WQ0002927_Residual Annual Report 2021_20220117

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BOONE
BOONE
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Southern
Agricultural
outhern
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Southern
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S[ outhern
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Southern
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Southern
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Southern
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SOUTHERNAG Souther [Southern
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SOUTHERNAG Southern Southem
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SOUTHERNAG1 Southern
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N
21
N
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L 105.0
N
N
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21
N
149.001
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50#
MILORGANITE
50#
MILORGANITE
50#
MILORGANITE
50#
MILORGANITE
50#
MILORGANITE
50#
MILORGANITE
50#
MILORGANITE
50#
MILORGANITE
50#
MILORGANITE
50#
MILORGANITE
50#
MILORGANITE
50#
MILORGANITE
50PRO
50PRO
50PRO
50PRO
50PRO
Henderson
50PRO
50PRO
50PRO
50PRO
50PRO
50PRO
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Watauga Total:
NC Total:
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lorganite
PFNITROGEN FERTILIZER 41
Summary of Sample Results
2021
Parameter
Units
Highest
Day
Annual
Average
Federal
Limit1
Arsenic
mg/kg
9.5
4.1
41
Cadmium
mg/kg
2.7
0.48
39
Copper
mg/kg
290
240
1,500
Lead
mg/kg
40
22
300
Mercury
mg/kg
0.52
0.24
17
Molybdenum
mg/kg
15
10
75
Nickel
mg/kg
42
24
420
Selenium
mg/kg
11
4.2
100
Zinc
mg/kg
880
420
2,800
PCB Aroclors (total)
mg/kg
0.30
0.054
Dioxin Toxic Equivalent2
pg/g
13
5.1
1. Monthly average
3. Dioxin Toxic Equivalent is the sum of the concentrations of various
dioxins, furans, and polychlorinated biphenyls multiplied by individual
toxic equivalency factors, as established by the U.S. Environmental
Protection Agency

P'...MMSD
PARTNERS FOR A CLEANER ENVIRONMENT
January 14, 2022
TO:
FROM: Zach Vogel
Laboratory Project Manager
Memorandum
Brett Kelly, llir Aliji, Dion Doege, and Sam Lieven
COPY: Pamela Bechler, Alfredo Sotomayor, Steve Unger, Sid Arora, Jaime Staufenbeil, Tom
Nowicki, Beth Stroik, Kim Walden, Kori Kenney, Ethan Guyant, Lab File
SUBJECT: Annual Milorganite Report — 2021
Attached is the Annual Milorganite report for the year 2021. The boron and mercury analyses were performed
by Pace Analytical Services, Inc. in Green Bay, Wisconsin (Wisconsin Certification #: 405132750). The nitrogen
profile analyses were performed by Midwest Laboratories in Omaha, Nebraska when listed. All other analyses
were performed by Milwaukee Metropolitan Sewerage District in Milwaukee, WI (Wisconsin Certification #:
241325920, Florida NELAP Certification #: E571010).
There was no Milorganite production on the following dates:
• May 24, 2021
• May 31, 2021
• June 15 through June 17, 2021
• August 29, 2021
• October 5, 2021
• October 9 through October 18, 2021
Please contact the Central Laboratory if there are any questions or comments regarding these data. Thank you.
Data Review By:
Puyide,
Pamela Bechler Date
Laboratory Supervisor
Data/Report Review By:
�4 1` /'1- Zo2 Z
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

MMSD Central Laboratory Certification Outline
Test
Method
Wisconsin DNR
DATCP
Florida (TNI)
Aqueousa
Solid"
Aqueousa
Aqueousa
Solid"
Alkalinity by Colorimetry
EPA 310.2
X
Aluminum by ICP
SW846 6010 C
X
X
Ammonia as N by Colorimetry
SM 4500 NH3 G
X
Ammonia as N by ISE
SM 4500 NH3 D
X
X
Ammonia as N by Titration
SM 4500 NH3 C
X
X
Antimony by ICP
EPA 200.7
X
X
Arsenic by ICP
SW846 6010 C
X
X
Arsenic by ICP
EPA 200.7
X
X
Beryllium by ICP
EPA 200.7
X
Biochemical Oxygen Demand (BOD) by 5-day Assay
SM 5210 B
X
X
Cadmium by ICP
SW846 6010 C
X
X
Cadmium by ICP
EPA 200.7
X
X
Calcium by ICP
EPA 200.7
X
Carbonaceous BOD (cBOD) by 5-day Assay
SM 5210 B
X
Chemical Oxygen Demand (COD) by Colorimetry
SM 5220 D
X
Chloride by Colorimetry
SM 4500 CI- E
X
X
Chlorophyll -a by Colorimetry
SM 10200 H
X
Chromium, Total, by ICP
SW846 6010 C
X
X
Chromium, Total, by ICP
EPA 200.7
X
X
Cobalt by ICP
SW846 6010 C
X
X
Cobalt by ICP
EPA 200.7
X
X
Copper by ICP
SW846 6010 C
X
X
Copper by ICP
EPA 200.7
X
X
E. coil
SM 9223 B
X
Fecal Coliform in Biosolids
EPA 1680
X
Fecal Coliform
SM 9221 E
X
Fecal Coliform
SM 9222 D
X
X
Hardness, Total as CaCO3, by Calculation
SM 2340 B
X
Hexane Extractable Material (HEM, Oil & Grease)
EPA 1664 B
X
X
Iron by ICP
SW846 6010 C
X
X
Iron by ICP
EPA 200.7
X
Kjeldahl Nitrogen, Total, by Colorimetry
EPA 351.2
X
Lead by ICP
SW846 6010 C
X
X
Lead by ICP
EPA 200.7
X
X
Magnesium by ICP
EPA 200.7
X
Manganese by ICP
EPA 200.7
X
X
Molybdenum by ICP
SW846 6010 C
X
X
Molybdenum by ICP
EPA 200.7
X
X
Nickel by ICP
SW846 6010 C
X
X
Nickel by ICP
EPA 200.7
X
X
Nitrate + Nitrite by Colorimetry
EPA 353.2
X
X
Nitrate by Colorimetry
EPA 353.2
X
X
Nitrite by Colorimetry
EPA 353.2
X
X
Organic Carbon, Total (TOC)
EPA 5310 C
X
pH
EPA 9045
X
Phosphorus, Total, by Colorimetry
EPA 365.1
X
X
Phosphorus, Total, by ICP
SW846 6010 C
X
X
Potassium by ICP
SW846 6010 C
X
X
Residue, Fixed (% Ash)
SM 2540 G
X
Residue, Nonfilterable (TSS)
SM 2540 D
X
Residue, Total (%TS)
SM 2540 G
X
X
Residue, Total (TS)
SM 2540 B
X
Residue, Volatile (% VS)
SM 2540 G
X
Residue, Volatile (VS)
SM 2540 E
X
Residue, Volatile, Nonfilterable (VSS)
SM 2540 B
X
Selenium by ICP
SW846 6010 C
X
X
Selenium by ICP
EPA 200.7
X
X
Silica Gel Treated HEM (SGT-I-IEM)
EPA 1664 B
X
X
Silver by ICP
EPA 200.7
X
X
Sulfide, by Titration
40 CFR Part 425
X
Thallium by ICP
EPA 200.7
X
Tin by ICP
EPA 200.7
X
X
Titanium by ICP
EPA 200.7
X
X
Total Coliform
SM 9221 B
X
Vanadium by ICP
EPA 200.7
X
X
Zinc by ICP
SW846 6010 C
X
X
Zinc by ICP
EPA 200.7
X
X
a Non -potable water. b Biosolids, Leachates, Soils, Tissues, and Wastes
Wisconsin Department of Natural Resources (DNR) Laboratory ID: 241325920
Wisconsin Department of Agriculture, Trade and Consumer Protection (DATCP) License Number: 115088
Florida Department of Health, Bureau of Public Health Laboratories (TNI) Laboratory ID: E571010
Revised: 08/11/2021 Page 1 of 1

MMSD
PARTNERS FOI II CLIMB PI11A0111011
ARSENIC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
4.9 mg/kg D.W.
2.8
11
3.
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
5 mg/kg D.W. 2.8 11 3.
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
5.4 mg/kg D.W. 2.8 10 3.
SW846: 6010C MMSD
01/04/21 DM0104/21000488
4 mg/kg D.W. 2.8 11 3.
SW846: 6010C MMSD
01/05/21 DM0105/21000504
5.2 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/06/21 DM0106/21000535
4.4 mg/kg D.W. 2.8 10 3. SW846: 6010C MMSD
01/07/21 DM0107/21000551
4.6 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/08/21 DM0108/21000562
4.3 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/09/21 DM0109/21000581
4.3 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/10/21 DM0110/21000594
3.6 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/11/21 DM0111/21000632
4.9 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/12/21 DM0112/21000648
4.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/13/21 DM0113/21000679
3.3 mg/kg D.W. 2.8 10 3, Q3. SW846: 6010C MMSD
01/14/21 DM0114/21000754
4.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
01/15/21 DM0115/21000765
3.6 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/16/21 DM0116/21000784 3.7 mg/kg D.W. 2.8 10 3. SW846: 6010C MMSD
01/17/21 DM0117/21000797 4.6 mg/kg D.W. 2.8 11 3, Q3.
SW846: 6010C MMSD
01/18/21 DM0118/21000824
< 2.8 mg/kg D.W. 2.8 11
SW846: 6010C MMSD
01/19/21 DM0119/21000842
2.9 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/20/21 DM0120/21000926
4.1 mg/kg D.W. 2.8 10 3. SW846: 6010C MMSD
01/21/21 DM0121/21000942
6.2 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/22/21 DM0122/21000953
< 2.8 mg/kg D.W. 2.8 11
SW846: 6010C MMSD
01/23/21 DM0123/21000972
< 2.8 mg/kg D.W. 2.8 11
SW846: 6010C MMSD
01/24/21 DM0124/21001059
5.4 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/25/21 DM0125/21001088
4.1 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/26/21 DM0126/21001106
4.6 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
01/27/21 DM0127/21001137
4.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
01/28/21 DM0128/21001153
5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
01/29/21 DM0129/21001164
4.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
01/30/21 DM0130/21001304
3.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
01/31/21 DM0131/21001317
3.1 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
02/01/21 DM0201/21001344
4.6 mg/kg D.W. 2.7 10 D2, 3, Q3.
SW846: 6010C MMSD
02/02/21 DM0202/21001397
< 2.8 mg/kg D.W. 2.8 11
SW846: 6010C MMSD
02/03/21 DM0203/21001428
3.3 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
02/04/21 DM0204/21001444
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
02/05/21 DM0205/21001455
4.3 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
02/06/21 DM0206/21001476
3.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
02/07/21 DM0207/21001489
3.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
02/08/21 DM0208/21001609
4.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
02/09/21 DM0209/21001625
3.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
02/10/21 DM0210/21001656
4.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
02/11/21 DM0211/21001672 3.8 mg/kg D.W. 2.8 10 3.
SW846: 6010C MMSD
02/12/21 DM0212/21001706 4.6 mg/kg D.W. 2.8 11 3.
SW846: 6010C MMSD
02/13/21 DM0213/21001725 4.5 mg/kg D.W. 2.8 10 3. SW846: 6010C MMSD
02/14/21 DM0214/21001738
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
02/15/21 DM0215/21001793
4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
Page 1 of 121
SYS/rptlMiloMonthlyDW 10/21/21 q Printed: 1/13/22 14.24

