WQ0032016_Monitoring - 11-2021_20211222 (2)

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DWR - NonDischarge Monitoring Report Submittal
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NORTH CAROLINA
Enrlranmenlel QHaflly
Monitoring Report Submittal
..............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................
Permit Number#* WQ0032016
Name of Facility:* Rose Hill Plantation
Month:* November Year:* 2021
Report Information
Type* Upload Document*
GW-59 Rose Hill(WQ0032016)GW- 4.32MB
59(with lab results)Nov
2021.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1,NDAR-2,NDMLR,GW-59).
Confirmation Email Address:* [e-mail]
Name of Submitter:* Kimber Reese
Signature:
Date of submittal: 12/22/2021
This will be filled in automatically
Initial Review

Reviewer: Mokashi, Poorva
Is the project number correct?* WQ0032016
Is the monitoring report accepted?* Yes No
Regional Office* Asheville
Accepted Date: 1/21/2022

CW.59A REPOR'!" FORM r)-7)
Peril it ht )
(Submit 2m,each monitoring period with('IE-59forms.)
1 Enter date monitoring results were due.( ) Will this monitoring report(GW-59 and GW-59A) YES NO
be submitted after the established due date?
2 Was any required information missing on the GW-59 report forms?
YES ,NO '
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3 Are any of the monitor wells in need of repair or maintenance(damaged casing, unlocked or missing cap,missing YES NO
identification plate,area overgrown,etc.)?lithe answer is "Yes",contact the Regional Office far guidance.
4 Are any monitored constituents equal to or above the established standards? YES N,
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES"list the affected wells individually with constituent(s)and concentration(s)
exceeding standards in the space provided below.
5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s)exceeding
standards, concentration(s)reported, and sample collection date for each occurrence (for the last two years).
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11.3I ( .:,
6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located;contact the Regional Office.
7 Is the permittee implementing previously approved actions required by the Division involving this YES NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days;an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines, and/or penalties.
8 The person completing this portion(GW-59A)of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report(Compliance Report GW-59A)is true and complete to the best of my knowledge.
Signature of Permittee(or Authorized Agent) Date
2,11/200.3

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original OEPARTMENTOF ENVIRONMENTAL QUALITY-OW.OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING: I copy t�: INFORMATIONPROCESSINGIINIT
andCOMPLIANCE REPORT FORM 1 17MAIL SERVICE CE.NTER,RALEIGH,NC27669.18t7
FACILITY INFORMATION Please Pnnt Dearly orType PERMIT Number: Expiration Date: 2128/2022
Facility Name: Rose I-till Plantation Development,LLC Non-Discharge_ UIC
Permit Name(if different): NPDES Other woaa32at%
-----------------_.
Facility Address: 3041 New Leicester Highway TYPE OF PERMITTED OPERATION BEING MONITORED
Leicester ' NC 28748 County Buncombe ❑ Lagoon ❑ Remediation: Infiltration Gallery
Spray Field ❑ Remediation:
Contact Person: Bob Barr Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name.Well#1(MW A on OW-1b) No. of wells to be sampled: 3 LI Water Source Heat Pump 0 Other Surface Irrigation
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): Well#1 Upgradient Date sample collected: 11/2412021 FIELD ANALYSES: WAS
Well Depth: 69 ft. Well Diameter: 2 in. pH 00400: 6.4 units Temp.aaato. 13.8 °C DRY at
Depth to Water Level 82546:33.8 4Mhos time of
p ft. below measuring point Screened interval: ft. to 69 ft. Spec.Cond.axis.): 45.5 p sampling,
Measuring Point is 2.5 ft. above land surface Relative M.P.Elevation: ft. Odor 00085: None
check
Volume of water pumped/bailed before sampling: gallons Appearance Cloudy herein
Samples for metals were collected unfiltered: El YES ❑ NO and field acidified: 0 YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:12113f2o21 Laboratory Name: Pace Analytical Certification No. 40
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO2)as N 00620 0.043 mg/L Zn-Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus:Total as P mess 0.060 mg/L
Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units):
(Note_ Use MPN method for highly turbid samples)
)issolved Solids:Total 70300 43.0 mg/L Al-Aluminum cites mg/L
pH (Lab)00403 units Ba-Barium 01a07 ugiL
TOC 00680 <1.0 mg/L Ca-Calcium oosis mg/L
Chloride 00940 <1.0 mg/L Cd-Cadmium 01027 ugiL
Arsenic 01002 ugiL Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ugiL Fe Iron 01045 ugiL (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? Li Yes(1) ❑ No(0)
Specific Conductance 00095 ttMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200B
Total Ammonia 00e10 0.11 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen,NN as N Ammonia Nitrogen,Total)
Mn-Manganese moss ugiL , method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs. mg/L VOC Removal%
I certify that,to the best of my knowledge and belief,the information submitted in this report is true.accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
Robert P.Barr/Authorized Agent S i"21-Z.I
Permittee(or Authorized Agent)Name and Title-Please print or type Signature of Permittee for Authorized Agent) (Date)
GW-59 Rev.06-0 7-2018

