6010D
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information.
Area Code and Phone
[phone]
Name and Official Title (type or print)
Mike Everett Chief Operator
Date Signed
Signature

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name
Address
Town of Boone Jimmy Smith Wastewater Treatment Plant
201 Casey Lane
P.O. Box 192
City Boone State NC
Facility Contact Mike Everett
Signatory
Zip 28607
Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC
Zip 28607
3. MONITORING PERIOD
YEAR
FROM 21
MO
7
DAY
1
TO
YEAR
21
MO
9
DAY
30
4. NPDES PERMIT NUMBER
NC0020621
5. SLUDGE PERMIT NUMBER
WQ0013263 (Class A)
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Sample Measurement
14,300
-
MG/KG
1
Grab
EPA-6010D
Sample Measurement
ND
75
MG/KG
1
Grab
EPA-6010D
Sample Measurement
1.40
85
MG/KG
1
Grab
EPA-6010D
Sample Measurement
17,000
-
MG/KG
1
Grab
EPA-6010D
Sample Measurement
471
4300
MG/KG
1
Grab
EPA-6010D
Sample Measurement
15.6
840
MG/KG
1
Grab
EPA-6010D
Sample Measurement
2580
-
MG/KG
1
Grab
EPA-6010D
Sample Measurement
0.27
57
MG/KG
1
Grab
EPA-7471B
Sample Measurement
4.20
75
MG/KG
1
Grab
EPA-6010D
Sample Measurement
13.8
420
MG/KG
1
Grab
EPA-6010D
10. CERTIFICATION
1 certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Mike Everett Chief Opera r
Area Code and Phone
[phone]
Date Signed
1-31- )0-
Si nature
, a. (

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name
Address
Town of Boone Jimmy Smith Wastewater Treatment Plant
201 Casey Lane
P.O. Box 192
City Boone State NC
Facility Contact Mike Everett
Signatory
Zip 28607
Phone [phone]
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC
Zip 28607
3. MONITORING PERIOD
YEAR
FROM 21
MO
10
DAY
1
TO
YEAR
21
MO
12
DAY
31
4. NPDES PERMIT NUMBER
NC0020621
5. SLUDGE PERMIT NUMBER
WQ0013263 (Class A)
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant Concentration
(dry weight)
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Reg Limit
Units
Potassium
Selenium
Sodium
Zinc
% Total Solids
Ammonia Nitrogen
Nitrate -Nitrite Nitrogen
Total Phosphorous
Total Kjeldahl Nitrogen
pH
PAN
SAR
Sample Measurement
2530
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
4.6
100
MG/KG
1
Grab
EPA6010D
Sample Measurement
1000
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
848
7500
MG/KG
1
Grab
EPA6010D
Sample Measurement
91.4
-
MG/KG
1
Grab
SM2540G
Sample Measurement
1,100
-
MG/KG
1
Grab
EPA350.1
Sample Measurement
2.8
-
MG/KG
1
Grab
EPA353.2
Sample Measurement
16,300
-
MG/KG
1
Grab
EPA365.1
Sample Measurement
57000
-
MG/KG
1
Grab
EPA351.2
Sample Measurement
,
6.4
-
su
1
Grab
EPA9045D
NA
17300
-
NA
1
Grab
NONE
NA
1.8
9.99
NA
1
Grab
EPA-6010D
10. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Mike E verett Chief Operator
Signature
Area Code and Phone
[phone]
Date Signed

CLASS A RESIDUALS POLLUTANT LIMITS
1. NAME AND ADDRESS OF FACILITY
Facility Name Town of Boone Jimmy Smith Wastewater Treatment Plant
Address 201 Casey Lane
P.O. Box 192
City Boone State NC
Zip 28607
Facility Contact Mike Everett Phone [phone]
Signatory
2. NAME AND ADDRESS OF FACILITY OWNER
Facility owner's Name Town of Boone
Address P.O. Box 192
City Boone
State NC
Zip 28607
3. MONITORING PERIOD
YEAR
FROM 21
MO
10
DAY
1
TO
YEAR
21
MO
12
DAY
31
4. NPDES PERMIT NUMBER
NC0020621
5. SLUDGE PERMIT NUMBER
WQ0013263 (Class A)
6. INSTRUCTIONS: Complete the form based on the results of all analyses performed during the monitoring period using approved analytical method.
Complete a separate sheet for each monitoring period during the reporting period.
Parameter
Pollutant
Concentration
(dry weight)
Reg Limit
Units
Frequency of
Analysis
Sample Type
(Grab or Composite)
Analytical
Method
Avg.
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Sample Measurement
15000
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
ND
75
MG/KG
1
Grab
EPA6010D
Sample Measurement
1.5
85
MG/KG
1
Grab
EPA6010D
Sample Measurement
21,200
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
503
4300
MG/KG
1
Grab
EPA6010D
Sample Measurement
16.2
840
MG/KG
1
Grab
EPA6010D
Sample Measurement
2430
-
MG/KG
1
Grab
EPA6010D
Sample Measurement
0.4500
57
MG/KG
1
Grab
EPA7471 B
Sample Measurement
4.6
75
MG/KG
1
Grab
EPA6010D
Sample Measurement
13.6
420
MG/KG
1
Grab
EPA6010D
10. CERTIFICATION
.I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons directly responsible for gathering the information
submitted, it is to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information.
Name and Official Title (type or print)
Mike Everett Chief Operator
Area Code and Phone
[phone]
Signature In r
A liuf7t1.71-Date
Signed

Please
Permit Number
Facility Name
NPDES #
or WQ # (residual only facilities)
WWTP Name
note
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding laboratory analysis.
that your permit may contain additional parameters to be analyzed than thise requred to be
Laboratory
WQ0013263
Town of Boone
NC0020621
Town of Boone Jimmy Smith Wastewater Treatment Plant
summarized on this form.
1) Research & Analytical Labs Inc.
2) Water Quality Services, Inc.
3)Pace Analytical Services LLC
Date Sampled (Grab)
Ceiling Con
1/28/2021
4/8/2021
7/15/2021
10/21/2021
Quarter
Limit mg/kg
1st
2nd
3rd
4th
Parameters (mg/kg ary
Aluminum
NA 14,100
16200
14,300
15,000
Arsenic
75 ND
ND
ND
ND
Cadmium
85 1.70
1.4
1.40
1.5
Calcium
NA 14,900
16200
17,000
21,200
Copper
4300 447
379
471
503
Lead
840 15.8
12.9
15.6
16.2
Magnesium
NA 2,140
2,330
2,580
2,430
Mercury
57 0.3600 -
0.2330
0.27
0.4500
Molybdenum
75 ND
ND
4.20
4.60
Nickel
420 13.2
13.0
13.8
13.6
Potassium
NA 3,100
3,890
2,550
2,530
Selenium
100 6.60
6.30
5.20
_
4.60
Sodium
NA 1000
1,390
987
1,000
Zinc
7500 744
700
850
848
Ammonia Nitrogen
NA 596
884
1,250
1,100
Nitrate -Nitrite Nitrogen
NA nd
ND
ND
2.8
Total Phosphorous
NA 15400
15,800
15,000
16,300
Total Kjeldahl Nitrogen
NA 54700
53400
47,300
57000
_
_
_
pH
NA 6.1
5.8
_
6.3
6.4
PAN
NA 16500
16,200
14,400
17300
SAR
9.99
2.10
2.80
2.00
1.80
% Total Solids
NA
90.7
90.8
91.1
91.4
X , Q . I- 31 D-�--
(SIGNATURE OF PREPARER) DATE
"t certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. ) am aware that there are
Significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant
WQ Permit Number: WQ0013263
NPDES Number: NC0020621
Monitoring Period: From 1/1/2021 To 3/31/2021
- Please indicate level achieved and alternative performed:
Class A:
Alternative 1 1 1
Alternative 2 LI
Alternative 3 L
Alternative 4 LI
Alternative 5 RI
Alternative 6 r
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost Cl
Heat Drying IA
Heat Treatment LI
Thermophilic L
Beta Ray [1
Gamma Ray E1
Pasteurization
Class B:
Alternative 1 1
Alternative 2 LI
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ®
Air Diying0
Composting LI
Aerobic Digestion Li
Anaerobic Digestion LI
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2x10tothe
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight
9
20
44
MPN/g
Quarterly
grab
9221-E
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
- Please indicate option performed:
Alt.1 (VS reduction)
[l
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench) 11
Alt. 4 (Spec. 02 uptake)
Li
Alt. 5 (14-Day Aerobic)
®
Alt. 6 (Alk. Stabilization 0
Alt 7 (Drying - Stable) i1
Alt. 8 (Drying - Unstable)
LI
Alt, 9 (Injection)
Alt. 10 (Incorporation) ®
No vector attraction reduction alternatives were performed
El
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Everett Chief Operator NA
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
1-31--��
gAjtael
Signature of Preparer*
r, re,Euk)
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant
WQ Permit Number: WQ0013263
NPDES Number: NC0020621
Monitoring Period: From 4/1/2021
To
6/30/2021
Please indicate level achieved and alternative performed:
Class A:
Alternative 1 EJ
Alternative 2 L.
Alternative 3 Li
Alternative 4 El
Alternative 5 El
Alternative 6 IA
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost El
Heat Drying Ii
Heat Treatment 0
Thermophilic LI
Beta Ray C
Gamma Ray El
Pasteurization El
Class B:
Alternative 1 El
Alternative 2 l
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization IA
Air Dryingll
Composting 0
Aerobic Digestion El
Anaerobic Digestion El
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
13
18
27
MPN/G
Quarterly
grab
9221 E
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
- Please incate option perf
diormed:
Alt.1 (VS reduction)
Alt. 2 (40-day bench) ®
Alt. 3 (30-day bench) [1
Alt. 4 (Spec. 02 uptake)
L.1
Alt. 5 (14-Day Aerobic)
El
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) RI
Alt. 8 (Drying - Unstable)
El
Alt. 9 (Injection)
El
Alt. 10 (Incorporation) El
No vector attraction reduction alternatives were performed
,
El
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Everett Chief Operator NA
Land Applier Name and Title (if applicable)(type or print)
Preparer Name and Title (type or print)
IAEA; U- , F�
Signature of Preparer*
131- --
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant
WQ Permit Number: WQ0013263
NPDES Number: NC0020621
Monitoring Period: From 7/1/2021 To 9/30/2021
2) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 El
Alternative 2 1I
Alternative 3 D
Alternative 4 1
Alternative 5 P
Alternative 6 El
If applicable to alternative performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost LI
Heat Drying P1
Heat Treatment
Thermophilic LI
Beta Ray ®
Gamma Ray 1
Pasteurization
Class B:
Alternative 1 0
Alternative 2 1
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization L1
Air Drying®
Composting El
Aerobic Digestion EA
Anaerobic Digestion CI
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
Sample
T e
Type
Analytical
Tech -
nique
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
17
27
43
MPN/G
Quarterly
-
grab
9221 E
Salmonella bacteria
(in lieu of fecal
coliforin)
3 MPN per 4 grams
total solid (dry
weight)
-Please indicate option performed:
Alt.1 (VS reduction)
Alt. 2 (40-day bench) l
Alt. 3 (30-day bench)
Alt. 4 (Spec. 02 uptake)
El
Alt. 5 (14-Day Aerobic)
El
Alt. 6 (A1k. Stabilization Ll
Alt 7 (Drying - Stable) P1
Alt. 8 (Drying - Unstable)
El
Alt. 9 (Injection)
0
Alt. 10 (Incorporation) ®
No vector attraction reduction a ternatives were performed
El
CERTIFICATION STATEMENT (please check the appropriate statement)
LEI "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Everett Chief Operator NA
Land Applier Name and Title (if applicable)(type or print)
I-3l'aa-
Date Signature of Land Applier (if applicable) Date
Preparer Name and Title (type or print)
j-LaQ 60-em
Signature of Preparer*
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone
WQ Permit Number: WQ0013263
NPDES Number: NC0020621
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant
Monitoring Period: From 10/12021 To 12/31/2021
- Please indicate level achieved and alternative performed:
Class A:
Alternative 1 0
Alternative 2 1 1
Alternative 3 El
Alternative 4 El
Alternative 5 El
Alternative 6 El
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost
Heat Drying 4
Heat Treatment El
Thermophilic LI
Beta Ray
Gamma Ray LI
Pasteurization
,
Class B:
Alternative 1 1
Alternative 2
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Air Dryingl.
Composting IA
Aerobic Digestion El
Anaerobic Digestion El
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
umber of
Excee-
deuces
Frequency
of Analysis
Sample
Type
Analytical
Tech -
moue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
154
270
473
MPN/G
Quarterly
grab
9221 E
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
-Please indicate option per
formed:
Alt.1 (VS reduction)
l
Alt. 2 (40-day bench) l l
Alt. 3 (30-day bench) li
Alt. 4 (Spec. 02 uptake)
li
Alt. 5 (14-Day Aerobic)
El
Alt. 6 (Alk. Stabilization CJ
Alt 7 (Drying - Stable) v
Alt. 8 (Drying - Unstable)
L i
Alt. 9 (Injection)
0
Alt, 10 (Incorporation) [1
No vector attraction reduction alternatives were performed
LI
CERTIFICATION STATEMENT (please check the appropriate statement)
Cl "I certify, udder penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Everett Chief Operator NA
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
1-31---
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

H urn er
Exhaust
to
Atmosphere-
-
• Fuel'
sl=:ram-
-Cake
Lra'Il z-kt
• Stearn
Steam
Condensate
Aeffu -
==SC'
O CIL��GIti
o
• Thin-Sfudge-
•
L'
• -�: ram=
•
Condensatef' - -
Cooling H2O
Off
Clean' - -
Exh a ust
to -
Atmosphere
off
Gases=
`.-
_:.��stt-.:-�f% v� 4=• y-4�-__'.__ �-• �'Yr_-
-i �
Gases t
'F=,V;r__'y-�--ci=J
Coaling H2O
Filtered Gases
- .Flow Diagram
Boone WJW.T.P

• ROTOR AIR VENT
CoNNEciloN
'HOLLOW SHAFT.
GEARBOX
EXHAUST VAPOR OUTLET
SEALED ACCESS COVER
SCRAPER 'BAR —N4
STEAM /.
VAPOR DOME ----
. • DISC.
CONDENSATE PIPE
.BAFFLE PLATE.
STATOR.
SUPPORT SADDLE
MATERIAL OUTLET
FOUNDATION
END . VI EW .SECTI ON • .
EXHAUST VAPOR OUTLET •
VAPOR DOME
MATERIAL INLET '
I 1-1 .1. I 1
L., I 'A
L
Tr'N'
• L
• Ill
PADDLES.
FOUNDATION
SIDE. VIEW SECTION
MATERIAL INLET
At1as.Stor(1.ROTADISC®.
INDIRECT HEATED DISC DRIER ." •
Figige 1
I •
SCRAPER BARS.
ROTOR ARMS
DISCS
SEAL
ROTOR. BEARING •
sIPHOW:TUBE
CONDENSATE OUTLET
ROTARY STEAM JOINT
STEAM INLET . .
ROTOR SHAFT
STEAM j'
CONDENSATE PIPES '
MATERIAL OUTLET
SUPPORT SADDLE'.

