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(!IceAnalyticZ
W".pacalabs.culn
July 22, 2021
Mr. Bernie Kelly
Davidson River Village, LLC
P.O. Box 880
Pisgah Forest, NC 28768
RE: Project: July 2021
Pace Project No.: 92547500
Dear Mr. Kelly:
Pace Analytical Sorvices, LLC
2225 Riverside Dr.
Asheville, NO 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on July 01, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNIINELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely, \`
Chris Derouen
ch([e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page t of 19

aceAnalytical'
Wmilicelabs.com
Project: July 2021
Pace Project No.: 92647500
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirglniaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntan consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville. NC 28604
[phone]
Page 2 of 19

aceAnalytical e
www.Picehbs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
July 2021
92547500
Analyles
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92547600001
Q88V2
EPA6010D
SHt
6
PASI-A
EPA6020B
JOR
- 1
PASI-A
EPA7470A
S00
1
PASI-A
SM 254OC-2011
ZMC
1
PASI-A
EPA 300.0 Rev 2.11993
CDC
1
PASI-A
EPA 350.1 Rev 2.D 1993
NGP
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
92547500002
ASB-01
EPA6010D
SH1
6
PASI-A
EPA 60208
JOR
1
PASI-A
EPA 7470A
SOO
1
PASI-A
SM 254OC-2011
ZMC
1
PASI-A
EPA 300.0 Rev 2.1 1093
CDC
1
PASI-A
EPA350.1 Rev2.01993
NGP
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
92647500003
ASS-02
EPA 601 OD
SH1
6
PASI-A
EPA6020B
JOR
1
PASI-A
EPA7470A
SOO
1
PASI-A
SM 254OC-2011
ZMC
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.01993
NGP
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
PASI-A - Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 19

Pace Analytical services, LLC
aeeAnalytical 0 2226 Riverside Dr.
28804
82e)264-7176
www.parelinsom Asheville()2C
' 827776
i
ANALYTICAL RESULTS
Project: July 2021
Pace Project No.: 92547500
Sample: Q88V2 Lab ID: 92547600001 Collected: 07/0V21 14:10 Received: 07/01/21 17:02 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua[
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
07/01/21 14:10
Collected By
Mark
1
07/01121 14:10
Swann
Collected Date
711121
1
07/01121 14:10
Collected Time
14:10
1
07f01121 14:10
pH
5.22 Sid. Units
1
07101/21 14:10
Temperature
18.6 deg C
1
07/0V21 14:10
Static Water Level
62.03 feet
1
07/01121 14:10
Specific Conductance
16.9 umhos/cm
1
0710112114:10
Oxidation Potential
95.1 my
1
D7/01121 14:10
Oxygen, Dissolved
6.51 mglL
1
07/01121 14:10
7782-44-7
Turbidity
3.21 NTU
1
07101/2114:10
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method:
EPA 3010A
Pace Analytical Services - Asheville
Arsenic
NO ug/L 10.0
1 07/1312111:50
0711312122:45
7440.38.2
Chromium
34.2 ug/L 5.0
1 07/1312111:50
07/1312122:45
7440-47-3
Iron
30700 ug/L 50.0
1 07/13/2111:50
07fl 3121 22:45
7439-89.6 Mt
Lead
11.6 ug1L 5.0
1 07/13/21 11:50
07/13121 22:45
7439-92-1
Manganese
1680 ug/L 5.0
1 07/1312111:50
07/1312122:45
7439-96-5 M1
Sodium
29900 ug/L 5000
1 07/1312111:50
07/1312122:45
7440.23-5 M1
6020 MET ICPMS
Analytical Method: EPA6020B Preparation Method: EPA3010A
Pace Analytical Services -Asheville
Cobalt
ND ug1L 1.0
1 0710712113:27
07107/21 21:26
744D-48-4
7470 Mercury
Analytical Method: EPA 7470A Preparation Method:
EPA 7470A
PaceAnalytical Services -Asheville
Mercury
NO ug/L 0.20
1 07/0612113:20
0710912112:50
7439.97-6
2540C Total Dissolved Solids
Analytical Method: SM 264OC-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
ND mg/L 25.0
1
07/06/21 14:29
300.0 IC Anions 28 Days
Analytical Method: EPA 300,0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
NO mg]L 1.0
1
0710312117:40
14808.79.8
350.1 Ammonia
Analytical Method: EPA350.1 Rev 2.01993
PaceAnalytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
07114/2113:19
7664-41-7
5310B TOC
Analytical Method: SM 53108-2011
Pace Analytical Services - Asheville
Total Organic Carbon
NO ril 1.0
1
07/0912117:54
7440.44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 07/22/2021 09:36 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 19