MMSD
PARTNERS FOI II CLIMB Br11A0111011
ARSENIC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
3.5 mg/kg D.W.
2.7
10
3.
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
3.1 mg/kg D.W. 2.8 11 3.
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
3.5 mg/kg D.W. 2.8 11 3.
SW846: 6010C MMSD
02/19/21 DM0219/21001986
3.2 mg/kg D.W. 2.8 10 3.
SW846: 6010C MMSD
02/20/21 DM0220/21002005
3.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
02/21/21 DM0221/21002072
3.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
02/22/21 DM0222/21002230
3.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
02/23/21 DM0223/21002246
6.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
02/24/21 DM0224/21002281
3.5 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
02/25/21 DM0225/21002320
3.1 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
02/26/21 DM0226/21002386
3.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
02/27/21 DM0227/21002405
3.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
02/28/21 DM0228/21002478
3.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/01/21 DM0301/21002611
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/02/21 DM0302/21002629
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/03/21 DM0303/21002660 4.8 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
03/04/21 DM0304/21002717 6.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/05/21 DM0305/21002728
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/06/21 DM0306/21002747
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/07/21 DM0307/21002858
3.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/08/21 DM0308/21003336
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/09/21 DM0309/21003371
5.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/10/21 DM0310/21003402
3.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/11/21 DM0311/21003456
4.1 mg/kg D.W. 2.7 10 3, Q3. SW846: 6010C MMSD
03/12/21 DM0312/21003522
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/13/21 DM0313/21003541
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/14/21 DM0314/21003554
4.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/15/21 DM0315/21003747
3.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/16/21 DM0316/21003801
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/17/21 DM0317/21003878
4.4 mg/kg D.W. 2.7 10 3, Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/19/21 DM0319/21003905
3.7 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
03/20/21 DM0320/21004076
3.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/21/21 DM0321/21004093
3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/22/21 DM0322/21004120
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/23/21 DM0323/21004136
4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/24/21 DM0324/21004167
4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/25/21 DM0325/21004242
3.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
03/26/21 DM0326/21004253
3.3 mg/kg D.W. 2.8 10 3. SW846: 6010C MMSD
03/27/21 DM0327/21004272
3.4 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
03/28/21 DM0328/21004285
3.3 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
03/29/21 DM0329/21004312 3.7 mg/kg D.W. 2.8 11 3.
SW846: 6010C MMSD
03/30/21 DM0330/21004388 3.3 mg/kg D.W. 2.8 11 3.
SW846: 6010C MMSD
03/31/21 DM0331/21004600 3.9 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
04/01/21 DM0401/21004616
2.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
04/02/21 DM0402/21004627
3.3 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
Page 2 of 121
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MMSD
PARTNERS FOI A CLEANER DI10111M
ARSENIC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
4.5 mg/kg D.W.
2.7
10
3.
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
4.4 mg/kg D.W. 2.7 10 3.
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
< 2.8 mg/kg D.W. 2.8 10
SW846: 6010C MMSD
04/06/21 DM0406/21004758
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
04/07/21 DM0407/21004843
3.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/08/21 DM0408/21004861
3.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/09/21 DM0409/21004912
< 2.8 mg/kg D.W. 2.8 11
SW846: 6010C MMSD
04/10/21 DM0410/21004931
2.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
04/11/21 DM0411/21005023
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
04/12/21 DM0412/21005052
3.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/13/21 DM0413/21005199
6.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/14/21 DM0414/21005230
4.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/15/21 DM0415/21005248
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/16/21 DM0416/21005259
4.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
04/17/21 DM0417/21005468
4.3 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
04/18/21 DM0418/21005481 4.4 mg/kg D.W. 2.8 11 3.
SW846: 6010C MMSD
04/19/21 DM0419/21005508 4.9 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
04/20/21 DM0420/21005839
< 2.8 mg/kg D.W. 2.8 11
SW846: 6010C MMSD
04/21/21 DM0421/21005870
4.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/22/21 DM0422/21005981
4.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/23/21 DM0423/21005992
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/24/21 DM0424/21006057
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/25/21 DM0425/21006272
3.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/26/21 DM0426/21006299
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/27/21 DM0427/21006315
5.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/28/21 DM0428/21006346
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/29/21 DM0429/21006362
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
04/30/21 DM0430/21006373
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/01/21 DM0501/21006429
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/02/21 DM0502/21006442
3.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/03/21 DM0503/21006676
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/04/21 DM0504/21006691
5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/05/21 DM0505/21006722
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/06/21 DM0506/21006781
3.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/07/21 DM0507/21006834
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/08/21 DM0508/21006981
4.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/09/21 DM0509/21006994
4.5 mg/kg D.W. 2.8 10 3. SW846: 6010C MMSD
05/10/21 DM0510/21007021
4.4 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
05/11/21 DM0511/21007171
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/12/21 DM0512/21007202
4.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/13/21 DM0513/21007217
3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/14/21 DM0514/21007309 3.6 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
05/15/21 DM0515/21007328 < 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
05/16/21 DM0516/21007341 3.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/17/21 DM0517/21007382
4.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/18/21 DM0518/21007440
3.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
Page 3 of 121
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MMSD
PARTNERS FOI A CIEJAEA Br1110111011
ARSENIC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
4.5 mg/kg D.W.
2.7
10
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
4.3 mg/kg D.W. 2.8 11 3.
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
4.2 mg/kg D.W. 2.8 11 3.
SW846: 6010C MMSD
05/22/21 DM0522/21008072
4.4 mg/kg D.W. 2.8 11 3.
SW846: 6010C MMSD
05/23/21 DM0523/21008085
4.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/25/21 DM0525/21008288
5.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/26/21 DM0526/21008319
5.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/27/21 DM0527/21008484
3.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/28/21 DM0528/21008495
5.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/29/21 DM0529/21008515
5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
05/30/21 DM0530/21008530
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/01/21 DM0601/21008902
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
06/02/21 DM0602/21008935
5.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/03/21 DM0603/21008950
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/04/21 DM0604/21009184
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/05/21 DM0605/21009203 5 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
06/06/21 DM0606/21009287 4.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/07/21 DM0607/21009314
5.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/08/21 DM0608/21009334
4.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/09/21 DM0609/21009365
3.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/10/21 DM0610/21009538
3.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/11/21 DM0611/21009549
5.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/12/21 DM0612/21009568
6.2 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
06/13/21 DM0613/21009602
6.9 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
06/14/21 DM0614/21009629
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
06/18/21 DM0618/21009979
3.9 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
06/19/21 DM0619/21010314
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/20/21 DM0620/21010332
3.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/21/21 DM0621/21010359
2.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/22/21 DM0622/21010375
3.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/23/21 DM0623/21010408
3.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/24/21 DM0624/21010670
3.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/25/21 DM0625/21010681
4.4 mg/kg D.W. 2.8 10 3. SW846: 6010C MMSD
06/26/21 DM0626/21010702
4.3 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
06/27/21 DM0627/21010807
4.9 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD
06/28/21 DM0628/21010860
5.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/29/21 DM0629/21010875
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
06/30/21 DM0630/21011438
5 mg/kg D.W. 2.8 10 3. SW846: 6010C MMSD
07/01/21 DM0701/21011453
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/02/21 DM0702/21011465
3.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/03/21 DM0703/21011485
4 mg/kg D.W. 2.7 10 3, T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 4.2 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
07/05/21 DM0705/21011572 4.7 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
07/06/21 DM0706/21011693 4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/07/21 DM0707/21011727
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/08/21 DM0708/21011742
5.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
Page 4 of 121
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MMSD
PARTNERS FOI II CLIMB Br11A0111011
ARSENIC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
5.1 mg/kg D.W.
2.7
10
3.
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
4.7 mg/kg D.W. 2.7 10 3.
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
5.1 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
07/12/21 DM0712/21012283
4.9 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
07/13/21 DM0713/21012298
2.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/14/21 DM0714/21012332
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/15/21 DM0715/21012390
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/16/21 DM0716/21012563
5.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/17/21 DM0717/21012583
5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/18/21 DM0718/21012596
4.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/19/21 DM0719/21012624
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/20/21 DM0720/21012639
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
07/21/21 DM0721/21012760
4.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/22/21 DM0722/21012775
4.3 mg/kg D.W. 2.8 10 3. SW846: 6010C MMSD
07/23/21 DM0723/21013074
4.4 mg/kg D.W. 2.8 10 3. SW846: 6010C MMSD
07/24/21 DM0724/21013378 4.9 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
07/25/21 DM0725/21013391 4.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/26/21 DM0726/21013419
3.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/27/21 DM0727/21013434
5.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/28/21 DM0728/21013470
3.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/29/21 DM0729/21013614
3.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/30/21 DM0730/21013629
4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
07/31/21 DM0731/21013739
3.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/01/21 DM0801/21013752
3.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/02/21 DM0802/21013891
3.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/03/21 DM0803/21013906
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
08/04/21 DM0804/21013940
< 2.7 mg/kg D.W. 2.7 10
SW846: 6010C MMSD
08/05/21 DM0805/21014673
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/06/21 DM0806/21014685
3.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/07/21 DM0807/21014705
4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/08/21 DM0809/21014718
3.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/09/21 DM0809/21014746
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/10/21 DM0810/21014847
9.5 mg/kg D.W. 2.7 10 D2, 3, Q2.
SW846: 6010C MMSD
08/11/21 DM0811/21014867
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/12/21 DM0812/21015285
4.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/13/21 DM0813/21015297
5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/14/21 DM0814/21015317
5.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/15/21 DM0815/21015330
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/16/21 DM0816/21015410
4.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/17/21 DM0817/21015425
5.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/18/21 DM0818/21016031
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/19/21 DM0819/21016046 3.9 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
08/20/21 DM0820/21016068 4 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
08/21/21 DM0821/21016088 4.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/22/21 DM0822/21016196
4.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/23/21 DM0823/21016224
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
Page 5of121
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MMSD
PARTNERS FOI A CIEJAEA DI1011f{R[
ARSENIC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
4 mg/kg D.W.
2.7
10
3.
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
4.1 mg/kg D.W. 2.7 10 3.
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
5.1 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
08/27/21 DM0827/21016407
4.3 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
08/28/21 DM0828/21016427
4.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/30/21 DM0830/21016468
5.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
08/31/21 DM0831/21016483
3.2 mg/kg D.W. 2.7 10 D2, 3. SW846: 6010C MMSD
09/01/21 DM0901/21016598
5.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/02/21 DM0902/21016659
5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/03/21 DM0903/21016671
4.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/04/21 DM0904/21017055
5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/05/21 DM0905/21017068
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/06/21 DM0906/21017096
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/07/21 DM0907/21017306
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/08/21 DM0908/21017338
5.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/09/21 DM0909/21017408 4.8 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD
09/10/21 DM0910/21017420 3.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/11/21 DM0911/21017699
3.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/12/21 DM0912/21017712
3.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/13/21 DM0913/21017740
3.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/14/21 DM0914/21017755
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903
4.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150012-1
09/17/21 DM0917/21018105
5.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125
5.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138
5 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236
4 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 150123-1
09/21/21 DM0921/21018251
4.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150123-1
09/22/21 DM0922/21018480
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/23/21 DM0923/21018564
4.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD
09/24/21 DM0924/21018818
5.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838
5.3 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023
4.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051
5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066
5.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228
4.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243
4.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150305-1
10/01/21 DM 1001 /21019255
4.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384
4.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397
4.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 3.1 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD 150431-1
10/07/21 DM1007/21019760 3.4 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD 150431-1
10/08/21 DM1008/21019772 3.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600
3.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150655-1
Page 6 of 121
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MMSD
PARTNERS FOI A CIEJAEA Br1110111011
ARSENIC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
10/21/21
DM 1021 /21020689
3.6 mg/kg D.W.
2.7
10
3.
SW846: 6010C
MMSD
150655-1
10/22/21
DM 1022/21020701
7.3 mg/kg D.W. 2.7 10 3.
SW846: 6010C
MMSD 150703-1
10/23/21
DM 1023/21020883
5 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD 150703-1
10/24/21
DM1024/21021034
5.8 mg/kg D.W. 2.7 10 3.
SW846: 6010C MMSD 150703-1
10/25/21
DM 1025/21021062
3.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150703-1
10/26/21
DM 1026/21021077
4.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150756-1
10/27/21
DM1027/21021161
5.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150756-1
10/28/21
DM 1028/21021226
3.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150831-1
10/29/21
DM1029/21021510
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150831-1
10/30/21
DM 1030/21021530
4.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150831-1
10/31/21
DM 1031 /21021574
4.7 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 150831-1
11/01/21
DM 1101 /21021608
4.1 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 150831-1
11/02/21
DM1102/21021623
5.1 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 150884-1
11/03/21
DM1103/21021720
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150884-1
11/04/21
DM1104/21021735
5.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 3.8 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150964-1
11/07/21
DM1107/21022553
4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150964-1
11/08/21
DM1108/21022581
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150964-1
11/09/21
DM 1109/21022596
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 150964-2
11/10/21
DM1110/21022680
4 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151039-2
11/11/21
DM 1111 /21022695
3.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151039-2
11/12/21
DM1112/21022707
3.9 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151039-3
11/13/21
DM1113/21022731
4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151039-1
11/14/21
DM1114/21022744
3.7 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151039-3
11/15/21
DM1115/21022772
4.5 mg/kg D.W. 2.8 10 3. SW846: 6010C MMSD 151085-1
11/16/21
DM1116/21022787
4.6 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151085-1
11/17/21
DM1117/21023039
4.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151122-1
11/18/21
DM1118/21023056
4.7 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151122-1
11/19/21
DM1119/21023181
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151175-1
11/20/21
DM1120/21023201
5 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151175-1
11/21/21
DM 1121 /21023214
3.6 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151175-1
11/22/21
DM1122/21023555
4 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151175-1
11/23/21
DM1123/21023570
3.6 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151252-1
11/24/21
DM1124/21023611
4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151266-1
11/25/21
DM1125/21023795
4.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151266-1
11/26/21
DM1126/21023807
4.2 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151266-1
11/27/21
DM1127/21023827
4.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151266-1
11/28/21
DM1128/21023899
4.9 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151266-1
11/29/21
DM1129/21023927
4.2 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151294-1
11/30/21
DM1130/21024167
4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151317-1
12/01/21 DM1201/21024282 3.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151317-2
12/02/21 DM1202/21024297 4.4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151342-1
12/03/21 DM1203/21024309 4.9 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151371-1
12/04/21
DM 1204/21024329
3.6 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151371-1
12/05/21
DM 1205/21024739
4.5 mg/kg D.W. 2.8 11 D2, 3, Q3.
SW846: 6010C MMSD 151371-1
Page 7of121
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MMSD
PARTNERS FOI II CLIMB11A0111011
ARSENIC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e •
a.
QC Batch
ID
12/06/21
DM1206/21024767
4.4 mg/kg D.W.
2.8
11
3.
SW846: 6010C
MMSD
151391-1
12/07/21
DM 1207/21024782
3.8 mg/kg D.W. 2.8 11 3.
SW846: 6010C
MMSD 151422-1
12/08/21 DM 1208/21024816
3.8 mg/kg D.W. 2.8 11 3.
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 3.2 mg/kg D.W. 2.8 11 3.
SW846: 6010C MMSD 151471-2
12/10/21 DM1210/21024844 4 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151498-1
12/11/21 DM1211/21024864 4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151498-1
12/12/21 DM1212/21025174 4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151498-1
12/13/21 DM1213/21025205 3.5 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151543-1
12/14/21 DM1214/21025220 3.5 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151576-1
12/15/21 DM1215/21025299 3.9 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151576-1
12/16/21 DM1216/21025314 4 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151645-1
12/17/21 DM1217/21025326 3.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151645-1
12/18/21 DM1219/21025346 4 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151645-1
12/19/21 DM1219/21025621 3.5 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151645-1
12/20/21 DM1220/21025649 3.5 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151645-2
12/21/21 DM1221/21025664 4.3 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151668-1
12/22/21 DM1222/21025700 4.2 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151750-1
12/23/21 DM1223/21025779 4.2 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151750-2
12/24/21 DM1224/21025791 4 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151750-2
12/25/21 DM1225/21025811 3.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151750-2
12/26/21 DM1226/21025824 3.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151750-2
12/27/21 DM1227/21025917 4.1 mg/kg D.W. 2.7 10 3. SW846: 6010C MMSD 151750-2
12/28/21 DM1228/21025932 4.4 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151750-2
12/29/21 DM1229/21025966 4.7 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151827-1
12/30/21 DM1230/21025981 4.8 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151827-1
12/31/21 DM1231/21026033 4.5 mg/kg D.W. 2.8 11 3. SW846: 6010C MMSD 151827-1
Avg Result: 4.1 mg/kg D.W. Min LOD: 2.7 mg/kg D.W.
Max Result: 9.5 mg/kg D.W. Max LOD: 2.8 mg/kg D.W.
Page 8 of 121
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MMSD
PARTNERS FOI II CLIMB PI11A0111011
CADMIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
0.38 mg/kg D.W.
0.12
0.48
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
0.38 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
0.36 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C MMSD
01/04/21 DM0104/21000488 0.26 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C MMSD
01/05/21 DM0105/21000504 0.48 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/06/21 DM0106/21000535 0.48 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
01/07/21 DM0107/21000551 0.48 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
01/08/21 DM0108/21000562 0.4 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/09/21 DM0109/21000581 0.41 mg/kg D.W. 0.12 0.49 3. SW846: 6010C MMSD
01/10/21 DM0110/21000594 0.41 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/11/21 DM0111/21000632 0.36 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/12/21 DM0112/21000648 0.38 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/13/21 DM0113/21000679 0.4 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/14/21 DM0114/21000754 0.36 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
01/15/21 DM0115/21000765 0.34 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/16/21 DM0116/21000784 0.34 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/17/21 DM0117/21000797 0.36 mg/kg D.W. 0.12 0.48 3, Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 0.62 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
01/19/21 DM0119/21000842 0.47 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/20/21 DM0120/21000926 0.45 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/21/21 DM0121/21000942 0.45 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/22/21 DM0122/21000953 0.54 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
01/23/21 DM0123/21000972 0.49 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
01/24/21 DM0124/21001059 0.41 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/25/21 DM0125/21001088 0.32 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/26/21 DM0126/21001106 0.34 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
01/27/21 DM0127/21001137 0.44 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
01/28/21 DM0128/21001153 0.33 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
01/29/21 DM0129/21001164 0.24 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
01/30/21 DM0130/21001304 0.25 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
01/31/21 DM0131/21001317 0.26 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
02/01/21 DM0201/21001344 0.4 mg/kg D.W. 0.12 0.48 D2, 3, Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 0.62 mg/kg D.W. 0.12 0.48 D2. SW846: 6010C MMSD
02/03/21 DM0203/21001428 0.3 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
02/04/21 DM0204/21001444 0.61 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
02/05/21 DM0205/21001455 0.38 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
02/06/21 DM0206/21001476 0.38 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
02/07/21 DM0207/21001489 0.38 mg/kg D.W. 0.11 0.46 3. SW846: 6010C MMSD
02/08/21 DM0208/21001609 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
02/09/21 DM0209/21001625 0.44 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
02/10/21 DM0210/21001656 0.61 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
02/11/21 DM0211/21001672 0.44 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
02/12/21 DM0212/21001706 0.46 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
02/13/21 DM0213/21001725 0.48 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
02/14/21 DM0214/21001738 0.67 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
02/15/21 DM0215/21001793 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
Page 9 of 121
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MMSD
PARTNERS FOI II CLIMB11A0111011
CADMIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
0.28 mg/kg D.W.
0.12
0.48
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
0.24 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
0.23 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C MMSD
02/19/21 DM0219/21001986 0.28 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C MMSD
02/20/21 DM0220/21002005 0.29 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
02/21/21 DM0221/21002072 0.27 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
02/22/21 DM0222/21002230 0.36 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
02/23/21 DM0223/21002246 0.47 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
02/24/21 DM0224/21002281 0.3 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
02/25/21 DM0225/21002320 0.3 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
02/26/21 DM0226/21002386 0.59 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
02/27/21 DM0227/21002405 0.62 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
02/28/21 DM0228/21002478 0.65 mg/kg D.W. 0.12 0.47 D2. SW846: 6010C MMSD
03/01/21 DM0301/21002611 0.31 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
03/02/21 DM0302/21002629 0.69 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
03/03/21 DM0303/21002660 0.44 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
03/04/21 DM0304/21002717 0.59 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
03/05/21 DM0305/21002728 0.42 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
03/06/21 DM0306/21002747 0.42 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
03/07/21 DM0307/21002858 0.46 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
03/08/21 DM0308/21003336 0.46 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
03/09/21 DM0309/21003371 0.61 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
03/10/21 DM0310/21003402 0.44 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
03/11/21 DM0311/21003456 0.8 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
03/12/21 DM0312/21003522 0.46 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
03/13/21 DM0313/21003541 0.5 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
03/14/21 DM0314/21003554 0.44 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
03/15/21 DM0315/21003747 0.4 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
03/16/21 DM0316/21003801 0.71 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
03/17/21 DM0317/21003878 0.44 mg/kg D.W. 0.12 0.47 3, Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 < 0.12 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
03/19/21 DM0319/21003905 0.41 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
03/20/21 DM0320/21004076 0.42 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
03/21/21 DM0321/21004093 0.42 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
03/22/21 DM0322/21004120 0.39 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
03/23/21 DM0323/21004136 0.36 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
03/24/21 DM0324/21004167 0.34 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
03/25/21 DM0325/21004242 0.44 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
03/26/21 DM0326/21004253 0.34 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
03/27/21 DM0327/21004272 0.36 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
03/28/21 DM0328/21004285 0.34 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
03/29/21 DM0329/21004312 0.36 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
03/30/21 DM0330/21004388 0.36 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
03/31/21 DM0331/21004600 0.42 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
04/01/21 DM0401/21004616 0.43 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
04/02/21 DM0402/21004627 0.4 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
Page 10 of 121
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MMSD
PARTNERS FOI A CLEANER DI10111M
CADMIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
0.42 mg/kg D.W.
0.12
0.48
3.
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
0.34 mg/kg D.W. 0.12 0.47 3.
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
0.44 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C MMSD
04/06/21 DM0406/21004758 0.63 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
04/07/21 DM0407/21004843 0.38 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
04/08/21 DM0408/21004861 0.36 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
04/09/21 DM0409/21004912 0.4 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
04/10/21 DM0410/21004931 0.4 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
04/11/21 DM0411/21005023 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
04/12/21 DM0412/21005052 0.48 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
04/13/21 DM0413/21005199 0.61 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
04/14/21 DM0414/21005230 0.38 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
04/15/21 DM0415/21005248 0.35 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
04/16/21 DM0416/21005259 0.3 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
04/17/21 DM0417/21005468 0.3 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
04/18/21 DM0418/21005481 0.32 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
04/19/21 DM0419/21005508 0.39 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
04/20/21 DM0420/21005839 0.72 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
04/21/21 DM0421/21005870 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
04/22/21 DM0422/21005981 0.35 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
04/23/21 DM0423/21005992 0.32 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
04/24/21 DM0424/21006057 0.36 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
04/25/21 DM0425/21006272 0.34 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
04/26/21 DM0426/21006299 0.62 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
04/27/21 DM0427/21006315 0.65 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
04/28/21 DM0428/21006346 0.27 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
04/29/21 DM0429/21006362 0.32 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
04/30/21 DM0430/21006373 0.31 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
05/01/21 DM0501/21006429 0.29 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
05/02/21 DM0502/21006442 0.32 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
05/03/21 DM0503/21006676 0.27 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
05/04/21 DM0504/21006691 0.65 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
05/05/21 DM0505/21006722 0.52 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
05/06/21 DM0506/21006781 0.38 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
05/07/21 DM0507/21006834 0.47 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
05/08/21 DM0508/21006981 0.42 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
05/09/21 DM0509/21006994 0.42 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
05/10/21 DM0510/21007021 0.36 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
05/11/21 DM0511/21007171 0.42 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
05/12/21 DM0512/21007202 0.42 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
05/13/21 DM0513/21007217 0.64 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
05/14/21 DM0514/21007309 0.31 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
05/15/21 DM0515/21007328 0.35 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
05/16/21 DM0516/21007341 0.34 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
05/17/21 DM0517/21007382 0.32 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
05/18/21 DM0518/21007440 0.74 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
Page 11 of 121
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MMSD
PARTNERS FOI A CLEANER DI10111M
CADMIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
0.32 mg/kg D.W.
0.12
0.47
3.
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
0.49 mg/kg D.W. 0.12 0.48
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
0.47 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C MMSD
05/22/21 DM0522/21008072 0.39 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C MMSD
05/23/21 DM0523/21008085 0.34 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
05/25/21 DM0525/21008288 0.4 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
05/26/21 DM0526/21008319 0.32 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
05/27/21 DM0527/21008484 0.64 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
05/28/21 DM0528/21008495 0.31 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
05/29/21 DM0529/21008515 0.34 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
05/30/21 DM0530/21008530 0.32 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/01/21 DM0601/21008902 0.76 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
06/02/21 DM0602/21008935 0.29 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/03/21 DM0603/21008950 0.33 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/04/21 DM0604/21009184 0.32 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
06/05/21 DM0605/21009203 0.28 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/06/21 DM0606/21009287 0.28 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/07/21 DM0607/21009314 0.36 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
06/08/21 DM0608/21009334 0.31 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/09/21 DM0609/21009365 0.29 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/10/21 DM0610/21009538 0.38 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/11/21 DM0611/21009549 0.66 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
06/12/21 DM0612/21009568 0.75 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
06/13/21 DM0613/21009602 0.66 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
06/14/21 DM0614/21009629 0.71 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
06/18/21 DM0618/21009979 0.44 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
06/19/21 DM0619/21010314 0.37 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/20/21 DM0620/21010332 0.39 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/21/21 DM0621/21010359 0.32 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/22/21 DM0622/21010375 0.42 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
06/23/21 DM0623/21010408 0.38 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/24/21 DM0624/21010670 0.29 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/25/21 DM0625/21010681 0.44 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
06/26/21 DM0626/21010702 0.43 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
06/27/21 DM0627/21010807 0.47 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
06/28/21 DM0628/21010860 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
06/29/21 DM0629/21010875 0.8 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
06/30/21 DM0630/21011438 0.59 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
07/01/21 DM0701/21011453 0.42 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
07/02/21 DM0702/21011465 0.42 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
07/03/21 DM0703/21011485 0.44 mg/kg D.W. 0.12 0.47 3, T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 0.38 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
07/05/21 DM0705/21011572 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
07/06/21 DM0706/21011693 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
07/07/21 DM0707/21011727 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
07/08/21 DM0708/21011742 0.46 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
Page 12 of 121
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MMSD
PARTNERS FOI II CLIMB11A0111011
CADMIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
0.46 mg/kg D.W.
0.11
0.47
3.
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
0.44 mg/kg D.W. 0.11 0.47 3.
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
0.46 mg/kg D.W. 0.11 0.47 3.
SW846: 6010C MMSD
07/12/21 DM0712/21012283 0.46 mg/kg D.W. 0.11 0.47 3.
SW846: 6010C MMSD
07/13/21 DM0713/21012298 0.71 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
07/14/21 DM0714/21012332 0.37 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
07/15/21 DM0715/21012390 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
07/16/21 DM0716/21012563 0.52 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
07/17/21 DM0717/21012583 0.52 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
07/18/21 DM0718/21012596 0.46 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
07/19/21 DM0719/21012624 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
07/20/21 DM0720/21012639 2.5 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
07/21/21 DM0721/21012760 0.57 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
07/22/21 DM0722/21012775 0.36 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
07/23/21 DM0723/21013074 0.38 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
07/24/21 DM0724/21013378 0.38 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD
07/25/21 DM0725/21013391 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
07/26/21 DM0726/21013419 0.32 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
07/27/21 DM0727/21013434 0.61 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
07/28/21 DM0728/21013470 0.32 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
07/29/21 DM0729/21013614 0.44 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
07/30/21 DM0730/21013629 0.48 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
07/31/21 DM0731/21013739 0.5 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
08/01/21 DM0801/21013752 0.46 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
08/02/21 DM0802/21013891 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
08/03/21 DM0803/21013906 2.7 mg/kg D.W. 0.11 0.47 D2. SW846: 6010C MMSD
08/04/21 DM0804/21013940 2.7 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
08/05/21 DM0805/21014673 2.7 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
08/06/21 DM0806/21014685 0.44 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
08/07/21 DM0807/21014705 0.44 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
08/08/21 DM0809/21014718 0.44 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
08/09/21 DM0809/21014746 0.44 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
08/10/21 DM0810/21014847 0.56 mg/kg D.W. 0.12 0.47 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 0.62 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
08/12/21 DM0812/21015285 0.59 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
08/13/21 DM0813/21015297 0.62 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
08/14/21 DM0814/21015317 0.66 mg/kg D.W. 0.11 0.46
SW846: 6010C MMSD
08/15/21 DM0815/21015330 0.78 mg/kg D.W. 0.11 0.46
SW846: 6010C MMSD
08/16/21 DM0816/21015410 0.55 mg/kg D.W. 0.11 0.46
SW846: 6010C MMSD
08/17/21 DM0817/21015425 0.91 mg/kg D.W. 0.11 0.46
SW846: 6010C MMSD
08/18/21 DM0818/21016031 0.67 mg/kg D.W. 0.11 0.46
SW846: 6010C MMSD
08/19/21
08/20/21
08/21/21
DM0819/21016046
DM0820/21016068
DM0821/21016088
0.64 mg/kg D.W. 0.11 0.46
SW846: 6010C MMSD
0.7 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
0.6 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
08/22/21 DM0822/21016196 0.6 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
08/23/21 DM0823/21016224 0.54 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
Page 13 of 121
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MMSD
PARTNERS FOI A CLEANER LY *011101t
CADMIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
0.67 mg/kg D.W.
0.12
0.47
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
0.55 mg/kg D.W. 0.12 0.47
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
0.44 mg/kg D.W. 0.12 0.47 3.
SW846: 6010C MMSD
08/27/21 DM0827/21016407 0.4 mg/kg D.W. 0.12 0.47 3.
SW846: 6010C MMSD
08/28/21 DM0828/21016427 0.46 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
08/30/21 DM0830/21016468 0.42 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD
08/31/21 DM0831/21016483 2.4 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
09/01/21 DM0901/21016598 0.58 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
09/02/21 DM0902/21016659 0.69 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
09/03/21 DM0903/21016671 0.5 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD
09/04/21 DM0904/21017055 0.54 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
09/05/21 DM0905/21017068 0.48 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
09/06/21 DM0906/21017096 0.52 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
09/07/21 DM0907/21017306 0.52 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
09/08/21 DM0908/21017338 0.48 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
09/09/21 DM0909/21017408 0.44 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
09/10/21 DM0910/21017420 0.69 mg/kg D.W. 0.12 0.47 SW846: 6010C MMSD
09/11/21 DM0911/21017699 0.58 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
09/12/21 DM0912/21017712 0.48 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
09/13/21 DM0913/21017740 0.38 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD
09/14/21 DM0914/21017755 0.46 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 0.49 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 0.48 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD 150012-1
09/17/21 DM0917/21018105 0.64 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 0.57 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 0.55 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 0.45 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 150123-1
09/21/21 DM0921/21018251 0.55 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD 150123-1
09/22/21 DM0922/21018480 0.5 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD
09/23/21 DM0923/21018564 0.52 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD
09/24/21 DM0924/21018818 0.44 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 0.43 mg/kg D.W. 0.11 0.46 3. SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 0.44 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 0.41 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 0.46 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 0.46 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 0.48 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 0.47 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 0.44 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 0.43 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 0.48 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 0.46 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 150431-1
10/07/21 DM1007/21019760 0.46 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD 150431-1
10/08/21 DM1008/21019772 0.43 mg/kg D.W. 0.11 0.46 3. SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 0.43 mg/kg D.W. 0.11 0.46 3. SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 0.54 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD 150655-1
Page 14 of 121
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MMSD
PARTNERS FOI A WAR DI1011f{R[
CADMIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
10/21/21
DM 1021 /21020689
0.42 mg/kg D.W.
0.11
0.47
3.
SW846: 6010C
MMSD
150655-1
10/22/21
DM 1022/21020701
0.9 mg/kg D.W. 0.11 0.47
SW846: 6010C
MMSD 150703-1
10/23/21 DM1023/21020883
0.87 mg/kg D.W. 0.11 0.46
SW846: 6010C MMSD 150703-1
10/24/21 DM1024/21021034 0.88 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 0.85 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 0.75 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 0.82 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 0.42 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 150831-1
10/29/21 DM1029/21021510 0.42 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 150831-1
10/30/21 DM1030/21021530 0.46 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 150831-1
10/31/21 DM1031/21021574 0.45 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 150831-1
11/01/21 DM1101/21021608 0.42 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 150831-1
11/02/21 DM1102/21021623 0.48 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 0.46 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 0.46 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 0.36 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 0.33 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 0.32 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 0.33 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 0.33 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 0.36 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151039-2
11/11/21 DM1111/21022695 0.35 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 0.36 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 0.4 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 151039-1
11/14/21 DM1114/21022744 0.38 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 0.34 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151085-1
11/16/21 DM1116/21022787 0.36 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 151085-1
11/17/21 DM1117/21023039 0.35 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 151122-1
11/18/21 DM1118/21023056 0.36 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 151122-1
11/19/21 DM1119/21023181 0.32 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 151175-1
11/20/21 DM1120/21023201 0.34 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151175-1
11/21/21 DM1121/21023214 0.28 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151175-1
11/22/21 DM1122/21023555 0.28 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151175-1
11/23/21 DM1123/21023570 0.27 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151252-1
11/24/21 DM1124/21023611 0.37 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151266-1
11/25/21 DM1125/21023795 0.37 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151266-1
11/26/21 DM1126/21023807 0.33 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151266-1
11/27/21 DM1127/21023827 0.37 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151266-1
11/28/21 DM1128/21023899 0.36 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151266-1
11/29/21 DM1129/21023927 0.41 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 151294-1
11/30/21 DM1130/21024167 0.41 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 151317-1
12/01/21 DM1201/21024282 0.39 mg/kg D.W. 0.11 0.47 3. SW846: 6010C MMSD 151317-2
12/02/21 DM1202/21024297 0.46 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 151342-1
12/03/21 DM1203/21024309 0.36 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 151371-1
12/04/21 DM1204/21024329 0.37 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151371-1
12/05/21 DM1205/21024739 0.38 mg/kg D.W. 0.12 0.48 D2, 3, Q3. SW846: 6010C MMSD 151371-1
Page 15 of 121
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MMSD
PARTNERS FOI A CLEANER DI1011MR
CADMIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e •
a.
QC Batch
ID
12/06/21
DM1206/21024767
0.5 mg/kg D.W.
0.12
0.48
SW846: 6010C
MMSD
151391-1
12/07/21
DM 1207/21024782
0.35 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C
MMSD 151422-1
12/08/21 DM 1208/21024816
0.44 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 0.37 mg/kg D.W. 0.12 0.48 3.
SW846: 6010C MMSD 151471-2
12/10/21 DM1210/21024844 0.47 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151498-1
12/11/21 DM1211/21024864 0.45 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 151498-1
12/12/21 DM1212/21025174 0.48 mg/kg D.W. 0.11 0.47
SW846: 6010C MMSD 151498-1
12/13/21 DM1213/21025205 0.36 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151543-1
12/14/21 DM1214/21025220 0.58 mg/kg D.W. 0.12 0.47
SW846: 6010C MMSD 151576-1
12/15/21 DM1215/21025299 0.51 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD 151576-1
12/16/21 DM1216/21025314 0.45 mg/kg D.W. 0.12 0.47 3. SW846: 6010C MMSD 151645-1
12/17/21 DM1217/21025326 0.43 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151645-1
12/18/21 DM1219/21025346 0.41 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151645-1
12/19/21 DM1219/21025621 0.39 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151645-1
12/20/21 DM1220/21025649 0.39 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151645-2
12/21/21 DM1221/21025664 0.46 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151668-1
12/22/21 DM1222/21025700 0.45 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151750-1
12/23/21 DM1223/21025779 0.44 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151750-2
12/24/21 DM1224/21025791 0.43 mg/kg D.W. 0.12 0.49 3. SW846: 6010C MMSD 151750-2
12/25/21 DM1225/21025811 0.55 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD 151750-2
12/26/21 DM1226/21025824 0.42 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151750-2
12/27/21 DM1227/21025917 0.44 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151750-2
12/28/21 DM1228/21025932 0.48 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD 151750-2
12/29/21 DM1229/21025966 0.51 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD 151827-1
12/30/21 DM1230/21025981 0.48 mg/kg D.W. 0.12 0.48 3. SW846: 6010C MMSD 151827-1
12/31/21 DM1231/21026033 0.5 mg/kg D.W. 0.12 0.48
SW846: 6010C MMSD 151827-1
Avg Result: 0.48 mg/kg D.W. Min LOD: 0.11 mg/kg D.W.
Max Result: 2.7 mg/kg D.W. Max LOD: 0.12 mg/kg D.W.
Page 16 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
COPPER ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
220 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
230 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
220 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
01/04/21 DM0104/21000488 240 mg/kg D.W. 6.7 26
SW846: 6010C MMSD
01/05/21 DM0105/21000504 240 mg/kg D.W. 6.8 26
SW846: 6010C MMSD
01/06/21 DM0106/21000535 240 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
01/07/21 DM0107/21000551 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/08/21 DM0108/21000562 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/09/21 DM0109/21000581 240 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
01/10/21 DM0110/21000594 230 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
01/11/21 DM0111/21000632 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/12/21 DM0112/21000648 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/13/21 DM0113/21000679 230 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/14/21 DM0114/21000754 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
01/15/21 DM0115/21000765 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/16/21 DM0116/21000784 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/17/21 DM0117/21000797 250 mg/kg D.W. 6.7 26 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 250 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/19/21 DM0119/21000842 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/20/21 DM0120/21000926 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
01/21/21 DM0121/21000942 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/22/21 DM0122/21000953 240 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
01/23/21 DM0123/21000972 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/24/21 DM0124/21001059 240 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
01/25/21 DM0125/21001088 220 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
01/26/21 DM0126/21001106 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
01/27/21 DM0127/21001137 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
01/28/21 DM0128/21001153 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
01/29/21 DM0129/21001164 240 mg/kg D.W. 6.5 25 SW846: 6010C MMSD
01/30/21 DM0130/21001304 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
01/31/21 DM0131/21001317 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
02/01/21 DM0201/21001344 230 mg/kg D.W. 6.7 25 Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 250 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
02/03/21 DM0203/21001428 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
02/04/21 DM0204/21001444 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/05/21 DM0205/21001455 250 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
02/06/21 DM0206/21001476 250 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
02/07/21 DM0207/21001489 250 mg/kg D.W. 6.5 25 SW846: 6010C MMSD
02/08/21 DM0208/21001609 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/09/21 DM0209/21001625 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/10/21 DM0210/21001656 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/11/21 DM0211/21001672 220 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
02/12/21 DM0212/21001706 230 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
02/13/21 DM0213/21001725 240 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
02/14/21 DM0214/21001738 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/15/21 DM0215/21001793 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
Page 17 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
COPPER ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
230 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
220 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
210 mg/kg D.W. 6.7 26
SW846: 6010C MMSD
02/19/21 DM0219/21001986 210 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
02/20/21 DM0220/21002005 210 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
02/21/21 DM0221/21002072 210 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
02/22/21 DM0222/21002230 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/23/21 DM0223/21002246 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/24/21 DM0224/21002281 210 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
02/25/21 DM0225/21002320 210 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
02/26/21 DM0226/21002386 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/27/21 DM0227/21002405 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
02/28/21 DM0228/21002478 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/01/21 DM0301/21002611 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/02/21 DM0302/21002629 200 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/03/21 DM0303/21002660 210 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
03/04/21 DM0304/21002717 220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
03/05/21 DM0305/21002728 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/06/21 DM0306/21002747 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/07/21 DM0307/21002858 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
03/08/21 DM0308/21003336 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/09/21 DM0309/21003371 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/10/21 DM0310/21003402 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/11/21 DM0311/21003456 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/12/21 DM0312/21003522 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/13/21 DM0313/21003541 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/14/21 DM0314/21003554 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/15/21 DM0315/21003747 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/16/21 DM0316/21003801 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/17/21 DM0317/21003878 240 mg/kg D.W. 6.6 25 Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/19/21 DM0319/21003905 230 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
03/20/21 DM0320/21004076 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/21/21 DM0321/21004093 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/22/21 DM0322/21004120 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/23/21 DM0323/21004136 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/24/21 DM0324/21004167 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/25/21 DM0325/21004242 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
03/26/21 DM0326/21004253 210 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
03/27/21 DM0327/21004272 200 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
03/28/21 DM0328/21004285 220 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
03/29/21 DM0329/21004312 220 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
03/30/21 DM0330/21004388 220 mg/kg D.W. 6.7 26
SW846: 6010C MMSD
03/31/21 DM0331/21004600 200 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
04/01/21 DM0401/21004616 220 mg/kg D.W. 6.7 25 Q3. SW846: 6010C MMSD
04/02/21 DM0402/21004627 220 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
Page 18 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOWN
COPPER ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
230 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
220 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
230 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
04/06/21 DM0406/21004758 240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
04/07/21 DM0407/21004843 230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
04/08/21 DM0408/21004861 220 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
04/09/21 DM0409/21004912 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
04/10/21 DM0410/21004931 220 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
04/11/21 DM0411/21005023 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/12/21 DM0412/21005052 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/13/21 DM0413/21005199 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/14/21 DM0414/21005230 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/15/21 DM0415/21005248 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/16/21 DM0416/21005259 210 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
04/17/21 DM0417/21005468 210 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
04/18/21 DM0418/21005481 220 mg/kg D.W. 6.7 25
SW846: 6010C MMSD
04/19/21 DM0419/21005508 230 mg/kg D.W. 6.8 26
SW846: 6010C MMSD
04/20/21 DM0420/21005839 220 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
04/21/21 DM0421/21005870 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/22/21 DM0422/21005981 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/23/21 DM0423/21005992 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/24/21 DM0424/21006057 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/25/21 DM0425/21006272 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/26/21 DM0426/21006299 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/27/21 DM0427/21006315 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/28/21 DM0428/21006346 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/29/21 DM0429/21006362 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
04/30/21 DM0430/21006373 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/01/21 DM0501/21006429 200 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/02/21 DM0502/21006442 200 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/03/21 DM0503/21006676 200 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/04/21 DM0504/21006691 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/05/21 DM0505/21006722 200 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/06/21 DM0506/21006781 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/07/21 DM0507/21006834 220 mg/kg D.W. 6.5 25 SW846: 6010C MMSD
05/08/21 DM0508/21006981 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/09/21 DM0509/21006994 210 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
05/10/21 DM0510/21007021 210 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
05/11/21 DM0511/21007171 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/12/21 DM0512/21007202 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/13/21 DM0513/21007217 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
05/14/21 DM0514/21007309 210 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
05/15/21 DM0515/21007328 210 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
05/16/21 DM0516/21007341 230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
05/17/21 DM0517/21007382 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/18/21 DM0518/21007440 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
Page 19 of 121
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MMSD
PARTNERS FOI A CLIMB E1n* r 1
COPPER ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
220 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
240 mg/kg D.W. 6.7 25
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
250 mg/kg D.W. 6.7 26
SW846: 6010C MMSD
05/22/21 DM0522/21008072 240 mg/kg D.W. 6.7 26
SW846: 6010C MMSD
05/23/21 DM0523/21008085 230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
05/25/21 DM0525/21008288 230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
05/26/21 DM0526/21008319 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/27/21 DM0527/21008484 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/28/21 DM0528/21008495 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/29/21 DM0529/21008515 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
05/30/21 DM0530/21008530 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/01/21 DM0601/21008902 250 mg/kg D.W. 6.6 25 Q2. SW846: 6010C MMSD
06/02/21 DM0602/21008935 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/03/21 DM0603/21008950 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/04/21 DM0604/21009184 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/05/21 DM0605/21009203 230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/06/21 DM0606/21009287 240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
06/07/21 DM0607/21009314 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/08/21 DM0608/21009334 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/09/21 DM0609/21009365 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/10/21 DM0610/21009538 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/11/21 DM0611/21009549 230 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
06/12/21 DM0612/21009568 290 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
06/13/21 DM0613/21009602 220 mg/kg D.W. 6.7 26 Q2. SW846: 6010C MMSD
06/14/21 DM0614/21009629 230 mg/kg D.W. 6.6 25 Q2. SW846: 6010C MMSD
06/18/21 DM0618/21009979 210 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
06/19/21 DM0619/21010314 200 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/20/21 DM0620/21010332 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/21/21 DM0621/21010359 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/22/21 DM0622/21010375 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/23/21 DM0623/21010408 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/24/21 DM0624/21010670 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/25/21 DM0625/21010681 230 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
06/26/21 DM0626/21010702 220 mg/kg D.W. 6.8 26 SW846: 6010C MMSD
06/27/21 DM0627/21010807 230 mg/kg D.W. 6.7 26 SW846: 6010C MMSD
06/28/21 DM0628/21010860 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/29/21 DM0629/21010875 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
06/30/21 DM0630/21011438 230 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
07/01/21 DM0701/21011453 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/02/21 DM0702/21011465 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/03/21 DM0703/21011485 240 mg/kg D.W. 6.6 25 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/05/21 DM0705/21011572 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/06/21 DM0706/21011693 240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/07/21 DM0707/21011727 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/08/21 DM0708/21011742 260 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
Page 20 of 121
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MMSD
PARTNERS FOI A CLIMB Br
COPPER ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
240 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
240 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
240 mg/kg D.W. 6.5 25
SW846: 6010C MMSD
07/12/21 DM0712/21012283 250 mg/kg D.W. 6.5 25
SW846: 6010C MMSD
07/13/21 DM0713/21012298 260 mg/kg D.W. 6.5 25
SW846: 6010C MMSD
07/14/21 DM0714/21012332 240 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/15/21 DM0715/21012390 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/16/21 DM0716/21012563 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/17/21 DM0717/21012583 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/18/21 DM0718/21012596 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/19/21 DM0719/21012624 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/20/21 DM0720/21012639 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/21/21 DM0721/21012760 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/22/21 DM0722/21012775 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
07/23/21 DM0723/21013074 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD
07/24/21 DM0724/21013378 230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/25/21 DM0725/21013391 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
07/26/21 DM0726/21013419 230 mg/kg D.W. 6.6 25 Q2. SW846: 6010C MMSD
07/27/21 DM0727/21013434 250 mg/kg D.W. 6.6 25 Q2. SW846: 6010C MMSD
07/28/21 DM0728/21013470 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/29/21 DM0729/21013614 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
07/30/21 DM0730/21013629 240 mg/kg D.W. 6.5 25 SW846: 6010C MMSD
07/31/21 DM0731/21013739 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/01/21 DM0801/21013752 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/02/21 DM0802/21013891 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/03/21 DM0803/21013906 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/04/21 DM0804/21013940 260 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/05/21 DM0805/21014673 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/06/21 DM0806/21014685 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/07/21 DM0807/21014705 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/08/21 DM0809/21014718 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/09/21 DM0809/21014746 260 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/10/21 DM0810/21014847 250 mg/kg D.W. 6.6 25 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/12/21 DM0812/21015285 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/13/21 DM0813/21015297 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/14/21 DM0814/21015317 240 mg/kg D.W. 6.5 25 SW846: 6010C MMSD
08/15/21 DM0815/21015330 250 mg/kg D.W. 6.4 25 SW846: 6010C MMSD
08/16/21 DM0816/21015410 290 mg/kg D.W. 6.5 25 SW846: 6010C MMSD
08/17/21 DM0817/21015425 270 mg/kg D.W. 6.5 25 SW846: 6010C MMSD
08/18/21 DM0818/21016031 260 mg/kg D.W. 6.5 25 SW846: 6010C MMSD
08/19/21 DM0819/21016046 260 mg/kg D.W. 6.5 25 Q3. SW846: 6010C MMSD
08/20/21 DM0820/21016068 280 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/21/21 DM0821/21016088 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/22/21 DM0822/21016196 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
08/23/21 DM0823/21016224 270 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
Page 21 of 121
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MMSD
PARTAFRS FOI A OAR LY * I lB
COPPER ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
280 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
270 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/27/21 DM0827/21016407 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/28/21 DM0828/21016427 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/30/21 DM0830/21016468 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
08/31/21 DM0831/21016483 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/01/21 DM0901/21016598 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/02/21 DM0902/21016659 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/03/21 DM0903/21016671 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/04/21 DM0904/21017055 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/05/21 DM0905/21017068 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/06/21 DM0906/21017096 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/07/21 DM0907/21017306 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/08/21 DM0908/21017338 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/09/21 DM0909/21017408 230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/10/21 DM0910/21017420 230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD
09/11/21 DM0911/21017699 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/12/21 DM0912/21017712 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/13/21 DM0913/21017740 210 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/14/21 DM0914/21017755 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 260 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150012-1
09/17/21 DM0917/21018105 260 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 260 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 250 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 150123-1
09/21/21 DM0921/21018251 260 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150123-1
09/22/21 DM0922/21018480 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/23/21 DM0923/21018564 260 mg/kg D.W. 6.6 25 SW846: 6010C MMSD
09/24/21 DM0924/21018818 260 mg/kg D.W. 6.5 25 SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 250 mg/kg D.W. 6.5 25 SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 260 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 250 mg/kg D.W. 6.5 25 SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 260 mg/kg D.W. 6.5 25 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 260 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 250 mg/kg D.W. 6.6 25 Q3. SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 260 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150431-1
10/07/21 DM1007/21019760 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150431-1
10/08/21 DM1008/21019772 240 mg/kg D.W. 6.5 25
SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 260 mg/kg D.W. 6.5 25 SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 260 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150655-1
Page 22 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
COPPER ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
10/21/21
DM 1021 /21020689
250 mg/kg D.W.
6.6
25
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
240 mg/kg D.W. 6.6 25
SW846: 6010C
MMSD 150703-1
10/23/21 DM1023/21020883
230 mg/kg D.W. 6.5 25
SW846: 6010C MMSD 150703-1
10/24/21 DM1024/21021034 220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 230 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 220 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150831-1
10/29/21 DM1029/21021510 220 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150831-1
10/30/21 DM1030/21021530 230 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150831-1
10/31/21 DM1031/21021574 230 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 150831-1
11/01/21 DM1101/21021608 220 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 150831-1
11/02/21 DM1102/21021623 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 240 mg/kg D.W. 6.5 25
SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 250 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 250 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 260 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151039-2
11/11/21 DM1111/21022695 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 250 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 151039-1
11/14/21 DM1114/21022744 250 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 250 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 151085-1
11/16/21 DM1116/21022787 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 151085-1
11/17/21 DM1117/21023039 260 mg/kg D.W. 6.6 25 Q3. SW846: 6010C MMSD 151122-1
11/18/21 DM1118/21023056 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 151122-1
11/19/21 DM1119/21023181 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 151175-1
11/20/21 DM1120/21023201 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 151175-1
11/21/21 DM1121/21023214 230 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151175-1
11/22/21 DM1122/21023555 240 mg/kg D.W. 6.8 26 SW846: 6010C MMSD 151175-1
11/23/21 DM1123/21023570 220 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 151252-1
11/24/21 DM1124/21023611 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 151266-1
11/25/21 DM1125/21023795 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151266-1
11/26/21 DM1126/21023807 230 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151266-1
11/27/21 DM1127/21023827 240 mg/kg D.W. 6.8 26 SW846: 6010C MMSD 151266-1
11/28/21 DM1128/21023899 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 151266-1
11/29/21 DM1129/21023927 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 151294-1
11/30/21 DM1130/21024167 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 151317-1
12/01/21 DM1201/21024282 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 151317-2
12/02/21 DM1202/21024297 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 151342-1
12/03/21 DM1203/21024309 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 151371-1
12/04/21 DM1204/21024329 230 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 151371-1
12/05/21 DM1205/21024739 240 mg/kg D.W. 6.7 26 Q3. SW846: 6010C MMSD 151371-1
Page 23 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
COPPER ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e •
a.
QC Batch
ID
12/06/21
DM1206/21024767
240 mg/kg D.W.
6.7
26
SW846: 6010C
MMSD
151391-1
12/07/21
DM 1207/21024782
230 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151422-1
12/08/21 DM 1208/21024816
240 mg/kg D.W. 6.7 26
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 230 mg/kg D.W. 6.8 26
SW846: 6010C MMSD 151471-2
12/10/21 DM1210/21024844 260 mg/kg D.W. 6.8 26
SW846: 6010C MMSD 151498-1
12/11/21 DM1211/21024864 250 mg/kg D.W. 6.6 25
SW846: 6010C MMSD 151498-1
12/12/21 DM1212/21025174 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 151498-1
12/13/21 DM1213/21025205 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151543-1
12/14/21 DM1214/21025220 250 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 151576-1
12/15/21 DM1215/21025299 240 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 151576-1
12/16/21 DM1216/21025314 240 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 151645-1
12/17/21 DM1217/21025326 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151645-1
12/18/21 DM1219/21025346 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151645-1
12/19/21 DM1219/21025621 240 mg/kg D.W. 6.8 26 SW846: 6010C MMSD 151645-1
12/20/21 DM1220/21025649 240 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151645-2
12/21/21 DM1221/21025664 250 mg/kg D.W. 6.8 26
SW846: 6010C MMSD 151668-1
12/22/21 DM1222/21025700 250 mg/kg D.W. 6.7 26
SW846: 6010C MMSD 151750-1
12/23/21 DM1223/21025779 260 mg/kg D.W. 6.8 26 SW846: 6010C MMSD 151750-2
12/24/21 DM1224/21025791 260 mg/kg D.W. 6.8 26 SW846: 6010C MMSD 151750-2
12/25/21 DM1225/21025811 260 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151750-2
12/26/21 DM1226/21025824 250 mg/kg D.W. 6.8 26 SW846: 6010C MMSD 151750-2
12/27/21 DM1227/21025917 260 mg/kg D.W. 6.6 25 SW846: 6010C MMSD 151750-2
12/28/21 DM1228/21025932 260 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 151750-2
12/29/21 DM1229/21025966 260 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151827-1
12/30/21 DM1230/21025981 260 mg/kg D.W. 6.7 26 SW846: 6010C MMSD 151827-1
12/31/21 DM1231/21026033 260 mg/kg D.W. 6.7 25 SW846: 6010C MMSD 151827-1
Avg Result: 240 mg/kg D.W. Min LOD: 6.4 mg/kg D.W.
Max Result: 290 mg/kg D.W. Max LOD: 6.8 mg/kg D.W.
Page 24 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
IRON ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
50000 mg/kg D.W.
82
330
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
51000 mg/kg D.W. 82 330
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
48000 mg/kg D.W. 82 330
SW846: 6010C MMSD
01/04/21 DM0104/21000488 52000 mg/kg D.W. 82 330
SW846: 6010C MMSD
01/05/21 DM0105/21000504 51000 mg/kg D.W. 83 330
SW846: 6010C MMSD
01/06/21 DM0106/21000535 51000 mg/kg D.W. 81 330
SW846: 6010C MMSD
01/07/21 DM0107/21000551 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/08/21 DM0108/21000562 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/09/21 DM0109/21000581 51000 mg/kg D.W. 83 330 SW846: 6010C MMSD
01/10/21 DM0110/21000594 48000 mg/kg D.W. 83 330 SW846: 6010C MMSD
01/11/21 DM0111/21000632 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/12/21 DM0112/21000648 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/13/21 DM0113/21000679 49000 mg/kg D.W. 81 330 SW846: 6010C MMSD
01/14/21 DM0114/21000754 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
01/15/21 DM0115/21000765 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/16/21 DM0116/21000784 49000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/17/21 DM0117/21000797 49000 mg/kg D.W. 82 330 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 52000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/19/21 DM0119/21000842 47000 mg/kg D.W. 82 330 Q3. SW846: 6010C MMSD
01/20/21 DM0120/21000926 43000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/21/21 DM0121/21000942 45000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/22/21 DM0122/21000953 46000 mg/kg D.W. 83 330 SW846: 6010C MMSD
01/23/21 DM0123/21000972 51000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/24/21 DM0124/21001059 50000 mg/kg D.W. 83 330 SW846: 6010C MMSD
01/25/21 DM0125/21001088 44000 mg/kg D.W. 83 330 SW846: 6010C MMSD
01/26/21 DM0126/21001106 45000 mg/kg D.W. 82 330 SW846: 6010C MMSD
01/27/21 DM0127/21001137 44000 mg/kg D.W. 81 330 SW846: 6010C MMSD
01/28/21 DM0128/21001153 48000 mg/kg D.W. 81 320 SW846: 6010C MMSD
01/29/21 DM0129/21001164 50000 mg/kg D.W. 80 320 SW846: 6010C MMSD
01/30/21 DM0130/21001304 54000 mg/kg D.W. 81 320 SW846: 6010C MMSD
01/31/21 DM0131/21001317 52000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/01/21 DM0201/21001344 51000 mg/kg D.W. 81 330 Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 54000 mg/kg D.W. 82 330 Q3. SW846: 6010C MMSD
02/03/21 DM0203/21001428 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/04/21 DM0204/21001444 51000 mg/kg D.W. 81 330 SW846: 6010C MMSD
02/05/21 DM0205/21001455 52000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/06/21 DM0206/21001476 51000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/07/21 DM0207/21001489 52000 mg/kg D.W. 79 320 SW846: 6010C MMSD
02/08/21 DM0208/21001609 53000 mg/kg D.W. 81 320 SW846: 6010C MMSD
02/09/21 DM0209/21001625 53000 mg/kg D.W. 81 330 SW846: 6010C MMSD
02/10/21 DM0210/21001656 49000 mg/kg D.W. 81 330 SW846: 6010C MMSD
02/11/21 DM0211/21001672 46000 mg/kg D.W. 82 330
SW846: 6010C MMSD
02/12/21 DM0212/21001706 48000 mg/kg D.W. 82 330
SW846: 6010C MMSD
02/13/21 DM0213/21001725 52000 mg/kg D.W. 81 330
SW846: 6010C MMSD
02/14/21 DM0214/21001738 55000 mg/kg D.W. 81 330 SW846: 6010C MMSD
02/15/21 DM0215/21001793 56000 mg/kg D.W. 81 330 SW846: 6010C MMSD
Page 25 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
IRON ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
55000 mg/kg D.W.
81
330
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
50000 mg/kg D.W. 82 330
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
48000 mg/kg D.W. 82 330
SW846: 6010C MMSD
02/19/21 DM0219/21001986 50000 mg/kg D.W. 81 330
SW846: 6010C MMSD
02/20/21 DM0220/21002005 50000 mg/kg D.W. 80 320
SW846: 6010C MMSD
02/21/21 DM0221/21002072 50000 mg/kg D.W. 81 320
SW846: 6010C MMSD
02/22/21 DM0222/21002230 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
02/23/21 DM0223/21002246 52000 mg/kg D.W. 81 330 SW846: 6010C MMSD
02/24/21 DM0224/21002281 49000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/25/21 DM0225/21002320 53000 mg/kg D.W. 82 330 SW846: 6010C MMSD
02/26/21 DM0226/21002386 52000 mg/kg D.W. 81 320 SW846: 6010C MMSD
02/27/21 DM0227/21002405 52000 mg/kg D.W. 80 320 SW846: 6010C MMSD
02/28/21 DM0228/21002478 50000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/01/21 DM0301/21002611 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/02/21 DM0302/21002629 45000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/03/21 DM0303/21002660 42000 mg/kg D.W. 81 320
SW846: 6010C MMSD
03/04/21 DM0304/21002717 46000 mg/kg D.W. 81 330
SW846: 6010C MMSD
03/05/21 DM0305/21002728 44000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/06/21 DM0306/21002747 42000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/07/21 DM0307/21002858 41000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/08/21 DM0308/21003336 42000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/09/21 DM0309/21003371 45000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/10/21 DM0310/21003402 44000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/11/21 DM0311/21003456 52000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/12/21 DM0312/21003522 46000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/13/21 DM0313/21003541 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/14/21 DM0314/21003554 43000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/15/21 DM0315/21003747 45000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/16/21 DM0316/21003801 50000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/17/21 DM0317/21003878 46000 mg/kg D.W. 81 330 Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 44000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/19/21 DM0319/21003905 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD
03/20/21 DM0320/21004076 49000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/21/21 DM0321/21004093 48000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/22/21 DM0322/21004120 48000 mg/kg D.W. 80 320 SW846: 6010C MMSD
03/23/21 DM0323/21004136 48000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/24/21 DM0324/21004167 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
03/25/21 DM0325/21004242 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
03/26/21 DM0326/21004253 49000 mg/kg D.W. 82 330 SW846: 6010C MMSD
03/27/21 DM0327/21004272 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD
03/28/21 DM0328/21004285 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
03/29/21 DM0329/21004312 51000 mg/kg D.W. 82 330
SW846: 6010C MMSD
03/30/21 DM0330/21004388 53000 mg/kg D.W. 82 330
SW846: 6010C MMSD
03/31/21 DM0331/21004600 52000 mg/kg D.W. 82 330
SW846: 6010C MMSD
04/01/21 DM0401/21004616 51000 mg/kg D.W. 82 330 Q3. SW846: 6010C MMSD
04/02/21 DM0402/21004627 44000 mg/kg D.W. 82 330 SW846: 6010C MMSD
Page 26 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOWN
IRON ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
41000 mg/kg D.W.
81
330
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
49000 mg/kg D.W. 80 320
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
52000 mg/kg D.W. 81 330
SW846: 6010C MMSD
04/06/21 DM0406/21004758 52000 mg/kg D.W. 81 330
SW846: 6010C MMSD
04/07/21 DM0407/21004843 50000 mg/kg D.W. 81 330
SW846: 6010C MMSD
04/08/21 DM0408/21004861 50000 mg/kg D.W. 81 330
SW846: 6010C MMSD
04/09/21 DM0409/21004912 50000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/10/21 DM0410/21004931 51000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/11/21 DM0411/21005023 51000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/12/21 DM0412/21005052 41000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/13/21 DM0413/21005199 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/14/21 DM0414/21005230 44000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/15/21 DM0415/21005248 47000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/16/21 DM0416/21005259 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/17/21 DM0417/21005468 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/18/21 DM0418/21005481 46000 mg/kg D.W. 82 330
SW846: 6010C MMSD
04/19/21 DM0419/21005508 45000 mg/kg D.W. 83 330
SW846: 6010C MMSD
04/20/21 DM0420/21005839 52000 mg/kg D.W. 82 330 SW846: 6010C MMSD
04/21/21 DM0421/21005870 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/22/21 DM0422/21005981 51000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/23/21 DM0423/21005992 51000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/24/21 DM0424/21006057 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/25/21 DM0425/21006272 50000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/26/21 DM0426/21006299 49000 mg/kg D.W. 80 320 SW846: 6010C MMSD
04/27/21 DM0427/21006315 55000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/28/21 DM0428/21006346 53000 mg/kg D.W. 81 330 SW846: 6010C MMSD
04/29/21 DM0429/21006362 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
04/30/21 DM0430/21006373 46000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/01/21 DM0501/21006429 43000 mg/kg D.W. 81 320 SW846: 6010C MMSD
05/02/21 DM0502/21006442 41000 mg/kg D.W. 81 320 SW846: 6010C MMSD
05/03/21 DM0503/21006676 42000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/04/21 DM0504/21006691 50000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/05/21 DM0505/21006722 42000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/06/21 DM0506/21006781 41000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/07/21 DM0507/21006834 40000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/08/21 DM0508/21006981 40000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/09/21 DM0509/21006994 40000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/10/21 DM0510/21007021 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD
05/11/21 DM0511/21007171 44000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/12/21 DM0512/21007202 45000 mg/kg D.W. 81 320 SW846: 6010C MMSD
05/13/21 DM0513/21007217 52000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/14/21 DM0514/21007309 48000 mg/kg D.W. 81 330
SW846: 6010C MMSD
05/15/21 DM0515/21007328 46000 mg/kg D.W. 81 320
SW846: 6010C MMSD
05/16/21 DM0516/21007341 48000 mg/kg D.W. 80 320
SW846: 6010C MMSD
05/17/21 DM0517/21007382 46000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/18/21 DM0518/21007440 50000 mg/kg D.W. 81 330 SW846: 6010C MMSD
Page 27 of 121
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MMSD
PARTNERS FOI A CLIMB E1n* r 1
IRON ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
48000 mg/kg D.W.
81
320
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
44000 mg/kg D.W. 82 330
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
46000 mg/kg D.W. 82 330
SW846: 6010C MMSD
05/22/21 DM0522/21008072 48000 mg/kg D.W. 82 330
SW846: 6010C MMSD
05/23/21 DM0523/21008085 49000 mg/kg D.W. 81 330
SW846: 6010C MMSD
05/25/21 DM0525/21008288 49000 mg/kg D.W. 80 320
SW846: 6010C MMSD
05/26/21 DM0526/21008319 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
05/27/21 DM0527/21008484 55000 mg/kg D.W. 80 320 SW846: 6010C MMSD
05/28/21 DM0528/21008495 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/29/21 DM0529/21008515 47000 mg/kg D.W. 81 330 SW846: 6010C MMSD
05/30/21 DM0530/21008530 46000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/01/21 DM0601/21008902 56000 mg/kg D.W. 80 320 SW846: 6010C MMSD
06/02/21 DM0602/21008935 52000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/03/21 DM0603/21008950 51000 mg/kg D.W. 80 320 SW846: 6010C MMSD
06/04/21 DM0604/21009184 53000 mg/kg D.W. 80 320 SW846: 6010C MMSD
06/05/21 DM0605/21009203 49000 mg/kg D.W. 81 320
SW846: 6010C MMSD
06/06/21 DM0606/21009287 48000 mg/kg D.W. 81 320
SW846: 6010C MMSD
06/07/21 DM0607/21009314 48000 mg/kg D.W. 80 320 SW846: 6010C MMSD
06/08/21 DM0608/21009334 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/09/21 DM0609/21009365 47000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/10/21 DM0610/21009538 46000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/11/21 DM0611/21009549 53000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/12/21 DM0612/21009568 54000 mg/kg D.W. 82 330 SW846: 6010C MMSD
06/13/21 DM0613/21009602 55000 mg/kg D.W. 82 330 SW846: 6010C MMSD
06/14/21 DM0614/21009629 54000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/18/21 DM0618/21009979 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD
06/19/21 DM0619/21010314 46000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/20/21 DM0620/21010332 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/21/21 DM0621/21010359 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/22/21 DM0622/21010375 54000 mg/kg D.W. 80 320 SW846: 6010C MMSD
06/23/21 DM0623/21010408 57000 mg/kg D.W. 81 320 SW846: 6010C MMSD
06/24/21 DM0624/21010670 57000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/25/21 DM0625/21010681 56000 mg/kg D.W. 82 330 SW846: 6010C MMSD
06/26/21 DM0626/21010702 55000 mg/kg D.W. 83 330 SW846: 6010C MMSD
06/27/21 DM0627/21010807 54000 mg/kg D.W. 82 330 SW846: 6010C MMSD
06/28/21 DM0628/21010860 54000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/29/21 DM0629/21010875 59000 mg/kg D.W. 81 330 SW846: 6010C MMSD
06/30/21 DM0630/21011438 53000 mg/kg D.W. 81 330 SW846: 6010C MMSD
07/01/21 DM0701/21011453 53000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/02/21 DM0702/21011465 47000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/03/21 DM0703/21011485 48000 mg/kg D.W. 81 330 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 54000 mg/kg D.W. 81 320
SW846: 6010C MMSD
07/05/21 DM0705/21011572 50000 mg/kg D.W. 81 330
SW846: 6010C MMSD
07/06/21 DM0706/21011693 50000 mg/kg D.W. 81 320
SW846: 6010C MMSD
07/07/21 DM0707/21011727 51000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/08/21 DM0708/21011742 50000 mg/kg D.W. 81 320 SW846: 6010C MMSD
Page 28 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
IRON ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
52000 mg/kg D.W.
80
320
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
49000 mg/kg D.W. 80 320
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
50000 mg/kg D.W. 80 320
SW846: 6010C MMSD
07/12/21 DM0712/21012283 50000 mg/kg D.W. 80 320
SW846: 6010C MMSD
07/13/21 DM0713/21012298 54000 mg/kg D.W. 80 320
SW846: 6010C MMSD
07/14/21 DM0714/21012332 53000 mg/kg D.W. 80 320
SW846: 6010C MMSD
07/15/21 DM0715/21012390 53000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/16/21 DM0716/21012563 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/17/21 DM0717/21012583 50000 mg/kg D.W. 81 330 SW846: 6010C MMSD
07/18/21 DM0718/21012596 52000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/19/21 DM0719/21012624 55000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/20/21 DM0720/21012639 62000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/21/21 DM0721/21012760 58000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/22/21 DM0722/21012775 57000 mg/kg D.W. 82 330 SW846: 6010C MMSD
07/23/21 DM0723/21013074 54000 mg/kg D.W. 82 330 SW846: 6010C MMSD
07/24/21 DM0724/21013378 55000 mg/kg D.W. 81 330
SW846: 6010C MMSD
07/25/21 DM0725/21013391 56000 mg/kg D.W. 81 320
SW846: 6010C MMSD
07/26/21 DM0726/21013419 58000 mg/kg D.W. 81 330 SW846: 6010C MMSD
07/27/21 DM0727/21013434 62000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/28/21 DM0728/21013470 60000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/29/21 DM0729/21013614 56000 mg/kg D.W. 81 320 SW846: 6010C MMSD
07/30/21 DM0730/21013629 55000 mg/kg D.W. 80 320 SW846: 6010C MMSD
07/31/21 DM0731/21013739 56000 mg/kg D.W. 81 330 SW846: 6010C MMSD
08/01/21 DM0801/21013752 56000 mg/kg D.W. 81 330 SW846: 6010C MMSD
08/02/21 DM0802/21013891 60000 mg/kg D.W. 81 330 SW846: 6010C MMSD
08/03/21 DM0803/21013906 61000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/04/21 DM0804/21013940 58000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/05/21 DM0805/21014673 62000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/06/21 DM0806/21014685 56000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/07/21 DM0807/21014705 55000 mg/kg D.W. 81 320 SW846: 6010C MMSD
08/08/21 DM0809/21014718 55000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/09/21 DM0809/21014746 53000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/10/21 DM0810/21014847 59000 mg/kg D.W. 81 320 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 55000 mg/kg D.W. 81 330 SW846: 6010C MMSD
08/12/21 DM0812/21015285 58000 mg/kg D.W. 81 330 SW846: 6010C MMSD
08/13/21 DM0813/21015297 52000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/14/21 DM0814/21015317 45000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/15/21 DM0815/21015330 44000 mg/kg D.W. 79 320 SW846: 6010C MMSD
08/16/21 DM0816/21015410 48000 mg/kg D.W. 79 320 SW846: 6010C MMSD
08/17/21 DM0817/21015425 55000 mg/kg D.W. 79 320 SW846: 6010C MMSD
08/18/21 DM0818/21016031 53000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/19/21 DM0819/21016046 54000 mg/kg D.W. 80 320
SW846: 6010C MMSD
08/20/21 DM0820/21016068 51000 mg/kg D.W. 80 320
SW846: 6010C MMSD
08/21/21 DM0821/21016088 54000 mg/kg D.W. 80 320
SW846: 6010C MMSD
08/22/21 DM0822/21016196 53000 mg/kg D.W. 80 320 SW846: 6010C MMSD
08/23/21 DM0823/21016224 54000 mg/kg D.W. 80 320 SW846: 6010C MMSD
Page 29 of 121
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MMSD
PARTAFRS FOI A OAR NNW
IRON ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
52000 mg/kg D.W.
81
320
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
52000 mg/kg D.W. 80 320
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
51000 mg/kg D.W. 81 320
SW846: 6010C MMSD
08/27/21 DM0827/21016407 52000 mg/kg D.W. 81 320
SW846: 6010C MMSD
08/28/21 DM0828/21016427 51000 mg/kg D.W. 81 320
SW846: 6010C MMSD
08/30/21 DM0830/21016468 50000 mg/kg D.W. 80 320
SW846: 6010C MMSD
08/31/21 DM0831/21016483 50000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/01/21 DM0901/21016598 51000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/02/21 DM0902/21016659 45000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/03/21 DM0903/21016671 42000 mg/kg D.W. 81 330 SW846: 6010C MMSD
09/04/21 DM0904/21017055 40000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/05/21 DM0905/21017068 41000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/06/21 DM0906/21017096 41000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/07/21 DM0907/21017306 41000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/08/21 DM0908/21017338 46000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/09/21 DM0909/21017408 53000 mg/kg D.W. 81 320
SW846: 6010C MMSD
09/10/21 DM0910/21017420 50000 mg/kg D.W. 81 320
SW846: 6010C MMSD
09/11/21 DM0911/21017699 51000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/12/21 DM0912/21017712 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD
09/13/21 DM0913/21017740 46000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/14/21 DM0914/21017755 54000 mg/kg D.W. 81 320 SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 51000 mg/kg D.W. 81 320 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 49000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150012-1
09/17/21 DM0917/21018105 47000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 49000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 51000 mg/kg D.W. 82 330 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 52000 mg/kg D.W. 82 330 SW846: 6010C MMSD 150123-1
09/21/21 DM0921/21018251 51000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150123-1
09/22/21 DM0922/21018480 45000 mg/kg D.W. 81 320 SW846: 6010C MMSD
09/23/21 DM0923/21018564 44000 mg/kg D.W. 80 320 SW846: 6010C MMSD
09/24/21 DM0924/21018818 46000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 48000 mg/kg D.W. 79 320 SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 49000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 50000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 44000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 45000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 46000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 47000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 50000 mg/kg D.W. 81 320 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 53000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150431-1
10/07/21 DM1007/21019760 52000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150431-1
10/08/21 DM1008/21019772 55000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 51000 mg/kg D.W. 79 320 SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 51000 mg/kg D.W. 81 320 SW846: 6010C MMSD 150655-1
Page 30 of 121
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MMSD
PARTNERS FOI A CLIMB NNW
IRON ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
10/21/21
DM 1021 /21020689
46000 mg/kg D.W.
80
320
SW846: 6010C
MMSD
150655-1
10/22/21
DM 1022/21020701
48000 mg/kg D.W. 80 320
SW846: 6010C
MMSD 150703-1
10/23/21 DM1023/21020883
47000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150703-1
10/24/21 DM1024/21021034 48000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 46000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 48000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 49000 mg/kg D.W. 81 320 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 48000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150831-1
10/29/21 DM1029/21021510 47000 mg/kg D.W. 81 320 SW846: 6010C MMSD 150831-1
10/30/21 DM1030/21021530 47000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150831-1
10/31/21 DM1031/21021574 49000 mg/kg D.W. 82 330 SW846: 6010C MMSD 150831-1
11/01/21 DM1101/21021608 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 150831-1
11/02/21 DM1102/21021623 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 47000 mg/kg D.W. 81 320 SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 48000 mg/kg D.W. 80 320 SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 54000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 53000 mg/kg D.W. 80 320
SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 50000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 46000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 47000 mg/kg D.W. 81 330 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151039-2
11/11/21 DM1111/21022695 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 46000 mg/kg D.W. 81 330 SW846: 6010C MMSD 151039-1
11/14/21 DM1114/21022744 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 47000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151085-1
11/16/21 DM1116/21022787 47000 mg/kg D.W. 81 320 SW846: 6010C MMSD 151085-1
11/17/21 DM1117/21023039 47000 mg/kg D.W. 81 330 Q3. SW846: 6010C MMSD 151122-1
11/18/21 DM1118/21023056 45000 mg/kg D.W. 81 320 SW846: 6010C MMSD 151122-1
11/19/21 DM1119/21023181 44000 mg/kg D.W. 81 330 SW846: 6010C MMSD 151175-1
11/20/21 DM1120/21023201 45000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151175-1
11/21/21 DM1121/21023214 47000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151175-1
11/22/21 DM1122/21023555 48000 mg/kg D.W. 83 330 SW846: 6010C MMSD 151175-1
11/23/21 DM1123/21023570 44000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151252-1
11/24/21 DM1124/21023611 48000 mg/kg D.W. 81 330 SW846: 6010C MMSD 151266-1
11/25/21 DM1125/21023795 49000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151266-1
11/26/21 DM1126/21023807 45000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151266-1
11/27/21 DM1127/21023827 47000 mg/kg D.W. 83 330 SW846: 6010C MMSD 151266-1
11/28/21 DM1128/21023899 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151266-1
11/29/21 DM1129/21023927 45000 mg/kg D.W. 80 320 SW846: 6010C MMSD 151294-1
11/30/21 DM1130/21024167 46000 mg/kg D.W. 81 320 SW846: 6010C MMSD 151317-1
12/01/21 DM1201/21024282 47000 mg/kg D.W. 80 320
SW846: 6010C MMSD 151317-2
12/02/21 DM1202/21024297 47000 mg/kg D.W. 81 320
SW846: 6010C MMSD 151342-1
12/03/21 DM1203/21024309 47000 mg/kg D.W. 81 320
SW846: 6010C MMSD 151371-1
12/04/21 DM1204/21024329 43000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151371-1
12/05/21 DM1205/21024739 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151371-1
Page 31 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
IRON ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a.
QC Batch
ID
12/06/21
DM1206/21024767
48000 mg/kg D.W.
82
330
SW846: 6010C
MMSD
151391-1
12/07/21
DM 1207/21024782
43000 mg/kg D.W. 82 330
SW846: 6010C
MMSD 151422-1
12/08/21 DM 1208/21024816
42000 mg/kg D.W. 82 330
SW846: 6010C MMSD 151471-1
12/09/21 DM1209/21024832 42000 mg/kg D.W. 83 330
SW846: 6010C MMSD 151471-2
12/10/21 DM1210/21024844 44000 mg/kg D.W. 83 330
SW846: 6010C MMSD 151498-1
12/11/21 DM1211/21024864 45000 mg/kg D.W. 81 320
SW846: 6010C MMSD 151498-1
12/12/21 DM1212/21025174 46000 mg/kg D.W. 80 320 SW846: 6010C MMSD 151498-1
12/13/21 DM1213/21025205 44000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151543-1
12/14/21 DM1214/21025220 49000 mg/kg D.W. 81 330 SW846: 6010C MMSD 151576-1
12/15/21 DM1215/21025299 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151576-1
12/16/21 DM1216/21025314 46000 mg/kg D.W. 81 330 SW846: 6010C MMSD 151645-1
12/17/21 DM1217/21025326 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151645-1
12/18/21 DM1219/21025346 48000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151645-1
12/19/21 DM1219/21025621 49000 mg/kg D.W. 83 330 SW846: 6010C MMSD 151645-1
12/20/21 DM1220/21025649 49000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151645-2
12/21/21 DM1221/21025664 48000 mg/kg D.W. 82 330
SW846: 6010C MMSD 151668-1
12/22/21 DM1222/21025700 48000 mg/kg D.W. 82 330
SW846: 6010C MMSD 151750-1
12/23/21 DM1223/21025779 47000 mg/kg D.W. 83 330 SW846: 6010C MMSD 151750-2
12/24/21 DM1224/21025791 47000 mg/kg D.W. 83 340 SW846: 6010C MMSD 151750-2
12/25/21 DM1225/21025811 47000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151750-2
12/26/21 DM1226/21025824 46000 mg/kg D.W. 83 330 SW846: 6010C MMSD 151750-2
12/27/21 DM1227/21025917 47000 mg/kg D.W. 81 330 SW846: 6010C MMSD 151750-2
12/28/21 DM1228/21025932 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151750-2
12/29/21 DM1229/21025966 47000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151827-1
12/30/21 DM1230/21025981 45000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151827-1
12/31/21 DM1231/21026033 46000 mg/kg D.W. 82 330 SW846: 6010C MMSD 151827-1
Avg Result: 49000 mg/kg D.W. Min LOD: 79 mg/kg D.W.
Max Result: 62000 mg/kg D.W. Max LOD: 83 mg/kg D.W.
Page 32 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
LEAD ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
16 mg/kg D.W.
1.3
5.3
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
16 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
15 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
01/04/21 DM0104/21000488 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/05/21 DM0105/21000504 16 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
01/06/21 DM0106/21000535 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/07/21 DM0107/21000551 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/08/21 DM0108/21000562 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/09/21 DM0109/21000581 16 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
01/10/21 DM0110/21000594 15 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
01/11/21 DM0111/21000632 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/12/21 DM0112/21000648 14 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/13/21 DM0113/21000679 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/14/21 DM0114/21000754 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/15/21 DM0115/21000765 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/16/21 DM0116/21000784 14 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
01/17/21 DM0117/21000797 15 mg/kg D.W. 1.3 5.3 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 18 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
01/19/21 DM0119/21000842 20 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/20/21 DM0120/21000926 19 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/21/21 DM0121/21000942 22 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/22/21 DM0122/21000953 18 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
01/23/21 DM0123/21000972 19 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/24/21 DM0124/21001059 18 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
01/25/21 DM0125/21001088 14 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
01/26/21 DM0126/21001106 16 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
01/27/21 DM0127/21001137 17 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
01/28/21 DM0128/21001153 16 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
01/29/21 DM0129/21001164 16 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
01/30/21 DM0130/21001304 19 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
01/31/21 DM0131/21001317 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/01/21 DM0201/21001344 16 mg/kg D.W. 1.3 5.3 Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 18 mg/kg D.W. 1.3 5.3 D2. SW846: 6010C MMSD
02/03/21 DM0203/21001428 14 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/04/21 DM0204/21001444 18 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/05/21 DM0205/21001455 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/06/21 DM0206/21001476 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/07/21 DM0207/21001489 15 mg/kg D.W. 1.2 5.1
SW846: 6010C MMSD
02/08/21 DM0208/21001609 14 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
02/09/21 DM0209/21001625 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/10/21 DM0210/21001656 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/11/21
02/12/21
02/13/21
DM0211/21001672
DM0212/21001706
DM0213/21001725
16 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
17 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
15 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
02/14/21 DM0214/21001738 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/15/21 DM0215/21001793 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
Page 33 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
LEAD ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
15 mg/kg D.W.
1.3
5.3
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
12 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
14 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
02/19/21 DM0219/21001986 12 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/20/21 DM0220/21002005 11 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
02/21/21 DM0221/21002072 11 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
02/22/21 DM0222/21002230 12 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
02/23/21 DM0223/21002246 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/24/21 DM0224/21002281 14 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
02/25/21 DM0225/21002320 12 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
02/26/21 DM0226/21002386 15 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
02/27/21 DM0227/21002405 16 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
02/28/21 DM0228/21002478 17 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/01/21 DM0301/21002611 14 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/02/21 DM0302/21002629 18 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/03/21
03/04/21
DM0303/21002660
DM0304/21002717
15 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
19 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
03/05/21 DM0305/21002728 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
03/06/21 DM0306/21002747 15 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/07/21 DM0307/21002858 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
03/08/21 DM0308/21003336 14 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
03/09/21 DM0309/21003371 16 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/10/21 DM0310/21003402 14 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/11/21 DM0311/21003456 19 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
03/12/21 DM0312/21003522 18 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/13/21 DM0313/21003541 18 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/14/21 DM0314/21003554 16 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/15/21 DM0315/21003747 17 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/16/21 DM0316/21003801 18 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/17/21 DM0317/21003878 17 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
03/18/21 DM0318/21003894 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
03/19/21 DM0319/21003905 19 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
03/20/21 DM0320/21004076 17 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/21/21 DM0321/21004093 16 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/22/21 DM0322/21004120 15 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
03/23/21 DM0323/21004136 15 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
03/24/21 DM0324/21004167 14 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
03/25/21 DM0325/21004242 17 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
03/26/21 DM0326/21004253 18 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
03/27/21 DM0327/21004272 17 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
03/28/21 DM0328/21004285 18 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
03/29/21
03/30/21
03/31/21
DM0329/21004312
DM0330/21004388
DM0331/21004600
16 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
22 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
16 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
04/01/21 DM0401/21004616 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/02/21 DM0402/21004627 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
Page 34 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOWN
LEAD ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
17 mg/kg D.W.
1.3
5.3
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
15 mg/kg D.W.
1.2 5.2
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
15 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
04/06/21 DM0406/21004758 19 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/07/21 DM0407/21004843 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/08/21 DM0408/21004861 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/09/21 DM0409/21004912 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/10/21 DM0410/21004931 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/11/21 DM0411/21005023 24 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/12/21 DM0412/21005052 20 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/13/21 DM0413/21005199 23 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/14/21 DM0414/21005230 18 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/15/21 DM0415/21005248 19 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
04/16/21 DM0416/21005259 17 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/17/21 DM0417/21005468 17 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/18/21
04/19/21
DM0418/21005481
DM0419/21005508
18 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
17 mg/kg D.W.
1.3 5.4
SW846: 6010C MMSD
04/20/21 DM0420/21005839 21 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
04/21/21 DM0421/21005870 17 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
04/22/21 DM0422/21005981 18 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
04/23/21 DM0423/21005992 17 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
04/24/21 DM0424/21006057 17 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
04/25/21 DM0425/21006272 19 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/26/21 DM0426/21006299 16 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
04/27/21 DM0427/21006315 19 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
04/28/21 DM0428/21006346 16 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
04/29/21 DM0429/21006362 15 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
04/30/21 DM0430/21006373 15 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
05/01/21 DM0501/21006429 16 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
05/02/21 DM0502/21006442 16 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
05/03/21 DM0503/21006676 15 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
05/04/21 DM0504/21006691 19 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
05/05/21 DM0505/21006722 17 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
05/06/21 DM0506/21006781 19 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
05/07/21 DM0507/21006834 21 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
05/08/21 DM0508/21006981 20 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
05/09/21 DM0509/21006994 20 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
05/10/21 DM0510/21007021 18 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
05/11/21 DM0511/21007171 20 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
05/12/21 DM0512/21007202 21 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
05/13/21 DM0513/21007217 22 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
05/14/21
05/15/21
05/16/21
DM0514/21007309
DM0515/21007328
DM0516/21007341
19 mg/kg D.W.
1.3 5.2
SW846: 6010C MMSD
19 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
23 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
05/17/21 DM0517/21007382 53 mg/kg D.W. 1.2 5.2 Q3. SW846: 6010C MMSD
05/18/21 DM0518/21007440 38 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
Page 35 of 121
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MMSD
PARTNERS FOI A CLIMB E1n* r 1
LEAD ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
22 mg/kg D.W.
1.2
5.2
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
32 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
26 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
05/22/21 DM0522/21008072 27 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
05/23/21 DM0523/21008085 27 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
05/25/21 DM0525/21008288 21 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
05/26/21 DM0526/21008319 21 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
05/27/21 DM0527/21008484 24 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
05/28/21 DM0528/21008495 22 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
05/29/21 DM0529/21008515 21 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
05/30/21 DM0530/21008530 20 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
06/01/21 DM0601/21008902 31 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
06/02/21 DM0602/21008935 27 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
06/03/21 DM0603/21008950 21 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
06/04/21 DM0604/21009184 27 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
06/05/21
06/06/21
DM0605/21009203
DM0606/21009287
44 mg/kg D.W.
1.3 5.2
SW846: 6010C MMSD
22 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
06/07/21 DM0607/21009314 27 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
06/08/21 DM0608/21009334 33 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
06/09/21 DM0609/21009365 20 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
06/10/21 DM0610/21009538 24 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
06/11/21 DM0611/21009549 28 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
06/12/21 DM0612/21009568 29 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
06/13/21 DM0613/21009602 47 mg/kg D.W. 1.3 5.3 Q3. SW846: 6010C MMSD
06/14/21 DM0614/21009629 24 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
06/18/21 DM0618/21009979 21 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
06/19/21 DM0619/21010314 30 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
06/20/21 DM0620/21010332 21 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
06/21/21 DM0621/21010359 32 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
06/22/21 DM0622/21010375 22 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
06/23/21 DM0623/21010408 34 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
06/24/21 DM0624/21010670 25 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
06/25/21 DM0625/21010681 23 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
06/26/21 DM0626/21010702 27 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD
06/27/21 DM0627/21010807 26 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
06/28/21 DM0628/21010860 26 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
06/29/21 DM0629/21010875 28 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
06/30/21 DM0630/21011438 23 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
07/01/21 DM0701/21011453 42 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
07/02/21 DM0702/21011465 40 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/03/21 DM0703/21011485 31 mg/kg D.W. 1.3 5.3 T9. SW846: 6010C MMSD
07/04/21
07/05/21
07/06/21
DM0704/21011516
DM0705/21011572
DM0706/21011693
29 mg/kg D.W.
1.3 5.2
SW846: 6010C MMSD
28 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD
31 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
07/07/21 DM0707/21011727 31 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/08/21 DM0708/21011742 32 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
Page 36 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
LEAD ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
31 mg/kg D.W.
1.2
5.2
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
30 mg/kg D.W.
1.2 5.2
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
28 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
07/12/21 DM0712/21012283 29 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/13/21 DM0713/21012298 34 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/14/21 DM0714/21012332 28 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/15/21 DM0715/21012390 28 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/16/21 DM0716/21012563 34 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/17/21 DM0717/21012583 32 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
07/18/21 DM0718/21012596 33 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/19/21 DM0719/21012624 31 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/20/21 DM0720/21012639 64 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/21/21 DM0721/21012760 52 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/22/21 DM0722/21012775 69 mg/kg D.W. 1.3 5.3 Q3. SW846: 6010C MMSD
07/23/21 DM0723/21013074 83 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
07/24/21 DM0724/21013378 94 mg/kg D.W. 1.3 5.3 SW846: 6010C MMSD
07/25/21 DM0725/21013391 48 mg/kg D.W. 1.3 5.2 Q2. SW846: 6010C MMSD
07/26/21 DM0726/21013419 50 mg/kg D.W. 1.3 5.3 Q2. SW846: 6010C MMSD
07/27/21 DM0727/21013434 44 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
07/28/21 DM0728/21013470 29 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/29/21 DM0729/21013614 28 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/30/21 DM0730/21013629 28 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
07/31/21 DM0731/21013739 31 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
08/01/21 DM0801/21013752 26 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
08/02/21 DM0802/21013891 26 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
08/03/21 DM0803/21013906 33 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/04/21 DM0804/21013940 38 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/05/21 DM0805/21014673 35 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/06/21 DM0806/21014685 27 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/07/21 DM0807/21014705 30 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/08/21 DM0809/21014718 30 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/09/21 DM0809/21014746 35 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/10/21 DM0810/21014847 43 mg/kg D.W. 1.2 5.2 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 41 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
08/12/21 DM0812/21015285 41 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
08/13/21 DM0813/21015297 40 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/14/21 DM0814/21015317 52 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/15/21 DM0815/21015330 60 mg/kg D.W. 1.2 5.1
SW846: 6010C MMSD
08/16/21 DM0816/21015410 84 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/17/21 DM0817/21015425 58 mg/kg D.W. 1.2 5.1
SW846: 6010C MMSD
08/18/21 DM0818/21016031 59 mg/kg D.W. 1.2 5.2 Q2. SW846: 6010C MMSD
08/19/21
08/20/21
08/21/21
DM0819/21016046
DM0820/21016068
DM0821/21016088
49 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
100 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
40 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
08/22/21 DM0822/21016196 45 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/23/21 DM0823/21016224 37 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
Page 37 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
LEAD ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
40 mg/kg D.W.
1.2
5.2
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
41 mg/kg D.W.
1.2 5.2
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
42 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD
08/27/21 DM0827/21016407 38 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
08/28/21 DM0828/21016427 38 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
08/30/21 DM0830/21016468 39 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
08/31/21 DM0831/21016483 50 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
09/01/21 DM0901/21016598 43 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
09/02/21 DM0902/21016659 44 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
09/03/21 DM0903/21016671 48 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
09/04/21 DM0904/21017055 52 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
09/05/21 DM0905/21017068 49 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
09/06/21 DM0906/21017096 50 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
09/07/21 DM0907/21017306 50 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
09/08/21 DM0908/21017338 47 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
09/09/21
09/10/21
DM0909/21017408
DM0910/21017420
40 mg/kg D.W.
1.3 5.2
SW846: 6010C MMSD
42 mg/kg D.W.
1.3 5.2
SW846: 6010C MMSD
09/11/21 DM0911/21017699 40 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
09/12/21 DM0912/21017712 39 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD
09/13/21 DM0913/21017740 40 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD
09/14/21 DM0914/21017755 39 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 41 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 45 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150012-1
09/17/21 DM0917/21018105 48 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 43 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 40 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 38 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150123-1
09/21/21 DM0921/21018251 42 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD 150123-1
09/22/21 DM0922/21018480 45 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
09/23/21 DM0923/21018564 42 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD
09/24/21 DM0924/21018818 44 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 41 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 39 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 37 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 38 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 35 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 35 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 34 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 33 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 32 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 31 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD 150376-1
10/06/21
10/07/21
10/08/21
DM1006/21019735
DM1007/21019760
DM1008/21019772
29 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 150431-1
28 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 150431-1
28 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 28 mg/kg D.W. 1.2 5.1
SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 32 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150655-1
Page 38 of 121
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MMSD
PARTNERS FOI A CLIMB MOM
LEAD ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
10/21/21
DM 1021 /21020689
27 mg/kg D.W.
1.2
5.2
SW846: 6010C
MMSD
150655-1
10/22/21
DM 1022/21020701
30 mg/kg D.W.
1.2 5.2
SW846: 6010C
MMSD 150703-1
10/23/21 DM1023/21020883
29 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 150703-1
10/24/21 DM1024/21021034 28 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 30 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 31 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 29 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 25 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150831-1
10/29/21 DM1029/21021510 25 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150831-1
10/30/21 DM1030/21021530 25 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150831-1
10/31/21 DM1031/21021574 25 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150831-1
11/01/21 DM1101/21021608 24 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150831-1
11/02/21 DM1102/21021623 26 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 26 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 24 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 150884-1
11/05/21
11/06/21
DM1105/21021747
DM1106/21021767
26 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 150964-1
24 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 23 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 23 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 24 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 24 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151039-2
11/11/21 DM1111/21022695 24 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 25 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 26 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151039-1
11/14/21 DM1114/21022744 24 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 24 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151085-1
11/16/21 DM1116/21022787 26 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 151085-1
11/17/21 DM1117/21023039 29 mg/kg D.W. 1.3 5.2
SW846: 6010C MMSD 151122-1
11/18/21 DM1118/21023056 22 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 151122-1
11/19/21 DM1119/21023181 25 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151175-1
11/20/21 DM1120/21023201 28 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151175-1
11/21/21 DM1121/21023214 23 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD 151175-1
11/22/21 DM1122/21023555 22 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD 151175-1
11/23/21 DM1123/21023570 19 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151252-1
11/24/21 DM1124/21023611 22 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151266-1
11/25/21 DM1125/21023795 26 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151266-1
11/26/21 DM1126/21023807 20 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151266-1
11/27/21 DM1127/21023827 24 mg/kg D.W. 1.3 5.4
SW846: 6010C MMSD 151266-1
11/28/21 DM1128/21023899 22 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151266-1
11/29/21 DM1129/21023927 22 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 151294-1
11/30/21 DM1130/21024167 23 mg/kg D.W. 1.2 5.2
SW846: 6010C MMSD 151317-1
12/01/21
12/02/21
12/03/21
DM 1201 /21024282
DM 1202/21024297
DM 1203/21024309
23 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 151317-2
21 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 151342-1
20 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 151371-1
12/04/21 DM1204/21024329 19 mg/kg D.W. 1.3 5.3
SW846: 6010C MMSD 151371-1
12/05/21 DM1205/21024739 19 mg/kg D.W. 1.3 5.3 D2, Q3. SW846: 6010C MMSD 151371-1
Page 39 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
LEAD ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result
LOD LOQ QA Flags
Ana Ica ' e • a.
QC Batch
ID
12/06/21
DM1206/21024767
23 mg/kg D.W.
1.3
5.3
SW846: 6010C
MMSD
151391-1
12/07/21
DM 1207/21024782
20 mg/kg D.W.
1.3 5.3
SW846: 6010C
MMSD 151422-1
12/08/21 DM 1208/21024816
21 mg/kg D.W.
1.3 5.4
SW846: 6010C MMSD 151471-1
12/09/21 DM1209/21024832 20 mg/kg D.W.
1.3 5.4
SW846: 6010C MMSD 151471-2
12/10/21 DM1210/21024844 21 mg/kg D.W.
1.3 5.4
SW846: 6010C MMSD 151498-1
12/11/21 DM1211/21024864 20 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 151498-1
12/12/21 DM1212/21025174 21 mg/kg D.W.
1.2 5.2
SW846: 6010C MMSD 151498-1
12/13/21 DM1213/21025205 22 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151543-1
12/14/21 DM1214/21025220 40 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151576-1
12/15/21 DM1215/21025299 24 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151576-1
12/16/21 DM1216/21025314 27 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151645-1
12/17/21 DM1217/21025326 23 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151645-1
12/18/21 DM1219/21025346 22 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151645-1
12/19/21 DM1219/21025621 21 mg/kg D.W.
1.3 5.4
SW846: 6010C MMSD 151645-1
12/20/21 DM1220/21025649 20 mg/kg D.W.
1.3 5.4
SW846: 6010C MMSD 151645-2
12/21/21
12/22/21
DM 1221 /21025664
DM1222/21025700
20 mg/kg D.W.
1.3 5.4
SW846: 6010C MMSD 151668-1
22 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151750-1
12/23/21 DM1223/21025779 20 mg/kg D.W.
1.3 5.4
SW846: 6010C MMSD 151750-2
12/24/21 DM1224/21025791 20 mg/kg D.W.
1.3 5.4
SW846: 6010C MMSD 151750-2
12/25/21 DM1225/21025811 19 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151750-2
12/26/21 DM1226/21025824 19 mg/kg D.W.
1.3 5.4
SW846: 6010C MMSD 151750-2
12/27/21 DM1227/21025917 20 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151750-2
12/28/21 DM1228/21025932 20 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151750-2
12/29/21 DM1229/21025966 21 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151827-1
12/30/21 DM1230/21025981 22 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151827-1
12/31/21 DM1231/21026033 21 mg/kg D.W.
1.3 5.3
SW846: 6010C MMSD 151827-1
Avg Result: 26 mg/kg D.W. Min LOD: 1.2 mg/kg D.W.
Max Result: 100 mg/kg D.W. Max LOD: 1.3 mg/kg D.W.
Page 40 of 121
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MMSD
PARTNERS FOI II CLIMB DINAM M
MOLYBDENUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
9.5 mg/kg D.W.
0.44
1.7
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
9.7 mg/kg D.W.
0.44 1.7
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
9.2 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
01/04/21 DM0104/21000488 9.6 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/05/21 DM0105/21000504 9.6 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/06/21 DM0106/21000535 9.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
01/07/21 DM0107/21000551 9.5 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
01/08/21 DM0108/21000562 9.5 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/09/21 DM0109/21000581 9.5 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/10/21 DM0110/21000594 9.1 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/11/21 DM0111/21000632 9.3 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/12/21 DM0112/21000648 9.3 mg/kg D.W. 0.44 1.7 Q3. SW846: 6010C MMSD
01/13/21 DM0113/21000679 9.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
01/14/21 DM0114/21000754 9.4 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
01/15/21 DM0115/21000765 9.1 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
01/16/21
01/17/21
DM0116/21000784
DM0117/21000797
9.1 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
9.3 mg/kg D.W. 0.44
1.7 Q3.
SW846: 6010C MMSD
01/18/21 DM0118/21000824 10 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/19/21 DM0119/21000842 9.4 mg/kg D.W. 0.44 1.7 Q3. SW846: 6010C MMSD
01/20/21 DM0120/21000926 9.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
01/21/21 DM0121/21000942 9.6 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/22/21 DM0122/21000953 10 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/23/21 DM0123/21000972 10 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/24/21 DM0124/21001059 9.9 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/25/21 DM0125/21001088 8.5 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/26/21 DM0126/21001106 8.7 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
01/27/21 DM0127/21001137 8.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
01/28/21 DM0128/21001153 9.4 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
01/29/21 DM0129/21001164 10 mg/kg D.W. 0.42 1.6
SW846: 6010C MMSD
01/30/21 DM0130/21001304 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
01/31/21 DM0131/21001317 9.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/01/21 DM0201/21001344 8.7 mg/kg D.W. 0.43 1.7 D2, Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 10 mg/kg D.W. 0.44 1.7 Q3. SW846: 6010C MMSD
02/03/21 DM0203/21001428 9.4 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
02/04/21 DM0204/21001444 9.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/05/21 DM0205/21001455 9.8 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
02/06/21 DM0206/21001476 9.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/07/21 DM0207/21001489 9.8 mg/kg D.W. 0.42 1.6
SW846: 6010C MMSD
02/08/21 DM0208/21001609 9.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/09/21 DM0209/21001625 9.5 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/10/21 DM0210/21001656 9.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/11/21
02/12/21
02/13/21
DM0211/21001672
DM0212/21001706
DM0213/21001725
8.9 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
9.4 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
10 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
02/14/21 DM0214/21001738 15 mg/kg D.W. 0.43 1.7 Q3. SW846: 6010C MMSD
02/15/21 DM0215/21001793 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
Page 41 of 121
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MMSD
PARTNERS FOI A CLEANER Eri1EONFF{Ml
MOLYBDENUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
10 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
9.6 mg/kg D.W.
0.44 1.7
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
9.4 mg/kg D.W.
0.44 1.7
SW846: 6010C MMSD
02/19/21 DM0219/21001986 9.8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/20/21 DM0220/21002005 9.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/21/21 DM0221/21002072 9.8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/22/21 DM0222/21002230 9.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/23/21 DM0223/21002246 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/24/21 DM0224/21002281 8.9 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
02/25/21 DM0225/21002320 9.2 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
02/26/21 DM0226/21002386 9.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/27/21 DM0227/21002405 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
02/28/21 DM0228/21002478 9.4 mg/kg D.W. 0.43 1.7 Q3. SW846: 6010C MMSD
03/01/21 DM0301/21002611 8.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/02/21 DM0302/21002629 9.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/03/21
03/04/21
DM0303/21002660
DM0304/21002717
8.2 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
8.9 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
03/05/21 DM0305/21002728 8.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/06/21 DM0306/21002747 8.5 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/07/21 DM0307/21002858 8.8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/08/21 DM0308/21003336 8.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/09/21 DM0309/21003371 9.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/10/21 DM0310/21003402 8.5 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/11/21 DM0311/21003456 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/12/21 DM0312/21003522 9.1 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/13/21 DM0313/21003541 9.8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/14/21 DM0314/21003554 8.4 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/15/21 DM0315/21003747 9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/16/21 DM0316/21003801 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/17/21 DM0317/21003878 9.3 mg/kg D.W. 0.43 1.7 Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 8.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/19/21 DM0319/21003905 8.4 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
03/20/21 DM0320/21004076 8.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/21/21 DM0321/21004093 8.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/22/21 DM0322/21004120 8.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/23/21 DM0323/21004136 8.3 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/24/21 DM0324/21004167 8.1 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/25/21 DM0325/21004242 8.4 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/26/21 DM0326/21004253 8.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/27/21 DM0327/21004272 8.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
03/28/21 DM0328/21004285 8.4 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
03/29/21
03/30/21
03/31/21
DM0329/21004312
DM0330/21004388
DM0331/21004600
8.5 mg/kg D.W.
0.44 1.7
SW846: 6010C MMSD
8.1 mg/kg D.W.
0.44 1.7
SW846: 6010C MMSD
8 mg/kg D.W.
0.44 1.7
SW846: 6010C MMSD
04/01/21 DM0401/21004616 8.1 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
04/02/21 DM0402/21004627 8.6 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
Page 42 of 121
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MMSD
PARTNERS FOI A CLEAMJ LY *ONWi1Kt
MOLYBDENUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
8.5 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
9 mg/kg D.W.
0.43 1.7
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
9.7 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
04/06/21 DM0406/21004758 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/07/21 DM0407/21004843 8.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/08/21 DM0408/21004861 8.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/09/21 DM0409/21004912 8.1 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/10/21 DM0410/21004931 8 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
04/11/21 DM0411/21005023 8.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/12/21 DM0412/21005052 7.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/13/21 DM0413/21005199 8.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/14/21 DM0414/21005230 7.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/15/21 DM0415/21005248 8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/16/21 DM0416/21005259 7.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/17/21 DM0417/21005468 7.6 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
04/18/21
04/19/21
DM0418/21005481
DM0419/21005508
7.8 mg/kg D.W.
0.44 1.7
SW846: 6010C MMSD
7.6 mg/kg D.W.
0.44 1.7
SW846: 6010C MMSD
04/20/21 DM0420/21005839 8.7 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
04/21/21 DM0421/21005870 7.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/22/21 DM0422/21005981 7.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/23/21 DM0423/21005992 8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/24/21 DM0424/21006057 8.1 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/25/21 DM0425/21006272 8.4 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/26/21 DM0426/21006299 9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/27/21 DM0427/21006315 9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/28/21 DM0428/21006346 8.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/29/21 DM0429/21006362 8.1 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
04/30/21 DM0430/21006373 7.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/01/21 DM0501/21006429 7.5 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/02/21 DM0502/21006442 7.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/03/21 DM0503/21006676 7.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/04/21 DM0504/21006691 8.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/05/21 DM0505/21006722 8.4 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/06/21 DM0506/21006781 7.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/07/21 DM0507/21006834 8.3 mg/kg D.W. 0.42 1.6
SW846: 6010C MMSD
05/08/21 DM0508/21006981 8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/09/21 DM0509/21006994 7.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/10/21 DM0510/21007021 7.6 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
05/11/21 DM0511/21007171 7.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/12/21 DM0512/21007202 7.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/13/21 DM0513/21007217 8.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/14/21
05/15/21
05/16/21
DM0514/21007309
DM0515/21007328
DM0516/21007341
7.9 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
8.1 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
8.2 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
05/17/21 DM0517/21007382 8.3 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/18/21 DM0518/21007440 8.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
Page 43 of 121
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MMSD
PARTNERS FOI A CLE1MJ EIl*OUW1 R
MOLYBDENUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
8.4 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
8.3 mg/kg D.W.
0.44 1.7
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
8.6 mg/kg D.W.
0.44 1.7
SW846: 6010C MMSD
05/22/21 DM0522/21008072 8.4 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
05/23/21 DM0523/21008085 8.5 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/25/21 DM0525/21008288 8.8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/26/21 DM0526/21008319 8.8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/27/21 DM0527/21008484 9.4 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/28/21 DM0528/21008495 8.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/29/21 DM0529/21008515 8.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
05/30/21 DM0530/21008530 8.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/01/21 DM0601/21008902 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/02/21 DM0602/21008935 9.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/03/21 DM0603/21008950 9.4 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/04/21 DM0604/21009184 9.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/05/21
06/06/21
DM0605/21009203
DM0606/21009287
9.6 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
9.5 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
06/07/21 DM0607/21009314 9.3 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/08/21 DM0608/21009334 9.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/09/21 DM0609/21009365 9.4 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/10/21 DM0610/21009538 9.2 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/11/21 DM0611/21009549 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/12/21 DM0612/21009568 10 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
06/13/21 DM0613/21009602 10 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
06/14/21 DM0614/21009629 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/18/21 DM0618/21009979 9.2 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
06/19/21 DM0619/21010314 9.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/20/21 DM0620/21010332 9.3 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/21/21 DM0621/21010359 9.4 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/22/21 DM0622/21010375 9.5 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/23/21 DM0623/21010408 9.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/24/21 DM0624/21010670 9.6 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/25/21 DM0625/21010681 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/26/21 DM0626/21010702 9.6 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
06/27/21 DM0627/21010807 9.8 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD
06/28/21 DM0628/21010860 9.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/29/21 DM0629/21010875 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
06/30/21 DM0630/21011438 9.4 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/01/21 DM0701/21011453 9.8 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/02/21 DM0702/21011465 9.7 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/03/21 DM0703/21011485 10 mg/kg D.W. 0.43 1.7 T9. SW846: 6010C MMSD
07/04/21
07/05/21
07/06/21
DM0704/21011516
DM0705/21011572
DM0706/21011693
11 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
10 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
10 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
07/07/21 DM0707/21011727 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/08/21 DM0708/21011742 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
Page 44 of 121
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MMSD
PARTNERS FOI II CLIMB LY *OU 1M
MOLYBDENUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
10 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
9.9 mg/kg D.W.
0.43 1.7
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
10 mg/kg D.W.
0.42 1.7
SW846: 6010C MMSD
07/12/21 DM0712/21012283 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/13/21 DM0713/21012298 11 mg/kg D.W. 0.42 1.7
SW846: 6010C MMSD
07/14/21 DM0714/21012332 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/15/21 DM0715/21012390 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/16/21 DM0716/21012563 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/17/21 DM0717/21012583 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/18/21 DM0718/21012596 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/19/21 DM0719/21012624 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/20/21 DM0720/21012639 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/21/21 DM0721/21012760 15 mg/kg D.W. 0.43 1.7 Q3. SW846: 6010C MMSD
07/22/21 DM0722/21012775 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/23/21 DM0723/21013074 9.9 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/24/21
07/25/21
DM0724/21013378
DM0725/21013391
10 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
10 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
07/26/21 DM0726/21013419 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/27/21 DM0727/21013434 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/28/21 DM0728/21013470 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/29/21 DM0729/21013614 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
07/30/21 DM0730/21013629 10 mg/kg D.W. 0.42 1.7
SW846: 6010C MMSD
07/31/21 DM0731/21013739 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/01/21 DM0801/21013752 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/02/21 DM0802/21013891 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/03/21 DM0803/21013906 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/04/21 DM0804/21013940 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/05/21 DM0805/21014673 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/06/21 DM0806/21014685 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/07/21 DM0807/21014705 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/08/21 DM0809/21014718 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/09/21 DM0809/21014746 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/10/21 DM0810/21014847 12 mg/kg D.W. 0.43 1.7 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/12/21 DM0812/21015285 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/13/21 DM0813/21015297 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/14/21 DM0814/21015317 11 mg/kg D.W. 0.42 1.6
SW846: 6010C MMSD
08/15/21 DM0815/21015330 9.6 mg/kg D.W. 0.42 1.6
SW846: 6010C MMSD
08/16/21 DM0816/21015410 13 mg/kg D.W. 0.42 1.6 Q3. SW846: 6010C MMSD
08/17/21 DM0817/21015425 11 mg/kg D.W. 0.42 1.6
SW846: 6010C MMSD
08/18/21 DM0818/21016031 10 mg/kg D.W. 0.42 1.6
SW846: 6010C MMSD
08/19/21
08/20/21
08/21/21
DM0819/21016046
DM0820/21016068
DM0821/21016088
10 mg/kg D.W.
0.42 1.6
SW846: 6010C MMSD
11 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
11 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
08/22/21 DM0822/21016196 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/23/21 DM0823/21016224 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
Page 45 of 121
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MMSD
PARTNERS FOI A CLEAMJ LY *ONWi1Kt
MOLYBDENUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
11 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
11 mg/kg D.W.
0.43 1.7
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
11 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
08/27/21 DM0827/21016407 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/28/21 DM0828/21016427 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/30/21 DM0830/21016468 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
08/31/21 DM0831/21016483 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/01/21 DM0901/21016598 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/02/21 DM0902/21016659 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/03/21 DM0903/21016671 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/04/21 DM0904/21017055 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/05/21 DM0905/21017068 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/06/21 DM0906/21017096 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/07/21 DM0907/21017306 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/08/21 DM0908/21017338 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/09/21
09/10/21
DM0909/21017408
DM0910/21017420
11 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
11 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD
09/11/21 DM0911/21017699 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/12/21 DM0912/21017712 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/13/21 DM0913/21017740 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/14/21 DM0914/21017755 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150012-1
09/17/21 DM0917/21018105 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 11 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 150123-1
09/21/21 DM0921/21018251 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150123-1
09/22/21 DM0922/21018480 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/23/21 DM0923/21018564 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD
09/24/21 DM0924/21018818 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 11 mg/kg D.W. 0.42 1.6
SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 11 mg/kg D.W. 0.42 1.6
SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 11 mg/kg D.W. 0.42 1.7
SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 10 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150376-1
10/06/21
10/07/21
10/08/21
DM 1006/21 01 9735
DM 1007/21 01 9760
DM 1008/21 01 9772
12 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD 150431-1
12 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD 150431-1
12 mg/kg D.W.
0.42 1.6
SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 12 mg/kg D.W. 0.42 1.6
SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 14 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150655-1
Page 46 of 121
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MMSD
PARTAERS FOI A CLEAMJ P11110UW1M[
MOLYBDENUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e •
a .
QC Batch
ID
10/21/21
DM 1021 /21020689
12 mg/kg D.W.
0.43
1.7
SW846: 6010C
MMSD
150655-1
10/22/21
DM 1022/21020701
12 mg/kg D.W.
0.43 1.7
SW846: 6010C
MMSD 150703-1
10/23/21 DM1023/21020883
12 mg/kg D.W.
0.42 1.6
SW846: 6010C
MMSD 150703-1
10/24/21 DM1024/21021034 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 13 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 11 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150831-1
10/29/21 DM1029/21021510 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150831-1
10/30/21 DM1030/21021530 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150831-1
10/31/21 DM1031/21021574 12 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 150831-1
11/01/21 DM1101/21021608 12 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 150831-1
11/02/21 DM1102/21021623 12 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150884-1
11/05/21
11/06/21
DM1105/21021747
DM1106/21021767
12 mg/kg D.W.
0.42 1.6
SW846: 6010C MMSD 150964-1
13 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 13 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 13 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 12 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151039-2
11/11/21 DM1111/21022695 12 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151039-1
11/14/21 DM1114/21022744 12 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 12 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151085-1
11/16/21 DM1116/21022787 13 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151085-1
11/17/21 DM1117/21023039 13 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151122-1
11/18/21 DM1118/21023056 13 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151122-1
11/19/21 DM1119/21023181 13 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151175-1
11/20/21 DM1120/21023201 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151175-1
11/21/21 DM1121/21023214 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151175-1
11/22/21 DM1122/21023555 14 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151175-1
11/23/21 DM1123/21023570 15 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151252-1
11/24/21 DM1124/21023611 14 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151266-1
11/25/21 DM1125/21023795 14 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151266-1
11/26/21 DM1126/21023807 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151266-1
11/27/21 DM1127/21023827 14 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151266-1
11/28/21 DM1128/21023899 14 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151266-1
11/29/21 DM1129/21023927 14 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151294-1
11/30/21 DM1130/21024167 14 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151317-1
12/01/21
12/02/21
12/03/21
DM 1201 /21024282
DM 1202/21024297
DM 1203/21024309
14 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD 151317-2
14 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD 151342-1
14 mg/kg D.W.
0.43 1.7
SW846: 6010C MMSD 151371-1
12/04/21 DM1204/21024329 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151371-1
12/05/21 DM1205/21024739 13 mg/kg D.W. 0.44 1.7 D2, Q3. SW846: 6010C MMSD 151371-1
Page 47 of 121
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MMSD
PARTNERS FOI A CLEAMJ pnl*O111i1Kt
MOLYBDENUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e •
a.
QC Batch
ID
12/06/21
DM1206/21024767
13 mg/kg D.W.
0.44
1.7
SW846: 6010C
MMSD
151391-1
12/07/21
DM 1207/21024782
12 mg/kg D.W.
0.44 1.7
SW846: 6010C
MMSD 151422-1
12/08/21 DM 1208/21024816
12 mg/kg D.W.
0.44 1.7
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 12 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151471-2
12/10/21 DM1210/21024844 14 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151498-1
12/11/21 DM1211/21024864 14 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151498-1
12/12/21 DM1212/21025174 14 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151498-1
12/13/21 DM1213/21025205 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151543-1
12/14/21 DM1214/21025220 13 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151576-1
12/15/21 DM1215/21025299 13 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151576-1
12/16/21 DM1216/21025314 13 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151645-1
12/17/21 DM1217/21025326 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151645-1
12/18/21 DM1219/21025346 14 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151645-1
12/19/21 DM1219/21025621 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151645-1
12/20/21 DM1220/21025649 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151645-2
12/21/21
12/22/21
DM 1221 /21025664
DM1222/21025700
13 mg/kg D.W.
0.44 1.7
SW846: 6010C MMSD 151668-1
13 mg/kg D.W.
0.44 1.7
SW846: 6010C MMSD 151750-1
12/23/21 DM1223/21025779 14 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151750-2
12/24/21 DM1224/21025791 14 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151750-2
12/25/21 DM1225/21025811 14 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151750-2
12/26/21 DM1226/21025824 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151750-2
12/27/21 DM1227/21025917 14 mg/kg D.W. 0.43 1.7
SW846: 6010C MMSD 151750-2
12/28/21 DM1228/21025932 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151750-2
12/29/21 DM1229/21025966 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151827-1
12/30/21 DM1230/21025981 12 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151827-1
12/31/21 DM1231/21026033 13 mg/kg D.W. 0.44 1.7
SW846: 6010C MMSD 151827-1
Avg Result: 10 mg/kg D.W. Min LOD: 0.42 mg/kg D.W.
Max Result: 15 mg/kg D.W. Max LOD: 0.44 mg/kg D.W.
Page 48 of 121
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MMSD
PARTAERS FOI A CLEAA#R MOM
NICKEL ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
19 mg/kg D.W.
0.99
3.9
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
20 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD
01/03/21
DM0103/21000076
18 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
01/04/21 DM0104/21000488 21 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
01/05/21
DM0105/21000504
20 mg/kg D.W. 1 4
SW846: 6010C MMSD
01/06/21 DM0106/21000535 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
01/07/21 DM0107/21000551 19 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
01/08/21
DM0108/21000562
20 mg/kg D.W. 0.99 4 SW846: 6010C MMSD
01/09/21
DM0109/21000581
20 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/10/21
DM0110/21000594
19 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/11/21 DM0111/21000632 20 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
01/12/21 DM0112/21000648 20 mg/kg D.W. 0.99 3.9 Q3. SW846: 6010C MMSD
01/13/21 DM0113/21000679 22 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
01/14/21 DM0114/21000754 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
01/15/21 DM0115/21000765 19 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
01/16/21
01/17/21
DM0116/21000784
DM0117/21000797
19 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
19 mg/kg D.W.
0.99 4 Q3.
SW846: 6010C MMSD
01/18/21
DM0118/21000824
24 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/19/21
DM0119/21000842
23 mg/kg D.W. 0.99 4 SW846: 6010C MMSD
01/20/21 DM0120/21000926 22 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
01/21/21 DM0121/21000942 23 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
01/22/21
DM0122/21000953
22 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/23/21
DM0123/21000972
23 mg/kg D.W. 0.99 4 SW846: 6010C MMSD
01/24/21
DM0124/21001059
22 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/25/21
DM0125/21001088
18 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/26/21
DM0126/21001106
19 mg/kg D.W. 1 4 SW846: 6010C MMSD
01/27/21 DM0127/21001137 19 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
01/28/21 DM0128/21001153 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
01/29/21 DM0129/21001164 22 mg/kg D.W. 0.96 3.8
SW846: 6010C MMSD
01/30/21 DM0130/21001304 25 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
01/31/21 DM0131/21001317 22 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
02/01/21
DM0201/21001344
21 mg/kg D.W. 0.98 3.9 D2, Q3.
SW846: 6010C MMSD
02/02/21 DM0202/21001397 25 mg/kg D.W. 0.99 3.9 Q3. SW846: 6010C MMSD
02/03/21 DM0203/21001428 22 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
02/04/21 DM0204/21001444 25 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
02/05/21 DM0205/21001455 23 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
02/06/21 DM0206/21001476 25 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
02/07/21 DM0207/21001489 24 mg/kg D.W. 0.96 3.8
SW846: 6010C MMSD
02/08/21 DM0208/21001609 23 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
02/09/21 DM0209/21001625 24 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
02/10/21 DM0210/21001656 24 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
02/11/21
02/12/21
02/13/21
DM0211/21001672
DM0212/21001706
DM0213/21001725
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
02/14/21 DM0214/21001738 23 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
02/15/21 DM0215/21001793 23 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
Page 49 of 121
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MMSD
PARTNERS FOI A CLIMB MOM
NICKEL ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
22 mg/kg D.W.
0.98
3.9
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
21 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD
02/18/21
DM0218/21001975
20 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
02/19/21 DM0219/21001986 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
02/20/21 DM0220/21002005 21 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
02/21/21 DM0221/21002072 20 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
02/22/21 DM0222/21002230 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
02/23/21 DM0223/21002246 24 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
02/24/21 DM0224/21002281 20 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
02/25/21
DM0225/21002320
20 mg/kg D.W. 1 4 SW846: 6010C MMSD
02/26/21 DM0226/21002386 25 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
02/27/21 DM0227/21002405 26 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
02/28/21 DM0228/21002478 25 mg/kg D.W. 0.98 3.9 Q3. SW846: 6010C MMSD
03/01/21 DM0301/21002611 20 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
03/02/21 DM0302/21002629 23 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
03/03/21
03/04/21
DM0303/21002660
DM0304/21002717
20 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
03/05/21 DM0305/21002728 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/06/21 DM0306/21002747 21 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
03/07/21 DM0307/21002858 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/08/21 DM0308/21003336 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/09/21 DM0309/21003371 26 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/10/21 DM0310/21003402 22 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/11/21 DM0311/21003456 30 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/12/21 DM0312/21003522 22 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
03/13/21 DM0313/21003541 23 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
03/14/21 DM0314/21003554 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/15/21 DM0315/21003747 22 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
03/16/21 DM0316/21003801 27 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
03/17/21 DM0317/21003878 24 mg/kg D.W. 0.98 3.9 Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 22 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/19/21
DM0319/21003905
22 mg/kg D.W. 0.99 4 SW846: 6010C MMSD
03/20/21 DM0320/21004076 23 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
03/21/21 DM0321/21004093 22 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
03/22/21 DM0322/21004120 22 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
03/23/21 DM0323/21004136 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/24/21 DM0324/21004167 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/25/21 DM0325/21004242 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/26/21 DM0326/21004253 23 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/27/21 DM0327/21004272 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
03/28/21 DM0328/21004285 21 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
03/29/21
03/30/21
03/31/21
DM0329/21004312
DM0330/21004388
DM0331/21004600
21 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
21 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
20 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
04/01/21 DM0401/21004616 21 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
04/02/21 DM0402/21004627 23 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
Page 50 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOWN
NICKEL ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
22 mg/kg D.W.
0.98
3.9
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
22 mg/kg D.W.
0.97 3.9
SW846: 6010C
MMSD
04/05/21
DM0405/21004742
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
04/06/21 DM0406/21004758 26 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/07/21 DM0407/21004843 23 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/08/21 DM0408/21004861 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/09/21 DM0409/21004912 21 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
04/10/21 DM0410/21004931 20 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
04/11/21 DM0411/21005023 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/12/21 DM0412/21005052 19 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/13/21 DM0413/21005199 23 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/14/21 DM0414/21005230 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/15/21 DM0415/21005248 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/16/21 DM0416/21005259 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/17/21 DM0417/21005468 19 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
04/18/21 DM0418/21005481 20 mg/kg D.W. 0.99 3.9 SW846: 6010C MMSD
04/19/21 DM0419/21005508 19 mg/kg D.W. 1 4 SW846: 6010C MMSD
04/20/21
DM0420/21005839
24 mg/kg D.W. 1 4 SW846: 6010C MMSD
04/21/21 DM0421/21005870 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/22/21 DM0422/21005981 20 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
04/23/21 DM0423/21005992 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/24/21 DM0424/21006057 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/25/21 DM0425/21006272 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/26/21 DM0426/21006299 20 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
04/27/21 DM0427/21006315 23 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/28/21 DM0428/21006346 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/29/21 DM0429/21006362 19 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