Town_ of B o orle Was-Eewa-Eer-TTeaim-Lent Plant
. Class A Drier Time/Temp eraf e Op era•tinb Parameters
Discharge Volume; I 6. 7 ct7lu- ,
12 Wet product Density:.
g Maximum Feed Rate:- (Ibs/hr)
Wet Feed Volume =3750/62 = (car)
`I DriedProduotDensi
5• ty: (lbs/ct)
6 Dried Product Discharge
667/ ORate: cf- (b)
• 7 Average Volume Flow (wet to dr
y): (cFlhr)
& Product Volpme ofTST-40
9 Drier: (c�
Pereznte
10 gePro dtictVoid Space.; °o
Net Product Volume =459x.40= Co
11 EfiataPedResidmace Tim e; (hr) .
TE/k aER4:TU
I
2
InletTemp ei•atureRange (F)
Outlet TernperatureRange (F) •
` —, Feed Volume; 60.5 cF1u-
Ne oduct oume: 275.4cf =`fAl
un• u'F� 1,.3:L `� .^J.y�T-rr„xt {ram ¢v, �r
44
' c l.' crime P i/� i.:i r :fri 1%4 -
i n9iu�F�i:l�;n.r•-i'a4t•'OP • i:;ii;� v+41 4. q- r h� •A:
„•;+ice --00*i;0► -•,_•4j,.0 ,—„,..�,{ .
62.0
3750.0
60.5
40,0
667, 0
16.7
'3 B.6 -
459.0
0.4
. 275.4
7.1 "
I85-2I0
210220
• Average or"�Yel-Feed Volume(3) indDriedProduct Volume (6)
Net Drier Volume (I 0) ditided by Average Product Volume (7)

Drier Log
Date/Ti
me
b;
p
�,
Steam
Preas. Set
int :
I~ v
•0
v)•P
b�T-ao. -
iJrier
Discharge
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HC114
12/21/98

Drier Log
DATE _jo 011
D a te/Ti
me
57-10- al
oo SS -
IIIMINIMMINIMINIIIIMMI
/cy7iLis
Yizzi
/too
/1700
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-
HC114
12/28/98

D ATE ‘81 � _
Date/Ti
me
,4,1 t/ogoo
7
t
•.
/fa7
3
110 /uu . 3
140
Zola
2I22
2
0.11 /01oO R5 /as -3
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JI /0
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105,0
2o /22-3
/6600 3 ?,a., /tit
39,zoozz
/1906 56_ 190/a r7
largo q itsi as
a its l.22Y
`y't�•- w %-4
2c2 00-
a1
Z 9 2q
2-7 7
Drier Log C3Rd Q(J,r\
(os
(Ps
27 7 GS
2Z10,5
I3 70
a� 7s
a- a? 75
2�
24-
oi�
955
�`4'24to too via 1 lS r-.2 2 S a
/q?oo 3 PO/A20
• Notes:
:ply( (ji.) 2.634 %or1rr.t. ,o n
-16
7_5
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ct
0
31
100
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75 S
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12/28/98

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12/28/9S

Town of Boone Wastewater Treatment Plant
2021 Class Residuals Production
Run Gallons Digester Total
No. Run Date Processed % Solids Dry Tons
1 1/4/2021 150,086 1.96 12.30
2 1/11/2021 257,895 2.23 24.00
3 2/1/2021 126,834 2.51 13.30
4 2/8/2021 249,440 2.49 25.90
5 2/15/2021 209,276 2.56 22.30
6 2/22/2021 317,085 2.54 33.60
7 3/1/2021 186,023 2.33 18.10
8 3/8/2021 141,631 2.55 15.10
9 3/15/2021 162,770 2.21 15.00
10 3/22/2021 42,278 2.65 4.70
11 3/29/2021 188,137 2.67 20.90
12 4/12/2021 272,693 2.65 30.10
13 4/19/2021 173,340 2.44 17.60
14 4/27/2021 175,454 2.34 17.10
15 5/3/2021 156,428 2.39 15.60
16 5/10/2021 207,162 2.42 20.90
17 5/24/2021 232,529 2.64 25.60
18 6/7/2021 160,656 2.84 19.00
19 6/14/2021 114,150 2.31 11.00
20 6/21/2021 92,878 2.81 10.90
21 6/28/2021 109,923 2.58 11.80
22 7/12/2021 131,062 3.16 17.30
23 7/19/2021 141,631 3.02 17.80
24 7/26/2021 154,315 3.10 19.90
25 8/2/2021 105,695 2.98 13.10
26 8/9/2021 141,631 2.89 17.70
27 8/16/2021 124,720 2.93 15.20
28 8/23/2021 116,265 3.00 14.50
29 8/30/2021 164,884 2.92 20.10
30 9/8/2021 63,417 2.76 7.30
31 9/13/2021 154,314 2.78 17.80
32 9/20/2021 200,826 2.63 22.00
33 9/27/2021 226,187 2.48 23.40
34 10/4/2021 207,162 2.79 24.10
35 10/11/2021 114,151 2.80 13.30
36 10/18/2021 78,214 1.80 5.90
Notes

37 11/1/2021 188,137 3.00 23.50
38 11/8/2021 158,543 3.12 20.60
39 11/15/2021 114,150 2.68 12.80
40 11/22/2021 139,517 3.14 18.19
41 11/29/2021 35,936 2.67 4.00
42 12/13/2021 173,340 2.82 20.30
43 12/202021 145,859 2.70 16.90
44
Totals 6,806,624 750.49

Town of Boone Wastewater Treatment Plant
2021 Class A Residuals Distibution Log
Qtr
Month
Date
Recipient
Address
Dry
Tons
Intended Use
Month
Total
1
Jan
4-Jan
Kyle Hayes
491 Dogcreek Rd Crumpler NC 28617
6.3
Pasture
Feb
2-Feb
Freddie Rupard
P.O. Box 1982 Blowing Rock N.C.
43.3
Pasture
Mar
6-Mar
Martha Ford
674 Ford Rd Boone NC 28607
79.3
Pasture
8-Mar
John Sturgill
3410 Roundabout Rd Creston NC 28615
50.0
Pasture
9-Mar
Todd Young
3009 Jim Davis Rd Grassy Creek NC 28631
22.5
Hay Fields
9-Mar
Jeff Roten
860 Jones Rd Creston NC 28615
53.8
Pasture
11-Mar
Lloyd Lambert
635 Harless Rd West Jefferson NC 28694
113.8
Hay Fields
27-Mar
Len Ford
1304 Ford Rd Boone NC 28607
4.0
Pasture
373
2
Apr
12-Apr
Jerry Bare
348 Bare Ridge Rd West Jefferson NC 28694
50.0
Pasture
14-Apr
Chad Denny
6175 Big Laurel Rd Creston NC 28615
37.5
Pasture
May
20-May
George Ashley
142 Edno St Boone NC 28607
15.0
Hay Fields
26-May
John Sturgill
3410 Roundabout Rd Creston NC 28615
20.0
Pasture
27-May
Martha Ford
674 Ford Rd Boone NC 28607
17.8
Pasture
Jun
1-Jun
Charles Norris
4190 Big Hill Rd Todd NC 28684
57.00
Pasture
197.30
3
Aug
19-Aug
Gary Clawson
AM Cheek Rd Fleetwood NC
11.3
Pasture
23-Aug
Lloyd Lambert
635 Harless Rd West Jefferson NC 28694
66.3
Pasture
Sept
1-Sep
Ronnie Mattheson
471 Mack Branch Rd Mtn. City Tn.
12.5
Pasture
90
4
Nov
29-Nov
Jeff Bolger
5229 Hwy 221 N Jefferson NC 28694
23.5
Pasture
23.500
•
Qtr
Month
Date
Recipient
Address
Dry
Tons
Intended Use
Month
Total
TOTAL
684

High Country 6-1-0 Siiosoludis
Produced by the Town of Boone
P.O. Drawer 192, Boone, NC 28607
High Country 6-1-0 (HC 610) is a high organic content fertilizer manufactured by the Town of Boone
Wastewater Treatment Facility. This product produces superior results on lawns, flower beds and
shrubs providing nutrients at the rates indicated below:
Guaranteed Analysis
Total Nitrogen 6%
Water Insoluble Nitrogen 3.5%
Available Phosphoric Acid 1%
Soluble Potash 0%
Iron
1%
Lawn -Sod Establishment:
Turf Maintenance:
Plant Bed Establishment:
Planting Bed Maintenance:
Recommended Application Rates
Apply HC 610 at rate of 30 Ibs per 1000 sq feet.
Apply HC 610 at a rate of 10-15 Ibs per 1000 sq feet.
Apply HC 610 at a rate of 2 Ibs per 100 sq feet into soil.
Apply HC 610 at a rate of 2 Ibs per 100 sq feet in Spring/Fall
Warnings: HC 610 is environmentally safe when used as directed, but can become a hazard if
mismanaged. This product should not be used on soils intended for food crop production. '
Cover HC 610 with a tarp or plastic during transportation. Store HC 610 in a dry area away from wells
or surface water where it could be washed into streams; keep product away from children's play
areas.
Limited Warranty and Disclaimer: The Town of Boone warrants that HC 610 meets the specifications
stated above, and that the heavy metal content is less than or equal to the limitations specified in the
EPA and NC Dept of Environmental and Natural Resources sludge quality criteria for land application.
If HC 610 fails to meet its specification, the buyer's sole remedy shall be the recovery of the purchase
price. Under no circumstances shall the Town of Boone be liable for any other damages, including
direct, indirect, consequential or special damages.
The undersigned Buyer agrees to abide by the following Restrictions:
HC 610 shall not be applied to land except in accordance with the instructions contained herein.
HC 610 shall not be applied to any site that is flooded, frozen, or snow-covered.
HC 610 shall not be applied within 100 feet of any water supply, stream, river, or lake.
Adequate measures shall be provided to prevent surface runoff from carrying this product into any
surface waters.
Buyer Signature
Date
Name (Print): Quantity:
Ibs/tons
Street/Route: Intended Use:.
City/State/Zip: Amount Collected:
Telephone: Loaded By:

(eAnaIYtical
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February 11, 2021
Karen Reece
Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
RE: Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Dear Karen Reece:
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Enclosed are the analytical results for sample(s) received by the laboratory on January 28, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
336-996-2841
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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CERTIFICATIONS
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC,
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SAMPLE SUMMARY
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Lab ID Sample ID Matrix Date Collected Date Received
92519208001 Biosolids
Solid 01/28/21 07:15 01/28/21 15:16
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Lab ID Sample ID
Method
Analytes
Analysts Reported Laboratory
92519208001 Biosolids
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
EPA 6010D
EPA 6010D
EPA 7471B
SM 254OG-2011
SW-846
EPA 9045D
None
EPA 350.1 Rev 2.0 1993 Mod.
EPA 351.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
KQ, SH1 13 PASI-A
RDT 1 PASI-A
SOO 1 PASI-A
KDF 1 PASI-C
KDF 1 PASI-C
SMK 1 PASI-A
DMN 1 PASI-A
KDF1 1 PASI-A
MFO 1 PASI-A
CJL 1 PASI-A
KDF1 1 PASI-A
Page 4 of 18