Pace Analytical Services, LLC
ace fl na11 � ical 2225 eNCRiverside8 04
V li /wllwwrpalc}a'lalbis com Asheville, NC 268n4
[phone]
ANALYTICAL RESULTS
Project: July 2021
Pace Project No.: 92547500
Sample: ASB-01 Lab ID: 92547500002 Collected: 07/01/21 15:21 Received: 07101/21 17:02 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
07/01/21 15:21
Collected By
Mark
1
07/01/21 15:21
Swann
Collected Date
711121
1
07/01/21 15:21
Collected Time
15:21
1
07/01/21 15:21
pH
5.36 Sid. Units
1
07/01/21 15:21
Temperature
22.7 deg C
1
07/01/21 15:21
Static Water Level
9.00 (eel
1
07/01121 15:21
Specific Conductance
0.9 umhos/cm
1
07/01/21 15:21
Oxidation Potential
51.0 my
1
07/01/21 15:21
Oxygen, Dissolved
7.10 mg/L
1
07101/21 15:21
7782-44-7
Turbidity
5.42 NTU
1
07/01/21 15:21
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
Arsenic
ND ug/L 10.0
1 0711312111:50
07113/2122:58
7440-38-2
Chromium
ND ug/L 5.0
1 07113/2111:50
07/13/2122:58
7440-47-3
Iron
1880 ug/L 50.0
1 07113121 11:50
07113/21 22:58
7439-89-6
Lead
ND ug/L 5.0
1 07113/21 11:50
07/13/21 22:58
7439.92-1
Manganese
1770 ug/L 5.0
1 07113/2111:50
07/13/2122:68
7439-96-5
Sodium
28100 ug/L 5000
1 07/13121 11:50
07/13/21 22:58
7440-23-5
6020 MET ICPMS
Analytical Method: EPA 60208 Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Cobalt
4.2 ug/L 1.0
1 07/07/21 13:27
07/07/21 21:29
7440-48-4
7470 Mercury
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
Mercury
NO ug/L 0.20
1 07106/21 13:20
07/09/21 12:52
7439-97-6
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
251 mglL 25.0
1
07/06/21 14:29
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
PaceAnalytical Services -Asheville
Sulfate
8.3 mg/L 1.0
1
07/0312118:26
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mglL 0A0
1
0711412113:21
7664-41-7
5310E TOC
Analytical Method: SM 53108-2011
Pace Analytical Services -Asheville
Total Organic Carbon
NO mglL 1.0
1
(17109121 18:11
7440-44.0
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Dale: 071221202109:36AM
without the written consent of Pace Analytical Services, L-C.
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ANALYTICAL RESULTS
Pace Analytical Sorvices, LLC
2225 Riverside Dr
Asheville, NC 28804
(8281254-7176
Project: July 2021
Pace Project No.: 92547500
Sample: ASE-02 Lab ID: 92547500003 Collected: 07/01/21 15:30 Received: 07/01/21 17:02 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
07101121 15:30
Collected By
Mark
1
07/01/21 15:30
Swann
Collected Date
711121
1
07/01/21 15:30
Collected Time
15:30
1
07/01/21 15:30
pH
5.76 Sid. Units
1
07/01/21 15:30
Temperature
19.0 deg C
1
07/01/21 15:30
Static Water Level
9.15 feet
1
07/01/21 15:30
Specific Conductance
76.5 umhos/cm
1
07101/2115:30
Oxidation Potential
89.0 my
1
07/01/21 15:30
Oxygen, Dissolved
4.18 mg1L
1
07/01/21 15:30
7782-44.7
Turbidity
1.04 NTU
1
07/0112115:30
-
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Arsenic
ND ug/L 10.0
1 07/13121 11:50
07/13/21 23:02
7440-38-2
Chromium
ND uglL 5.0
1 07/13/2111:50
07113/2123:02
7440-47-3
Iron
NO uglL 50.0
1 0711312111:60
07113/2123:02
7439.89-6
Lead
NO ug/L 5.0
1 07113/2111:60
0711312123:02
7439-92-1
Manganese
NO ug/L 5.0
1 0711312111:50
07A 3/2123:02
7439-96.5
Sodium
7890 ug/L 5000
1 07/13/21 11:50
07/13/21 23:02
7440-23.5
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA 3010A
Pace Analytical Services - Asheville
Cobalt
ND ug/L 1.0
1 07/07/2113:27
07107/2121:34
7440-48-4
7470 Mercury
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
-
Mercury
ND ug/L 0.20
1 07/06/2113:20
07/0912112:55
7439-97-6
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
51.0 mg/L 25.0
1
07/06/21 14:29
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
5.0 mg/L 1.0
1 -
07/03121 18:42
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.01993
Pace Analytical Services - Asheville
Nitrogen. Ammonia
NO mglL 0.10
1
07114121 13:22
7664-41-7
5310E TOC
Analytical Method: SM 531OB-2011
Pace Analytical Services - Asheville
Total Organic Carbon
ND mg/L 1.0
1
07/0912118:31
7440-44-0
REPORT OF LABORATORY
ANALYSIS
This report shall not be feproeuced, except in full.
Date: 07/22/202109:36 AM
without the wriden consent of Pace Analytical Services, LLC.
Page 6 of 19

