NC0024911_Groundwater Monitoring Report June 2021_20210721

•QSEWERA0,
CC Metropolitan Sewerage. District
may
OF BUNCOMBE COUNTY, NORTH CAROLINA
�o e�
SB GP
F COUNTY, NONE"
July 21, 2021
Division of Water Resources
Information Processing Unit J
1617 Mail Service Center JUL 2 3 2021
Raleigh, NC 27699-1617
Water AQ Asheville Regional office Regional
Information Processing Unit:
Please find attached the Groundwater Quality Monitoring Reports for June 2021 from The Metropolitan
Sewerage District of Buncombe County (MSD). These monitoring report forms have additional
identification on the Well ID line, MW-05, MW-06R, MW-07, MW-08R, for ease of reference.
Monitoring Well 05 exceeding allowable limits for manganese and pH. Monitoring Well 06R exceeding
allowable limits for manganese, iron, and pH. Monitoring Well 07 exceeded allowable limits for
manganese and pH. Monitoring Well 08R exceeded allowable limits for manganese and iron.
Please do not hesitate to contact me at 828-225-8224 with questions regarding the attached reports.
Sincerely,
I
Roger Edwards
Director of Operations & Pretreatment
MSD of Buncombe County
-Protecting Our Natural Resources-
2028 RIVERSIDE DRIVE, ASHEVILLE, NORTH CAROLINA 28804 TELEPHONE: [phone] FAX: [phone] WEBSITE: www.msdbe.org

GW-59A COMPLIANCE REPORT FORM Permit # NCO024911
(Subndi one each monitoring period with GlY-59 form.)
I
Enter date monitoring results were due. (_07/3112021_) Will this monitoring report (GW-59 and GW-59A)
YES
O
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question 1 or 2 is "YES'; list in the space provided below the well identification numbers) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? Ifthe answer is "Yes", contact the Regional 0irice far guidance.
4
Are any monitored constituents equal to or above the established standards?
YE
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
MW-05 MW-06R MW-07 MW-08R
pH 5.4 pH 5.4 pH 5.9
Mn 9,980 ug/L Mn 176 ug/L Mn 15,000 ug/L
Fe 5,360 ug/L Fe 50,700 ug/L
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is ONO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
MW-06 pH Mn Fa MW416R pH Mn Fe MW-07 pH Mn Fe MW-08R pH Mn Fe
1112/19 5.8 482 ug/L
1012119 5.7 302 ug1L 1012/19 6.1 12,700 ug1L 50,800 ug/L 10/2119 62 10.400 ug/L 2,860 ug/L
112120 5.9 533 ug1L 524 ug/L 1/2/20 6.3 10,000 ug/L 43,000 ug1L 112120 6.2 125 uglL 627 uglL 1/2120 11,700 ug2 18,800 ug/L
618120 5.6 6/8/20 5.5 7,880 ug1L 1,820 ug/L 618120 5.9 308 ug/L 447 ug/L 618120 19,700 ug/L 70.700 u &
10123120 5.4 10/23120 52 9,330 uglL 5,410 ug/L 10/23/20 5.9 831 ug/L 10/23/20 14.800 ug4 61,600 ug/L
1/15120215.6 1/1512021 5.3 8,510 ugIL 1,250 ugIL 1115120216.0 334 ug/L 1/15/2021 20,100 ug1L 69,000 ug/L
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be
reauired to determine the impact the waste disposal system is having at the review and compliance
boundaries surroundina this facility. Failure to do so may subject the permittee to a Notice of Violation.
fines. and/or penalties,
g
The person completing this portion (G W-59A) of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to the address provided at the top of the current G W-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
(Compliaannce Report GpW-59A) is true and complete to the best of my knowledge.
report (Compliance
it oa,U 1�--�iisnx�d 07�2/ �202 /
ig ture of Permittee (or Authorized Agent) D e
GW-59A 12/8/2003

'aceAnalytical
www.pacolainson
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
July 08, 2021
Mr. Roger Edwards
Metropolitan Sewerage District
2028 Riverside Drive
Asheville, NC 28804
RE: Project: MWs 6/24/21
Pace Project No.: 92546332
Dear Mr. Edwards:
Enclosed are the analytical results for sample(s) received by the laboratory on June 24, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
cc: Ms. Shannon Bergeron, Metropolitan Sewerage District
Mr. John Gosnell, Metropolitan Sewerage District
Mr. Chad Ledford, Metropolitan Sewerage District
Mr. Dwayne Martin, Metropolitan Sewerage District
Ms. Cassandra McKnight, MSD of Buncombe County
Patrick Smith, MSD of Buncombe County, NC
Mr. Alan Taylor, Metropolitan Sewerage District
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

aceAnalytical e
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: MWs6/24/21
Pace Project No.: 92546332
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification M E87627
Kentucky UST Certification M 84
Virginia/VELAP Certification M 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
North Carolina Drinking Water Certification M 37712 Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23

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Pace Analytical Services, LLC
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Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project:
MWs 6/24/21
Pace Project No.:
92546332
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92546332001
MW.05
EPA 200.7 Rev 4.41994
SH1
10
PASI-A
EPA 245.1 Rev 3.01994
RDT
1
PASI-A
SM 254OC-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.01993
NGP
1
PASI-A
EPA 353.2 Rev-2.0-1993-MFO
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
92546332002
MW-06R
EPA 200.7 Rev 4.41994
SH1
10
PASI-A
EPA 245.1 Rev 3.0 1994
RDT
1
PASI-A
SM 254OC-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.01993
NGP
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 531 OB-2011
MDW
1
PASI-A
92546332003
MW-08R
EPA 200.7 Rev 4.41994
SHi
10
PASI-A
EPA 245.1 Rev 3.0 1994
RDT
1
PASI-A
SM 254OC-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.01993
NGP
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
92546332004
MW.07
EPA 200.7 Rev 4.41994
SHi
10
PASI-A
EPA 245.1 Rev 3.01994
RDT
1
PASI-A
SM 254OC-2011
JP1
1
PASI-A
EPA 300.0 Rev 2.1 1993
CDC
1
PASI-A
EPA 350.1 Rev 2.01993
NGP
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
SM 4500-CI-E-2011
MDW
1
PASI-A
SM 531OB-2011
MDW
1
PASI-A
PASI-A= Pace Analytical Services -Asheville
PASI-C = Pace Analytical
Services -Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 23