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ANALYTICAL RESULTS
Project: BioSolids-Quarterly 1/28/21
Pace Protect No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Sample: Biosolids Lab ID: 92519208001 Collected: 01/28/21 07:15 Received: 01/28/21 15:16 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050E
Pace Analytical Services -Asheville
Aluminum 14100 mg/kg 44.5 5 02/10/21 08:59 02/11/21 11:24 7429-90-5 M1
Arsenic ND mg/kg 2.2 1 02/10/21 08:59 02/10/21 20:08 7440-38-2
Cadmium 1.7 mg/kg 0.089 1 02/10/21 08:59 02/10/21 20:08 7440-43-9
Calcium 14900 mg/kg 111 5 02/10/21 08:59 02/11/21 11:24 7440-70-2 M1
Copper 447 mg/kg 4.4 1 02/10/21 08:59 02/10/21 20:08 7440-50-8
Lead 15.8 mg/kg 0.89 1 02/10/21 08:59 02/10/21 20:08 7439-92-1
Magnesium 2140 mg/kg 8.9 1 02/10/21 08:59 02/10/21 20:08 7439-95-4
Molybdenum ND mg/kg 4.4 1 02/10/21 08:59 02/10/21 20:08 7439-98-7 BC
Nickel 13.2 mg/kg 0.44 1 02/10/21 08:59 02/10/21 20:08 7440-02-0
Potassium 3100 mg/kg 445 1 02/10/21 08:59 02/10/21 20:08 7440-09-7
Selenium 6.6 mg/kg 0.89 1 02/10/21 08:59 02/10/21 20:08 7782-49-2
Sodium 1000 mg/kg 445 1 02/10/21 08:59 02/10/21 20:08 7440-23-5
Zinc 744 mg/kg 0.89 1 02/10/21 08:59 02/10/21 20:08 7440-66-6 M1
Sodium Adsorption Ratio, SAR Analytical Method: EPA 6010D
Pace Analytical Services - Asheville
Sodium Adsorption Ratio 2.1 meq/L 1 02/11/21 15:07 N2
7471 Mercury Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Pace Analytical Services - Asheville
Mercury 0.36 mg/kg 0.058 20 02/01/21 12:15 02/01/21 14:21 7439-97-6
2540G Total Percent Solids Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids 90.7 % 0.10 1 02/02/21 16:42
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
Date: 02/11/2021 06:37 PM
Analytical Method: SW-846
Pace Analytical Services - Charlotte
9.3 % 0.10 1 02/02/21 16:33
Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
6.1 Std. Units 0.10 1 02/08/21 16:11
N2
H3
Analytical Method: None
Pace Analytical Services - Asheville
16500 mg/kg 1 02/11/21 14:35 N2
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350,1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
596 mg/kg 10.2 1 02/04/21 11:26 02/05/21 10:38 7664-41-7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Sample: Biosolids Lab ID: 92519208001 Collected: 01/28/21 07:15 Received: 01/28/21 15:16 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
365.1 Phosphorus, Total
Phosphorus
Date: 02/11/2021 06:37 PM
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
54700 mg/kg
2760 50 02/02/21 20:19 02/04/21 05:17 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
ND mg/kg 4.4 1 01/29/21 21:57 01/30/21 01:41
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
15400 mg/kg
285 300 02/01/21 19:44 02/02/21 13:52 7723-14-0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
QC Batch: 596646 Analysis Method: EPA 7471 B
QC Batch Method: EPA7471B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92519208001
METHOD BLANK: 3146536 Matrix: Solid
Associated Lab Samples: 92519208001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 02/01/21 14:02
LABORATORY CONTROL SAMPLE: 3146537
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0.087 104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3146538 3146539
MS MSD
92519288001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury mg/kg ND 0.026 0.025 0.020 0.020 75 77 75-125 0 20
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 02/11/2021 06:37 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
QC Batch: 598898 Analysis Method: EPA6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92519208001
METHOD BLANK: 3157376 Matrix: Solid
Associated Lab Samples: 92519208001
Parameter
Blank Reporting
Units Result Limit Analyzed Qualifiers
Aluminum mg/kg ND 10.0 02/10/21 20:01
Arsenic mg/kg ND 2.5 02/10/21 20:01
Cadmium mg/kg ND 0.10 02/10/21 20:01
Calcium mg/kg ND 25.0 02/10/21 20:01
Copper mg/kg ND 5.0 02/10/21 20:01
Lead mg/kg ND 1.0 02/10/21 20:01
Magnesium mg/kg ND 10.0 02/10/21 20:01
Molybdenum mg/kg ND 5.0 02/10/21 20:01 BC
Nickel mg/kg ND 0.50 02/10/21 20:01
Potassium mg/kg ND 500 02/10/21 20:01
Selenium mg/kg ND 1.0 02/10/21 20:01
Sodium mg/kg ND 500 02/10/21 20:01
Zinc mg/kg ND 1.0 02/10/21 20:01
LABORATORY CONTROL SAMPLE: 3157377
Parameter
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits
Qualifiers
Aluminum mg/kg 500 490 98 80-120
Arsenic mg/kg 50 48.8 98 80-120
Cadmium mg/kg 50 47.8 96 80-120
Calcium mg/kg 500 470 94 80-120
Copper mg/kg 50 50.0 100 80-120
Lead mg/kg 50 48.0 96 80-120
Magnesium mg/kg 500 462 92 80-120
Molybdenum mg/kg 50 50.9 102 80-120
Nickel mg/kg 50 49.0 98 80-120
Potassium mg/kg 500 ND 99 80-120
Selenium mg/kg 50 45.4 91 80-120
Sodium mg/kg 500 494J 99 80-120
Zinc mg/kg 50 47.0 94 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3157378 3157379
MS MSD
92519208001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Aluminum mg/kg 14100 444 460 15500 16000 307 397 75-125 3 20 M1
Arsenic mg/kg ND 44.4 46 40.4 42.1 87 88 75-125 4 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 02/11/2021 06:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3157378 3157379
MS MSD
92519208001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Cadmium mg/kg 1.7 44.4 46 39.5 41.0 85 86 75-125 4 20
Calcium mg/kg 14900 444 460 15600 16100 158 273 75-125 3 20 M1
Copper mg/kg 447 44.4 46 484 501 82 119 75-125 4 20
Lead mg/kg 15.8 44.4 46 52.2 53.8 82 83 75-125 3 20
Magnesium mg/kg 2140 444 460 2480 2570 76 94 75-125 4 20
Molybdenum mg/kg ND 44.4 46 43.4 45.2 88 89 75-125 4 20
Nickel mg/kg 13.2 44.4 46 50.0 51.7 83 84 75-125 3 20
Potassium mg/kg 3100 444 460 3510 3610 91 110 75-125 3 20
Selenium mg/kg 6.6 44.4 46 42,6 44.7 81 83 75-125 5 20
Sodium mg/kg 1000 444 460 1380 1430 86 93 75-125 3 20
Zinc mg/kg 744 44.4 46 764 791 45 103 75-125 3 20 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 02/11/2021 06:37 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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0
QUALITY CONTROL DATA
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
QC Batch: 597006 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92519208001
SAMPLE DUPLICATE: 3148195
92519317001 Dup Max
Parameter Units Result Result RPD RPD
Qualifiers
Percent Moisture
%
95.4 95.5 0 25 N2
SAMPLE DUPLICATE: 3148452
92519508002 Dup Max
Parameter Units Result Result RPD RPD
Qualifiers
Percent Moisture
72.7 72.4 0 25 N2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 02/11/2021 06:37 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: BloSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
QC Batch: 598260 Analysis Method: EPA 9045D
QC Batch Method: EPA9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92519208001
SAMPLE DUPLICATE: 3154878
92519614001 Dup Max
Parameter Units Result Result RPD RPD
Qualifiers
pH at 25 Degrees C Std. Units 7,4 7.5 1 10 H3
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 02/11/2021 06:37 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
QC Batch: 597648 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92519208001
METHOD BLANK: 3151331 Matrix: Solid
Associated Lab Samples: 92519208001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/kg ND 8.9 02/05/21 10:31
LABORATORY CONTROL SAMPLE: 3151332
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 431 430 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3151333 3151334
MS MSD
92518686001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Ammonia mg/kg ND 2650 2600 2350 2410 89 93 90-110 3 10 M1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 02/11/2021 06:37 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
QC Batch: 596992 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92519208001
METHOD BLANK: 3148078 Matrix: Solid
Associated Lab Samples: 92519208001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 02/04/21 03:58
LABORATORY CONTROL SAMPLE: 3148079
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg 1000 995 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3148080 3148081
MS MSD
92517895001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 2250 2530 2530 5270 4720 119 98 90-110 11 10 M1,R1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 02/11/2021 06:37 PM
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
QC Batch: 596474 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92519208001
METHOD BLANK: 3145906 Matrix: Solid
Associated Lab Samples: 92519208001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/kg ND 4.0 01/30/21 01:39
LABORATORY CONTROL SAMPLE: 3145907
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/kg 25 25.4 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3145908 3145909
MS MSD
92519208001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, NO2 plus NO3 mg/kg ND 27.3 27.3 28.6 28.8 97 98 90-110 1 10
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 02/11/2021 06:37 PM
REPORT OF LABORATORY ANALYSIS
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®
QUALITY CONTROL DATA
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
QC Batch: 596623 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92519208001
METHOD BLANK: 3146351 Matrix: Solid
Associated Lab Samples: 92519208001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 1.0 02/02/21 12:38
LABORATORY CONTROL SAMPLE: 3146352
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 50 48.3 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3146353 3146354
MS MSD
92518457001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Phosphorus mg/kg 122 90.3 85.4 182 178 66 66 90-110 2 10 M1
Results presented on thls page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 02/11/2021 06:37 PM
REPORT OF LABORATORY ANALYSIS
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QUALIFIERS
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC -Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte Is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
Date: 02/11/2021 06:37 PM
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: BioSolids-Quarterly 1/28/21
Pace Project No.: 92519208
Pace Analytical Services, LLC
106 Short St.
Kernersville, NC 27284
336-996-2841
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92519208001 Biosolids EPA 3050B 598898 EPA 6010D 598934
92519208001 Biosolids EPA 6010D 599381
92519208001 Biosolids EPA7471B 596646 EPA7471B 596716
92519208001 Biosolids SM 2540G-2011 597274
92519208001 Biosolids SW-846 597006
92519208001 Biosolids EPA 9045D 598260
92519208001 Biosolids None 599447
92519208001 Biosolids EPA 350.1 Rev 2.0 1993 597648 EPA 350.1 Rev 2.0 1993 597672
Mod. Mod,
92519208001 Biosolids EPA 351.2 Rev 2.0 1993 596992 EPA 351.2 Rev 2.0 1993 597511
92519208001 Biosolids EPA 353.2 Rev 2.0 1993 596474 EPA 353.2 Rev 2.0 1993 596476
92519208001 Biosolids EPA 365.1 Rev 2.0 1993 596623 EPA 365.1 Rev 2.0 1993 596896
Date: 02/11/2021 06:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 18

Section A
Required Client! Information:
Company:
Address
Email To:
Phone:
Town. of Boone WWTP
PO Drawer 192
Bgone, NC 28607
karen_reace(8Mownofboone: ne
828/268-6270
Requested Due Date
Fax
828/268-6279
Section 13'
Required Project Information:
Report To:
CHAIN -OP -CUSTODY 1 Analytical Request Documen
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be complete:
Section C
Invoice Information:
mike everette(a�townofboone.net
Copy To: rude.broschinski/Mtownofbdone.ne
Purchase Order
Protect Name: Biosolida-Quarterly
Protect Number.
Atienllon
Rudy Broschinski
ompany Name:
Address.
Pace Quota:
Town of Boone VWUT.P
rudy. broschinskl(attownofboone.net
Pace Project Manager
Pace Ptogle
12890
Stephanie Knott
.lal.t:! 1
Re Ire
gt
RegutaYtiSYA98pcyi
NC DEQ-Division of Water Resources
tili:�l. 6 14 � ;tent I �tl
ed Ana yslsj Filtered y1
181110.
North Carolina I W000132E3
i
I MATRIX cone
MATRIX CODE (sae valid cades"tu lefl) I
SAMPLE TYPE (G=GRAB C=COMP)
COLLECTED
SAMPLE TEMP AT COLLECTION
!G+ry
Preservatives jr{;
NH3-N (EPA 350,1), TKN (EPA
351,2), NO3-NO2 (EPA353.2)
-
Tatal Phosphorus (EPA 365.1)
o ,.
Aluminum, Arsenic, Cadmium,
Calcium, Copper, Lead; Magnesium,
Molybdenum, Nickel, Pbtaslum,
SeleNum, Sodium, Zinc (EPA EOIOD)
SodiumAbsorplion Rale (SAR)
calculation
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2