04/30/21 DM0430/21006373 18 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
05/01/21 DM0501/21006429 18 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
05/02/21 DM0502/21006442 18 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
05/03/21 DM0503/21006676 18 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
05/04/21 DM0504/21006691 22 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
05/05/21 DM0505/21006722 19 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
05/06/21 DM0506/21006781 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
05/07/21 DM0507/21006834 21 mg/kg D.W. 0.96 3.8
SW846: 6010C MMSD
05/08/21 DM0508/21006981 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
05/09/21 DM0509/21006994 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
05/10/21 DM0510/21007021 20 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD
05/11/21 DM0511/21007171 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
05/12/21 DM0512/21007202 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
05/13/21 DM0513/21007217 25 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
05/14/21
05/15/21
05/16/21
DM0514/21007309
DM0515/21007328
DM0516/21007341
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
21 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
25 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
05/17/21 DM0517/21007382 23 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
05/18/21 DM0518/21007440 25 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
Page 51 of 121
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MMSD
PARTNERS FOI A CLIMB E1n* r 1
NICKEL ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
24 mg/kg D.W.
0.97
3.9
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
22 mg/kg D.W.
0.99 3.9
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
21 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
05/22/21 DM0522/21008072
21 mg/kg D.W. 1 4
SW846: 6010C MMSD
05/23/21 DM0523/21008085
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
05/25/21 DM0525/21008288
21 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
05/26/21 DM0526/21008319
22 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
05/27/21 DM0527/21008484
24 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
05/28/21 DM0528/21008495
19 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
05/29/21 DM0529/21008515
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
05/30/21 DM0530/21008530
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/01/21 DM0601/21008902
24 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
06/02/21 DM0602/21008935
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/03/21 DM0603/21008950
20 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
06/04/21 DM0604/21009184
20 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
06/05/21
06/06/21
DM0605/21009203
DM0606/21009287
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/07/21 DM0607/21009314
19 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
06/08/21 DM0608/21009334
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/09/21 DM0609/21009365
19 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/10/21 DM0610/21009538
19 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/11/21 DM0611/21009549
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/12/21 DM0612/21009568
23 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
06/13/21 DM0613/21009602
22 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
06/14/21 DM0614/21009629
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/18/21 DM0618/21009979
20 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
06/19/21 DM0619/21010314
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/20/21 DM0620/21010332
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/21/21 DM0621/21010359
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/22/21 DM0622/21010375
21 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
06/23/21 DM0623/21010408
21 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
06/24/21 DM0624/21010670
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/25/21 DM0625/21010681
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/26/21 DM0626/21010702
21 mg/kg D.W. 1 4 SW846: 6010C MMSD
06/27/21 DM0627/21010807
21 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD
06/28/21 DM0628/21010860
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/29/21 DM0629/21010875
27 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
06/30/21 DM0630/21011438
21 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
07/01/21 DM0701/21011453
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
07/02/21 DM0702/21011465
23 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
07/03/21 DM0703/21011485
23 mg/kg D.W. 0.98 3.9 T9. SW846: 6010C MMSD
07/04/21
07/05/21
07/06/21
DM0704/21011516
DM0705/21011572
DM0706/21011693
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
23 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
07/07/21 DM0707/21011727
23 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
07/08/21 DM0708/21011742
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
Page 52 of 121
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MMSD
PARTAFRS FOI II CLIMB NNW
NICKEL ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
23 mg/kg D.W.
0.97
3.9
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
22 mg/kg D.W.
0.97 3.8
SW846: 6010C
MMSD
07/11/21
DM0711 /21012255
23 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
07/12/21 DM0712/21012283 22 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
07/13/21 DM0713/21012298 26 mg/kg D.W. 0.96 3.8
SW846: 6010C MMSD
07/14/21 DM0714/21012332 22 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
07/15/21 DM0715/21012390 22 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
07/16/21 DM0716/21012563 21 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
07/17/21 DM0717/21012583 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
07/18/21 DM0718/21012596 21 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
07/19/21 DM0719/21012624 21 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
07/20/21 DM0720/21012639 25 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
07/21/21 DM0721/21012760 22 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
07/22/21
DM0722/21012775
22 mg/kg D.W. 0.98 3.9 Q2. SW846: 6010C MMSD
07/23/21 DM0723/21013074 25 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
07/24/21
07/25/21
DM0724/21013378
DM0725/21013391
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
20 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
07/26/21 DM0726/21013419 19 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
07/27/21 DM0727/21013434 24 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
07/28/21 DM0728/21013470 21 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
07/29/21 DM0729/21013614 20 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
07/30/21 DM0730/21013629 21 mg/kg D.W. 0.96 3.8
SW846: 6010C MMSD
07/31/21 DM0731/21013739 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
08/01/21 DM0801/21013752 20 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
08/02/21 DM0802/21013891 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
08/03/21 DM0803/21013906 26 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
08/04/21 DM0804/21013940 25 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
08/05/21 DM0805/21014673 27 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
08/06/21 DM0806/21014685 21 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
08/07/21 DM0807/21014705 21 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
08/08/21 DM0809/21014718 22 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
08/09/21 DM0809/21014746 24 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
08/10/21
DM0810/21014847
29 mg/kg D.W. 0.97 3.9 D2, Q2.
SW846: 6010C MMSD
08/11/21 DM0811/21014867 25 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
08/12/21 DM0812/21015285 27 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD
08/13/21 DM0813/21015297 27 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD
08/14/21 DM0814/21015317 32 mg/kg D.W. 0.96 3.8
SW846: 6010C MMSD
08/15/21 DM0815/21015330 37 mg/kg D.W. 0.95 3.8
SW846: 6010C MMSD
08/16/21 DM0816/21015410 38 mg/kg D.W. 0.96 3.8
SW846: 6010C MMSD
08/17/21 DM0817/21015425 36 mg/kg D.W. 0.96 3.8
SW846: 6010C MMSD
08/18/21 DM0818/21016031 33 mg/kg D.W. 0.96 3.8
SW846: 6010C MMSD
08/19/21
08/20/21
08/21/21
DM0819/21016046
DM0820/21016068
DM0821/21016088
36 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD
42 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
30 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
08/22/21 DM0822/21016196 31 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
08/23/21 DM0823/21016224 28 mg/kg D.W. 0.97 3.9
SW846: 6010C MMSD
Page 53 of 121
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MMSD
PARTNERS FOI A OAR NNW
NICKEL ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
30 mg/kg D.W.
0.98
3.9
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
27 mg/kg D.W.
0.97 3.9
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
27 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
08/27/21 DM0827/21016407
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
08/28/21 DM0828/21016427
27 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
08/30/21 DM0830/21016468
26 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
08/31/21 DM0831/21016483
28 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
09/01/21 DM0901/21016598
26 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD
09/02/21 DM0902/21016659
24 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
09/03/21 DM0903/21016671
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
09/04/21 DM0904/21017055
25 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
09/05/21 DM0905/21017068
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
09/06/21 DM0906/21017096
26 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
09/07/21 DM0907/21017306
24 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
09/08/21 DM0908/21017338
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
09/09/21
09/10/21
DM0909/21017408
DM0910/21017420
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
09/11/21 DM0911/21017699
23 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
09/12/21 DM0912/21017712
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
09/13/21 DM0913/21017740
22 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
09/14/21 DM0914/21017755
23 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023
27 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 150012-1
09/17/21 DM0917/21018105
27 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125
28 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138
26 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236
26 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 150123-1
09/21/21 DM0921/21018251
27 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 150123-1
09/22/21 DM0922/21018480
27 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD
09/23/21 DM0923/21018564
28 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD
09/24/21 DM0924/21018818
29 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838
28 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023
28 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051
28 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066
27 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228
25 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243
26 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD 150305-1
10/01/21 DM 1001 /21019255
24 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384
25 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397
25 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 150376-1
10/06/21
10/07/21
10/08/21
DM 1006/21019735
DM 1007/21019760
DM 1008/21019772
26 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 150431-1
26 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD 150431-1
26 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600
26 mg/kg D.W.
0.95 3.8
SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674
35 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 150655-1
Page 54 of 121
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MMSD
PARTNERS FOI A CLIMB NNW
NICKEL ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
10/21/21
DM 1021 /21020689
26 mg/kg D.W.
0.97
3.9
SW846: 6010C
MMSD
150655-1
10/22/21
DM 1022/21020701
27 mg/kg D.W.
0.97 3.8
SW846: 6010C
MMSD 150703-1
10/23/21 DM1023/21020883
26 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD 150703-1
10/24/21 DM1024/21021034
26 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062
26 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077
26 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161
28 mg/kg D.W. 0.98 3.9 D2, Q2.
SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226
24 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 150831-1
10/29/21 DM1029/21021510
23 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 150831-1
10/30/21 DM1030/21021530
23 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 150831-1
10/31/21 DM 1031 /21021574
25 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 150831-1
11/01/21 DM 1101 /21021608
24 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 150831-1
11/02/21 DM1102/21021623
25 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735
24 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD 150884-1
11/05/21
11/06/21
DM1105/21021747
DM1106/21021767
25 mg/kg D.W.
0.96 3.8
SW846: 6010C MMSD 150964-1
26 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680
24 mg/kg D.W. 0.99 4 SW846: 6010C MMSD 151039-2
11/11/21 DM1111/21022695
24 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707
25 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 151039-1
11/14/21 DM1114/21022744
26 mg/kg D.W. 0.99 4 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 151085-1
11/16/21 DM1116/21022787
26 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 151085-1
11/17/21 DM1117/21023039
25 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 151122-1
11/18/21 DM1118/21023056
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 151122-1
11/19/21 DM1119/21023181
24 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 151175-1
11/20/21 DM1120/21023201
27 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 151175-1
11/21/21 DM 1121 /21023214
25 mg/kg D.W. 1 4 SW846: 6010C MMSD 151175-1
11/22/21 DM1122/21023555
25 mg/kg D.W. 1 4 SW846: 6010C MMSD 151175-1
11/23/21 DM1123/21023570
26 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 151252-1
11/24/21 DM1124/21023611
26 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 151266-1
11/25/21 DM1125/21023795
28 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 151266-1
11/26/21 DM1126/21023807
27 mg/kg D.W. 0.99 4 SW846: 6010C MMSD 151266-1
11/27/21 DM1127/21023827
29 mg/kg D.W. 1 4 SW846: 6010C MMSD 151266-1
11/28/21 DM1128/21023899
28 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 151266-1
11/29/21 DM1129/21023927
29 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 151294-1
11/30/21 DM1130/21024167
28 mg/kg D.W.
0.97 3.9
SW846: 6010C MMSD 151317-1
12/01/21
12/02/21
12/03/21
DM 1201 /21024282
DM 1202/21024297
DM 1203/21024309
28 mg/kg D.W.
0.97 3.8
SW846: 6010C MMSD 151317-2
28 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 151342-1
27 mg/kg D.W.
0.98 3.9
SW846: 6010C MMSD 151371-1
12/04/21 DM1204/21024329
26 mg/kg D.W.
0.99 3.9
SW846: 6010C MMSD 151371-1
12/05/21 DM1205/21024739
27 mg/kg D.W. 0.99 4 D2, Q3.
SW846: 6010C MMSD 151371-1
Page 55 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
NICKEL ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a.
QC Batch
ID
12/06/21
DM1206/21024767
26 mg/kg D.W.
0.99
3.9
SW846: 6010C
MMSD
151391-1
12/07/21
DM 1207/21024782
25 mg/kg D.W. 0.99 4
SW846: 6010C
MMSD 151422-1
12/08/21 DM 1208/21024816
26 mg/kg D.W. 1 4
SW846: 6010C MMSD 151471-1
12/09/21 DM1209/21024832 25 mg/kg D.W. 1 4
SW846: 6010C MMSD 151471-2
12/10/21 DM1210/21024844 28 mg/kg D.W. 1 4
SW846: 6010C MMSD 151498-1
12/11/21 DM1211/21024864 26 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD 151498-1
12/12/21 DM1212/21025174 26 mg/kg D.W. 0.97 3.8
SW846: 6010C MMSD 151498-1
12/13/21 DM1213/21025205 24 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD 151543-1
12/14/21 DM1214/21025220 25 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD 151576-1
12/15/21 DM1215/21025299 26 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD 151576-1
12/16/21 DM1216/21025314 25 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD 151645-1
12/17/21 DM1217/21025326 24 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD 151645-1
12/18/21 DM1219/21025346 24 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD 151645-1
12/19/21 DM1219/21025621 22 mg/kg D.W. 1 4 SW846: 6010C MMSD 151645-1
12/20/21 DM1220/21025649 23 mg/kg D.W. 1 4 SW846: 6010C MMSD 151645-2
12/21/21 DM1221/21025664 23 mg/kg D.W. 1 4 SW846: 6010C MMSD 151668-1
12/22/21 DM1222/21025700 23 mg/kg D.W. 0.99 4 SW846: 6010C MMSD 151750-1
12/23/21 DM1223/21025779 24 mg/kg D.W. 1 4 SW846: 6010C MMSD 151750-2
12/24/21 DM1224/21025791 24 mg/kg D.W. 1 4 SW846: 6010C MMSD 151750-2
12/25/21 DM1225/21025811 23 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD 151750-2
12/26/21 DM1226/21025824 23 mg/kg D.W. 1 4 SW846: 6010C MMSD 151750-2
12/27/21 DM1227/21025917 24 mg/kg D.W. 0.98 3.9
SW846: 6010C MMSD 151750-2
12/28/21 DM1228/21025932 24 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD 151750-2
12/29/21 DM1229/21025966 24 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD 151827-1
12/30/21 DM1230/21025981 24 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD 151827-1
12/31/21 DM1231/21026033 24 mg/kg D.W. 0.99 3.9
SW846: 6010C MMSD 151827-1
Avg Result: 23 mg/kg D.W. Min LOD: 0.95 mg/kg D.W.
Max Result: 42 mg/kg D.W. Max LOD: 1 mg/kg D.W.
Page 56 of 121
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MMSD
PARTAERS FOI A CLEAMJ EYlt*OUW1M[
PHOSPHORUS ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
28000 mg/kg D.W.
23
89
AO.
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
29000 mg/kg D.W. 23 90 AO.
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
27000 mg/kg D.W. 23 89 AO.
SW846: 6010C MMSD
01/04/21 DM0104/21000488 26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
01/05/21 DM0105/21000504 27000 mg/kg D.W. 24 90
SW846: 6010C MMSD
01/06/21 DM0106/21000535 27000 mg/kg D.W. 23 89
SW846: 6010C MMSD
01/07/21 DM0107/21000551 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/08/21 DM0108/21000562 27000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/09/21 DM0109/21000581 28000 mg/kg D.W. 24 91 SW846: 6010C MMSD
01/10/21 DM0110/21000594 26000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/11/21 DM0111/21000632 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/12/21 DM0112/21000648 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/13/21 DM0113/21000679 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/14/21 DM0114/21000754 28000 mg/kg D.W. 23 88 AO. SW846: 6010C MMSD
01/15/21 DM0115/21000765 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/16/21 DM0116/21000784 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/17/21 DM0117/21000797 27000 mg/kg D.W. 24 90 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 29000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/19/21 DM0119/21000842 28000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/20/21 DM0120/21000926 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/21/21 DM0121/21000942 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
01/22/21 DM0122/21000953 28000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/23/21 DM0123/21000972 29000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/24/21 DM0124/21001059 29000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/25/21 DM0125/21001088 26000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/26/21 DM0126/21001106 26000 mg/kg D.W. 24 90 SW846: 6010C MMSD
01/27/21 DM0127/21001137 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
01/28/21 DM0128/21001153 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
01/29/21 DM0129/21001164 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD
01/30/21 DM0130/21001304 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
01/31/21 DM0131/21001317 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/01/21 DM0201/21001344 26000 mg/kg D.W. 23 89 D2, Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 29000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/03/21 DM0203/21001428 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/04/21 DM0204/21001444 29000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/05/21 DM0205/21001455 28000 mg/kg D.W. 23 90 SW846: 6010C MMSD
02/06/21 DM0206/21001476 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/07/21 DM0207/21001489 28000 mg/kg D.W. 22 86 SW846: 6010C MMSD
02/08/21 DM0208/21001609 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/09/21 DM0209/21001625 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/10/21 DM0210/21001656 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/11/21 DM0211/21001672 26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
02/12/21 DM0212/21001706 26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
02/13/21 DM0213/21001725 26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
02/14/21 DM0214/21001738 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/15/21 DM0215/21001793 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
Page 57 of 121
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MMSD
WARS F4t A CLIMB 1111101110111
PHOSPHORUS ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
26000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
25000 mg/kg D.W. 23 90
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
02/19/21 DM0219/21001986 25000 mg/kg D.W. 23 89
SW846: 6010C MMSD
02/20/21 DM0220/21002005 24000 mg/kg D.W. 23 88
SW846: 6010C MMSD
02/21/21 DM0221/21002072 25000 mg/kg D.W. 23 88
SW846: 6010C MMSD
02/22/21 DM0222/21002230 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/23/21 DM0223/21002246 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/24/21 DM0224/21002281 23000 mg/kg D.W. 23 89 SW846: 6010C MMSD
02/25/21 DM0225/21002320 24000 mg/kg D.W. 24 90 SW846: 6010C MMSD
02/26/21 DM0226/21002386 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/27/21 DM0227/21002405 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
02/28/21 DM0228/21002478 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/01/21 DM0301/21002611 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/02/21 DM0302/21002629 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/03/21 DM0303/21002660 24000 mg/kg D.W. 23 88
SW846: 6010C MMSD
03/04/21 DM0304/21002717 26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
03/05/21 DM0305/21002728 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/06/21 DM0306/21002747 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/07/21 DM0307/21002858 23000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/08/21 DM0308/21003336 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/09/21 DM0309/21003371 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/10/21 DM0310/21003402 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/11/21 DM0311/21003456 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/12/21 DM0312/21003522 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/13/21 DM0313/21003541 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/14/21 DM0314/21003554 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/15/21 DM0315/21003747 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/16/21 DM0316/21003801 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD
03/17/21 DM0317/21003878 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/18/21 DM0318/21003894 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/19/21 DM0319/21003905 27000 mg/kg D.W. 24 90 SW846: 6010C MMSD
03/20/21 DM0320/21004076 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/21/21 DM0321/21004093 26000 mg/kg D.W. 23 87 SW846: 6010C MMSD
03/22/21 DM0322/21004120 26000 mg/kg D.W. 23 87 SW846: 6010C MMSD
03/23/21 DM0323/21004136 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/24/21 DM0324/21004167 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/25/21 DM0325/21004242 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
03/26/21 DM0326/21004253 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/27/21 DM0327/21004272 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/28/21 DM0328/21004285 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
03/29/21 DM0329/21004312 26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
03/30/21 DM0330/21004388 26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
03/31/21 DM0331/21004600 24000 mg/kg D.W. 23 89
SW846: 6010C MMSD
04/01/21 DM0401/21004616 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/02/21 DM0402/21004627 24000 mg/kg D.W. 23 90 SW846: 6010C MMSD
Page 58 of 121
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MMSD
PARTNERS FOI A CLEANER DI10111M
PHOSPHORUS ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
23000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
23000 mg/kg D.W. 23 88
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
24000 mg/kg D.W. 23 89
SW846: 6010C MMSD
04/06/21 DM0406/21004758 27000 mg/kg D.W. 23 89
SW846: 6010C MMSD
04/07/21 DM0407/21004843 25000 mg/kg D.W. 23 88
SW846: 6010C MMSD
04/08/21 DM0408/21004861 25000 mg/kg D.W. 23 89
SW846: 6010C MMSD
04/09/21 DM0409/21004912 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/10/21 DM0410/21004931 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/11/21 DM0411/21005023 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/12/21 DM0412/21005052 22000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/13/21 DM0413/21005199 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/14/21 DM0414/21005230 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/15/21 DM0415/21005248 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/16/21 DM0416/21005259 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/17/21 DM0417/21005468 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
04/18/21 DM0418/21005481 24000 mg/kg D.W. 23 89
SW846: 6010C MMSD
04/19/21 DM0419/21005508 24000 mg/kg D.W. 24 90
SW846: 6010C MMSD
04/20/21 DM0420/21005839 26000 mg/kg D.W. 24 90 SW846: 6010C MMSD
04/21/21 DM0421/21005870 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/22/21 DM0422/21005981 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/23/21 DM0423/21005992 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/24/21 DM0424/21006057 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/25/21 DM0425/21006272 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/26/21 DM0426/21006299 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/27/21 DM0427/21006315 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/28/21 DM0428/21006346 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/29/21 DM0429/21006362 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
04/30/21 DM0430/21006373 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/01/21 DM0501/21006429 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/02/21 DM0502/21006442 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/03/21 DM0503/21006676 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/04/21 DM0504/21006691 23000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/05/21 DM0505/21006722 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/06/21 DM0506/21006781 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/07/21 DM0507/21006834 24000 mg/kg D.W. 23 87 SW846: 6010C MMSD
05/08/21 DM0508/21006981 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/09/21 DM0509/21006994 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/10/21 DM0510/21007021 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/11/21 DM0511/21007171 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/12/21 DM0512/21007202 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/13/21 DM0513/21007217 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
05/14/21 DM0514/21007309 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
05/15/21 DM0515/21007328 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
05/16/21 DM0516/21007341 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
05/17/21 DM0517/21007382 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/18/21 DM0518/21007440 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
Page 59 of 121
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MMSD
PARTNERS FOI A CLEANER LY *ONFf1N1
PHOSPHORUS ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
24000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
25000 mg/kg D.W. 23 89
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
25000 mg/kg D.W. 23 89
SW846: 6010C MMSD
05/22/21 DM0522/21008072 25000 mg/kg D.W. 24 90
SW846: 6010C MMSD
05/23/21 DM0523/21008085 26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
05/25/21 DM0525/21008288 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
05/26/21 DM0526/21008319 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/27/21 DM0527/21008484 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/28/21 DM0528/21008495 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/29/21 DM0529/21008515 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
05/30/21 DM0530/21008530 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/01/21 DM0601/21008902 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/02/21 DM0602/21008935 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/03/21 DM0603/21008950 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/04/21 DM0604/21009184 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/05/21 DM0605/21009203 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
06/06/21 DM0606/21009287 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
06/07/21 DM0607/21009314 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/08/21 DM0608/21009334 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/09/21 DM0609/21009365 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/10/21 DM0610/21009538 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/11/21 DM0611/21009549 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/12/21 DM0612/21009568 29000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/13/21 DM0613/21009602 28000 mg/kg D.W. 23 90 SW846: 6010C MMSD
06/14/21 DM0614/21009629 29000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/18/21 DM0618/21009979 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/19/21 DM0619/21010314 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/20/21 DM0620/21010332 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/21/21 DM0621/21010359 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/22/21 DM0622/21010375 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/23/21 DM0623/21010408 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/24/21 DM0624/21010670 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/25/21 DM0625/21010681 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/26/21 DM0626/21010702 27000 mg/kg D.W. 24 90 SW846: 6010C MMSD
06/27/21 DM0627/21010807 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/28/21 DM0628/21010860 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
06/29/21 DM0629/21010875 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
06/30/21 DM0630/21011438 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
07/01/21 DM0701/21011453 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/02/21 DM0702/21011465 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/03/21 DM0703/21011485 24000 mg/kg D.W. 23 88 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 24000 mg/kg D.W. 23 88
SW846: 6010C MMSD
07/05/21 DM0705/21011572 24000 mg/kg D.W. 23 88
SW846: 6010C MMSD
07/06/21 DM0706/21011693 25000 mg/kg D.W. 23 88
SW846: 6010C MMSD
07/07/21 DM0707/21011727 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/08/21 DM0708/21011742 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
Page 60 of 121
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MMSD
PARTNERS FOI II CLIMB Br11A0111011
PHOSPHORUS ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
25000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
24000 mg/kg D.W. 23 87
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
24000 mg/kg D.W. 23 87
SW846: 6010C MMSD
07/12/21 DM0712/21012283 26000 mg/kg D.W. 23 87
SW846: 6010C MMSD
07/13/21 DM0713/21012298 27000 mg/kg D.W. 23 87
SW846: 6010C MMSD
07/14/21 DM0714/21012332 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
07/15/21 DM0715/21012390 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/16/21 DM0716/21012563 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/17/21 DM0717/21012583 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/18/21 DM0718/21012596 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/19/21 DM0719/21012624 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/20/21 DM0720/21012639 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/21/21 DM0721/21012760 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/22/21 DM0722/21012775 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD
07/23/21 DM0723/21013074 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
07/24/21 DM0724/21013378 26000 mg/kg D.W. 23 89
SW846: 6010C MMSD
07/25/21 DM0725/21013391 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
07/26/21 DM0726/21013419 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/27/21 DM0727/21013434 29000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/28/21 DM0728/21013470 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/29/21 DM0729/21013614 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
07/30/21 DM0730/21013629 28000 mg/kg D.W. 23 87 SW846: 6010C MMSD
07/31/21 DM0731/21013739 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/01/21 DM0801/21013752 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/02/21 DM0802/21013891 29000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/03/21 DM0803/21013906 29000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/04/21 DM0804/21013940 29000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/05/21 DM0805/21014673 30000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/06/21 DM0806/21014685 28000 mg/kg D.W. 23 87 SW846: 6010C MMSD
08/07/21 DM0807/21014705 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/08/21 DM0809/21014718 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/09/21 DM0809/21014746 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/10/21 DM0810/21014847 26000 mg/kg D.W. 23 88 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/12/21 DM0812/21015285 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/13/21 DM0813/21015297 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/14/21 DM0814/21015317 22000 mg/kg D.W. 23 87 SW846: 6010C MMSD
08/15/21 DM0815/21015330 20000 mg/kg D.W. 22 86 SW846: 6010C MMSD
08/16/21 DM0816/21015410 20000 mg/kg D.W. 23 86 SW846: 6010C MMSD
08/17/21 DM0817/21015425 24000 mg/kg D.W. 23 86 SW846: 6010C MMSD
08/18/21 DM0818/21016031 23000 mg/kg D.W. 23 87 SW846: 6010C MMSD
08/19/21 DM0819/21016046 23000 mg/kg D.W. 23 87
SW846: 6010C MMSD
08/20/21 DM0820/21016068 23000 mg/kg D.W. 23 87
SW846: 6010C MMSD
08/21/21 DM0821/21016088 26000 mg/kg D.W. 23 87
SW846: 6010C MMSD
08/22/21 DM0822/21016196 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
08/23/21 DM0823/21016224 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
Page 61 of 121
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MMSD
PARTAFRS FOI A CIFJAH! Br11A0111011
PHOSPHORUS ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
26000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
25000 mg/kg D.W. 23 88
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
25000 mg/kg D.W. 23 88
SW846: 6010C MMSD
08/27/21 DM0827/21016407 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
08/28/21 DM0828/21016427 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
08/30/21 DM0830/21016468 26000 mg/kg D.W. 23 87
SW846: 6010C MMSD
08/31/21 DM0831/21016483 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/01/21 DM0901/21016598 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD
09/02/21 DM0902/21016659 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/03/21 DM0903/21016671 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD
09/04/21 DM0904/21017055 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/05/21 DM0905/21017068 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/06/21 DM0906/21017096 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/07/21 DM0907/21017306 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/08/21 DM0908/21017338 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/09/21 DM0909/21017408 27000 mg/kg D.W. 23 88
SW846: 6010C MMSD
09/10/21 DM0910/21017420 26000 mg/kg D.W. 23 88
SW846: 6010C MMSD
09/11/21 DM0911/21017699 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/12/21 DM0912/21017712 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/13/21 DM0913/21017740 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/14/21 DM0914/21017755 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 24000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150012-1
09/17/21 DM0917/21018105 24000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 27000 mg/kg D.W. 23 90 SW846: 6010C MMSD 150123-1
09/21/21 DM0921/21018251 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150123-1
09/22/21 DM0922/21018480 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/23/21 DM0923/21018564 25000 mg/kg D.W. 23 88 SW846: 6010C MMSD
09/24/21 DM0924/21018818 26000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 26000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 28000 mg/kg D.W. 23 88
SW846: 6010C MMSD 150431-1
10/07/21 DM1007/21019760 27000 mg/kg D.W. 23 87
SW846: 6010C MMSD 150431-1
10/08/21 DM1008/21019772 26000 mg/kg D.W. 23 87
SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 26000 mg/kg D.W. 22 86 SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150655-1
Page 62 of 121
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MMSD
PARTNERS FOI A CLE/MJ PI1110UW1M[
PHOSPHORUS ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
10/21/21
DM 1021 /21020689
26000 mg/kg D.W.
23
88
SW846: 6010C
MMSD
150655-1
10/22/21
DM 1022/21020701
29000 mg/kg D.W. 23 87
SW846: 6010C
MMSD 150703-1
10/23/21 DM1023/21020883
29000 mg/kg D.W. 23 87
SW846: 6010C MMSD 150703-1
10/24/21 DM1024/21021034 29000 mg/kg D.W. 23 88
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 30000 mg/kg D.W. 23 87
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 26000 mg/kg D.W. 23 87
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150831-1
10/29/21 DM1029/21021510 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150831-1
10/30/21 DM1030/21021530 26000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150831-1
10/31/21 DM1031/21021574 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150831-1
11/01/21 DM1101/21021608 25000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150831-1
11/02/21 DM1102/21021623 26000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 27000 mg/kg D.W. 23 87
SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 28000 mg/kg D.W. 23 88
SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 27000 mg/kg D.W. 24 90 SW846: 6010C MMSD 151039-2
11/11/21 DM1111/21022695 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 28000 mg/kg D.W. 23 90 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD 151039-1
11/14/21 DM1114/21022744 29000 mg/kg D.W. 24 90 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151085-1
11/16/21 DM1116/21022787 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD 151085-1
11/17/21 DM1117/21023039 28000 mg/kg D.W. 23 88 Q3. SW846: 6010C MMSD 151122-1
11/18/21 DM1118/21023056 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD 151122-1
11/19/21 DM1119/21023181 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 151175-1
11/20/21 DM1120/21023201 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151175-1
11/21/21 DM1121/21023214 28000 mg/kg D.W. 24 90 SW846: 6010C MMSD 151175-1
11/22/21 DM1122/21023555 28000 mg/kg D.W. 24 90 SW846: 6010C MMSD 151175-1
11/23/21 DM1123/21023570 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151252-1
11/24/21 DM1124/21023611 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151266-1
11/25/21 DM1125/21023795 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151266-1
11/26/21 DM1126/21023807 27000 mg/kg D.W. 23 90 SW846: 6010C MMSD 151266-1
11/27/21 DM1127/21023827 28000 mg/kg D.W. 24 91 SW846: 6010C MMSD 151266-1
11/28/21 DM1128/21023899 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151266-1
11/29/21 DM1129/21023927 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD 151294-1
11/30/21 DM1130/21024167 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD 151317-1
12/01/21 DM1201/21024282 28000 mg/kg D.W. 23 88
SW846: 6010C MMSD 151317-2
12/02/21 DM1202/21024297 28000 mg/kg D.W. 23 88
SW846: 6010C MMSD 151342-1
12/03/21 DM1203/21024309 28000 mg/kg D.W. 23 88
SW846: 6010C MMSD 151371-1
12/04/21 DM1204/21024329 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151371-1
12/05/21 DM1205/21024739 28000 mg/kg D.W. 24 90 SW846: 6010C MMSD 151371-1
Page 63 of 121
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MMSD
PARTNERS FOI A CLEANER DI1101110N1
PHOSPHORUS ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a.
QC Batch
ID
12/06/21
DM1206/21024767
29000 mg/kg D.W.
23
90
SW846: 6010C
MMSD
151391-1
12/07/21
DM 1207/21024782
27000 mg/kg D.W. 24 90
SW846: 6010C
MMSD 151422-1
12/08/21 DM1208/21024816
27000 mg/kg D.W. 24 90
SW846: 6010C MMSD 151471-1
12/09/21 DM1209/21024832 26000 mg/kg D.W. 24 90
SW846: 6010C MMSD 151471-2
12/10/21 DM1210/21024844 27000 mg/kg D.W. 24 91
SW846: 6010C MMSD 151498-1
12/11/21 DM1211/21024864 27000 mg/kg D.W. 23 88
SW846: 6010C MMSD 151498-1
12/12/21 DM1212/21025174 27000 mg/kg D.W. 23 87 SW846: 6010C MMSD 151498-1
12/13/21 DM1213/21025205 27000 mg/kg D.W. 23 90 SW846: 6010C MMSD 151543-1
12/14/21 DM1214/21025220 28000 mg/kg D.W. 23 88 SW846: 6010C MMSD 151576-1
12/15/21 DM1215/21025299 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151576-1
12/16/21 DM1216/21025314 27000 mg/kg D.W. 23 88 SW846: 6010C MMSD 151645-1
12/17/21 DM1217/21025326 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151645-1
12/18/21 DM1219/21025346 27000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151645-1
12/19/21 DM1219/21025621 26000 mg/kg D.W. 24 90 SW846: 6010C MMSD 151645-1
12/20/21 DM1220/21025649 27000 mg/kg D.W. 24 90 SW846: 6010C MMSD 151645-2
12/21/21 DM1221/21025664 27000 mg/kg D.W. 24 90
SW846: 6010C MMSD 151668-1
12/22/21 DM1222/21025700 27000 mg/kg D.W. 23 90
SW846: 6010C MMSD 151750-1
12/23/21 DM1223/21025779 28000 mg/kg D.W. 24 90 SW846: 6010C MMSD 151750-2
12/24/21 DM1224/21025791 28000 mg/kg D.W. 24 91 SW846: 6010C MMSD 151750-2
12/25/21 DM1225/21025811 28000 mg/kg D.W. 23 90 SW846: 6010C MMSD 151750-2
12/26/21 DM1226/21025824 28000 mg/kg D.W. 24 90 SW846: 6010C MMSD 151750-2
12/27/21 DM1227/21025917 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151750-2
12/28/21 DM1228/21025932 29000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151750-2
12/29/21 DM1229/21025966 28000 mg/kg D.W. 23 90 SW846: 6010C MMSD 151827-1
12/30/21 DM1230/21025981 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151827-1
12/31/21 DM1231/21026033 28000 mg/kg D.W. 23 89 SW846: 6010C MMSD 151827-1
Avg Result: 26000 mg/kg D.W. Min LOD: 22 mg/kg D.W.
Max Result: 30000 mg/kg D.W. Max LOD: 24 mg/kg D.W.
Page 64 of 121
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MMSD
PARTNERS FOI II CLIMB DINAM M
POTASSIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
3800 mg/kg D.W.
290
860
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
4000 mg/kg D.W. 290 860
SW846: 6010C
MMSD
01/03/21
DM0103/21000076
3600 mg/kg D.W. 290 860 Q2.
SW846: 6010C MMSD
01/04/21
DM0104/21000488
3800 mg/kg D.W. 290 860
SW846: 6010C MMSD
01/05/21
DM0105/21000504
3800 mg/kg D.W. 290 870
SW846: 6010C MMSD
01/06/21
DM0106/21000535
3300 mg/kg D.W. 280 860
SW846: 6010C MMSD
01/07/21
DM0107/21000551
3300 mg/kg D.W. 290 860
SW846: 6010C MMSD
01/08/21
DM0108/21000562
4000 mg/kg D.W. 290 860
SW846: 6010C MMSD
01/09/21
DM0109/21000581
4100 mg/kg D.W. 290 880
SW846: 6010C MMSD
01/10/21
DM0110/21000594
4000 mg/kg D.W. 290 870
SW846: 6010C MMSD
01/11/21
DM0111/21000632
3800 mg/kg D.W. 290 860
SW846: 6010C MMSD
01/12/21
DM0112/21000648
4000 mg/kg D.W. 290 860
SW846: 6010C MMSD
01/13/21
DM0113/21000679
4200 mg/kg D.W. 280 860
SW846: 6010C MMSD
01/14/21
DM0114/21000754
4100 mg/kg D.W. 280 850
SW846: 6010C MMSD
01/15/21
DM0115/21000765
3900 mg/kg D.W. 290 860
SW846: 6010C MMSD
01/16/21 DM0116/21000784 3700 mg/kg D.W. 280 860
SW846: 6010C MMSD
01/17/21 DM0117/21000797 3800 mg/kg D.W. 290 860
SW846: 6010C MMSD
01/18/21
DM0118/21000824
3700 mg/kg D.W. 290 870
SW846: 6010C MMSD
01/19/21
DM0119/21000842
4200 mg/kg D.W. 290 860
SW846: 6010C MMSD
01/20/21
DM0120/21000926
4300 mg/kg D.W. 290 860
SW846: 6010C MMSD
01/21/21
DM0121/21000942
4400 mg/kg D.W. 290 860
SW846: 6010C MMSD
01/22/21
DM0122/21000953
3900 mg/kg D.W. 290 870
SW846: 6010C MMSD
01/23/21
DM0123/21000972
3700 mg/kg D.W. 290 870
SW846: 6010C MMSD
01/24/21
DM0124/21001059
4000 mg/kg D.W. 290 870
SW846: 6010C MMSD
01/25/21
DM0125/21001088
4800 mg/kg D.W. 290 870
SW846: 6010C MMSD
01/26/21
DM0126/21001106
4500 mg/kg D.W. 290 870
SW846: 6010C MMSD
01/27/21
DM0127/21001137
4400 mg/kg D.W. 280 850
SW846: 6010C MMSD
01/28/21
DM0128/21001153
3900 mg/kg D.W. 280 850
SW846: 6010C MMSD
01/29/21
DM0129/21001164
4600 mg/kg D.W. 280 840
SW846: 6010C MMSD
01/30/21
DM0130/21001304
4800 mg/kg D.W. 280 850
SW846: 6010C MMSD
01/31/21
DM0131/21001317
4600 mg/kg D.W. 290 860
SW846: 6010C MMSD
02/01/21
DM0201/21001344
3900 mg/kg D.W. 280 860
SW846: 6010C MMSD
02/02/21
DM0202/21001397
3800 mg/kg D.W. 290 860 Q3. SW846: 6010C MMSD
02/03/21
DM0203/21001428
4500 mg/kg D.W. 290 860
SW846: 6010C MMSD
02/04/21
DM0204/21001444
3900 mg/kg D.W. 280 860
SW846: 6010C MMSD
02/05/21
DM0205/21001455
4100 mg/kg D.W. 290 860
SW846: 6010C MMSD
02/06/21
DM0206/21001476
4000 mg/kg D.W. 290 860
SW846: 6010C MMSD
02/07/21
DM0207/21001489
4100 mg/kg D.W. 280 830
SW846: 6010C MMSD
02/08/21
DM0208/21001609
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/09/21
DM0209/21001625
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/10/21
DM0210/21001656
4800 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/11/21 DM0211/21001672 4700 mg/kg D.W. 280 860
SW846: 6010C MMSD
02/12/21 DM0212/21001706 5300 mg/kg D.W. 290 860
SW846: 6010C MMSD
02/13/21 DM0213/21001725 4600 mg/kg D.W. 280 860
SW846: 6010C MMSD
02/14/21
DM0214/21001738
4400 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/15/21
DM0215/21001793
4100 mg/kg D.W. 280 850
SW846: 6010C MMSD
Page 65 of 121
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MMSD
PARTNERS FOI A WAR 11111A01110111
POTASSIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
4200 mg/kg D.W.
280
860
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
4800 mg/kg D.W. 290 860
SW846: 6010C
MMSD
02/18/21
DM0218/21001975
4800 mg/kg D.W. 290 860
SW846: 6010C MMSD
02/19/21
DM0219/21001986
5300 mg/kg D.W. 280 860
SW846: 6010C MMSD
02/20/21
DM0220/21002005
5400 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/21/21
DM0221/21002072
5400 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/22/21
DM0222/21002230
5000 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/23/21
DM0223/21002246
4300 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/24/21
DM0224/21002281
4400 mg/kg D.W. 290 860
SW846: 6010C MMSD
02/25/21
DM0225/21002320
4600 mg/kg D.W. 290 870
SW846: 6010C MMSD
02/26/21
DM0226/21002386
4400 mg/kg D.W. 280 850
SW846: 6010C MMSD
02/27/21
DM0227/21002405
4200 mg/kg D.W. 280 840
SW846: 6010C MMSD
02/28/21
DM0228/21002478
4400 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/01/21
DM0301/21002611
5000 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/02/21
DM0302/21002629
4700 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/03/21 DM0303/21002660 4800 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/04/21 DM0304/21002717 4700 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/05/21
DM0305/21002728
4900 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/06/21
DM0306/21002747
5000 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/07/21
DM0307/21002858
4800 mg/kg D.W. 280 860
SW846: 6010C MMSD
03/08/21
DM0308/21003336
4600 mg/kg D.W. 280 860 Q3. SW846: 6010C MMSD
03/09/21
DM0309/21003371
4000 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/10/21
DM0310/21003402
3900 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/11/21
DM0311/21003456
3900 mg/kg D.W. 280 860
SW846: 6010C MMSD
03/12/21
DM0312/21003522
3900 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/13/21
DM0313/21003541
4800 mg/kg D.W. 280 840
SW846: 6010C MMSD
03/14/21
DM0314/21003554
4700 mg/kg D.W. 280 850 Q2. SW846: 6010C MMSD
03/15/21
DM0315/21003747
4700 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/16/21
DM0316/21003801
4300 mg/kg D.W. 280 840
SW846: 6010C MMSD
03/17/21
DM0317/21003878
4600 mg/kg D.W. 280 850 Q3. SW846: 6010C MMSD
03/18/21
DM0318/21003894
4500 mg/kg D.W. 280 860
SW846: 6010C MMSD
03/19/21
DM0319/21003905
4900 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/20/21
DM0320/21004076
4800 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/21/21
DM0321/21004093
4500 mg/kg D.W. 280 840
SW846: 6010C MMSD
03/22/21
DM0322/21004120
4700 mg/kg D.W. 280 840
SW846: 6010C MMSD
03/23/21
DM0323/21004136
5000 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/24/21
DM0324/21004167
5000 mg/kg D.W. 280 860
SW846: 6010C MMSD
03/25/21
DM0325/21004242
5200 mg/kg D.W. 280 850
SW846: 6010C MMSD
03/26/21
DM0326/21004253
5100 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/27/21
DM0327/21004272
5000 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/28/21
DM0328/21004285
4900 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/29/21 DM0329/21004312 5000 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/30/21 DM0330/21004388 4600 mg/kg D.W. 290 860
SW846: 6010C MMSD
03/31/21 DM0331/21004600 5100 mg/kg D.W. 290 860
SW846: 6010C MMSD
04/01/21
DM0401/21004616
5000 mg/kg D.W. 290 860 Q3. SW846: 6010C MMSD
04/02/21
DM0402/21004627
4800 mg/kg D.W. 290 860
SW846: 6010C MMSD
Page 66 of 121
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MMSD
PARTNERS FOI A CLEANER DI10111M
POTASSIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
4400 mg/kg D.W.
280
860
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
4200 mg/kg D.W. 280 850
SW846: 6010C
MMSD
04/05/21
DM0405/21004742
4600 mg/kg D.W. 280 860
SW846: 6010C MMSD
04/06/21
DM0406/21004758
4600 mg/kg D.W. 280 860
SW846: 6010C MMSD
04/07/21
DM0407/21004843
4200 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/08/21
DM0408/21004861
4400 mg/kg D.W. 280 860
SW846: 6010C MMSD
04/09/21
DM0409/21004912
4300 mg/kg D.W. 290 860
SW846: 6010C MMSD
04/10/21
DM0410/21004931
4400 mg/kg D.W. 290 860
SW846: 6010C MMSD
04/11/21
DM0411 /21005023
4400 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/12/21
DM0412/21005052
4400 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/13/21
DM0413/21005199
4500 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/14/21
DM0414/21005230
4300 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/15/21
DM0415/21005248
4000 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/16/21
DM0416/21005259
4500 mg/kg D.W. 290 860
SW846: 6010C MMSD
04/17/21
DM0417/21005468
4300 mg/kg D.W. 290 860
SW846: 6010C MMSD
04/18/21 DM0418/21005481 4000 mg/kg D.W. 290 860
SW846: 6010C MMSD
04/19/21 DM0419/21005508 4200 mg/kg D.W. 290 870
SW846: 6010C MMSD
04/20/21
DM0420/21005839
4000 mg/kg D.W. 290 870
SW846: 6010C MMSD
04/21/21
DM0421/21005870
4100 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/22/21
DM0422/21005981
4000 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/23/21
DM0423/21005992
3900 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/24/21
DM0424/21006057
3800 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/25/21
DM0425/21006272
3900 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/26/21
DM0426/21006299
3800 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/27/21
DM0427/21006315
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/28/21
DM0428/21006346
3900 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/29/21
DM0429/21006362
3700 mg/kg D.W. 280 850
SW846: 6010C MMSD
04/30/21
DM0430/21006373
4100 mg/kg D.W. 280 840
SW846: 6010C MMSD
05/01/21
DM0501 /21006429
4400 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/02/21
DM0502/21006442
4500 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/03/21
DM0503/21006676
4600 mg/kg D.W. 280 860
SW846: 6010C MMSD
05/04/21
DM0504/21006691
4200 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/05/21
DM0505/21006722
4100 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/06/21
DM0506/21006781
4300 mg/kg D.W. 280 860
SW846: 6010C MMSD
05/07/21
DM0507/21006834
3900 mg/kg D.W. 280 840
SW846: 6010C MMSD
05/08/21
DM0508/21006981
4000 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/09/21
DM0509/21006994
4300 mg/kg D.W. 280 860
SW846: 6010C MMSD
05/10/21
DM0510/21007021
3900 mg/kg D.W. 290 860
SW846: 6010C MMSD
05/11/21
DM0511 /21007171
4000 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/12/21
DM0512/21007202
3900 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/13/21
DM0513/21007217
3600 mg/kg D.W. 280 860
SW846: 6010C MMSD
05/14/21 DM0514/21007309 3700 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/15/21 DM0515/21007328 3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/16/21 DM0516/21007341 3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/17/21
DM0517/21007382
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/18/21
DM0518/21007440
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD
Page 67 of 121
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MMSD
PARTNERS FOI A CLEANER DI10111M
POTASSIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
3300 mg/kg D.W.
280
850
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
3600 mg/kg D.W. 290 860
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
3300 mg/kg D.W. 290 860
SW846: 6010C MMSD
05/22/21 DM0522/21008072
3400 mg/kg D.W. 290 870
SW846: 6010C MMSD
05/23/21 DM0523/21008085
3700 mg/kg D.W. 280 860
SW846: 6010C MMSD
05/25/21 DM0525/21008288
3300 mg/kg D.W. 280 840
SW846: 6010C MMSD
05/26/21 DM0526/21008319
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/27/21 DM0527/21008484
3300 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/28/21 DM0528/21008495
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/29/21 DM0529/21008515
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
05/30/21 DM0530/21008530
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/01/21 DM0601/21008902
3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/02/21 DM0602/21008935
3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/03/21 DM0603/21008950
3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/04/21 DM0604/21009184
3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/05/21 DM0605/21009203 3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/06/21 DM0606/21009287 3700 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/07/21 DM0607/21009314
3900 mg/kg D.W. 280 840
SW846: 6010C MMSD
06/08/21 DM0608/21009334
3700 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/09/21 DM0609/21009365
3800 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/10/21 DM0610/21009538
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/11/21 DM0611/21009549
3400 mg/kg D.W. 280 860
SW846: 6010C MMSD
06/12/21 DM0612/21009568
3500 mg/kg D.W. 290 860
SW846: 6010C MMSD
06/13/21 DM0613/21009602
3500 mg/kg D.W. 290 860
SW846: 6010C MMSD
06/14/21 DM0614/21009629
3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/18/21 DM0618/21009979
3500 mg/kg D.W. 290 860
SW846: 6010C MMSD
06/19/21 DM0619/21010314
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/20/21 DM0620/21010332
3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/21/21 DM0621/21010359
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/22/21 DM0622/21010375
2900 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/23/21 DM0623/21010408
2900 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/24/21 DM0624/21010670
3100 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/25/21 DM0625/21010681
3300 mg/kg D.W. 280 860
SW846: 6010C MMSD
06/26/21 DM0626/21010702
3400 mg/kg D.W. 290 870
SW846: 6010C MMSD
06/27/21 DM0627/21010807
3200 mg/kg D.W. 290 860
SW846: 6010C MMSD
06/28/21 DM0628/21010860
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/29/21 DM0629/21010875
3100 mg/kg D.W. 280 850
SW846: 6010C MMSD
06/30/21 DM0630/21011438
3300 mg/kg D.W. 280 860
SW846: 6010C MMSD
07/01/21 DM0701/21011453
3300 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/02/21 DM0702/21011465
3300 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/03/21 DM0703/21011485
3000 mg/kg D.W. 280 850 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 3000 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/05/21 DM0705/21011572 2900 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/06/21 DM0706/21011693 3000 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/07/21 DM0707/21011727
2800 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/08/21 DM0708/21011742
3000 mg/kg D.W. 280 850
SW846: 6010C MMSD
Page 68 of 121
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MMSD
PARTNERS FOI II CLIMB PI11A0111011
POTASSIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
3200 mg/kg D.W.
280
850
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
3100 mg/kg D.W. 280 840
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
3200 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/12/21 DM0712/21012283
3400 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/13/21 DM0713/21012298
3100 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/14/21 DM0714/21012332
3000 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/15/21 DM0715/21012390
3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/16/21 DM0716/21012563
3700 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/17/21 DM0717/21012583
3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/18/21 DM0718/21012596
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/19/21 DM0719/21012624
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/20/21 DM0720/21012639
3000 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/21/21 DM0721/21012760
3300 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/22/21 DM0722/21012775
3400 mg/kg D.W. 280 860
SW846: 6010C MMSD
07/23/21 DM0723/21013074
4200 mg/kg D.W. 280 860
SW846: 6010C MMSD
07/24/21 DM0724/21013378 3800 mg/kg D.W. 280 860
SW846: 6010C MMSD
07/25/21 DM0725/21013391 3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/26/21 DM0726/21013419
3300 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/27/21 DM0727/21013434
3000 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/28/21 DM0728/21013470
3200 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/29/21 DM0729/21013614
3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
07/30/21 DM0730/21013629
3300 mg/kg D.W. 280 840
SW846: 6010C MMSD
07/31/21 DM0731/21013739
3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/01/21 DM0801/21013752
3000 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/02/21 DM0802/21013891
3300 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/03/21 DM0803/21013906
2900 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/04/21 DM0804/21013940
2700 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/05/21 DM0805/21014673
3200 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/06/21 DM0806/21014685
3100 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/07/21 DM0807/21014705
3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/08/21 DM0809/21014718
3100 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/09/21 DM0809/21014746
3400 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/10/21 DM0810/21014847
3500 mg/kg D.W. 280 850 D2, Q2.
SW846: 6010C MMSD
08/11/21 DM0811/21014867
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/12/21 DM0812/21015285
3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/13/21 DM0813/21015297
3500 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/14/21 DM0814/21015317
3200 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/15/21 DM0815/21015330
2600 mg/kg D.W. 280 830
SW846: 6010C MMSD
08/16/21 DM0816/21015410
2700 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/17/21 DM0817/21015425
2800 mg/kg D.W. 280 830
SW846: 6010C MMSD
08/18/21 DM0818/21016031
2600 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/19/21 DM0819/21016046 2700 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/20/21 DM0820/21016068 2600 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/21/21 DM0821/21016088 3300 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/22/21 DM0822/21016196
3200 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/23/21 DM0823/21016224
3100 mg/kg D.W. 280 840
SW846: 6010C MMSD
Page 69 of 121
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MMSD
PARTNERS FOI A CLEANER DI10111M
POTASSIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
3100 mg/kg D.W.
280
850
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
3300 mg/kg D.W. 280 850
SW846: 6010C
MMSD
08/26/21
DM0826/21016342
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/27/21
DM0827/21016407
3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/28/21
DM0828/21016427
3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
08/30/21
DM0830/21016468
3400 mg/kg D.W. 280 840
SW846: 6010C MMSD
08/31/21
DM0831/21016483
3900 mg/kg D.W. 280 850
SW846: 6010C MMSD
09/01/21
DM0901 /21016598
3600 mg/kg D.W. 280 840
SW846: 6010C MMSD
09/02/21
DM0902/21016659
3800 mg/kg D.W. 280 850
SW846: 6010C MMSD
09/03/21
DM0903/21016671
4200 mg/kg D.W. 280 860
SW846: 6010C MMSD
09/04/21
DM0904/21017055
3700 mg/kg D.W. 280 840
SW846: 6010C MMSD
09/05/21
DM0905/21017068
4100 mg/kg D.W. 280 850
SW846: 6010C MMSD
09/06/21
DM0906/21017096
3900 mg/kg D.W. 280 840
SW846: 6010C MMSD
09/07/21
DM0907/21017306
4100 mg/kg D.W. 280 850
SW846: 6010C MMSD
09/08/21
DM0908/21017338
4100 mg/kg D.W. 280 850
SW846: 6010C MMSD
09/09/21 DM0909/21017408 3500 mg/kg D.W. 280 850
SW846: 6010C MMSD
09/10/21 DM0910/21017420 3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
09/11/21
DM0911 /21017699
3400 mg/kg D.W. 280 840
SW846: 6010C MMSD
09/12/21
DM0912/21017712
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD
09/13/21
DM0913/21017740
3800 mg/kg D.W. 280 850
SW846: 6010C MMSD
09/14/21
DM0914/21017755
3500 mg/kg D.W. 280 850
SW846: 6010C MMSD 149990-1
09/15/21
DM0915/21017903
3700 mg/kg D.W. 280 850
SW846: 6010C MMSD 149990-1
09/16/21
DM0916/21018023
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD 150012-1
09/17/21
DM0917/21018105
3000 mg/kg D.W. 280 860
SW846: 6010C MMSD 150074-1
09/18/21
DM0918/21018125
3000 mg/kg D.W. 280 850
SW846: 6010C MMSD 150074-1
09/19/21
DM0919/21018138
3000 mg/kg D.W. 290 860
SW846: 6010C MMSD 150074-1
09/20/21
DM0920/21018236
3300 mg/kg D.W. 290 860
SW846: 6010C MMSD 150123-1
09/21/21
DM0921/21018251
3300 mg/kg D.W. 280 850
SW846: 6010C MMSD 150123-1
09/22/21
DM0922/21018480
3700 mg/kg D.W. 280 850
SW846: 6010C MMSD
09/23/21
DM0923/21018564
4000 mg/kg D.W. 280 840
SW846: 6010C MMSD
09/24/21
DM0924/21018818
3800 mg/kg D.W. 280 840
SW846: 6010C MMSD 150235-1
09/25/21
DM0925/21018838
3900 mg/kg D.W. 280 840
SW846: 6010C MMSD 150235-1
09/26/21
DM0926/21019023
3800 mg/kg D.W. 280 840
SW846: 6010C MMSD 150235-1
09/27/21
DM0927/21019051
4000 mg/kg D.W. 280 840
SW846: 6010C MMSD 150235-2
09/28/21
DM0928/21019066
4100 mg/kg D.W. 280 850
SW846: 6010C MMSD 150235-3
09/29/21
DM0929/21019228
3600 mg/kg D.W. 280 840 Q2. SW846: 6010C MMSD 150305-1
09/30/21
DM0930/21019243
3900 mg/kg D.W. 280 840
SW846: 6010C MMSD 150305-1
10/01/21
DM 1001 /21019255
4200 mg/kg D.W. 280 840
SW846: 6010C MMSD 150305-1
10/02/21
DM1002/21019384
4000 mg/kg D.W. 280 840
SW846: 6010C MMSD 150305-1
10/03/21
DM1003/21019397
3900 mg/kg D.W. 280 850
SW846: 6010C MMSD 150305-1
10/04/21
DM1004/21019425
3700 mg/kg D.W. 280 850
SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 3100 mg/kg D.W. 280 850
SW846: 6010C MMSD 150431-1
10/07/21 DM1007/21019760 3000 mg/kg D.W. 280 840
SW846: 6010C MMSD 150431-1
10/08/21 DM1008/21019772 2700 mg/kg D.W. 280 840
SW846: 6010C MMSD 150445-1
10/19/21
DM 1019/21020600
3100 mg/kg D.W. 280 830
SW846: 6010C MMSD 150655-1
10/20/21
DM 1020/21020674
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD 150655-1
Page 70 of 121
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MMSD
PARTNERS FOI A CLEANER DI1101110N1
POTASSIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
10/21/21
DM 1021 /21020689
3500 mg/kg D.W.
280
840
SW846: 6010C
MMSD
150655-1
10/22/21
DM 1022/21020701
3800 mg/kg D.W. 280 840
SW846: 6010C
MMSD 150703-1
10/23/21 DM1023/21020883
4000 mg/kg D.W. 280 840
SW846: 6010C MMSD 150703-1
10/24/21 DM1024/21021034
4000 mg/kg D.W. 280 850
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062
4300 mg/kg D.W. 280 840 D2, Q2.
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077
4200 mg/kg D.W. 280 840
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161
3900 mg/kg D.W. 280 850
SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226
3800 mg/kg D.W. 280 850
SW846: 6010C MMSD 150831-1
10/29/21 DM1029/21021510
3800 mg/kg D.W. 280 850
SW846: 6010C MMSD 150831-1
10/30/21 DM1030/21021530
3700 mg/kg D.W. 280 850
SW846: 6010C MMSD 150831-1
10/31/21 DM 1031 /21021574
3500 mg/kg D.W. 290 860
SW846: 6010C MMSD 150831-1
11/01/21 DM 1101 /21021608
3800 mg/kg D.W. 290 860
SW846: 6010C MMSD 150831-1
11/02/21 DM1102/21021623
4000 mg/kg D.W. 290 860
SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720
3600 mg/kg D.W. 280 850
SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735
3400 mg/kg D.W. 280 840
SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 3200 mg/kg D.W. 280 840
SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 3000 mg/kg D.W. 280 850
SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553
3200 mg/kg D.W. 280 860
SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581
3600 mg/kg D.W. 280 860
SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596
3900 mg/kg D.W. 280 860
SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680
4000 mg/kg D.W. 290 860
SW846: 6010C MMSD 151039-2
11/11/21 DM1111/21022695
4100 mg/kg D.W. 290 860
SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707
4300 mg/kg D.W. 290 860
SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731
4100 mg/kg D.W. 280 850
SW846: 6010C MMSD 151039-1
11/14/21 DM1114/21022744
4100 mg/kg D.W. 290 860
SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772
3800 mg/kg D.W. 290 860
SW846: 6010C MMSD 151085-1
11/16/21 DM1116/21022787
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD 151085-1
11/17/21 DM1117/21023039
3300 mg/kg D.W. 280 850 Q2, Q3.
SW846: 6010C MMSD 151122-1
11/18/21 DM1118/21023056
3500 mg/kg D.W. 280 850
SW846: 6010C MMSD 151122-1
11/19/21 DM1119/21023181
4000 mg/kg D.W. 280 850
SW846: 6010C MMSD 151175-1
11/20/21 DM1120/21023201
4000 mg/kg D.W. 290 860
SW846: 6010C MMSD 151175-1
11/21/21 DM 1121 /21023214
3700 mg/kg D.W. 290 870
SW846: 6010C MMSD 151175-1
11/22/21 DM1122/21023555
3900 mg/kg D.W. 290 870
SW846: 6010C MMSD 151175-1
11/23/21 DM1123/21023570
3500 mg/kg D.W. 290 860
SW846: 6010C MMSD 151252-1
11/24/21 DM1124/21023611
3300 mg/kg D.W. 280 860
SW846: 6010C MMSD 151266-1
11/25/21 DM1125/21023795
3400 mg/kg D.W. 290 860
SW846: 6010C MMSD 151266-1
11/26/21 DM1126/21023807
3300 mg/kg D.W. 290 860
SW846: 6010C MMSD 151266-1
11/27/21 DM1127/21023827
3500 mg/kg D.W. 290 870
SW846: 6010C MMSD 151266-1
11/28/21 DM1128/21023899
3400 mg/kg D.W. 290 860
SW846: 6010C MMSD 151266-1
11/29/21 DM1129/21023927
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD 151294-1
11/30/21 DM1130/21024167
3100 mg/kg D.W. 280 850
SW846: 6010C MMSD 151317-1
12/01/21 DM1201/21024282 3200 mg/kg D.W. 280 840
SW846: 6010C MMSD 151317-2
12/02/21 DM1202/21024297 3100 mg/kg D.W. 280 850
SW846: 6010C MMSD 151342-1
12/03/21 DM1203/21024309 3100 mg/kg D.W. 280 850
SW846: 6010C MMSD 151371-1
12/04/21 DM 1204/21024329
3400 mg/kg D.W. 290 860
SW846: 6010C MMSD 151371-1
12/05/21 DM 1205/21024739
3500 mg/kg D.W. 290 870
SW846: 6010C MMSD 151371-1
Page 71 of 121
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MMSD
PARTNERS FOI A CLEANER DI1101110N1
POTASSIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a.
QC Batch
ID
12/06/21
DM1206/21024767
3600 mg/kg D.W.
290
860
SW846: 6010C
MMSD
151391-1
12/07/21
DM 1207/21024782
3800 mg/kg D.W. 290 870
SW846: 6010C
MMSD 151422-1
12/08/21
DM1208/21024816
3700 mg/kg D.W. 290 870 98.
SW846: 6010C MMSD 151471-1
12/09/21
DM 1209/21024832
3600 mg/kg D.W. 290 870 98.
SW846: 6010C MMSD 151471-2
12/10/21
DM1210/21024844
3700 mg/kg D.W. 290 870
SW846: 6010C MMSD 151498-1
12/11/21
DM 1211 /21024864
3800 mg/kg D.W. 280 850
SW846: 6010C MMSD 151498-1
12/12/21
DM1212/21025174
3500 mg/kg D.W. 280 840
SW846: 6010C MMSD 151498-1
12/13/21
DM 1213/21025205
3200 mg/kg D.W. 290 860
SW846: 6010C MMSD 151543-1
12/14/21
DM1214/21025220
3400 mg/kg D.W. 280 850
SW846: 6010C MMSD 151576-1
12/15/21
DM1215/21025299
3900 mg/kg D.W. 290 860
SW846: 6010C MMSD 151576-1
12/16/21
DM1216/21025314
3800 mg/kg D.W. 280 850
SW846: 6010C MMSD 151645-1
12/17/21
DM1217/21025326
3300 mg/kg D.W. 290 860
SW846: 6010C MMSD 151645-1
12/18/21
DM1219/21025346
3000 mg/kg D.W. 290 860
SW846: 6010C MMSD 151645-1
12/19/21
DM1219/21025621
2900 mg/kg D.W. 290 870
SW846: 6010C MMSD 151645-1
12/20/21
DM 1220/21025649
3300 mg/kg D.W. 290 870
SW846: 6010C MMSD 151645-2
12/21/21 DM1221/21025664 3200 mg/kg D.W. 290 870
SW846: 6010C MMSD 151668-1
12/22/21 DM1222/21025700 3300 mg/kg D.W. 290 860
SW846: 6010C MMSD 151750-1
12/23/21
DM1223/21025779
3300 mg/kg D.W. 290 870
SW846: 6010C MMSD 151750-2
12/24/21
DM1224/21025791
3300 mg/kg D.W. 290 880
SW846: 6010C MMSD 151750-2
12/25/21
DM1225/21025811
3400 mg/kg D.W. 290 860
SW846: 6010C MMSD 151750-2
12/26/21
DM 1226/21025824
3500 mg/kg D.W. 290 870
SW846: 6010C MMSD 151750-2
12/27/21
DM1227/21025917
3400 mg/kg D.W. 280 860
SW846: 6010C MMSD 151750-2
12/28/21
DM1228/21025932
3700 mg/kg D.W. 290 860
SW846: 6010C MMSD 151750-2
12/29/21
DM1229/21025966
3800 mg/kg D.W. 290 860
SW846: 6010C MMSD 151827-1
12/30/21
DM 1230/21025981
3900 mg/kg D.W. 290 860
SW846: 6010C MMSD 151827-1
12/31/21
DM 1231 /21026033
3900 mg/kg D.W. 290 860
SW846: 6010C MMSD 151827-1
Avg Result: 3800 mg/kg D.W. Min LOD: 280 mg/kg D.W.
Max Result: 5400 mg/kg D.W. Max LOD: 290 mg/kg D.W.
Page 72 of 121
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MMSD
PARTAERS FOI A CLEAAfM PA1110MFW{A'[
SELENIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
4.7 mg/kg D.W.
1.9
7.9
3.
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
4.9 mg/kg D.W.
1.9 7.9
3.
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
4.2 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD
01/04/21 DM0104/21000488 4.8 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD
01/05/21 DM0105/21000504 4 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
01/06/21 DM0106/21000535 6.1 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
01/07/21 DM0107/21000551 4.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
01/08/21 DM0108/21000562 3.8 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
01/09/21 DM0109/21000581 4.2 mg/kg D.W. 1.9 8 3. SW846: 6010C MMSD
01/10/21 DM0110/21000594 3.6 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
01/11/21 DM0111/21000632 4.5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
01/12/21 DM0112/21000648 2.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
01/13/21 DM0113/21000679 2.6 mg/kg D.W. 1.9 7.8 3, Q3. SW846: 6010C MMSD
01/14/21 DM0114/21000754 3.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
01/15/21 DM0115/21000765 3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
01/16/21 DM0116/21000784 2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
01/17/21 DM0117/21000797 < 1.9 mg/kg D.W. 1.9 7.9 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 7 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
01/19/21 DM0119/21000842 < 1.9 mg/kg D.W. 1.9 7.9
SW846: 6010C MMSD
01/20/21 DM0120/21000926 3.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
01/21/21 DM0121/21000942 3.5 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
01/22/21 DM0122/21000953 2 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
01/23/21 DM0123/21000972 < 1.9 mg/kg D.W. 1.9 7.9
SW846: 6010C MMSD
01/24/21 DM0124/21001059 3 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
01/25/21 DM0125/21001088 4.8 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
01/26/21 DM0126/21001106 5.4 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
01/27/21 DM0127/21001137 3.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
01/28/21 DM0128/21001153 5.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
01/29/21 DM0129/21001164 5.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
01/30/21 DM0130/21001304 4.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
01/31/21 DM0131/21001317 5.1 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/01/21 DM0201/21001344 6.2 mg/kg D.W. 1.9 7.8 D2, 3, Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 3 mg/kg D.W. 1.9 7.9 D2, 3. SW846: 6010C MMSD
02/03/21 DM0203/21001428 5.1 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
02/04/21 DM0204/21001444 5.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/05/21 DM0205/21001455 6.6 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
02/06/21 DM0206/21001476 5.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/07/21 DM0207/21001489 5.3 mg/kg D.W. 1.8 7.6 3. SW846: 6010C MMSD
02/08/21 DM0208/21001609 4.5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
02/09/21 DM0209/21001625 5.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/10/21 DM0210/21001656 5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/11/21 DM0211/21001672 4.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/12/21 DM0212/21001706 4.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/13/21 DM0213/21001725 5.1 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/14/21 DM0214/21001738 4.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/15/21 DM0215/21001793 3.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
Page 73 of 121
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MMSD
PARTNERS FOI II CLIMB11A0111011
SELENIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
4.2 mg/kg D.W.
1.9
7.8
3.
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
5.3 mg/kg D.W.
1.9 7.9
3.
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
4.6 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD
02/19/21 DM0219/21001986 3.2 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD
02/20/21 DM0220/21002005 2.4 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
02/21/21 DM0221/21002072 3.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
02/22/21 DM0222/21002230 4.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/23/21 DM0223/21002246 4.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/24/21 DM0224/21002281 3.1 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
02/25/21 DM0225/21002320 3.5 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
02/26/21 DM0226/21002386 2.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
02/27/21 DM0227/21002405 3 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
02/28/21 DM0228/21002478 < 1.9 mg/kg D.W. 1.9 7.8 D2. SW846: 6010C MMSD
03/01/21 DM0301/21002611 5.7 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
03/02/21 DM0302/21002629 < 1.9 mg/kg D.W. 1.9 7.7
SW846: 6010C MMSD
03/03/21 DM0303/21002660 4.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/04/21 DM0304/21002717 5.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/05/21 DM0305/21002728 5.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/06/21 DM0306/21002747 6.1 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
03/07/21 DM0307/21002858 6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/08/21 DM0308/21003336 6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/09/21 DM0309/21003371 6.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/10/21 DM0310/21003402 3.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/11/21 DM0311/21003456 3.8 mg/kg D.W. 1.9 7.8 3, Q3. SW846: 6010C MMSD
03/12/21 DM0312/21003522 4.6 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
03/13/21 DM0313/21003541 5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
03/14/21 DM0314/21003554 4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/15/21 DM0315/21003747 4.6 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
03/16/21 DM0316/21003801 2.3 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
03/17/21 DM0317/21003878 3.4 mg/kg D.W. 1.9 7.8 3, Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 6.1 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/19/21 DM0319/21003905 6.4 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
03/20/21 DM0320/21004076 8.2 mg/kg D.W. 1.9 7.7
SW846: 6010C MMSD
03/21/21 DM0321/21004093 6.5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
03/22/21 DM0322/21004120 5.5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
03/23/21 DM0323/21004136 4.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/24/21 DM0324/21004167 4.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/25/21 DM0325/21004242 6.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/26/21 DM0326/21004253 5.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/27/21 DM0327/21004272 5.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/28/21 DM0328/21004285 5.9 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
03/29/21 DM0329/21004312 3.5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
03/30/21 DM0330/21004388 4.6 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
03/31/21 DM0331/21004600 5.3 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
04/01/21 DM0401/21004616 3.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/02/21 DM0402/21004627 3.7 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
Page 74 of 121
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MMSD
PARTNERS FOI A CLEANER DI10111M
SELENIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
3.5 mg/kg D.W.
1.9
7.8
3.
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
3.2 mg/kg D.W.
1.9 7.7
3.
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
3.2 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD
04/06/21 DM0406/21004758 5.5 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD
04/07/21 DM0407/21004843 3.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/08/21 DM0408/21004861 4.5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/09/21 DM0409/21004912 4.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/10/21 DM0410/21004931 4.5 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
04/11/21 DM0411/21005023 5.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/12/21 DM0412/21005052 3.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/13/21 DM0413/21005199 4.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/14/21 DM0414/21005230 7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/15/21 DM0415/21005248 3.1 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/16/21 DM0416/21005259 4.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/17/21 DM0417/21005468 4.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/18/21 DM0418/21005481 3.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/19/21 DM0419/21005508 5.4 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
04/20/21 DM0420/21005839 5.2 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
04/21/21 DM0421/21005870 4.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/22/21 DM0422/21005981 3.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
04/23/21 DM0423/21005992 4.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/24/21 DM0424/21006057 4.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/25/21 DM0425/21006272 5.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/26/21 DM0426/21006299 3.1 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
04/27/21 DM0427/21006315 3.5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/28/21 DM0428/21006346 4.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/29/21 DM0429/21006362 4.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
04/30/21 DM0430/21006373 3.7 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
05/01/21 DM0501/21006429 4.5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/02/21 DM0502/21006442 3.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/03/21 DM0503/21006676 4.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/04/21 DM0504/21006691 3.1 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
05/05/21 DM0505/21006722 3.5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
05/06/21 DM0506/21006781 4.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/07/21 DM0507/21006834 3.6 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
05/08/21 DM0508/21006981 4.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/09/21 DM0509/21006994 4.1 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/10/21 DM0510/21007021 5.3 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
05/11/21 DM0511/21007171 5.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/12/21 DM0512/21007202 4.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/13/21 DM0513/21007217 4.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/14/21 DM0514/21007309 4.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/15/21 DM0515/21007328 4.3 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
05/16/21 DM0516/21007341 4.7 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
05/17/21 DM0517/21007382 6.9 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
05/18/21 DM0518/21007440 5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
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MMSD
PARTNERS FOI II CLIMB PI11A0111011
SELENIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
6.4 mg/kg D.W.
1.9
7.7
J.
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
5.7 mg/kg D.W.
1.9 7.8
3.
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
4.8 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD
05/22/21 DM0522/21008072 3.5 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD
05/23/21 DM0523/21008085 5.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/25/21 DM0525/21008288 5.3 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
05/26/21 DM0526/21008319 5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/27/21 DM0527/21008484 7.4 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
05/28/21 DM0528/21008495 5.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/29/21 DM0529/21008515 5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
05/30/21 DM0530/21008530 5.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/01/21 DM0601/21008902 5.3 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
06/02/21 DM0602/21008935 4.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/03/21 DM0603/21008950 6 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
06/04/21 DM0604/21009184 5.1 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
06/05/21 DM0605/21009203 4.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/06/21 DM0606/21009287 4.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/07/21 DM0607/21009314 5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
06/08/21 DM0608/21009334 6.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/09/21 DM0609/21009365 5.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/10/21 DM0610/21009538 4.1 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/11/21 DM0611/21009549 5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/12/21 DM0612/21009568 5.8 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
06/13/21 DM0613/21009602 5.8 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
06/14/21 DM0614/21009629 3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/18/21 DM0618/21009979 4.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/19/21 DM0619/21010314 5.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/20/21 DM0620/21010332 4.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/21/21 DM0621/21010359 4.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/22/21 DM0622/21010375 4 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
06/23/21 DM0623/21010408 5.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/24/21 DM0624/21010670 6.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/25/21 DM0625/21010681 6.1 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/26/21 DM0626/21010702 5.5 mg/kg D.W. 1.9 8 3. SW846: 6010C MMSD
06/27/21 DM0627/21010807 5.2 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD
06/28/21 DM0628/21010860 6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/29/21 DM0629/21010875 2.5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
06/30/21 DM0630/21011438 3.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/01/21 DM0701/21011453 5.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/02/21 DM0702/21011465 3.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/03/21 DM0703/21011485 2.6 mg/kg D.W. 1.9 7.8 3, T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 3.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/05/21 DM0705/21011572 4.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/06/21 DM0706/21011693 5.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/07/21 DM0707/21011727 6.7 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
07/08/21 DM0708/21011742 5.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
Page 76 of 121
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MMSD
PARTNERS FOI II CLIMB11A0111011
SELENIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
4.7 mg/kg D.W.
1.9
7.7
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
5.4 mg/kg D.W.
1.9 7.7
3.
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
4.2 mg/kg D.W. 1.9 7.7 3.
SW846: 6010C MMSD
07/12/21 DM0712/21012283 4.2 mg/kg D.W. 1.9 7.7 3.
SW846: 6010C MMSD
07/13/21 DM0713/21012298 4.9 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
07/14/21 DM0714/21012332 3.3 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
07/15/21 DM0715/21012390 5.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/16/21 DM0716/21012563 4.4 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
07/17/21 DM0717/21012583 4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/18/21 DM0718/21012596 4.1 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
07/19/21 DM0719/21012624 3.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/20/21 DM0720/21012639 5.3 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
07/21/21 DM0721/21012760 4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/22/21 DM0722/21012775 3.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/23/21 DM0723/21013074 < 1.9 mg/kg D.W. 1.9 7.8
SW846: 6010C MMSD
07/24/21 DM0724/21013378 3.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/25/21 DM0725/21013391 2.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/26/21 DM0726/21013419 4.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/27/21 DM0727/21013434 5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/28/21 DM0728/21013470 6 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
07/29/21 DM0729/21013614 2.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
07/30/21 DM0730/21013629 3.6 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
07/31/21 DM0731/21013739 4.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
08/01/21 DM0801/21013752 4.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
08/02/21 DM0802/21013891 4.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
08/03/21 DM0803/21013906 4.6 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
08/04/21 DM0804/21013940 6.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
08/05/21 DM0805/21014673 10 mg/kg D.W. 1.9 7.7
SW846: 6010C MMSD
08/06/21 DM0806/21014685 3.1 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
08/07/21 DM0807/21014705 3.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
08/08/21 DM0809/21014718 2.1 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
08/09/21 DM0809/21014746 3.5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
08/10/21 DM0810/21014847 5.1 mg/kg D.W. 1.9 7.8 D2, 3, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 3.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
08/12/21 DM0812/21015285 4.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
08/13/21 DM0813/21015297 3.4 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
08/14/21 DM0814/21015317 4.1 mg/kg D.W. 1.8 7.6 3. SW846: 6010C MMSD
08/15/21 DM0815/21015330 2.8 mg/kg D.W. 1.8 7.6 3. SW846: 6010C MMSD
08/16/21 DM0816/21015410 3 mg/kg D.W. 1.8 7.6 3. SW846: 6010C MMSD
08/17/21 DM0817/21015425 3.9 mg/kg D.W. 1.8 7.6 3. SW846: 6010C MMSD
08/18/21 DM0818/21016031 3.6 mg/kg D.W. 1.8 7.6 3. SW846: 6010C MMSD
08/19/21 DM0819/21016046 3.4 mg/kg D.W. 1.9 7.6 3. SW846: 6010C MMSD
08/20/21 DM0820/21016068 4 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
08/21/21 DM0821/21016088 3.6 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
08/22/21 DM0822/21016196 4.4 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
08/23/21 DM0823/21016224 < 1.9 mg/kg D.W. 1.9 7.7
SW846: 6010C MMSD
Page 77 of 121
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MMSD
PARTAFRS FOI A C/DAEA11A0111011
SELENIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
3 mg/kg D.W.
1.9
7.8
3.
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
3.7 mg/kg D.W.
1.9 7.7
3.
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
3.4 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD
08/27/21 DM0827/21016407 3.7 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD
08/28/21 DM0828/21016427 4.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
08/30/21 DM0830/21016468 2.4 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
08/31/21 DM0831/21016483 6.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
09/01/21 DM0901/21016598 5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
09/02/21 DM0902/21016659 3.9 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
09/03/21 DM0903/21016671 3.5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
09/04/21 DM0904/21017055 3.2 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
09/05/21 DM0905/21017068 3.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
09/06/21 DM0906/21017096 3.4 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
09/07/21 DM0907/21017306 3.1 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
09/08/21 DM0908/21017338 4.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
09/09/21 DM0909/21017408 4.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
09/10/21 DM0910/21017420 3.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
09/11/21 DM0911/21017699 4.1 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
09/12/21 DM0912/21017712 3.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
09/13/21 DM0913/21017740 < 1.9 mg/kg D.W. 1.9 7.8
SW846: 6010C MMSD
09/14/21 DM0914/21017755 4.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 4.6 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 4.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 150012-1
09/17/21 DM0917/21018105 < 1.9 mg/kg D.W. 1.9 7.8
SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 < 1.9 mg/kg D.W. 1.9 7.8
SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 < 1.9 mg/kg D.W. 1.9 7.8
SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 2.7 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 150123-1
09/21/21 DM0921/21018251 2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 150123-1
09/22/21 DM0922/21018480 3.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD
09/23/21 DM0923/21018564 2.3 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD
09/24/21 DM0924/21018818 3.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 4.8 mg/kg D.W. 1.8 7.6 3. SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 4.5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 3.6 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 4.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 4.2 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 4.1 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 4.5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 3.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 2.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150431-1
10/07/21 DM1007/21019760 2.5 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150431-1
10/08/21 DM1008/21019772 2.3 mg/kg D.W. 1.9 7.6 3. SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 4 mg/kg D.W. 1.8 7.6 3. SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 3.6 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150655-1
Page 78 of 121
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MMSD
PARTNERS FOI II CLIMB PI11A0111011
SELENIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
10/21/21
DM 1021 /21020689
4.1 mg/kg D.W.
1.9
7.7
3.
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
< 1.9 mg/kg D.W.
1.9 7.7
SW846: 6010C
MMSD 150703-1
10/23/21 DM1023/21020883
7.3 mg/kg D.W. 1.9 7.6 3.
SW846: 6010C MMSD 150703-1
10/24/21 DM1024/21021034
2 mg/kg D.W. 1.9 7.7 3.
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 < 1.9 mg/kg D.W. 1.9 7.7 D2, Q2. SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 5.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 11 mg/kg D.W. 1.9 7.8
SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 3.3 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150831-1
10/29/21 DM1029/21021510 3.5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 150831-1
10/30/21 DM1030/21021530 3.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 150831-1
10/31/21 DM1031/21021574 3.9 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 150831-1
11/01/21 DM1101/21021608 3.9 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 150831-1
11/02/21 DM1102/21021623 4.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 3.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 4.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 3.9 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 4.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 3.9 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 3.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 4.2 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 151039-2
11/11/21 DM1111/21022695 5 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 4.3 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 3.8 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 151039-1
11/14/21 DM1114/21022744 4.3 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 4.3 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 151085-1
11/16/21 DM1116/21022787 3.2 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 151085-1
11/17/21 DM1117/21023039 4.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 151122-1
11/18/21 DM1118/21023056 3.5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 151122-1
11/19/21 DM1119/21023181 5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 151175-1
11/20/21 DM1120/21023201 4.7 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 151175-1
11/21/21 DM1121/21023214 4.2 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 151175-1
11/22/21 DM1122/21023555 4.2 mg/kg D.W. 1.9 8 3. SW846: 6010C MMSD 151175-1
11/23/21 DM1123/21023570 5 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 151252-1
11/24/21 DM1124/21023611 4.4 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 151266-1
11/25/21 DM1125/21023795 3.7 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 151266-1
11/26/21 DM1126/21023807 4.2 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 151266-1
11/27/21 DM1127/21023827 5.1 mg/kg D.W. 1.9 8 3. SW846: 6010C MMSD 151266-1
11/28/21 DM1128/21023899 4.1 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 151266-1
11/29/21 DM1129/21023927 3.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 151294-1
11/30/21 DM1130/21024167 3.1 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 151317-1
12/01/21 DM1201/21024282 2.8 mg/kg D.W. 1.9 7.7 3. SW846: 6010C MMSD 151317-2
12/02/21 DM1202/21024297 4.7 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 151342-1
12/03/21 DM1203/21024309 4.1 mg/kg D.W. 1.9 7.8 3. SW846: 6010C MMSD 151371-1
12/04/21 DM1204/21024329 4.4 mg/kg D.W. 1.9 7.9 3. SW846: 6010C MMSD 151371-1
12/05/21 DM1205/21024739 4.4 mg/kg D.W. 1.9 7.9 D2, 3, Q3. SW846: 6010C MMSD 151371-1
Page 79 of 121
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MMSD
PARTNERS FOI II CLIMB11A0111011
SELENIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result
LOD LOQ QA Flags
• na Ica ' e • a.
QC Batch
ID
12/06/21
DM1206/21024767
4 mg/kg D.W.
1.9
7.9
3.
SW846: 6010C
MMSD
151391-1
12/07/21
DM 1207/21024782
3 mg/kg D.W.
1.9 7.9
3.
SW846: 6010C
MMSD 151422-1
12/08/21 DM 1208/21024816
4.1 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151471-1
12/09/21 DM1209/21024832 3.4 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151471-2
12/10/21 DM1210/21024844 4.4 mg/kg D.W. 1.9 8 3.
SW846: 6010C MMSD 151498-1
12/11/21 DM1211/21024864 4.3 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD 151498-1
12/12/21 DM1212/21025174 4.2 mg/kg D.W. 1.9 7.7 3.
SW846: 6010C MMSD 151498-1
12/13/21 DM1213/21025205 2.7 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151543-1
12/14/21 DM1214/21025220 2.8 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD 151576-1
12/15/21 DM1215/21025299 2 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD 151576-1
12/16/21 DM1216/21025314 4.6 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD 151645-1
12/17/21 DM1217/21025326 4.4 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151645-1
12/18/21 DM1219/21025346 4.5 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151645-1
12/19/21 DM1219/21025621 4.6 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151645-1
12/20/21 DM1220/21025649 4.1 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151645-2
12/21/21 DM1221/21025664 4 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151668-1
12/22/21 DM1222/21025700 3.9 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151750-1
12/23/21 DM1223/21025779 4.6 mg/kg D.W. 1.9 8 3.
SW846: 6010C MMSD 151750-2
12/24/21 DM1224/21025791 4.2 mg/kg D.W. 1.9 8 3.
SW846: 6010C MMSD 151750-2
12/25/21 DM1225/21025811 4 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151750-2
12/26/21 DM1226/21025824 4.4 mg/kg D.W. 1.9 8 3.
SW846: 6010C MMSD 151750-2
12/27/21 DM1227/21025917 5.2 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD 151750-2
12/28/21 DM1228/21025932 4.8 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD 151750-2
12/29/21 DM1229/21025966 4 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151827-1
12/30/21 DM1230/21025981 3 mg/kg D.W. 1.9 7.9 3.
SW846: 6010C MMSD 151827-1
12/31/21 DM1231/21026033 3.8 mg/kg D.W. 1.9 7.8 3.
SW846: 6010C MMSD 151827-1
Avg Result: 4.2 mg/kg D.W. Min LOD: 1.8 mg/kg D.W.
Max Result: 11 mg/kg D.W. Max LOD: 1.9 mg/kg D.W.
Page 80 of 121
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MMSD
PARTNERS FOI A OAR Br1110111011
Solids (% Moisture)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Analytica ' e o. a.
QC Batch
ID
01/01/21
DM0101/21000012
5.9 %
0.1
SM 2540 G (1997)
MMSD
01/02/21
DM0102/21000031
6.2 % 0.1
SM 2540 G (1997) MMSD
01/03/21 DM0103/21000076
5.6 % 0.1
SM 2540 G (1997) MMSD
01/04/21 DM0104/21000488
SM 2540 G (1997) MMSD
01/05/21 DM0105/21000504
6.9 % 0.1
SM 2540 G (1997) MMSD
01/06/21 DM0106/21000535 5.5 % 0.1
SM 2540 G (1997) MMSD
01/07/21 DM0107/21000551 5.7 % 0.1
SM 2540 G (1997) MMSD
01/08/21 DM0108/21000562 6.4 % 0.1
SM 2540 G (1997) MMSD
01/09/21 DM0109/21000581 7.4 % 0.1 SM 2540 G (1997) MMSD
01/10/21 DM0110/21000594 6.8 % 0.1 SM 2540 G (1997) MMSD
01/11/21 DM0111/21000632 5.8 % 0.1 SM 2540 G (1997) MMSD
01/12/21 DM0112/21000648 5.8 % 0.1 SM 2540 G (1997) MMSD
01/13/21 DM0113/21000679 5.5 % 0.1 SM 2540 G (1997) MMSD
01/14/21 DM0114/21000754
5%
0.1
SM 2540 G (1997) MMSD
01/15/21 DM0115/21000765 5.7 % 0.1 SM 2540 G (1997) MMSD
01/16/21
01/17/21
DM0116/21000784
DM0117/21000797
5.5 % 0.1
SM 2540 G (1997) MMSD
6.4 % 0.1
SM 2540 G (1997) MMSD
01/18/21 DM0118/21000824 6.6 % 0.1 SM 2540 G (1997) MMSD
01/19/21 DM0119/21000842 6.4 % 0.1 SM 2540 G (1997) MMSD
01/20/21 DM0120/21000926 5.6 % 0.1 SM 2540 G (1997) MMSD
01/21/21 DM0121/21000942 6.1 % 0.1 SM 2540 G (1997) MMSD
01/22/21 DM0122/21000953 6.8 % 0.1 SM 2540 G (1997) MMSD
01/23/21 DM0123/21000972 6.5 % 0.1 SM 2540 G (1997) MMSD
01/24/21 DM0124/21001059 6.8 % 0.1 SM 2540 G (1997) MMSD
01/25/21 DM0125/21001088 6.9 % 0.1 SM 2540 G (1997) MMSD
01/26/21 DM0126/21001106 6.6 % 0.1 SM 2540 G (1997) MMSD
01/27/21 DM0127/21001137 5.1 % 0.1 SM 2540 G (1997) MMSD
01/28/21 DM0128/21001153 4.9 % 0.1 SM 2540 G (1997) MMSD
01/29/21 DM0129/21001164 3.5 % 0.1 SM 2540 G (1997) MMSD
01/30/21 DM0130/21001304 4.6 % 0.1 SM 2540 G (1997) MMSD
01/31/21 DM0131/21001317 5.7 % 0.1 SM 2540 G (1997) MMSD
02/01/21 DM0201/21001344 5.4 % 0.1 SM 2540 G (1997) MMSD
02/02/21 DM0202/21001397 6.1 % 0.1 SM 2540 G (1997) MMSD
02/03/21 DM0203/21001428 6 % 0.1 SM 2540 G (1997) MMSD
02/04/21 DM0204/21001444 5.4 % 0.1 SM 2540 G (1997) MMSD
02/05/21 DM0205/21001455 6.2 % 0.1 SM 2540 G (1997) MMSD
02/06/21 DM0206/21001476 5.7 % 0.1 SM 2540 G (1997) MMSD
02/07/21 DM0207/21001489 2.6 % 0.1 SM 2540 G (1997) MMSD
02/08/21 DM0208/21001609 4.5 % 0.1 SM 2540 G (1997) MMSD
02/09/21 DM0209/21001625
5%
0.1
SM 2540 G (1997) MMSD
02/10/21 DM0210/21001656 5.1 % 0.1 SM 2540 G (1997) MMSD
02/11/21
02/12/21
02/13/21
DM0211/21001672
DM0212/21001706
DM0213/21001725
5.6 % 0.1
SM 2540 G (1997) MMSD
5.7 % 0.1
SM 2540 G (1997) MMSD
5.5 % 0.1
SM 2540 G (1997) MMSD
02/14/21 DM0214/21001738
5%
0.1
SM 2540 G (1997) MMSD
02/15/21 DM0215/21001793 5.1 % 0.1 SM 2540 G (1997) MMSD
Page 81 of 121
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MMSD
PARTNERS FOI A OAR Br1110111011
Solids (% Moisture)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Analytica ' e o. a.
QC Batch
ID
02/16/21
DM0216/21001841
5.3 %
0.1
SM 2540 G (1997)
MMSD
02/17/21
DM0217/21001872
6.2 % 0.1
SM 2540 G (1997) MMSD
02/18/21 DM0218/21001975
5.9 % 0.1
SM 2540 G (1997) MMSD
02/19/21 DM0219/21001986
5.5 % 0.1
SM 2540 G (1997) MMSD
02/20/21 DM0220/21002005
4.4 % 0.1
SM 2540 G (1997) MMSD
02/21/21 DM0221/21002072 4.5 % 0.1
SM 2540 G (1997) MMSD
02/22/21 DM0222/21002230 4.9 % 0.1
SM 2540 G (1997) MMSD
02/23/21 DM0223/21002246 5.2 % 0.1
SM 2540 G (1997) MMSD
02/24/21 DM0224/21002281 5.9 % 0.1 SM 2540 G (1997) MMSD
02/25/21 DM0225/21002320 6.7 % 0.1 SM 2540 G (1997) MMSD
02/26/21 DM0226/21002386 4.8 % 0.1 SM 2540 G (1997) MMSD
02/27/21 DM0227/21002405 4 % 0.1 SM 2540 G (1997) MMSD
02/28/21 DM0228/21002478 4.6 % 0.1 SM 2540 G (1997) MMSD
03/01/21 DM0301/21002611 4.3 % 0.1 SM 2540 G (1997) MMSD
03/02/21 DM0302/21002629 4.4 % 0.1 SM 2540 G (1997) MMSD
03/03/21
03/04/21
DM0303/21002660
DM0304/21002717
4.5 % 0.1
SM 2540 G (1997) MMSD
5.2 % 0.1
SM 2540 G (1997) MMSD
03/05/21 DM0305/21002728
5%
0.1
SM 2540 G (1997) MMSD
03/06/21 DM0306/21002747 4.3 % 0.1 SM 2540 G (1997) MMSD
03/07/21 DM0307/21002858 5.4 % 0.1 SM 2540 G (1997) MMSD
03/08/21 DM0308/21003336 5.3 % 0.1 SM 2540 G (1997) MMSD
03/09/21 DM0309/21003371 4.6 % 0.1 SM 2540 G (1997) MMSD
03/10/21 DM0310/21003402 4.7 % 0.1 SM 2540 G (1997) MMSD
03/11/21 DM0311/21003456 5.4 % 0.1 SM 2540 G (1997) MMSD
03/12/21 DM0312/21003522 4.4 % 0.1 SM 2540 G (1997) MMSD
03/13/21 DM0313/21003541 4.2 % 0.1 SM 2540 G (1997) MMSD
03/14/21 DM0314/21003554 4.6 % 0.1 SM 2540 G (1997) MMSD
03/15/21 DM0315/21003747 4.3 % 0.1 SM 2540 G (1997) MMSD
03/16/21 DM0316/21003801 3.9 % 0.1 SM 2540 G (1997) MMSD
03/17/21 DM0317/21003878
5%
0.1
SM 2540 G (1997) MMSD
03/18/21 DM0318/21003894 5.3 % 0.1 SM 2540 G (1997) MMSD
03/19/21 DM0319/21003905 6.4 % 0.1 SM 2540 G (1997) MMSD
03/20/21 DM0320/21004076 4.3 % 0.1 SM 2540 G (1997) MMSD
03/21/21 DM0321/21004093 3.9 % 0.1 SM 2540 G (1997) MMSD
03/22/21 DM0322/21004120 4 % 0.1 SM 2540 G (1997) MMSD
03/23/21 DM0323/21004136 4.8 % 0.1 SM 2540 G (1997) MMSD
03/24/21 DM0324/21004167 5.4 % 0.1 SM 2540 G (1997) MMSD
03/25/21 DM0325/21004242 4.9 % 0.1 SM 2540 G (1997) MMSD
03/26/21 DM0326/21004253 5.6 % 0.1 SM 2540 G (1997) MMSD
03/27/21 DM0327/21004272 5.7 % 0.1 SM 2540 G (1997) MMSD
03/28/21 DM0328/21004285 6 % 0.1 SM 2540 G (1997) MMSD
03/29/21
03/30/21
03/31/21
DM0329/21004312
DM0330/21004388
DM0331/21004600
5.8 % 0.1
SM 2540 G (1997) MMSD
5.9 % 0.1
SM 2540 G (1997) MMSD
5.9 % 0.1
SM 2540 G (1997) MMSD
04/01/21 DM0401/21004616 5.8 % 0.1 SM 2540 G (1997) MMSD
04/02/21 DM0402/21004627 6.2 % 0.1 SM 2540 G (1997) MMSD
Page 82 of 121
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MMSD
PARTNERS FOI A OAR Br1110111011
Solids (% Moisture)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Analytica ' e o. a.
QC Batch
ID
04/03/21
DM0403/21004646
5.3
0.1
SM 2540 G (1997)
MMSD
04/04/21
DM0404/21004659
4.4 % 0.1
SM 2540 G (1997) MMSD
04/05/21 DM0405/21004742
5.5 % 0.1
SM 2540 G (1997) MMSD
04/06/21 DM0406/21004758
5.3 % 0.1
SM 2540 G (1997) MMSD
04/07/21 DM0407/21004843
5%
0.1
SM 2540 G (1997) MMSD
04/08/21 DM0408/21004861 5.4 % 0.1
SM 2540 G (1997) MMSD
04/09/21 DM0409/21004912 5.7 % 0.1
SM 2540 G (1997) MMSD
04/10/21 DM0410/21004931 5.9 % 0.1
SM 2540 G (1997) MMSD
04/11/21 DM0411/21005023 5.1 % 0.1 SM 2540 G (1997) MMSD
04/12/21 DM0412/21005052 5.1 % 0.1 SM 2540 G (1997) MMSD
04/13/21 DM0413/21005199 5.3 % 0.1 SM 2540 G (1997) MMSD
04/14/21 DM0414/21005230 5.2 % 0.1 SM 2540 G (1997) MMSD
04/15/21 DM0415/21005248 4.8 % 0.1 SM 2540 G (1997) MMSD
04/16/21 DM0416/21005259 5.7 % 0.1 SM 2540 G (1997) MMSD
04/17/21 DM0417/21005468 5.8 % 0.1 SM 2540 G (1997) MMSD
04/18/21
04/19/21
DM0418/21005481
DM0419/21005508
5.8 % 0.1
SM 2540 G (1997) MMSD
6.8 % 0.1
SM 2540 G (1997) MMSD
04/20/21 DM0420/21005839 6.7 % 0.1 SM 2540 G (1997) MMSD
04/21/21 DM0421/21005870 4.7 % 0.1 SM 2540 G (1997) MMSD
04/22/21 DM0422/21005981 4.5 % 0.1 SM 2540 G (1997) MMSD
04/23/21 DM0423/21005992 4.7 % 0.1 SM 2540 G (1997) MMSD
04/24/21 DM0424/21006057 4.8 % 0.1 SM 2540 G (1997) MMSD
04/25/21 DM0425/21006272 5.1 % 0.1 SM 2540 G (1997) MMSD
04/26/21 DM0426/21006299 4.4 % 0.1 SM 2540 G (1997) MMSD
04/27/21 DM0427/21006315 4.8 % 0.1 SM 2540 G (1997) MMSD
04/28/21 DM0428/21006346
5%
0.1
SM 2540 G (1997) MMSD
04/29/21 DM0429/21006362 4.8 % 0.1 SM 2540 G (1997) MMSD
04/30/21 DM0430/21006373 4.1 % 0.1 SM 2540 G (1997) MMSD
05/01/21 DM0501/21006429 4.7 % 0.1 SM 2540 G (1997) MMSD
05/02/21 DM0502/21006442 4.6 % 0.1 SM 2540 G (1997) MMSD
05/03/21 DM0503/21006676 5.4 % 0.1 SM 2540 G (1997) MMSD
05/04/21 DM0504/21006691 4.4 % 0.1 SM 2540 G (1997) MMSD
05/05/21 DM0505/21006722 4.3 % 0.1 SM 2540 G (1997) MMSD
05/06/21 DM0506/21006781 5.4 % 0.1 SM 2540 G (1997) MMSD
05/07/21 DM0507/21006834 3.6 % 0.1 SM 2540 G (1997) MMSD
05/08/21 DM0508/21006981 5.2 % 0.1 SM 2540 G (1997) MMSD
05/09/21 DM0509/21006994 5.5 % 0.1 SM 2540 G (1997) MMSD
05/10/21 DM0510/21007021 6.1 % 0.1 SM 2540 G (1997) MMSD
05/11/21 DM0511/21007171 5.2 % 0.1 SM 2540 G (1997) MMSD
05/12/21 DM0512/21007202 4.8 % 0.1 SM 2540 G (1997) MMSD
05/13/21 DM0513/21007217 5.4 % 0.1 SM 2540 G (1997) MMSD
05/14/21
05/15/21
05/16/21
DM0514/21007309
DM0515/21007328
DM0516/21007341
4.9 % 0.1
SM 2540 G (1997) MMSD
4.5 % 0.1
SM 2540 G (1997) MMSD
4.3 % 0.1
SM 2540 G (1997) MMSD
05/17/21 DM0517/21007382 4.3 % 0.1 SM 2540 G (1997) MMSD
05/18/21 DM0518/21007440
5%
0.1
SM 2540 G (1997) MMSD
Page 83 of 121
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MMSD
PARTNERS FOI A CLEANER LY *ONFf1N1
Solids (% Moisture)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Analytica ' e o. a.
QC Batch
ID
05/19/21
DM0519/21007895
4.5
0.1
SM 2540 G (1997)
MMSD
05/20/21
DM0520/21007969
5.8 % 0.1
SM 2540 G (1997) MMSD
05/21/21 DM0521/21007980
6 % 0.1
SM 2540 G (1997) MMSD
05/22/21 DM0522/21008072
6.6 % 0.1
SM 2540 G (1997) MMSD
05/23/21 DM0523/21008085
5.3 % 0.1
SM 2540 G (1997) MMSD
05/25/21 DM0525/21008288 4.2 % 0.1
SM 2540 G (1997) MMSD
05/26/21 DM0526/21008319 4.6 % 0.1
SM 2540 G (1997) MMSD
05/27/21 DM0527/21008484 4.4 % 0.1
SM 2540 G (1997) MMSD
05/28/21 DM0528/21008495 5.1 % 0.1 SM 2540 G (1997) MMSD
05/29/21 DM0529/21008515 5.1 % 0.1 SM 2540 G (1997) MMSD
05/30/21 DM0530/21008530
5%
0.1
SM 2540 G (1997) MMSD
06/01/21 DM0601/21008902 4.3 % 0.1 SM 2540 G (1997) MMSD
06/02/21 DM0602/21008935 4.8 % 0.1 SM 2540 G (1997) MMSD
06/03/21 DM0603/21008950 4.4 % 0.1 SM 2540 G (1997) MMSD
06/04/21 DM0604/21009184 4.3 % 0.1 SM 2540 G (1997) MMSD
06/05/21
06/06/21
DM0605/21009203
DM0606/21009287
4.8 % 0.1
SM 2540 G (1997) MMSD
4.7 % 0.1
SM 2540 G (1997) MMSD
06/07/21 DM0607/21009314 4.1 % 0.1 SM 2540 G (1997) MMSD
06/08/21 DM0608/21009334 4.6 % 0.1 SM 2540 G (1997) MMSD
06/09/21 DM0609/21009365 5.2 % 0.1 SM 2540 G (1997) MMSD
06/10/21 DM0610/21009538 5.2 % 0.1 SM 2540 G (1997) MMSD
06/11/21 DM0611/21009549 5.4 % 0.1 SM 2540 G (1997) MMSD
06/12/21 DM0612/21009568 6 % 0.1 SM 2540 G (1997) MMSD
06/13/21 DM0613/21009602 6.2 % 0.1 SM 2540 G (1997) MMSD
06/14/21 DM0614/21009629 4.7 % 0.1 SM 2540 G (1997) MMSD
06/18/21 DM0618/21009979 5.8 % 0.1 SM 2540 G (1997) MMSD
06/19/21 DM0619/21010314 4.6 % 0.1 SM 2540 G (1997) MMSD
06/20/21 DM0620/21010332 4.7 % 0.1 SM 2540 G (1997) MMSD
06/21/21 DM0621/21010359 4.9 % 0.1 SM 2540 G (1997) MMSD
06/22/21 DM0622/21010375 4.3 % 0.1 SM 2540 G (1997) MMSD
06/23/21 DM0623/21010408 4.6 % 0.1 SM 2540 G (1997) MMSD
06/24/21 DM0624/21010670 5.1 % 0.1 SM 2540 G (1997) MMSD
06/25/21 DM0625/21010681 5.6 % 0.1 SM 2540 G (1997) MMSD
06/26/21 DM0626/21010702 7.1 % 0.1 SM 2540 G (1997) MMSD
06/27/21 DM0627/21010807 6 % 0.1 SM 2540 G (1997) MMSD
06/28/21 DM0628/21010860 5.2 % 0.1 SM 2540 G (1997) MMSD
06/29/21 DM0629/21010875 4.9 % 0.1 SM 2540 G (1997) MMSD
06/30/21 DM0630/21011438 5.5 % 0.1 SM 2540 G (1997) MMSD
07/01/21 DM0701/21011453 4.8 % 0.1 SM 2540 G (1997) MMSD
07/02/21 DM0702/21011465 4.6 % 0.1 SM 2540 G (1997) MMSD
07/03/21 DM0703/21011485
5%
0.1 T9. SM 2540 G (1997) MMSD
07/04/21
07/05/21
07/06/21
DM0704/21011516
DM0705/21011572
DM0706/21011693
4.8 % 0.1
SM 2540 G (1997) MMSD
4.9 % 0.1
SM 2540 G (1997) MMSD
4.6 % 0.1
SM 2540 G (1997) MMSD
07/07/21 DM0707/21011727 4.4 % 0.1 SM 2540 G (1997) MMSD
07/08/21 DM0708/21011742 4.7 % 0.1 SM 2540 G (1997) MMSD
Page 84 of 121
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MMSD
PARTNERS FOI A CLEANER LY *0111011
Solids (% Moisture)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Analytica ' e o. a.
QC Batch
ID
07/09/21
DM0709/21011754
4.3
0.1
SM 2540 G (1997)
MMSD
07/10/21
DM0710/21012238
3.9 % 0.1
SM 2540 G (1997) MMSD
07/11/21 DM0711/21012255
3.6 % 0.1
SM 2540 G (1997) MMSD
07/12/21 DM0712/21012283
3.8 % 0.1
SM 2540 G (1997) MMSD
07/13/21 DM0713/21012298
3.7 % 0.1
SM 2540 G (1997) MMSD
07/14/21 DM0714/21012332 4.2 % 0.1
SM 2540 G (1997) MMSD
07/15/21 DM0715/21012390 4.5 % 0.1
SM 2540 G (1997) MMSD
07/16/21 DM0716/21012563 4.4 % 0.1
SM 2540 G (1997) MMSD
07/17/21 DM0717/21012583 4.9 % 0.1 SM 2540 G (1997) MMSD
07/18/21 DM0718/21012596 4.3 % 0.1 SM 2540 G (1997) MMSD
07/19/21 DM0719/21012624 4.6 % 0.1 SM 2540 G (1997) MMSD
07/20/21 DM0720/21012639 4.4 % 0.1 SM 2540 G (1997) MMSD
07/21/21 DM0721/21012760 4.8 % 0.1 SM 2540 G (1997) MMSD
07/22/21 DM0722/21012775 5.6 % 0.1 SM 2540 G (1997) MMSD
07/23/21 DM0723/21013074 5.6 % 0.1 SM 2540 G (1997) MMSD
07/24/21
07/25/21
DM0724/21013378
DM0725/21013391
5.4 % 0.1
SM 2540 G (1997) MMSD
4.8 % 0.1
SM 2540 G (1997) MMSD
07/26/21 DM0726/21013419
5%
0.1
SM 2540 G (1997) MMSD
07/27/21 DM0727/21013434 4.8 % 0.1 SM 2540 G (1997) MMSD
07/28/21 DM0728/21013470 4.2 % 0.1 SM 2540 G (1997) MMSD
07/29/21 DM0729/21013614 4.6 % 0.1 SM 2540 G (1997) MMSD
07/30/21 DM0730/21013629 3.6 % 0.1 SM 2540 G (1997) MMSD
07/31/21 DM0731/21013739
5%
0.1
SM 2540 G (1997) MMSD
08/01/21 DM0801/21013752
5%
0.1
SM 2540 G (1997) MMSD
08/02/21 DM0802/21013891 4.9 % 0.1 SM 2540 G (1997) MMSD
08/03/21 DM0803/21013906 4.1 % 0.1 SM 2540 G (1997) MMSD
08/04/21 DM0804/21013940 4 % 0.1 SM 2540 G (1997) MMSD
08/05/21 DM0805/21014673 4.1 % 0.1 SM 2540 G (1997) MMSD
08/06/21 DM0806/21014685 3.9 % 0.1 SM 2540 G (1997) MMSD
08/07/21 DM0807/21014705 4.7 % 0.1 SM 2540 G (1997) MMSD
08/08/21 DM0809/21014718 4.3 % 0.1 SM 2540 G (1997) MMSD
08/09/21 DM0809/21014746 4.2 % 0.1 SM 2540 G (1997) MMSD
08/10/21 DM0810/21014847 4.5 % 0.1 SM 2540 G (1997) MMSD
08/11/21 DM0811/21014867
5%
0.1
SM 2540 G (1997) MMSD
08/12/21 DM0812/21015285
5%
0.1
SM 2540 G (1997) MMSD
08/13/21 DM0813/21015297 4.1 % 0.1 SM 2540 G (1997) MMSD
08/14/21 DM0814/21015317 3.2 % 0.1 SM 2540 G (1997) MMSD
08/15/21 DM0815/21015330 2.5 % 0.1 SM 2540 G (1997) MMSD
08/16/21 DM0816/21015410
3%
0.1
SM 2540 G (1997) MMSD
08/17/21 DM0817/21015425 2.8 % 0.1 SM 2540 G (1997) MMSD
08/18/21 DM0818/21016031 3.1 % 0.1 SM 2540 G (1997) MMSD
08/19/21
08/20/21
08/21/21
DM0819/21016046
DM0820/21016068
DM0821/21016088
3.3 % 0.1
SM 2540 G (1997) MMSD
3.8 % 0.1
Dl.
SM 2540 G (1997) MMSD
4 % 0.1
SM 2540 G (1997) MMSD
08/22/21 DM0822/21016196 4.3 % 0.1 SM 2540 G (1997) MMSD
08/23/21 DM0823/21016224 4.2 % 0.1 SM 2540 G (1997) MMSD
Page 85 of 121
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MMSD
PARTNERS FOI A OAR Br1110111011
Solids (% Moisture)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Analytica ' e o. a.
QC Batch
ID
08/24/21
DM0824/21016239
4.7 %
0.1
SM 2540 G (1997)
MMSD
08/25/21
DM0825/21016327
4.4 % 0.1
SM 2540 G (1997) MMSD
08/26/21 DM0826/21016342
4.5 % 0.1
SM 2540 G (1997) MMSD
08/27/21 DM0827/21016407
4.8 % 0.1
SM 2540 G (1997) MMSD
08/28/21 DM0828/21016427
4.8 % 0.1
SM 2540 G (1997) MMSD
08/30/21 DM0830/21016468 3.8 % 0.1
SM 2540 G (1997) MMSD
08/31/21 DM0831/21016483 4.5 % 0.1
SM 2540 G (1997) MMSD
09/01/21 DM0901/21016598 4 % 0.1
SM 2540 G (1997) MMSD
09/02/21 DM0902/21016659 4.3 % 0.1 SM 2540 G (1997) MMSD
09/03/21 DM0903/21016671 5.3 % 0.1 SM 2540 G (1997) MMSD
09/04/21 DM0904/21017055 4.2 % 0.1 SM 2540 G (1997) MMSD
09/05/21 DM0905/21017068 4.7 % 0.1 SM 2540 G (1997) MMSD
09/06/21 DM0906/21017096 4.2 % 0.1 SM 2540 G (1997) MMSD
09/07/21 DM0907/21017306 4.4 % 0.1 SM 2540 G (1997) MMSD
09/08/21 DM0908/21017338 4.8 % 0.1 SM 2540 G (1997) MMSD
09/09/21
09/10/21
DM0909/21017408
DM0910/21017420
4.8 % 0.1
SM 2540 G (1997) MMSD
4.8 % 0.1
SM 2540 G (1997) MMSD
09/11/21 DM0911/21017699 4.2 % 0.1 SM 2540 G (1997) MMSD
09/12/21 DM0912/21017712 5.1 % 0.1 SM 2540 G (1997) MMSD 149896-1
09/13/21 DM0913/21017740 4.8 % 0.1 SM 2540 G (1997) MMSD 149920-1
09/14/21 DM0914/21017755 4.6 % 0.1 SM 2540 G (1997) MMSD 149947-1
09/15/21 DM0915/21017903 4.7 % 0.1 SM 2540 G (1997) MMSD 149977-1
09/16/21 DM0916/21018023 5.1 % 0.1 SM 2540 G (1997) MMSD 150004-1
09/17/21 DM0917/21018105 5.4 % 0.1 SM 2540 G (1997) MMSD 150018-1
09/18/21 DM0918/21018125 5.2 % 0.1 SM 2540 G (1997) MMSD 150021-1
09/19/21 DM0919/21018138 5.7 % 0.1 SM 2540 G (1997) MMSD 150039-1
09/20/21 DM0920/21018236 6.3 % 0.1 SM 2540 G (1997) MMSD 150063-1
09/21/21 DM0921/21018251 4.9 % 0.1 SM 2540 G (1997) MMSD 150084-1
09/22/21 DM0922/21018480 4.7 % 0.1 SM 2540 G (1997) MMSD 150117-1
09/23/21 DM0923/21018564 4.2 % 0.1 SM 2540 G (1997) MMSD 150139-1
09/24/21 DM0924/21018818 3.8 % 0.1 SM 2540 G (1997) MMSD 150152-1
09/25/21 DM0925/21018838 3.1 % 0.1 SM 2540 G (1997) MMSD 150156-1
09/26/21 DM0926/21019023 4 % 0.1 SM 2540 G (1997) MMSD 150169-1
09/27/21 DM0927/21019051 3.6 % 0.1 SM 2540 G (1997) MMSD 150190-1
09/28/21 DM0928/21019066 4.4 % 0.1 SM 2540 G (1997) MMSD 150208-1
09/29/21 DM0929/21019228 4 % 0.1 SM 2540 G (1997) MMSD 150224-1
09/30/21 DM0930/21019243 3.7 % 0.1 SM 2540 G (1997) MMSD 150254-1
10/01/21 DM1001/21019255 4.2 % 0.1 SM 2540 G (1997) MMSD 150269-1
10/02/21 DM1002/21019384 3.9 % 0.1 SM 2540 G (1997) MMSD 150272-1
10/03/21 DM1003/21019397 4.3 % 0.1 SM 2540 G (1997) MMSD 150294-1
10/04/21 DM1004/21019425 4.8 % 0.1 SM 2540 G (1997) MMSD 150320-1
10/06/21
10/07/21
10/08/21
DM 1006/21019735
DM 1007/21019760
DM 1008/21019772
4.4 % 0.1
SM 2540 G (1997) MMSD 150369-1
4 % 0.1
SM 2540 G (1997) MMSD 150391-1
3.4 % 0.1
SM 2540 G (1997) MMSD 150419-1
10/19/21 DM1019/21020600 2.6 % 0.1 SM 2540 G (1997) MMSD 150592-1
10/20/21 DM1020/21020674 4.5 % 0.1 SM 2540 G (1997) MMSD 150617-1
Page 86 of 121
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MMSD
PARTNERS FOI A OAR Br1110111011
Solids (% Moisture)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Analytica ' e o. a.
QC Batch
ID
10/21/21
DM 1021 /21020689
4.2 %
0.1
SM 2540 G (1997)
MMSD
150638-1
10/22/21
DM 1022/21020701
3.9 % 0.1
SM 2540 G (1997) MMSD 150659-1
10/23/21 DM1023/21020883
3.3 % 0.1
SM 2540 G (1997) MMSD 150663-1
10/24/21 DM1024/21021034
4.3 % 0.1
SM 2540 G (1997) MMSD 150673-1
10/25/21 DM1025/21021062
4 % 0.1
SM 2540 G (1997) MMSD 150694-1
10/26/21 DM1026/21021077 3.8 % 0.1
SM 2540 G (1997) MMSD 150716-1
10/27/21 DM1027/21021161 4.7 % 0.1
SM 2540 G (1997) MMSD 150745-1
10/28/21 DM1028/21021226 4.4 % 0.1
SM 2540 G (1997) MMSD 150773-1
10/29/21 DM1029/21021510 4.6 % 0.1 SM 2540 G (1997) MMSD 150780-1
10/30/21 DM1030/21021530 5.1 % 0.1 SM 2540 G (1997) MMSD 150784-1
10/31/21 DM1031/21021574 5.9 % 0.1 SM 2540 G (1997) MMSD 150796-1
11/01/21 DM1101/21021608 6 % 0.1 SM 2540 G (1997) MMSD 150815-1
11/02/21 DM1102/21021623 5.8 % 0.1 SM 2540 G (1997) MMSD 150838-1
11/03/21 DM1103/21021720 4.7 % 0.1 SM 2540 G (1997) MMSD 150856-1
11/04/21 DM1104/21021735 4.1 % 0.1 SM 2540 G (1997) MMSD 150870-1
11/05/21
11/06/21
DM1105/21021747
DM1106/21021767
3.6 % 0.1
SM 2540 G (1997) MMSD 150888-1
4.4 % 0.1
SM 2540 G (1997) MMSD 150891-1
11/07/21 DM1107/21022553 5.4 % 0.1 SM 2540 G (1997) MMSD 150902-1
11/08/21 DM1108/21022581 5.4 % 0.1 SM 2540 G (1997) MMSD 150923-1
11/09/21 DM1109/21022596 5.4 % 0.1 SM 2540 G (1997) MMSD 150940-1
11/10/21 DM1110/21022680 6.4 % 0.1 SM 2540 G (1997) MMSD 150969-1
11/11/21 DM1111/21022695 6.1 % 0.1 SM 2540 G (1997) MMSD 150977-1
11/12/21 DM1112/21022707 6.2 % 0.1 SM 2540 G (1997) MMSD 150989-1
11/13/21 DM1113/21022731
5%
0.1
SM 2540 G (1997) MMSD 150992-1
11/14/21 DM1114/21022744 6.4 % 0.1 SM 2540 G (1997) MMSD 151002-1
11/15/21 DM1115/21022772 5.6 % 0.1 SM 2540 G (1997) MMSD 151022-1
11/16/21 DM1116/21022787 4.7 % 0.1 SM 2540 G (1997) MMSD 151055-1
11/17/21 DM1117/21023039 4.9 % 0.1 SM 2540 G (1997) MMSD 151076-1
11/18/21 DM1118/21023056 4.7 % 0.1 SM 2540 G (1997) MMSD 151100-1
11/19/21 DM1119/21023181 5.2 % 0.1 SM 2540 G (1997) MMSD 151125-1
11/20/21 DM1120/21023201 5.8 % 0.1 SM 2540 G (1997) MMSD 151128-1
11/21/21 DM1121/21023214 6.5 % 0.1 SM 2540 G (1997) MMSD 151138-1
11/22/21 DM1122/21023555 7.2 % 0.1 SM 2540 G (1997) MMSD 151157-1
11/23/21 DM1123/21023570 5.7 % 0.1 SM 2540 G (1997) MMSD 151179-1
11/24/21 DM1124/21023611 5.3 % 0.1 SM 2540 G (1997) MMSD 151203-1
11/25/21 DM1125/21023795 6 % 0.1 SM 2540 G (1997) MMSD 151207-1
11/26/21 DM1126/21023807 6.4 % 0.1 SM 2540 G (1997) MMSD 151211-1
11/27/21 DM1127/21023827 7.3 % 0.1 SM 2540 G (1997) MMSD 151215-1
11/28/21 DM1128/21023899 5.7 % 0.1 SM 2540 G (1997) MMSD 151230-1
11/29/21 DM1129/21023927 4.4 % 0.1 SM 2540 G (1997) MMSD 151260-1
11/30/21 DM1130/21024167 4.5 % 0.1 SM 2540 G (1997) MMSD 151277-1
12/01/21
12/02/21
12/03/21
DM 1201 /21024282
DM 1202/21024297
DM1203/21024309
4.1 % 0.1
SM 2540 G (1997) MMSD 151301-1
4.7 % 0.1
SM 2540 G (1997) MMSD 151324-1
4.7 % 0.1
SM 2540 G (1997) MMSD 151349-1
12/04/21 DM1204/21024329 5.9 % 0.1 SM 2540 G (1997) MMSD 151354-1
12/05/21 DM1205/21024739 6.5 % 0.1 SM 2540 G (1997) MMSD 151365-1
Page 87 of 121
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MMSD
PARTNERS FOI II CLIMB Br1110111Allft
Solids (% Moisture)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Analytica ' e o. a.
QC Batch
ID
12/06/21
DM1206/21024767
6.3 %
0.1
SM 2540 G (1997)
MMSD
151383-1
12/07/21
DM 1207/21024782
6.5 % 0.1
SM 2540 G (1997) MMSD 151405-1
12/08/21 DM1208/21024816
6.6 % 0.1
SM 2540 G (1997) MMSD 151439-1
12/09/21 DM 1209/21024832
6.9 % 0.1
SM 2540 G (1997) MMSD 151455-1
12/10/21 DM1210/21024844
7.4 % 0.1
SM 2540 G (1997) MMSD 151474-1
12/11/21 DM1211/21024864 4.6 % 0.1
SM 2540 G (1997) MMSD 151477-1
12/12/21 DM1212/21025174 3.8 % 0.1
SM 2540 G (1997) MMSD 151485-1
12/13/21 DM 1213/21025205 6.3 % 0.1
SM 2540 G (1997) MMSD 151511-1
12/14/21 DM1214/21025220
5%
0.1
SM 2540 G (1997) MMSD 151536-1
12/15/21 DM1215/21025299 5.7 % 0.1 SM 2540 G (1997) MMSD 151564-1
12/16/21 DM1216/21025314 5.1 % 0.1 SM 2540 G (1997) MMSD 151581-1
12/17/21 DM1217/21025326 6.1 % 0.1 SM 2540 G (1997) MMSD 151588-1
12/18/21 DM1219/21025346 5.9 % 0.1 SM 2540 G (1997) MMSD 151591-1
12/19/21 DM1219/21025621 6.8 % 0.1 SM 2540 G (1997) MMSD 151597-1
12/20/21 DM1220/21025649 6.6 % 0.1 SM 2540 G (1997) MMSD 151628-1
12/21/21
12/22/21
DM 1221 /21025664
DM1222/21025700
6.7 % 0.1
SM 2540 G (1997) MMSD 151655-1
6.4 % 0.1
SM 2540 G (1997) MMSD 151675-1
12/23/21 DM1223/21025779
7%
0.1
SM 2540 G (1997) MMSD 151688-1
12/24/21 DM1224/21025791 7.5 % 0.1 SM 2540 G (1997) MMSD 151691-1
12/25/21 DM1225/21025811 6.2 % 0.1 SM 2540 G (1997) MMSD 151693-1
12/26/21 DM 1226/21025824
7%
0.1
SM 2540 G (1997) MMSD 151698-1
12/27/21 DM1227/21025917 5.3 % 0.1 SM 2540 G (1997) MMSD 151706-1
12/28/21 DM1228/21025932 5.8 % 0.1 SM 2540 G (1997) MMSD 151727-1
12/29/21 DM1229/21025966 6.2 % 0.1 SM 2540 G (1997) MMSD 151747-1
12/30/21 DM1230/21025981 5.9 % 0.1 SM 2540 G (1997) MMSD 151755-1
12/31/21 DM1231/21026033 5.8 % 0.1 SM 2540 G (1997) MMSD 151758-1
Avg Result: 5 % Min LOD: 0.1 %
Max Result: 7.5 % Max LOD: 0.1 %
Page 88 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
ZINC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
320 mg/kg D.W.
4.8
15
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
330 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD
01/03/21 DM0103/21000076
310 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
01/04/21 DM0104/21000488 320 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
01/05/21 DM0105/21000504 330 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
01/06/21 DM0106/21000535 320 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
01/07/21 DM0107/21000551 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/08/21 DM0108/21000562 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/09/21 DM0109/21000581 340 mg/kg D.W. 4.9 15 SW846: 6010C MMSD
01/10/21 DM0110/21000594 320 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/11/21 DM0111/21000632 320 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/12/21 DM0112/21000648 320 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/13/21 DM0113/21000679 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/14/21 DM0114/21000754 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
01/15/21 DM0115/21000765 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/16/21 DM0116/21000784 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/17/21 DM0117/21000797 350 mg/kg D.W. 4.8 15 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/19/21 DM0119/21000842 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/20/21 DM0120/21000926 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/21/21 DM0121/21000942 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/22/21 DM0122/21000953 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/23/21 DM0123/21000972 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/24/21 DM0124/21001059 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/25/21 DM0125/21001088 310 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/26/21 DM0126/21001106 310 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
01/27/21 DM0127/21001137 310 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
01/28/21 DM0128/21001153 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
01/29/21 DM0129/21001164 350 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
01/30/21 DM0130/21001304 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
01/31/21 DM0131/21001317 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/01/21 DM0201/21001344 340 mg/kg D.W. 4.8 15 D2, Q3. SW846: 6010C MMSD
02/02/21 DM0202/21001397 370 mg/kg D.W. 4.8 15 Q3. SW846: 6010C MMSD
02/03/21 DM0203/21001428 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/04/21 DM0204/21001444 380 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/05/21 DM0205/21001455 370 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/06/21 DM0206/21001476 370 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/07/21 DM0207/21001489 370 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
02/08/21 DM0208/21001609 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/09/21 DM0209/21001625 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/10/21 DM0210/21001656 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/11/21 DM0211/21001672 330 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
02/12/21 DM0212/21001706 330 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
02/13/21 DM0213/21001725 350 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
02/14/21 DM0214/21001738 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/15/21 DM0215/21001793 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
Page 89 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
ZINC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
330 mg/kg D.W.
4.8
15
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
320 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
320 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
02/19/21 DM0219/21001986 320 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
02/20/21 DM0220/21002005 310 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
02/21/21 DM0221/21002072 310 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
02/22/21 DM0222/21002230 320 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/23/21 DM0223/21002246 320 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/24/21 DM0224/21002281 310 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/25/21 DM0225/21002320 320 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
02/26/21 DM0226/21002386 330 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
02/27/21 DM0227/21002405 350 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
02/28/21 DM0228/21002478 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/01/21 DM0301/21002611 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/02/21 DM0302/21002629 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/03/21 DM0303/21002660 350 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
03/04/21 DM0304/21002717 360 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
03/05/21 DM0305/21002728 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/06/21 DM0306/21002747 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/07/21 DM0307/21002858 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/08/21 DM0308/21003336 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/09/21 DM0309/21003371 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/10/21 DM0310/21003402 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/11/21 DM0311/21003456 400 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/12/21 DM0312/21003522 370 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/13/21 DM0313/21003541 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/14/21 DM0314/21003554 310 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/15/21 DM0315/21003747 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/16/21 DM0316/21003801 370 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
03/17/21 DM0317/21003878 380 mg/kg D.W. 4.7 15 Q3. SW846: 6010C MMSD
03/18/21 DM0318/21003894 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/19/21 DM0319/21003905 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/20/21 DM0320/21004076 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/21/21 DM0321/21004093 350 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
03/22/21 DM0322/21004120 350 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
03/23/21 DM0323/21004136 330 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/24/21 DM0324/21004167 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/25/21 DM0325/21004242 330 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
03/26/21 DM0326/21004253 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/27/21 DM0327/21004272 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/28/21 DM0328/21004285 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
03/29/21 DM0329/21004312 320 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
03/30/21 DM0330/21004388 310 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
03/31/21 DM0331/21004600 300 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
04/01/21 DM0401/21004616 310 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/02/21 DM0402/21004627 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
Page 90 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOWN
ZINC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
370 mg/kg D.W.
4.8
15
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
340 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
350 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
04/06/21 DM0406/21004758 360 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
04/07/21 DM0407/21004843 370 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
04/08/21 DM0408/21004861 340 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
04/09/21 DM0409/21004912 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/10/21 DM0410/21004931 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/11/21 DM0411/21005023 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/12/21 DM0412/21005052 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/13/21 DM0413/21005199 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/14/21 DM0414/21005230 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/15/21 DM0415/21005248 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/16/21 DM0416/21005259 340 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/17/21 DM0417/21005468 330 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/18/21 DM0418/21005481 340 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
04/19/21 DM0419/21005508 340 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
04/20/21 DM0420/21005839 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
04/21/21 DM0421/21005870 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/22/21 DM0422/21005981 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/23/21 DM0423/21005992 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/24/21 DM0424/21006057 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/25/21 DM0425/21006272 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/26/21 DM0426/21006299 330 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/27/21 DM0427/21006315 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/28/21 DM0428/21006346 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/29/21 DM0429/21006362 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
04/30/21 DM0430/21006373 330 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
05/01/21 DM0501/21006429 320 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/02/21 DM0502/21006442 320 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/03/21 DM0503/21006676 320 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
05/04/21 DM0504/21006691 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/05/21 DM0505/21006722 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/06/21 DM0506/21006781 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
05/07/21 DM0507/21006834 380 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
05/08/21 DM0508/21006981 370 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/09/21 DM0509/21006994 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
05/10/21 DM0510/21007021 350 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
05/11/21 DM0511/21007171 340 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/12/21 DM0512/21007202 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/13/21 DM0513/21007217 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
05/14/21 DM0514/21007309 360 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
05/15/21 DM0515/21007328 360 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
05/16/21 DM0516/21007341 370 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
05/17/21 DM0517/21007382 370 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/18/21 DM0518/21007440 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
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MMSD
PARTNERS F41 A CLEAA#M MOM
ZINC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
370 mg/kg D.W.
4.7
15
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
360 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD
05/21/21 DM0521/21007980
370 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
05/22/21 DM0522/21008072 360 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
05/23/21 DM0523/21008085 360 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
05/25/21 DM0525/21008288 380 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
05/26/21 DM0526/21008319 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/27/21 DM0527/21008484 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/28/21 DM0528/21008495 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/29/21 DM0529/21008515 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
05/30/21 DM0530/21008530 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/01/21 DM0601/21008902 390 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/02/21 DM0602/21008935 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/03/21 DM0603/21008950 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/04/21 DM0604/21009184 390 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/05/21 DM0605/21009203 360 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
06/06/21 DM0606/21009287 390 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
06/07/21 DM0607/21009314 450 mg/kg D.W. 4.7 14 Q3. SW846: 6010C MMSD
06/08/21 DM0608/21009334 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/09/21 DM0609/21009365 360 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/10/21 DM0610/21009538 350 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/11/21 DM0611/21009549 390 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/12/21 DM0612/21009568 390 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/13/21 DM0613/21009602 400 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/14/21 DM0614/21009629 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/18/21 DM0618/21009979 360 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/19/21 DM0619/21010314 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/20/21 DM0620/21010332 370 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/21/21 DM0621/21010359 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/22/21 DM0622/21010375 380 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/23/21 DM0623/21010408 410 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/24/21 DM0624/21010670 390 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/25/21 DM0625/21010681 400 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/26/21 DM0626/21010702 400 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/27/21 DM0627/21010807 400 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
06/28/21 DM0628/21010860 400 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/29/21 DM0629/21010875 420 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
06/30/21 DM0630/21011438 390 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
07/01/21 DM0701/21011453 420 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/02/21 DM0702/21011465 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/03/21 DM0703/21011485 450 mg/kg D.W. 4.7 15 T9. SW846: 6010C MMSD
07/04/21 DM0704/21011516 440 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
07/05/21 DM0705/21011572 450 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
07/06/21 DM0706/21011693 460 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
07/07/21 DM0707/21011727 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/08/21 DM0708/21011742 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
Page 92 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
ZINC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
460 mg/kg D.W.
4.7
15
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
450 mg/kg D.W. 4.7 14
SW846: 6010C
MMSD
07/11/21 DM0711/21012255
460 mg/kg D.W. 4.7 14
SW846: 6010C MMSD
07/12/21 DM0712/21012283 450 mg/kg D.W. 4.7 14
SW846: 6010C MMSD
07/13/21 DM0713/21012298 470 mg/kg D.W. 4.7 14
SW846: 6010C MMSD
07/14/21 DM0714/21012332 440 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
07/15/21 DM0715/21012390 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/16/21 DM0716/21012563 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/17/21 DM0717/21012583 450 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/18/21 DM0718/21012596 450 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/19/21 DM0719/21012624 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/20/21 DM0720/21012639 480 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/21/21 DM0721/21012760 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/22/21 DM0722/21012775 450 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
07/23/21 DM0723/21013074 410 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
07/24/21 DM0724/21013378 410 mg/kg D.W. 4.8 15
SW846: 6010C MMSD
07/25/21 DM0725/21013391 420 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
07/26/21 DM0726/21013419 440 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/27/21 DM0727/21013434 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/28/21 DM0728/21013470 450 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/29/21 DM0729/21013614 450 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
07/30/21 DM0730/21013629 460 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
07/31/21 DM0731/21013739 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/01/21 DM0801/21013752 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/02/21 DM0802/21013891 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/03/21 DM0803/21013906 520 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/04/21 DM0804/21013940 520 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
08/05/21 DM0805/21014673 520 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
08/06/21 DM0806/21014685 530 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
08/07/21 DM0807/21014705 520 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/08/21 DM0809/21014718 530 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/09/21 DM0809/21014746 560 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/10/21 DM0810/21014847 600 mg/kg D.W. 4.7 15 D2, Q2. SW846: 6010C MMSD
08/11/21 DM0811/21014867 570 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/12/21 DM0812/21015285 560 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/13/21 DM0813/21015297 560 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
08/14/21 DM0814/21015317 540 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
08/15/21 DM0815/21015330 490 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
08/16/21 DM0816/21015410 480 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
08/17/21 DM0817/21015425 540 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
08/18/21 DM0818/21016031 500 mg/kg D.W. 4.6 14 SW846: 6010C MMSD
08/19/21 DM0819/21016046 480 mg/kg D.W. 4.6 14
SW846: 6010C MMSD
08/20/21 DM0820/21016068 500 mg/kg D.W. 4.7 14
SW846: 6010C MMSD
08/21/21 DM0821/21016088 520 mg/kg D.W. 4.7 14
SW846: 6010C MMSD
08/22/21 DM0822/21016196 530 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
08/23/21 DM0823/21016224 560 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
Page 93 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
ZINC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
560 mg/kg D.W.
4.7
15
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
540 mg/kg D.W. 4.7 15
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
500 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
08/27/21 DM0827/21016407 490 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
08/28/21 DM0828/21016427 500 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
08/30/21 DM0830/21016468 530 mg/kg D.W. 4.7 14
SW846: 6010C MMSD
08/31/21 DM0831/21016483 550 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/01/21 DM0901/21016598 560 mg/kg D.W. 4.7 14 SW846: 6010C MMSD
09/02/21 DM0902/21016659 540 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/03/21 DM0903/21016671 570 mg/kg D.W. 4.8 15 SW846: 6010C MMSD
09/04/21 DM0904/21017055 590 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/05/21 DM0905/21017068 560 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/06/21 DM0906/21017096 570 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/07/21 DM0907/21017306 560 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/08/21 DM0908/21017338 520 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/09/21 DM0909/21017408 510 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
09/10/21 DM0910/21017420 490 mg/kg D.W. 4.7 15
SW846: 6010C MMSD
09/11/21 DM0911/21017699 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/12/21 DM0912/21017712 480 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/13/21 DM0913/21017740 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/14/21 DM0914/21017755 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 149990-1
09/15/21 DM0915/21017903 480 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 149990-1
09/16/21 DM0916/21018023 510 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150012-1
09/17/21 DM0917/21018105 520 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150074-1
09/18/21 DM0918/21018125 530 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150074-1
09/19/21 DM0919/21018138 500 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150074-1
09/20/21 DM0920/21018236 500 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150123-1
09/21/21 DM0921/21018251 540 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150123-1
09/22/21 DM0922/21018480 500 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/23/21 DM0923/21018564 500 mg/kg D.W. 4.7 15 SW846: 6010C MMSD
09/24/21 DM0924/21018818 520 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150235-1
09/25/21 DM0925/21018838 490 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 150235-1
09/26/21 DM0926/21019023 480 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150235-1
09/27/21 DM0927/21019051 470 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150235-2
09/28/21 DM0928/21019066 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150235-3
09/29/21 DM0929/21019228 460 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150305-1
09/30/21 DM0930/21019243 470 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150305-1
10/01/21 DM1001/21019255 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150305-1
10/02/21 DM1002/21019384 480 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 150305-1
10/03/21 DM1003/21019397 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150305-1
10/04/21 DM1004/21019425 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150376-1
10/06/21 DM1006/21019735 490 mg/kg D.W. 4.7 15
SW846: 6010C MMSD 150431-1
10/07/21 DM1007/21019760 490 mg/kg D.W. 4.7 14
SW846: 6010C MMSD 150431-1
10/08/21 DM1008/21019772 470 mg/kg D.W. 4.6 14
SW846: 6010C MMSD 150445-1
10/19/21 DM1019/21020600 500 mg/kg D.W. 4.6 14 SW846: 6010C MMSD 150655-1
10/20/21 DM1020/21020674 880 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150655-1
Page 94of121
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MMSD
PARTNERS F41 A CLEAA#M MOM
ZINC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
10/21/21
DM 1021 /21020689
510 mg/kg D.W.
4.7
15
SW846: 6010C
MMSD
150655-1
10/22/21
DM1022/21020701
510 mg/kg D.W. 4.7 14
SW846: 6010C
MMSD 150703-1
10/23/21 DM1023/21020883
490 mg/kg D.W. 4.6 14
SW846: 6010C MMSD 150703-1
10/24/21 DM1024/21021034 470 mg/kg D.W. 4.7 15
SW846: 6010C MMSD 150703-1
10/25/21 DM1025/21021062 490 mg/kg D.W. 4.7 14
SW846: 6010C MMSD 150703-1
10/26/21 DM1026/21021077 480 mg/kg D.W. 4.7 14
SW846: 6010C MMSD 150756-1
10/27/21 DM1027/21021161 480 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150756-1
10/28/21 DM1028/21021226 480 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150831-1
10/29/21 DM1029/21021510 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150831-1
10/30/21 DM1030/21021530 480 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150831-1
10/31/21 DM1031/21021574 480 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150831-1
11/01/21 DM1101/21021608 460 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150831-1
11/02/21 DM1102/21021623 490 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150884-1
11/03/21 DM1103/21021720 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150884-1
11/04/21 DM1104/21021735 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 150884-1
11/05/21 DM1105/21021747 470 mg/kg D.W. 4.7 14
SW846: 6010C MMSD 150964-1
11/06/21 DM1106/21021767 500 mg/kg D.W. 4.7 15
SW846: 6010C MMSD 150964-1
11/07/21 DM1107/21022553 490 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150964-1
11/08/21 DM1108/21022581 480 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150964-1
11/09/21 DM1109/21022596 490 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 150964-2
11/10/21 DM1110/21022680 460 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151039-2
11/11/21 DM1111/21022695 450 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151039-2
11/12/21 DM1112/21022707 470 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151039-3
11/13/21 DM1113/21022731 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 151039-1
11/14/21 DM1114/21022744 460 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151039-3
11/15/21 DM1115/21022772 440 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151085-1
11/16/21 DM1116/21022787 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 151085-1
11/17/21 DM1117/21023039 480 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 151122-1
11/18/21 DM1118/21023056 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 151122-1
11/19/21 DM1119/21023181 450 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 151175-1
11/20/21 DM1120/21023201 480 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151175-1
11/21/21 DM1121/21023214 440 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151175-1
11/22/21 DM1122/21023555 450 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151175-1
11/23/21 DM1123/21023570 440 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151252-1
11/24/21 DM1124/21023611 460 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151266-1
11/25/21 DM1125/21023795 470 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151266-1
11/26/21 DM1126/21023807 430 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151266-1
11/27/21 DM1127/21023827 460 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151266-1
11/28/21 DM1128/21023899 470 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151266-1
11/29/21 DM1129/21023927 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 151294-1
11/30/21 DM1130/21024167 490 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 151317-1
12/01/21 DM1201/21024282 490 mg/kg D.W. 4.7 15
SW846: 6010C MMSD 151317-2
12/02/21 DM1202/21024297 480 mg/kg D.W. 4.7 15
SW846: 6010C MMSD 151342-1
12/03/21 DM1203/21024309 480 mg/kg D.W. 4.7 15
SW846: 6010C MMSD 151371-1
12/04/21 DM1204/21024329 430 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151371-1
12/05/21 DM1205/21024739 450 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151371-1
Page 95 of 121
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MMSD
PARTNERS F41 A CLEAA#M MOM
ZINC ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID Result LOD LOQ QA Flags Ana Ica ' e •
a.
QC Batch
ID
12/06/21
DM1206/21024767
470 mg/kg D.W.
4.8
15
SW846: 6010C
MMSD
151391-1
12/07/21
DM 1207/21024782
430 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151422-1
12/08/21 DM 1208/21024816
450 mg/kg D.W. 4.8 15
SW846: 6010C
MMSD 151471-1
12/09/21 DM1209/21024832 440 mg/kg D.W. 4.8 15
SW846: 6010C MMSD 151471-2
12/10/21 DM1210/21024844 480 mg/kg D.W. 4.8 15
SW846: 6010C MMSD 151498-1
12/11/21 DM1211/21024864 460 mg/kg D.W. 4.7 15
SW846: 6010C MMSD 151498-1
12/12/21 DM1212/21025174 470 mg/kg D.W. 4.7 14 SW846: 6010C MMSD 151498-1
12/13/21 DM1213/21025205 450 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151543-1
12/14/21 DM1214/21025220 470 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 151576-1
12/15/21 DM1215/21025299 460 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151576-1
12/16/21 DM1216/21025314 460 mg/kg D.W. 4.7 15 SW846: 6010C MMSD 151645-1
12/17/21 DM1217/21025326 460 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151645-1
12/18/21 DM1219/21025346 450 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151645-1
12/19/21 DM1219/21025621 440 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151645-1
12/20/21 DM1220/21025649 440 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151645-2
12/21/21 DM1221/21025664 440 mg/kg D.W. 4.8 15
SW846: 6010C MMSD 151668-1
12/22/21 DM1222/21025700 460 mg/kg D.W. 4.8 15
SW846: 6010C MMSD 151750-1
12/23/21 DM1223/21025779 460 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151750-2
12/24/21 DM1224/21025791 460 mg/kg D.W. 4.9 15 SW846: 6010C MMSD 151750-2
12/25/21 DM1225/21025811 450 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151750-2
12/26/21 DM1226/21025824 450 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151750-2
12/27/21 DM1227/21025917 470 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151750-2
12/28/21 DM1228/21025932 460 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151750-2
12/29/21 DM1229/21025966 480 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151827-1
12/30/21 DM1230/21025981 480 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151827-1
12/31/21 DM1231/21026033 470 mg/kg D.W. 4.8 15 SW846: 6010C MMSD 151827-1
Avg Result: 420 mg/kg D.W. Min LOD: 4.6 mg/kg D.W.
Max Result: 880 mg/kg D.W. Max LOD: 4.9 mg/kg D.W.
Page 96 of 121
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MMSD
PARTNERS F(t A CLEANER LY *OMlf{Ml
Phosphorus - Total % DW (Calc.)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
01/01/21
DM0101/21000012
2.8 % D.W.
0.1
0.1
AO.
SW846: 6010C
MMSD
01/02/21
DM0102/21000031
2.9%D.W. 0.1 0.1 AO.
SW846: 6010C
MMSD
01/03/21
DM0103/21000076
2.7%D.W. 0.1 0.1 AO.
SW846: 6010C MMSD
01/04/21
DM0104/21000488
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
01/05/21 DM0105/21000504 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/06/21 DM0106/21000535 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/07/21 DM0107/21000551 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/08/21 DM0108/21000562 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/09/21 DM0109/21000581 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/10/21 DM0110/21000594 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/11/21 DM0111/21000632 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/12/21 DM0112/21000648 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/13/21 DM0113/21000679 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/14/21
DM0114/21000754
2.8 % D.W. 0.1 0.1 AO. SW846: 6010C MMSD
01/15/21 DM0115/21000765 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/16/21 DM0116/21000784 2.7 % D.W. 0.1 0.1 SW846: 6010C MMSD
01/17/21 DM0117/21000797 2.7 % D.W. 0.1 0.1 Q3. SW846: 6010C MMSD
01/18/21 DM0118/21000824 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/19/21 DM0119/21000842 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/20/21 DM0120/21000926 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/21/21 DM0121/21000942 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/22/21 DM0122/21000953 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/23/21 DM0123/21000972 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/24/21 DM0124/21001059 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/25/21 DM0125/21001088 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/26/21 DM0126/21001106 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/27/21 DM0127/21001137 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/28/21 DM0128/21001153 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/29/21 DM0129/21001164 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/30/21 DM0130/21001304 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
01/31/21 DM0131/21001317 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/01/21
DM0201/21001344
2.6 % D.W. 0.1 0.1 D2, Q3.
SW846: 6010C MMSD
02/02/21 DM0202/21001397 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/03/21 DM0203/21001428 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/04/21 DM0204/21001444 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/05/21 DM0205/21001455 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/06/21 DM0206/21001476 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/07/21 DM0207/21001489 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/08/21 DM0208/21001609 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/09/21 DM0209/21001625 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/10/21 DM0210/21001656 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/11/21
02/12/21
02/13/21
DM0211/21001672
DM0212/21001706
DM0213/21001725
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/14/21 DM0214/21001738 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
02/15/21 DM0215/21001793 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
Page 97 of 121
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MMSD
WARS RS F4t A (WAR pmt011101
Phosphorus - Total % DW (Calc.)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
02/16/21
DM0216/21001841
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
02/17/21
DM0217/21001872
2.5 % D.W.
0.1 0.1
SW846: 6010C
MMSD
02/18/21 DM0218/21001975
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/19/21 DM0219/21001986
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/20/21 DM0220/21002005
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
02/21/21 DM0221/21002072
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/22/21 DM0222/21002230
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
02/23/21 DM0223/21002246
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/24/21 DM0224/21002281
2.3 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/25/21 DM0225/21002320
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
02/26/21 DM0226/21002386
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/27/21 DM0227/21002405
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
02/28/21 DM0228/21002478
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/01/21 DM0301/21002611
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
03/02/21 DM0302/21002629
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/03/21
03/04/21
DM0303/21002660
DM0304/21002717
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/05/21 DM0305/21002728
2.3 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/06/21 DM0306/21002747
2.3 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/07/21 DM0307/21002858
2.3 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/08/21 DM0308/21003336
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/09/21 DM0309/21003371
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/10/21 DM0310/21003402
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/11/21 DM0311/21003456
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/12/21 DM0312/21003522
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/13/21 DM0313/21003541
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/14/21 DM0314/21003554
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
03/15/21 DM0315/21003747
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/16/21 DM0316/21003801
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/17/21 DM0317/21003878
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/18/21 DM0318/21003894
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/19/21 DM0319/21003905
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/20/21 DM0320/21004076
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/21/21 DM0321/21004093
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/22/21 DM0322/21004120
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/23/21 DM0323/21004136
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/24/21 DM0324/21004167
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/25/21 DM0325/21004242
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/26/21 DM0326/21004253
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/27/21 DM0327/21004272
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/28/21 DM0328/21004285
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
03/29/21
03/30/21
03/31/21
DM0329/21004312
DM0330/21004388
DM0331/21004600
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
04/01/21 DM0401/21004616
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/02/21 DM0402/21004627
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
Page 98 of 121
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MMSD
WARS RS F4t A (WAR pmt011101
Phosphorus - Total % DW (Calc.)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
04/03/21
DM0403/21004646
2.3 % D.W.
0.1
0.1
SW846: 6010C
MMSD
04/04/21
DM0404/21004659
2.3 % D.W.
0.1 0.1
SW846: 6010C
MMSD
04/05/21 DM0405/21004742
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
04/06/21 DM0406/21004758
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/07/21 DM0407/21004843
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/08/21 DM0408/21004861
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/09/21 DM0409/21004912
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/10/21 DM0410/21004931
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/11/21 DM0411/21005023
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/12/21 DM0412/21005052
2.2 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/13/21 DM0413/21005199
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/14/21 DM0414/21005230
2.3 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/15/21 DM0415/21005248
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
04/16/21 DM0416/21005259
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
04/17/21 DM0417/21005468
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
04/18/21
04/19/21
DM0418/21005481
DM0419/21005508
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
04/20/21 DM0420/21005839
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/21/21 DM0421/21005870
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
04/22/21 DM0422/21005981
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/23/21 DM0423/21005992
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/24/21 DM0424/21006057
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/25/21 DM0425/21006272
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/26/21 DM0426/21006299
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/27/21 DM0427/21006315
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/28/21 DM0428/21006346
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/29/21 DM0429/21006362
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
04/30/21 DM0430/21006373
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
05/01/21 DM0501/21006429
2.3 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/02/21 DM0502/21006442
2.3 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/03/21 DM0503/21006676
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
05/04/21 DM0504/21006691
2.3 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/05/21 DM0505/21006722
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
05/06/21 DM0506/21006781
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/07/21 DM0507/21006834
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
05/08/21 DM0508/21006981
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
05/09/21 DM0509/21006994
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
05/10/21 DM0510/21007021
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
05/11/21 DM0511/21007171
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/12/21 DM0512/21007202
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/13/21 DM0513/21007217
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/14/21
05/15/21
05/16/21
DM0514/21007309
DM0515/21007328
DM0516/21007341
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/17/21 DM0517/21007382
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
05/18/21 DM0518/21007440
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
Page 99 of 121
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MMSD
WARS RS F4t A (WAR pmt011101
Phosphorus - Total % DW (Calc.)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
05/19/21
DM0519/21007895
2.4%D.W.
0.1
0.1
SW846: 6010C
MMSD
05/20/21
DM0520/21007969
2.5 % D.W.
0.1 0.1
SW846: 6010C
MMSD
05/21/21
DM0521/21007980
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/22/21
DM0522/21008072
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
05/23/21 DM0523/21008085 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
05/25/21 DM0525/21008288 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
05/26/21 DM0526/21008319 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
05/27/21 DM0527/21008484 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
05/28/21 DM0528/21008495 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
05/29/21 DM0529/21008515 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
05/30/21 DM0530/21008530 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/01/21 DM0601/21008902 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/02/21 DM0602/21008935 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/03/21 DM0603/21008950 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/04/21 DM0604/21009184 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/05/21
06/06/21
DM0605/21009203
DM0606/21009287
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
06/07/21 DM0607/21009314 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/08/21 DM0608/21009334 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/09/21 DM0609/21009365 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/10/21 DM0610/21009538 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/11/21 DM0611/21009549 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/12/21 DM0612/21009568 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/13/21 DM0613/21009602 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/14/21 DM0614/21009629 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/18/21 DM0618/21009979 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/19/21 DM0619/21010314 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/20/21 DM0620/21010332 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/21/21 DM0621/21010359 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/22/21 DM0622/21010375 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/23/21 DM0623/21010408 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/24/21 DM0624/21010670 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/25/21 DM0625/21010681 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/26/21 DM0626/21010702 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/27/21 DM0627/21010807 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/28/21 DM0628/21010860 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/29/21 DM0629/21010875 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
06/30/21 DM0630/21011438 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/01/21 DM0701/21011453 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/02/21 DM0702/21011465 2.4 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/03/21
DM0703/21011485
2.4 % D.W. 0.1 0.1 T9. SW846: 6010C MMSD
07/04/21
07/05/21
07/06/21
DM0704/21011516
DM0705/21011572
DM0706/21011693
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
07/07/21 DM0707/21011727 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/08/21 DM0708/21011742 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
Page 100 of 121
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MMSD
WARS RS F4t A (WAR pmt011101
Phosphorus - Total % DW (Calc.)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
07/09/21
DM0709/21011754
2.5 % D.W.
0.1
0.1
SW846: 6010C
MMSD
07/10/21
DM0710/21012238
2.4%D.W.
0.1 0.1
SW846: 6010C
MMSD
07/11/21
DM0711 /21012255
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
07/12/21
DM0712/21012283
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
07/13/21 DM0713/21012298 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/14/21 DM0714/21012332 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/15/21 DM0715/21012390 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/16/21 DM0716/21012563 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/17/21 DM0717/21012583 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/18/21 DM0718/21012596 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/19/21 DM0719/21012624 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/20/21 DM0720/21012639 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/21/21 DM0721/21012760 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/22/21 DM0722/21012775 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/23/21 DM0723/21013074 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/24/21
07/25/21
DM0724/21013378
DM0725/21013391
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
07/26/21 DM0726/21013419 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/27/21 DM0727/21013434 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/28/21 DM0728/21013470 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/29/21 DM0729/21013614 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/30/21 DM0730/21013629 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
07/31/21 DM0731/21013739 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/01/21 DM0801/21013752 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/02/21 DM0802/21013891 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/03/21 DM0803/21013906 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/04/21 DM0804/21013940 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/05/21 DM0805/21014673 3 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/06/21 DM0806/21014685 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/07/21 DM0807/21014705 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/08/21 DM0809/21014718 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/09/21 DM0809/21014746 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/10/21
DM0810/21014847
2.6 % D.W. 0.1 0.1 D2, Q2.
SW846: 6010C MMSD
08/11/21 DM0811/21014867 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/12/21 DM0812/21015285 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/13/21 DM0813/21015297 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/14/21 DM0814/21015317 2.2 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/15/21 DM0815/21015330 2 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/16/21 DM0816/21015410 2 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/17/21 DM0817/21015425 2.4 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/18/21 DM0818/21016031 2.3 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/19/21
08/20/21
08/21/21
DM0819/21016046
DM0820/21016068
DM0821/21016088
2.3 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.3 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
08/22/21 DM0822/21016196 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
08/23/21 DM0823/21016224 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
Page 101 of 121
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MMSD
WARS RS F4t A (WAR pmt011101
Phosphorus - Total % DW (Calc.)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
08/24/21
DM0824/21016239
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
08/25/21
DM0825/21016327
2.5 % D.W.
0.1 0.1
SW846: 6010C
MMSD
08/26/21 DM0826/21016342
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
08/27/21 DM0827/21016407
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
08/28/21 DM0828/21016427
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
08/30/21 DM0830/21016468
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
08/31/21 DM0831/21016483
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/01/21 DM0901/21016598
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/02/21 DM0902/21016659
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/03/21 DM0903/21016671
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/04/21 DM0904/21017055
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
09/05/21 DM0905/21017068
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/06/21 DM0906/21017096
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/07/21 DM0907/21017306
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/08/21 DM0908/21017338
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/09/21
09/10/21
DM0909/21017408
DM0910/21017420
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/11/21 DM0911/21017699
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/12/21 DM0912/21017712
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/13/21 DM0913/21017740
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/14/21 DM0914/21017755
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/15/21 DM0915/21017903
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/16/21 DM0916/21018023
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
09/17/21 DM0917/21018105
2.4%D.W.
0.1 0.1
SW846: 6010C MMSD
09/18/21 DM0918/21018125
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/19/21 DM0919/21018138
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/20/21 DM0920/21018236
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/21/21 DM0921/21018251
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/22/21 DM0922/21018480
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/23/21 DM0923/21018564
2.5 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/24/21 DM0924/21018818
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/25/21 DM0925/21018838
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/26/21 DM0926/21019023
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/27/21 DM0927/21019051
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/28/21 DM0928/21019066
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/29/21 DM0929/21019228
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
09/30/21 DM0930/21019243
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
10/01/21 DM 1001 /21019255
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
10/02/21 DM1002/21019384
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
10/03/21 DM1003/21019397
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
10/04/21 DM1004/21019425
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
10/06/21
10/07/21
10/08/21
DM1006/21019735
DM1007/21019760
DM1008/21019772
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
10/19/21 DM1019/21020600
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
10/20/21 DM1020/21020674
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
Page 102 of 121
SYS/rptlMiloMonthlyDW 10/21/21 17 Printed: 1/13/22 14.24