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DM OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING: and 1 co to INFORMATION PROCESSING UNIT
py : _ - -
COMPLIANCE REPORT FORM 1647 MAIL SERVICE CENTER,FtALEIGH,NC 276994617
FACILITY INFORMATION Please Pnbt Deady or Type
PERMIT Number: Expiration Date 2/28/2022
Facility Name: Rose Hill Plantation Development,LLC Non-Discharge UIC
Permit Name(if different): NPDES Other vv00832016
Facility Address: 3041 New Leicester Highway TYPE OF PERMITTED OPERATION BEING MONITORED
Leicester NC 28748 County Buncombe El Lagoon El Remediation: Infiltration Gallery
0 Spray Field El Remediation:
Contact Person: Bob Barr Telephone#. [phone] 0 Rotary Distributor El Land Application of Sludge
El Well Location/Site Name:Well#2(MW B on OW-lb) No. of wells to be sampled. 3 Ill Water Source Heat Pump other: Surface Irrigation
(from Permit)
SAMPLING INFORMATION If WELL
WELL ID NUMBER(from Permit): Well#2 downgradient Date sample collected: 11/24/2021 FIELD ANALYSES: WAS
Well Depth: 30 ft. Well Diameter: 2 in, pH 00400: 5.6 units Temp. nom: 13-1 'c DRY at
Depth to Water Level 82546:12.34 ft. below measuring point Screened Interval: 10 ft. to 30 ft. Spec.Cond.00e94: 18.7 uMhos time of
sampling,
Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation. ft. Odor 00085 None check
Volume of water pumped/bailed before sampling: gallons Appearance Cloudy here:
Samples for metals were collected unfiltered. •YES El NO and field acidified: .YES El NO
LABORATORY INFORMATION
Date sample analyzed.12/13/2021 Laboratory Name: Pace Analytical Certification No. 40
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead olo5i ug/L
Coliform: MF Fecal 31616 <1 /100mL Nitrate(NO3)as N 00620 0.39 mg/L Zn-Zinc ot 092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.050 mg/L
[Note Use IVIPN method for highly turbid samples)
Orthophosphate 70607 mg/L Other(Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 <25.0 mgit Al-Aluminum 81185 mg/L
pH (Lab)00403 units Ba-Barium 010o7 ug/L.
TOC 00680 <1.0 mg/L Ca-Calcium 38818 mg/L
Chloride 00940 1 A mg/L Cd-Cadmium 01027 ug/L
Arsenic 01002 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS:(by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe-Iron 01045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00848 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? * Yes(1) El No(0)
Specific Conductance 00095 1.IMhos K-Potassium 00937 mg/L VOC 7873 , method# SM 6200B
Total Ammonia 00610 0.12 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrogen.NFI3as N:Ammonia Nitrogen Total)
Mn-Manganese 01055 ug/L method#
TKN as N 00625 mg/L Ni-Nickel 01067 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
i certify that,to the best of my knowledge and belief,the information submitted in this report is true,accurate,and complete,and that the laboratory analytical data was produced using approved methods of analysis by a
_
DVVR-ceitified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
0-41/42.--"-
Robert P.Barr/Authorized Agent 12.-?_f-IS
Permit-tee(or Authorized Agent)Name and Trtle-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.06-07-2018

SUBMIT FORM ON YELLOW PAPER ONLY
Mail original DEPARTMENT OF ENVIRONMENTAL QUALITY-DtV OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING: IN 3RMAlION PROCESSING UNIT
COMPLIANCE REPORT FORM and copy to: 1s17''MAIL SERVICECENTER-RtALEI H,NC27099-15'17
FACILITY INFORMATION Please Pont Clearly or Type PERMIT Number: Expiration Date: 2r28/2022
Facility Name: Rose Hill Plantation Development,LLC Non-Discharge UIC
Permit Name(if different): NPDES Other WQ0032016
Facility Address: 3041 New Leicester Highway TYPE OF PERMITTED OPERATION BEING MONITORED
Leicester NC 28748 County Buncombe ❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
Contact Person: Bob Barr Telephone#: [phone] ❑ Rotary Distributor CILand Application of Sludge
Well Location/Site Name:Well#3 No.of wells to be sampled: 3 ❑ Water Source Heat Pump LI Other: Surface Irrigation
(from Permit)
SAMPLING INFORMATION hlf WELL
WELL ID NUMBER(from Permit): Well##3 Date sample collected: 11/24/2021 FIELD ANALYSES: WAS
Well Depth: 14 ft. Well Diameter: 2 in. pH 00400: 6.3 units Temp.comp. 18.4 BC DRY at
Depth to Water Level 82546:4.88 ft. below measuring point Screened Interval: 4 ft. to 14 ft. Spec. Cond. 00094- 85.8 µMhos time of
sampling,
Measuring Point is 0 ft.above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check
Volume of water pumped/bailed before sampling: gallons Appearance Cloudy here:
Samples for metals were collected unfiltered: 0 YES ❑ NO and field acidified: ❑■ YES ❑ NO r
LABORATORY INFORMATION
Date sample analyzed:12/1312821 Laboratory Name: Pace Analytical Certification No. 40
PARAMETERS NOTE:Values should reflect dissolved and colloidal concentrations.
COD ao335 mg/L Nitrite(NO2)as N 00615 mg/L Pb-Lead 01051 ug/L
Coliform: ME Fecal 31616 <1 /100mL Nitrate(NO3)as N o062a <0.040 mg/L Zn-Zinc a1092 mg/L
Coliform: ME Total 31604 /100mL Phosphorus:Total as P 06665 0.62 mg/L
Note Use MPN method for h ghly turbid samples} Orthophosphate 70507 mg/L Other(Specify Compounds and Concentration Units).
Dissolved Solids:Total 70300 54.0 mg/L Al-Aluminum o1105 mg/L
pH(Lab)00403 units Ba-Barium 01007 ug/L
TOC 00680 <1.0 mg/L Ca-Calcium 00916 mg/L
Chloride 00940 3.4 mg/L Cd-Cadmium 01027 ug/L
Arsenic a1o02 ug/L Chromium:Total 01034 ug/L
Grease and Oils 00552 mg/L Cu-Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ugiL Fe-Iron D1045 ug/L (Specify test and method#.ATTACH LAB REPORT.)
Sulfate 00945 mg/L Hg-Mercury 71900 ug/L Lab Report Attached? 0 Yes(1) ❑ No(0)
Specific Conductance 0a0s5 ttMhos K-Potassium 00937 mg/L VOC 7873 , method# Sill 62008
Total Ammonia 00610 <0.10 mg/L Mg-Magnesium 00927 mg/L , method#
(Ammonia Nitrog€n,NH.,as N,Ammonia Nitrogen.Total) Mn-Manganese 01055 ug/L , method#
TKN as N 00625 mgiL Ni-Nickel a1o67 ug/L , method#
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that.to the best of my knowledge and belief,the information submitted in this report is true.accurate,and complete,and that the laboratory analytical data was produ d using approved methods of analysis by a
Di+ rtified laboratory. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations.
Robert P.Barr/Authorized Agent I`
Permittee(or Authorized Agent)Name and Tile-Please print or type Signature of Permittee(or Authorized Agent) (Date)
GW-59 Rev.06-07-2018