aceAnalytical e
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: MWs 6/24/21
Pace Project No.: 92546332
Sample: MW-05
Parameters
Monitoring Well Data
Performed by
Collected By
Collected Date
Collected -Time - -
pH
Temperature
Static Water Level
Specific Conductance
Odor
Appearance
200.7 MET ICP
Arsenic
Barium
Cadmium
Chromium
Iron
Lead
Manganese
Selenium
Silver
Sodium
245.1 Mercury
Mercury
2540C Total Dissolved Solids
Total Dissolved Solids
300.0 IC Anions 28 Days
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
363.2 Nitrogen, N021NO3 unpres
Nitrogen, Nitrate
Date: 07/08/2021 02:53 PM
ANALYTICAL RESULTS
Lab ID: 92546332001 Collected: 06/24/21 10:36 Received: 06/24/21 16:22 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method:
Pace Analytical Services - Charlotte
Pace
1
06/29/21 08:14
Danielle
1
06/29/21 08:14
Schuler
6/24121
1
06/29/21 08:14
10:3c
1
nni7a/91 AAAA
5.43 Sid. Units
1
06/29/21 08:14
15.7 deg C
1
06/29121 08:14
16.63 feet
1
06/29/21 08:14
31.9 umhos/cm
1
06129/2108:14
None
1
06129/21 08:14
Clear
1
06/29/21 08:14
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
ND ug/L
10.0
1
07/06/21 12:05 07/06/21 20:54 7440-38-2
11.8 ug/L
5.0
1
07/06/21 12:05 07/06/21 20:54 7440-39-3
NO ug/L
1.0
1
07/06/21 12:05 07/06/21 20:54 744043-9
ND ug/L
5.0
1
07/06/21 12:05 07/06/21 20:54 7440.47-3
ND ug/L
50.0
1
07/06/21 12:05 07/06/21 20:64 7439-89-6
ND ug/L
5.0
1
07/06/21 12:05 07/06/21 20:54 7439-92-1
8.8 ug/L
5.0
1
07/06/21 12:05 07/06/21 20:54 7439-96.5
NO ug/L
10.0
1
07/06/21 12:05 07/06/21 20:54 7782-49-2
NO ug/L
5.0
1
07/06/21 12:05 07/06/21 20:54 7440-22.4
NO ug/L
5000
1
07/06/21 12:05 07/06/21 20:54 7440-23-5
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
ND ug/L
0.20
1
06/29/21 15:13 06/29/21 18:18 7439-97-6
Analytical Method: SM 254OC-2011
Pace Analytical Services -Asheville
28.0 mg/L
25.0
1
07/01/2107:18
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services -Asheville
-
3.8 mg/L
1.0
1
06/26/2100:32 14808-79-8
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
ND mg/L
0.10
1
07/06/21 10:08 7664-41-7
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
ND mg/L
0.040
1
06/25/2101:24 14797-55-8
REPORT OF LABORATORY ANALYSIS'
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 23

• aceAnalytical e
%, x.panlabr.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: MWs 6/24/21
Pace Project No.: 92546332
Sample: MW-05 Lab ID: 92546332001 Collected: 06/24/21 10:36 Received: 06/24/21 16:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
4500 Chloride Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride 1.4 mg/L 1.0 1 07/01/2119:06 16887-00-6
6310B TOC Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon NU mg 06/29/21-19:A8-7440-44=0
Date: 07/08/2021 02:53 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 5 of 23

Pace Analytical Services, LLC
2225 Riverside Dr.
. ace Analytical 0 Asheville, NC 28804
Ww pscslabsxom [phone]
ANALYTICAL RESULTS
Project: MWs 6/24/21
Pace Project No.: 92546332
Sample: MW-06R Lab ID: 92546332002 Collected: 06/24/21 12:45 Received: 06/24/21 16:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
- Pace
1
06/29/21 08:16
Collected By
Mark
1
06/29/21 08:16
Swann
Collected Date
6/24121
1
06/29/21 08:16
Collected Time
12:46
1
06/29/21 08:16
PH
6.36 Slid. Units
1
06/29/21 08:16
Temperature
26.9 deg C
1
06/29/21 08:16
Static Water Level
10.20 feet
1
06/29/21 08:16
Specific Conductance
273.1 umhos/cm
1
06/29/21 08:16
Odor
None
1
06/29/21 08:16
Appearance
Clear
1
06/29/21 08:16
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Arsenic
ND ug/L
10.0
1
07/06/21 12:05 07/06/21 20:57 7440-38-2
Barium
67.0 ug/L
5.0
1
07/06/21 12:05 07/06/21 20:57 7440-39-3
Cadmium
ND ug/L
1.0
1
07/06/21 12:05 07/06/21 20:57 7440-43-9
Chromium
ND ug/L
5.0
1
07/06/21 12:05 07/06/21 20:57 7440-47.3
Iron
6360 ug/L
50.0
1
07/06/21 12:05 07/06/21 20:57 7439-89-6
Lead
ND ug/L
5.0
1
07/06/21 12:05 07/06/21 20:57 7439-92-1
Manganese
9980 ug/L
5.0
1
07/06/21 12:05 07/06/21 20:57 7439-96-5
Selenium
ND ug/L
10.0
1
07/06/21 12:05 07/06/21 20:57 7782.49-2
Silver
ND ug/L
5.0
1
07/06/21 12:05 07/06/21 20:57 7440-22-4
Sodium
15600 ug/L
5000
1
07/06/21 12:05 07/06/21 20:67 7440-23.5
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
ND ug/L
0.20
1
06/29/21 15:13 06/29/21 18:20 7439-97-6
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
PaceAnalytical Services - Asheville
Total Dissolved Solids
177 mg/L
25.0
1
07/01/21 07:18
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
84.8 mg/L
1.0
1
06/2612100:45 14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
0.18 mg/L
0.10
1
07/06/2110:10 7664-41-7
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.082 mg/L
0.040
1
06/25/21 01:28 14797-55-8
REPOR-T-OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 07/08/2021 02:53 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 23