(9aceAnalytical
www.pacelabs.com
April 26, 2021
Karen Reece
Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
RE: Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Dear Karen Reece:
Enclosed are the analytical results for sample(s) received by the laboratory on April 08, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
704-977-0981
Project Manager
Enclosures
cc: Rudy Broschinski, Town of Boone
Mike Everett, Town of Boone
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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CERTIFICATIONS
Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE SUMMARY
Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Lab ID Sample ID Matrix Date Collected Date Received
92532146001 Bio Solids
Solid 04/08/21 07:45 04/08/21 15:10
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92532146001 Bio Solids
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
EPA 6010D KQ, SH1 13 PASI-A
EPA 6010D RDT 1 PASI-A
EPA 7471 B SOO 1 PASI-A
SM 2540G-2011 KDF 1 PASI-C
SW-846 KDF 1 PASI-C
EPA 9045D SMK 1 PASI-A
None EWS 1 PASI-A
TKN+NO3+NO2 Calculation EWS 1 PASI-A
EPA 350.1 Rev 2.0 1993 Mod. NAL 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 CJL 3 PASI-A
EPA 365.1 Rev 2.0 1993 KDF1 1 PASI-A
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Sample: Bio Solids Lab ID: 92532146001 Collected: 04/08/21 07:45 Received: 04/08/21 15:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050E
Pace Analytical Services - Asheville
Aluminum 16200 mg/kg 41.1 5 04/13/21 15:33 04/15/21 11:44 7429-90-5
Arsenic ND mg/kg 2.1 1 04/13/21 15:33 04/15/21 11:47 7440-38-2
Cadmium 1.4 mg/kg 0.082 1 04/13/21 15:33 04/15/21 11:47 7440-43-9
Calcium 16200 mg/kg 103 5 04/13/21 15:33 04/16/21 00:31 7440-70-2
Copper 379 mg/kg 4.1 1 04/13/21 15:33 04/15/21 11:47 7440-50-8
Lead 12.9 mg/kg 0.82 1 04/13/21 15:33 04/15/21 11:47 7439-92-1
Magnesium 2330 mg/kg 8.2 1 04/13/21 15:33 04/15/21 11:47 7439-95-4
Molybdenum ND mg/kg 4.1 1 04/13/21 15:33 04/15/21 11:47 7439-98-7
Nickel 13.0 mg/kg 0.41 1 04/13/21 15:33 04/15/21 11:47 7440-02-0
Potassium 3890 mg/kg 411 1 04/13/21 15:33 04/14/21 16:11 7440-09-7
Selenium 6.3 mg/kg 0.82 1 04/13/21 15:33 04/15/21 11:47 7782-49-2
Sodium 1390 mg/kg 411 1 04/13/21 15:33 04/14/21 16:11 7440-23-5
Zinc 700 mg/kg 0.82 1 04/13/21 15:33 04/15/21 11:47 7440-66-6
Sodium Adsorption Ratio, SAR
Sodium Adsorption Ratio
7471 Mercury
Mercury
2540G Total Percent Solids
Analytical Method: EPA 6010D
Pace Analytical Services - Asheville
2.8 meq/L 1 04/22/21 14:04 N2
Analytical Method: EPA7471B Preparation Method: EPA7471B
Pace Analytical Services - Asheville
0.23 mg/kg 0.016 5 04/12/21 16:08 04/13/21 12:42 7439-97-6
Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids 90.8
Percent Moisture Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture 9.2
9045 pH Soil Analytical Method: EPA 9045D
Pace Analytical Services -Asheville
5.8 Std. Units 0.10 1
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
Total Nitrogen Calculation
Nitrogen
Date: 04/26/2021 03:41 PM
0.10 1
0.10 1
Analytical Method: None
Pace Analytical Services - Asheville
16200 mg/kg
Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services -Asheville
53400 mg/kg
1
40.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
04/09/21 18:18
04/09/21 18:06
04/19/21 16:08
04/21/21 15:26
04/21/21 14:54 7727-37-9
N2
H3
N2
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Project: Town of Boone WWTP
Pace Project No.: 92532146
Sample: Bio Solids Lab ID: 92532146001 Collected: 04/08/21 07:45 Received: 04/08/21 15:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
Date: 04/26/2021 03:41 PM
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod, Preparation Method: EPA 350,1 Rev 2.0 1993 Mod.
Pace Analytical Services -Asheville
884 mg/kg 10.4 1 04/13/21 10:08 04/13/21 15:42 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351,2 Rev 2.0 1993
Pace Analytical Services - Asheville
53400 mg/kg
2750 50 04/19/21 19:27 04/21/21 01:33 7727-37-9 M6
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2,0 1993
Pace Analytical Services -Asheville
ND
ND
ND
mg/kg
mg/kg
mg/kg
4.2
4.2
4.2
04/09/21 22:10 04/09/21 23:45
04/09/21 22:10 04/09/21 23:45 14797-55-8
04/09/21 22:10 04/09/21 23:45 14797-65-0
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
15800 mg/kg
270 250 04/13/21 14:50 04/14/21 10:04 7723-14-0
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 613073 Analysis Method: EPA 74718
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92532146001
METHOD BLANK: 3226862 Matrix: Solid
Associated Lab Samples: 92532146001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 04/13/21 12:18
LABORATORY CONTROL SAMPLE: 3226863
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0.085 102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3226864 3226865
MS MSD
92532508004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec %a Rec Limits RPD RPD Qual
Mercury mg/kg ND 0.027 0.027 0.024 0.026 90 98 75-125 8 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 04/26/2021 03:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
aceAnalytical
www.pacelabs.eom
QUALITY CONTROL DATA
Project: Town of Boone WWTP
Pace Project No.: 92532146
QC Batch: 613332 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050E Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92532146001
METHOD BLANK: 3228032 Matrix: Solid
Associated Lab Samples: 92532146001
Parameter
Blank Reporting
Units Result Limit Analyzed Qualifiers
Aluminum mg/kg ND 10.0 04/14/21 14:50
Arsenic mg/kg ND 2.5 04/14/21 14:50
Cadmium mg/kg ND 0.10 04/14/21 14:50
Calcium mg/kg ND 25.0 04/14/21 14:50
Copper mg/kg ND 5.0 04/14/21 14:50
Lead mg/kg ND 1.0 04/14/21 16:04
Magnesium mg/kg ND 10.0 04/14/21 14:50
Molybdenum mg/kg ND 5.0 04/14/21 14:50
Nickel mg/kg ND 0.50 04/14/21 14:50
Potassium mg/kg ND 500 04/14/21 14:50
Selenium mg/kg ND 1.0 04/14/21 14:50
Sodium mg/kg ND 500 04/14/21 14:50
Zinc mg/kg ND 1.0 04/14/21 16:04
LABORATORY CONTROL SAMPLE: 3228033
Parameter
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
Aluminum mg/kg 500 507 101 80-120
Arsenic mg/kg 50 45.3 91 80-120
Cadmium mg/kg 50 46.1 92 80-120
Calcium mg/kg 500 460 92 80-120
Copper mg/kg 50 49.4 99 80-120
Lead mg/kg 50 46.5 93 80-120
Magnesium mg/kg 500 451 90 80-120
Molybdenum mg/kg 50 50.4 101 80-120
Nickel mg/kg 50 47.2 94 80-120
Potassium mg/kg 500 ND 95 80-120
Selenium mg/kg 50 43.5 87 80-120
Sodium mg/kg 500 487J 97 80-120
Zinc mg/kg 50 43.8 88 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3228034 3228035
MS MSD
92530242001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Aluminum mg/kg 800 819 844 2240 3870 176 363 75-125 53 20 M1,R1
Arsenic mg/kg ND 81.9 84.4 72.1 77.4 87 91 75-125 7 20
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 04/26/2021 03:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 20

aceAnalytical
wuw.pecalWf<om
www.pacelabs,cam
QUALITY CONTROL DATA
Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3228034 3228035
MS MSD
92530242001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Cadmium mglkg ND 81.9 84.4 74.0 78.5 90 93 75-125 6 20
Calcium mg/kg 4380 819 844 8900 8840 552 528 75-125 1 20 M1
Copper mglkg ND 81.9 84.4 84.4 88.9 101 103 75-125 5 20
Lead mglkg ND 81.9 84.4 76.0 79.3 91 92 75-125 4 20
Magnesium mglkg 531 819 844 1290 1410 93 104 75-125 9 20
Molybdenum mg/kg ND 81.9 84.4 80.9 84.1 99 99 75-125 4 20
Nickel mg/kg ND 81.9 84.4 76.1 81.2 92 95 75-125 6 20
Potassium mglkg 1640 819 844 2560 2800 112 137 75-125 9 20 M1
Selenium mg/kg 3.0 81.9 84.4 73.9 78.1 87 89 75-125 6 20
Sodium mg/kg ND 819 844 845 905 98 102 75-125 7 20
Zinc mg/kg 11.5 81.9 84.4 84.3 90.2 89 93 75-125 7 20
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 04/26/2021 03:41 PM
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
www.pacetabs.cam
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QUALITY CONTROL DATA
Project: Town of Boone WWTP
Pace Project No.: 92532146
QC Batch: 612845 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92532146001
SAMPLE DUPLICATE: 3226086
92532342001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 84.0 84.8 1 25 N2
SAMPLE DUPLICATE: 3226087
92532465006 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture
%
11.6 10.9 6 25 N2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 04/26/2021 03:41 PM
REPORT OF LABORATORY ANALYSIS
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Page 10 of 20

4eAnaIyticaI
wweo.�n,ea.� www.pacelabs,com
QUALITY CONTROL DATA
Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 614500 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92532146001
SAMPLE DUPLICATE: 3234044
92531556001 Dup
Parameter Units Result Result
RPD
Max
RPD
Qualifiers
pH at 25 Degrees C
Std. Units 6.9 6.8 1 10 H3
SAMPLE DUPLICATE: 3234045
92533267001 Dup
Parameter Units Result Result
RPD
Max
RPD
Qualifiers
pH at 25 Degrees C Std. Units 5.6 5.5 1 10 H3
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 04/26/2021 03:41 PM
REPORT OF LABORATORY ANALYSIS
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www.pacelabs.com
QUALITY CONTROL DATA
Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 613297
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Associated Lab Samples: 92532146001
Analysis Method: EPA 350,1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
METHOD BLANK: 3227814 Matrix: Solid
Associated Lab Samples: 92532146001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/kg ND 9.6 04/13/21 15:13
LABORATORY CONTROL SAMPLE: 3227815
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 481 480 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3227816 3227817
MS MSD
92530806001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Ammonia mg/kg 128 1670 1830 1900 2030 106 104 90-110 7 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3227818 3227819
MS MSD
92530809001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Ammonia mg/kg 197 1870 1840 2100 2040 102 100 90-110 3 10
Results presented on thls page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 04/26/2021 03:41 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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(/eAnaIYticaI
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QUALITY CONTROL DATA
Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 614299 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92532146001
METHOD BLANK: 3233082 Matrix: Solid
Associated Lab Samples: 92532146001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 04/21/21 00:59
LABORATORY CONTROL SAMPLE: 3233083
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg 1000 976 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3233084 3233085
MS MSD
92532146001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 53400 1050 1050 50300 52100 -294 -120 90-110 4 10 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3235951 3235952
MS MSD
92533265002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 1650 1390 1390 5580 4290 283 190 90-110 26 10 M1,R1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 04/26/2021 03:41 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 13 of 20

(/eAnaIYticaI
www.pacelabs,cam
QUALITY CONTROL DATA
Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 612861 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92532146001
METHOD BLANK: 3226118 Matrix: Solid
Associated Lab Samples: 92532146001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mglkg ND 4.0 04/09/21 23:30
Nitrogen, Nitrite mg/kg ND 4.0 04/09/21 23:30
Nitrogen, NO2 plus NO3 mg/kg ND 4.0 04/09/21 23:30
LABORATORY CONTROL SAMPLE: 3226119
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mglkg 15 15.0 100 90-110
Nitrogen, Nitrite mg/kg 10 9.8 98 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 24.8 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3226120 3226121
MS MSD
92532265001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Nitrate mg/kg ND 98.4 98.4 106 106 108 108 90-110 1 10
Nitrogen, Nitrite mg/kg ND 65.8 65.8 67.6 68.3 101 102 90-110 1 10
Nitrogen, NO2 plus NO3 mg/kg ND 164 164 174 174 105 105 90-110 0 10
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 04/26/2021 03:41 PM
REPORT OF LABORATORY ANALYSIS
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Page 14 of 20

(/eAnaIYticaI
www.pacelabs.com
QUALITY CONTROL DATA
Project: Town of Boone WWTP
Pace Project No.: 92532146
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 613268 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92532146001
METHOD BLANK: 3227753 Matrix: Solid
Associated Lab Samples: 92532146001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 0.93 04/14/21 09:50
LABORATORY CONTROL SAMPLE: 3227754
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 49 49.3 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3227755 3227756
MS MSD
92532211001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Phosphorus
mg/kg 2320 112 110 2370 2190 46 -121 90-110 8 10 M6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 04/26/2021 03:41 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 15 of 20

aceAnalytical
www.pacelabs.cam
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QUALIFIERS
Project: Town of Boone WWTP
Pace Project No.: 92532146
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
Date: 04/26/2021 03:41 PM
REPORT OF LABORATORY ANALYSIS
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aceAnalytical®
www.pacelabs,com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Town of Boone WWTP
Pace Project No.: 92532146
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92532146001 Bio Solids EPA 3050B 613332 EPA 6010D 613506
92532146001 Bio Solids EPA 6010D 615574
92532146001 Bio Solids EPA 7471 B 613073 EPA 7471 B 613192
92532146001 Bio Solids SM 2540G-2011 613670
92532146001 Bio Solids SW-846 612845
92532146001 Bio Solids EPA 9045D 614500
92532146001 Bio Solids None 615289
92532146001 Bio Solids TKN+NO3+NO2 615264
Calculation
92532146001 Bio Solids EPA 350.1 Rev 2.0 1993 613297 EPA 350.1 Rev 2.0 1993 613354
Mod. Mod.
92532146001 Bio Solids EPA 351.2 Rev 2.0 1993 614299 EPA 351.2 Rev 2.0 1993 615055
92532146001 Bio Solids EPA 353.2 Rev 2.0 1993 612861 EPA 353.2 Rev 2.0 1993 612863
92532146001 Bio Solids EPA 365.1 Rev 2.0 1993 613268 EPA 365.1 Rev 2.0 1993 613453
Date: 04/26/2021 03:41 PM
REPORT OF LABORATORY ANALYSIS
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Section A
tared Client information;
CHAIN -OF -CUSTODY I Analytical Request Document wp# • 92532146
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must he completed
$Required ProjectInfornmtlon: Invelcelnfonuation: 111111 1111111111111111.
-- — — 92532146
Company Town -of Boone WWTP
Report -rot ::verett_ e. ownoftmannet
Altar6xx. Rudy Broschinski _..
Address: PO Drawer 192
Copy Tcc rude.brOSChinskletownofboom" net
ComPanY Name:. Town of Boone W WTP
Boone, NC 28607
Aadre= rudv:brosohinskiraJtownotboone:net
le.itVegkittiu ZiP--- MBiv ePi -aigtAIE
Erna° To: karen.reeneetownorcoone,net
Plrthase 0rtieri3.
Pecs-Qimle:
NC DEQ-DHisJon of Water Resources
Fax
Pnorrx 82B/268-B270 J' 828/26B-6279
PrziectName; Biosolids-Quarterly
P Pr Mangor_ aStephanie Knott
i wls p "+ c_ * �W0
n - ? 4�'"r�mi1. e�'smt
Requested Diu Date:
Project Number. a_
Pace ROW #: 42893
North Cetofma 1YJQ0013263
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F 1! -__ DATE Signod: _ 1 l 1