ace Analytical e
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I
QUALITY CONTROL DATA
Project: July 2021
Pace Project No.: 92547500
OC Balch: 631402 Analysis Method: EPA7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92547500001, 92547500002, 92547500003
METHOD BLANK: 3317327 Matrix: Water
Associated Lab Samples: 92547500001, 92547500002, 92547500003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 0710912112:33
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville. NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 3317328
Spike LCS LCS % Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Mercury ug/L 2.5 2.4 95 80.120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3317329
3317330
MS
MSD
92547248010 Spike
Spike
MS MSD
MS MSD % Rao
Parameter Units Result Conc.
Conc.
Result Result
%Rec %Rec Limits RPD Qual
Mercury ug/L ND 2.5
2.5
1.5 0.39
58 14 75-125 117 M1,R1
Results presented on this page are In the units Indicated by the "Units" column except where as alternate unit is presented to the right of the moult.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Dale: 07122/202109:36 AM without the etinen consent of Paw Analytical Services,LLC.
Page 7 of 19

aceAnalytical e
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I
QUALITY CONTROL DATA
Project: July 2021
Pace Project No.: 92547500
QC Balch: 632977 Analysis Method: EPA 601 DO
QC Batch Method: EPA 301 CA Analysis Description: 6010 PAET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92547500001, 92547500002, 92547500003
METHOD BLANK: 3324751
Matrix: Water
Associated Lab Samples:
92547500001, 92547500002, 92547500003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
u9/L
ND
10.0
07/1312122:35
Chromium
ug/L
NO
6.0
0711312122:35
Iron
ug/L
NO
50.0
0711312122:35
Lead
ug/L
NO
5.0
07/13/21 22:35
Manganese
ug/L
NO
5.0
07113/2122:35
Sodium
ug/L
NO
5000
07113/2122:35
LABORATORY CONTROL SAMPLE: 3324752
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Spike
LCS
LCS
%Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Arsenic
ug/L
500
503
101
80-120
Chromium
ug/L
600
516
103
80-120
Iron
uglL
5000
5230
105
80-120
Lead
uglL
500
509
102
80-120
Manganese
ug/L
500
511
102
80-120
Sodium
ug/L
5000
5330
107
80-120
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
3325555
3325566
MS
MSD
92547600001
Spike
Spike
MS
MSD
MS
MSD
% Rae
Parameter
Units
Result
Cone.
Cone.
Result
Result
%Rec
%Rec
Limits
RPD Qual
Arsenic
ug/L
ND
500
500
494
495
98
98
75-125
0
Chromium
ug1L
34.2
500
500
585
585
110
110
75-125
0
Iron
ug/L
30700
5000
5000
4970
4970
514
-514
75-125
0 Mt
Lead
ug/L
11.6
500
500
481
484
94
95
75-125
1
Manganese
ug1L
1680
500
50o
499
499
-237
-237
75-125
0 M7
Sodium
ug/L
29900
5000
5000
10700
10809
-383
-381
75.125
1 M11
Results presented on this page are in the units indicated by the 'UmW column except where an alternato unit Is presented to the right or the rvauh.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Dale: 07/22/2021 09:36 AM without the wdhen consent of Pace Analytical Services, LLC.
Page 8 of 19