'aceAnalytical e
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: MWs 6/24/21
Pace Project No.: 92546332
Sample: MW-06R Lab ID: 92546332002 Collected: 06/24/21 12:45 Received: 06/24/21 16:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500 Chloride
Analytical Method: SM 4500-CI•E-2011
Pace Analytical Services -Asheville
Chloride
9.7 mg/L
6310B TOC
Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
110tal-01TIOITC11iT on
ND ma
Date: 07/08/2021 02:53 PM
1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
07/01 /21 19:07 16887.00-6
Page 7 of 23

Pace Analytical Services, LLC
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aceAnalytical Asheville, NC 28804
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ANALYTICAL RESULTS
Project: MWs 6/24/21
Pace Project No.: 92546332
Sample: MW-08R Lab ID: 92646332003 Collected: 06/24/21 14:40 Received: 06/24/21 16:22 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
06/29/21 08:17
Collected By
Danielle
1
06/29/21 08:17
Schuler
Collected Date
6124121
1
06/29/21 08:17
Collected Time
15:27
1
06/29/21 08.17
pH
6.67 Std. Units
1
06/29/21 08:17
Temperature
22.0 deg C
1
06/29/21 08:17
Static Water Level
10.33 feet
1
06/29/21 08:17
Specific Conductance
554 umhos/cm
1
06/29/21 08:17
Odor
None
1
06/29/21 08:17
Appearance
Yellow-
1
06/29/21 08:17
orange to
Clear
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services - Asheville
Arsenic
NO ug/L
10.0
1
07/06/21 12:05 07/06/21 21:01 7440-38-2
Barium
40.4 ug/L
5.0
1
07/06/21 12:05 07/06/21 21:01 7440-39-3
Cadmium
NO ug/L
1.0
1
07/06/21 12:05 07/06/21 21:01 7440-43-9
Chromium
NO ug/L
5.0
1
07/06/21 12:05 07/06/21 21:01 7440-47.3
Iron
50700 ug/L
50.0
1
07/06/21 12:05 07/06/21 21:01 7439.89.6
Lead
NO ug/L
5.0
1
07/06/21 12:05 07/06/21 21:01 7439-92-1
Manganese
16000 ug/L
25.0
5
07/06/21 12:05 07/07/21 16:11 7439-96-5
Selenium
NO ug/L
10.0
1
07/06/21 12:05 07/06/21 21:01 7782.49-2
Silver
NO ug/L
5.0
1
07/06/21 12:05 07/06/21 21:01 7440-22-4
Sodium
23100 ug/L
5000
1
07/06/21 12:05 07/06/21 21:01 7440-23-5
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
NO ug/L
0.20
1
06/29/21 15:13 06/29/21 18:22 7439.97.6
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
240 mg/L
25.0
1
07/01/21 07:19
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
93.0 mg/L
1.0
1
06/26/2100:59 14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
0.46 mg/L
0.10
1
07/06/21 10:11 7664-41-7
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
NO mg/L
0.040
1
06/25/21 01:33 14797.55-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/08/2021 02:53 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 23

aceAnalytical e
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: MWs 6/24/21
Pace Project No.: 92546332
Sample: MW-08R Lab ID: 92546332003 Collected: 06/24/21 14:40 Received: 06/24/21 16:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
4600 Chloride Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride 20.0 mg/L 1.0 1 07/01/2119:10 16887-00-6
5310B TOC Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Date: 07/08/2021 02:53 PM
-REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qual
Page 9 of 23

aceAnalytical e
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Pace Analytical Services, LLC
2226 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: MWs 6/24/21
Pace Project No.: 92546332
Sample: MW-07 Lab ID: 92646332004 Collected: 06/24/21 15:30 Received: 06/24/21 16:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data Analytical Method:
Pace Analytical Services - Charlotte
Performed by Pace 1 06/29/21 08:19
Collected By Mark 1 06/29/21 08:19
Swann
Collected Date 6124121 1 06/29/21 08:19
pH
5.91 Sid. Units
1
06/29/21 08:19
Temperature
27.1 deg C
1
06/29121 08:19
Static Water Level
10.86 feet
1
06/29/21 08:19
Specific Conductance
370.5 umhos/cm
1
06/29/21 08:19
Odor
None
1
06/29/21 08:19
Appearance
Clear
1
06/29/21 08:19
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services -Asheville
Arsenic
ND ug/L
10.0
1
07/06/21 12:05 07106/21 21:04 7440-38-2
Barium
40.7 ug/L
5.0
1
07/06/21 12:05 07/06/21 21:04 7440-39-3
Cadmium
ND ug/L
1.0
1
07/06/21 12:05 07/06/21 21:04 7440-43-9
Chromium
6.1 ug/L
5.0
1
07/06/21 12:05 07/06/21 21:04 7440-47-3 -
Iron
109 ug/L
50.0
1
07/06/21 12:05 07/06/21 21:04 7439-89-6
Lead
ND ug/L
5.0
1
07/06/21 12:05 07/06/21 21:04 7439-92-1
Manganese
176 ug/L
5.0_
1
07/06/21 12:05 07/06/21 21:04 7439-96-5
Selenium
ND ug/L
10.0
1
07/06/21 12:05 07/06/21 21:04 7782-49.2
Silver
ND ug/L
5.0
1
07/06/21 12:05 07/06/21 21:04 7440.22-4
Sodium
10300 ug/L
5000
1
07/06/21 12:05 07/06/21 21:04 7440-23-5
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
Pace Analytical Services -Asheville
Mercury
NO ug/L
0.20
1
06/29/21 15:13 06/29/21 18:25 7439-97-6
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
228 mg/L
25.0
1
07/01/21 07:19
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Pace Analytical Services -Asheville
Sulfate
97.8 mg/L
1.0
1
06/26/2101:12 14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
NO mg/L
0.10
1
07/06/2110:13 7664.41-7
363.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0
1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.67 mg/L
0.040
1
06/25/21 01:35 14797-55.8
REPORT OF LABORATO ARALYM
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Date: 07/08/2021 02:53 PM without the written consent of Pace Analytical Services, I.I.C. Page 10 of 23