laboratory receiving samples;
AaheviKe [] Eden
ouw5
totsitri
[l Cammerctal
tuetody Sgel present? °Yes
e
Packing Mrtertsi: 094bie Wrap ['Bubble Bags
Thermometer: 01� 0
DR gunk,,
Cooler Temp 1't): � Co ctrtm Factor: Add/Subtract ('C)
Cattier Temp Corrected ('C):
Document Name:
Conditices
Document Na ;
FCAR-0-035-itev.06
Greenwood [❑ Hurrtersvllh 0
cusps 0Ctient
Other:
Sealsfiltact? 0Yes�- ON°
Nano Other
type of tie at °Blua
Document Revised: febrvery 7, win
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IssuingAuthorky:
Pace Carvltri s amity Office
Rate&] Mechanicsv UeD
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prte/MltiihParsonExamining Contents;
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Biological Tisane Fr
°Yes °No /A
Templftouid be abaue freezing to ET
Damples out of temp criteria. Simplex onto, coolie/ pracea
tudbetun
USDA Reguteted Soil ( A, water sample)
Old samples origin -mane zone within the United Stites: CA, NY, or SC (check maps)? Old sup triellate tram a forego source (intern*UoraUy,
fir hrcludi Hawaii and Puerto Rico)? Oyes B cI
Commests/ntscrepency:.
Chain of Custody Present?
k7ra Quo
❑N/A
1.
Samples Arrevedwithin Hold Time?
C]N/A
2.
'
Start Hale Time Analysts 1472 hr.)?
��Otto
Der KJNo
ON/A
3.
M
Rush 'rum Astound lime Raquehted?
Yes
ON/A
Sufficient Volume?
__Of
la QNo
Or/A
5.
Correct Corntafners Used?
-Pace Containers WrdP
Ye/s -. Onto
1. tl IINo
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6.
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0,6 QNo
tJN/A .
7,
,
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_ pYes grre
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-includes UateirimeADIAnoiysis Matrbv
. Dies (7Na
_ _
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,--
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10.
'rep Blank Present?
Trip RtankCustody Seale Present?
Des [(No
Do CINa
1 1/A
/A'
12.
COMIMIYis/SANK! DISCREPANCY
Field Dtta!squired? DYes C1u*
Usti() of stilt containers:
WENT NOTItICATIO N /IQOCUIION
Person contacted:
Project Monger SCURF Review:
Project Manager SRF Review:
Dote/Time:
Deng
Date:
Page 19 of 20

i
Daurmeet Name:
Sam • e Condition • • 1t ttariptjtGUill
Document No,:
'Check mark tap hole of boot tf pH and/or dechlarinatian 1s • Project If
verified and within the acceptance -range for•predervation
samples.
oxitoona: VOA, Cgtfnrm, TOG dU and Grow, 0140/801.5 {water/ DOC, Wig
"eattam half of box is to list number of bottle
Y
v
a�
v
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C
Document Ukiah FearuafY 7, 2011
Pegs 1of2
IssurndAuthortcy:
Pace Carolinas QuAflgl Office
4
2•
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sample lb
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pif span neteipt
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adjusted
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tat le
Note: Whenever there Is a dhvopancy affecting North Carolina carnaltante samples, a copy of this (ern WI 1t be tsnt to the North Caronna OgeNa Cart! t c1nen Office (1.e. Page 20 of 20
Out at haid,:ncarect preserve Oa, out o temp, moon-actcontalnars. 9

(eAnaIYticaI
www.pacalabs.cam
August 11, 2021
Karen Reece
Town of Boone VVVVTP
PO Drawer 192
Boone, NC 28607
RE: Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Dear Karen Reece:
Enclosed are the analytical results for sample(s) received by the laboratory on July 15, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNUNELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
704-977-0981
Project Manager
Enclosures
cc: Rudy Broschinski, Town of Boone
Mike Everett, Town of Boone
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC,
Page 1 of 18

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CERTIFICATIONS
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersvilie, NC 27284
[phone]
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersviile, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 2 of 18

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SAMPLE SUMMARY
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Lab ID Sample ID Matrix Date Collected Date Received
92549877001 Biosolids
Solid 07/15/21 07:30 07/15/21 13:10
REPORT OF LABORATORY ANALYSIS
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to
SAMPLE ANALYTE COUNT
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersvilie, NC 27284
[phone]
Lab ID Sample ID
Method
Analytes
Analysts Reported Laboratory
92549877001 Biosolids
EPA 6010D DS 13 PASI-A
EPA 6010D RDT 1 PASI-A
EPA 7471 B SOO 1 PASI-A
SM 2540G-2011 KDF 1 PASI-C
SW-846 KDF 1 PASI-C
EPA 9045D SMK 1 PASI-A
None DMN 1 PASI-A
TKN+NO3+NO2 Calculation EWS 1 PASI-A
EPA 350,1 Rev 2.0 1993 Mod. KDF1 1 PASI-A
EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A
EPA 353.2 Rev 2.0 1993 MFO 3 PASI-A
EPA 365.1 Rev 2.0 1993 KDF1 1 PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 18

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ANALYTICAL RESULTS
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
[phone]
Project: Town of Boone
Pace Project No.: 92549877
Sample: Biosolids Lab ID: 92549877001 Collected: 07/15/21 07:30 Received: 07/15/21 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual.
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum 14300 mg/kg 39.2 5 07/25/21 15:32 07/26/21 21:54 7429-90-5
Arsenic ND mg/kg 2.0 1 07/25/21 15:32 07/26/21 18:06 7440-38-2
Cadmium 1.4 mg/kg 0.078 1 07/25/21 15:32 07/26/21 18:06 7440-43-9
Calcium 17000 mg/kg 98.1 5 07/25/21 15:32 07/26/21 21:54 7440-70-2
Copper 471 mg/kg 3.9 1 07/25/21 15:32 07/26/21 18:06 7440-50-8
Lead 15.6 mg/kg 0.78 1 07/25/21 15:32 07/26/21 18:06 7439-92-1
Magnesium 2580 mg/kg 7.8 1 07/25/21 15:32 07/26/21 18:06 7439-95-4
Molybdenum 4.2 mg/kg 3.9 1 07/25/21 15:32 07/26/21 18:06 7439-98-7
Nickel 13.8 mg/kg 0.39 1 07/25/21 15:32 07/26/21 18:06 7440-02-0
Potassium 2550 mg/kg 392 1 07/25/21 15:32 07/26/21 18:06 7440-09-7
Selenium 5.2 mg/kg 0.78 1 07/25/21 15:32 07/26/21 18:06 7782-49-2
Sodium 987 mg/kg 392 1 07/25/21 15:32 07/26/21 18:06 7440-23-5
Zinc 850 mg/kg 3.9 5 07/25/21 15:32 07/26/21 21:54 7440-66-6
Sodium Adsorption Ratio, SAR
Sodium Adsorption Ratio
Analytical Method: EPA6010D
Pace Analytical Services - Asheville
2.0 meq/L
1
07/29/21 15:50 N2
7471 Mercury Analytical Method: EPA 74718 Preparation Method: EPA 7471 B
Pace Analytical Services - Asheville
Mercury 0.27 mg/kg 0.014 5 07/19/21 14:04 07/19/21 17:40 7439-97-6
2540G Total Percent Solids Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids 91.1 % 0.10 1 07/16/21 17:32
Percent Moisture Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture 8.9 % 0.10 1 07/16/21 17:26
9045 pH Soil Analytical Method: EPA 9045D
Pace Analytical Services - Asheville
pH at 25 Degrees C 6.3 Std. Units 0.10 1 07/19/21 16:23
Plant Available Nitrogen Analytical Method: None
Pace Analytical Services - Asheville
Plant Available Nitrogen 14400 mg/kg 1 07/27/21 15:56
Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation
Pace Analytical Services - Asheville
Nitrogen 47300 mg/kg 40.0 1 07/27/21 14:26 7727-37-9
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
N2
H3
N2
Page 5 of 18

aceAnalytical®
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ANALYTICAL RESULTS
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Sample: Biosolids Lab ID: 92549877001 Collected: 07/15/21 07:30 Received: 07/15/21 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
Date: 08/11/2021 01:06 PM
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Pace Analytical Services - Asheville
1250 mg/kg 21.1 2 07/22/21 13:32 07/23/21 08:22 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services - Asheville
47300 mg/kg
Analytical Method: EPA 353.2 Rev 2.
Pace Analytical Services - Asheville
ND
ND
ND
mg/kg
mg/kg
mg/kg
Analytical Method: EPA 365.1 Rev 2
Pace Analytical Services -Asheville
15000 mg/kg
2610 50 07/26/21 21:42 07/27/21 05:58 7727-37-9
0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
4.3
4.3
4.3
07/16/21 22:34 07/17/21 00:12
07/16/21 22:34 07/17/21 00:12 14797-55-8
07/16/21 22:34 07/17/21 00:12 14797-65-0
.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
233 250 07/20/21 16:00 07/21/21 08:29 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
M1
Page 6 of 18

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QUALITY CONTROL DATA
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
[phone]
QC Batch: 634254 Analysis Method: EPA 7471 B
QC Batch Method: EPA7471B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92549877001
METHOD BLANK: 3331083 Matrix: Solid
Associated Lab Samples: 92549877001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 07/19/21 16:19
LABORATORY CONTROL SAMPLE: 3331084
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0,083 0.082 98 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3331085 3331086
MS MSD
92549407002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury mg/kg ND 0.078 0.074 0.076 0.072 97 98 75-125 5 20
Results presented on thls page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 7 of 18

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QUALITY CONTROL DATA
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 635760 Analysis Method: EPA 6010D
QC Batch Method: EPA3050B Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92549877001
METHOD BLANK: 3338402 Matrix: Solid
Associated Lab Samples: 92549877001
Parameter
Blank Reporting
Units Result • Limit Analyzed Qualifiers
Aluminum mg/kg ND 10.0 07/26/21 17:37
Arsenic mg/kg ND 2.5 07/26/21 17:37
Cadmium mg/kg ND 0.10 07/26/21 17:37
Calcium mg/kg ND 25.0 07/26/21 17:37
Copper mg/kg ND 5.0 07/26/21 17:37
Lead mg/kg ND 1.0 07/26/21 17:37
Magnesium mg/kg ND 10.0 07/26/21 17:37
Molybdenum mg/kg ND 5.0 07/26/21 17:37
Nickel mg/kg ND 0.50 07/26/21 17:37
Potassium mg/kg ND 500 07/26/21 17:37
Selenium mg/kg ND 1.0 07/26/21 17:37
Sodium mg/kg ND 500 07/26/21 17:37
Zinc mg/kg ND 1.0 07/26/21 17:37
LABORATORY CONTROL SAMPLE: 3338403
Parameter
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
Aluminum mg/kg 500 491 98 80-120
Arsenic mg/kg 50 44.5 89 80-120
Cadmium mg/kg 50 47.0 94 80-120
Calcium mg/kg 500 488 98 80-120
Copper mg/kg 50 50.2 100 80-120
Lead mg/kg 50 47.2 94 80-120
Magnesium mg/kg 500 488 98 80-120
Molybdenum mg/kg 50 51.2 102 80-120
Nickel mg/kg 50 48.7 97 80-120
Potassium mg/kg 500 ND 100 80-120
Selenium mg/kg 50 42.4 85 80-120
Sodium mg/kg 500 500 100 80-120
Zinc mg/kg 50 45.5 91 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3338404 3338405
MS MSD
92548233001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Aluminum mg/kg 840 481 492 1610 2550 161 348 75-125 45 20 M1,R1
Arsenic mg/kg ND 48.1 49.2 42.7 46.4 89 94 75-125 8 20
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 18