riFllYf�,.
��k R
, Pace Analytical Services,LLC
m
/'aceAnalftical 2225 e NC ode L�1
r.
Asheville,NC 28804
www.pacelah9.com [phone]
i
ANALYTICAL RESULTS
Project: Rose Hill MWs 11/24/21
Pace Project No.: 92574373
Sample: MW-1 Lab ID: 92574373001 Collected: 11/24/21 11:20 Received: 11/24/21 12.35 Matrix: Water
Parameters Results Units Report Limit DP Prepared Analyzed CAS No. Qual
Monitoring Well Data Analytical Method:
Pace Analytical Services-Charlotte
Performed by Pace 1 12/13/21 12':11
Collected By RMB 1 12/13/21 12:11
Collected Date 11/24/21 1 12/13/21 12:11
Collected Time 11:20 1 12/13/21 12:11
pH 6.4 Std,Units 1 12/13/21 12:11
Temperature 13.8 deg C 1 12/13/21 12:11
Static Water Level 33.80 feet 1 12/13/21 12:11
Specific Conductance 45.5 umhos/cm 1 12/13/21 12:11
Turbidity 69.5 NTU 1 12/13/21 12:11
Carbon dioxide None mg/L 1 12/13/21 12:11 124-38-9
Odor Cloudy 1 12/13/21 12:11
6246E MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Benzene ND ug/L 0.50 1 12/08/21 11:36 71-43-2
Bromobenzene ND ug/L 0.50 1 12/08/21 11:36 108-86-1
Bromochloromethane ND ug/L 0.50 1 12/08/21 11:36 74-97-5
Bromodichioromethane ND ug/L 0.50 1 12/08/21 11:36 75-27-4
Bromoform ND ug/L 0.50 1 12/08/21 11:36 75-25-2
Bromomethane ND ug/L 5.0 1 12/08/21 11:36 74-83-9
n-Butylbenzene ND ug/L 0.50 1 12/08/21 11:36 104-51-8
sec-Butylbenzene ND ug/L 0.50 1 12/08/21 11:36 135-98-8
tert-Butylbenzene ND ug/L 0.50 1 12/08/21 11:36 98-06-6
Carbon tetrachloride ND ug/L 0.50 1 12/08/21 11:36 56-23-5
Chlorobenzene ND ug/L 0.50 1 12/08/2111.36 108-90-7
Chloroethane ND ug/L 1.0 1 12/08/21 11:36 75-00-3
Chloroform ND ug/L 0.50 1 12/08/21 11:36 67-66-3
Chloromethane ND ug/L 1.0 1 12/08/21 11:36 74-87-3
2-Chlorotoluene ND ug/L 0.50 1 12/08/21 11:36 95-49-8
4-Chlorotoluene ND ug/L 0.50 1 12/08/21 11:36 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 12/08/21 11:36 96-12-8
Dibromochloromethane ND ug/L 0.50 1 12/08/21 11:36 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 0.50 1 12/08/21 11:36 106-93A
Dibromomethane ND ug/L 0.50 1 12/08/21 11:36 74-95-3
1,2-Dichlorobenzene ND ug/L. 0.50 1 12/08/21 11:36 95-50-1
1,3-Dichlorobenzene ND ug/L 0.50 1 12/08/21 11:36 541-73-1
1,4-Dichlorobenzene ND ug/L 0.50 1 12/08/21 11:36 106-46-7
Dichlorodifluoromethane ND ug/L 0.50 1 12/08/21 11:36 75-71-8
1,1-Dichloroethane ND ug/L 0.50 1 12/08/21 11:36 75-34-3
1,2-Dichloroethane ND ug/L 0.50 1 12/08/21 11:36 107-06-2
1,1-Dichloroethene ND ug/L 0,50 1 12/08/21 11:36 75-35-4
cis-1,2-Dichloroethene ND ug/L 0.50 1 12/08/21 11:36 156-59-2
trans-1,2-Dichloroethene ND ug/L 0.50 1 12/08/21 11:36 156-60-5
1,2-Dichloropropane ND ug/L 0.50 1 12/08/21 11:36 78-87-5
1,3-Dichloropropane ND ug/L 0.50 1 12/08/21 11:36 142-28-9
2,2-Dichloropropane ND ug/L 0.50 1 12/08/21 11:36 594-20-7
REPORT OF LABORATORY ANALYSIS
This report,shall not be reproduced,except in full,
Date: 12/13/2021 01:56 PM without the written consent of Pace Analytical Services,LLC Page 4 of 29