aceAnalytical e
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ANALYTICAL RESULTS
Project: MWs 6/24/21
Pace Project No.: 92546332
Sample: MW-07 Lab ID: 92646332004 Collected: 06/24/21 15:30 Received: 06/24/21 16:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500 Chloride Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride 6.2 mg/L 1.0 1 07/0112119:11 16887-00.6
6310E TOC Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
- T6tah0rganicCTrrb on 3�rrg/L I.0 1 06/29/29-20.,40-7440-44-0 --
Date: 07/08/2021 02:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C.
Page 11 of 23

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: MWs 6/24/21
Pace Project No.: 92546332
QC Batch: 630370 Analysis Method: EPA 245.1 Rev 3.0 1994
QC Batch Method: EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury
Laboratory: PaceAnalytical Services -Asheville
Associated Lab Samples: 92546332001,92546332002,92546332003,92546332004
METHOD BLANK: 3312096 Matrix: Water
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
LABORATORY CONTROL SAMPLE: 3312097
Spike
Parameter Units Conc.
Mercury ug/L 2.5
LCS LCS % Rec
Result % Rao Limits Qualifiers
2.5 100 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3312098 3312099
MS MSD
92546309001 Spike Spike MS MSD MS MSD % Rao
Parameter Units Result Cone. Conc. Result Result %Rec %Rec Limits RPD Qual
Mercury ug/L NO 2.5 2.5 2.5 2.4 98 94 70-130 4
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3312100 3312101
MS MSD
92546363001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.4 2.4 94 95 70-130 0
Results presentee on this page are in the units Intl icatee by the "Units' column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/08/2021 02:53 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 23

m
aceAnalytical
www.pscelsb,.cam
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: MWs 6/24/21
Pace Project No.: 92546332
QC Batch: 631459 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
METHOD BLANK: 3317466 Matrix: Water
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Arsenic
ug/L
NO
10.0
07/06/2119:39
Barium
ug/L
NO
5.0
07/06/2119:39
Cadmium
ug/L
NO
1.0
07/06/2119:39
Chromium
ug/L
NO
5.0
07/0612119:39
Iron
ug/L
NO
50.0
07/06/2119:39
Lead
ug/L
NO
5.0
07/06/2119:39
Manganese
ug/L
ND
5.0
0710612119:39
Selenium
ug/L
ND
10.0
07/06/2119:39
Silver
ug/L
NO
5.0
07/0612119:39
Sodium
ug/L
NO
5000
07/06/2119:39
LABORATORY CONTROL SAMPLE:
Parameter
3317467
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rao
Limits Qualifiers
Arsenic
ug/L
500
488
98
85-115
Barium
ug/L
500
483
97
85-115
Cadmium
ug/L
500
485
97
85-115
Chromium
ug/L
500
496
99
85.115
Iron
ug/L
5000
4560
91
85-115
Lead
ug/L
500
472
94
85-115
Manganese
ug/L
500
485
97
85-115
Selenium
ug/L
500
468
94
85-115
Silver
ug/L
250
243
97
85-115
Sodium
ug/L
5000
4990J
100
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
3317468
MS
92546151001
Spike
Parameter
Units
Result
Conc.
Arsenic
ug/L
ND
500
Barium
ug/L
15.8
500
Cadmium
ug/L
NO
500
Chromium
ug/L
7.3
500
Iron
ug/L
849
5000
Lead
ug/L
NO
500
Manganese
ug/L
79.0
500
Selenium
ug/L
NO
500
3317469
MSD
Spike
MS
MSD
MS
MSD
%Rec
Conc.
Result
Result
%Rec
%Rec
Limits
RPD
500
506
500
100
99
70.130
1
500
502
488
97
94
70.130
3
500
494
483
99
97
70.130
2
500
510
498
101
98
70-130
2
5000
5440
5320
92
89
70-130
2
500
474
467
94
93
70-130
2
500
564
547
97
94
70.130
3
500
469
460
94
92
70.130
2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
Qual
REPORT OF LABORATORY ANALYSIS
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Date: 07/08/2021 02:63 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 23

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: MWs 6/24121
Pace Project No.: 92546332
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3317468 3317469
MS MSD
92546151001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Silver ug/L ND 250 250 247 241 99 96 70-130 2
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3317470
3317471
MS
MSD
546318001—SpikeSpikeMS
MSDMSMSD—%Rem
-- - -
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Qual
Arsenic
ug/L
NO
500
500
499
499
100
100
70-130
0
Barium
ug/L
22.8
500
500
485
485
92
92
70-130
0
Cadmium
ug/L
ND
500
500
481
484
96
97
70-130
1
Chromium
ug/L
ND
500
500
484
491
97
98
70-130
1
Iron
ug/L
63.8
5000
5000
4450
4490
88
89
70-130
1
Lead
ug/L
ND
500
500
452
456
90
91
70-130
1
Manganese
ug/L
183
500
500
646
654
93
94
70-130
1
Selenium
ug/L
ND
500
500
481
485
96
96
70-130
1
Silver
ug/L
ND
250
250
242
242
97
97
70.130
0
Sodium
ug/L
13100
5000
5000
17700
17800
92
94
70-130
1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the rosulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced except in full,
Date: 07/08/2021 02:53 PM without the written consent of Pace Analytical Services, U.C.
Page 14 of 23