aceAnalytical®
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QUALITY CONTROL DATA
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3338404 3338405
MS MSD
92548233001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Cadmium mg/kg 0.17 48,1 49.2 44.5 48.0 92 97 75-125 8 20
Calcium mg/kg 7390 481 492 19800 10400 2590 606 75-125 63 20 ER,M1,
Copper mg/kg ND 48.1 49.2 53.6 54.4 105 104 75-125 2 20
Lead mg/kg 1.3 48.1 49.2 43.7 47.0 88 93 75-125 7 20
Magnesium mg/kg 730 481 492 1240 1280 105 112 75-125 4 20
Molybdenum mg/kg ND 48.1 49.2 46.8 50.7 97 102 75-125 8 20
Nickel mg/kg 2.0 48.1 49.2 44.3 49.2 88 96 75-125 10 20
Potassium mg/kg 1760 481 492 2440 2320 144 115 75-125 5 20 M1
Selenium mg/kg ND 48.1 49.2 44.3 47.2 90 94 75-125 6 20
Sodium mg/kg ND 481 492 504 500 100 97 75-125 1 20
Zinc mg/kg 17.2 48.1 49.2 81.9 63.3 135 94 75-125 26 20 M1,R1
Results presented on thls page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 634059 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92549877001
SAMPLE DUPLICATE: 3330340
92550119004 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture
14.6 13.5 8 25 N2
SAMPLE DUPLICATE: 3330341
92550095001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 3.1 3.1 1 25 N2
Results resented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result,
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersvilie, NC 27284
[phone]
QC Batch: 634133 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92549877001
SAMPLE DUPLICATE: 3330592
92548517001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
pH at 25 Degrees C Std. Units 4.9 5.9 18 10 D6,H3
SAMPLE DUPLICATE: 3330593
92548895001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
pH at 25 Degrees C Std. Units 8.4 e.4 0 10 H3
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result..
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 635148 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92549877001
METHOD BLANK: 3335044 Matrix: Solid
Associated Lab Samples: 92549877001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/kg ND 10.0 07/23/21 08:03
LABORATORY CONTROL SAMPLE: 3335045
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 446 448 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3335046 3335047
MS MSD
92550599001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Ammonia
mg/kg 70.2 435 467 503 526 100 98 90-110 5 10
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result,
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kemersville, NC 27284
[phone]
QC Batch: 635901 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92549877001
METHOD BLANK: 3339101 Matrix: Solid
Associated Lab Samples: 92549877001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 07/27/21 05:28
LABORATORY CONTROL SAMPLE: 3339102
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg 1000 966 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3339103 3339104
MS MSD
92550047001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 22400 44100 46400 65300 75800 97 115 90-110 15 10 M1,R1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 634076 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92549877001
METHOD BLANK: 3330430 Matrix: Solid
Associated Lab Samples: 92549877001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Nitrate mg/kg ND 4.0 07/17/21 00:10
Nitrogen, Nitrite mg/kg ND 4,0 07/17/21 00:10
Nitrogen, NO2 plus NO3 mg/kg ND 4.0 07/17/21 00:10
LABORATORY CONTROL SAMPLE: 3330431
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 15 15.3 102 90-110
Nitrogen, Nitrite mg/kg 10 10.3 103 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 25.6 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3330432 3330433
MS MSD
92549877001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Nitrate mg/kg ND 16.1 16,4 19.1 19.1 119 116 90-110 0 10
Nitrogen, Nitrite mg/kg ND 10.8 11 12.0 11.8 109 105 90-110 2 10
Nitrogen, NO2 plus NO3 mg/kg ND 26.9 27.3 31.1 30.9 112 109 90-110 1 10 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersvllle, NC 27284
[phone]
QC Batch: 634510
QC Batch Method: EPA 365.1 Rev 2.0 1993
Associated Lab Samples: 92549877001
Analysis Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services - Asheville
METHOD BLANK: 3332102 Matrix: Solid
Associated Lab Samples: 92549877001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 0.98 07/21/21 08:17
LABORATORY CONTROL SAMPLE: 3332103
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 50 51.0 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3332104 3332105
MS MSD
92546822001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Phosphorus
mg/kg 95.5 75.7 77.2 134 156 50 79 90-110 15 10 M1,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3332106 3332107
MS MSD
92546822002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Phosphorus mg/kg 112 54.3 69.4 98.4 157 -25 64 90-110 46 10 M1,R1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall notbe reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 18

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QUALIFIERS
Project: Town of Boone
Pace Project No.: 92549877
.a r
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
H3 - Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 18

www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Town of Boone
Pace Project No.: 92549877
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92549877001 Biosolids EPA 3050B 635760 EPA 6010D 635777
92549877001 Biosolids EPA 6010D 636888
92549877001 Biosolids EPA 7471 B 634254 EPA 7471 B 634325
92549877001 Biosolids SM 2540G-2011 638905
92549877001 Biosolids SW-846 634059
92549877001 Biosolids EPA 9045D 634133
92549877001 Biosolids None 636246
92549877001 Biosolids TKN+NO3+NO2 636206
Calculation
92549877001 Biosolids EPA 350.1 Rev 2.0 1993 635148 EPA 350.1 Rev 2.0 1993 635289
Mod. Mod.
92549877001 Biosolids EPA 351.2 Rev 2,0 1993 635901 EPA 351.2 Rev 2.0 1993 636039
92549877001 Biosolids EPA 353.2 Rev 2.0 1993 634076 EPA 353.2 Rev 2.0 1993 634078
92549877001 Biosolids EPA 365.1 Rev 2.0 1993 634510 EPA 365.1 Rev 2.0 1993 634757
Date: 08/11/2021 01:06 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 18

Section A
equlred Client Information:
Section.B
Required Project information:
CHAIN -OF -CUSTODY / Analytical Request Dacumenj!
The Cha-to-of-Custody. is:a LEGAL DOCUMEI'(T. All releventfields •must be completel
Section C
invoice Information:
am,.
25498.
Company:- Town of Boone WWTP
Report To: mike:everettel townofboone.net
Adentlon:. Rudy Broschinski
4 ` ._. ""'-----''
Address: PO Drawer 192
Copy Te; rudy.broschinskii townofbo0ne.net:
company Name: Town' -of Boone WWTP
Address: rudv.broschinskl(oltownofboone.net
M. 41 611t°nu. 9sri,iti'It:Regufatpry'ggencWi°..".w l."da!b l`.i.k,lr.:: hlN
Boone; NC 28607
EmallTT: karen.reece(6tow11ofboone.net
Purchase Order#.
Pace Quote;
NODEQDivisionofWater Resources
.11
Phone: [phone] FM 828l268-6279
PmJect Neme: Bios0llds-QUarte[1y
Pace ProJecCManager. Stephanie Knott
. e I t 1'7fjt M wlr, 1�' 1
IStillltv�aahl'�u.,r .it,) t,,,,�n, � .- Btafe'�Loca foP�it4•!,, W . wt vr�r-r d� �v'
Requested Due Date:
Protect Number '3),
Pace Prafile#: 12890
North Carolina f WQ0013263
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SIGNATURE ofSAMPLER: r P
DATE Signed: '7 . )5._a,
CO

aceAnalyttical
www.pacelahs,com
November 10, 2021
Karen Reece
Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
RE: Project: Town of Boone-Biosolids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Dear Karen Reece:
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
704-977-0981
Project Manager
Enclosures
cc: Rudy Broschinski, Town of Boone
Mike Everett, Town of Boone
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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CERTIFICATIONS
Project: Town of Boone-Biosoiids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersvllle, NC 27284
[phone]
Pace Analytical Services Charlotte
9800 KinceyAve. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE SUMMARY
Project: Town of Boone-Biosolids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersvllle, NC 27284
[phone]
Lab ID Sample ID Matrix Date Collected Date Received
92568117001 Biosolids
Solid 10/21/21 08:00 10/21/21 13:30
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: Town of Boone-Biosolids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92568117001 Biosolids
PASI-A = Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
EPA 6010D DS, RDT 13 PASI-A
EPA 6010D RDT 1 PASI-A
EPA 7471 B DBB1 1 PASI-A
SM 2540G-2011 KDF 1 PASI-C
SW-846 KDF 1 PASI-C
EPA9045D ASB 1 PASI-A
None DMN 1 PASI-A
EPA365.1 Rev 2.01993 MDW 1 PASI-A
SM 4500-CN-E-2011 DMN 1 PASI-A
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Project: Town of Boone-Biosolids
Pace Project No.: 92568117
Sample: Biosolids Lab ID: 92568117001 Collected: 10/21/21 08:00 Received: 10/21/21 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
Aluminum 15000 mg/kg 45.6 5 10/26/21 12:44 11/03/21 13:03 7429-90-5
Arsenic ND mg/kg 2.3 1 10/26/21 12:44 11/02/21 18:07 7440-38-2
Cadmium 1.5 mg/kg 0.091 1 10/26/21 12:44 11/02/21 18:07 7440-43-9
Calcium 21200 mg/kg 114 5 10/26/21 12:44 11/03/21 13:03 7440-70-2
Copper 503 mg/kg 4.6 1 10/26/21 12:44 11/02/21 18:07 7440-50-8
Lead 16.2 mg/kg 0.91 1 10/26/21 12:44 11/02/21 18:07 7439-92-1
Magnesium
2430 mg/kg 9.1 1 10/26/21 12:44 11/02/21 18:07 7439-95-4
Molybdenum 4.6 mg/kg 4.6 1 10/26/21 12:44 11/02/21 18:07 7439-98-7
Nickel 13.6 mg/kg 0.46 1 10/26/21 12:44 11/02/21 18:07 7440-02-0
Potassium 2530 mg/kg 456 1 10/26/21 12:44 11/02/21 18:07 7440-09-7
Selenium 4.6 mg/kg 0.91 1 10/26/21 12:44 11/02/21 18:07 7782-49-2
Sodium 1000 mg/kg 456 1 10/26/21 12:44 11/02/21 18:07 7440-23-5
Zinc 848 mg/kg 0.91 1 10/26/21 12:44 11/02/21 18:07 7440-66-6
Sodium Adsorption Ratio, SAR
Sodium Adsorption Ratio
Analytical Method: EPA 6010D
Pace Analytical Services - Asheville
1.8 meq/L
1
7471 Mercury Analytical Method: EPA 74718 Preparation Method: EPA 7471 B
Pace Analytical Services - Asheville
0.45 mg/kg
Mercury
11/05/21 08:19 N2
0.035 10 10/28/21 10:20 11 /01 /21 14:22 7439-97-6
2540G Total Percent Solids Analytical Method: SM 2540G-2011
Pace Analytical Services - Charlotte
Total Solids 91.4 % 0.10 1 10/22/21 14:09
Percent Moisture Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture 8.6 % 0.10 1 10/22/21 13:59
9045 pH Soil Analytical Method: EPA9045D
Pace Analytical Services -Asheville
pH at 25 Degrees C 6.4 Std. Units 0.10 1 11/03/21 19:02
Plant Available Nitrogen Analytical Method: None
Pace Analytical Services -Asheville
Plant Available Nitrogen 17300 mg/kg 1
365.1 Phosphorus, Total
Phosphorus
Date: 11/10/2021 08:14 AM
N2
H3
11/09/21 17:47 N2
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
16300 mg/kg
268 250 10/28/21 00:38 10/28/21 15:41 7723-14-0
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Town of Boone-Biosolids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersvllle, NC 27284
[phone]
Sample: Biosolids Lab ID: 92568117001 Collected: 10/21/21 08:00 Received: 10/21/21 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500CNE Cyanide, Total
Cyanide
Date: 11/10/2021 08:14 AM
Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011
Pace Analytical Services -Asheville
ND mg/kg
1.4 5 11/02/21 11:15 11/03/21 16:12 57-12-5 D3,M1
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Town of Boone-Biosolids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 655813 Analysis Method: EPA 74718
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92568117001
METHOD BLANK: 3438115 Matrix: Solid
Associated Lab Samples: 92568117001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0036 11/01/21 13:16
LABORATORY CONTROL SAMPLE: 3438116
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.05 0.051 102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3438117 3438118
MS MSD
92567625001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury mg/kg ND 0.044 0.043 0.034 0.035 75 79 75-125 3 20
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 11/10/2021 08:14 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Town of Boone-Biosolids
Pace Protect No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 654864 Analysis Method: EPA 6010D
QC Batch Method: EPA3050B Analysis Description: 6010 MET
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92568117001
METHOD BLANK: 3433902 Matrix: Solid
Associated Lab Samples: 92568117001
Parameter
Blank Reporting
Units Result Limit Analyzed Qualifiers
Aluminum mg/kg ND 10.0 11/02/21 16:51
Arsenic mg/kg ND 2.5 11/02/21 16:51
Cadmium mg/kg ND 0.10 11/02/21 16:51
Calcium mg/kg ND 25.0 11/02/21 16:51
Copper mg/kg ND 5.0 11/02/21 16:51
Lead mg/kg ND 1.0 11/02/21 16:51
Magnesium mg/kg ND 10.0 11/02/21 16:51
Molybdenum mg/kg ND 5.0 11/02/21 16:51
Nickel mg/kg ND 0.50 11/02/21 16:51
Potassium mg/kg ND 500 11/02/21 16:51
Selenium mg/kg ND 1.0 11/02/21 16:51
Sodium mg/kg ND 500 11/02/21 16:51
Zinc mg/kg ND 1.0 11/02/21 16:51
LABORATORY CONTROL SAMPLE: 3433903
Parameter
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
Aluminum mg/kg 500 500 100 80-120
Arsenic mg/kg 50 47.0 94 80-120
Cadmium mg/kg 50 47.0 94 80-120
Calcium mg/kg 500 483 97 80-120
Copper mg/kg 50 51.3 103 80-120
Lead mg/kg 50 48.2 96 80-120
Magnesium mg/kg 500 483 97 80-120
Molybdenum mg/kg 50 52.1 104 80-120
Nickel mg/kg 50 48.8 98 80-120
Potassium mg/kg 500 502 100 80-120
Selenium mg/kg 50 42.6 85 80-120
Sodium mg/kg 500 496J 99 80-120
Zinc mg/kg 50 46.9 94 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3433904 3433905
MS MSD
35671696013 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Aluminum mg/kg 1400 373 373 3100 3240 455 493 75-125 4 20 M1
Arsenic mg/kg 9,9 37,3 37,3 45,4 46.3 95 97 75-125 2 20
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 11/10/2021 08:14 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Protect: Town of Boone-Biosolids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3433904 3433905
MS MSD
35671696013 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qua!
Cadmium mg/kg 0.23 37.3 37.3 35.4 36.2 94 96 75-125 2 20
Calcium mg/kg 43600 373 373 36800 36400 -1830 -1930 75-125 1 20 E,M1
Copper mg/kg 5.2 37.3 37.3 43.0 44.5 101 105 75-125 3 20
Lead mg/kg 4.7 37.3 37.3 37.7 39.0 88 92 75-125 3 20
Magnesium mg/kg 222 373 373 729 617 136 106 75-125 17 20 M1
Molybdenum mg/kg 0.19U 37.3 37.3 36.9 37.7 99 101 75-125 2 20
Nickel mg/kg 1.1 37.3 37.3 34.8 35.8 90 93 75-125 3 20
Potassium mg/kg 379U 373 373 446 469 106 113 75-125 5 20
Selenium mg/kg 0.55J 37.3 37.3 32.7 33.4 86 88 75-125 2 20
Sodium mg/kg 189U 373 373 487 508 89 94 75-125 4 20
Zinc mg/kg 12.4 37.3 37.3 43.2 46.9 83 92 75-125 8 20
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 11/10/2021 08:14 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Town of Boone-Biosolids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 654493 Analysis Method: SW-846
QC Batch Method: SW-846 Analysis Description: Dry Weight/Percent Moisture
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92568117001
SAMPLE DUPLICATE: 3431947
92568202004 Dup
Parameter Units Result Result
RPD
Max
RPD Qualifiers
Percent Moisture
OA
13.4 14.1 5 25 N2
SAMPLE DUPLICATE: 3433207
92568121001 Dup
Parameter Units Result Result
RPD
Max
RPD Qualifiers
Percent Moisture % 11.5 11.4 1 25 N2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 11/10/2021 08:14 AM
REPORT OF LABORATORY ANALYSIS
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e
QUALITY CONTROL DATA
Project: Town of Boone-Biosolids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 657195 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92568117001
SAMPLE DUPLICATE: 3444812
92568849001 Dup
Parameter Units Result Result
RPD
Max
RPD
Qualifiers
pH at 25 Degrees C Std. Units 12.4 12.4 0 10 E,H3
SAMPLE DUPLICATE: 3444813
92570116001 Dup
Parameter Units Result Result
RPD
Max
RPD
Qualifiers
pH at 25 Degrees C Std. Units
5.6 5.6 0 10 H3
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 11/10/2021 08:14 AM
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Town of Boone-Biosollds
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 655706 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92568117001
METHOD BLANK: 3437598 Matrix: Solid
Associated Lab Samples: 92568117001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 0.96 10/28/21 15:35
LABORATORY CONTROL SAMPLE: 3437599
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 48.1 48.8 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3437600 3437601
MS MSD
92565408001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec ,% Rec Limits RPD RPD Qual
Phosphorus
mg/kg 85,6 69.6 69.6 209 169 177 120 90-110 21 10 M1,R1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
Date: 11/10/2021 08:14 AM
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Town of Boone-Biosolids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
QC Batch: 656581 Analysis Method: SM 4500-CN-E-2011
QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 4500CNE Cyanide, Total
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92568117001
METHOD BLANK: 3441911 Matrix: Solid
Associated Lab Samples: 92568117001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide mg/kg ND 0.30 11/03/21 16:00
LABORATORY CONTROL SAMPLE: 3441912
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Cyanide mg/kg 2.6 2.6 101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3441913 3441914
MS MSD
92568117001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Cyanide mg/kg ND 2.5 3 1.4 ND 31 2 80-120 10 D3,M1
Results presented on this page are In the units Indicated by the"Units" column except where an alternate unit Is presented to the right of the result.
Date: 11/10/2021 08:14 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 33