Pace Analytical Services,LLC
44,
raceArelytical
2225 Riverside Dr,
Asheville,NC 28804
/ www.pacelatis.com [phone]
,
I
ANALYTICAL RESULTS
Project: Rose Hill MWs 11/24/21
Pace Project No.: 92574373
Sample: MW-1 Lab ID: 92574373001 Collected: 11/24/21 11:20 Received: 11/24/21 12:35 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Dual
6200B MSV Analytical Method:SM 62008
Pace Analytical Services-Charlotte
1,1-Dichloropropene ND ug/L 0.50 1 12/08/21 11:36 563-58-6
cis-1,3-Dichloropropene ND ug/L 0.50 1 12/08/21 1136 10061-01-5
trans-1,3-Dichloropropene ND ug/L 0.50 1 12/08/21 11,36 10061-02-6
Diisopropyl ether ND ug/L 0.50 1 12/08/21 11:36 108-20-3
Ethylbenzene ND ug/L 0.50 1 12/08/211 11:36 100-41-4
Hexachloro-1,3-butadiene ND ug/L 2.0 1 12/08/21 11:36 87-68-3
lsopropylbenzene(Cumene) ND ug/L 0.50 1 12/08/21 11:36 98-82-8
Methylene Chloride ND ug/L 2.0 1 12/08/21 11:36 75-09-2
Methyl-tert-butyl ether ND ug/L 0.50 1 12/08/21 11:36 1634-04-4
Naphthalene ND ug/L 2.0 1 12/08/21 11:36 91-20-3
n-Propylbenzene ND ug/L 0.50 1 12/08/21 11:36 103-65-1
Styrene ND ug/L 0.50 1 12/08/21 1136 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 12/08/21 11:36 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 12/08/21 11:36 79-34-5
Tetrachloroethene ND ug/L 0.50 1 12/08/21 11:36 127-18-4
Toluene ND ug/L 0.50 1 12/08/21 1136 108-88-3
1,2,3-Trichlorobenzene ND ug/L 2.0 1 12/08/21 11.36 87-61-6
1,2,4-Trichlorobenzene ND ug/L 2.0 1 12/08/21 1136 120-82-1
1,1,1-Trichloroethane ND ug/L 0.50 1 12/08/21 11:36 71-55-6
1,1,2-Trichloroethane ND ug/L 0.50 1 12/08/21 11:36 79-00-5
Trichloroethene ND ug/L 0.50 1 12/08/21 11:36 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 12/08/21 11:36 75-69-4
1,2,3-Trichloropropane ND ug/L 0.50 1 12/08/21 11:36 96-18-4
1,2,4-Trimethylbenzene ND ug/L 0.50 1 12/08/21 11:36 95-63-6
1,3,5-Trimethylbenzene ND ug/L 0.50 1 12/08/21 11:36 108-67-8
Vinyl chloride ND ug/L 1.0 1 12/08/21 11:36 75-01-4
m&p-Xylene ND ug/L 1.0 1 12/08/21 1136 179601-23-1
o-Xylene ND ug/L 0.50 1 12/08/21 11:36 95-47-6
Surrogates
1,2-Dichloroethane-d4(S) 94 % 70-130 1 12/08/21 11:36 17060-07-0
4-Bromofluorobenzene(S) 102 °./0 70-130 1 12/08/21 11:36 460-00-4
Toluene-d8(S) 108 % 70-130 'I 12/08/21 11:36 2037-26-5
2540C Total Dissolved Solids Analytical Method:SM 2540C-2015
Pace Analytical Services-Asheville
Total Dissolved Solids 43.0 mg/L 25.0 1 11/30/21 16:28
MBIO 9222D Fecal Coliform AVL Analytical Method:SM 9222D-2015 Preparation Method:SM 9222D-2015
Pace Analytical Services-Asheville
Fecal Coliforms ND CFU/100 rnL 1.0 1 11/24/21 1455 11/25/21 13:00
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 0.11 mg/L 0.10 1 12/08/21 1218 7664-41.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except on full,
Date:12/13/2021 01:56 PM without the written consent of Pace Analytical Services,ILLC, Page 5 of 29