aceAnalXicala
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: MWs 6124/21
Pace Project No.: 92546332
QC Batch: 630835 Analysis Method: SM 254OC-2011
QC Batch Method: SM 254OC-2011 Analysis Description: 2540C Total Dissolved Solids
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546332001. 92546332002, 92546332003, 92546332004
METHOD BLANK: 3314308 Matrix: Water
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Dissolved Solids mg/L ND 25.0 07/01/21 07:18
LABORATORY CONTROL SAMPLE: 3314309
Spike
Parameter Units Conc.
Total Dissolved Solids mg/L 250
SAMPLE DUPLICATE: 3314310
92546332001
Parameter Units Result
Total Dissolved Solids mg/L 28.0
LCS LCS % Rao
Result %Rec Limits Qualifiers
252 101 90.110
Dup
Result RPD Qualifiers
35.0 22
Results presented on this page are in the units indicated by the "Units" column except where an allemate unit is presented to the right or the result.
Date: 07/08/2021 02:53 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical services, LLC.
Page 15 of 23

-a eAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28604
[phone]
QUALITY CONTROL DATA
Project: MWs 6/24/21
Pace Project No.: 92546332
QC Batch: 629647 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
METHOD BLANK: 3309102 Matrix: Water
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
Blank Reporting
Parameter Units Result Limit Analyzed
Sulfate
Qualifiers
LABORATORY CONTROL SAMPLE: 3309103
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rao Limits Qualifiers
Sulfate mg/L 50 48.3 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3309104 3309105
MS MSD
92546312002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Sulfate mg/L 75.9 50 50 114 112 75 73 90-110 1 M1
Results presented on this page are in the units Indlcaled by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSTS -
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Date: 07/08/2021 02:53 PM without the written consent of Pace Analytical Services, LLC.
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aceAnaljftal e
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: MWs 6/24/21
Pace Project No.: 92546332
QC Batch: 631405 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
METHOD BLANK: 3317337 Matrix: Water
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/L ND 0.10 07/06/21 09:33
LABORATORY CONTROL SAMPLE: 3317338
Spike LCS LCS
Parameter Units Cone. Result %Rec
Nitrogen, Ammonia mg/L 5 5.0 100
% Rae
Limits Qualifiers
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3317339 3317340
MS MSD
92546134001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone, Cone. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 0.11 5 5 5.0 4.9 98 96 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3317341 3317342
MS MSD
92546135001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 11.2 5 5 16.0 15.9 95 93 90.110 1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Date: 07/08/2021 02:53 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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• aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 2BB04
[phone]
QUALITY CONTROL DATA
Project: MWs 6/24/21
Pace Project No.: 92546332
QC Batch: 629527 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546332001
METHOD BLANK: 3308448
Associated Lab Samples: 92646332001
Parameter Units
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
LABORATORY CONTROL SAMPLE: 3308449
Spike LCS LCS % Rae
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 103 90.110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3308450 3308451
MS MSD
92546306001 Spike Spike MS MSD MS MSD % Rae
Parameter Units Result Cone. Cone. Result Result % Rae % Rae Limits RPD Qua]
Nitrogen, Nitrate mg/L 0.11 1.5 1.5 1.6 1.6 101 99 90.110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3308452 3308453
MS MSD
92546191002 Spike Spike MS MSD MS MSD % Rae
Parameter Units Result Cone. Cone. Result Result % Rae % Rae Limits RPD Qual
Nitrogen, Nitrate mg/L 0.37 1.5 1.5 1.8 1.8 98 98 90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/08/2021 02:53 PM without the written consent of Pace Analytical Services, LLC.
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aceAnalXical e
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: MWs 6/24/21
Pace Project No.: 92546332
QC Batch: 629528
Analysis Method:
QC Batch Method: EPA 353.2 Rev 2.0 1993
Analysis Description:
Laboratory:
Associated Lab Samples: 92546332002, 92546332003, 92546332004
METHOD BLANK: 3308454
Matrix: Water
Associated Lab Samples: 92546332002, 92546332003, 92546332004
Blank Reporting
Parameter Units
Result Limit
Nitrogen, Nitrate
mg/L
LABORATORY CONTROL SAMPLE: 3308455
Parameter Units
Nitrogen, Nitrate mg/L
EPA 353.2 Rev 2.0 1993
353.2 Nitrate + Nitrite, Unpres.
Pace Analytical Services -Asheville
Analyzed Qualifiers
ND 0,040 06/2512101:26
Spike LCS LCS %Rec
Cone. Result %Rec Limits Qualifiers'
1.5 1.5 99 90-110
MATRIX SPIKE R MATRIX SPIKE DUPLICATE: 3308456
MS MSD
92546332002 Spike Spike
Parameter Units Result Cone. Cone.
Nitrogen, Nitrate mg/L 0.082 1.5 1.5
3308457
MS MSD MS MSD % Rec
Result Result % Rec % Rec Limits RPD
1.5 1.6 96 99 90-110 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Dale: 07/08/2021 02:53 PM
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: MWs 6/24/21
Pace Project No.: 92546332
QC Batch: 631037 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
METHOD BLANK: 3316463 Matrix: Water
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg/L NO 1.0 07101/2118:43
LABORATORY CONTROL SAMPLE: 3315464
Spike LCS LCS % Rae
Parameter Units Cone. Result %Rec Limits Qualifiers
Chloride mg/L 20 21.1 105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3315465
MS MSD
92545692001 Spike Spike
Parameter Units Result Cone. Cone.
Chloride mg/L 203 10 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3315467
MS MSD
92546016001 Spike Spike
Parameter Units Result Cone. Cone.
Chloride mg/L 160 10 10
3315466
MS MSD
Result Result
204 213
3315468
MS MSD % Rae
%Rec %Rec Limits RPD Qual
14 102 90-110 4 M1
MS MSD MS MSD %Rec
Result Result %Rec %Rec Limits RPD Qual
173 168 138 86 90-110 3 M1
Results presented on this page are in the units Ind tested by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS -
This report shall not be reproduced, except in full,
Date: 07/08/2021 02:53 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 23