(eAnaIY1IcaI
www.pacelabs,cam
QUALIFIERS
Project: Town of Boone-Biosolids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte Is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable,
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected,
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
E Analyte concentration exceeded the calibration range. The reported result Is estimated,
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditatlons/certifications is available upon request.
R1 RPD value was outside control limits.
Date: 11/10/2021 08:14 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Town of Boone-Biosolids
Pace Project No.: 92568117
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Lab ID
Sample ID QC Batch Method
Analytical
QC Batch Analytical Method Batch
92568117001 Biosolids EPA 3050E 654864 EPA 6010D 655360
92568117001 Biosolids EPA 6010D 657765
92568117001 Biosolids EPA7471B 655813 EPA7471B 656153
92568117001 Biosolids SM 2540G-2011 655296
92568117001 Biosolids SW-846 654493
92568117001 Biosolids EPA 9045D 657195
92568117001 Biosolids None 658618
92568117001 Biosolids EPA 365.1 Rev 2.0 1993 655706 EPA 365.1 Rev 2.0 1993 655991
92568117001 Biosolids SM 4500-CN-E-2011 656581 SM 4500-CN-E-2011 656875
Date: 11/10/2021 08:14 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 33

Section A
Required' Client Information:
Company: Town of Boone.WWTP
Address -
PO Drawer 192
CHAIN -OF -CUSTODY / Analytical Request:Do
The •Chain -of -Custody is -a LEGAL DOCUMENT_ All relevant fields must I
Section a
Required Protect Information:
Report To: mike.everette • townofhoone ,et
Copy To; rude:[e-mail]
Boone. NC 28607
EmallTo: keren.reecetownofboone.net
Phone:
828/268-6270
Fax [phone]
Requested Due Dale::
Purchase.Order*
Project Name: Biosolid
Project Number. # f,.{
SAMPLE ID
Sample Ids must be unique
MATRIX CODE
Drinking Wm* Ow
w•t•, WT
Waste Water ww
Product P
a (ISolld eL
011 OL
Wipe wP
Atr. AR
Other or
7L�ua TS
SAMPLE TYPE (.=GRAB GCOMPj
ST
DAT
11i
o$oLiD5
SL
G
n
ItaVoC
III
-D
01
CD
0
W
W
Section C
Invoice information:
Attention:: Rud Broschlnski.
Company Name: Town, of Boone W WTP
WOt{ : 92566117
1
Address: rudy.broschinski(Wtownofboone.net
i544111iLviuLht tejl rtW. ; (IPAftiiiiii t6ti-aitiiai IIIl,iiFi 11 I j,r;, : ti.:.��
Pace Quota:
NC DEQ-Division of Water Resources
f-Quarted y
YP
Pace Project Manager Stephanie Knott
(I �� II 1-111n 1 li r 1. n rr ,J, lr'ra I1t' 1 to '
15 t„1, . ._rt.taw-�r ItlBtgtehLoc�tivNl�l�11;1 G+n +.rl�ull,u i,�i
Pace Profile.#: 12890
North Carolina / WQOO13263
ll/P^;t1d!1I(11u111'.RRqueatgt1A/1fly+t8'Fit4fR
i/i'N0N8�A1101.,
3 u+nt
V r-1
1tt iilI;pIInn
4
COLLECTED
SAMPLE TEMP AT COLLECTION
Preservatives
11'
11lj11
NH3-N (EPA 350.1), TM (EPA
3512), NO3-NO2 (EPA3532)
z
Total Phosph,ni (EPA 365,1)
Percent Total Solids (EM 2540G)
Aluminum, Arsenic, Cadmium,
Calcium, Copper, Lead, Magnesium,
Molybdenum, Nickel, Potassium,
Selenium, Sodium, Zinc (EPA 60100)
Sodium Absorp000 Rate (SAR)
calculation
Mercury (EPA 747 lie)
1g
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g Z

ace Analytical®
Report of Analysis
Pace Analytical LLC
1377 South Park Drive
Kernersville, NC 27284
Attention: Stephanie Knott
Project Name: Town of Boone-Biosolids
Project Number: 92568117
Lot Number:WJ24006
Date Completed:11 /07/2021
,fr----7}-7--
11 /09/2021 3:31 PM
Approved and released by:
Project Manager I: Blaire M. Gagne
ARAB
ANSI NationalAareditallon Baud
ACCREDITED
-1111=0011---
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel: [phone] Fax: [phone] www.pacelabs.com
Page 17 of 33
Page 1 of 17

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653
NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Pace Analytical LLC
Lot Number: WJ24006
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation:
Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium,
Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal
Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011,
Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid
Chemical Material: TOC Walkley-Black.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report please contact the Pace Project Manager listed on the
cover page.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 18 of 33
Page 2 of 17

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Pace Analytical LLC
Lot Number: WJ24006
Project Name: Town of Boone-Biosolids
Project Number: 92568117
Sample Number Sample ID Matrix Date Sampled Date Received
001 BIOSOLIDS Solid 10/21/20210800 10/22/2021
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 19 of 33
Page 3 of 17

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Pace Analytical LLC
Lot Number: WJ24006
Project Name: Town of Boone-Biosolids
Project Number: 92568117
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 BIOSOLIDS Solid Ammonia - N (gas 350.1 1100 mg/kg 5
001 BIOSOLIDS Solid Nitrate -Nitrite - N (soluble) 353.2 2.8 mg/kg 5
001 BIOSOLIDS Solid TKN 351.2 57000 S mg/kg 5
(3 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 20 of 33
Page 4 of 17

Inorganic non-metals
Client: Pace Analytical LLC
Description: BIOSOLIDS
Date Sampled:10/21/2021 0800
Date Received:10/22/2021
Project Name: Town of Boone-Biosolids
Project Number: 92568117
Laboratory ID: WJ24006-001
Matrix: Solid
% Solids: 82.7 10/24/2021 1941
Run Prep Method
1
1
1
350.1
351.4
Analytical Method Dilution Analysis Date Analyst
(Ammonia - N ) 350.1 25 11/04/2021 2101 DRD
(Nitrate-Nitr) 353.2 1 10/30/2021 1219 AAB
(TKN) 351.2 50 10/28/2021 1330 DMA 10/27/2021 1335 20311
Prep Date
Batch
20966
20702
Parameter
Ammonia - N (gas diffusion)
Nitrate -Nitrite - N (soluble)
TKN
CAS Analytical
Number Method Result Q LOQ Units Run
350.1 1100 30 mg/kg 1
353.2 2.8 0.24 mg/kg 1
351.2 57000 S 3000 mg/kg 1
LOQ = Limit of Quantitalion
ND = Not detected at or above the LOQ
H = Out of holding time
B = Detected in the method blank
N = Recovery is out of criteria
W = Reported on wet weight basis
E = Quanfitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 21 of 33
Page 5 of 17

QC Summary
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WJ24006
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com Page 22 of 33
Page 6 of 17

Inorganic non-metals - MB
Sample ID: WQ20311-001
Batch: 20311
Analytical Method: 351.2
Matrix: Solid
Prep Method: 351.4
Prep Date: 10/27/2021 1335
Parameter Result Q Dil LOQ Units Analysis Date
TKN ND 1 50 mg/kg 10/28/2021 1258
LOQ = Limit of Quantltation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
• = RSD Is out of criteria + = RPD Is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
QC Data for Lot Number: WJ24006
Page 23 of 33
Page 7 of 17

Inorganic non-metals - LCS
Sample ID: WQ20311-002
Batch: 20311
Analytical Method: 351.2
Parameter
TKN
Matrix: Solid
Prep Method: 351.4
Prep Date: 10/27/2021 1335
Spike
Amount Result %Rec
(mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date
500 450 1 90 80-120 10/28/20211258
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
• = RSD is out of criteria + = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WJ24006
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 24 of 33
Page 8 of 17

Inorganic non-metals - MS
Sample ID: WJ24006-001MS
Batch: 20311
Analytical Method: 351.2
Parameter
TKN
Matrix: Solid
Prep Method: 351.4
Prep Date: 10/27/2021 1335
Sample Spike
Amount Amount Result %Rec
(mg/kg) (mg/kg) (mg/kg) Q DU % Rec Limit Analysis Date
57000 600 55000 N 50 -293 80-120 10/28/2021 1330
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery Is out of criteria
P = The RPD between two GC columns exceeds 40%
' = RSD Is out of criteria + = RPD Is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
QC Data for Lot Number: WJ24006
Page 25 of 33
Page 9 of 17

Inorganic non-metals - MSD
Sample ID: WJ24006-001MD
Batch: 20311
Analytical Method: 351.2
Parameter
TKN
Matrix: Solid
Prep Method: 351.4
Prep Date: 10/27/2021 1335
Sample Spike
Amount Amount Result %Rec % RPD
(mg/kg) (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
57000 600 53000 N 50 -626 3.7 80-120 20 10/28/2021 1333
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery Is out of criteria
P = The RPD between two GC columns exceeds 40%
*= RSD Is out of criteria + = RPD Is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WJ24006
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,pacelabs.com
Page 26 of 33
Page 10 of 17

Inorganic non-metals - MB
Sample ID: WQ20702-001
Batch: 20702
Analytical Method: 353.2
Parameter Result Q Dil
Nitrate -Nitrite - N (soluble) ND 1
Matrix: Solid
LOQ
0.20
Units Analysis Date
mg/kg 10/30/20211209
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
* = RSD is out of criteria + = RPD Is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
QC Data for Lot Number: WJ24006
Page 27 of 33
Page 11 of 17

Inorganic non-metals - LCS
Sample ID: WQ20702-002
Batch: 20702
Analytical Method: 353.2
Parameter
Nitrate -Nitrite - N (soluble)
Matrix: Solid
Spike
Amount Result
(mg/kg) (mg/kg) Q Dil
0.80 0.85 1
% Rec
106
%Rec
Limit Analysis Date
90-110 10/30/2021 1211
LOQ = Limit of Quantitatlon ND = Not detected at or above the LOQ
' = RSD Is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WJ24006
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs,com
Page 28 of 33
Page 12 of 17

Inorganic non-metals - MB
Sample ID: WQ20966-001
Batch: 20966
Analytical Method: 350.1
Matrix: Solid
Prep Method: 350.1
Parameter Result Q Dil LOQ Units Analysis Date
Ammonia - N (gas diffusion) ND 1 1.0 mg/kg 11/04/2021 2003
LOQ = Limit of Quantitatlon ND = Not detected at or above the LOQ N = Recovery Is out of criteria
P = The RPD between two GC columns exceeds 40%
= RSD Is out of criteria + = RPD Is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WJ24006
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 33
Page 13 of 17