MMSD
WARS RS F4t A (WAR pmt011101
Phosphorus - Total % DW (Calc.)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a •
QC Batch
ID
10/21/21
DM 1021 /21020689
2.6 % D.W.
0.1
0.1
SW846: 6010C
MMSD
10/22/21
DM 1022/21020701
2.9 % D.W.
0.1 0.1
SW846: 6010C
MMSD
10/23/21
DM 1023/21020883
2.9 % D.W.
0.1 0.1
SW846: 6010C MMSD
10/24/21
DM 1024/21021034
2.9 % D.W.
0.1 0.1
SW846: 6010C MMSD
10/25/21 DM1025/21021062 3 % D.W. 0.1 0.1
SW846: 6010C MMSD
10/26/21 DM1026/21021077 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
10/27/21 DM1027/21021161 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
10/28/21 DM1028/21021226 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
10/29/21 DM1029/21021510 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
10/30/21 DM1030/21021530 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
10/31/21 DM1031/21021574 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/01/21 DM1101/21021608 2.5 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/02/21 DM1102/21021623 2.6 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/03/21 DM1103/21021720 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/04/21 DM1104/21021735 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/05/21
11/06/21
DM1105/21021747
DM1106/21021767
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
11/07/21 DM1107/21022553 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/08/21 DM1108/21022581 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/09/21 DM1109/21022596 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/10/21 DM1110/21022680 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/11/21 DM1111/21022695 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/12/21 DM1112/21022707 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/13/21 DM1113/21022731 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/14/21 DM1114/21022744 2.9 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/15/21 DM1115/21022772 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/16/21 DM1116/21022787 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/17/21
DM 1117/21023039
2.8 % D.W. 0.1
0.1 Q3.
SW846: 6010C MMSD
11/18/21 DM1118/21023056 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/19/21 DM1119/21023181 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/20/21 DM1120/21023201 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/21/21 DM1121/21023214 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/22/21 DM1122/21023555 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/23/21 DM1123/21023570 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/24/21 DM1124/21023611 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/25/21 DM1125/21023795 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/26/21 DM1126/21023807 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/27/21 DM1127/21023827 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/28/21 DM1128/21023899 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/29/21 DM1129/21023927 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
11/30/21 DM1130/21024167 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
12/01/21
12/02/21
12/03/21
DM 1201 /21024282
DM 1202/21024297
DM 1203/21024309
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/04/21 DM1204/21024329 2.7 % D.W. 0.1 0.1
SW846: 6010C MMSD
12/05/21 DM1205/21024739 2.8 % D.W. 0.1 0.1
SW846: 6010C MMSD
Page 103 of 121
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MMSD
WARS F4t A CLIMB 1111101110111
Phosphorus - Total % DW (Calc.)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Daily Composite
Sample Date Sample ID
Result LOD LOQ QA Flags Ana Ica ' e • a .
QC Batch
ID
12/06/21
DM1206/21024767
2.9 % D.W.
0.1
0.1
SW846: 6010C
MMSD
12/07/21
DM 1207/21024782
2.7 % D.W.
0.1 0.1
SW846: 6010C
MMSD
12/08/21 DM 1208/21024816
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/09/21 DM 1209/21024832
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/10/21 DM1210/21024844
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/11/21 DM1211/21024864
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/12/21 DM1212/21025174
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/13/21 DM 1213/21025205
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/14/21 DM1214/21025220
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/15/21 DM1215/21025299
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/16/21 DM1216/21025314
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/17/21 DM1217/21025326
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/18/21 DM1219/21025346
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/19/21 DM1219/21025621
2.6 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/20/21 DM 1220/21025649
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/21/21
12/22/21
DM 1221 /21025664
DM1222/21025700
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
2.7 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/23/21 DM1223/21025779
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/24/21 DM1224/21025791
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/25/21 DM1225/21025811
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/26/21 DM 1226/21025824
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/27/21 DM1227/21025917
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/28/21 DM1228/21025932
2.9 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/29/21 DM1229/21025966
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/30/21 DM 1230/21025981
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
12/31/21 DM1231/21026033
2.8 % D.W.
0.1 0.1
SW846: 6010C MMSD
Avg Result: 2.6 % D.W. Min LOD: 0.1 % D.W.
ALUMINUM ICP Dry wt.
Max Result: 3 % D.W. Max LOD: 0.1 % D.W.
Milorganite Weekly Composite
Sample 'a e Sample ID
Result LOD LOQ QA Flags na Ica ' e o
QC Batch
ID
01/09/21
WMCO2/21000596
7400 mg/kg D.W.
61
210
B8.
SW846: 6010C
MMSD
02/13/21
WM CO7/21001740
5400 mg/kg D.W. 60 210 98.
SW846: 6010C
MMSD
03/13/21
WM C 11 /21003556
5000 mg/kg D.W. 60 210 98.
SW846: 6010C MMSD
04/10/21
05/08/21
WMC15/21005026
WMC19/21006996
5400 mg/kg D.W. 60 210 98.
SW846: 6010C MMSD
7300 mg/kg D.W. 60 210 98. SW846: 6010C MMSD
06/12/21 WMC24/21009604
8100 mg/kg D.W. 60 210 98. SW846: 6010C MMSD
07/10/21 WMC28/21012257
9000 mg/kg D.W. 60 210 98. SW846: 6010C MMSD
08/07/21 WMC32/21014720
Avg Result: 6800 mg/kg D.W.
7200 mg/kg D.W. 60 210 98. SW846: 6010C MMSD
Min LOD: 60 mg/kg D.W.
Max Result: 9000 mg/kg D.W. Max LOD: 61 mg/kg D.W.
SYS/rptlMiloMonthlyDW 10/21/21 17
Page 104 of 121
Printed: 1/13/22 14.24