Pace Analytical Services,LLC
2225 Riverside Dr.
aceAna/ytical Asheville,NC 28804
wvempacelalmcom
[phone]
ANALYTICAL RESULTS
Project: Rose Hill MWs 11/24/21
Pace Project No.: 92574373
Sample: MW-1 Lab ID: 92574373001 Collected: 11/24/21 11:20 Received. 11/24/21 12:35 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
353.2 Nitrogen,NO2/NO3 unpres Analytical Method:EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen, Nitrate 0.043 mg/L 0.040 1 11/25/21 0004 14797-55-8
365.1 Phosphorus,Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365i1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus 0.060 mg/L 0.050 1 12/06/21 22:17 12/07/21 17:51 7723-14-0
4500 Chloride Analytical Method:SM 4500-Cl-E-2011
Pace Analytical Services-Asheville
Chloride ND mg/L 1.0 1 12/06/21 10:24 16887-00-6
5310B TOC Analytical Method:SM 5310B-2014
Pace Analytical Services-Asheville
Total Organic Carbon ND mg/L 1.0 1 12/07/21 20:09 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:12/13/2021 01:56 PM without the written consent of Pace Analytical Services,LLC, Page 6 of 29

Pace Analytical Services,LLC
Dr
2225 Riverside Dr.
aceAnalytical Asheville,NC 28804
www.pacolabs.com [phone]
f
I
ANALYTICAL RESULTS
Project: Rose Hill MWs 11/24/21
Pace Project No.: 92574373
Sample: MW-2 Lab ID: 92574373002 Collected: 11/24/21 11:30 Received: 11/24/21 12:35 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qua)
Monitoring Well Data Analytical Method:
Pace Analytical Services-Charlotte
Performed by Pace 1 12/13/21 12:13
Collected By RMB 1 12/13/21 12:13
Collected Date 11/24/21 1 12/13/21 12:13
Collected Time 11:30 1 12/13/21 12:13
pH 5.6 Std.Units 1 12/13/21 12:13
Temperature 13.1 deg C 1 12/13/21 12:13
Static Water Level 12.34 feet 1 12/13/21 12:13
Specific Conductance 18.7 umhos/cm 1 12/13/21 12:13
Turbidity 69.9 NT U 1 12/13/21 12:13
Odor None 1 12/13/21 12:13
Appearance Cloudy 1 12/13/21 12:13
6200B MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
Benzene ND ug/L 0.50 1 12/08/21 11:53 71-43-2
Bromobenzene ND ug/L 0.50 1 12/08/21 11:53 108-86-1
Bromochloromethane ND ug/L 0.50 1 12/08/21 11:53 74-97-5
Bromodichloromethane ND ug/L 0.50 1 12/08/21 11:53 75-27-4
Bromoform ND ug/L 0.50 1 12/08/21 11:53 75-25-2
Bromomethane ND ug/L 5.0 1 12/08/21 11:53 74-83-9
n-Butylbenzene ND ug/L 0,50 1 12/08/21 11.53 104-51-8
sec-Butylbenzene ND ug/L 0.50 1 12/08/21 11:53 135-98-8
tert-Butylbenzene ND ug/L 0.50 1 12/108/21 11:53 98-06-6
Carbon tetrachloride ND ug/L 0.50 1 12/08/21 11:53 56-23-5
Chlorobenzene ND ug/L 0.50 1 12/08/21 11:53 108-90-7
Chloroethane ND ug/L 1.0 1 12/08/21 11:53 75-00-3
Chloroform ND ug/L 0.50 1 12/08/21 11:53 67-66-3
Chloromethane ND ug/L 1.0 1 12/08/21 11:53 74-87-3
2-Chlorotoluene ND ug/L 0.50 1 12/08/21 11:53 95-49-8
4-Chiorotoluene ND ug/L 0.50 1 12/08/21 11:53 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 12/08/21 11:53 96-12-8
Dibromochloromethane ND ug/L 0.50 1 12/08/21 11:53 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 0.50 1 12/08/21 11:53 106-93-4
Dibromomethane ND ug/L 0.50 1 12/08/21 11:53 74-95-3
1,2-Dichlorobenzene ND ug/L 0.50 1 12/08/21 11:53 95-50-1
1,3-Dichlorobenzene ND ug/L 0,50 1 12/08/21 11:53 541-73-1
1,4-Dichlorobenzene ND ug/L 0.50 1 12/08/21 11:53 106-46-7
Dichlorodifluoromethane ND ug/L 0.50 1 12/08/21 11:53 75-71-8
1,1-Dichbroethane ND ug/L. 0.50 1 12/08/21 11:53 75-34-3
1,2-Dichloroethane ND ug/L 0.50 1 12/08/21 11:53 107-06-2
1,1-Dichloroethene ND ug/L 0.50 1 12/08/21 11:53 75-35-4
cis-1,2-Dichloroethene ND ug/L 0.50 1 12/08/21 11;53 156-59-2
trans-1,2-Dichloroethene ND ug/L 0.50 1 12/08/21 11:53 156-60-5
1,2-Dichloropropane ND ug/L 0.50 1 12/08/21 11:53 78-87-5
1,3-Dichloropropane ND ug/L 0.50 1 12/08/21 11:53 142-28-9
2,2-Dichloropropane ND ug/L 0.50 1 12/08/21 11:53 594-20-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except In full,
Date: 12/13/2021 01:56 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 29