Inorganic non-metals - MB
Sample ID: WQ20966-001
Batch: 20966
Analytical Method: 350.1
Parameter
Ammonia - NI (gas diffusion)
Matrix: Solid
Prep Method: 350.1
Result Q Dil LOQ Units Analysis Date
ND 1 1.0 mg/kg 11/04/20212003
LOQ = Limit of Quantitation ND = Not detected at or above the LOQ
* = RSD Is out of criteria
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
+ = RPD Is out of criteria
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) QC Data for Lot Number: WJ24006
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 29 of 33
Page 13 of 17

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 31 of 33
Page 15 of 17

aternal Transfer Chain of Custody
1111011111111111
Markorder. e256S117
tepariie Knctt
aceAitalytical itemsrsv!i:a
377 Scut Park Drive.
:erhersvrpe, NC 27284-
!tole 7-34-977-0981
S mplos Pt A-49ged irLt:eC C.
Wcrkorder Name. Town of L none-Rfost lid s
%811kcanura..c 4,4 t r"w a ,. 9.; „t:.
State Of Origin:.NC;:
Cert. Needed: F— Yes
Owner ReaeM d Date
CeAnNYtiCat
Wire epiicrt■hs.cam
M©
10121/2021:.Results Fig ucsted By; 11bit2021
Pactnn Iytit; :.WatsLGritKrilxia
1061ia tale rdrit Ctsivrx
• .VWSt.. Columbia, Sc: 29172
Phone (pC13)791-9700
:era
:strigg
Bkix5ds:
P&-
1 Ol21+'2021:047. 7
2,SSet17001
rlNtft
Solid
0
10211I
W.1240D6
ems:
tf+ 3 U3i OBI LY
Transfers
2
3
ued By
Coder Tern pendure on Receipt
'In order:ir maintain •diem` c nrdetrfiality'location/ time or -the: sampling sl:e,sampler's .n8me and signahrre.may not be provided OP this COC docurnerJ
This chain of custody Is considered complete es is since farnret na aves e rn he:oi rrerlebor 1crY
DateTnie
acei+te5U31
Date, mlma
Gusted Seal : = or N Received en Ice Yj or N
Thursday, OU[ber.21 20Z1.2:'3:3S PM
Sa>lnples Intact
MITALL-c-oeirem0a2411arcCS Papa 1 of 1
PACE ANALYTICAL SERVICES, LLC
................_.

PACE ANALYTICAL SERVICES, LLC
r�:.�ir>alyZ,ieal
5arnpis Receipt Cdnrxi itst (SRO (M1 001aC-15)
Issuing Atithoriry: Pace ENV - vx.r t
Sample Receipt Clhceklist (SRC)
✓.4.,:a, l::DRW 1 L0'241'2021
Lot l!: U1:246116
R[:tttS0d19/29/202L
Page lef3.
t'lhi : ,n-o %.VVIY, m..1pw“-.-.,...,.,,,-..
Mort ()free i : • Puce *►I.�r` ,/ Fcdl?x Other:
liallal
J
1Vo
1. Were custody sev,Is rent on the cooler'?
2. IC custody seals were /resent, were the , intact and unbroken'
IMO
Not©iimo
NA Chlorineirp ID: Tested bar: rtti
pH Ship ID. _ _
214928
` temperature upon receipt %Solid Snap -Cup ID:
Original temperature upon recaipt1 Derive (Corrected)
4.9 "4.9 °C NA jN. ht;; NA fNA cc NA iNA .-:`'}C
OTetu Blank [ Jkgaittst 1 titrleg lit Gun ID: S 1( [;un Correction Factor. ''O
Muihixi; ,ela1�ure
El Wet tee l }cc Pa_oic.4 Dri Ice [1 None
Nettled
0 Yes
of coe[ant:
r
El No
✓ NA
rJ t
3. If teir perntltte of any cooler exceed i 6.G°t„ was Project Manager Notified?
PM.wt75 Notified by: phone I email / face -try -,face (circle one).
161 ea
!
• I•t15
4. Is the rammercial colirler'R Isxckintr Milt titlsuitiail trt this fiottn7
® Ycs. LJ too
. jt�t`4r4 proper eusrady procedures (relinRuish "rer t ivud) fstlltn�ted? .
Cj
e ,
No
, byere > mr 1e ID listed on the COC7
❑,f Ycs
Na
7. Wir4 dtrt?1e Ii s )Iyte4 on �3t1 ample cOnttt¢ters?
Yes
Syr,
�, �N catlectien date time tasted on thet('C+
y
� No
9. 1V s co[Iect m elate & limo listed do till samplo tttt3rt4L1ter ?
J ye
j "No
IQ, pid ail container label inform tion (If), chic; Curti:) agree c4irh the COC7
E71 Yes
No
I I. t4`ere testa to be perfarmcd [;sled on the Ct 1C? . _
Ycs
Na
12, D d al I sampl a arrive in tha proper coattuiners for each test and, or in good eondhiuit
(uttlttnlcci lids on etc.}'Z
LJNo
1 i2SS:itfCQtlat491'fItj7lerttl7.1rt1e�lV{ttltt�lle�
©Ycs.
yr
L i N�
14.1'f'ere atl samp1c rx cw XI ►vtthin n the hold:ttg tliti qr 4$ hours, Kmchever come3 that?
Ye
fl Nc
15, ,°orP any samp[c cnn[�itters m:ie�inpjexces5 [circle one) �atr 1 des Not list �i on C UC7
El 1/0.
ONO
N.
16. For VOA and RSK i75 ,antp1ea, were bubbles present "pea -size" (r, of 6mrti in diameter)
[r arty, of the VOA vials?
yes
LJNo
[LNA
17. Were 211 lntairnteta141nutrtenl 5 imP1G3 rece'ive1 at a pII of <2?
Y; y
Li No
j i
NA
IS, Were dl cYaili e ,' amptes received at a PH H > 12 aerd su[tide samples received at a pii - y?
Yes
0Ne
•t9.
QNA
We.'r all 8 lica:bte Ni-I TK, lt4 ariide hettoii625.1/6O .3 <4.5tn /L) srttr )raree of
P[� y N ( ) F
residual chloride? .--—
Yt s
0 NO
EINA_
2O, VC o t1ite❑t remarks/requests (i.e. requested dilutions; MS/Map deli ations, eto,..)
ea -ready transcribed From the COG Into the come:tent section in LBWS?
l Yes
>F. No
21. Was the note number listed on the Cdtitaittet label? If w, Quom g
Rumple
Preservation
(Must
be completed for any sample(s) Inporrectly pre:served Or %vial Iteadspaee.)
Siintple(s) A were received inconectty presanredand were adjusted accordingly
NA anL of t irtle one; 112SO4, (NO3, HC1, NaO1i using SR ii KA .
in sample rra oh'ing with
Time of preservation NA'._,, ,. If more than one preservative is needed, please note i_r the cetnnient.L below.
Samp)ci(s) NA were received with bubbles , 6 mni in diameter.
Stti:tples(s) MA ____ we r. coh"ed wttl3TRC > COniglL, (If 019 is no) and were
in with sodium thiosulfate (NaaS,O1) with Shealy ID: NA .
sniimpt : receiving
adjusted acuvdirig[y
SR bareede labels app[idt by: XDRW Dato: 1iA24 2421
Comments:
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 33 of 33
Page 17 of 17

WATER QUALITY LAB & OPERATIONS, INC.
P.D.BOX 1107
BANNER ELK, NC 28604
CLIENT: TOWN QFB0ONEVVVVTP
ADDRESS: P.O.BOX 102
CITY: BODNE
STATE: NC Z|P28O07
LOGIN TIME:
SAMPLER:
RECEIVED DATE: 18-Feb'21
REPORTED DATE: 22-Mar-21
AM
TOTAL SOLIDS
FECALCOURJRM
1
00.8
24
Y6
MPN/g
SLUDGE
SLUDGE
10Feb-21
P|
TOTAL SOLIDS
FECALCOL|FORN1
2
81.1
32
%
MPN/o
SLUDGE
SLUDGE
19-Feb-21
P|
TOTAL SOLIDS
FECALCOL|FORM
3
91.3
17
Y6
K8PN/o
SLUDGE
SLUDGE
10-Feb'21
P|
TOTAL SOLIDS
FECALCOL|FORM
4
90.0
44
Y6
MPN/g
SLUDGE
SLUDGE
10-Feb'21
Pi
TOTAL SOLIDS
FECALCDL|FORM
5
01.2
A
96
K4PN/o
SLUDGE
SLUDGE
10-Feb'21
P|
TOTAL SOLIDS
FECALCOL|FORM
6
92.3
17
Y6
K8PN/g
SLUDGE
SLUDGE
10-Feb'21
P|
TOTAL SOLIDS
FE[ALCOL|FDRM
7
91.7
27
Y6
K8PN/g
SLUDGE
SLUDGE
18-Feb-21
P|
REPORTED BY: NC CERTIFIED LAB # 544

WATER QUALITY LAB & OPERATIONS, INC.
P.O.BOX 11G7
BANNER ELK, NC28G04
CLIENT: TOWN OFBOONEVVVVTP
ADDRESS: P.O.BOX 102
CITY: BOONE
STATE: NC ZIP 28807
REPORTED DATE: 23-Apr-21
RECEIVED DATE: 15'App21
TOTAL SOLIDS
FECALCOUFORM
1
91.3
27
Y6
MPN/g
SLUDGE
SLUDGE
18'App21
P(
TOTAL SOLIDS
FECAL COL|FORM
2
00.4
17
Y6
MPN/o
SLUDGE
SLUDGE
10-Apr21
P|
TOTAL SOLIDS
FECALC{}L(F(]FlK8
3
93.2
10
Y6
K4PN/g
SLUDGE
SLUDGE
18-Apr21
Pi
TOTAL SOLIDS
FECALCOLiFOF(K4
4
03.4
27
Y6
K8PN/g
SLUDGE
SLUDGE
18+Apr-21
Pi
TOTAL SOLIDS
FECALC{}L|FORK4
5
91.2
18
Y6
K8PN/o
SLUDGE
SLUDGE
16-Apr21
P|
TOTAL SOLIDS
FECALCOL|FORK4
6
90.2
19
Y6
yWPN/o
SLUDGE
SLUDGE
10-Apr21
P|
TOTAL SOLIDS
FEC/\LCDL|F{}RKA
7
01.3
13
Y6
MPN/o
SLUDGE
SLUDGE
16`4pr-21
P|
REPORTED BY: NC CERTIFIED LAB # 544
PAUL\GENHOUR,SUPERVISOR

WATER QUALITY LAB & OPERATIONS, INC.
P.O.BOX 11O7
BANNER ELK, NC28GO4
CLIENT: TOWN QFBOONEV08TP
ADDRESS: P.O.BOX 102
CITY: 8OONE
STATE: NC Z|P28G07
RECEIVED DATE: 22-u|-21
ON
TOTAL SOLIDS
1
00.9
96
SLUDGE
26-Ju|'21
FECALCOLiF{}RN
27
K�PN/
SLUDGE
2�Jul-21
P\
TOTAL SOLIDS
2
01.3
%
SLUDGE
20Jul-21
FECALCOL\FDRM
10
��PN/o
SLUDGE
23,]u|-21
P(
TOTAL SOLIDS
3
01.8
Y6
SLUDGE
26'Ju|-21
FECALCOL|FDRyW
20
K4PN/g
SLUDGE
23'Ju\-21
P|
TOTAL SOLIDS
4
904
Y6
SLUDGE
26'Ju\-21
FECALCC)L|FORNi
32
W4PN/g
SLUDGE
23'Ju|'21
P|
TOTAL SOLIDS
5
90.1
Y6
SLUDGE
20'Ju|'21
FECALC{}LiFDRN1
43
K4PN/o
SLUDGE
23-Ju|-21
P\
TOTAL SOLIDS
8
81.7
Y6
SLUDGE
26-Ju|-21
FECALC{}L\FORK4
20
MPN/g
SLUDGE
23-Ju\-21
P|
TOTAL SOLIDS
7
01.9
Y6
SLUDGE
28-Ju|-21
FECALC{}L|FORM
17
K8PN/o
SLUDGE
23'Ju|-21
P|
REPORTED BY: NC CERTIFIED LAB # 544
PAUL|SENHOUR,SUPERVISOR

WATER QUALITY LAB & OPERATIONS, INC.
P.O.BOX 1107
BANNER ELK, NC2O8U4
CLIENT: TOWN OF BOONEVVVVTp
ADDRESS: P.D.BOX 102
CITY: B0ONE
STATE: NC ZIP 28607
REPORTED DATE: 3-Nov-21
RECEIVED DATE: 21-}ot-21
COM
TOTAL SOLIDS
FECALCOL|FURK8
1
00.9
��
%
�pN�
SLUDGE
SLUDGE
"^~~~^
___-'_�
22�)o-21
P|
TOTAL SOLIDS
FECAL(�OL|FDR�W
2
03.8
458
Y6
�WPN/g
SLUDGE
SLUDGE
22'Oot��1
p\
TOTAL SOLIDS
3
02.8
Y6
SLUDGE
FECALCOL(FDRK8
302
K4PN/g
SLUDGE
�2'Od,21
P\
TOTAL SOLIDS
4
92.3
Y6
SLUDGE
FECALCDL|FORM
184
yWPN/g
SLUDGE
22-Oct-21
P|
TOTAL SOLIDS
5
03.7
96
SLUDGE
FECALCC)L|FORK8
258
[WPN/g
SLUDGE
22'Oot�!1
P(
TOTAL SOLIDS
8
93.8
Y6
SLUDGE
FECALCOL|FORW1
373
MPN/o
SLUDGE
22'Oct-21
P|
TOTAL SOLIDS
T
01.3
Y6
SLUDGE
REPORTED BY: - NC CERTIFIED LAB # 544