MMSD
WARS F(t A CLIMB 1111101110111
(Milo) Ammonia in Fertilizer
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e o. a.
QC Batch
ID
01/09/21
WMCO2/21000596
0.24 %
0.01
AOAC 920.03 (mod) Midwest
Laboratories
02/13/21
WM C07/21001740
0.23 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
03/13/21 WMC11/21003556
0.2 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
04/10/21 WMC15/21005026
0.23 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
05/08/21 WMC19/21006996
0.27 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
06/12/21 WMC24/21009604
0.22 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
07/10/21 WMC28/21012257
0.26 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
08/07/21 WMC32/21014720
0.25 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
09/11/21 WMC37/21017714
0.2 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
10/09/21 WMC41/21019807
0.18 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
11/13/21 WMC46/21022746
0.25 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
12/11/21 WMC50/21025262
0.25 % 0.01
AOAC 920.03 (mod) Midwest
Laboratories
Avg Result: 0.23 %
BORON ICP Dry wt.
Min LOD: 0.01 %
Max Result: 0.27 %
Max LOD: 0.01 %
Samp a la e ample ID Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/09/21
WMCO2/21000596
23 mg/kg D.W.
5.4
20.6
EPA 6010
Pace -GB
02/13/21
WM CO7/21001740
24 mg/kg D.W. 5.4 20.6
EPA 6010
Pace -GB
03/13/21 WMC11/21003556
24 mg/kg D.W. 5.2 20
EPA 6010
Pace -GB
04/10/21 WMC15/21005026 22 mg/kg D.W. 5.5 20.9
EPA 6010 Pace -GB
05/08/21 WMC19/21006996 20 mg/kg D.W. 1.1 4.2
EPA 6010D Pace -GB
06/12/21 WMC24/21009604 23 mg/kg D.W. 2.2 8.4
EPA 6010D Pace -GB
07/10/21 WMC28/21012257 18 mg/kg D.W. 1.1 4.2 AX. EPA 6010D Pace -GB
08/07/21 WMC32/21014720 19 mg/kg D.W. 2.1 8.1
EPA 6010D Pace -GB
09/11/21
10/09/21
WMC37/21017714
WMC41/21019807
24 mg/kg D.W.
2.2 8.4
EPA 6010D Pace -GB
24 mg/kg D.W.
2.2 8.3
EPA 6010D Pace -GB
11/13/21 WMC46/21022746 21 mg/kg D.W. 2.2 8.3
EPA 6010D Pace -GB
12/11/21 WMC50/21025262 18 mg/kg D.W. 1.1 4.2
EPA 6010D Pace -GB
Avg Result: 22 mg/kg D.W. Min LOD: 1.1 mg/kg D.W.
Max Result: 24 mg/kg D.W. Max LOD: 5.5 mg/kg D.W.
Page 105 of 121
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MMSD
PARTAERS FOI A CLEAMJ pn1101111Mt
CHROMIUM ICP Dry wt.
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e o. a. QC Batch
ID
01/09/21
WMCO2/21000596
160 mg/kg D.W.
0.4
1.2
SW846: 6010C
MMSD
02/13/21
WM CO7/21001740
320 mg/kg D.W.
0.4 1.2
SW846: 6010C
MMSD
03/13/21 WMC11/21003556
260 mg/kg D.W.
0.4 1.2
SW846: 6010C MMSD
04/10/21 WMC15/21005026 270 mg/kg D.W. 0.4 1.2
SW846: 6010C MMSD
05/08/21 WMC19/21006996 280 mg/kg D.W. 0.4 1.2
SW846: 6010C MMSD
06/12/21 WMC24/21009604 250 mg/kg D.W. 0.4 1.2
SW846: 6010C MMSD
07/10/21 WMC28/21012257 200 mg/kg D.W. 0.4 1.2
SW846: 6010C MMSD
08/07/21 WMC32/21014720 230 mg/kg D.W. 0.4 1.2
SW846: 6010C MMSD
Avg Result: 250 mg/kg D.W. Min LOD: 0.4 mg/kg D.W.
COBALT ICP Dry wt.
Max Result: 320 mg/kg D.W. Max LOD: 0.4 mg/kg D.W.
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab QC Batch
ID
01/09/21
WMCO2/21000596
2.8 mg/kg D.W.
0.3
1.2
B8.
SW846: 6010C
MMSD
02/13/21
03/13/21
04/10/21
WMC07/21001740
WMC11/21003556
WMC15/21005026
3 mg/kg D.W.
0.29 1.2
B8.
SW846: 6010C
MMSD
3 mg/kg D.W. 0.29 1.2 88.
SW846: 6010C MMSD
3 mg/kg D.W. 0.3 1.2 88.
SW846: 6010C MMSD
05/08/21 WMC19/21006996 3 mg/kg D.W. 0.29 1.2 88. SW846: 6010C MMSD
06/12/21 WMC24/21009604 3 mg/kg D.W. 0.3 1.2 88. SW846: 6010C MMSD
07/10/21 WMC28/21012257 3.4 mg/kg D.W. 0.29 1.2 88. SW846: 6010C MMSD
08/07/21 WMC32/21014720 3.6 mg/kg D.W. 0.29 1.2 88. SW846: 6010C MMSD
Avg Result: 3.1 mg/kg D.W. Min LOD: 0.29 mg/kg D.W.
Max Result: 3.6 mg/kg D.W. Max LOD: 0.3 mg/kg D.W.
Page 106 of 121
SYS/rptlMiloMonthlyDW 10/21/21 17 Printed: 1/13/22 14.24