Pace Analytical Services,LLC
2225 Rverside Dr,
.---, aceAnalytical
Asheville,NC 28804
www.pacolas.com
[phone]
i
ANALYTICAL RESULTS
Project: Rose Hill MWs 11/24/21
Pace Project No.: 92574373
Sample: MW-2 Lab ID: 92574373002 Collected: 11/24/21 11:30 Received: 11/24/21 12:35 Matrix: Water
Parameters Results Units Report Limit DE Prepared Analyzed CAS No. Dual
6200B MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
1,1-Dichloropropene ND ug/L 0.50 1 12/08/21 11:53 563-58-6
cis-1,3-Dichloropropene ND ug/L 0.50 1 12/08/21 11:53 10061-01-5
trans-1,3-Dichloropropene ND ug/L 0.50 1 12/08/21 11:53 10061-02-6
Diisopropyl ether ND ug/L 0.50 1 12/08/21 11:53 108-20-3
Ethylbenzene ND ug/L 0.50 1 12/08/21 11:53 100-41-4
Hexachloro-1,3-butadiene ND ug/L 2.0 1 12/08/21 11:53 87-68-3
isopropylbenzene(Cumene) ND ug/L 0.50 1 12/08/21 11:53 98-82-8
Methylene Chloride ND ug/L 2.0 1 12/08/21 11.53 75-09-2
Methyl-tert-butyl ether ND ug/L 0.50 1 12/08/21 11:53 1634-04-4
Naphthalene ND ug/L 2.0 1 12/08/21 11:53 91-20-3
n-Propylbenzene ND ug/L 0.50 1 12/08/21 11:53 103-65-1
Styrene ND ug/L 0.50 1 12/08/21 11:53 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 12/08/21 11:53 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 12/08/21 11:53 79-34-5
Tetrachloroethene ND ug/L 0.50 1 12/08/21 11:53 127-18-4
Toluene ND ug/L 0.50 11 12/08/21 11:53 108-88-3
1,2,3-Trichlorobenzene ND ug/L 2.0 1 12/08/21 11:53 87-61-6
1,2,4-Trichlorobenzene ND ug/L 2,0 1 12/08/21 11:53 120-82-1
1,1,1-Trichloroethane ND ug/L 0.50 1 12/08/21 11.53 71-55-6
1,1,2-Trichioroethane ND ug/L 0.50 1 12/08/21 11:53 79-00-5
Trichloroethene ND ug/L 0.50 1 12/08/21 11:53 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 12/08/21 11:53 75-69-4
1,2,3-Trichloropropane ND uglL 0.50 1 12/08/21 11:53 96-18-4
1,2,4-Trimethylbenzene ND ug/L 0.50 1 12/08/21 11:53 95-63-6
1,3,5-Trimethylbenzene ND ug/L 0.50 1 12/08/21 11:53 108-67-8
Vinyl chloride ND ug/L 1.0 1 12/08/21 11:53 75-01-4
m&p-Xylene ND ug/L 1.0 1 12/08/21 11:53 179601-23-1
o-Xylene ND ug/L 0.50 1 12/08/21 11:53 95-47-6
Surrogates
1,2-Dichloroethane-d4(S) 95 % 70-130 1 12/08/21 11:53 17060-07-0
4-Bromofluorobenzene(S) 100 % 70-130 1 12/08/21 11:53 450-00-4
Toluene-d8(S) 103 % 70-130 1 12/08/21 11:53 2037-26-5
2540C Total Dissolved Solids Analytical Method:SM 2540C-2015
Pace Analytical Services-Asheville
Total Dissolved Solids ND mg/L 25.0 1 11/30/21 16:28
MBIO 9222D Fecal Coliform AVL Analytical Method:SM 9222D-2015 Preparation Method:SM 9222D-2015
Pace Analytical Services-Asheville
Fecal Coliforms ND CFU/100 mL 1.0 1 11/24/21 14:55 11/25/21 13:00
350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia 0.12 mg/L 0.10 1 12/08/21 12:23 7664-41-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date: 12/13/2021 01:56 PM without the written consent of Pace Analytical Services,LL.D. Page 8 of 29

Pace Analytical Services,LLC
2225 Riverside Dr.
it;_
ace Analytical Asheville,NC 28804
www.pacolabs.com [phone]
ANALYTICAL RESULTS
Project: Rose Hill MWs 11/24/21
Pace Project No.: 92574373
Sample: MW-2 Lab ID: 92574373002 Collected: 11/24/21 11:30 Received: 11/24/21 1235 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
353.2 Nitrogen, NO2/NO3 unpres Analytical Method:EPA 353.2 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Nitrate 0.39 mg/L. 0.040 1 11/25/21 00:08 14797-55-8
365.1 Phosphorus,Total Analytical Method:EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus ND mg/L 0.050 1 12/06/21 22:17 12/07/21 17:52 7723-14-0
4500 Chloride Analytical Method:SM 4500-CI-E-2011
Pace Analytical Services-Asheville
Chloride 1.4 mg/L 1.0 1 12/06/21 10:26 16887-00-6
5310B TOC Analytical Method:SM 5310B-2014
Pace Analytical Services-Asheville
Total Organic Carbon ND mg/L 1.0 1 12/07/21 20:24 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date: 12/13/2021 01:56 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 29