aceAnalytical e
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QUALITY CONTROL DATA
Project: July 2021
Pace Project No.: 92547500
QC Balch: 631774 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92547500001, 92547500002, 92547500003
METHOD BLANK: 3318803 Matrix: Water
Associated Lab Samples: 92547500001, 92547500002, 92547500003
Blank Reporling
Parameter Units Result Limit Analyzed Qualifiers
Cobalt uglL NO 1.0 0710712119:29
LABORATORY CONTROL SAMPLE: 3318804
Spike
Parameter Units Cone.
Cobalt ug/L 50
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LCS LCS % Rec
Result %Rec Limits Qualifiers
50.2 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3318805 3318806
MS MSD
92647248001 Spike Spike MS MSD MS MSD % Rae
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual
Cobalt ug/L ND 50 50 49.2 48.2 98 96 75-125 2
Results presented on this page are In the units Indicated by the "units' column except where an alternate unit Is pmsentod to the nglit of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull.
Date: 07/22/202109:36 AM without the written consent or Pace Analytical Services,LLC.
Page 9 of 19

.00-41111
aceAnalXical e
anvw.pacelabs.com
QUALITY CONTROL DATA
Project: July 2021
Pace Project No.: 92547500
QC Batch: 631478 Analysis Method: SM 2540C•2011
QC Batch Method: SM 254OC-2011 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92547500D01, 92547500002. 92547500003
METHOD BLANK: 3317514 Matrix: Water
Associated Lab Samples: 92547500001, 92547500002.92547500003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids mglL NO 25.0 07106/21 14:29
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville. NC 26804
[phone]
LABORATORY CONTROL SAMPLE: 3317515
Spike LCS LCS % Rec
Parameter Units Conic. Result %Rec Limits Qualifiers
Total Dissolved Solids mglL 250 252 101 90-110
SAMPLE DUPLICATE: 3317516
92547250001 Oup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mglL 703 781 11
SAMPLE DUPLICATE: 3317517
92547567001 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg1L 11200 10800 5
Results presented on this peso are In the units Indicated by the "Units^ column except whom an altemate unit is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 07I22y2021 09:36 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 19