MMSD
PARTNERS Ka A CLLJ I LYfl.h
MERCURY by M. 7471 (sludge)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Sample Date Sample ID Result LOD LOQ QA Flags na Ica ' e o
QC Batch
ID
01/02/21
WMC01 /21000078
0.15 mg/kg D.W.
0.023
0.079
EPA 7471
Pace -GB
01/09/21
WM CO2/21000596
0.17 mg/kg D.W. 0.021 0.074
EPA 7471
Pace -GB
01/16/21 WMCO3/21000799
0.22 mg/kg D.W. 0.022 0.077
EPA 7471
Pace -GB
01/23/21 WMC04/21001061 0.19 mg/kg D.W. 0.021 0.072
EPA 7471 Pace -GB
01/30/21 WMC05/21001319 0.39 mg/kg D.W. 0.018 0.063
EPA 7471 Pace -GB
02/06/21 WMC06/21001491 0.3 mg/kg D.W. 0.022 0.076 AX. EPA 7471 Pace -GB
02/13/21 WMCO7/21001740 0.16 mg/kg D.W. 0.021 0.073
EPA 7471 Pace -GB
02/20/21 WMCO8/21002074 0.24 mg/kg D.W. 0.019 0.067
EPA 7471 Pace -GB
02/27/21 WMCO9/21002480 0.12 mg/kg D.W. 0.021 0.073
EPA 7471 Pace -GB
03/06/21 WMC10/21002860 0.25 mg/kg D.W. 0.02 0.068
EPA 7471 Pace -GB
03/13/21 WMC11/21003556 0.16 mg/kg D.W. 0.02 0.07
EPA 7471 Pace -GB
03/20/21 WMC12/21004095 0.21 mg/kg D.W. 0.021 0.074
EPA 7471 Pace -GB
03/27/21 WMC13/21004287 0.19 mg/kg D.W. 0.021 0.075
EPA 7471 Pace -GB
04/03/21 WMC14/21004661 0.18 mg/kg D.W. 0.02 0.071
EPA 7471 Pace -GB
04/10/21 WMC15/21005026 0.27 mg/kg D.W. 0.019 0.067
EPA 7471 Pace -GB
04/17/21
04/24/21
WMC16/21005483
WMC17/21006274
0.18 mg/kg D.W. 0.02 0.07
EPA 7471 Pace -GB
0.17 mg/kg D.W. 0.021 0.072
EPA 7471 Pace -GB
05/01/21 WMC18/21006444 0.17 mg/kg D.W. 0.021 0.075
EPA 7471 Pace -GB
05/08/21 WMC19/21006996 0.18 mg/kg D.W. 0.02 0.071
EPA 7471 Pace -GB
05/15/21 WMC20/21007343 0.14 mg/kg D.W. 0.02 0.07
EPA 7471 Pace -GB
05/22/21 WMC21/21008087 0.18 mg/kg D.W. 0.021 0.072
EPA 7471 Pace -GB
05/29/21 WMC22/21008532 0.19 mg/kg D.W. 0.022 0.075
EPA 7471 Pace -GB
06/05/21 WMC23/21009289 0.35 mg/kg D.W. 0.02 0.069
EPA 7471 Pace -GB
06/12/21 WMC24/21009604 0.22 mg/kg D.W. 0.021 0.074
EPA 7471 Pace -GB
06/19/21 WMC25/21010334 0.18 mg/kg D.W. 0.022 0.076 AX. EPA 7471 Pace -GB
06/26/21 WMC26/21010809 0.26 mg/kg D.W. 0.021 0.074
EPA 7471 Pace -GB
07/03/21 WMC27/21011518 0.31 mg/kg D.W. 0.021 0.074 AX. EPA 7471 Pace -GB
07/10/21 WMC28/21012257 0.2 mg/kg D.W. 0.019 0.068
EPA 7471 Pace -GB
07/17/21 WMC29/21012598 0.17 mg/kg D.W. 0.021 0.073
EPA 7471 Pace -GB
07/24/21 WMC30/21013393 0.27 mg/kg D.W. 0.021 0.075 AX. EPA 7471 Pace -GB
07/31/21 WMC31/21013754 0.17 mg/kg D.W. 0.022 0.076
EPA 7471 Pace -GB
08/07/21 WMC32/21014720 0.42 mg/kg D.W. 0.022 0.077
EPA 7471 Pace -GB
08/14/21 WMC33/21015332 0.27 mg/kg D.W. 0.018 0.064
EPA 7471 Pace -GB
08/21/21 WMC34/21016198 0.52 mg/kg D.W. 0.02 0.069
EPA 7471 Pace -GB
08/28/21 WMC35/21016442 0.33 mg/kg D.W. 0.019 0.066
EPA 7471 Pace -GB
09/04/21 WMC36/21017070 0.38 mg/kg D.W. 0.021 0.074
EPA 7471 Pace -GB
09/11/21 WMC37/21017714 0.31 mg/kg D.W. 0.021 0.075
EPA 7471 Pace -GB
09/18/21 WMC38/21018140 0.32 mg/kg D.W. 0.019 0.068
EPA 7471 Pace -GB
09/25/21 WMC39/21019025 0.23 mg/kg D.W. 0.021 0.074
EPA 7471 Pace -GB
10/02/21 WMC40/21019399 0.31 mg/kg D.W. 0.019 0.066
EPA 7471 Pace -GB
10/09/21 WMC41/21019807 0.21 mg/kg D.W. 0.019 0.065
EPA 7471 Pace -GB
10/23/21
10/30/21
11/06/21
WMC43/21021036
WMC44/21021576
WMC45/21022555
0.24 mg/kg D.W. 0.021 0.072
EPA 7471 Pace -GB
0.26 mg/kg D.W. 0.022 0.079
EPA 7471 Pace -GB
0.13 mg/kg D.W. 0.021 0.074
EPA 7471 Pace -GB
11/13/21 WMC46/21022746 0.25 mg/kg D.W. 0.02 0.071
EPA 7471 Pace -GB
11/20/21 WMC47/21023216 0.24 mg/kg D.W. 0.022 0.076
EPA 7471 Pace -GB
Page 107 of 121
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MMSD
PARIIFRS Ka A CLLJ I LY fl.h
MERCURY by M. 7471 (sludge)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Sample Date Sample ID
Result LOD LOQ QA Flags na Ica ' e o
QC Batch
ID
11/27/21
WMC48/21023901
0.24 mg/kg D.W.
0.021
0.074
EPA 7471
Pace -GB
12/04/21
WM C49/21024741
0.24 mg/kg D.W. 0.023 0.082
EPA 7471
Pace -GB
12/11/21 WMC50/21025262
0.17 mg/kg D.W. 0.02 0.069
EPA 7471
Pace -GB
12/18/21 WMC51/21025623
0.25 mg/kg D.W. 0.02 0.07
EPA 7471 Pace -GB
12/25/21 WMC52/21026035
0.29 mg/kg D.W. 0.02 0.072
EPA 7471 Pace -GB
Avg Result: 0.24 mg/kg D.W. Min LOD: 0.018 mg/kg D.W.
NITRATE NITROGEN
Max Result: 0.52 mg/kg D.W. Max LOD: 0.023 mg/kg D.W.
Sa e Dat- Sample ID
Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/09/21
WMCO2/21000596
< 0.01
0.01
WC PROC 32
Midwest
Laboratories
02/13/21
WMC07/21001740
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
03/13/21 WMC11/21003556
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
04/10/21 WMC15/21005026
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
05/08/21 WMC19/21006996
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
06/12/21 WMC24/21009604
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
07/10/21 WMC28/21012257
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
08/07/21 WMC32/21014720
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
09/11/21 WMC37/21017714
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
10/09/21 WMC41/21019807
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
11/13/21 WMC46/21022746
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
12/11/21 WMC50/21025262
< 0.01 % 0.01
WC PROC 32 Midwest
Laboratories
Avg Result: 0 % Min LOD: 0.01 %
Max Result: 0.01 % Max LOD: 0.01 %
Page 108 of 121
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MMSD
PARTNERS F4t A CLIMB DI* OW
NITROGEN-Total(Auto)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e o. a
QC Batch
ID
01/09/21
WMCO2/21000596
6.6 %
0.01
MWL WC PROC 55
Midwest
Laboratories
02/13/21
WM C07/21001740
6.9 % 0.01
MWL WC PROC 55 Midwest
Laboratories
03/13/21 WMC11/21003556
6.9 % 0.01
MWL WC PROC 55 Midwest
Laboratories
04/10/21 WMC15/21005026
6.8 % 0.01
MWL WC PROC 55 Midwest
Laboratories
05/08/21 WMC19/21006996
6.6 % 0.01
MWL WC PROC 55 Midwest
Laboratories
06/12/21 WMC24/21009604
6.2 % 0.01
MWL WC PROC 55 Midwest
Laboratories
07/10/21 WMC28/21012257
6 % 0.01
MWL WC PROC 55 Midwest
Laboratories
08/07/21 WMC32/21014720
6 % 0.01
MWL WC PROC 55 Midwest
Laboratories
09/11/21 WMC37/21017714
5.7 % 0.01
MWL WC PROC 55 Midwest
Laboratories
10/09/21 WMC41/21019807
6 % 0.01
MWL WC PROC 55 Midwest
Laboratories
11/13/21 WMC46/21022746
6.5 % 0.01
MWL WC PROC 55 Midwest
Laboratories
12/11/21 WMC50/21025262
6.6 % 0.01
MWL WC PROC 55 Midwest
Laboratories
Avg Result: 6.4 %
NITROGEN -Water Insoluble
Min LOD: 0.01 %
Max Result: 6.9 %
Max LOD: 0.01 %
Samp a la e ample ' Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/09/21
WMCO2/21000596
5%
0.01
AOAC (16) 945.01
Midwest
Laboratories
02/13/21
WMC07/21001740
5.9 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
03/13/21 WMC11/21003556
5.3 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
04/10/21 WMC15/21005026
5.6 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
05/08/21 WMC19/21006996
5.4 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
06/12/21 WMC24/21009604
5%
0.01
AOAC (16) 945.01 Midwest
Laboratories
07/10/21 WMC28/21012257
4.7 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
08/07/21 WMC32/21014720
5.1 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
09/11/21 WMC37/21017714
4.7 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
10/09/21 WMC41/21019807
4.8 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
11/13/21 WMC46/21022746
5%
0.01
AOAC (16) 945.01 Midwest
Laboratories
12/11/21 WMC50/21025262
5.5 % 0.01
AOAC (16) 945.01 Midwest
Laboratories
Avg Result: 5.2 % Min LOD: 0.01 %
Max Result: 5.9 % Max LOD: 0.01 %
Page 109 of 121
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MMSD
PARTNERS F41 A CLEAA#M MINIM,
pH -Solids
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e o. a.
QC Batch
ID
01/02/21
WMC01 /21000078
6.25 Stnd. Units
0.1
SW846: 9045D
MMSD
01/09/21
WM CO2/21000596
6.18 Stnd. Units 0.1
SW846: 9045D
MMSD
01/16/21 WM CO3/21 000799
6.17 Stnd. Units 0.1
SW846: 9045D MMSD
01/23/21 WMC04/21001061 6.18 Stnd. Units 0.1
SW846: 9045D MMSD
01/30/21 WMC05/21001319 6.12 Stnd. Units 0.1
SW846: 9045D MMSD
02/06/21 WMC06/21001491 6.25 Stnd. Units 0.1
SW846: 9045D MMSD
02/13/21 WM C07/21 001740 6 Stnd. Units 0.1
SW846: 9045D MMSD
02/20/21 WM C08/21 002074 5.91 Stnd. Units 0.1
SW846: 9045D MMSD
02/27/21 WM C09/21 002480 5.89 Stnd. Units 0.1 SW846: 9045D MMSD
03/06/21 WMC10/21002860 5.97 Stnd. Units 0.1 SW846: 9045D MMSD
03/13/21 WMC11/21003556 5.95 Stnd. Units 0.1 SW846: 9045D MMSD
03/20/21 WMC12/21004095 5.99 Stnd. Units 0.1 SW846: 9045D MMSD
03/27/21 WMC13/21004287 5.99 Stnd. Units 0.1 SW846: 9045D MMSD
04/03/21 WMC14/21004661 6.04 Stnd. Units 0.1 SW846: 9045D MMSD
04/10/21 WMC15/21005026 6.14 Stnd. Units 0.1 SW846: 9045D MMSD
04/17/21 WMC16/21005483 6.21 Stnd. Units 0.1
SW846: 9045D MMSD
04/24/21 WMC17/21006274 6.23 Stnd. Units 0.1
SW846: 9045D MMSD
05/01/21 WMC18/21006444 6.2 Stnd. Units 0.1 SW846: 9045D MMSD
05/08/21 WMC19/21006996 6.18 Stnd. Units 0.1 SW846: 9045D MMSD
05/15/21 WM C20/21 007343 6.18 Stnd. Units 0.1 SW846: 9045D MMSD
05/22/21 WMC21/21008087 6.39 Stnd. Units 0.1 SW846: 9045D MMSD
05/29/21 WMC22/21008532 6.4 Stnd. Units 0.1 SW846: 9045D MMSD
06/05/21 WMC23/21009289 6.49 Stnd. Units 0.1 SW846: 9045D MMSD
06/12/21 WMC24/21009604 6.39 Stnd. Units 0.1 SW846: 9045D MMSD
06/19/21 WMC25/21010334 6.32 Stnd. Units 0.1 SW846: 9045D MMSD
06/26/21 WMC26/21010809 6.38 Stnd. Units 0.1 SW846: 9045D MMSD
07/03/21 WMC27/21011518 6.34 Stnd. Units 0.1 SW846: 9045D MMSD
07/10/21 WMC28/21012257 6.37 Stnd. Units 0.1 SW846: 9045D MMSD
07/17/21 WMC29/21012598 6.32 Stnd. Units 0.1 SW846: 9045D MMSD
07/24/21 WMC30/21 01 3393 6.35 Stnd. Units 0.1 SW846: 9045D MMSD
07/31/21 WMC31/21013754 6.34 Stnd. Units 0.1 SW846: 9045D MMSD
08/07/21 WMC32/21014720 6.36 Stnd. Units 0.1 SW846: 9045D MMSD
08/14/21 WMC33/21015332 6.38 Stnd. Units 0.1 SW846: 9045D MMSD 149911-1
08/21/21 WMC34/21016198 6.52 Stnd. Units 0.1 SW846: 9045D MMSD 149911-1
08/28/21 WMC35/21016442 6.46 Stnd. Units 0.1 SW846: 9045D MMSD 149911-1
09/04/21 WMC36/21017070 6.45 Stnd. Units 0.1 SW846: 9045D MMSD 149911-1
09/11/21 WMC37/21017714 6.46 Stnd. Units 0.1 SW846: 9045D MMSD 149911-1
09/18/21 WMC38/21018140 6.33 Stnd. Units 0.1 SW846: 9045D MMSD 150429-1
09/25/21 WMC39/21019025 6.38 Stnd. Units 0.1 SW846: 9045D MMSD 150429-1
10/02/21 WMC40/21 01 9399 6.32 Stnd. Units 0.1 SW846: 9045D MMSD 150429-1
10/09/21 WMC41/21019807 6.31 Stnd. Units 0.1 SW846: 9045D MMSD 150429-1
10/23/21 WMC43/21021036 6.17 Stnd. Units 0.1
SW846: 9045D MMSD 150952-1
10/30/21 WMC44/21021576 6.16 Stnd. Units 0.1
SW846: 9045D MMSD 150952-1
11/06/21 WMC45/21022555 6.31 Stnd. Units 0.1
SW846: 9045D MMSD 150952-1
11/13/21 WMC46/21022746 6.29 Stnd. Units 0.1 SW846: 9045D MMSD 151251-1
11/20/21 WMC47/21023216 6.29 Stnd. Units 0.1 SW846: 9045D MMSD 151251-1
Page 110 of 121
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MMSD
PARTAFRS F4t A OAR MINIM
pH -Solids
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Sample Date Sample ID
Result
LOD LOQ QA Flags
•na Ica 'e o. a.
QC Batch
ID
11/27/21
WMC48/21023901
6.35 Stnd. Units
0.1
SW846: 9045D
MMSD
151251-1
12/04/21
WMC49/21024741
6.26 Stnd. Units 0.1
SW846: 9045D
MMSD 151929-1
12/11/21 WMC50/21025262
6.17 Stnd. Units 0.1
SW846: 9045D MMSD 151929-1
12/18/21 WMC51/21025623 6.23 Stnd. Units 0.1
SW846: 9045D MMSD 151929-1
12/25/21 WMC52/21026035 6.22 Stnd. Units 0.1
SW846: 9045D MMSD 151929-1
Avg Result: 6.2 Stnd. Units Min LOD: 0.1 Stnd. Units
PHOSPHORUS ICP Dry wt.
Max Result: 6.52 Stnd. Units Max LOD: 0.1 Stnd. Units
Sa e Dat- ample •
Result
LOD LOQ QA Flags
Analytical Method Lab
QC Batch
ID
09/11/21
WMC37/21017714
25000 mg/kg D.W.
23
89
SW846: 6010C
MMSD
150517-1
10/09/21
WM C41 /21019807
28000 mg/kg D.W. 23 88
SW846: 6010C
MMSD 151576-1
11/13/21 WMC46/21022746
28000 mg/kg D.W. 23 89 S5.
SW846: 6010C MMSD 151576-1
12/11/21 WMC50/21025262 29000 mg/kg D.W. 23 89
SW846: 6010C MMSD 151576-1
Avg Result: 28000 mg/kg D.W. Min LOD: 23 mg/kg D.W.
Max Result: 30000 mg/kg D.W. Max LOD: 24 mg/kg D.W.
Page 111 of 121
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MMSD
PARTNERS FOI A CLEANER Eri1101110N1
Solids (% Moisture)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e o. a.
QC Batch
ID
01/02/21
WMC01 /21000078
6.2 %
0.1
SM 2540 G (1997)
MMSD
01/16/21
WM CO3/21000799
6 % 0.1
SM 2540 G (1997) MMSD
01/23/21 WMC04/21001061
SM 2540 G (1997) MMSD
01/30/21 WMC05/21001319
5.7 % 0.1
SM 2540 G (1997) MMSD
02/06/21 WMC06/21001491
5.9 % 0.1
SM 2540 G (1997) MMSD
02/13/21 WMCO7/21001740 4.8 % 0.1
SM 2540 G (1997) MMSD
02/20/21 WMCO8/21002074 5.2 % 0.1
SM 2540 G (1997) MMSD
02/27/21 WMCO9/21002480 5.5 % 0.1
SM 2540 G (1997) MMSD
03/06/21 WMC10/21002860 4.5 % 0.1 SM 2540 G (1997) MMSD
03/13/21 WMC11/21003556
5%
0.1
SM 2540 G (1997) MMSD
03/20/21 WMC12/21004095 4.8 % 0.1 SM 2540 G (1997) MMSD
03/27/21 WMC13/21004287 5.2 % 0.1 SM 2540 G (1997) MMSD
04/03/21 WMC14/21004661 5.5 % 0.1 SM 2540 G (1997) MMSD
04/10/21 WMC15/21005026 5.7 % 0.1 SM 2540 G (1997) MMSD
04/17/21 WMC16/21005483 5.4 % 0.1 SM 2540 G (1997) MMSD
04/24/21
05/01/21
WMC17/21006274
WMC18/21006444
5.3 % 0.1
SM 2540 G (1997) MMSD
4.5 % 0.1
SM 2540 G (1997) MMSD
05/08/21 WMC19/21006996 4.9 % 0.1 SM 2540 G (1997) MMSD
05/15/21 WMC20/21007343 5.1 % 0.1 SM 2540 G (1997) MMSD
05/22/21 WMC21/21008087 5.6 % 0.1 SM 2540 G (1997) MMSD
05/29/21 WMC22/21008532
5%
0.1
SM 2540 G (1997) MMSD
06/05/21 WMC23/21009289
5%
0.1
SM 2540 G (1997) MMSD
06/12/21 WMC24/21009604 5.2 % 0.1 SM 2540 G (1997) MMSD
06/19/21 WMC25/21010334 5.6 % 0.1 SM 2540 G (1997) MMSD
06/26/21 WMC26/21010809 5.3 % 0.1 SM 2540 G (1997) MMSD
07/03/21 WMC27/21011518 5.4 % 0.1 SM 2540 G (1997) MMSD
07/10/21 WMC28/21012257 4.7 % 0.1 SM 2540 G (1997) MMSD
07/17/21 WMC29/21012598 4.3 % 0.1 SM 2540 G (1997) MMSD
07/24/21 WMC30/21013393 5.1 % 0.1 SM 2540 G (1997) MMSD
07/31/21 WMC31/21013754 4.7 % 0.1 SM 2540 G (1997) MMSD
08/07/21 WMC32/21014720
5%
0.1
SM 2540 G (1997) MMSD
08/14/21 WMC33/21015332 4.6 % 0.1 SM 2540 G (1997) MMSD
08/21/21 WMC34/21016198 3.6 % 0.1 SM 2540 G (1997) MMSD
08/28/21 WMC35/21016442 4.8 % 0.1 SM 2540 G (1997) MMSD
09/04/21 WMC36/21017070 4.6 % 0.1 SM 2540 G (1997) MMSD
09/11/21 WMC37/21017714 5.4 % 0.1 SM 2540 G (1997) MMSD 149896-1
09/18/21 WMC38/21018140 5.3 % 0.1 SM 2540 G (1997) MMSD 150039-1
09/25/21 WMC39/21019025 4.8 % 0.1 SM 2540 G (1997) MMSD 150169-1
10/02/21 WMC40/21019399 4.2 % 0.1 SM 2540 G (1997) MMSD 150294-1
10/09/21 WMC41/21019807 4.6 % 0.1 SM 2540 G (1997) MMSD 150419-1
10/23/21 WMC43/21021036 4.1 % 0.1 SM 2540 G (1997) MMSD 150673-1
10/30/21
11/06/21
11/13/21
WM C44/21021576
WMC45/21022555
WMC46/21022746
4.8 % 0.1
SM 2540 G (1997) MMSD 150796-1
4.9 % 0.1
SM 2540 G (1997) MMSD 150902-1
6 % 0.1 S5. SM 2540 G (1997)
MMSD
11/20/21 WMC47/21023216 5.5 % 0.1 SM 2540 G (1997) MMSD 151138-1
11/27/21 WMC48/21023901 6.2 % 0.1 SM 2540 G (1997) MMSD 151230-1
Page 112 of 121
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MMSD
PARTNERS F4t A CLEAMJ pnl*ONi01(1
Solids (% Moisture)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Sample Date Sample ID Result LOD LOQ QA Flags • na Ica ' e o. a.
QC Batch
ID
12/04/21
WMC49/21024741
5.3 %
0.1
SM 2540 G (1997)
MMSD
151365-1
12/11/21
WM C50/21025262
6 % 0.1
SM 2540 G (1997) MMSD 151485-1
12/18/21 WMC51/21025623
5.7 % 0.1
SM 2540 G (1997)
MMSD 151597-1
12/25/21 WMC52/21026035
6.6 % 0.1
SM 2540 G (1997)
MMSD 151706-1
Min LOD: 0.1 %
Solids (% Volatile)
Max LOD: 0.1 %
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/09/21
WMCO2/21000596
73 % 0.1 55. SM 2540 G (1997)
MMSD
02/13/21
WM CO7/21001740
74 % 0.1 55. SM 2540 G (1997) MMSD
03/13/21 WMC11/21003556
75 % 0.1
SM 2540 G (1997) MMSD
04/10/21 WMC15/21005026
74 % 0.1
SM 2540 G (1997) MMSD
05/08/21 WMC19/21006996
74 % 0.1
SM 2540 G (1997) MMSD
06/12/21
07/10/21
08/07/21
WMC24/21009604
WMC28/21012257
WMC32/21014720
71 % 0.1
SM 2540 G (1997) MMSD
69 % 0.1
SM 2540 G (1997) MMSD
69 % 0.1
SM 2540 G (1997) MMSD
09/11/21 WMC37/21017714 68 % 0.1
SM 2540 G (1997) MMSD 149895-1
10/09/21 WMC41/21019807 70 % 0.1
SM 2540 G (1997) MMSD 150420-1
11/13/21 WMC46/21022746
72 % 0.1
SM 2540 G (1997) MMSD 151005-1
12/11/21 WMC50/21025262
73 % 0.1
SM 2540 G (1997) MMSD 151486-1
Avg Result: 72 %
Solids (% Total)
Min LOD: 0.1 %
Max Result: 75 %
Max LOD: 0.1 %
Sample Dat Sample ID
Result LOD LOQ QA Flags
Analytical Method
Lab
QC Batch
ID
01/09/21
WMCO2/21000596
94 % 0.1 55. SM 2540 G (1997)
MMSD
02/13/21
WM CO7/21001740
95 % 0.1 55. SM 2540 G (1997)
MMSD
Avg Result: 94 %
Phosphorus - Water Extractable
Min LOD: 0.1 %
Max Result: 98 %
Max LOD: 0.1 %
Sample Date Sample ID Result LOD LOQ QA Flags Analytical Method Lab
QC Batch
ID
01/09/21
WM CO2/21000596
0.015 % of Total P
0
WDNR Guidance
MMSD
02/13/21
WM CO7/21001740
0.017 % of Total P
0
WDNR Guidance
MMSD
03/13/21 WMC11/21003556
0.018%ofTotalP 0
WDNR Guidance MMSD
04/10/21 WMC15/21005026 0.016 % of Total P 0
WDNR Guidance MMSD
05/08/21 WMC19/21006996 0.019 % of Total P 0
WDNR Guidance MMSD
06/12/21 WMC24/21009604 0.017 % of Total P 0
WDNR Guidance MMSD
07/10/21 WMC28/21012257 0.013 % of Total P 0
WDNR Guidance MMSD
08/07/21 WMC32/21014720 0.01 % of Total P 0
WDNR Guidance MMSD
09/11/21 WMC37/21017714 0.017 % of Total P 0 WDNR Guidance MMSD
10/09/21 WMC41/21019807 0.011 % of Total P 0
WDNR Guidance MMSD
11/13/21 WMC46/21022746 0.014 % of Total P 0
WDNR Guidance MMSD
12/11/21 WMC50/21025262 0.018 % of Total P 0
WDNR Guidance MMSD
Avg Result: 0.015 % of Total P Min LOD: 0 % of Total P
Max Result: 0.019 % of Total P Max LOD: 0 % of Total P
SYS/rptlMiloMonthlyDW 10/21/21 17
Page 113 of 121
Printed: 1/13/22 14.24