Pace Analytical Services,LLC
cer
*aceAnalitical 2225 Riverside Dr.
-...,. Asheville,NC 28804
/ www.pacolatmcom [phone]
1
ANALYTICAL RESULTS
Project: Rose Hill MWs 11/24/21
Pace Project No.: 92574373
Sample: MW-3B Lab ID: 92574373003 Collected: 11/24/21 1200i Received: 11/24/21 12:35 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Monitoring Well Data Analytical Method.
Pace Analytical Services-Charlotte
Performed by Pace 1 12/13/21 12:14
Collected By RMB 1 12/13/21 12:14
Collected Date 11/24/21 1 12/13/21 12:14
Collected Time 12:00 1 12/13/21 12:14
pH 6.3 Std.Units 1 12/13/21 12:14
Temperature 13.4 deg C 1 12/13/21 12:14
Static Water Level 4.88 feet 1 12/13/21 12:14
Specific Conductance 85.8 umhos/cm 1 12/13/21 12:14
Turbidity 99.3 NTU 1 12/13/21 12:14
Odor Sulfur 1 12/13/21 12:14
Appearance Cloudy 1 12/13/21 12:14
6200B MSV Analytical Method: SM 6200B
Pace Analytical Services-Charlotte
Benzene ND ug/L 0.50 1 12/08/21 12:11 71-43-2
Bromobenzene ND ug/L 0.50 1 12/08/21 12:11 108-86-1
Bromochloromethane ND ug/L 0.50 1 12/08/21 1211 74-97-5
Bromodichloromethane ND ug/L 0.50 1 12/08/21 12:11 75-27-4
Bromoform ND ug/L 0.50 1 12/08/21 1211 75-25-2
Bromomethane ND ug/L 5.0 1 12/08/21 12:11 74-83-9
n-Butylbenzene ND ug/L 0.50 1 12/08/21 12:11 104-51-8
sec-Butylbenzene ND ug/L 0.50 1 12/08/21 12:11 135-98-8
tert-Butylbenzene ND ug/L 0.50 11 12/08/21 12:11 98-06-6
Carbon tetrachloride ND ug/L 0.50 1 12/08/21 12:11 56-23-5
Chlorobenzene ND ug/L 0.50 1 12/08/21 12:11 108-90-7
Chloroethane ND ug/L 1.0 1 12/08/21 12:11 75-00-3
Chloroform ND ugit 0.50 1 12/08/21 12:11 67-66-3
Chloromethane ND ug/L 1.0 1 12/08/21 12:11 74-87-3
2-Chlorotoluene ND ug/L 0.50 1 12/08/21 12:11 95-49-8
4-Chlorotoluene ND ug/L 0.50 1 12/08/21 12:11 106-43-4
1,2-Dibromo-3-chtoropropane ND ug/L 1.0 1 12/08/21 12:11 96-12-8
Dibromochloromethane ND ugfL 0.50 1 12/08/21 12:11 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 0.50 1 12/08/21 12:11 106-93-4
Dibromornethane ND ug/L 0.50 1 12/08/21 12:11 74-95-3
1,2-Dichlorobenzene ND ug/L 0.50 1 12/08/21 12;11 95-50-1
1,3-Dichlorobenzene ND ug/L 0.50 'I 12/08/21 12:11 541-73-1
1,4-Dichlorobenzene ND ug/L 0.50 1 12/08/21 12:11 106-46-7
Dichlorodifluoromethane ND Lig/L 0.50 1 12/08/21 12:11 75-71-8
1,1-Dichloroethane ND ug/L 0.50 1 12/08/21 12:11 75-34-3
1,2-Ehchloroethane ND ug/L 0.50 1 12/08/21 12:11 107-06-2
1,1-Dichloroethene ND ug/L 0.50 1 12/08/21 12:11 75-35-4
cis-1,2-Dichloroethene ND ug/L 0.50 1 12/08/21 12:11 156-59-2
trans-12-Dtchloroethene ND ug/L 0.50 1 12/08/21 12:11 156-60-5
1,2-Dichloropropane ND uglL 0.50 1 12/08/21 1211 78-87-5
1,3-Dichloropropane NO ug/L 0.50 1 12/08/21 12:11 142-28-9
2,2-Dichloropropane ND ug/L 0.50 1 12/08/21 1211 594-20-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date: 12/13/2021 01;56 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 29