ace Analytical"
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NO 28804
[phone]
Project: July 2021
Pace Project No.: 92547500
QC Batch: 631408
Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993
Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services
-Asheville
Associated Lab Samples: 92547500001, 92547500002,
92547500003
METHOD BLANK: 3317347
Matrix: Water
Associated Lab Samples: 92547500001, 92547500002, 92547500003
Blank Reporting
Parameter Units
Result Limit
Analyzed Oualifiers
Sulfate mg/L
NO 1.0
07/03/2113:05
LABORATORY CONTROL SAMPLE: 3317348
Spike LCS
LCS % Rae
Parameter Units
Cone. Result
%Rec Limits
Qualifiers
Sulfate mg/L
50 50.4
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3317349 3317350
MS MSD
92547372001
Spike Spike MS
MSD MS
MSD
%Rec
Parameter Units Result
Corl Cone. Result
Result %Rec
%Rec
Limits RPD Qual
Sulfate mg/L 43.0
5o 50 96.1
96.5 106
107
90.110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3317351 3317352
MS MSD
92547500001
Spike Spike MS
MSD MS
MSD
% Rae
Parameter Units Result
Conc. Cone. Result
Result %Rec
%Rec
Limits RPD Qual
Sulfate mg/L NO
50 50 52.6
53.0 105
105
9D.110 1
Results presented on thls page are In the units indicated by the "Units' column except where an alternate unit is presented to the right of Iho result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Dale: 07/2212021 09:36 AM without the wnuen consent of Pace Analytical services. LLC.
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aceAnapical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville. NC 28804
(828l2544M
Project:
July 2021
Pace Project No.:
92547500
QC Batch:
633108
Analysis Method: EPA 350.1 Rev 2.0 1993
OC Batch Method:
EPA 350.1 Rev 2.0 1993
Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92547500001, 92547500002, 92547500003
METHOD BLANK: 3326549 Matrix: Water
Associated Lab Samples: 92547500001, 92547500002, 92547500003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/L ND 0.10 0711412112:66
LABORATORY CONTROL SAMPLE: 3325550
Spike LCS LCS % Rae
Parameter Units Cone. Result %Rec Limits Qualifiers
Nitrogen, Ammonia mg/L 5 5.1 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3325551 3325552
MS MSD
92547315002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qua[
Nitrogen, Ammonia mg/L 2.6 5 5 7.7 7.7 103 103 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3325553 3325554
MS MSD
925473190D1 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result % Rae % Rae Limits RPD Qual
Nitrogen, Ammonia ni NO 5 5 4.9 4.9 97 97 90-110 0
Results presented on this page are In the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This lepon shall not be reproduced, except in full,
Dale: 07122/2021 09:36 AM without the written consent of Pace Analytical Services, I.I.C.
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IceAnaljdical-
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr
Asheville, NC 28904
[phone]
Project: July 2021
Pace Project No.: 92547500
QC Batch: 632255
Analysis Method: SM 5310B.2011
QC Batch Method: SM 531OB-2011
Analysis Description: 6310B TOG
Laboratory: Pace
Analytical Services - Asheville
Associated Lab Samples: 92547500001, 92547500002,
92547500003
METHOD BLANK: 3321332
Matrix: Water
Associated Lab Samples: 92547500001. 92547500002,
92547500003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Total Organic Carbon mglL
NO 1.0
07/1)B/2118:19
LABORATORY CONTROL SAMPLE: 3321333
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
%Rec Limits Qualifiers
Total Organic Carbon mg/L
25 22.9
92 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3321334 3321335
MS MSD
92547470001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc. Conc. Result
Result %Rec °h Rec
Limits RPD Quai
Total Organic Carbon mg/L NO
25 25 24.8
24.9 98 98
90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3321336 3321337
MS MSD
92547471001
Spike Spike MS
MSD MS MSD
%Rec
Parameter Units Result
Conc. Conc. Result
Result %Rec %Rec
Limits RPD Qual
Total Organic Carbon mg/L 3.4
25 25 27.9
28.0 98 99
90.110 1
Results presented on this page are in the units Indicated by the "Unfts' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/22/2021 09:36 AM without the written consent or Pace Analytical Services, L-C.
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QUALIFIERS
Project: July 2021
Pace Project No.: 92547500
DEFINITIONS
DF - Dilution Factor, if reported. represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
POL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP -Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 Is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyses.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
RI RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2226 Riverside Dr.
Asheville. NC 28804
[phone]
Project:
Pace Project No.:
July 2021
92547500
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92647500001
Q88V2
92547500002
ABB-01
92547500003
ASB-02
92547500001
088V2
EPA3010A
632977
EPA6010D
633162
92647500002
ASB-01
EPA3010A
632977
EPA6010D
633162
92547500003
ASB-02
EPA3010A
632977
EPA6010D
633152
92547600001
Q88V2
EPA 3010A
631774
EPA 60208
631954
92547600002
ASB-01
EPA 3010A
631774
EPA6020B
631954
92547500003
ASB-02
EPA3010A
631774
EPA 60208
631954
92547500001
Q88V2
EPA 7470A
631402
EPA 7470A
631623
92547500002
ASB-01
EPA 7470A
631402
EPA 7470A
631623
92647600003
ASB-02
EPA 7470A
631402
EPA 7470A
631623
92647600001
Q88V2
SM 2640C-2011
631478
92547500002
ASB-01
SM 2640C-2011
631478
92547500003
ASB-02
SM 2540C-2011
631478
92547500001
Q88V2
EPA 3DO.0 Rev 2.11993
631408
92547600002
ASB-01
EPA 300.0 Rev 2.1 1993
631408
92647600003
ASB•02
EPA 300,0 Rev 2.11993
631408
92547500001
Q88V2
EPA 350.1 Rev 2.0 1993
633108
92647500002
ASS-01
EPA 350.1 Rev 2.01993
633108
92547500003
ASB-02
EPA 350.1 Rev 2.01993
633108
92547500001
Q88V2
SM 6310B-2011
632255
92647500002
ASB-01
SM 5310E-2011
632255
92547500003
ASB-02
SM 5310B-2011
632255
Date: 07/22/2021 09:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 15 of 19