PARTNERS Ka A CLEANER 11n1*OM10111
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite Weekly Composite
Page 114 of 121
SYS/rptlMiloMonthlyDW 10/21/21 17 Printed: 1/13/22 14.24

MMSD
PARTNERS Ka A CLEANER 1111*OM10111
FECAL COLIFORM SLUDGE
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite (Outfall 006) PRODUCTION
Sample Date Sample ID Result LOD LOQ QA Flags
na Ica ' e o Lab
QC Batch
ID
01/05/21
21000710
19 MPN/g TS
0.2
EPA 1680
MMSD
01/12/21
21001371
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
01/19/21 21001822
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
01/26/21 21002195
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
02/02/21 21002507
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
02/09/21 21002800
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
02/16/21 21003494
0.21 MPN/g TS 0.19
EPA 1680 MMSD
02/23/21 21003853
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
03/02/21 21004350
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
03/09/21 21004569
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
03/16/21 21004992
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
03/23/21 21005822
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
03/30/21 21006155
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
04/13/21 21006930
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
04/20/21 21007414 < 0.2 MPN/g TS 0.2 EPA 1680 MMSD
04/27/21 21008161
05/04/21 21008583
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
05/11/21 21009267
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
05/18/21 21009703
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
05/25/21 21010237
< 0.18 MPN/g TS 0.18
EPA 1680 MMSD
06/01/21 21010778 < 1.9 MPN/g TS 1.9
AO. EPA 1680 MMSD
06/08/21 21011270
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
06/22/21 21012528
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
06/29/21 21013172
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
07/06/21 21013781 < 0.19 MPN/g TS 0.19 Q2. EPA 1680 MMSD
07/13/21 21014462
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
07/20/21 21015226
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
07/27/21 21015938
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
08/03/21 21016520 1.9 MPN/g TS 1.9 EPA 1680 MMSD
08/10/21 21017148
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
08/24/21 21018406
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
08/31/21 21018961
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
09/07/21 21019296 140 MPN/g TS 1.9 EPA 1680 MMSD
09/14/21 21019839 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 150008-1
09/21/21 21020475 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 150137-1
09/28/21 21021002 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 150249-1
10/20/21 21022830 < 0.18 MPN/g TS 0.18 EPA 1680 MMSD 150687-1
10/26/21 21023248 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 150774-1
11/09/21 21024070 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 150983-1
11/16/21 21024363 14 MPN/g TS 0.19 EPA 1680 MMSD 151105-1
11/23/21 21024720 < 0.2 MPN/g TS 0.2
EPA 1680
MMSD 151250-1
11/30/21 21025009 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 151323-1
12/07/21 21025371 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 151459-1
12/14/21 21025593 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 151598-1
12/21/21 21026062 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 151713-1
12/28/21 21026149 < 0.19 MPN/g TS 0.19 EPA 1680 MMSD 151781-1
Page 115 of 121
SYS/rptlMiloMonthlyDW 10/21/21 17 Printed: 1/13/22 14.24

Annual Milorganite Report DW
January 1 to December 31, 2021
PARTNERS Ka A CLIMB 1111*OMli1Mt
Milorganite (Outfall 006) PRODUCTION
FECAL COLIFORM SLUDGE
QC Batch
ID
Min LOD: 0.18 MPN/g TS
Max LOD: 1.9 MPN/g TS
Page 116 of 121
SYS/rptlMiloMonthlyDW 10/21/21 17 Printed: 1/13/22 14.24

MMSD
PARTNERS FOI A OAR MOM
I B
Solids (% Total)
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite (Outfall 006) PRODUCTION
Sample Date Sample ID Result LOD LOQ QA Flags
na Ica ' e o Lab
QC Batch
ID
01/05/21
21000710
91 %
0.1
SM 2540 G (1997)
MMSD
01/12/21
21001371
94 % 0.1
SM 2540 G (1997) MMSD
01/19/21 21001822
94 % 0.1
SM 2540 G (1997) MMSD
01/26/21 21002195
93 % 0.1
SM 2540 G (1997) MMSD
02/02/21 21002507
95 % 0.1
SM 2540 G (1997) MMSD
02/09/21 21002800
95 % 0.1
SM 2540 G (1997) MMSD
02/16/21 21003494
94 % 0.1
SM 2540 G (1997) MMSD
02/23/21 21003853 96 % 0.1
SM 2540 G (1997) MMSD
03/02/21 21004350 96 % 0.1 SM 2540 G (1997) MMSD
03/09/21 21004569 94 % 0.1 SM 2540 G (1997) MMSD
03/16/21 21004992 96 % 0.1 SM 2540 G (1997) MMSD
03/23/21 21005822 96 % 0.1 SM 2540 G (1997) MMSD
03/30/21 21006155 94 % 0.1 SM 2540 G (1997) MMSD
04/13/21 21006930 95 % 0.1 SM 2540 G (1997) MMSD
04/20/21 21007414 91 % 0.1 SM 2540 G (1997) MMSD
04/27/21 21008161 96 % 0.1 SM 2540 G (1997) MMSD
05/04/21 21008583 95 % 0.1 SM 2540 G (1997) MMSD
05/11/21 21009267 94 % 0.1 SM 2540 G (1997) MMSD
05/18/21 21009703 94 % 0.1 SM 2540 G (1997) MMSD
05/25/21 21010237 97 % 0.1 SM 2540 G (1997) MMSD
06/01/21 21010778 96 % 0.1 SM 2540 G (1997) MMSD
06/08/21 21011270 96 % 0.1 SM 2540 G (1997) MMSD
06/22/21 21012528 95 % 0.1 SM 2540 G (1997) MMSD
06/29/21 21013172 96 % 0.1 SM 2540 G (1997) MMSD
07/06/21 21013781 95 % 0.1 SM 2540 G (1997) MMSD
07/13/21 21014462 96 % 0.1 SM 2540 G (1997) MMSD
07/20/21 21015226 95 % 0.1 SM 2540 G (1997) MMSD
07/27/21 21015938 96 % 0.1 SM 2540 G (1997) MMSD
08/03/21 21016520 96 % 0.1 SM 2540 G (1997) MMSD
08/10/21 21017148 96 % 0.1 SM 2540 G (1997) MMSD
08/24/21 21018406 96 % 0.1 SM 2540 G (1997) MMSD
08/31/21 21018961 96 % 0.1 SM 2540 G (1997) MMSD
09/07/21 21019296 96 % 0.1 SM 2540 G (1997) MMSD
09/14/21 21019839 96 % 0.1 SM 2540 G (1997) MMSD 149919-1
09/21/21 21020475 95 % 0.1 SM 2540 G (1997) MMSD 150073-1
09/28/21 21021002 96 % 0.1 SM 2540 G (1997) MMSD 150186-1
10/20/21 21022830 98 % 0.1 SM 2540 G (1997) MMSD 150588-1
10/26/21 21023248 97 % 0.1 SM 2540 G (1997) MMSD 150695-1
11/09/21 21024070 95 % 0.1 SM 2540 G (1997) MMSD 150928-1
11/16/21 21024363 95 % 0.1 SM 2540 G (1997) MMSD 151030-1
11/23/21 21024720 90 % 0.1 SM 2540 G (1997) MMSD 151161-1
11/30/21
12/07/21
12/14/21
21025009
21025371
21025593
96 % 0.1
SM 2540 G (1997) MMSD 151264-1
93 % 0.1
SM 2540 G (1997) MMSD 151388-1
95 % 0.1
SM 2540 G (1997) MMSD 151514-1
12/21/21 21026062 94 % 0.1 SM 2540 G (1997) MMSD 151632-1
12/28/21 21026149 94 % 0.1 SM 2540 G (1997) MMSD 151708-1
Page 117 of 121
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MMSD
PARTNERS F(t A CLIMB E1n)OOMli1M1
Solids (% Total)
Sample Date S:
Avg Result: 95 %
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite (Outfall 006) PRODUCTION
QC Batch
ID
FECAL COLIFORM SLUDGE
Min LOD: 0.1 %
Max Result: 98 %
Max LOD: 0.1 %
Milorganite (Outfall 009) BAGGING
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
Lab
QC Batch
ID
01/05/21
21000712
1.4 MPN/g TS
0.19
EPA 1680
MMSD
02/09/21
21002802
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
03/09/21 21004571
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
04/13/21 21006932
1.1 MPN/g TS 0.19
EPA 1680
MMSD
05/11/21 21009269
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
06/08/21 21011272
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
07/13/21 21014464
2.1 MPN/g TS 1.9
Q2.
EPA 1680 MMSD
08/17/21 21017789
14 MPN/g TS 0.19
EPA 1680 MMSD
08/24/21 21018407
0.47 MPN/g TS 0.19
EPA 1680 MMSD
09/14/21 21019841
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150008-1
10/26/21 21023250
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150774-1
11/09/21 21024074
< 1.9 MPN/g TS 1.9
EPA 1680
MMSD 150983-1
12/14/21 21025597
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151598-1
Min LOD: 0.19 MPN/g TS
Solids (% Total)
Max LOD: 1.9 MPN/g TS
Samp e Date Sample ID
Result LOD LOQ QA Flags Analytical Method
Lab
QC Batch
ID
01/05/21
21000712
95 %
0.1
SM 2540 G (1997)
MMSD
02/09/21
21002802
94 % 0.1
SM 2540 G (1997) MMSD
03/09/21 21004571
95 % 0.1
SM 2540 G (1997) MMSD
04/13/21 21006932
94 % 0.1
SM 2540 G (1997) MMSD
05/11/21 21009269
95 % 0.1
SM 2540 G (1997) MMSD
06/08/21 21011272
95 % 0.1
SM 2540 G (1997) MMSD
07/13/21 21014464
08/17/21 21017789
94% 0.1
SM 2540 G (1997) MMSD
95 % 0.1
SM 2540 G (1997) MMSD
08/24/21 21018407
95 % 0.1
SM 2540 G (1997) MMSD
09/14/21 21019841
95 % 0.1
SM 2540 G (1997) MMSD 149919-1
10/26/21 21023250
96 % 0.1
SM 2540 G (1997) MMSD 150695-1
11/09/21 21024074
12/14/21 21025597
95 % 0.1
SM 2540 G (1997) MMSD 150928-1
96 % 0.1
SM 2540 G (1997) MMSD 151514-1
Avg Result: 95 %
Min LOD: 0.1 %
Max Result: 98 % Max LOD: 0.1 %
Page 118 of 121
SYS/rptlMiloMonthlyDW 10/21/21 17 Printed: 1/13/22 14.24

MMSD
PARTNERS Ka A CLIMB 1111101110111
FECAL COLIFORM SLUDGE
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite (Outfall 008) SHIPPING
Sample Date Sample ID
Result
LOD LOQ QA Flags
•na Ica 'e o. a.
QC Batch
ID
01/05/21
21000711
2.1 MPN/g TS
1.9
EPA 1680
MMSD
02/09/21
21002801
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
03/09/21 21004570
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
04/13/21 21006931
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
05/11/21 21009268
< 0.19 MPN/g TS 0.19
Q3.
EPA 1680 MMSD
06/08/21 21011271
1.4 MPN/g TS 0.19
EPA 1680 MMSD
07/13/21 21014463
0.47 MPN/g TS 0.19
EPA 1680 MMSD
08/10/21 21017149
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
09/21/21 21020476
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150137-1
10/26/21 21023249
1.1 MPN/g TS 0.19
EPA 1680
MMSD 150774-1
11/09/21 21024073
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150983-1
12/14/21 21025595
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151598-1
Min LOD: 0.19 MPN/g TS
Solids (% Total)
Max LOD: 1.9 MPN/g TS
Sample Date Sample ID
Result
LOD LOQ QA Flags
Analytical Method Lab
QC Batch
ID
01/05/21
21000711
95 %
0.1
SM 2540 G (1997)
MMSD
02/09/21
21002801
94 % 0.1
SM 2540 G (1997) MMSD
03/09/21 21004570
95 % 0.1
SM 2540 G (1997) MMSD
04/13/21 21006931
94 % 0.1
SM 2540 G (1997) MMSD
05/11/21 21009268
95 % 0.1
SM 2540 G (1997) MMSD
06/08/21 21011271
95 % 0.1
SM 2540 G (1997) MMSD
07/13/21 21014463
96 % 0.1
SM 2540 G (1997) MMSD
08/10/21 21017149 96 % 0.1
SM 2540 G (1997) MMSD
09/21/21 21020476 95 % 0.1
SM 2540 G (1997) MMSD 150073-1
10/26/21 21023249 96 % 0.1
SM 2540 G (1997) MMSD 150695-1
11/09/21 21024073 96 % 0.1
SM 2540 G (1997) MMSD 150928-1
12/14/21 21025595 95 % 0.1
SM 2540 G (1997) MMSD 151514-1
Avg Result: 95 % Min LOD: 0.1 %
Max Result: 98 % Max LOD: 0.1 %
Page 119 of 121
SYS/rptlMiloMonthlyDW 10/21/21 17 Printed: 1/13/22 14.24

MMSD
PARTNERS FOI A CLLJ I LY *OU ANI
FECAL COLIFORM SLUDGE
Annual Milorganite Report DW
January 1 to December 31, 2021
Milorganite (Spring Valley) BAGGING
Sample Date Sample ID
Result LOD LOQ QA Flags
na Ica e o
QC Batch
ID
01/26/21
21002185
0.21 MPN/g TS
0.19
EPA 1680
MMSD
03/09/21
21004562
<0.19MPN/gTS 0.19
EPA 1680
MMSD
04/13/21 21006927
4.9 MPN/g TS 0.19
EPA 1680
MMSD
05/11/21 21009233
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD
06/08/21 21011242
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
07/13/21 21014418
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
08/10/21 21017140
< 0.19 MPN/g TS 0.19
EPA 1680 MMSD
09/14/21 21019846
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 150008-1
10/26/21 21023242
< 1.9 MPN/g TS 1.9
EPA 1680
MMSD 150774-1
12/07/21 21025357
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151459-1
12/14/21 21025590
< 0.19 MPN/g TS 0.19
EPA 1680
MMSD 151598-1
Min LOD: 0.19 MPN/g TS
Solids (% Total)
Max LOD: 1.9 MPN/g TS
Sample Date Sample ID
Result LOD LOQ QA Flags Analytical Method
Lab
QC Batch
ID
01/26/21
21002185
94 %
0.1
SM 2540 G (1997)
MMSD
03/09/21
21004562
95 % 0.1
SM 2540 G (1997) MMSD
04/13/21 21006927
95 % 0.1
SM 2540 G (1997) MMSD
05/11/21 21009233
95 % 0.1
SM 2540 G (1997) MMSD
06/08/21 21011242
95 % 0.1
SM 2540 G (1997) MMSD
07/13/21 21014418
95 % 0.1
SM 2540 G (1997) MMSD
08/10/21 21017140
96 % 0.1
SM 2540 G (1997) MMSD
09/14/21 21019846
95 % 0.1
SM 2540 G (1997) MMSD 149919-1
10/26/21 21023242
96 % 0.1
SM 2540 G (1997) MMSD 150695-1
12/07/21 21025357
95 % 0.1
SM 2540 G (1997) MMSD 151388-1
12/14/21 21025590
96 % 0.1
SM 2540 G (1997) MMSD 151514-1
Avg Result: 95 %
Min LOD: 0.1 %
Max Result: 98 % Max LOD: 0.1 %
Page 120 of 121
SYS/rptlMiloMonthlyDW 10/21/21 17 Printed: 1/13/22 14.24

MMSD
PARTNERS F01 A CLEANER WON11[11l
Annual Milorganite Report DW
January 1 to December 31, 2021
Flag Descriptions
AO Other -- Flag requires additional explanation.
IS Insufficient sample volume for analysis.
AX Qualified data - see contract laboratory report.
B3 Target analyte detected in method blank > 10% of sample
concentration.
B7 LCS recovery was above control limits.
] Estimated concentration above the adjusted method detection limit
and below the adjusted Limit of Quantification.
LA Not analyzed - laboratory accident.
M1 Too numerous to count.
B8 LCS recovery was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits.
131 Duplicate precision control limit was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not allow completing the analysis.
D5 The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
Hi Sample was received past holding time.
H3 Analysis performed beyond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
H5 Analysis performed beyond holding time.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to spreading colonies.
M5 Incubator/water bath temperature was outside method
requirements.
M7 Microbiology sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data (Water Quality only).
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
S5 Reading was not confirmed by a constant weight measurement.
S6 Dried solid residue yield outside of method specifications (<2.5mg
or >200mg).
SD Supplemental details provided (Water Quality only).
T3 The BOD dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
T5 GGA BOD was above method acceptance criteria.
T6 Sample supersaturated with dissolved oxygen for BOD analysis.
T7 The BOD dilution water D.O. increase was > 0.2 mg/L.
T8 Sample matrix did not allow adjusting sample pH for BOD.
T9 Sample is outside of the prescribed method temperature range.
Page 121 of 121
SYS/rptlMiloMonthlyDW 10/21/21 17 Printed: 1/13/22 14.24

PARTNERS FOR A CLEANER ENVIRONMENT
January 13, 2022
TO:
FROM:
COPY:
SUBJECT:
Memorandum
Tom Nowicki and Steve Unger
Zach Vogel
Laboratory Project Manager
S. Mertens, A. Sotomayor, E. Guyant, K. Walden, E. Stroik, P. Bechler, Lab File
2021 Annual Milorganite PCB Report
Attached is the Annual PCB Milorganite report for the year 2021. Daily Milorganite samples are 24-hour
composite samples, representative of a full day of production. All analyses were performed by Pace Analytical
Services, Inc. in Green Bay, WI (Wisconsin Certification #: 405132750). Full laboratory results are available upon
request.
There was no Milorganite production on the following dates:
• May 24, 2021
• May 31, 2021
• June 15 through June 17, 2021
• August 29, 2021
• October 5, 2021
• October 9 through October 18, 2021
Data/Report Review By:
/ `'✓` ffi,; 1-/3-Zo2z
Zach Vogel Date
Laboratory Project Manager
Milwaukee Metropolitan Sewerage District
260 West Seeboth Street, Milwaukee, WI 53204

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
DrP_17A7 DrP_17SA DrP_1771 DrP_1727 DrP_17AR DrP_17an DfP_1/11A Tnl I DfP Arnrinr
1/1/21 < 32 32 < 32 < 32 < 32 < 32 < 32 32
1/2/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
1/3/21 < 32 33 < 32 < 32 < 32 < 32 < 32 33
1/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/5/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/6/21 < 32 36 < 32 < 32 < 32 < 32 < 32 36
1/7/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
1/8/21 < 32 41 < 32 < 32 < 32 < 32 < 32
1/9/21 < 33 47 < 33 < 33 < 33 < 33 < 33
1/10/21 < 33 40 < 33 < 33 < 33 < 33 < 33 40
1/11/21 < 32 42 < 32 < 32 < 32 < 32 < 32
1/12/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/13/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/14/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/15/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/16/21 < 32 34 < 32 < 32 < 32 < 32 < 32
1/17/21 < 33 34 < 33 < 33 < 33 < 33 < 33
1/18/21 < 33 35 < 33 < 33 < 33 < 33 < 33 35
1/19/21 < 33 39 < 33 < 33 < 33 < 33 < 33
1/20/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/21/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/22/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/23/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/24/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/25/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/26/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
1/27/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/28/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
1/29/21 < 32 40 < 32 < 32 < 32 < 32 < 32
1/30/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
1/31/21 < 33 45 < 33 < 33 < 33 < 33 < 33
2/1/21 < 32 44 < 32 < 32 < 32 < 32 < 32
2/2/21 < 32 40 < 32 < 32 < 32 < 32 < 32
2/3/21 < 32 36 < 32 < 32 < 32 < 32 < 32 36
2/4/21 < 32 41 < 32 < 32 < 32 < 32 < 32
2/5/21 < 32 39 < 32 < 32 < 32 < 32 < 32
2/6/21 < 32 44 < 32 < 32 < 32 < 32 < 32
2/7/21 <31 41 <31 <31 <31 <31 <31 41
2/8/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/9/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/10/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/11/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/12/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33
2/13/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/14/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/15/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/16/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/17/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
< 32
< 33
41
47
42
< 32
< 32
< 32
34
34
39
< 32
< 32
< 33
< 33
< 33
< 32
< 32
40
45
44
40
41
39
44
< 32
< 32
< 33
< 32
< 32

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
DrP_17A7 DrP_17SA DrP_1771 DrP_1727 DrP_17AR DrP_17an DfP_1/11A Tnl I DfP Arnrinr
2/18/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
2/19/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/20/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/21/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/22/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/23/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/24/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/25/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33
2/26/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/27/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
2/28/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/1/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/2/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/3/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/5/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/6/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/7/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/8/21 < 32 40 < 32 < 32 < 32 < 32 < 32
3/9/21 < 32 36 < 32 < 32 < 32 < 32 < 32
3/10/21 < 32 32 < 32 < 32 < 32 < 32 < 32
3/11/21 < 32 44 < 32 < 32 < 32 < 32 < 32 44
3/12/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/13/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/14/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/15/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/16/21 < 32 38 < 32 < 32 < 32 < 32 < 32
3/17/21 < 32 49 < 32 < 32 < 32 < 32 < 32
3/18/21 < 32 36 < 32 < 32 < 32 < 32 < 32
3/19/21 < 32 53 < 32 < 32 < 32 < 32 < 32 53
3/20/21 < 32 54 < 32 < 32 < 32 < 32 < 32
3/21/21 < 32 50 < 32 < 32 < 32 < 32 < 32
3/22/21 < 32 44 < 32 < 32 < 32 < 32 < 32
3/23/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/24/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/25/21 < 32 34 < 32 < 32 < 32 < 32 < 32
3/26/21 < 32 33 < 32 < 32 < 32 < 32 < 32
3/27/21 < 32 33 < 32 < 32 < 32 < 32 < 32 33
3/28/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
3/29/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/30/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
3/31/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/1/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/2/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/3/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/5/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/6/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
< 32
< 32
< 33
< 32
< 32
< 32
< 32
< 32
< 32
< 32
40
36
32
< 32
< 32
< 32
38
49
36
54
50
44
< 32
34
33
< 32
< 32
< 32
< 32
< 32

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
DrP_17A7 DrP_17SA DrP_1771 DrP_1727 DrP_17AR DrP_17an DfP_1/11A Tnl I DfP Arnrinr
4/7/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/8/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/9/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/10/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/11/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/12/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/13/21 < 32 42 < 32 < 32 < 32 < 32 < 32 42
4/14/21 < 32 33 < 32 < 32 < 32 < 32 < 32
4/15/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/16/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/17/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/18/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33
4/19/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33
4/20/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
4/21/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/22/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/23/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/24/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/25/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/26/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/27/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/28/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/29/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
4/30/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/1/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/2/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/3/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/5/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/6/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/7/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/8/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/9/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/10/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
5/11/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/12/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/13/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/14/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/15/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/16/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/17/21 < 32 38 < 32 < 32 < 32 < 32 < 32
5/18/21 < 32 < 32 < 32 < 32 < 32 55 < 32 55
5/19/21 < 32 38 < 32 < 32 < 32 < 32 < 32
5/20/21 < 32 34 < 32 < 32 < 32 < 32 < 32
5/21/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33
5/22/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
5/23/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/25/21 < 32 39 < 32 < 32 < 32 < 32 < 32 39
< 32
< 32
33
< 32
< 32
< 33
< 33
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
38
38
34
< 33

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
DrP_17A7 DrP_17SA DrP_1771 DrP_1727 DrP_17AR DrP_17an DfP_1/11A Tnl I DfP Arnrinr
5/26/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/27/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/28/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/29/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
5/30/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/1/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/2/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/3/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/5/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/6/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/7/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/8/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33
6/9/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/10/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/11/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/12/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/13/21 < 33 < 33 < 33 < 33 < 33 < 33 < 33 < 33
6/14/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/18/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/19/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/20/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/21/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/22/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/23/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/24/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/25/21 < 32 38 < 32 < 32 < 32 < 32 < 32
6/26/21 < 33 48 < 33 < 33 < 33 < 33 < 33
6/27/21 < 32 44 < 32 < 32 < 32 < 32 < 32
6/28/21 < 32 40 < 32 < 32 < 32 36 < 32 75
6/29/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
6/30/21 < 32 46 < 32 < 32 < 32 < 32 < 32
7/1/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
7/2/21 < 32 34 < 32 < 32 < 32 < 32 < 32 34
7/3/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
7/4/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
7/5/21 < 32 < 32 < 32 < 32 < 32 < 32 < 32
7/6/21 < 32 33 < 32 < 32 < 32 < 32 < 32 33
7/7/21 < 32 39 < 32 < 32 < 32 < 32 < 32 39
7/8/21 < 32 34 < 32 < 32 < 32 < 32 < 32
7/9/21 41 37 < 32 < 32 < 32 < 32 < 32
7/10/21 39 34 < 32 < 32 < 32 < 32 < 32 73
7/11/21 40 34 < 32 < 32 < 32 < 32 < 32
7/12/21 36 43 < 32 < 32 < 32 < 32 < 32
7/13/21 41 34 < 32 < 32 < 32 < 32 < 32
7/14/21 60 37 < 32 < 32 < 32 < 32 < 32 97
7/15/21 51 42 < 32 < 32 < 32 < 32 < 32 92
7/16/21 45 35 < 32 < 32 < 32 < 32 < 32 80
< 32
< 32
< 32
< 32
< 32
< 32
< 33
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
< 32
38
48
44
< 32
46
< 32
< 32
< 32
< 32
34
78
74
79
74

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
DrP_17A7 DrP_17SA DrP_1771 DrP_1727 DrP_17AR DrP_17an DfP_1/11A Tnl I DfP Arnrinr
7/17/21 49 39 < 32 < 32 < 32 < 32 < 32 88
7/18/21 58 38 < 32 < 32 < 32 < 32 < 32 96
7/19/21 67 47 < 32 < 32 < 32 < 32 < 32 110
7/20/21 79 73 < 32 < 32 < 32 < 32 < 32
7/21/21 80 59 < 32 < 32 < 32 < 32 < 32
7/22/21 86 55 < 32 < 32 < 32 < 32 < 32 140
7/23/21 71 49 < 32 < 32 < 32 < 32 < 32 120
7/24/21 88 54 < 32 < 32 < 32 < 32 < 32
7/25/21 96 56 < 32 < 32 < 32 < 32 < 32
7/26/21 100 52 < 32 < 32 < 32 < 32 < 32 160
7/27/21 96 56 < 32 < 32 < 32 < 32 < 32
7/28/21 100 64 < 32 < 32 < 32 < 32 < 32
7/29/21 100 56 < 32 < 32 < 32 < 32 < 32
7/30/21 93 56 < 32 < 32 < 32 < 32 < 32 150
7/31/21 120 59 < 32 < 32 < 32 < 32 < 32
8/1/21 93 54 < 32 < 32 < 32 < 32 < 32
8/2/21 120 74 < 32 < 32 < 32 < 32 < 32
8/3/21 110 54 < 32 < 32 < 32 < 32 < 32 160
8/4/21 110 53 < 32 < 32 < 32 < 32 < 32
8/5/21 110 58 < 32 < 32 < 32 < 32 < 32
8/6/21 100 50 < 32 < 32 < 32 < 32 < 32
8/7/21 110 49 < 32 < 32 < 32 < 32 < 32 160
8/8/21 92 44 < 32 < 32 < 32 < 32 < 32
8/9/21 120 72 < 32 < 32 < 32 < 32 < 32
8/10/21 97 64 < 32 < 32 < 32 < 32 < 32
8/11/21 120 80 < 32 < 32 < 32 33 < 32 230
8/12/21 110 100 < 32 < 32 < 32 < 32 < 32
8/13/21 99 70 < 32 < 32 < 32 < 32 < 32
8/14/21 86 70 <31 <31 <31 <31 <31
8/15/21 85 71 <31 <31 <31 <31 <31 160
8/16/21 95 60 <31 <31 <31 <31 <31
8/17/21 82 59 <31 <31 <31 <31 <31
8/18/21 73 72 < 31 < 31 < 31 35 < 31
8/19/21 70 62 < 32 < 32 < 32 34 < 32 160
8/20/21 120 68 < 32 < 32 < 32 < 32 < 32
8/21/21 120 80 < 32 < 32 < 32 < 32 < 32
8/22/21 130 84 < 32 < 32 < 32 < 32 < 32
8/23/21 130 92 < 32 < 32 < 32 < 32 < 32 220
8/24/21 140 110 < 32 < 32 < 32 44 < 32 300
8/25/21 120 93 < 32 < 32 < 32 < 32 < 32
8/26/21 110 82 < 32 < 32 < 32 < 32 < 32
8/27/21 100 94 < 32 < 32 < 32 < 32 < 32 200
8/28/21 100 100 < 32 < 32 < 32 < 32 < 32
8/30/21 89 51 < 32 < 32 < 32 35 < 32
8/31/21 57 61 < 32 < 32 < 32 < 32 < 32
9/1/21 77 84 < 32 < 32 < 32 < 32 < 32 160
9/2/21 61 65 < 32 < 32 < 32 < 32 < 32 130
9/3/21 65 61 < 32 < 32 < 32 < 32 < 32 130
150
140
140
150
150
170
160
180
150
190
160
160
150
140
190
160
220
170
160
160
140
180
190
200
220
220
190
200
180
120

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
DrP_17A7 DrP_17SA DrP_1771 DrP_1727 DrP_17AR DrP_17an DfP_1/11A Tnl I DfP Arnrinr
9/4/21 55 69 < 32 < 32 < 32 < 32 < 32 120
9/5/21 52 60 < 32 < 32 < 32 < 32 < 32 110
9/6/21 57 60 < 32 < 32 < 32 < 32 < 32 120
9/7/21 87 71 < 32 < 32 < 32 < 32 < 32
9/8/21 88 88 < 32 < 32 < 32 < 32 < 32
9/9/21 82 68 < 32 < 32 < 32 < 32 < 32 150
9/10/21 59 57 < 32 < 32 < 32 < 32 < 32 120
9/11/21 53 58 < 32 < 32 < 32 < 32 < 32
9/12/21 46 54 < 32 < 32 < 32 < 32 < 32
9/13/21 40 53 < 32 < 32 < 32 < 32 < 32 93
9/14/21 45 55 < 32 < 32 < 32 < 32 < 32
9/15/21 32 48 < 32 < 32 < 32 < 32 < 32
9/16/21 88 78 < 32 < 32 < 32 < 32 < 32
9/17/21 51 52 < 33 < 33 < 33 < 33 < 33 100
9/18/21 52 55 < 32 < 32 < 32 < 32 < 32
9/19/21 36 55 < 32 < 32 < 32 < 32 < 32
9/20/21 60 70 < 32 < 32 < 32 < 32 < 32
9/21/21 79 61 < 32 < 32 < 32 < 32 < 32 140
9/22/21 57 48 < 32 < 32 < 32 < 32 < 32
9/23/21 57 65 < 32 < 32 < 32 < 32 < 32
9/24/21 61 75 < 32 < 32 < 32 < 32 < 32
9/25/21 54 71 < 32 < 32 < 32 < 32 < 32 120
9/26/21 79 100 < 56 < 56 < 56 < 56 < 56
9/27/21 56 70 < 32 < 32 < 32 < 32 < 32
9/28/21 56 69 < 32 < 32 < 32 < 32 < 32
9/29/21 58 69 < 32 < 32 < 32 < 32 < 32 130
9/30/21 53 71 < 32 < 32 < 32 < 32 < 32
10/1/21 38 50 < 32 < 32 < 32 < 32 < 32
10/2/21 37 52 < 32 < 32 < 32 < 32 < 32
10/3/21 63 86 < 32 < 32 < 32 < 32 < 32 150
10/4/21 79 98 < 32 < 32 < 32 < 32 < 32
10/6/21 46 82 < 32 < 32 < 32 32 < 32
10/7/21 43 74 < 32 < 32 < 32 < 32 < 32
10/8/21 50 71 < 31 < 31 < 31 < 31 < 31 120
10/19/21 <31 38 <31 <31 <31 <31 <31
10/20/21 49 42 < 32 < 32 < 32 < 32 < 32
10/21/21 < 32 40 < 32 < 32 < 32 < 32 < 32
10/22/21 32 38 < 32 < 32 < 32 < 32 < 32 70
10/23/21 < 32 42 < 32 < 32 < 32 < 32 < 32 42
10/24/21 < 32 38 < 32 < 32 < 32 < 32 < 32
10/25/21 < 32 38 < 32 < 32 < 32 < 32 < 32
10/26/21 34 44 < 32 < 32 < 32 < 32 < 32 78
10/27/21 < 32 35 < 32 < 32 < 32 < 32 < 32
10/28/21 < 32 32 < 32 < 32 < 32 < 32 < 32
10/29/21 41 36 < 32 < 32 < 32 42 < 32
10/30/21 41 40 < 32 < 32 < 32 48 < 32 130
10/31/21 44 43 < 32 < 32 < 32 46 < 32 130
11/1/21 < 32 44 < 32 < 32 < 32 < 32 < 32 44
160
180
110
100
100
80
170
110
91
130
100
120
140
180
130
120
120
88
89
180
160
120
38
91
40
38
38
35
32
120

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
DrP_17A7 DrP_17SA DrP_1771 DrP_1727 DrP_17AR DrP_17an DfP_1/11A Tnl I DfP Arnrinr
11/2/21 < 33 55 < 33 < 33 < 33 < 33 < 33 55
11/3/21 < 32 56 < 32 < 32 < 32 < 32 < 32 56
11/4/21 < 32 53 < 32 < 32 < 32 < 32 < 32 53
11/5/21 < 32 47 < 32 < 32 < 32 < 32 < 32
11/6/21 < 32 46 < 32 < 32 < 32 < 32 < 32
11/7/21 < 32 52 < 32 < 32 < 32 < 32 < 32 52
11/8/21 33 44 < 32 < 32 < 32 < 32 < 32 77
11/9/21 < 32 43 < 32 < 32 < 32 < 32 < 32
11/10/21 < 33 59 < 33 < 33 < 33 < 33 < 33
11/11/21 < 33 65 < 33 < 33 < 33 < 33 < 33 65
11/12/21 < 32 57 < 32 < 32 < 32 < 32 < 32
11/13/21 < 32 61 < 32 < 32 < 32 < 32 < 32
11/14/21 < 32 55 < 32 < 32 < 32 < 32 < 32
11/15/21 < 32 35 < 32 < 32 < 32 < 32 < 32 35
11/16/21 < 32 47 < 32 < 32 < 32 < 32 < 32
11/17/21 < 32 85 < 32 < 32 < 32 < 32 < 32
11/18/21 < 32 58 < 32 < 32 < 32 < 32 < 32
11/19/21 38 65 < 32 < 32 < 32 < 32 < 32 100
11/20/21 < 32 63 < 32 < 32 < 32 < 32 < 32
11/21/21 < 32 57 < 32 < 32 < 32 < 32 < 32
11/22/21 < 33 56 < 33 < 33 < 33 < 33 < 33
11/23/21 < 33 49 < 33 < 33 < 33 < 33 < 33 49
11/24/21 < 32 47 < 32 < 32 < 32 < 32 < 32
11/25/21 < 32 46 < 32 < 32 < 32 < 32 < 32
11/26/21 < 32 46 < 32 < 32 < 32 < 32 < 32
11/27/21 < 33 41 < 33 < 33 < 33 < 33 < 33 41
11/28/21 < 32 48 < 32 < 32 < 32 < 32 < 32
11/29/21 < 32 49 < 32 < 32 < 32 < 32 < 32
11/30/21 < 32 47 < 32 < 32 < 32 < 32 < 32
12/1/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
12/2/21 < 32 44 < 32 < 32 < 32 < 32 < 32
12/3/21 < 32 48 < 32 < 32 < 32 < 32 < 32
12/4/21 < 32 46 < 32 < 32 < 32 < 32 < 32
12/5/21 < 33 45 < 33 < 33 < 33 < 33 < 33 45
12/6/21 < 32 50 < 32 < 32 < 32 < 32 < 32
12/7/21 < 33 43 < 33 < 33 < 33 < 33 < 33
12/8/21 < 32 43 < 32 < 32 < 32 < 32 < 32
12/9/21 < 33 36 < 33 < 33 < 33 < 33 < 33 36
12/10/21 < 32 39 < 32 < 32 < 32 < 32 < 32 39
12/11/21 < 32 35 < 32 < 32 < 32 < 32 < 32
12/12/21 <31 40 <31 <31 <31 <31 <31
12/13/21 < 32 46 < 32 < 32 < 32 < 32 < 32 46
12/14/21 < 32 44 < 32 < 32 < 32 < 32 < 32
12/15/21 < 32 46 < 32 < 32 < 32 < 32 < 32
12/16/21 < 32 48 < 32 < 32 < 32 < 32 < 32
12/17/21 < 32 50 < 32 < 32 < 32 < 32 < 32 50
12/18/21 < 32 48 < 32 < 32 < 32 < 32 < 32 48
12/19/21 < 33 41 < 33 < 33 < 33 < 33 < 33 41
47
46
43
59
57
61
55
47
85
58
63
57
56
47
46
46
48
49
47
44
48
46
50
43
43
35
40
44
46
48

2021 Milorganite Daily Production Samples
COLLECTION DATE PCB Aroclors (ug/kg D.W.)1
PCR-17117 PCR-17Sa PCR-1771 PCR-1737 PCR-1711R PCR-17F11 PCR-1(11F TntaI PCR Arnrinrc
12/20/21
12/21/21
12/22/21
12/23/21
12/24/21
12/25/21
12/26/21
12/27/21
12/28/21
12/29/21
12/30/21
12/31/21
C
35 45 < 33 < 33
34 36 < 33 < 33
36 34 < 33 < 33
< 33 58 < 33 < 33
< 33 50 < 33 < 33
< 33 53 < 33 < 33
< 33 50 < 33 < 33
< 32 48 < 32 < 32
< 32 35 < 32 < 32
< 33 41 < 33 < 33
< 32 38 < 32 < 32
< 32 42 < 32 < 32
< 33 < 33 < 33 80
< 33 < 33 < 33 71
< 33 < 33 < 33 70
< 33 < 33 < 33 58
< 33 < 33 < 33 50
< 33 < 33 < 33 53
< 33 < 33 < 33 50
< 32 < 32 < 32 48
< 32 < 32 < 32 35
< 33 < 33 < 33 41
< 32 < 32 < 32 38
< 32 < 32 < 32 42
'Samples analyzed by Pace Analytical Services, Green Bay, Wisconsin (WI Certification #405132750) by EPA 8082. All
results reported on a dry weight basis.