aceAnalXical
www.pacelabsxom
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: MWs 6/24/21
Pace Project No.: 92546332
QC Batch: 630380 Analysis Method: SM 531OB-2011
QC Balch Method: SM 531OB-2011 Analysis Description: 5310B TOO
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
METHOD BLANK: 3312161 Matrix: Water
Associated Lab Samples: 92546332001, 92546332002, 92546332003, 92546332004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Organic Carbon mg/L ND 1.0 06129/2116:28
LABORATORY CONTROL SAMPLE: 3312162
Parameter
Total Organic Carbon
Spike
Units Cone.
mg/L 25
LCS LCS % Rec
Result % Rec Limits Qualifiers
23.0 92 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3312163 3312164
MS MSD
92545608001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rae Limits RPD Qual
Total Organic Carbon mg/L 10.0 25 25 34.6 34.8 98 99 90.110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3312165 3312166
MS MSD
92646336012 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual
Total Organic Carbon mg/L 3680 25 25 28.5 28.6 99 100 90-110 0
ug/L
Results presented on this page are in the units Ind tested by the "Unite" column except where an alternate unit is presented to the right of the result
Date: 07/08/2021 02:53 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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ace Analytical
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Pace Analytical Services, LLC
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[phone]
QUALIFIERS
Project: MWs 6/24/21
Pace Project No.: 92546332
DEFINITIONS
DF - Dilution Factor, If reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative. data with known Precisionand
bias for a specific analyte in a specific -matrix
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RP.D values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute,
ANALYTE QUALIFIERS
MI Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABO ORYANALYSIS
Date: 07/08/2021 02:53 PM This report shall not be reproduced, except in full,
without the wniten consent of Pace Analytical Services, L-C.
Page 22 of 23

aceAnalytical
ww✓.psxtlses.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
MWs 6/24/21
92546332
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method Batch
92646332001
MW-05
92646332002
MW-06R
92646332003
MW-08R
92546332004
MW-07
92646332001
MW-05
EPA 200.7 Rev 4.4 1994
631459
EPA 200.7 Rev 4.4 1994 631669
92546332002
MW-06R
EPA 200.7 Rev 4.4 1994
631459
EPA 200.7 Rev 4.4 1994 631669
92546332003
MW-08R
EPA 200.7 Rev 4.4 1994
631459
EPA 200.7 Rev 4.4 1994 631669
92546332004
MW-07
EPA 200.7 Rev 4.4 1994
631459
EPA 200.7 Rev 4.4 1994 631669
92546332001
MW-05
EPA 245.1 Rev 3.0 1994
630370
EPA 245.1 Rev 3.0 1994 630402
92546332002
MW-06R
EPA 245.1 Rev 3.01994
630370
EPA 245.1 Rev 3.01994 630402
92546332003
MW-08R
EPA 245.1 Rev 3.0 1994
630370
EPA 245.1 Rev 3.0 1994 630402
92546332004
MW-07
EPA 245.1 Rev 3.0 1994
630370
EPA 245.1 Rev 3.0 1994 630402
92546332001
MW-05
SM 2540C-2011
630835
92546332002
MW-06R
SM 2540C-2011
630835
92546332003
MW-08R
SM 2540C-2011
630835
92546332004
MW-07
SM 2540C-2011
630835
92546332001
MW-05
EPA 300.0 Rev 2.1 1993
629647
92546332002
MW-06R
EPA 300.0 Rev 2.1 1993
629647
92546332003
MW-08R
EPA 300.0 Rev 2.1 1993
629647
92646332004
MW-07
EPA 300.0 Rev 2.1 1993
629647
92646332001
MW-05
EPA 350.1 Rev 2.01993
631405
92646332002
MW-06R
EPA 350.1 Rev 2.01993
631405
92546332003
MW-0811
EPA 350.1 Rev 2.01993
631405
92546332004
MW-07
EPA 350.1 Rev 2.01993
631405
92646332001
MW-05
EPA 353.2 Rev 2.01993
629527
92546332002
MW-06R
EPA 353.2 Rev 2.0 1993
629528
92546332003
MW-08R
EPA 353.2 Rev 2.0 1993
629528
92646332004
MW-07
EPA 353.2 Rev 2.0 1993
629528
92546332001
MW-05
SM 4500-CI-E-2011
631037
92646332002
MW-06R
SM 4500-CI-E-2011
631037
92646332003
MW-08R
SM 4500-CI-E-2011
631037
92546332004
MW-07
SM 4500-CI-E-2011
631037
92546332001
MW-05
SM 5310B-2011
630380
92546332002
MW-06R
SM 5310B-2011
630380
92546332003
MW-08R
SM 5310B-2011
630380
92546332004
MW-07
SM 5310B-2011
630380
Date: 07/08/2021 02:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the whiten consent of Pace Analytical Services, LLC.
Page 23 of 23