Pace Analytical Services,LLC
i-
2225 Riverside Dr.
aceAn .io
alytical Ashevilie,NC 28804
._.-
www.pacelabs.com [phone]
i
i
ANALYTICAL RESULTS
Project: Rose Hill MWs 11/24/21
Pace Project No,: 92574373
Sample: MW-3B Lab ID: 92574373003 Collected: 11/24/21 12:00 Received: 11/24/21 12:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method:SM 6200B
Pace Analytical Services-Charlotte
1,1-Dichloropropene ND ug/L 0.50 1 12/08/21 12:11 563-58-6
cis-1,3-Dichloropropene ND ug/L 0.50 1 12/08/21 12:11 10061-01-5
trans-1,3-Dichloropropene ND ug/L 0.50 1 12/08/21 12:11 10061-02-6
Ditsopropyl ether ND ug/L 0,50 1 12/08/21 12:11 108-20-3
Ethylbenzene ND ug/L 0.50 1 12/08/21 12:11 100-41-4
Hexachkoro-1,3-butadiene ND ug/L 2.0 1 12/08/21 12:11 87-68-3
lsopropylbenzene(Cumene) ND ug/L 0.50 1 12/08/21 12:11 98-82-8
Methylene Chloride ND ug/L 2.0 1 12/08/21 12:11 75-09-2
Methyl-tert-butyl ether ND ugfL 0.50 1 12/08/21 12:11 1634-04-4
Naphthalene ND ug/L 2.0 1 12/08/21 12:11 91-20-3
n-Propylbenzene ND ug/L 0.50 1 12/08/21 12:11 103-65-1
Styrene ND ug/L 0.50 1 12/08/21 12:11 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 12/08/21 12:11 630-20-6
1,1,2„2-Tetrachloroethane ND ug/L 0,50 1 12/08/21 12:11 79-34-5
Tetrachloroethene ND ug/L 0.50 1 12/08/21 12:11 127-18-4
Toluene ND ug/L 0.50 1 12/08/21 12:11 108-88-3
1,2,3-Trichlorobenzene ND ug/L 2,0 1 12/08/21 12:11 87-61-6
1,2,4-Trichlorobenzene ND ug/L 2.0 1 12/08/21 12:11 120-82-1
1,1,1-Trichkoroethane ND ug/L D.50 1 12/08/21 12:11 71-55-6
1,1,2-Trichloroethane ND ug/L 0.50 1 12/08/21 12:11 79-00-5
Trichloroethene ND ug/L 0.50 1 12/08/21 12:11 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 12/08/21 12:11 75-69-4
1,2,3-Trichloropropane ND ug/L 0.50 1 12/08/21 12:11 96-18-4
1,2,4-Trimethylbenzene ND ug/L 0.50 1 12/08/21 12:11 95-63-6
1,3,5-Trimethylbenzene ND ug/L 0.50 1 12/08/21 12:11 108-67-8
Vinyl chloride ND ug/L 1.0 1 12/08/21 12:11 75-01-4
m&p-Xylene ND ug/L 1.0 1 12/08/21 12:11 179601-23-1
o-Xylene ND ug/L 0.50 1 12/08/21 12:11 95-47-6
Surrogates
1,2-DicNoroethane-d4(S) 94 % 70-130 1 12/08/21 12:11 17060-07-0
4-Bromoftuorobenzene(S) 98 °/0 70-130 1 12/08/21 12:11 460-00-4
Toluene-d8(S) 103 % 70-130 1 12/08/21 12:11 2037-26-5
2540C Total Dissolved Solids Analytical Method:SM 2540C-2015
Pace Analytical Services-Asheville
Total Dissolved Solids 54.0 mg/L 25,0 1 11/30/21 16:28
MBIO 9222D Fecal Coliform AVL Analytical Method: SM 9222D-2015 Preparation Method:SM 9222'D-2015
Pace Analytical Services-Asheville
Fecal Coliforms ND CFU/100 mL 1.0 1 11/24/21 14:55 11/25/21 13:00
350.1 Ammonia Analytical Method:EPA 350.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Nitrogen,Ammonia ND mg/L 0.10 1 12/08/21 12:24 7664-41-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date: 12/13/2021 01:56 PM without the written consent ot Pace Analytical Services,LLC. Page 11 of 29

Pace Analytical Services,LLC
2225 Riverside Dr.
aceAnaI `�/�l ica1 Asheville,NC 28804
www.picelaas.eom
[phone]
ANALYTICAL RESULTS
Project: Rose Hill MWs 11/24/21
Pace Project No.: 92574373
Sample: MW-3B Lab ID: 92574373003 Collected: 11/24/21 12:00 Receved: 11/24/21 12:35 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual
353.2 Nitrogen,N021NO3 unpres Analytical Method: EPA 353.2 Rev 2,0 1993
Pace Analytical Services-Asheville
Nitrogen,Nitrate ND rng/L 0,20 5 11/25/21 00:19 14797-55-8
365,1 Phosphorus,Total Analytical Method:EPA 365.1 Rev 2.0 1993 Preparation Method:EPA 365.1 Rev 2.0 1993
Pace Analytical Services-Asheville
Phosphorus 0.62 mg/L 0.050 1 12/06/21 22:17 12/07/21 17:52 7723-14-0
4500 Chloride Analytical Method:SM 4500-Cl-E-2011
Pace Analytical Services-Asheville
Chloride 3.4 mg/L 1.0 1 12/06/21 10:29 16887-00-6
5310B TOC Analytical Method:SM 5310B-2014
Pace Analytical Services-Asheville
Total Organic Carbon ND mg/L 1,0 1 12/07/21 20:39 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date: 12/13/2021 01:56 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 29

Pace Analytical Services,LLC
or,
2225 Dr,
.*aceAnalytical AshevillRiversidee,NC 28804
www.pacelalbs.eem
[phone]
QUALIFIERS
Project: Rose Hill MWs 11/24/21
Pace Project No.: 92574373
DEFINITIONS
OF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUE-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
REPORT OF LABORATORY ANALYSIS
'This report shall not be reproduced,except in lull,
Date: 12/13/2021 01:56 PM without the written consent of Pace Analytical Services,L LC. Page 25 of 29

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Pace Analytical Services,LLC
a
2225 Rverside Dr.ceAnalytical(itr
Asheviffe,NC 28804
www.pacelabs.com
[phone]
December 13, 2021
Kimber Reese
RPB Systems Inc.
P.O. Box 1325
Asheville, NC 28802
RE: Project: Rose Hill MWs 11/24/21
Pace Project No.: 92574373
Dear Kimber Reese:
Enclosed are the analytical results for sample(s)received by the laboratory on November 24, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
If you have any questions concerning this report,please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
cc: Mr.Robert Barr, RPB Systems Inc.
Ms.Liz Barr, RPB Systems Inc.
Cody Pannell,RPB Systems
i
REPORT OF LABORATORY ANALYSIS
10 This report shall not be reproduced,except in fulf,
without the written consent of Pace Analytical Services,LLC. Page 1 of 29