APAW FR A CUM EMPIRIC
964
3/20/21 SU
Site Cade
Semple Date
WMC12
CuetanerID
Milorganite Priority Pollutants: Spring 2021
Milo. Priority Pollutant Sample
21004580
LIMS Number
OpSID Test Name Reported Value
MDL LOQ Flags Analysis Date Method Lab S
1253
1315 1,2-Diphenylhydrazlne Dry wt. < 960 ug/kg D.W.
1234 2,4,6-Tr chlarophenol Dry wt. < 1700 ug/kg D.W.
1226 2,4-Dichiorophenol Dry cat < 910 ug/kg D.W. 910 8600
1227 2,4-DimethylphenoI Dry wt < 2100 ug/kg D.W.
1,2,4-Trlchlorobenzene Dry wt
< 1200 ug/kg D.W.
1200
960 17000
1700 8600
17000
3/26/21 8270D
3/26/21 8270D
Test America B 3
Test America B 3
3/26/21 8270D
Test America B 3
1229 2,4-Dinitrophenol Dry wt < 40000 ug/kg D.W.
1252 2,4-Dinitrotoluene Dry wt < 1800 ug/kg D.W.
3/26/21 8270D
2100 8600 3/26/21 8270D
40000 84000 _ 3/26/21 8270D
1800 8600 3/26/21 8270D Test America B 3
Test America B 3
Test America B 3
Test America B 3
1317 2,6-Dlni rotoluene Dry wt < 1000 ug/kg D.W. 1000 8600 3/26/21 8270D Test America B 3
1249 2-Chloronaphthalene Dry wt. < 1400 ug/kg D.W. 1400 8600 3/26/21 8270D Test America B 3
1225 2-Chlorophenol Dry wt. < 1600 ug/kg D.W. 1600 17000 3/26/21 8270D Test America B 3
1230 2-Nltrophenol Dry wt < 2400 ug/kg D.W. 2400 8600 _ _ _ 3/26/21 8270D Test America B 3
1324 3,3'-Dichlorobenzidine Dry wt < 10000 ug/kg D.W. 10000 17000 3/26/21 8270D Test America B 3
1260 4,4-DDD Dry cat < 6.7 ug/kg D.W. 6.7 35 3/29/21 8081E Test America B 3
1259 4,4-DDE Dry wt < 7.3 ug/kg D.W. 7.3 35 3/29/21 80818 Test America B 3
4,4-DDT Dry cat < 8.1 ug/kg D.W. 8.1 35 3/29/21 80818 Test America B 3
4,6-Dinitro-o-Cresol Dry wt < 8600 ug/kg D.W. 8600 17000 3/26/21 8270D Test America B 3
4-Bromophenyl Phenyl Ether Dry wt < 1200 ug/kg D.W. 1200 8600 3/26/21 8270D Test America 8 3
4-Chloro-phenyl-phenyl ether Dry wt< 1100 ug/kg D.W. 1100 8600 3/26/21 8270D Test America B 3
1258
1228
1247
1250
1231
1254
1235
1318
1304
4-Nitrophenol Dry wt. < 6000 ug/kg D.W. 6000 17000
A-BHC-Alpha Dry wt. < 6.2 ug/kg D.W. 6.2 35
3/26/21 8270D Test America B 3
3/29/21 8081B
Acenaphthene Dry wt. < 1300 ug/kg D.W. 1300 8600
3/26/21 8270D
Acenaphthylene Dry wt. < 1100 ug/kg D.W. 1100
Aldrin Dry wt. < 8.5 ug/kg D.W. 8.5
524 ALUMINUM ICP Dry wt 3200 mg/kg D.W. 4.4
8600
35
10 AX 4/6/21 6010C Test America B 3
3/26/21 8270D
3/29/21 8081E
Test America B 3
Test America B 3
Test America B 3
Test America B 3
1236 Anthraoene Dry wt.
< 2100 ug/kg D.W.
2100 8600
545 ANTIMONY ICP Dry wt
3/26/21 8270D
Test America B 3
< 0.4 mg/kg D.W. 0.4 15 4/6/21 6010C
525 ARSENIC ICP Dry wt
1255
1237
1238
1239
1240
1241
1242
528
1256
1243
1244
1245
1246
Test America B 3
3 mg/kg D.W. 0.4 2 4/6/21 6010C
B-BHC-Beta Dry wt.
Benridine Dry wt.
Benzo(a)Anthracene Dry wt.
Test America B 3
< 6.2 ug/kg D.W. 6.2 35 3/29/21 80818
< 110000 ug/kg D.W. 110000 250000 3/26/21 8270D
Test America B 3
Test America 8 3
< 860 ug/kg D.W. 860 B600 3/26/21 8270D Test America B 3
1300 8600 3/26/21 8270D Test America B 3
Benzo(a)Pyrene Dry wt. < 1300 ug/kg D.W.
Benzo(b)Fluorantmene Dry wt. < 1400 ug/kg D.W. 1400 8600 3/26/21 8270D Test America B 3
Benzo(g,h,i)Perylene Dry wt. < 910 ug/kg D.W.
910 8600 3/26/21 8270D Test America B 3
Benzo(k)Fluorantmene Dry wt. < 1100 ug/kg D.W. 1100 8600 3/26/21 8270D Test America B 3
BERYLLIUM ICP Dry wt. 0.063 mg/kg D.W.
BHC-Delta Dry wt < 6.4 ug/kg D.W.
0.028 0.2 J 4/6/21 6010C Test America B 3
6.4 35 3/29/21 8081E Test America B 3
BIs(2-Chloroethoxy)Methane Dry wt < 1800 ug/kg D.W. 1800 8600 3/26/21 8270D Test America B 3
B1s(2-Ombroethyl)Ether Dry wt. < 1100 ug/kg D.W. 1100 8600 3/26/21 8270D Test America B 3
Bis(2-thlorolsopropyt)Ether Dry wt. < 1700 ug/kg D.W.
Bls(2-Ethylhexyl)Phthatate Dry wt. 7800 ug/kg D.W.
526 BORON ICP Dry wt. 14 mg/kg Q.W.
1700 8600 3/26/21 8270D Test America B 3
2900 8600 ] 3/26/21 8270D Test America B 3
0.19 2 4/6/21 6010C Test America B 3
1248 Butyl Benzyl Phthalate Dry wt. < 1400 ug/kg D.W. 1400 8600 3/26/21 8270D Test America B 3
530 CADMIUM ICP Dry wt < 0.03 mg/kg D.W.
529 CALCIUM ICP Dry wt
SYShp15Generie3 4/11/14 q
0.03 0.2 4/6/21 6010C Test America B 3
14000 mg/kg D.W. 3.3 50 AX. 4/6/21 6010C Test America B 3
Page 1 ors
Printed: 71 21 12:45

Milorganite Priority Pollutants: Spring 2021
MSD
PAI1%03 IRA CWS tlrnicir Blr
1305 Chlordane Dry wt. < 77 ug/kg D.W. 77 350 3/29/21 8081E Test America B 3
532 CHROMIUM ICP Dry wt. 210 mg/kg D.W. 0.2 0.5 4/6/21 6010C Test America B '
1251 Chrysene Dry wt. < 1900 ug/kg D.W. 1900 8600 3/26/21 8270D Test America 8 I
531 COBALT ICP Dry wt. 2.5 mg/kg D.W. 0.05 0.5 4/6/21 6010C Test America B 3
533 COPPER ICP Dry wt. 180 mg/kg D.W. 0.21 1 4/6/21 6010C Test America B 3
263 Cyanide - Total (solids) 4.4 mg/kg D.W. 0.45 0.94 3/30/21 9012E Test America B 3
1325 Dibenzo(a,h)Anthracene Dry wt. < 1500 ug/kg D,W, 1500 8600 3/26/21 8270D Test America B 3
1306 Dleidrin Dry wt. < 8.3 ug/kg D.W. 8.3 35 3/29/21 8081E Test America B 3
1314 Diethyl Phthalate Dry wt < 1100 ug/kg D.W. 1100 8600 3/26/21 8270D Test America B 3
1328 Dimethyl Phthalate Dry wt. < 1000 ug/kg D.W. 1000 8600 3/26/21 8270D Test America B 3
1320 DI-n-Butylphthalabe Dry wt. < 1500 ug/kg D.W. 1500 8600 3/26/21 8270D Test America B 3
1323 Di-n-octyl phthalate Dry wt 2100 ug/kg D.W. 1000 8600 3 3/26/21 8270D Test America B 3
1261 Endosulfan alpha Dry wt. < 6.6 ug/kg D.W. 6.6 35 3/29/21 8081E Test America B 3
1262 - Endosulfan beta Dry wt < 6.2 ug/kg D.W. 6.2 35 3/29/21 8081E Test America B 3
1263 Endosulfan Sulfate Dry wt. < 6.5 ug/kg D.W. 6.5 35 3/29/21 8081E Test America B 3
1265 Endrin Aldehyde Dry wt. < 8.8 ug/kg D.W. 8.8 35 3/29/21 8081E Test America B 3
1264 Endrin Dry wt. < 6.9 ug/kg D.W. 6.9 35 3/29/21 8081B Test America B 3
1321 Fluoranthene Dry wt. < 910 ug/kg D.W. 910 8600 3/26/21 82700 Test America B 3
1316 Fluorene Dry wt. < 1000 ug/kg D.W. 1000 8600 3/26/21 8270D Test America B 3
12- 66 Heptachlor Dry wt < 7.5 ug/kg D.W. 7.5 35 3/29/21 80818 Test America B 3
1267 Heptachforepoxide Dry wt. < 8.9 ug/kg D,W. 8.9 35 3/29/21 8081E Test America B 3
1330 Hexachlorobenzene Dry wt < 1200 ug/kg D.W. 1200 8600 3/26/21 8270D Test America 8 3
1327 Hexachlorobutadiene Dry wt. < 1300 ug/kg Q.W. 1300 8600 3/26/21 8270D Test America B 3
1308 Hexachlorocyclopentadfene Dry wt. < 1200 ug/kg D.W. 1200 8600 3/26/21 8270D Test America B 3
1329 Hexachloroethane Dry wt. < 1100 ug/kg D.W. 1100 8600 3/26/21 8270D Test America B 3
1326 Indeno(1,2,3-cd)Pyrene Dry Wt. < 1100 ug/kg D.W. 1100 8600 3/26/21 8270D Test America B 3
534 IRON ICP Dry wt. 34000 mg/kg D.W. 3.5 10 4/6/21 6010C Test America B 3
1311 Isophorone Dry wt. < 1800 ug/kg D.W. 1800 8600 3/26/21 8270D Test America B 3
544 LEAD ICP Dry wt. 17 mg/kg D.W. 0.24 1 4/6/21 6010C Test America B 3
538 MAGNESIUM ICP Dry wt. 3600 mg/kg D.W. 0.93 20 Ax. 4/6/21 6010C Test America B 3
-
539 MANGANESE ICP Dry wt. 890 mg/kg D.W. 0.032 0.2 M. 4/6/21 6010C Test America B 3
428 MERCURY by M. 7471(sludge) 0.12 mg/kg D.W. 0.015 0.038 AX. 3/25/21 7471E Test America B 3
540 MOLYBDENUM ICP Dry wt. 7.2 mg/kg D.W. 0.13 1 4/6/21 6010C Test America B 3
1312 Naphthalene Dry wt. < 1100 ug/kg D.W. 1100 8600 3/26/21 8270D Test America B 3
542 NICKEL ICP Dry wt. 20 mg/kg D.W. 0.23 5 4/6/21 6010C Test America B 3
1310 Nitrobenzene Dry wt < 960 ug/kg D.W. 960 8600 3/26/21 8270D Test America B 3
1307 N-Nitrasodlmethylamine Dry wt. < 3900 ug/kg D.W. 3900 17000 3/26/21 8270D Test America B 3
1309 N-Nitrosodi-n-propylamine Dry wt. < 1500 ug/kg D.W. 1500 8600 3/26/21 8270D Test America B 3
131- 3 N-Nitrosodiphenylamine Dry wt < 7000 ug/kg D.W. 7000 8600 3/26/21 8270D Test America B 3
678 PCB-1016 < 0.091 mg/kg D.W. 0.091 0.47 3/28/21 8082A Test America B 3
674 PCB-1221 < 0.091 mg/kg D.W. 0.091 0.47 3/28/21 8082A Test America B 3
675 PCB-1232 < 0.091 mg/kg D.W. 0.091 0.47 3/28/21 8082A Test America B 3
672 PCB-1242 < 0.091 mg/kg D.W. 0.091 0.47 3/28/21 8082A Test America B 3
676 PCB-1248 < 0.091 mg/kg D.W. 0.091 0.47 3/28/21 8082A Test America B 3
673 PCB-1254 < 0.22 mg/kg D.W. 0.22 0.47 3/28/21 8082A Test America B 3
677 PCB-1260 < 0.22 mg/kg D.W. 0.22 0.47 3/28/21 8082A Test America B 3
1224 p-Chloro-m-Cresol Dry wt. < 2100 ug/kg D.W. 2100 8600 3/26/21 82700 Test America B 3
1232 Penfathlorophenal Dry wt. < 8600 ug/kg D.W. 8600 17000 3/26/21 8270D Test America B 3
1319 Phenanthrene Dry wt. < 1300 ug/kg D.W. 1300 8600 3/26/21 8270D Test America B 3
1233 Phenol Dry wt < 1300 ug/kg D.W. 1300 8600 3/26/21 8270D Test America B 3
Page 2 of 4
SYSJ9r5Generrc3 4/11/14 4 Prided. 7R/21 12;45

Milorganite Priority Pollutants: Spring 2021
5
WTIIt neAate lni
543 PHOSPHORUS ICP Dry wt. 15000 mg/kg D.W. 140 360 AX 4/6/21 SM 4500 P E Test America B 3
536 POTASSIUM ICP Dry wt. 3200 mg/kg D.W. 20 30 AX. 4/6/21 6010C Test America B 3
1322 Pyrene Dry wt. < 1000 ug/kg D.W. 1000 8600 3/26/21 8270D Test America B 3
546 SELENIUM ICP Dry wt. 5.7 mg/kg D.W. 0.4 4 4/6/21 6010C Test America B 3
523 SILVER ICP Dry wt. 1.8 mg/kg D.W. 0.2 0.6 4/6/21 6010C Test America B 3
541 SODIUM ICP Dry M. 1300 mg/kg D.W. 13 140 4/6/21 6010C Test America B 3
550 THALLIUM ICP Dry wt. < 0.3 mg/kg D.W. 0.3 6 4/6/21 6010C Test America B 3
697 Total PCB Arodors < 0.22 mg/kg D.W. 0.22 0.47 3/28/21 8082A Test America B 3
1268 Toxaphene Dry wt. < 200 ug/kg D.W. 200 350 3/29/21 8081B Test America B 3
1257 Y-BHC-Gamma(Undane) Dry wt. < 6.4 ug/kg D.W. 6.4 _ 35 3/29/21 80818 Test America B 3
552 ZINC ICP Dry wt. 260 mg/kg D.W. 0.64 2 4/6/21 6010C Test America B 3
3122/21
Sample Date
SU
Site Code
Customer ID
21004581
LAMS Number
OpSID Test Name Reported Value r.1L}t. I C:.11
Analysis Date Method
I ,ili
1341
1,1,1-Trichloroe ane Dry wt. 3/27/21 8260C
3/27/21 8260C
3/27/21 8260C
3/27/21 8260C
1336 1,1-Dichloroethylene Dry wt. < 34 ug/kg D.W. 34 3/27/21 8260C
1355 1,2-Dlchlorobenzene Dry Wt. < 25 ug/kg D.W. 25 99 3/27/21 8260C
1340 1,2-Didmloroeihane Dry wt. < 40 ug/kg D.W. 40 99 3/27/21 8260C
1222 1,2-Didtloropropane Dry wt. < 16 ug/kg D.W. 16 99 3/27/21 8260C
1356 1,3-Dichlorobenzene Dry Wt < 26 ug/kg D.W. 26 99 3/27/21 8260C
1357 1,4-Dlchlorobenzene Dry Wt. < 14 ug/kg D.W. 14 99 3/27/21 8260C Test America B 3
1337 2-Chloroethylvinyl Ether Dry wt < 32 ug/kg D.W. 32 490 3/27/21 8260C Test America B 3
1334 Aaolein Dry wt. < 200 ug/kg D.W. 200 490 3/27/21 8260C Test America/3 3
1335 Aaylonitrile Dry wt. < 250 ug/kg D.W. 250 490 3/27/21 8260C Test America 8 3
1346 Benzene Dry wt. < 19 ug/kg D.W. 19 99 3/27/21 8260C Test America B 3
1343 Bromadlchloromethane Dry wt. < 20 ug/kg D.W. 20 99 3/27/21 8260C Test America B 3
1219 8romoform Dry wt. < 49 ug/kg D.W. 49 99 3/27/21 8260C Test America B 3
1342 Carbon Tetrachloride Dry wt. < 25 ug/kg D.W. 25 99 3/27/21 8260C Test America B 3
1352 Chlorobenzene Dry art. < 13 ug/kg D.W. 13 99 3/27/21 8260C Test America B 3
1220 Chloroethane Dry wt. < 21 ug/kg D.W. 21 99 _ 3/27/21 8260C Test America B 3
1339 Chloroform Dry wt. < 68 ug/kg D.W. 68 99 3/27/21 8260C Test America B 3
1344 ds-1,3-Dichloropropene Dry wt. < 24 ug/kg D.W. 24 99 3/27/21 8260C Test America B 3
1347 Dtbromochloromethane Dry wt. < 48 ug/kg D.W. 48 99 3/27/21 8260C Test America B 3
1353 Ethylbenzene Dry wt. < 29 ug/kg D.W. 29 99 3/27/21 8260C Test America B 3
1331 Methyl Bromide Dry wt. < 22 ug/kg D.W. 22 99 3/27/21 8260C Test America B 3
1354 Methyl Chloride dry wt. < 24 ug/kg D.W. 24 99 3/27/21 8260C Test America B 3
1333 Methylene Chloride Dry wt. < 20 ug/kg D.W. 20 99 3/27/21 8260C Test America B 3
1349 Tetrachloroethylene Dry wt. < 13 ug/kg D.W. 13 99 3/27/21 8260C Test America B 3
1351 Toluene Dry wt 120 ug/kg D.W. 26 99 3/27/21 8260C Test America B 3
1221 Trans-1,2-Didmloroethylene Dry wt. < 23 ug/kg D.W. 23 99 3/27/21 8260C Test America B 3
i223 Trans-1,3-Didllorropropene Dry wt. < 9.7 ug/kg D.W. 9.7 99 3/27/21 8260C Test America B 3
1345 Trichloroethylene Dry wt. < 27 ug/kg D.W. 27 99 3/27/21 8260C Test America B 3
1332 Vinyl Chloride Dry M. < 33 ug/kg D.W. 33 99 3/27/21 8260C Test America B 3
1350 1,1,2,2-Tetrachioroethane Dry wt.
1348 1,1,2-Trichloroethane Dry wt.
< 27 ug/kg D.W. 27
< 16 ug/kg D.W. 16
< 21 ug/kg D.W. 21
1338 1,1-Dichloroethane Dry wt.
< 31 ug/kg D.W. 31
99
SYSdp15Bfenedc3 4/11/14 tl
99
99
99
99
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Page 3of4
Printed: 7/9/21 12:45

Milorganite Priority Pollutants: Spring 2021
** The MDL for this test is the lowest level of precision shown, example: 4.1 would be "0.1".
*** The LOQ for this test is the lowest level of precision shown, example: 4.1 would be "0.1".
N.A. The MDL/LOQ is Not Available or Not Applicable for this test.
Column 5: Test Status. Not Started=8, Intermediate=7, Final-3, Analyst Approved 12, Not Reportable=15.
137
Flag DeialipHorrs
AO Other — Flag requires additional explanation.
AX Qualified data • see contract laboratory report.
B3 Target analyte detected In method blank > 10% of sample
concentration.
B7 LCS recovery was above control limits.
B8 LCS recovery was below control limits.
19 Low Level CCV recovery was outside of method atance limits.
Di Duplicate precision control rmlt was exceeded.
D2 Matrix spike precision control limit was exceeded.
D3 Sample Is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practices.
D4 Sample matrix interferences did not a low completing the analysis_
D5 The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed In the method
for the sample volume collected.
Hi Sample was received past holding time.
H3 Analysis performed beyond holding time-
H4 Initial analysis withIn holding time. Reanalysis for the required
dilution was past holding time.
HS Analysis performed beyond holding time.
SYShpt5Generk3 4/11/14 i
IS Insufficient sample volume for analysis.
3 Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit.
LA Not analyzed - laboratory accident.
Mi Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 spreading colonies unable to determine result.
M4 Results are an approximation due to spreading colonies.
MS Incubator/water bath temperature was outside method
requirements
M7 Microbiology sample received without adequate headspace.
M9 Target organism detected in associated method blank.
NR Not usable data (Water Quality only).
NU Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix spike recovery for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
S5 Reading was not confirmed by a constant weight measurement
SD Supplemental details provided (Water Quality only).
T3 The SOD dilution water D.O. depletion was > 0.2 mg/L.
T4 GGA SOD was below method acceptance criteria.
T5 GGA BOD was above method acceptance criteria.
T7 The SOD dilution water D.O. increase was > 0.2 mg/L.
TB Sample matrix did not allow adlustin$ sample pH for BOD.
T9 Sample is outside of the prescribed method temperature range.
Pegs 4of4
Printed: 7/9/21 12:45

hl
MMSD
ME FR Clf6Tht i9+9 IMIEIR
964
9/11/21
Semple Date
SU
Site Code
WMC37
Customer ID
Milorganite Priority Pollutant: Fall 2021
September 5 to 11, 2021
Milo. Priority Pollutant Sample
21019080
LIMS Number
OpSID Test Name
Reported Value
MDL
LOQ
Flags Analysis Date Method Lab S
1253 1,2,4-Trichtorobenzene Dry wt.
< 250 ug/kg D.W.
1315 1,2-01phenyfhydrazine Dry wt.
1234 2,4,6•Trichlorophenol Dry wt.
1226 2,4-Dichlorophenol Dry wt.
< 200 ug/kg D.W.
< 360 ug/kg D.W.
250
3500
9/21/21
200 3500
360 1800
8270D
9/21/21 8270D
9/21/21 8270D
< 190 ug/kg D.W. 190 1800
1227 2,4-DImethylphenol Dry wt
1229 2,4-Dlnitrophenol Dry wt.
1252 2,4-Dfnitrotoluene Dry wt.
1317 2,6-Dinitrotoluene Dry wt.
1249
1225
1230
1324
< 430 ug/kg D.W.
< 8200 ug/kg D.W.
< 370 ug/kg D.W.
< 210 ug/kg D.W.
430 1800
9/21/21 8270D
9/21/21 8270D
8200 17000
9/21/21 8270D
2-Chlaronaphthalene Dry wt
370 1800
210 1800
< 290 ug/kg D.W. 290 1800
2-Chkrcophenol Dry wt.
2-NItrophena1 Dry wt
3,3'-Dichlorobenzldlne Dry wt
< 330 ug/kg D.W.
< 500 ug/kg D.W.
330 3500
500 1800
< 2100 ug/kg D.W. 2100 3500
1260 4,4-DDD Dry wt.
1259 4,4-DDE Dry wt.
1258 4,4-DDT Dry wt.
< 6.6 ug/kg D.W. 6.6
34
< 7.2 ug/kg D.W. 7.2 34
< 8 ug/kg D.W. 8 34
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/21/21 8270D
9/20/21 8081E
9/20/21 80818
9/20/21 8081B
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
1228 4,6-Dinftro-o-Cresol Dry wt. < 1800 ug/kg D.W.
1800 3500
1247 4-Bromophenyt Phenyl Ether Dry wL < 250 ug/kg D.W. 250 1800
9/21/21 8270D
9/21/21 8270D
1250 4-Chloro-phenyl-phenyl ether Dry wt. < 220 ug/kg D.W. 220 1800
1231 4-Nltrophenol Dry wt. < 1200 ug/kg D.W.
Test America B 3
Test America B 3
Test America 8 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America 8 3
Test America B 3
Test America B 3
Test America B 3
9/21/21 8270D
1200 3500
9/21/21 8270D
Test Amerkd B 3
1254 A BHC-Alpha Dry wt. < 6.2 ug/kg D.W. 6.2
1235 Acenaphthene Dry wL < 260 ug/kg D.W. 260
1318 Aoenaphthytene Dry wt. < 230 ug/kg D.W. 230
34
9/20/21 8081E
1800
1800
9/21/21 8270D
9/21/21 8270D
1304 Aldrin Dry wt. < 8.4 ug/kg D.W. 8.4
524 ALUMINUM ICP Dry wt. 6500 mg/kg D.W. 4.6
1236 Anthracene Dry wt. < 440 ug/kg D.W. 440
545 ANTIMONY ICP Dry wt. < 0.42 mg/kg D.W. 0.42
525 ARSENIC ICP Dry wt. 4.9 mg/kg D.W. 0.42
34 9/20/21 80818
10 9/23/21 6010C
1800 9/21/21 8270D
16 9/21/21 6010C
2.1 9/21/21 6010C
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America 8 3
Test America B 3
1255 B-BHC-Beta Dry wt.
< 6.2 ug/kg D.W. 6.2 34
1237
1238
1239
1240
1241
9/20/21 808113
Benzidine Dry wt < 22000 ug/kg D.W. 22000 53000
9/21/21 8270D
Benzo(a)Antlxacene Dry wt
< 180 ug/kg D.W. 180 1800
Benzo(a)Pyrene Dry wt
Benzo(b)Ruoranthene Dry wt.
Benzo(g,h,I)Perylene Dry wt.
< 260 ug/kg D.W. 260 1800
Test America B 3
Test America B 3
Test America B 3
9/21/21 8270D
9/21/21 8270D
Test America B 3
Test America B 3
600 ug/kg D.W. 280 1800
< 190 ug/kg D.W. 190 1800
1242 Benzo(k)Fluoranthene Dry wt. < 230 ug/kg D.W. 230 1800
528 BERYLLIUM ICP Dry wt. 0.15 mg/kg D.W. 0.029 0.21
3
3
9/21/21 8270D
Test America B 3
9/21/21 8270D
9/21/21 8270D
1256 BHC-Delta Dry wL
1243
1244
1245
1246
526
< 6.4 ug/kg D.W. 6.4
34
81s(2-Chloroetlwxy)Methane Dry wt. < 380 ug/kg D.W. 380 1800
9/21/21 6010C
9/20/21 80818
9/21/21 8270D
815(2-Chloroethyl)Ether Dry wt. < 230 ug/kg D.W.
Bls(2-Chlorolsopropyl)Ether Dry wt. < 360 ug/kg D,W.
Bis(2-Ethylhexyl)Phthalate Dry wt. 6300 ug/kg D.W.
230 1800
9/21/21 8270D
Test America B 3
Test America B 3
360 1800
610 1800
BORON ICP Dry wt. 21 mg/kg D.W. 0.2
2.1
1248 Butyl Benzyl Phthalate Dry wt. < 290 ug/kg D.W. 290 1800
530 CADMIUM ICP Dry wt
529 CALCIUM ICP Dry wt.
SYShpI5Genafc31/11/14 If
0.74 mg/kg D.W. 0.031 0.21
24000 mg/kg D.W. 3.5
52
AX.
9/21/21 8270D
9/21/21 8270D
9/21/21 6010C
9/21/21 8270D
9/21/21 6010C
9/21/21 6010C
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
Test America 8 3
Test America B 3
Peg. 1 of
Printed: 11/2421 14:22

NMSD
WOO f0! a (S1ILIMIT
Milorganite Priority Pollutant: Fall 2021
September 5 to 11, 2021
1305 Chlordane Dry wt. < 76 ug/kg D.W. 76 340 9/20/21 8081B Test America B 3
532 CHROMIUM ICP Dry wt. 260 mg/kg D.W, 0.21 0.52 9/21/21 6010C Test America B 3
1251 Chrysene Dry wt. < 400 ug/kg D.W. 400 1800 9/21/21 8270D Test America B 3
531 COBALT ICP Dry wt. 4.1 mg/kg D.W. 0.052 0.52 9/21/21 6010C Test America B 3
533 COPPER ICP Dry wt. 240 mg/kg D.W. 0.22 1 9/21/21 6010C Test America B 3
263 Cyanide - Total (solids) < 2.3 mg/kg D.W. 2.3 4.7 9/16/21 9012E Test America B 3
1325 Dibenzo(a,h)Anthracene Dry wt. < 320 ug/kg D.W. 320 1800 9/21/21 8270D Test America B 3
1306 Dleldrin Dry wt. < 8.2 ug/kg D.W. 8.2 34 9/20/21 80818 Test America B 3
1314 Diethyl Phthalate Dry wt. < 230 ug/kg D.W. 230 1800 9/21/21 8270D Test America B 3
1328 - Dimethyl Phthalate Dry M. < 210 ug/kg D.W. 210 1800 9/21/21 8270D Test America B 3
1320 DI-n-Butylphthalate Dry wt. < 300 ug/kg D.W. 300 1800 9/21/21 8270D Test America B 3
1323 Di-n-octyl phthalate Dry wt. < 210 ug/kg D.W. 210 1800 9/21/21 8270D Test America B 3
1261 Endosulfan alpha Dry wt. < 6.6 ug/kg D.W. 6.6 34 9/20/21 80818 Test America B 3
1262 Endosulfan beta Dry wt. < 6.2 ug/kg D.W. 6.2 34 9/20/21 80818 Test America B 3
1263 Endosulfan Sulfate Dry wt. 23 ug/kg D.W. 6.4 34 ) 9/20/21 80818 Test America B 3
1265 Endrin Aldehyde Dry wt. < 8.7 ug/kg D.W. 8.7 34 9/20/21 80818 Test America B 3
1264 Endrin Dry M. < 6.8 ug/kg D.W. 6.8 34 9/20/21 80818 Test America B 3
1321 Auoranthene Dry wt. 640 ug/kg D.W. 190 1800 3 9/21/21 8270D Test America B 3
1316 Fluorene Dry wt. < 210 ug/kg D.W. 210 1800 9/21/21 8270D Test America B 3
1266 Heptachlor Dry M. < 7.4 ug/kg D.W. 7.4 34 9/20/21 8081E Test America B 3
1267 Heptachlorepoxide Dry wt. < 8.8 ug/kg D.W. 8.8 34 9/20/21 8081E - Test America B 3
1330 Hexachlorobenzene Dry M. < 240 ug/kg D.W. 240 1800 9/21/21 8270D Test America B 3
1327 Hexachlorobutadlene Dry wt. < 260 ug/kg D.W. 260 1800 - 9/21/21 8270D Test America B 3
1308 Hexadilorocydopentadiene Dry wt. < 240 ug/kg D.W. 240 1800 9/21/21 8270D Test America B 3
1329 Hexadrloroeihane Dry wt. < 230 ug/kg D.W. 230 1800 9/21/21 8270D Test America B 3
1326 Indeno(1,2,3-cd)Pyrene Dry Wt. < 220 ug/kg D.W. 220 1800 9/21/21 8270D Test America B 3
534 IRON ICP Dry Wt. 42000 mg/kg D.W. 3.7 10 9/21/21 6010C Test America B 3
1311 Isaphorone Dry wt. < 380 ug/kg D.W. 380 1800 9/21/21 8270D Test America B 3
544 LEAD ICP Dry wt. 51 mg/kg D.W. 0.25 1 9/21/21 6010C Test America B 3
538 MAGNESIUM ICP Dry M. 8600 mg/kg D.W. 0.97 21 9/21/21 6010C Test America B 3
539 MANGANESE ICP Drywt. 1200 mg/kg D.W. 0.033 0.21 9/21/21 6010C Test America B 3
428 MERCURY by M. 7471 (sludge) 0.28 mg/kg D.W. 0.0048 0.021 9/20/21 7471B Test America B 3
540 MOLYBDENUM ICP Dry wt. 11 mg/kg D.W. 0.14 1 9/21/21 6010C Test America B 3
1312 Naphthalene Dry wt. < 230 ug/kg D.W. 230 1800 9/21/21 8270D Test America B 3
542 NICKEL ICP Dry wt. 29 mg/kg D.W. 0.24 5.2 9/21/21 6010C Test America B 3
1310 Nitrobenzene Dry wt. < 200 ug/kg D.W. 200 1800 9/21/21 8270D Test America B 3
1307 N-NltrosodimethyIamine Dry wt. < 760 ug/kg D.W. 760 3500 9/21/21 8270D Test America B 3
1309 N-Nltrosodi-n-propylamine Dry wt. < 300 ug/kg D.W. 300 1800 9/21/21 8270D Test America B 3
1313 N-Nitrosodiphenylamine Dry M. < 1400 ug/kg D.W. 1400 1800 9/21/21 8270D Test America B 3
678 PCB-1016 < 0.041 mg/kg D.W. 0.041 0.21 9/16/21 8082A Test America B 3
674 PCB-1221 < 0.041 mg/kg D.W. 0.041 0.21 9/16/21 8082A Test America B 3
675 PCB-1232 < 0.041 mg/kg D.W. 0.041 0.21 9/16/21 8082A Test America B 3
672 PCB-1242 < 0.041 mg/kg D.W. 0.041 0.21 9/16/21 8082A Test America B 3
676 PCB-1248 < 0.041 mg/kg D.W. 0.041 0.21 9/16/21 8082A Test America B 3
673 PC3-1254 < 0.098 mg/kg D.W. 0.098 0.21 - 9/16/21 8082A Test America B 3
677 PCB-1260 < 0.098 mg/kg D.W. 0.098 0.21 9/16/21 8082A Test America B 3
1224 p-fhloro-m-Cresol Dry wt. < 440 ug/kg D.W. 440 1800 9/21/21 8270D Test America B 3
1232 Pentachlorophenol Dry M. < 1800 ug/kg D.W. 1800 3500 9/21/21 8270D Test America B 3
1319 Phenanthrene Dry wt. < 260 ug/kg D.W. 260 1800 9/21/21 8270D Test America B 3
1233 Phenol Dry wt. < 270 ug/kg D.W. 270 1800 9/21/21 8270D Test America B 3
Page 2of3
SYS/p75Generic3 4/11/14 (( Primed: 11/24/21 14.22

MNSD
Matti tHi1 titLI
543 PHOSPHORUS 1CP Dry wt
536 POTASSIUM ICP Dry wt.
23000 mg/kg D.W. 150 360
3200 mg/kg D.W. 21 31
1322 Pyrene Dry wt
Milorganite Priority Pollutant: Fall 2021
September 5 to 11, 2021
9/21/21 SM 4500 P E
9/21/21 6010C
530 ug/kg D.W. 210 1800
546 SELENIUM ICP Dry wt. 2.4 mg/kg D.W. 0.42 4.2
523 SILVER ICP Dry wt. 2.3 mg/kg D.W. 0.21 0.63
3
9/21/21 8270D
9/21/21 6010C
9/21/21 6010C
541 SODIUM ICP Dry wt
1500 mg/kg D.W. 14 150
1187 Solids for dry weight determination (T 95 %
1187 Solids for dry weight determination (r 94 %
550 THALLIUM ICP Dry wt.
Ink friar
9/21/21
9/23/21
9/21/21 Moisture
< 0.31 mg/kg D.W. 0.31 6.3
697 Total PCB Arodors < 0.098 mg/kg D.W. 0.098 0.21
1268 Toxaphene Dry wt. < 200 ug/kg D.W. 200 340
1257 Y BHC-Gamma(Undane) Dry wt.
552 ZINC ICP Dry wt.
6010C
Moisture
Test America B 3
Test America B 3
Test America B 3
Test Amen B 3
Test America B 3
Test America B 3
Test America B 3
Test America B 3
9/21/21 6010C Test America B 3
9/16/21 8082A Test America B 3
9/20/21 80818
< 6.3 ug/kg D.W. 6.3 34
510 mg/kg D.W. 0.67 2.1
** The MDL for this test is the lowest level of precision shown, example: 4.1 would be "0.1".
.r* The LOQ for this test is the lowest level of precision shown, example: 4.1 would be "0.1".
N.A. The MDL/LOQ is Not Available or Not Applicable for this test.
9/20/21 8081E
9/21/21 6010C
Column S: Test Status. Not Started=B, Intermedlate=7, Final=3, Analyst Approved=12, Not Reportable=15.
Test America B 3
Test America B 3
Test America B 3
107
Ping Descriptions
AO Other — Flag requires additional explanation.
AX Qualified data - see contract laboratory report.
B3 Target analyte detected in method blank > 10% of sample
concentration.
B7 LCS recovery was above control limits.
B8 LCS recover was below control limits.
B9 Low Level CCV recovery was outside of method acceptance limits.
Di Duplicate precision control limit was exceeded.
D2 Matrix spike pvcislon control limit was exceeded.
D3 Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory practic s.
D4 Sample matrix interferences did not allow completing the analysis.
D5 The reported result is an estimate because the concentration of
HEM In this sample exceeded the maximum allowed in the method
for the sample volume collected.
Hi Sample was received past holding time.
H3 Analysis performed levered holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
H5 Analysis performed bepel holding time
sys415Generic3 4/11/14 V
IS Insufficient sample volume for analysts.
3 Estimated concentration above the adjusted method detection limit
and below the adjusted reforteri limit.
LA Not arrplsed - laboratory accident
MIL Too numerous to count.
M2 Sample Incubation period outside method requirement
M3 Sprucing colonies - unable to determine result
M4 Results are an approx.matton due to spreading colonies.
M5 Incubator/water bath temperature was outside method
requirements.
M7 Microbiology sample received without adequate neadspecs.
M9 Target organism detected in associated method blank.
NR Not usable data (Water Quasi ty oft).
NU Not usable Data.
P2 Sample received with improper or Inadequate chemical preservation.
Q2 Matrix spike recover" for this sample was above control limits.
Q3 Matrix splice recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
remeements.
S5 Reading was not confirmed by a constant weight measurement
SG Dried solid residue yield outside of method specifications (<2.5mg
or >20000
SD Supplemental details policed (Water Quake crIt
T3 The BOD dilution water D.O. dtpleitIon was > 0.2 mg/L.
T4 GGA BOD was below method acceptance criteria.
T5 GGA BOD was above method acceptance criteria.
115 Sample sup#rslttrrated with dissolved oxygen for BOD analysis.
T7 The BOD dilution water D.O. increase was > 0.2 mot.
TS Sample matrix did not allow alusting sample pH for BOD.
T9 Sample is outside of the prescribed method temperature range.
Page 3of3
Prtnted: 1124/21 14:22

PIMSD
WEI1Dt A 41kw MOW
964
9/13/21
Sample Date
SU
Site Code
Customer ID
Milorganite Priority Pollutant: Fall 2021
September 13, 2021
Milo. Priority Pollutant Sample
21019981
LIMS Number
OpSID Test Name Reported Value ML:L I c Q FIIOS Analysis Date Method Lou • S
1341 1,1,1-Trithloroethane Dry wt.
< 23 ug/kg D,W.
23 B2 9/22/21 8260C
1350 1,1,2,2-Tetra hloroethane Dry wt. < 13 ug/kg D.W. 13 82 9/22/21 8260C
9/22/21 8260C
9/22/21 8260C Test America B 3
9/22./21 8260C Test America B 3
9/22/21 8260C Test America B 3
9/22/21 8260C Test America B 3
1222 1,2-Dichloroprapane Dry wt. < 13 ug/kg D.W. 13 82 9/22/21 8260C Test America B 3
1356 1,3-DIchlorobenzene Dry Wt. < 22 ug/kg D.W. 22 82 9/22/21 8260C Test America B 3
1357 1,4-DlWorobenzene Dry Wt. < 12 ug/kg D.W. 12 82 9/22/21 8260C Test America B 3
1348 1,1,2-Trichloroethane Dry wt. < 17 ug/kg D.W. 17 82
1338 1,1-Dichloroethane Dry wt. < 25 ug/kg D.W. 25 82
1336 1,1-Dichloroethylene Dry wt. < 29 ug/kg D.W. 29 82
1355 1,2-Dichlorobenzene Dry Wt. < 21 ug/kg D.W. 21 82
1340 1,2-DiWoroethane Dry wt. < 34 ug/kg D.W. 34 82
Test America B
Test America B 3
3
Test America B 3
1337 2-Chloroethylvinyl Ether Dry wt. < 26 ug/kg D.W. 26 410 9/22/21 8260C Test America B 3
1334 Acrolein Dry wt. < 170 ug/kg D.W. 170 410 9/22/21 8260C Test America B 3
1335 Acrylonitrile Dry wt. < 210 ug/kg D.W. 210 410 9/22/21 82660C Test America B 3
1346 Benzene Dry wt. < 16 ug/kg D.W. 16 82 9/22/21 8260C Test America B 3
1343 Bramodichloromethane Dry wt. < 16 ug/kg D.W. 16 82 9/22/21 8260C Test America B 3
1219 Bromoform Dry wt. < 41 ug/kg D.W. 41 82 9/22/21 8260C Test America B 3
1342 Carbon Tetrachloride Dry wt. < 21 ug/kg D.W. 21 82 9/22/21 8260C Test America B 3
1352 Chlorobenzene Dry wt. < 11 ug/kg D.W. 11 82 9/22/21 8260C Test America B 3
1220 Chloroethane Dry vet. < 17 ug/kg D.W. 17 82 9/22/21 8260C Test America 8 I
1339 Chloroform Dry wt. < 57 ug/kg D.W. 57 82 9/22/21 8260C Test America B J
1344 cis-1,3-Dichlaropropene Dry wt. < 20 ug/kg D.W. 20 82 9/22/21 8260C Test America 8 3
1347 Dibromochloromethane Dry wt. < 40 ug/kg D.W. 40 82 9/22/21 8260C Test America B 3
1353 Ethylbenzene Dry wt. < 24 ug/kg D.W. 24 82 9/22/21 8260C Test America B 3
1331 Methyl Bromide Dry wt. < 18 ug/kg D.W. 18 82 9/22/21 8260C Test America B 3
1354 Methyl Chloride dry wt. < 20 ug/kg D.W. 20 82 9/22/21 8260C Test America B 3
1333 Methylene Chloride Dry wt. < 16 ug/kg D.W. 16 82 9/22/21 8260C Test America B 3
1187 Solids for dry weight determination (T 95 % ••• 9/15/21 Moisture Test America B 3
1349 Tetrachloroethylene Dry wt. < 11 ug/kg D.W. 11 82 9/22/21 8260C Test America B 3
1351 Toluene Dry wt. 120 ug/kg D.W. 22 82 9/22/21 8260C Test America B 3
1221 Trans-1,2-Dichloroethylene Dry wt. < 19 ug/kg D,W. 19 82 9/22/21 8260C Test America B 3
1223 Trans-1,3-Dichloropropene Dry wt. < 8.1 ug/kg D,W. 8.1 82 9/22/21 8260C Test America B 3
1345 Trichloroethylene Dry wt. < 23 ug/kg D.W. 23 82 9/22/21 8260C Test America B 3
1332 Vinyl Chloride Dry wt < 28 ug/kg D.W. 28 82 9/22/21 8260C Test America B 3
Page 1o2
SYS rpt50erredc3 4.41H4 q Printed: 1 rt24/21 14.28

IIP1SD
Win II/ CUM PrY:rrlV;Yt
Milorganite Priority Pollutant: Fall 2021
September 13, 2021
** The MDL for this test is the lowest level of predsion shown, example: 4.1 would be "0.1".
*** The LOQ for this test Is the lowest level of precision shown, example: 4.1 would be "0.1".
N.A. The MDL/LOQ is Not Available or Not Applicable for this test.
Column S: Test Status. Not Started=8, Intermediate=7, Fina1=3, Analyst Approved=12, Not Reportable=15.
33
l
AO Other -- Flay requires additional explanation.
AX Qualified data - see contract laboranry report
B3 Target analyte detected in method blank > 10% of sample
concentration.
B7
B8
B9
DI
02
D3
D4
D5
LCS recovery was above control limits.
LCS r covey was below control limits.
Low Level CV recovery was outside of method acceptance limits.
Duplicate precision control limit was exceeded.
Matrix spike precision control limit was exceeded.
Sample is heterogeneous. Sample homogeneity could not be readily
achieved using routine laboratory prates.
Sample matrix interferences did not allow cnrnpldgnp the analysis.
The reported result is an estimate because the concentration of
HEM in this sample exceeded the maximum allowed in the method
for the sample volume collected.
Hi Sample was received past holding time.
H3 Analysis performed beond holding time.
H4 Initial analysis within holding time. Reanalysis for the required
dilution was past holding time.
H5 AnaNsls performed beyond holding time.
SYS rpt5G.nede3 4✓11114 q
IS Insufficient sample volume for analysis.
3 Estimated concentration above the adjusted method detection limit
and below the adjusted reporting limit.
LA Not analyzed - laboratory accident.
MI Too numerous to count.
M2 Sample incubation period outside method requirement.
M3 Spreading colonies - unable to determine result.
M4 Results are an approximation due to %reading colonies.
M5 Incubator/water bath temperature was outside method
relpirements.
M7 Microbiology sample received without adr:Fuate heidspce.
M9 Target organism detected in associated method blank.
N R Not usable data (Water Quellty only).
N U Not usable Data.
P2 Sample received with improper or inadequate chemical preservation.
Q2 Matrix 'Ike moor/ for this sample was above control limits.
Q3 Matrix spike recovery for this sample was below control limits.
RT Sample temperature upon receipt exceeded regulatory or project
requirements.
S5 Reading was not confirmed by a constant weight measurement
SS Dried solid residue yield outside of method specifications (<2.5mg
or >200mg).
SD Supplemental details provided (Water Quality only).
T3 The BOD dilution water D.O. depletion was > 0.2 q *L.
T4 GGA BOD was below method acceptance aiteria.
T5
T6
T7 The BOD dilution water D.O. increase was > 0.2 mg/L.
Ta Sample matrix did not allow ad s tug sample pH for BOD.
T9 Sample Is outside of the prescribed method temperature range.
GGA BOD was above method aoG9pmna criteria.
Sample supersaturated with dissoWed dxrygen for BOD analysis.
Pepe 2of2
Printed: 11/24/21 14:2e

Milorganite Dioxin Toxic Equivalent Concentrations 2021
Measured Concentration (pg/g or ppt)
Factor
CAS
Congener
1/9/2021
2/13/2021
3/13/2021
4/10/2021
5/8/2021
6/12/2021
7/10/2021
8/7/2021
9/11/2021
10/9/2021
11/13/2021
12/11/2021
EPA
Maine
1746-01-6
2,3,7,8- Tetrachlorodibenzo-p-dioxin
0
0
6.8
0
0
0
0
0
0
0
0
0
1.0
1.0
40321-76-4
1,2,3,7,8- Pentachlorodibenzo-p-dioxin
0
0
0
0
0
0
0
0
0
0
0
0
1.0
0.5
39227-28-6
1,2,3,4,7,8- Hexachlorodibenzo-p-dioxin
0
0
0
0
0
0
0
0
0
0
0
0
0.1
0.1
57663-85-7
1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin
0
0
0.0
0
0
0
10
7.4
13
6.3
0
0
0.1
0.1
19408-74-3
1,2,3,7,8,9- Hexachlorodibenzo-p-dioxin
0
6.2
0.0
0.0
0.0
0
7.3
0.0
8.5
0
0
0
0.1
0.1
35822-46-9
1,2,3,4,6,7,8- Heptachlorodibenzo-p-dioxin
75
62
59
58
85
84
180
210
240
140
120
79
0.01
0.01
3268-87-9
1,2,3,4,6,7,8,9- Octachlorodibenzo-p-dioxin
660
550
540
560
780
840
1600
1600
2400
1400
1300
880
0.0001
0.001
51207-31-9
2,3,7,8- Tetrachlorodibenzofuran
0.0
3.8
4.4
1.7
1.1
1.4
1.6
1.2
1.5
2.0
2.0
2.0
0.1
0.1
57117-41-6
1,2,3,7,8- Pentachlorodibenzofuran
0
0
0
0
0
0
0
0
0
0
0
0
0.05
0.05
57117-31-4
2,3,4,7,8- Pentachlorodibenzofuran
0
7.0
9
0
0
0
0
0
0
5.5
0
0
0.5
0.5
70648-26-9
1,2,3,4,7,8- Hexachlorodibenzofuran
0
0
0
0
0
0
0
0
0
0
0
0
0.1
0.1
57117-44-9
1,2,3,6,7,8- Hexachlorodibenzofuran
0
0
0
0
0
0
0
0
7
0
0
0
0.1
0.1
72918-21-9
1,2,3,7,8,9- Hexachlorodibenzofuran
0
0
0
0
0
0
0
0
0
0
0
0
0.1
0.1
60851-34-5
2,3,4,6,7,8- Hexachlorodibenzofuran
0
0
0
0
0
0
0
0
6.8
0
0
0
0.1
0.1
67562-39-4
1,2,3,4,6,7,8- Heptachlorodibenzofuran
31
20
18
22
34
31
78
47
110
48
37
26
0.01
0.01
55673-89-7
1,2,3,4,7,8,9- Heptachlorodibenzofuran
0
0
0
0
0
0
0
0
6.6
0
0
0
0.01
0.01
39001-02-0
1,2,3,4,6,7,8,9- Octachlorodibenzofuran
42
27
34
39
51
43
140
75
200
86
97
57
0.0001
0.001
32598-13-3
3,3',4,4'- Tetrachlorobiphenyl
232
141
192
184
182
163
338
993
673
414
450
365
0.0001
0.0005
70362-50-4
3,4,4',5- Tetrachlorobiphenyl
0
0
0
0
0
0
0
52
0
0
0
0
0.0001
57465-28-8
3,3',4,4',5- Pentachlorobiphenyl
0
0
0
0
0
0
0
0
0
0
0
0
0.1
0.1
32598-14-4
2,3,3',4,4'- Pentachlorobiphenyl
1230
940
1090
1020
1130
945
1560
1920
2280
1670
1970
1560
0.0001
0.0001
31508-00-6
2,3',4,4',5- Pentachlorobiphenyl
3030
1870
2510
2290
2350
2280
3850
4890
4940
3540
4460
3500
0.0001
0.0001
65510-44-3
2',3,4,4',5- Pentachlorobiphenyl
0
225
0
59
0
0
71
169
103
0
78
79
0.0001
0.0001
74472-37-0
2,3,4,4',5- Pentachlorobiphenyl
0
0
65.1
60.7
51.2
60.1
89
109
131
0
114
97
0.0005
0.0005
32774-16-6
3,3',4,4',5,5'- Hexachlorobiphenyl
0
0
0
0
0
0
0
0
0
0
0
0
0.01
0.01
38380-08-4
2,3,3',4,4',5-Hexachlorobiphenyl
571
415
423
375
433
440
679
954
964
805
766
613
0.0005
0.0005
69782-90-7
2,3,3',4,4',5'- Hexachlorobiphenyl
0
0
0
0
0
0
0
0
0
0
0
0
0.0005
0.0005
52663-72-6
2,3',4,4',5,5'-Hexachlorobiphenyl
191
124
152
120
146
154
280
298
328
250
244
201
0.00001
0.00001
39635-31-9
2,3,3',4,4',5,5'- Heptachlorobiphenyl
69
59
53
55
54.7
69.2
181
132
147
104
87
83
0.0001
0.0001
35065-30-6
2,2',3,3',4,4',5-Heptachlorobiphenyl
1430
1100
878
853
634
1150
1780
1990
2270
1970
1760
1460
0.0001
35065-29-3
2,2',3,4,4',5,5'-Heptachlorobiphenyl
1430
2650
2350
2230
1580
2640
4190
4800
5080
3940
4220
3160
0.0001
Total EPA Toxic Equivalent (TEQ)
1.9
5.9
13.0
1.6
2.0
2.0
5.6
4.9
8.9
6.6
3.1
2.3
Total Maine Toxic Equivalent (TEQ)
2.9
6.9
14.0
2.5
3.0
3.2
7.9
7.5
12.2
8.7
5.1
3.7
"0" means that the concentration was less than the level of detection