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Document Name: Field data Sheet
Date Issued: November 27, 2018
Page: 1 of
_.� $GEA7Td }'i16aY
Document Number: F-CAR-PLD-001-rev.02
Issuing Authority: Pace Humersville Quality
office
Field Data Sheet
/h
Name and Affiliation (Sampler(s):
Name and Affiliation (Inspector):
Well Information
Well ID: i� �f/' �J' Well Locked:
Well Diameter:
;l 1i
Total Well Depth: �`� ft
Static Water Level: l�ft.
Height of Water Column: �i5 i ft
_Project A y'V
:ld Data Sheet Review:
Date: ' 6 - a - t f By:
NO)
Construction: Steel/Stainless Steel)
Multi Factor*: /bJ r(Radius/12)2x3.14x7.48]
Casing V olume: I AD /5 / gallons
Cal. 3 Volumes: 6 0 t f gallons
Pump -Intake:- _ —1 ,1_ ft
Purge Information
Date Purged:_Start: /000 Finish: lO f Purge Rate: O W JM to
a
Purging Method: P ^ sa r Total Volume Purged: 1 ° `' (gallons% l�
Sampling Information
Date CollectedTime Collected: Qm)
/ yet
Sampling Equipment Used: Instrument ID: 0) 11
Bottle Type
3Pmj tL
'i I- 417, L
tFOJ—,,L
3 d - /
Preservation
NoVP
RAI l
yiai�4) � i
Analysis Required
%AS M/o ✓ Cl' JJV
Field Measurements/Observations
Sample Temp (°C): 15 • � Time: 10 3 Turbidity (ntu): l ' I Time: PRO
Diss Oxy (mg/L): S ' Cj Time:
I D 3
Fe 2+ mg/L: T'
Specific Cond. (uS): 3 )' y Time:
1 D 31g
Res. Cl (mg/L)/(µg/L)-----� e.
Sample pH (s.u.): S ' i 3 Time:
) 6 3(o
Odor: J l h v_ Time: t)& _
_ox ( ..mV): - r UJ Time:
ReD� D �'
)p 3(v
Appearance: C I M K Time: 1 a 3(9 ...
ReDox (EH value):YSI ProPlus +200mV
T ` b
Other: I Me:
General/Weather Observations: rJ cr D
c/c z c a, -�- A(
(sunny/cloudy/rainy) Temp.-7 o (°F) Wind 0- k (mph)
Sampler Sign
Stabilization
Time
Purged
Temp.
CC)
Diss Oxy.
(mg/L)
Cond,
(US)
pH (s.u.)
ReDox
Turbidity
removed
(gallons mis
Watei0ther
level (
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Document Name:
Document Issued: March 8, 2019
Field Data Sheet
Pag"Lof?—
CEi3Y731yIhL�il
� -
j
Document Number:
F-CAR-FLD-001.rev.03
Issueing Authority:
Pace Huntersville Quality Office
p „ ��
I✓ I
+ WeE Dia tai
i
Client:
ll 7
Location:�l�V'�I�
'p n�
'"��
I �l`}1.T7
Project: I
i
Well ID:
Reviewed.Date_and By;
6
Stabilization Test
8
Time
Purged
Temp.
(°C)
Diss Oxy.
(mg/L)
Spec.
Cond.
(us)
pH (s.u.)
ReDox (mV)
Turbidity
(ntu)
Volume Removed
(gallons�L)
circle one
Water level
(ft)
Other
10 5
Is_q
1.N�i
3-:).6
5,3;L
9w3>
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1030
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Date Imed: November
p�_,/�Document Name: Field data Sheet Page: 1 of �
l 5a�y70ef1D'aIYlCn^1 Issvv�g Authority: Pace Hunh
Document Number: F-CAR-FLD-001-xev.02 Office
Client: Location: 4 l i.t.v./de Project
Name and Affiliation (Sampler(s): Ig ? S Field Data Sheet Review:
Name and Affiliation (Inspector): Date: _._ By
Well Info Trmation
Well ID: Mt, - o y2 Well Locked:. / NO)
Well Diameter: 'L ' r Construction: 6
7teel/Stainless Steel)
Total Well Depth: %7- c t'F ft MultiFactor*: L) r(Radius/12)20.140481
StatcWater Level: 19ft Casing Volume: �I���, gallons
Height of Water Column: 6 . Z ") ft Cal. 3 Volumes: ; i Z 'gallons
Purge Information
Date Purged: p/�. Start: ii3 C Finish: Purge Rate: 1D0
Purging Method: Pt ,a4'nc-1e Total Volume Purged: 700c (gallons/3'
Sampling Information _
Date Collected: 6 / Lw/ )-I— Time Collected: (am/pm)
Sampling Equipment Used:Pe t Instrument ID: Y s P 6 �? F`f
Bottle Type
3 J4IAT,t
Preservation
AlIz .✓e
NN�s
Ql,aa �'h••-�f
Field Measurements/Observations
Sample Temp (-C): 7 d i Time: 1"tICTurbidity (ntu):
Analysis Required
� D 11 A/73 � Cc -i SsY
3. 0 I. Time: f� 4 -
Diss Oxy (mg/4 O, 6 Time: r Y- — Fe 2+ mg/L:
Specific Cond. (uS): Z 7) / Time: . V r Res. Cl (mg/Ly(µgf i : T me:
S j! Time: F r Odor: N9 L Time: f L
Sample. pH (s.u.): � --f -'z---
g T me: Appearance: Time:
ReDox (iaV): \ 3 C ce n
ReDox (EH value):YSI PIOPlus+20DmV CC) • i Other: �Sme:
General/Weather
Temp.77— C.F) Wind D •S `(mph)
Date:
'/ 6 -1 �- H1
Sampler Signature: I t/'y/ /
acanurzanun
aca*
Time
Temp.
ec.
nd.
p ( )ReDox
H s.u.
TurbidityWatera
OtherPurged
(C)
)
(mV)(ntu)
evel (ft)
�I��
?�,1i.L
jDissoxy-Cond,
S.6!
35,0
2).tqd,3C4�a1.
%rem7ved
a1.1
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Document Name:
Document Issued: March 8, 2019
Field Data Sheet
Page Nf a'"
fr"
(
Document Number:
F-CAR-FLD-001.rev.03
Issueing Authority:
Pace Huntersville Quality Office
Client: ,M 119
Location:
Project:i��/W' j
Well ID: f' j✓ - J 6'`
—Reviewed Date -and -By:
Stabilization Test
E 'lV U Diametex
D ulbp%catiam Factaa'
1
0-0408
1-2
0-0913
1625
0-1080
2
.0-1630
3
03670
j 4
0-6930
6
1.4690_
1#
2 5100
Time
Purged
Temp.Spec.
(°C)
DissOxy.
(mg/L)
Cond.
(US)
pH (s.u.)
ReDox (mV)
Turbidity
(ntu)
Volume Removed
(gallons/mis/L)
circle one
Water level
Water
Ift)
Other
1 o
zy 7
o. r
AJ-0
1�5 1
a '.l
I a.Zj
�fOJo
I0,'f�
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743,9
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Date Issued: November 27, 2018
Document Name: Field data Sheet
Page: l of te
II
J GeA?atytfcai
Issuing Authority: Pace Huntexsville Quality
��
Document Numbez: F-CAR-FLD-001-rev.02
Office
Field Data Sheet
Client: t S,? Location: Project#: A 177l- •%
Name and Affiliation (Sampler(s): DM IField Data Sheet Review:
Name and Affiliation (Inspector):
Well Information
Well ID: /17 V - DeA Well Locked:
Well Diameter: a 11
Construction:
Date: (� _ A i • L /
'NO)
:eel/Stainless Steel)
Total Well Depth: L),OQ ft MultiFactor*:, "0 [^(Radius/12)2x3.14x7.481
S tatic Water Level: /._eft. Casing Volume: f.Da�--I gallons
Height of Water Column: - L- 7 ft Cal. 3 Volumes: 6 f �3 gallons
Pump Intake: /� ft
Purge Information
Date Purged: d / L �. / ?-f Start: 15 05 Finish: I t Purge Rate:
By. /1, /' /
Purging Method Total Volume Purged: ) IO ) (gallont, DS'
Sampling_htformation
Date Collected: p � /�Lyj a 6 i Time Collected: 's 3 0 (am/pm)
Sampling Equipment Used: Instrument ID:O X 1 / 64"
Bottle Type
2i e L Aj
qs7,�
l P�gsTr �
Preservation
A/9 wc— .
&JOY
Analysis Required
71o%/✓, Cc - rD
Nth, (1
A%i(s.✓
�o
Field Measurements/Observations
Sample Temp (°C): 9gl 6 Time: 1, S Turbidity (ntu): Time: I S
Diss Oxy (mg/L): I a 7 Time: ' a
Specific Cond. (uS): S S y Time: 1 S a rI s. Cl m L
Sample pH (s.u.): (O• Time: 1 Sa Odor: AP 0 A-t- Time: (s
_.
ReDox (mV): l� % (% Time: 1 S�_Appearance: V� io TTime: ) S
cle4 �- At e A c{' G:A—f lr1
ReDox (EH value):YSI ProPlus +200mV Other: Time:
(3eneral/Weather Observations:
(sunny/cloudy/rainy) Temp. 1�ff) Wind Q / "(mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
CC)
v
Diss Oxy.
(mg/L)
Spec.
Cond.
(US)
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/@�
Water
level (ft)
Other
11515
1.�
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g4`i
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tT&j
Sob
10 ?
D.
(.o(
5 g
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le,�aceA
Document Name: Field data Sheet
Document Number. F-CAR-FLD-001-rev.02
Page: 1 of I
ig Authority. Pace Huntersville Quality
Office
#:P171.1- w1
Name and Affiliation (Sampler(s):_M l 1 Field Data Sheet Review:
Name and Affiliation (Inspector):—
-Date:
Well Information
Ill
Well ID: Al W a 7 Well Locked: ( / NO)
Well Diameter:
x 't
Total Well Depth: % t "o ft
Static Water Level: /0 ' 2 G ft.
Height of Water Column: 3, I tf- ft
Construction: VC Steel/Stainless Steel)
Multi Factor*: i 4S rRadius/l2)2x3.14x7.48]
Casing Volume: , 4 f/ ? hgallons
Cal. 3 Volumes: —t=pallom
i
By: ---
Purge Information
Date Purged:-b r/ Start: 0 Finish: r 3' Purge Rate: I —0—btivMrs
Purging Method: i'c us ill, � r L Total Volume Purged: � r/ L � (gallons/mis)
Sampling Information
Date Collected: / t�/ I Time Collected: ) (am/pm)
Sampling Equipment Usedh v, s h1 % ' t Instrument ID: y
s_Nf�xgey
Bottle Type Preservation Analysis Required
3 Pt9�Trt ol/i2(/C '6JS , Cc f�/�.d�+sue
AL s„ t Ni+s ri
✓Iq�l PAOSvtiu:'l ?Ov
Field Measurements/Observations �, 3 c
r r ib w.x
SampleTemp(°C): ), • Time: O Turbidity(ntu): Tz>i�e:
Diss Oxy (mg/4 016, Time: l F'f ' Fe 2+ mg/L: 'rime —
Specific Cond. (uS): Time: IOW" Res. Cl (mg/L)/(µg/L): `�1me —
Sample pH (s.u.): r 5 / Time: / If (-O Odor: N o -c Time: /
ReDox (mV): • 9 Time: ilf-rF-,:, Appearance: Time:
ReDox (EH value):YSI ProPlus +200mV a 5 Other:
('ieneral/Weather Observations: Sv,1W h J01 a
(�>i�cloudy/rainy) Temp. — rr ff) Wind 0-/u (mph)
Sampler Signature
Ca u4u....9 n.. Tm{
-------
Time
Purged
--- -- -
Temp. .
(eC)
D ss Ox .
y
(mg/L)
Spec.
Cond.
(US)
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
(gallons/mis)
Water
level (ft)
Other
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30-.s
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