Document Name: Document Revise) October 2R;2020
<4CBA7)dlylC9l. Sample Condition Upon Rate! pl(SCURI Page 1. of 2
Document No.: Issuing Aulllority:
F•CAR.C5•033•Rev.07 —I Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville f 'r Eden❑ Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicssviille❑ Atlanta❑ Kernersvllle❑
Client Name: VP / Project 71 WO# : 92547500
• •. \ [iJid$drl �C? V�I V 1II(. 4j,Q
Courier: ❑Fed Ex ❑UPS ❑USPS U_=❑C(C(ier—it 11111111111111111111111111
❑Commercial 2Pace rAt--,,'' ❑0ther.____ ,{,'" 92547500
Custody Seat Present? Dyes I,b{No Seals intact? Dyes (yNo \ 6
OMC/Initiah Person Examining Canlenl f:_7`? _ Z 1 7 i
Packing Material: WDubblo Wrap ❑Oubhle Rags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: Dyes ❑No MAIA
❑ IR Gvo ID: Q3 T� 7 Wet ❑Bled ❑None
Type of Ice:
Correction Factor:
Cooler Temp: _� Add/Suldract I'C) iempsllotdd 6e above (rcering to 6'C
[]Samples out a7 temp crim.a. Samples on <o, cooling process
Cooler Temp Corrected('C): ��°C- _ has begun
USDA Regulated Soil ( [gN/A, water sample)
Did samples originate in a quarantine zone within the United States: CA. NY. or SC(che<k mansl7 O�J samn!es originate Nornainrei2n source (intematinnally,
[]Yes ❑No
mtludngHawall and Puerto RituV oyes I,JNo
_
Comments/Oiscrepanry: J__Y
Chain or Custody Present?
s ❑No
❑N/A
San)PICS Arrived wilhin Hold Time?
--Og
jKjYQs
0141A
Short hold Time Analysis I<72 hr,)7
❑re? o n/A
_7. _
Rush Turn Around Time Requested?
Sufficient Volnnle?
Yes Na
___ Lam__?_____...
r(p�y�es !ru
4t-._—_.._
❑11 A
❑H/A ___
d.
____.___.—_ — _.
5. �— .. _
.�._
Conect Containers Used?
n Pate Coainers Used?
Conlalners Intact? •- _-
N1k4�YCI ❑rN
Nye I]No
Yen �INO
[.JN/A
I�N/A
err/A
6.
_
^7.
Dissolved anafysis: Samples Field Filtered?__
Oyes C]No
^Pas
_[Jim/A
s.
Sample labels MatchCOC?
-Includes Date/iimy/ID/AnalYsls hlasr
❑Do
---T___
off/n
9.
i
mix;
Noudspace !it VOA Vials)>5.6mmj?
.�]Yzc (ffifo ❑Ir/A
Trill Blank Prewnt?
Trip Blank Custody Seats Present/
❑Yaw ❑ ie
_[jres [jNo_
pwa
1/A,.
Ile
_ .___.._--.-..-.--..
COMMENTS/SAMPLE DISCREPANCY
FIcld Data Required? []Yes ❑Na
Cl ILntlD ufsplltcontainc_rs_ � ______
ENT NOTIFICATION/RESOLUTION
Pelson contacted: Date/linen:
Project Manager SCURF Review:
Project Manager SRF Review:
Date:
Date:
Page 16 of 19

oocumont Name:
Document Revised: October 28)2020
aceAnalytical •
Sample Condition Upon Recelpl(SCUR)
Page 2 of 2
Document ND.:
Issuing Authority:
F•CAR•CS-033Rev.07
Pace Carolinas Quality Office
*Check mark top half of box If pH and/or dechforination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Conform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHS
**Bottom half of box Is to list number of bottles
Project WO# : 92547500 -
PM: Col Due Date: 07/16/21
CLIENT: 93—DavidsonR
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pH Adjustment Log for Preserved Samples
sample t0
Type of Psetervative
pH upon receipt
Date preservation adjusted
Time preservation
Amoum of Praservative
lot Y
adjusted
added
Note: Whe never there is a discrepancy alCeding Noth Carolina compliancesamples, a copy of this rormwill to sent to the North Caroena DEHNR CerinKapon Vmc"'-C-
Out of hold, incorrect pretelyallve, out of comp, Incorrect container.
Page 17 of 19

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